sitewide environmental monitoring semiannual progress ... · the cms report concluded that...
TRANSCRIPT
Pinellas County Florida Site Environmental Restoration Project Sitewide Environmental Monitoring Semiannual Progress Report for the Young - Rainey STAR Center December 2012 Through May 2013 June 2013
LMSPINN01796
US Department of Energy Pinellas Sitewide Semiannual Progress Report for December 2012mdashMay 2013 June 2013 Doc No N01796 Page i
Contents Abbreviations iii 10 Introduction 1
11 Building 100 Area 2 12 Northeast Site 5 13 WWNA 7 14 Site Update 9 15 Waste Minimization 9
20 Water-Level Elevations 9 21 Groundwater Flow 9
30 Groundwater Sampling 10 31 Work Performed 10 32 Quality AssuranceQuality Control 11
40 Plume Stability Monitoring 12 50 Upcoming Tasks 13 60 References 13
Figures Figure 1 Young - Rainey STAR Center Location 16 Figure 2 Location of STAR Center Solid-Waste Management Units (SWMUs) 17 Figure 3 Building 100 Area Shallow Surficial Aquifer Flow March 2013 18 Figure 4 Building 100 Area Deep Surficial Aquifer Flow March 2013 19 Figure 5 Building 100 Area TCOPCs Concentrations March 2013 20 Figure 6 Building 100 Area South TCOPCs Concentrations March 2013 21 Figure 7 Building 100 Area TCE Concentrations March 2013 22 Figure 8 Building 100 Area cDCE Concentrations March 2013 23 Figure 9 Building 100 Area South cDCE Concentrations March 2013 24 Figure 10 Building 100 Area VC Concentrations March 2013 25 Figure 11 Building 100 Area South VC Concentrations March 2013 26 Figure 12 Building 100 Area 14-dioxane Concentrations March 2013 27 Figure 13 Building 100 Area South 14-dioxane Concentrations March 2013 28 Figure 14 Building 100 Area Plume Stability Monitoring Cross-Sections 29 Figure 15 Cross-Section E1-E2 30 Figure 16 Cross-Section E3-E4 31 Figure 17 Cross-Section E5-E6 32 Figure 18 Cross-Section S1-E2 33 Figure 19 Cross-Section S2-S3 34 Figure 20 Cross-Section S4-S5 35
Tables Table 1 Groundwater-Level Data at the STAR Center March 2013 36 Table 2 Surface Water Elevations March 2013 41
US Department of Energy Pinellas Sitewide Semiannual Progress Report for December 2012mdashMay 2013 June 2013 Doc No N01796 Page ii
Table 3 Field Measurements of Samples Collected at the STAR Center March 2013 42 Table 4 Relative Percent Difference (RPD) for Duplicate Samples March 2013 45 Table 5 COPC Concentrations at the Building 100 Area 46 Table 6 Sum of COPCs for Each Plume Stability Monitoring Cross-Section 49 Table 7 Area Under the Curve Values For Each Plume Stability Monitoring Cross-section 50
Plates Plate 1 Sitewide Shallow Surficial Aquifer Contours Pinellas Florida March 2013 Plate 2 Sitewide Deep Surficial Aquifer Contours Pinellas Florida March 2013
Appendix Appendix A Laboratory Reports March 2013 Semiannual Monitoring
US Department of Energy Pinellas Sitewide Semiannual Progress Report for December 2012mdashMay 2013 June 2013 Doc No N01796 Page iii
Abbreviations cDCE cis-12-dichloroethene
CMIP Corrective Measures Implementation Plan
CMS Corrective Measures Study
CMT continuous multichannel tubing
COPC contaminant of potential concern
CTL cleanup target level
11-DCE 11-dichloroethene
DOE US Department of Energy
EPA US Environmental Protection Agency
FAC Florida Administrative Code
FDEP Florida Department of Environmental Protection
ft feet (foot)
HSWA Hazardous and Solid Waste Amendments
IC Institutional Control
IWNF industrial wastewater neutralization facility
LDA large-diameter auger
LM Office of Legacy Management
MCL maximum contaminant level
μgL micrograms per liter
NAPL nonaqueous phase liquid
POTW Publicly Owned Treatment Works
QAQC quality assurancequality control
RBCA Risk-Based Corrective Action
RCRA Resource Conservation and Recovery Act
RFA RCRA Facility Assessment
RPD relative percent difference
SEEPro Site Environmental Evaluation for Projects
STAR Center Young - Rainey Science Technology and Research Center
SWMU solid-waste management unit
TCE trichloroethene
US Department of Energy Pinellas Sitewide Semiannual Progress Report for December 2012mdashMay 2013 June 2013 Doc No N01796 Page iv
TCOPCs total contaminants of potential concern
tDCE trans-12-dichloroethene
VC vinyl chloride
WWNA Wastewater Neutralization AreaBuilding 200 Area
US Department of Energy Pinellas Sitewide Semiannual Progress Report for December 2012mdashMay 2013 June 2013 Doc No N01796 Page 1
10 Introduction The Young - Rainey Science Technology and Research Center (STAR Center) at the Pinellas County Florida Site is a former US Department of Energy (DOE) facility constructed in the mid-1950s The 99-acre STAR Center is located in Largo Florida and lies in the northeast quarter of Section 13 Township 30 South Range 15 East (Figure 1) While it was owned by DOE the facility primarily manufactured neutron generators for nuclear weapons Other products manufactured at the STAR Center have included radioisotope-powered thermoelectric generators thermal batteries specialty capacitors crystal resonators neutron detectors lightning-arrestor connectors and vacuum-switch tubes In 1987 the US Environmental Protection Agency (EPA) performed a Resource Conservation and Recovery Act (RCRA) Facility Assessment (RFA) (EPA 1988) at the site to gather information on potential releases of hazardous materials In February of 1990 EPA issued a Hazardous and Solid Waste Amendments (HSWA) permit to DOE enabling DOE to investigate and perform remediation activities in those areas designated as solid-waste management units (SWMUs) contaminated by hazardous materials resulting from DOE operations On March 17 1995 DOE sold the facility to the Pinellas County Industrial Council The sales contract included clauses to ensure continued compliance with federal state and local regulations while DOE remediates the site On July 1 1999 the Pinellas County Industrial Council was disestablished and ownership of the STAR Center changed to the Pinellas County Industrial Development Authority In November 2000 the State of Florida received HSWA authorization from EPA The Florida Department of Environmental Protection (FDEP) issued a new HSWA permit to DOE in January 2002 The permit was reissued on August 21 2007 and was modified under the provisions of Section 403722 Florida Statutes and Chapters 62-4 62-160 62-730 62-777 and 62-780 Florida Administrative Code (FAC) to incorporate the Global Risk-Based Corrective Action (RBCA) regulations The permit was revised and reissued again on January 9 2012 The administration of DOE activities at the facility is the responsibility of the DOE Office of Legacy Management (LM) in Grand Junction Colorado SM Stoller Corporation a prime contractor to LM provides technical support to DOE for remediation and closure of all active SWMUs onsite The EPA RFA Report and the HSWA permit identified 15 sites at the former DOE facility that might have environmental contamination as a result of past activities Upon completion of the RCRA Facility Investigation (DOE 1991a) 11 of the 15 SWMUs were recommended by DOE and approved by EPA Region 4 and FDEP for no further action (DOE 1994) A twelfth site the Former Pistol Range Site was remediated in 1993 it was recommended by DOE and approved by EPA Region 4 and FDEP for no further action Two additional SWMUs the West Fenceline Site and the Wastewater Neutralization Area Building 200 Area (WWNA) were identified after the HSWA permit was issued bringing the total to 17 SWMUs that have been identified and investigated at the STAR Center The remediation of the West Fenceline Site was completed in 1997 and DOE recommendedand EPA Region 4 and FDEP approvedno further action for a total of 13 SWMUs remediated A Corrective Measures Study (CMS)Corrective Measures Implementation Plan (CMIP) was
US Department of Energy Pinellas Sitewide Semiannual Progress Report for December 2012mdashMay 2013 June 2013 Doc No N01796 Page 2
prepared and submitted in 1997 to EPA Region 4 and FDEP to address the contamination at the WWNA Therefore four active SWMUs currently exist at the STAR Center These four SWMUs are the Old Drum Storage Site (PIN06) the Industrial Drain LeaksBuilding 100 Area (PIN12) the Northeast Site (PIN15) and the WWNA (PIN18) Two SWMUs PIN06 and PIN12 are collectively known as the Building 100 Area Figure 2 depicts the location of the four SWMUs DOE plans to proceed with closure of the WWNA under RBCA Risk Management Option II and to apply the default poor quality arsenic cleanup target level (CTL) of 100 micrograms per liter (μgL) to onsite groundwater Closure monitoring was completed in October 2006 A No Further Action with Controls proposal for the site was approved by FDEP in May 2007 Acceptance of this closure proposal by FDEP indicates that both soil and groundwater cleanup are complete Closure of the site can be finalized once Institutional Controls (ICs) are implemented DOE is working with the landowner (Pinellas County Industrial Development Authority) to establish ICs at the STAR Center Once ICs are in place there will be no potential for current or future exposure to contaminated groundwater ICs will need to be established and approved by FDEP before a formal No Further Action determination can be made Currently DOE is working with the STAR Center to develop a covenant that incorporates the ICs that will then become part of DOErsquos Long-Term Surveillance and Maintenance Plan at this site Additional background information relative to each SWMU is briefly described below This document serves as the semiannual progress report for each of these four SWMUs The results of recent monitoring activities and a summary of ongoing and projected work are provided in this report 11 Building 100 Area The Building 100 Area is made up of two SWMUs the Industrial Drain LeaksBuilding 100 (PIN12) and the Old Drum Storage Site (PIN06) The Old Drum Storage Site lies beneath and adjacent to the northwest corner of the main building that covers approximately 11 acres located near the southeast corner of the STAR Center (Figure 2) Building 100 is the most notable feature of the STAR Center having housed the majority of the laboratory and production facilities during DOE ownership of the facility One source of contamination at the Building 100 Area is leaks from a liquid waste drain system composed of individual drainage systems previously used for health physics chemical sanitary and storm-water systems The drain systems were flushed grouted and abandoned by 1997 and some of the chemical drain systems were replaced by an aboveground system (DOE 1997a) The Old Drum Storage Site is the former location of a concrete storage pad This area was equipped with a drain and containment system and was once used to store hazardous waste The waste stored at this location included methylene chloride ignitable liquids arsenic and calcium chromate solids Empty drums containing residual waste solvents also were stored in this area A RCRA Facility Investigation was conducted in 1991 at the Pinellas Plant to fulfill the requirements of the HSWA permit and a RCRA Facility Investigation report was produced in 1991 A subsequent report addendum was completed in March 1992 Based on the findings in
US Department of Energy Pinellas Sitewide Semiannual Progress Report for December 2012mdashMay 2013 June 2013 Doc No N01796 Page 3
these two documents in accordance with the HWSA permit EPA notified DOE of the requirement for a CMS for the Old Drum Storage Site and the Industrial Drain Leaks Building 100 SWMUs The CMS report for the Industrial Drain LeaksBuilding 100 and the Old Drum Storage Site proposed remediation of these two SWMUs together (collectively referred to as the Building 100 Area) The report was submitted to EPA and was subsequently approved on June 9 1994 FDEP approved the CMS report on January 18 1995 The CMS report concluded that pump-and-treat with the existing air-stripping system was the preferred corrective measure for the Building 100 Area This conclusion was based on shallow monitoring-well data that suggested contamination was confined to shallow groundwater at the northwest corner of the building However that characterization was later found to be incomplete Two recovery wells were installed at the northwest corner of the building in 1995 The Building 100 Area Corrective Measures Implementation Plan (DOE 1996a) describes the installation of the wells and the operations and monitoring plan These recovery wells PIN12-RW01 and -RW02 extracted groundwater and pumped the water through secondary containment piping to the Northeast Site treatment system for pretreatment air stripping and discharge to the STAR Center industrial wastewater neutralization facility (IWNF) prior to transfer to the Publicly Owned Treatment Works (POTW) The Northeast Site treatment system was decommissioned in April 2004 so a smaller air-stripper treatment system was installed at the Northeast Site to treat the groundwater recovered via the two Building 100 Area recovery wells Subsequent to recovery well installation additional investigations were conducted by installing monitoring wells at multiple depths both outside the building and through the floor of the building In 1996 these investigations were summarized in the Building 100 Area Data Report (DOE 1996b) and the Building 100 Area Subsurface Investigations Phases I II and III (DOE 1996c) Results of these investigations indicated that (1) significant contaminant concentrations were present at intermediate and deep depths under the building and (2) low levels of contamination were present at the south and east sides of the building The Building 100 Area Data Report recommended that DOE continue operating the two recovery wells that were installed in accordance with the CMSCMIP conduct additional characterization under the building and east of the building conduct additional contaminant transport modeling and evaluate the potential for occurrence of dense nonaqueous phase liquids (NAPLs) These recommendations were addressed in the Building 100 Area Corrective Measures Implementation Plan Addendum (DOE 1998) A pilot test study was conducted in 2003ndash2004 to determine the effectiveness of enhanced biodegradation for this site (DOE 2005) The pilot test results were positive but the test did not result in significant elimination of vinyl chloride (VC) in low-concentration areas Therefore enhanced biodegradation technologies were not considered for use at the Building 100 Area at that time The Building 100 Area Corrective Measures Study Report Addendum (DOE 2006) was finalized in July 2006 The document concluded that DOErsquos original remediation objective of meeting maximum contaminant levels (MCLs) throughout the contaminant plume does not appear to be
US Department of Energy Pinellas Sitewide Semiannual Progress Report for December 2012mdashMay 2013 June 2013 Doc No N01796 Page 4
reasonable given current knowledge of the site At that time it appeared that containment of the contaminant plume had been achieved and it was determined that human health and the environment were protected The document proposed that ICs be placed on the site property to prevent inappropriate groundwater use and that MCLs for site-related contaminants of potential concern (COPCs) be applied as groundwater cleanup goals outside the IC boundary Because the two existing groundwater recovery wells did not contribute significantly to either contaminant plume containment or mass removal DOE also proposed shutting down these wells and the associated treatment system Operation of these recovery wells and the treatment system was terminated on August 21 2006 with the approval of FDEP An interim remedial action using a single recovery well to collect hydraulic information began in July 2009 and ended in May 2011 Located in the south plume near the southern STAR Center property boundary recovery well PIN12-RW03 had a radius of influence that likely captured the entire south plume as it exited the property Operation of this recovery well ceased in May 2011 to allow treatment of the groundwater produced during the Countyrsquos road work (discussed below) Pinellas County Utilities started a major water line replacement effort along Belcher Road in October 2010 and Pinellas County Public Works started a significant road construction project along Belcher and Bryan Dairy Roads in October 2011 In July 2011 DOE began treating groundwater produced by dewatering conducted during these projects Treatment ended in January 2012 The extracted groundwater was transported to an onsite air stripper for treatment and the treated water was discharged to the STAR Centerrsquos IWNF and subsequently discharged to the POTW Prior to the start of the water line and road projects DOE installed new monitoring wells at the property boundary along the two roads in October 2007 and in January and February 2008 to further define the contaminant plume This investigation confirmed that the plume was offsite south of Bryan Dairy Road on the county right-of-way DOE performed the required notification to FDEP regarding the offsite plume Additional plume delineation was conducted on the property at 8040 Bryan Dairy Road by the installation of three continuous multichannel tubing (CMT) wells in September 2009 (PIN12-0567 -0568 and -0569) Contaminant concentrations exceeded CTLs in well PIN12-0569 DOE reported this discovery to FDEP and to the property owner in October 2009 in accordance with FDEP notification requirements Two additional CMT wells were installed on this property in March 2010 (PIN12-0570 and -0571) To further investigate the extent of the offsite contamination to the south of the STAR Center plume delineation work was conducted at 10980 Belcher Road on August 16ndash30 2010 using direct-push technology to collect groundwater samples from temporary locations This property is located across Bryan Dairy Road immediately south of the Building 100 Area at the STAR Center The results of this investigation indicated that the contaminant plume enters the 10980 Belcher Road property on the western side and extends southeastward (in the direction of groundwater flow) to the southern property boundary DOE reported this discovery to FDEP and to the property owner in October 2010 in accordance with FDEP notification requirements The
US Department of Energy Pinellas Sitewide Semiannual Progress Report for December 2012mdashMay 2013 June 2013 Doc No N01796 Page 5
results of this investigation are reported in the Building 100 Area Off-Site Plume Delineation South of Bryan Dairy Road Data Report for Rally Stores Property (DOE 2010a) The results from that investigation suggested that the contaminant plume extended south onto property at 10950 Belcher Road Plume delineation was conducted at this property on December 6ndash16 2010 and April 4ndash6 2011 Additional delineation was conducted in the median of Belcher Road just east of this property on January 24ndash28 2011 The results of these investigations demonstrated that the contaminant plume extends in a southeasterly direction from the northern property boundary to the eastern property boundary but not to the median of Belcher Road The results of these investigations are reported in the South Belcher Road Data Report (Daniel 2011a) and the Better Business Forms Data Report (Daniel 2011b) Delineation of the eastern plume at the Building 100 Area was conducted in May June August and September 2011 This work identified a contaminant plume extending from under the eastern edge of Building 100 past the eastern STAR Center property boundary under Belcher Road and onto 11111 Belcher Road DOE made the required notification to FDEP regarding the offsite plume 14-dioxane was measured at elevated concentrations during this work and as a result was added as a COPC for the Building 100 Area in a letter from DOE to FDEP dated October 13 2011 (DOE 2011) Additional delineation at 11111 Belcher Road in March and April 2012 defined the extent of the eastern contaminant plume which appears to attenuate quickly after entering the property The Building 100 Area Site Assessment Report (DOE 2012a) summarizes the results of the plume delineation work conducted at the Building 100 Area and the adjacent private properties from 2007 to 2012 The action proposed in this document is to conduct plume stability monitoring of both the onsite and offsite plumes The Plume Stability Monitoring Plan for the Building 100 Area is included in the Site Monitoring Plan which is an Appendix to the Long-Term Surveillance and Maintenance Plan for the Pinellas Site (DOE 2012b) Plume stability monitoring began with the March 2013 sampling event 12 Northeast Site The Northeast Site is located in the northeast corner of the STAR Center (Figure 2) In the late 1960s before construction of the East Pond in 1968 drums of waste and construction debris were disposed of in the swampy area of the Northeast Site In 1986 an expansion of the East Pond was initiated to create additional storm-water retention capacity but excavation activities ceased when contamination was detected directly west of the pond EPA identified the Northeast Site as a SWMU (EPA 1992) An Interim CMS (DOE 1991b) was developed and submitted to EPA and approval of this document was received in October 1991 An interim groundwater recovery system for the Northeast Site was installed and operation commenced in January 1992 The groundwater treatment system as initially installed consisted of four recovery wells equipped with pneumatic pumps a holding tank centrifugal transfer pumps and approximately 2500 feet (ft) of transfer and secondary containment piping During 1993 DOE proposed a reconfigured system for the site consisting of four shallow and three deep recovery wells After EPA approved the upgrade the system was reconfigured and became operational on March 1 1994
US Department of Energy Pinellas Sitewide Semiannual Progress Report for December 2012mdashMay 2013 June 2013 Doc No N01796 Page 6
Between August and October 1995 a portion of the Northeast Site was excavated to remove debris drums of waste and other materials that could inhibit future corrective measures Location of the areas of excavation was based primarily on the results of a geophysical survey and knowledge of existing utility locations Detailed descriptions of the debris removal activities were submitted to EPA and FDEP as part of the Northeast Site Interim Measures Quarterly Progress Report (DOE 1996d) In 1996 DOE submitted the Northeast Site Corrective Measures Implementation Plan (DOE 1996e) to EPA Region 4 and FDEP This plan was approved by both regulatory agencies in 1997 As part of the Northeast Site CMS and CMIP a pump-and-treat system in conjunction with a subsurface hydrogeologic barrier wall to prevent migration of the contaminant plume was identified as the best available technology The pump-and-treat system included a pretreatment system for iron removal an air stripper unit and a tank for holding treated groundwater before discharge to the STAR Center IWNF prior to transfer to the POTW The treatment system was constructed in early 1997 and became operational by July 1997 processing groundwater from seven Northeast Site recovery wells and two Building 100 Area recovery wells Subsequently several additional recovery wells were installed at the Northeast Site and some of the old recovery wells were abandoned During 1997 anaerobic bioremediation and rotary steam-stripping pilot tests were conducted in the northern and southern portions of the Northeast Site respectively These tests were designed by the Innovative Treatment Remediation Demonstration group of regulatory and industry members to provide remedial options at the STAR Center At the conclusion of the field tests in July 1997 pump-and-treat technology resumed at the Northeast Site NAPLs were identified in a few monitoring and recovery wells in 1998 An Interim Measures Work Plan for Remediation of Non-Aqueous Phase Liquids at the Northeast Site (DOE 2001) was submitted to FDEP in late November 2001 The purpose of this document was to present the plan to remediate NAPLs at two areas (NAPL Areas A and B) of the Northeast Site using a thermal remediation method FDEP approved this document on January 10 2002 Construction of the NAPL Area A treatment system began in late May 2002 and system startup occurred on September 26 2002 NAPL treatment was completed on February 28 2003 The Northeast Site Area A NAPL Remediation Final Report (DOE 2003) describes the thermal remediation of Area A Construction of the NAPL Area B treatment system began in July 2004 and was completed in early August 2005 and operations began on August 16 2005 NAPL treatment was completed on August 29 2006 The Final Report Northeast Site Area B NAPL Remediation Project at the Young - Rainey STAR Center Largo Pinellas County Florida (DOE 2007) describes Area B remediation Monitoring wells were installed at the former NAPL areas to monitor the remaining dissolved-phase plumes Groundwater samples from a few of the wells continued to show high concentrations of contaminants Soil samples were collected from 12 soil borings in August 2007 to evaluate the potential for a contaminant source remaining in the subsurface at these locations Results indicated high contaminant concentrations in soil at most of these borings so a second phase of sampling was conducted in March and April 2008 during which samples were collected
US Department of Energy Pinellas Sitewide Semiannual Progress Report for December 2012mdashMay 2013 June 2013 Doc No N01796 Page 7
from 45 soil borings Ten additional borings were sampled in May and 11 more were sampled in June These 78 soil borings defined two areas containing a source of contamination To address this contamination source DOE prepared an interim remedial action plan for soil excavation using the large-diameter auger (LDA) method in accordance with the RBCA regulations and submitted the document to FDEP in August 2008 This plan was approved on August 22 2008 An engineering design was developed and a source removal subcontract was awarded in 2008 Source removal in the form of LDA excavation began on January 14 2009 and was completed on May 22 2009 Two hundred forty-three large-diameter and 352 small-diameter borings were completed Approximately 8387 cubic yards of soil were excavated including 4667 cubic yards removed as clean overburden and 3720 cubic yards of contaminated soils that were removed characterized for waste disposal and disposed of as nonhazardous waste at a RCRA Subtitle D landfill Additional information regarding the Northeast Site LDA work is available in the Data Report for Overburden Soil at the Northeast Site and the 45 Acre Site (DOE 2009a) and the Interim Remedial Action for Source Removal at the Northeast Site Final Report (DOE 2009b) As a follow-up to the LDA work emulsified soybean oil and the Dehalococcoides ethenogenes microorganism were injected into the subsurface at 75 points at the site in January and February 2010 The Injection of Emulsified Soybean Oil at the Northeast Site and 45 Acre Site (DOE 2010b) was prepared to describe the work required for this task This project has resulted in a significant decrease in contaminant mass and concentration around the former contaminant source areas and in the downgradient contaminant plume With the completion of the LDA project to remove contaminant source material and the follow-up enhanced bioremediation project DOE is proceeding to close the Northeast Site under the FDEPrsquos RBCA rules (Chapter 62-780680 FAC) The Closure Monitoring Plan for the Northeast Site and 45 Acre Site (DOE 2009c) describes the closure monitoring that is necessary under RBCA according to the requirements for Post Active Remediation Monitoring (Chapter 62-780750 FAC) Closure monitoring was implemented starting with the September 2009 sampling event and was completed in September 2012 COPCs concentrations decreased significantly over this time period DOE submitted the Site Rehabilitation Completion Report with No Further Action Proposal for the Northeast Site (DOE 2013) to FDEP in May 2013 That document proposes a risk-based closure for the Northeast Site under the Statersquos RBCA regulations 13 WWNA The WWNA (PIN18) includes the IWNF the area south of the IWNF (including the parking lot) and Building 200 (Figure 2) In April 1993 the WWNA and the Building 200 Area were identified as potential SWMUs and an RFA was conducted (EPA 1994) The RFA recommended that the WWNA and Building 200 be considered one SWMU and this SWMU is now referred to as the WWNA RFA field activities began in September 1994 and included soil characterization monitoring well installation and groundwater sampling Arsenic was identified as the major COPC Trichloroethene (TCE) and VC were detected at low concentrations in groundwater and were subsequently dismissed as COPCs once their concentrations decreased below cleanup levels
US Department of Energy Pinellas Sitewide Semiannual Progress Report for December 2012mdashMay 2013 June 2013 Doc No N01796 Page 8
A CMSCMIP (DOE 1997b) was completed for this SWMU in 1997 The recommended remediation alternative for the WWNA was groundwater recovery with the Building 100 Area wells and an additional recovery well located in the WWNA The CMIP recommended (1) that the recovery well in the WWNA withdraw surficial aquifer groundwater directly from the arsenic plume thereby reducing contaminant mass and preventing contaminant migration and (2) that the recovered water be discharged directly to the STAR Centerrsquos wastewater neutralization facility Because FDEP expressed concerns about elevated concentrations of arsenic in the soil DOE conducted extensive sampling and analysis of soil in January and February 1999 in an effort to locate the source of arsenic contamination Elevated levels of arsenic were identified at several locations and at various depths within the SWMU A treatability study was conducted to determine the leachability of arsenic from the soil into the groundwater The study concluded that arsenic leachability from the soil was very limited as demonstrated by a measured average soilwater distribution coefficient of 63 liters per kilogram DOE then conducted a statistical evaluation of arsenic soil data that resulted in the proposal to excavate two areas where the highest concentrations of arsenic were identified Follow-up monitoring of strategically located wells would then determine whether arsenic concentrations in the groundwater decrease with time This proposal was approved by FDEP in September 1999 An excavation plan was developed to address logistics sampling and analytical concerns and waste management issues regarding the generation of contaminated media This document and the statistical evaluation are included in the WWNA CMIP Addendum (DOE 2000) Excavation of the two areas was completed in early October 1999 Subsequently the existing recovery well was abandoned and two recovery wells were installed to continue plume control in the area In addition a third recovery well was created by converting the monitoring well with the highest arsenic concentration (PIN18-0501) to a recovery well On December 20 2005 DOE received concurrence from FDEP to shut down the groundwater recovery system and begin monitoring to determine a closure approach through FDEPrsquos RBCA regulations promulgated by the Florida Legislature in 2003 The 1-year RBCA closure monitoring program specified by FDEP began in October 2005 and was completed in October 2006 A No Further Action with Controls proposal was submitted to FDEP on March 14 2007 FDEP approved the document on May 24 2007 and requested that DOE submit an updated Statement of Basis for the WWNA Submittal of the Statement of Basis is awaiting finalization of ICs at the STAR Center The goal of the 1999 soil excavation was to remove the areas containing the highest arsenic concentrations such that the remaining soils met the industrial CTL of 12 milligrams per kilogram Soils containing arsenic concentrations above the residential CTL of 21 milligrams per kilogram were left in place because the current site use is solely industrial After the No Further Action with Controls proposal was submitted in 2007 FDEP expressed concern about arsenic exceeding the residential standard in shallow soils (less than 2 ft deep) In response DOE determined that a potential course of action was to identify the area where the residential arsenic
US Department of Energy Pinellas Sitewide Semiannual Progress Report for December 2012mdashMay 2013 June 2013 Doc No N01796 Page 9
standard is exceeded and apply an IC that would prohibit future residential development in this area Negotiations to apply the IC are ongoing 14 Site Update
FDEP verbally approved cessation of closure monitoring at the Northeast Site during a teleconference with DOE on January 17 2013
The Site Rehabilitation Completion Report with No Further Action Proposal for the Northeast Site (DOE 2013) was submitted to FDEP in May 2013
Twenty-seven new monitoring wells (ie nine well triples) were installed at the Building 100 Area in February 2013 to facilitate plume stability monitoring
Twenty monitoring wells at the Building 100 Area and three monitoring wells at the WWNA were abandoned on April 22 and 23 2013
The sitewide semiannual sampling was conducted March 4ndash14 2013 and included collection of water samples from 100 monitoring wells Water level measurements were obtained from all accessible monitoring wells recovery wells and ponds on March 5
The results of semiannual monitoring were reported (this document) 15 Waste Minimization The following materials were recycled at the Pinellas site from December 2012 through May 2013
31 pounds of paper
23 pounds of cardboard
7 pounds of plastic
43 pounds of magazines
1 pound of aluminum
16 pounds of batteries
20 Water-Level Elevations Depth-to-water measurements were taken at all accessible monitoring wells piezometers and ponds (including two offsite ponds) at the STAR Center on March 5 2013 The water levels were measured with an electronic water level indicator or directly from a staff gauge Groundwater elevations are listed in Table 1 21 Groundwater Flow Groundwater and surface water elevations were used to construct sitewide groundwater contour maps of the shallow and deep surficial aquifers (Plates 1 and 2 respectively) Individual contour maps were also constructed for the shallow and deep surficial aquifers at the Building 100 Area (Figures 3 and 4)
US Department of Energy Pinellas Sitewide Semiannual Progress Report for December 2012mdashMay 2013 June 2013 Doc No N01796 Page 10
For the past several years shallow groundwater beneath Building 100 has been observed to flow to the southeast under a very slight gradient and this flow pattern was observed again in March 2013 (Figure 3) A similar flow pattern was observed in the deep surficial aquifer (Figure 4) The hydraulic gradient in the Building 100 Area in March 2013 was about 0002 ftft onsite and about 0005 offsite Based on calculations using Darcyrsquos Law along with approximations of 1 ftday for hydraulic conductivity and 03 for effective porosity groundwater velocity in this area is estimated to be about 24 to 61 ftyear An aquifer test conducted in July 2009 in the area around recovery well RW03 indicated that the hydraulic conductivity of the surficial aquifer around well RW03 might be higher than that observed in other parts of the STAR Center Analysis of the aquifer test yielded an estimated hydraulic conductivity of 67 to 74 ftday which is higher than previous tests conducted in other areas of the STAR Center where estimated hydraulic conductivities were closer to 1 ftday Surface water elevations were recorded in March 2013 from the East South Southwest and West Ponds Pond 5 and the pond just east of Belcher Road (Table 2) All the ponds are hydraulically connected to the shallow surficial aquifer system (Plate 1)
30 Groundwater Sampling 31 Work Performed During the annual sampling event at the STAR Center in March 2013 groundwater samples were collected from 100 monitoring wells at the Building 100 Area Volatile organic compounds were analyzed in these samples using EPA SW-846 method 8260B and 14-dioxane was analyzed in the same samples using EPA method 8260B SIM Laboratory reports are provided in Appendix A The analytical results are discussed in Section 4 Figures 5ndash13 are plume maps for the Building 100 Area for March 2013 Figures 5 and 6 show the total COPCs (TCOPCs) concentrations TCOPCs is the sum of the individual COPC concentrations for each well The Building 100 Area COPCs are TCE cis-12-dichloroethene (cDCE) trans-12-dichloroethene (tDCE) 11-dichloroethene (11-DCE) VC and 14-dioxane Figures 7ndash13 show the plumes for the individual COPCs a plume map for tDCE is not shown because this COPC exceeded the CTL only in well 12-S35B All samples were collected in accordance with the Sampling and Analysis Plan for US Department of Energy Office of Legacy Management Sites (LMSPROS04351) using FDEP procedures All samples were submitted to TestAmerica Laboratories Inc in Denver Colorado for analysis TestAmerica Denver is accredited by the Florida Department of Health in accordance with the National Environmental Laboratory Accreditation Conference (certification number E87667) All monitoring wells were micropurged using a dedicated bladder pump or a peristaltic pump Sampling was performed when the field measurements stabilized in accordance with FDEP procedures Table 3 lists field measurements of temperature specific conductance turbidity pH oxidation-reduction potential and dissolved oxygen recorded at the time the samples were
US Department of Energy Pinellas Sitewide Semiannual Progress Report for December 2012mdashMay 2013 June 2013 Doc No N01796 Page 11
collected Measurements were made using a calibrated multiparameter meter with a flow cell and turbidity was measured using a nephelometer 32 Quality AssuranceQuality Control The results from the analytical laboratory TestAmerica Denver were checked for quality assurancequality control (QAQC) through duplicate samples and trip blanks The duplicate sample results were compared and the relative percent differences (RPDs) between the results were calculated (Table 4) trans-12-Dichloroethene in well PIN12-0580-2 VC in well PIN12-0582-2 and 11-dichloroethene in well PIN12-0587-2 all had RPD values that exceeded the EPA-recommended laboratory duplicate criterion of less than 20 RPD for results that are greater than 25 times the method detection limit These results were ldquoJrdquo qualified as estimated values due to the poor RPD value Table 4 also lists analytes in the duplicate samples from wells 12-0581-2 and 12-0582-2 that did not have an RPD calculated because the results were less than 25 times the method detection limit Some of these results show significant disagreement (eg 14-dioxane in well 12-0582-2) The poor precision of these results may be due to the fact that the laboratory diluted the original samples but not the duplicate samples These two wells were installed in February 2013 and sampled for the first time in March 2013 so historical data were not available to compare to the current results A detailed review of the chromatograms and mass spectra in the lab reports for original and duplicate samples collected from these wells confirmed the presence of the detected analytes in the duplicate samples This confirmation in combination with the results from temporary sampling points nearby in 2011 (see Section 11) strongly suggested that the results for the duplicate samples were the most representative for these wells Therefore the results from the original samples were excluded and the results from the duplicate samples are reported in this document This issue will be revisited after the second sampling event at these wells in September 2013 As specified in the Sampling and Analysis Plan for US Department of Energy Office of Legacy Management Sites duplicate samples should be collected at a frequency of one duplicate for every 20 or fewer samples For the STAR Center and the 45 Acre Site 119 samples and 6 duplicates were collected for volatiles analysis and 100 samples and 5 duplicates were collected for 14-dioxane analysis The duplicate requirements for this sampling event were met Six trip blanks and two equipment blanks also were collected during this event A data validation software module for identifying and tracking anomalous groundwater data within the Site Environmental Evaluation for Projects (SEEPro) database was used to generate a report of analytical results that fall outside of historical minimum or maximum values No anomalous results were identified
US Department of Energy Pinellas Sitewide Semiannual Progress Report for December 2012mdashMay 2013 June 2013 Doc No N01796 Page 12
40 Plume Stability Monitoring The Plume Stability Monitoring Plan for the Building 100 Area is included in an appendix to the Long-Term Surveillance and Maintenance Plan for the Pinellas Site (DOE 2012b) This plan defines the strategy to determine the stability of the onsite and offsite plumes The plume stability monitoring approach involves establishment of plume cross-sections using certain sets of wells and the determination of an area under the curve for each cross-section The cross-section lines are shown on Figure 14 The lateral cross-sections allow evaluation of the entire width of each plume as it emerges from under the building and at the site boundary if the plume is expanding laterally (concentrations increasing at the sides of the plume) this will be seen as an increase in the area under the curve The longitudinal cross-section in each plume will use wells in the centerline of the plume (the highest concentration area) to determine if the plume is expanding at its leading edge and if concentrations are decreasing stable or increasing in the plume centerline Each ldquodata pointrdquo in the cross-sections is the location of a well triple (ie wells with three different screened intervals) or a well pair The value plotted at each data point is the sum of COPC concentrations in all sampled intervals in the well pair or triple at that location For example in cross-section E1-E2 the northern data point will be the sum of TCE cDCE tDCE 11-DCE VC and 14-dioxane concentrations measured in wells 12-0555A 12-0555B and 12-0555C
For each sampling event a ldquocurverdquo will be plotted for each cross-section and then the area under the curve will be calculated The area under the curve values will be tracked from event to event and a trend line will be fit to the data The plume will be designated as unstable if an increasing trend is observed
In addition to the plume stability monitoring scheme presented above several wells that are not part of a cross-section will also be sampled to determine whether the plume is advancing at any of its boundaries (Figure 14) At each of these well locations the COPC concentrations from all screened intervals will be summed and the sum will be plotted For example for the well triple 0570 located on the Harrod property the COPC concentrations in all three screened intervals (0570-1 -2 and -3) will be summed and plotted A trend line will be fit to the plotted data and as with the area under the curve values the plume will be designated as unstable if an increasing trend is observed The March 2013 sampling event was the first plume stability monitoring event The COPCs concentrations from each well are listed in Table 5 The sum of COPCs at each ldquodata pointrdquo in each cross-section is listed in Table 6 Figures 15ndash20 show the curve plots for each cross-section The area under the curve for each cross-section is listed in Table 7 The area under the curve value is calculated using a spreadsheet it is not the sum of the COPCs in each cross-section Because the March 2013 sampling event was the first plume stability monitoring event the area under the curve values are not plotted because there is only one data point for each cross-section The area under the curve values will be plotted after the second plume stability monitoring event in September 2013
US Department of Energy Pinellas Sitewide Semiannual Progress Report for December 2012mdashMay 2013 June 2013 Doc No N01796 Page 13
50 Upcoming Tasks The following major tasks are planned for the next semiannual period (June through November 2013)
Plume stability monitoring at the Building 100 Area will continue with the semiannual sampling event in September 2013
60 References Daniel 2011a Joe Daniel Site Manager Pinellas Environmental Restoration Project SM Stoller Corporation letter (about the South Belcher Road Data Report) to Scott Surovchak Pinellas Site Manager Office of Legacy Management US Department of Energy April 4 Daniel 2011b Joe Daniel Site Manager Pinellas Environmental Restoration Project SM Stoller Corporation letter (about the Better Business Forms Data Report) to Scott Surovchak Pinellas Site Manager Office of Legacy Management US Department of Energy May 13 DOE (US Department of Energy) 1991a Environmental Restoration Program RCRA Facility Investigation Report Pinellas Plant (Draft) Albuquerque Operations Office Albuquerque New Mexico September DOE (US Department of Energy) 1991b Interim Corrective Measures Study Northeast Site Pinellas Plant Largo Florida May DOE (US Department of Energy) 1994 Statement of Basis for Twelve Solid Waste Management Units Recommended for No Further Action Pinellas Plant Largo Florida January DOE (US Department of Energy) 1996a Building 100 Area Corrective Measures Implementation Plan (Draft) Environmental Restoration Program Pinellas Plant Largo Florida January DOE (US Department of Energy) 1996b Building 100 Area Data Report October 1993 to July 1996 Office of Legacy Management Grand Junction Colorado November DOE (US Department of Energy) 1996c Building 100 Area Subsurface Investigations Phases I II and III Volumes 1 and 2 Office of Legacy Management Grand Junction Colorado January DOE (US Department of Energy) 1996d Northeast Site Interim Measures Quarterly Progress Report October through December 1995 Office of Legacy Management Grand Junction Colorado January DOE (US Department of Energy) 1996e Northeast Site Corrective Measures Implementation Plan Office of Legacy Management Grand Junction Colorado March
US Department of Energy Pinellas Sitewide Semiannual Progress Report for December 2012mdashMay 2013 June 2013 Doc No N01796 Page 14
DOE (US Department of Energy) 1997a Pinellas Plant Environmental Baseline Report prepared by Lockheed Martin Specialty Components Inc for DOE Pinellas Area Office June DOE (US Department of Energy) 1997b Corrective Measures Study ReportCorrective Measures Implementation Plan WWNABuilding 200 Office of Legacy Management Grand Junction Colorado June DOE (US Department of Energy) 1998 Building 100 Area Corrective Measures Implementation Plan Addendum Pinellas STAR Center Largo Florida February DOE (US Department of Energy) 2000 WWNABuilding 200 Corrective Measures Implementation Plan Addendum Office of Legacy Management Grand Junction Colorado January DOE (US Department of Energy) 2001 Interim Measures Work Plan for Remediation of Non-Aqueous Phase Liquids at the Northeast Site MAC-PIN 13105-1 prepared for DOE Grand Junction Office Grand Junction Colorado November DOE (US Department of Energy) 2003 Northeast Site Area A NAPL Remediation Final Report GJOminus2003minus482minusTAC prepared by US Department of Energy Grand Junction Colorado September DOE (US Department of Energy) 2005 Building 100 Area Enhanced Bioremediation Pilot Test Final Report DOE-LMGJ791-2005 Office of Legacy Management Grand Junction Colorado January DOE (US Department of Energy) 2006 Building 100 Area Corrective Measures Study Report Addendum DOE-LMGJ1241-2006 Office of Legacy Management Grand Junction Colorado July DOE (US Department of Energy) 2007 Final Report Northeast Site Area B NAPL Remediation Project at the Young - Rainey STAR Center Largo Pinellas County Florida DOE-LM1457-2007 Office of Legacy Management Grand Junction Colorado April DOE (US Department of Energy) 2009a Data Report for Overburden Soil at the Northeast Site and the 45 Acre Site LMSPINN01395 Office of Legacy Management Grand Junction Colorado July DOE (US Department of Energy) 2009b Interim Remedial Action for Source Removal at the Northeast Site Final Report LMSPINN01357 Office of Legacy Management Grand Junction Colorado September DOE (US Department of Energy) 2009c Closure Monitoring Plan for the Northeast Site and 45 Acre Site LMSPINN01401 Office of Legacy Management Grand Junction Colorado August
US Department of Energy Pinellas Sitewide Semiannual Progress Report for December 2012mdashMay 2013 June 2013 Doc No N01796 Page 15
DOE (US Department of Energy) 2010a Building 100 Area Off-Site Plume Delineation South of Bryan Dairy Road Data Report for Rally Stores Property LMSPINN01535 Office of Legacy Management Grand Junction Colorado October DOE (US Department of Energy) 2010b Injection of Emulsified Soybean Oil at the Northeast Site and 45 Acre Site LMSPINN01494 Office of Legacy Management Grand Junction Colorado April DOE (US Department of Energy) 2011 Scott Surovchak Pinellas Site Manager letter (about Groundwater Samples at the Young-Rainey STAR Center) to John Armstrong Remedial Project Manager FDEP October 13 DOE (US Department of Energy) 2012a Building 100 Area Site Assessment Report LMSPINN01747 Office of Legacy Management Grand Junction Colorado August DOE (US Department of Energy) 2012b Long-Term Surveillance and Maintenance Plan for the Pinellas Site LMSPINN01058-100 Office of Legacy Management Grand Junction Colorado November DOE (US Department of Energy) 2013 Site Rehabilitation Completion Report with No Further Action Proposal for the Northeast Site LMSPINN01778 Office of Legacy Management Grand Junction Colorado May EPA (US Environmental Protection Agency) 1988 RCRA Facility Assessment Department of EnergymdashFl6 890 090 008 June EPA (US Environmental Protection Agency) 1992 Letter to DOE Gerald W Johnson Approval of Pinellas Site Remedial Facility Investigation Report April EPA (US Environmental Protection Agency) 1994 RCRA Facility Assessment Report WWNABuilding 200 Area March Sampling and Analysis Plan for US Department of Energy Office of Legacy Management Sites LMSPROS04351 continually updated prepared by SM Stoller Corporation for the US Department of Energy Office of Legacy Management Grand Junction Colorado
US Department of Energy Pinellas Sitewide Semiannual Progress Report for December 2012mdashMay 2013 June 2013 Doc No N01796 Page 16
Figure 1 Young - Rainey STAR Center Location
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Figure 2 Location of STAR Center Solid-Waste Management Units (SWMUs)
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Figure 3 Building 100 Area Shallow Surficial Aquifer Flow March 2013
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Figure 4 Building 100 Area Deep Surficial Aquifer Flow March 2013
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Figure 5 Building 100 Area TCOPCs Concentrations March 2013
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Figure 6 Building 100 Area South TCOPCs Concentrations March 2013
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Figure 7 Building 100 Area TCE Concentrations March 2013
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Figure 8 Building 100 Area cDCE Concentrations March 2013
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Figure 9 Building 100 Area South cDCE Concentrations March 2013
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Figure 10 Building 100 Area VC Concentrations March 2013
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Figure 11 Building 100 Area South VC Concentrations March 2013
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Figure 12 Building 100 Area 14-dioxane Concentrations March 2013
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Figure 13 Building 100 Area South 14-dioxane Concentrations March 2013
US Department of Energy Pinellas Sitewide Semiannual Progress Report for December 2012mdashMay 2013 June 2013 Doc No N01796 Page 29
Figure 14 Building 100 Area Plume Stability Monitoring Cross-Sections
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Figure 15 Cross-Section E1-E2
0
50
100
150
200
250
300
350
400
450
0555 0554 0580 S71 S70 S69
E1 ‐ E2March 2013
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Figure 16 Cross-Section E3-E4
0
100
200
300
400
500
600
541542549 0581 0582 539540 S73 0583
E3 ‐ E4March 2013
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Figure 17 Cross-Section E5-E6
0
100
200
300
400
500
600
S67 0580 0582 0576 0578
E5 ‐ E6March 2013
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Figure 18 Cross-Section S1-E2
0
500
1000
1500
2000
2500
3000
3500
4000
4500
5000
0561 0584 0585 524525 S68 S69
S1 ‐ E2March 2013
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Figure 19 Cross-Section S2-S3
0
100
200
300
400
500
600
700
800
900
0586 0587 0588
S2 ‐ S3March 2013
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Figure 20 Cross-Section S4-S5
0
1000
2000
3000
4000
5000
6000
0585 0587 0569 0572 0574 0575
S4 ‐ S5March 2013
US Department of Energy Pinellas Sitewide Semiannual Progress Report for December 2012mdashMay 2013 June 2013 Doc No N01796 Page 36
Table 1 Groundwater-Level Data at the STAR Center March 2013
Location Measurement Water Depth
(ft bls)
Groundwater Elevation (ft amsl) Date Time
PIN02 Sitewide Piezometers
PZ03 352013 1023 421 1549
PZ04 352013 1029 283 1537
PZ05 352013 1018 356 1454
PZ08 352013 1012 439 1401
PZ09 352013 1344 412 1388
PZ10 352013 1003 454 1434
PZ11 352013 0945 483 1405
Building 100 Area
PIN12
0509 352013 1142 361 1443
0515 352013 0631 428 1362
0516 352013 0609 448 1352
0517 352013 0641 406 1384
0518 352013 0645 397 1397
0520 352013 1132 366 1435
0521 352013 1128 370 1435
0524 352013 0711 366 1375
0525 352013 0657 371 1371
0527 352013 1035 1272 535
0528 352013 1348 1213 547
0539 352013 1413 336 1324
0540 352013 1421 292 1318
0541 352013 0841 484 1282
0542 352013 1424 451 1319
0549 352013 0847 451 1315
0550-1 352013 1436 272 1198
0550-2 352013 1436 262 1208
0550-3 352013 1437 257 1213
0551-1 352013 1425 329 1211
0551-2 352013 1425 293 1247
0551-3 352013 1425 318 1222
0553A 352013 0800 450 1361
0553B 352013 0824 466 1345
0553C 352013 0828 464 1347
0554A 352013 0752 463 1361
0554B 352013 0750 463 1361
0554C 352013 0743 465 1359
0555A 352013 0754 412 1377
0555B 352013 0758 421 1368
0555C 352013 0759 420 1369
0559-1 352013 0926 535 1255
0559-2 352013 1132 507 1283
0559-3 352013 1133 689 1101
Table 1 (continued) Groundwater-Level Data at the STAR Center March 2013
US Department of Energy Pinellas Sitewide Semiannual Progress Report for December 2012mdashMay 2013 June 2013 Doc No N01796 Page 37
Location Measurement Water Depth
(ft bls)
Groundwater Elevation (ft amsl) Date Time
0560-1 352013 0640 394 1378
0560-2 352013 0639 385 1387
0560-3 352013 0640 370 1402
0561-1 352013 0647 431 1391
0561-2 352013 0656 436 1386
0561-3 352013 0656 434 1388
0562-1 352013 1135 489 1337
0562-2 352013 1140 487 1339
0562-3 352013 1141 484 1342
0563-1 352013 1141 349 1378
0563-2 352013 1342 346 1381
0563-3 352013 1343 341 1386
0564-1 352013 1453 296 1254
0564-2 352013 1454 307 1243
0564-3 352013 1455 313 1237
0565-1 352013 1506 412 1158
0565-2 352013 1507 416 1154
0565-3 352013 1508 413 1157
0566-1 352013 1530 426 1134
0566-2 352013 1530 421 1139
0566-3 352013 1531 423 1137
0567-1 352013 1410 413 1413
0567-2 352013 1411 433 1393
0567-3 352013 1412 457 1369
0568-1 352013 1418 436 1390
0568-2 352013 1419 461 1365
0568-3 352013 1420 459 1367
0569-1 352013 1430 463 1348
0569-2 352013 1431 488 1323
0569-3 352013 1432 488 1323
0571-1 352013 1445 529 1291
0571-2 352013 1446 540 1280
0571-3 352013 1447 534 1286
0572-1 352013 1515 330 1230
0572-2 352013 1516 330 1230
0573-1 352013 1537 328 1172
0573-2 352013 1537 328 1172
0573-3 352013 1537 330 1170
0574-1 352013 1518 541 1089
0574-2 352013 1519 533 1097
0574-3 352013 1520 537 1093
0575-1 352013 1509 491 1039
0575-2 352013 1511 487 1043
0576-1 352013 1411 465 1285
0576-2 352013 1412 453 1297
Table 1 (continued) Groundwater-Level Data at the STAR Center March 2013
US Department of Energy Pinellas Sitewide Semiannual Progress Report for December 2012mdashMay 2013 June 2013 Doc No N01796 Page 38
Location Measurement Water Depth
(ft bls)
Groundwater Elevation (ft amsl) Date Time
0576-3 352013 1412 452 1298
0577-1 352013 1202 464 1326
0577-2 352013 1203 464 1326
0577-3 352013 1204 464 1326
0578-1 352013 1355 425 1355
0578-2 352013 1356 429 1351
0578-3 352013 1357 431 1349
0579-1 352013 1451 421 1319
0579-2 352013 1451 424 1316
0579-3 352013 1452 425 1315
0580-1 352013 0940 486 1364
0580-2 352013 0941 491 1359
0580-3 352013 0942 490 1360
0581-1 352013 1055 412 1324
0581-2 352013 1056 413 1323
0581-3 352013 1057 415 1321
0582-1 352013 1100 353 1320
0582-2 352013 1101 353 1320
0582-3 352013 1102 355 1318
0583-1 352013 1111 342 1309
0583-2 352013 1112 335 1316
0583-3 352013 1113 337 1314
0584-1 352013 0857 379 1381
0584-2 352013 0858 383 1377
0584-3 352013 0859 387 1373
0585-1 352013 0903 368 1381
0585-2 352013 0904 373 1376
0585-3 352013 0905 377 1372
0586-1 352013 1350 387 1353
0586-2 352013 1351 382 1358
0586-3 352013 1352 383 1357
0587-1 352013 1354 402 1348
0587-2 352013 1355 398 1352
0587-3 352013 1356 399 1351
0588-1 352013 1357 396 1344
0588-2 352013 1358 394 1346
0588-3 352013 1359 396 1344
PZ01 352013 1427 415 1335
PZ02 352013 1443 520 1370
PZ03 352013 1437 354 1336
S29C 352013 0911 420 1431
S30B 352013 0918 415 1436
S31B 352013 0853 429 1422
S32B 352013 0900 418 1433
S33C 352013 0937 410 1441
Table 1 (continued) Groundwater-Level Data at the STAR Center March 2013
US Department of Energy Pinellas Sitewide Semiannual Progress Report for December 2012mdashMay 2013 June 2013 Doc No N01796 Page 39
Location Measurement Water Depth
(ft bls)
Groundwater Elevation (ft amsl) Date Time
S35B 352013 0951 439 1412
S36B 352013 0847 461 1390
S37B 352013 0931 408 1443
S67B 352013 1036 439 1408
S67C 352013 1037 448 1399
S67D 352013 1038 448 1400
S68B 352013 1408 404 1386
S68C 352013 1412 428 1362
S68D 352013 1412 424 1366
S69B 352013 0713 260 1340
S69C 352013 0722 262 1338
S69D 352013 0724 277 1323
S70B 352013 0732 311 1359
S70C 352013 0730 305 1365
S70D 352013 0726 323 1347
S71B 352013 0734 448 1392
S71C 352013 0737 480 1360
S71D 352013 0739 475 1365
S72B 352013 0833 495 1325
S72C 352013 0838 492 1328
S72D 352013 0840 491 1329
S73B 352013 0849 386 1314
S73C 352013 0911 386 1314
S73D 352013 0910 386 1314
PIN21
0502 352013 0912 250 1270
0503 352013 0925 263 1257
0503 352013 1357 346 1174
0504 352013 1400 390 1370
0512 352013 1405 388 1342
PIN15 Northeast Site
0506 352013 1108 327 1373
0507 352013 1104 322 1378
0513 352013 1058 1210 550
0520 352013 1100 339 1371
0530 352013 1053 371 1369
0534 352013 1104 222 1488
0535 352013 1057 379 1381
0537 352013 1109 428 1432
0568 352013 1044 448 1402
0569 352013 1040 427 1411
0573 352013 1125 442 1396
0574 352013 1128 428 1414
0594 352013 1112 465 1385
0595 352013 1135 449 1411
Table 1 (continued) Groundwater-Level Data at the STAR Center March 2013
US Department of Energy Pinellas Sitewide Semiannual Progress Report for December 2012mdashMay 2013 June 2013 Doc No N01796 Page 40
Location Measurement Water Depth
(ft bls)
Groundwater Elevation (ft amsl) Date Time
M16D 352013 1125 382 1438
M16S 352013 1123 381 1439
M24D 352013 1135 390 1390
M33D 352013 1134 325 1435
PIN18 WWNA
0503 352013 1137 346 1422
0507 352013 1343 370 1403
0523 352013 1116 522 1418
0524 352013 1119 477 1423
0525 352013 1118 457 1433
0526 352013 1017 466 1394
Abbreviations amsl = above mean sea level bls = below land surface
US Department of Energy Pinellas Sitewide Semiannual Progress Report for December 2012mdashMay 2013 June 2013 Doc No N01796 Page 41
Table 2 Surface Water Elevations March 2013
Location Measurement Surface Water
Elevation (ft amsl) Date Time
PIN01 Pond 5
P501 352013 1013 1360
P502 352013 1009 1389
PIN02 West Pond
W005 352013 1004 1409
PIN12 Belcher Road Pond
BR01 352013 1447 1295
PIN15 East Pond
E001 352013 1045 1377
PIN23 Southwest Pond
SW01 352013 1351 1359
PIN37 South Pond
S001 352013 1355 1361
S002 352013 1401 14661
Notes 1questionable value not used for water elevation contours Abbreviations amsl = above mean sea level
US Department of Energy Pinellas Sitewide Semiannual Progress Report for December 2012mdashMay 2013 June 2013 Doc No N01796 Page 42
Table 3 Field Measurements of Samples Collected at the STAR Center March 2013
Location Screen Depth (ft bls)
Temperature (degC)
Specific Conductance (micromhoscm)a
Turbidity (NTU)
pH
Oxidation Reduction Potential
(mV)
Dissolved Oxygen (mgL)
PIN12
0524 27ndash37 246 1426 4 661 -14 08
0525 12ndash22 241 742 29 679 -63 05
0539 95ndash195 241 1612 14 651 -46 06
0540 20ndash30 243 1457 13 653 -35 06
0541 10ndash20 277 784 16 660 -63 06
0542 20ndash30 281 796 7 661 -53 06
0549 30ndash40 273 1404 15 663 -52 07
0551-1 9ndash18 228 1004 3 665 39 15
0551-2 20ndash29 232 1055 13 665 44 11
0554A 3ndash13 216 650 9 648 40 08
0554B 13ndash23 227 682 11 665 -34 05
0554C 23ndash33 244 880 14 672 -63 06
0555A 25ndash125 233 379 - 660 -26 12
0555B 13ndash23 225 376 26 702 -30 10
0555C 23ndash33 210 534 16 679 -33 13
0561-1 9ndash18 223 511 13 682 9 05
0561-2 20ndash29 229 603 2 677 -12 05
0561-3 31ndash40 210 1055 1 658 -20 04
0565-1 9ndash18 219 1345 1 672 -36 11
0565-2 20ndash29 204 1250 1 668 -30 18
0565-3 31ndash40 222 1502 2 664 -31 14
0568-1 9ndash18 246 1819 4 670 -4 17
0568-2 20ndash29 252 1402 10 672 -27 16
0568-3 31ndash40 254 1798 10 673 -22 17
0569-1 9ndash18 205 1847 4 679 -14 14
0569-2 20ndash29 209 1248 7 674 -30 13
0569-3 31ndash40 214 1292 3 673 -31 14
0570-1 9ndash18 241 2048 4 676 -43 15
0570-2 20ndash29 267 1665 8 677 -20 -
0570-3 31ndash40 220 1363 9 676 37 11
0572-1 9ndash18 267 1638 6 671 -39 20
0572-2 20ndash29 267 1017 5 674 -23 16
0573-1 9ndash18 210 1594 7 666 -47 16
0573-2 20ndash29 231 1172 4 668 -45 17
0573-3 31ndash40 229 1514 1 661 -22 14
0574-1 9ndash18 202 1258 9 675 -24 18
0574-2 20ndash29 225 1274 5 673 -18 16
0574-3 31ndash40 237 1492 5 672 -19 18
0575-1 9ndash18 228 1323 5 674 -38 17
0575-2 20ndash29 218 1459 9 667 -35 14
0576-1 4ndash13 191 1112 2 663 59 15
0576-2 15ndash24 200 1099 6 664 26 12
0576-3 26ndash35 226 1719 9 672 48 12
Table 3 (continued) Field Measurements of Samples Collected at the STAR Center March 2013
US Department of Energy Pinellas Sitewide Semiannual Progress Report for December 2012mdashMay 2013 June 2013 Doc No N01796 Page 43
Location Screen Depth (ft bls)
Temperature (degC)
Specific Conductance (micromhoscm)a
Turbidity (NTU)
pH
Oxidation Reduction Potential
(mV)
Dissolved Oxygen (mgL)
0577-1 4ndash13 206 2069 6 642 40 18
0577-2 15ndash24 204 1458 3 648 41 19
0577-3 26ndash35 200 1245 3 668 30 -
0578-1 4ndash13 179 726 6 637 128 12
0578-2 15ndash24 193 901 3 647 73 13
0578-3 26ndash35 193 1077 4 647 38 13
0579-1 4ndash13 193 1324 5 614 36 15
0579-2 15ndash24 210 1084 6 653 26 16
0579-3 26ndash35 207 1439 31 669 4 16
0580-1 9ndash18 162 653 29 702 -66 12
0580-2 20ndash29 189 1260 13 710 -75 12
0580-3 31ndash40 218 1538 11 702 -108 13
0581-1 9ndash18 225 1350 11 688 -129 08
0581-2 20ndash29 237 1100 17 702 -136 08
0581-3 31ndash40 258 1484 11 671 -74 07
0582-1 9ndash18 263 2261 12 674 -113 06
0582-2 20ndash29 264 1234 9 676 -97 06
0582-3 31ndash40 267 1527 24 663 -55 07
0583-1 9ndash18 240 1224 47 689 -132 04
0583-2 20ndash29 234 1739 5 659 -83 07
0583-3 31ndash40 247 1779 13 668 -74 06
0584-1 9ndash18 178 696 12 711 -61 15
0584-2 20ndash29 192 1057 12 778 -143 12
0584-3 31ndash40 205 1617 14 689 -79 16
0585-1 9ndash18 236 778 11 705 -107 13
0585-2 20ndash29 249 1196 11 698 -116 12
0585-3 31ndash40 253 1621 9 678 -105 06
0586-1 8ndash17 210 604 16 714 -103 04
0586-2 19ndash28 233 717 8 715 -151 04
0586-3 30ndash39 243 1579 10 692 -113 06
0587-1 9ndash18 251 686 30 718 -140 04
0587-2 20ndash29 255 886 5 677 -80 06
0587-3 31ndash40 250 1363 15 679 -106 07
0588-1 9ndash18 179 926 15 713 -139 04
0588-2 20ndash29 172 1072 2 677 -85 05
0588-3 31ndash40 175 1511 8 685 -76 04
S30B 5ndash15 223 1030 19 692 -26 13
S33C 11ndash21 210 638 21 682 17 12
S35B 5ndash15 228 1766 5 654 47 14
S67B 10ndash1983 206 1067 8 676 -1 14
S67C 20ndash2983 210 891 18 679 -27 14
S67D 30ndash3983 211 842 10 678 -22 12
S68B 10ndash20 195 819 14 676 -75 06
S68C 18ndash28 200 955 4 666 2 06
Table 3 (continued) Field Measurements of Samples Collected at the STAR Center March 2013
US Department of Energy Pinellas Sitewide Semiannual Progress Report for December 2012mdashMay 2013 June 2013 Doc No N01796 Page 44
Location Screen Depth (ft bls)
Temperature (degC)
Specific Conductance (micromhoscm)a
Turbidity (NTU)
pH
Oxidation Reduction Potential
(mV)
Dissolved Oxygen (mgL)
S68D 30ndash40 204 1369 3 661 -22 06
S69B 10ndash20 242 687 30 684 -78 07
S69C 20ndash30 260 689 11 687 -12 08
S69D 30ndash40 250 1633 6 665 -25 08
S70B 10ndash20 242 931 220 678 -50 05
S70C 20ndash30 250 1420 143 658 -73 07
S70D 30ndash40 256 1553 22 655 -57 08
S71B 10ndash20 247 781 29 671 -73 05
S71C 20ndash30 262 1271 311 659 -51 06
S71D 30ndash40 267 1555 10 660 -56 07
S73B 10ndash20 274 1178 27 652 -314 00
S73C 20ndash30 279 1737 17 651 -134 10
S73D 30ndash40 267 1854 33 621 -66 12
Notes a Temperature corrected to 25 degC Abbreviations ndash = not measured bls = below land surface micromhoscm = micromhos per centimeter mgL = milligrams per liter mV = millivolts NTU = nephelometric turbidity units
US Department of Energy Pinellas Sitewide Semiannual Progress Report for December 2012mdashMay 2013 June 2013 Doc No N01796 Page 45
Table 4 Relative Percent Difference (RPD) for Duplicate Samples March 2013 (Reported in microgL)
Sample ID Duplicate ID Analyte Result MDL Duplicate
Result Duplicate
MDL RPD
PIN12-0580-2 PIN12-2450
11-Dichloroethane 67 022 62 022 8
14-Dioxane 160 44 190 44 17
cis-12-Dichloroethene 18 015 16 015 12
trans-12-Dichloroethene 50 015 40 015 22
Vinyl chloride 150 040 150 040 0
PIN12-0581-2 PIN12-2451
11-Dichloroethanea 94J 22 12 022
11-Dichloroethenea 23U 23 047J 023
cis-12-Dichloroethenea 29J 15 36 015
Methylene chloridea 37J 32 032U 032
Vinyl chloridea 10U 10 73 010
PIN12-0582-2 PIN12-2452
11-Dichloroethane 49 044 46 022 6
11-Dichloroethenea 063J 046 072J 023
14-Dioxanea 044U 044 170 88
Acetonea 73J 38 19U 19
cis-12-Dichloroethene 13 03 13 015 0
Naphthalenea 044U 044 023J 022
trans-12-Dichloroethene 23 03 25 015 8
Vinyl chloride 74 1 130 040 55
PIN12-0583-2 PIN12-2453 trans-12-Dichloroethene 22 015 26 015 17
Vinyl chloride 16 010 15 010 6
PIN12-0587-2 PIN12-2454
11-Dichloroethene 79 023 11 023 33
cis-12-Dichloroethene 190 075 220 15 15
trans-12-Dichloroethene 14 015 16 015 13
Vinyl chloride 71 05 82 10 14
Notes a An RPD was not calculated for these analytes because the result is less than 25 times the MDL Abbreviations J = Estimated value MDL = method detection limit RPD = relative percent difference U = not detected
US Department of Energy Pinellas Sitewide Semiannual Progress Report for December 2012mdashMay 2013 June 2013 Doc No N01796 Page 46
Table 5 COPC Concentrations at the Building 100 Area (microgL)a
Well TCE cis-12-DCE trans-12-
DCE 11-DCE
Vinyl chloride
14 Dioxane TCOPCs
CTLsb 30 700 1000 70 10 32
E1 to E2 Cross Section
0555A lt016 lt015 lt015 lt023 lt01 lt022 ND
0555B lt016 lt015 lt015 lt023 lt01 lt022 ND
0555C lt016 11 043J lt023 lt01 lt022 153
0554A lt016 lt015 lt015 lt023 lt01 lt022 ND
0554B lt016 lt015 lt015 lt023 lt01 lt044 ND
0554C lt016 16 55 1 88 76 1865
0580-1 lt016 054J lt015 lt023 42 4 874
0580-2 lt016 18 5J lt023 150J 160 333
0580-3 lt016 12 088J lt023 23 28 6388
S71B lt016 lt015 lt015 lt023 lt01 lt022 ND
S71C lt016 18 10 029J 44 34 10629
S71D lt016 29 17 06J 60 lt044 1066
S70B lt016 15 047J lt023 75 lt022 2297
S70C lt016 19 72 047J 22 15 6367
S70D lt016 23 92 068J 19 12 6388
S69B lt016 lt015 lt015 lt023 lt01 lt088 ND
S69C lt016 lt015 lt015 lt023 lt01 lt088 ND
S69D lt016 03J lt015 lt023 lt01 lt088 03
E3 to E4 Cross Section
0541 lt016 02J lt015 lt023 lt01 lt022 02
0542 lt064 lt06 lt06 lt092 lt04 lt044 ND
0549 lt016 017J lt015 lt023 lt01 lt044 017
0581-1 lt016 026J lt015 lt023 05J lt044 076
0581-2 lt016 36 lt015 047J 73 lt044 1137c
0581-3 lt032 lt03 lt03 lt046 lt02 lt044 ND
0582-1 lt016 lt015 lt015 lt023 12 lt044 12
0582-2 lt016 13 25 072J 130J 170J 31622c
0582-3 lt016 02J lt015 lt023 12 lt044 14
0539 lt016 16 13 lt023 53 38 939
0540 lt016 12 68 lt023 230 170J 4188
S73B lt016 14 05J lt023 11 lt044 129
S73C lt016 18 17 047J 230 130 39547
S73D lt016 021J lt015 lt023 047J lt088 068
0583-1 lt016 lt015 lt015 lt023 lt01 lt044 ND
0583-2 lt016 025J 22 lt023 16 lt44 1845
0583-3 lt016 lt015 lt015 lt023 lt01 lt088 ND
E5 to E6 Cross Section
S67B lt016 13 33 lt023 250 91 3573
S67C lt016 48 97 064J 65 lt088 12334
S67D lt016 62 19 lt023 11 lt022 191
0580-1 lt016 054J lt015 lt023 42 4 874
0580-2 lt016 18 5J lt023 150J 160 333
0580-3 lt016 12 088J lt023 23 28 6388
Table 5 (continued) COPC Concentrations at the Building 100 Area (microgL)a
US Department of Energy Pinellas Sitewide Semiannual Progress Report for December 2012mdashMay 2013 June 2013 Doc No N01796 Page 47
Well TCE cis-12-DCE trans-12-
DCE 11-DCE
Vinyl chloride
14 Dioxane TCOPCs
CTLsb 30 700 1000 70 10 32
0582-1 lt016 lt015 lt015 lt023 12 lt044 12
0582-2 lt016 13 25 072J 130J 170J 31622c
0582-3 lt016 02J lt015 lt023 12 lt044 14
0576-1 lt016 74 017J 2 15 36 6057
0576-2 lt016 89 021J 24 17 27J 5551
0576-3 lt016 046J lt015 lt023 12 lt088 166
0578-1 lt016 lt015 lt015 lt023 lt01 lt044 ND
0578-2 lt016 lt015 lt015 lt023 lt01 lt044 ND
0578-3 lt016 lt015 lt015 lt023 lt01 lt044 ND
S1 to E2 Cross Section
0561-1 lt016 lt015 lt015 lt023 lt01 lt022 ND
0561-2 lt016 lt015 lt015 lt023 lt01 lt044 ND
0561-3 lt016 lt015 lt015 lt023 lt01 lt044 ND
0584-1 lt016 lt015 lt015 lt023 lt01 lt044 ND
0584-2 lt016 035J lt015 lt023 lt01 lt044 035
0584-3 lt032 lt03 lt03 lt046 1J lt044 1
0585-1 53 59 041J 27 98 lt044 7721
0585-2 420 3500 17 160 420 lt88 4517
0585-3 071J 140 11 4 200 lt044 34581
0524 lt032 570 71 16 600 lt088 11931
0525 lt016 13 lt015 lt023 lt01 lt044 13
S68B lt016 lt015 lt015 lt023 lt01 lt044 ND
S68C lt064 53 lt06 lt092 lt04 45 98
S68D lt064 41 lt06 lt092 16 33 603
S69B lt016 lt015 lt015 lt023 lt01 lt088 ND
S69C lt016 lt015 lt015 lt023 lt01 lt088 ND
S69D lt016 03J lt015 lt023 lt01 lt088 03
S2 to S3 Cross Section
0586-1 lt016 036J lt015 lt023 lt01 lt044 036
0586-2 lt016 3 lt015 lt023 29 lt044 59
0586-3 lt016 053J lt015 lt023 15 lt044 203
0587-1 lt016 50 03J 13 13 lt044 646
0587-2 lt016 190 14 79J 71 lt044 2703
0587-3 lt016 280 22 16 130 lt044 4282
0588-1 lt064 lt06 lt06 lt092 lt04 lt044 ND
0588-2 lt016 12 lt015 lt023 16 66 346
0588-3 lt016 087J lt015 lt023 14 lt044 227
S4 to S5 Cross Section
0585-1 53 59 041J 27 98 lt044 7721
0585-2 420 3500 17 160 420 lt88 4517
0585-3 071J 140 11 4 200 lt044 34581
0587-1 lt016 50 03J 13 13 lt044 646
0587-2 lt016 190 14 79J 71 lt044 2703
0587-3 lt016 280 22 16 130 lt044 4282
0569-1 lt016 lt015 lt015 lt023 lt01 lt044 ND
Table 5 (continued) COPC Concentrations at the Building 100 Area (microgL)a
US Department of Energy Pinellas Sitewide Semiannual Progress Report for December 2012mdashMay 2013 June 2013 Doc No N01796 Page 48
Well TCE cis-12-DCE trans-12-
DCE 11-DCE
Vinyl chloride
14 Dioxane TCOPCs
CTLsb 30 700 1000 70 10 32
0569-2 lt064 22J lt06 lt092 lt04 16J 38
0569-3 lt064 54 lt06 25J 37 13J 948
0572-1 lt064 lt06 lt06 lt092 lt04 lt044 ND
0572-2 lt08 200 17J 10 42 lt044 2537
0574-1 lt064 73 lt06 lt092 12 lt044 193
0574-2 lt016 17 028J lt023 18 lt044 3528
0574-3 lt016 059J lt015 lt023 1 lt044 159
0575-1 lt064 lt06 lt06 lt092 lt04 19 19
0575-2 lt064 lt06 lt06 lt092 lt04 lt022 ND
Other Wells
0551-1 lt016 lt015 lt015 lt023 lt01 lt044 ND
0551-2 lt016 lt015 lt015 lt023 lt01 lt044 ND
0565-1 lt064 lt06 lt06 lt092 lt04 lt022 ND
0565-2 lt064 lt06 lt06 lt092 lt04 lt022 ND
0565-3 lt064 lt06 lt06 lt092 lt04 lt022 ND
0568-1 lt064 lt06 lt06 lt092 lt04 lt044 ND
0568-2 lt016 lt015 lt015 lt023 lt01 lt044 ND
0568-3 lt016 lt015 lt015 lt023 lt01 lt044 ND
0570-1 lt016 lt015 lt015 lt023 lt01 lt044 ND
0570-2 lt016 lt015 lt015 lt023 055J lt044 055
0570-3 lt016 lt015 lt015 lt023 34 lt044 34
0573-1 lt064 lt06 lt06 lt092 lt04 lt022 ND
0573-2 lt064 lt06 lt06 lt092 lt04 lt022 ND
0573-3 lt064 lt06 lt06 lt092 lt04 lt022 ND
0577-1 lt016 lt015 lt015 lt023 lt01 lt044 ND
0577-2 lt016 lt015 lt015 lt023 lt01 lt044 ND
0577-3 lt016 lt015 lt015 lt023 lt01 lt044 ND
0579-1 lt016 lt015 lt015 lt023 lt01 lt044 ND
0579-2 lt016 lt015 lt015 lt023 lt01 lt044 ND
0579-3 lt016 lt015 lt015 lt023 lt01 lt044 ND
S30B 23 43 45 054J 10 lt044 8104d
S33C 180 920 48 33 150 lt044 1331d
S35B 5500 40000 5100 940 12000 lt044 63540d
Notes a lt values are method detection limits b The offsite CTL is a factor of 10 lower than the listed onsite (poor water quality) CTL c As explained in Section 32 this table lists the results for duplicate samples for wells 12-0581-2 and 12-0582-2 d Wells S30B S33C and S35B were sampled to track potential source depletion under the northwest corner of the
building These wells are not part of the plume stability monitoring program Abbreviations J = Estimated value ND = Not detected
US Department of Energy Pinellas Sitewide Semiannual Progress Report for December 2012mdashMay 2013 June 2013 Doc No N01796 Page 49
Table 6 Sum of COPCs for Each Plume Stability Monitoring Cross-Section
Cross Section Sum of COPCs (microgL) E1 to E2 Cross Section
0555 153
0554 1865
0580 40562
S71 21289
S70 15052
S69 03
E3 to E4 Cross Section
054105420549 037
0581 1213
0582 31882
05390540 5127
S73 40905
0583 1845
E5 to E6 Cross Section
S67 49974
0580 40562
0582 31882
0576 11774
0578 0
S1 to E2 Cross Section
0561 0
0584 135
0585 494002
05240525 11944
S68 701
S69 03
S2 to S3 Cross Section
0586 829
0587 7631
0588 3687
S4 to S5 Cross Section
0585 494002
0587 7631
0569 986
0572 2537
0574 5617
0575 19
US Department of Energy Pinellas Sitewide Semiannual Progress Report for December 2012mdashMay 2013 June 2013 Doc No N01796 Page 50
Table 7 Area Under the Curve Values For Each Plume Stability Monitoring Cross-Section
Cross Section Area Under the Curve
March 2013 (dimensionless)
E1-E2 956
E3-E4 1262
E5-E6 1092
S1-E2 6206
S2-S3 786
S4-S5 3643
WestPond
East Pond
Pond 5
Southwest PondSouth Pond South Pond
Pond North of the45 Acre Site
Belcher Road Pond
12-0571-11291
12-S30B1436
12-S31B1422
12-S32B1433
12-S35B1412
12-S36B139
12-S37B1443
20-M0031488
12-S70B1359
12-S72B1325
12-S73B1314
12-S67B1408
12-S71B1392
12-S69B134
20-M40S1504
18-05251433
20-M0241445
23-SW011359
12-05091443
21-0502127
21-0504137
37-S0011361
15-05071378
15-05201371
15-05301369
15-05681402
15-05731396
01-P501136
02-W0051409
02-PZ051454
20-BP011426
02-PZ091388
02-PZ031549
02-PZ081401
01-P5021389
15-05951411
12-0567-11413
12-0568-1139
12-0569-11348
12-0564-11254
12-0565-11158
12-0566-11134
12-0573-11172
12-0575-11039
02-PZ101434
12-0576-11285
12-0577-11326
12-0579-11319
12-0572-1123
12-0587-11348
12-0588-11344
12-0582-1132
12-0581-11324
12-0580-11364
12-0585-11381
12-0584-11381
12-0554A1361
12-0563-11378
12-0560-11378
12-0559-11255
12-0561-11391 12-0539
1324
12-05411282
20-M0671461
20-M0691485
12-0553A1361
12-S68B1386
20-M0351465
15-M16S1439
12-0578-11355
12-0551-11211
12-0586-11353
12-0583-11309
12-0562-11337
12-0550-11198
20-M06515
12-0555A1377
21-05121342
02-PZ041537
12-0574-11089
15-E0011377
12-BR011295
11
15
15
15
14
14
14
12
12
12
12
15
15
15 15
15
13
13
13
13
13
13
14 14
14
14
14
1414
1414
14
14
14
14
15
15
WestPond
East Pond
Pond 5
Southwest PondSouth Pond South Pond
Pond North of the45 Acre Site
Belcher Road Pond
12-0571-11291
12-S30B1436
12-S31B1422
12-S32B1433
12-S35B1412
12-S36B139
12-S37B1443
20-M0031488
12-S70B1359
12-S72B1325
12-S73B1314
12-S67B1408
12-S71B1392
12-S69B134
20-M40S1504
18-05251433
20-M0241445
23-SW011359
12-05091443
21-0502127
21-0504137
37-S0011361
15-05071378
15-05201371
15-05301369
15-05681402
15-05731396
01-P501136
02-W0051409
02-PZ051454
20-BP011426
02-PZ091388
02-PZ031549
02-PZ081401
01-P5021389
15-05951411
12-0567-11413
12-0568-1139
12-0569-11348
12-0564-11254
12-0565-11158
12-0566-11134
12-0573-11172
12-0575-11039
02-PZ101434
12-0576-11285
12-0577-11326
12-0579-11319
12-0572-1123
12-0587-11348
12-0588-11344
12-0582-1132
12-0581-11324
12-0580-11364
12-0585-11381
12-0584-11381
12-0554A1361
12-0563-11378
12-0560-11378
12-0559-11255
12-0561-11391 12-0539
1324
12-05411282
20-M0671461
20-M0691485
12-0553A1361
12-S68B1386
20-M0351465
15-M16S1439
12-0578-11355
12-0551-11211
12-0586-11353
12-0583-11309
12-0562-11337
12-0550-11198
20-M06515
12-0555A1377
21-05121342
02-PZ041537
12-0574-11089
15-E0011377
12-BR011295
11
15
15
15
14
14
14
12
12
12
12
15
15
15 15
15
13
13
13
13
13
13
14 14
14
14
14
1414
1414
14
14
14
14
15
15
DATE PREPARED FILENAME
GRAND JUNCTION COLORADO
US DEPARTMENT OF ENERGY
Plate 1 Sitewide Shallow Surficial Aquifer Contours
Pinellas Florida March 2013
N0179900-01MPIN041001014000N01799N0179900-01mxd smithw 06252013 83621 AM
June 25 2013
0 150 300 Feet
Under DOE ContractNo DE-AC01-07LM00060
Prepared bySM Stoller Corporation
12-S35B1412
Well Number and Groundwater Elevation in Feet (amsl)
Monitoring Well
Extraction Well
Surface Sample
Piezometer
Water Level Not Used in Contouring
Water Elevation Contour in Feet (amsl)Contour Interval = 10 Foot
Inferred Water Elevation Contour in Feet (amsl)
Inferred Groundwater Flow Direction
Slurrywall
Fence
Road
Railroad
Tank
Building
Pond
14
WestPond
East Pond
Pond 5
Southwest PondSouth Pond South Pond
Pond North of the45 Acre Site
Belcher Road Pond
12-0571-31286
12-05201435
12-05211435
12-05181397
15-05341488
20-M0011456
20-M0051484
20-M0531446
12-S68D1366
12-S73D1314
12-S69D1323
12-S71D1365
12-S72D1329
18-05071403
20-05021437
20-M0361494
20-M38D1384
20-M40D1489
20-M0231436
18-05231418
20-M41D1463
12-S70D1347
20-M18D1463
20-M22D1483
12-05241375
12-05161352
15-M24D139
15-M33D1435
15-05351381
12-0550-31213
20-M0551417
20-M0591476
15-05691411
20-M0581475
12-05491315
12-0567-31369
12-0569-31323
12-0564-31237
12-0566-31137
12-0572-2123
12-0573-3117
02-PZ111405
12-0576-31298
12-0577-31326
12-PZ011335
12-PZ02137
12-PZ031336
12-0579-31315
12-0586-31357 12-0587-3
1351
12-0588-31344
12-0583-31314
12-0582-31318
12-0581-31321
12-0580-3136
12-0584-31373
12-0554C1359
12-0559-31101 12-0561-3
1388
12-0551-31222
15-05941385
20-M0151434
20-M0661589
20-M0681482
12-0553C1347
12-0555C1369
20-M0561428
12-S67D14
12-0574-31093
12-0565-31157
12-0575-21043
12-0560-31402
12-0585-31372
12-0562-31342 12-0563-3
1386
20-M0571461
12-0568-31367
12-0578-31349
14
11
11
15
15
15
12
12
12
14
14
14
1414
14
13
13
13
13
13
1414
14 14
14
14
14
14
15
15
14
14
WestPond
East Pond
Pond 5
Southwest PondSouth Pond South Pond
Pond North of the45 Acre Site
Belcher Road Pond
12-0571-31286
12-05201435
12-05211435
12-05181397
15-05341488
20-M0011456
20-M0051484
20-M0531446
12-S68D1366
12-S73D1314
12-S69D1323
12-S71D1365
12-S72D1329
18-05071403
20-05021437
20-M0361494
20-M38D1384
20-M40D1489
20-M0231436
18-05231418
20-M41D1463
12-S70D1347
20-M18D1463
20-M22D1483
12-05241375
12-05161352
15-M24D139
15-M33D1435
15-05351381
12-0550-31213
20-M0551417
20-M0591476
15-05691411
20-M0581475
12-05491315
12-0567-31369
12-0569-31323
12-0564-31237
12-0566-31137
12-0572-2123
12-0573-3117
02-PZ111405
12-0576-31298
12-0577-31326
12-PZ011335
12-PZ02137
12-PZ031336
12-0579-31315
12-0586-31357 12-0587-3
1351
12-0588-31344
12-0583-31314
12-0582-31318
12-0581-31321
12-0580-3136
12-0584-31373
12-0554C1359
12-0559-31101 12-0561-3
1388
12-0551-31222
15-05941385
20-M0151434
20-M0661589
20-M0681482
12-0553C1347
12-0555C1369
20-M0561428
12-S67D14
12-0574-31093
12-0565-31157
12-0575-21043
12-0560-31402
12-0585-31372
12-0562-31342 12-0563-3
1386
20-M0571461
12-0568-31367
12-0578-31349
14
11
11
15
15
15
12
12
12
14
14
14
1414
14
13
13
13
13
13
1414
14 14
14
14
14
14
15
15
14
14
DATE PREPARED FILENAME
GRAND JUNCTION COLORADO
US DEPARTMENT OF ENERGY
Plate 2 Sitewide Deep Surficial Aquifer Contours
Pinellas Florida March 2013
N0179900-02MPIN041001014000N01799N0179900-02mxd smithw 06252013 84035 AM
June 25 2013
0 150 300 Feet
Under DOE ContractNo DE-AC01-07LM00060
Prepared bySM Stoller Corporation
18-05071403
Well Number and Groundwater Elevation in Feet (amsl)
Monitoring Well
Extraction Well
Surface Sample
Piezometer
Water Level Not Used in Contouring
Water Elevation Contour in Feet (amsl)Contour Interval = 10 Foot
Inferred Water Elevation Contour in Feet (amsl)
Inferred Groundwater Flow Direction
Slurrywall
Fence
Road
Railroad
Tank
Building
Pond
14
Appendix A
Laboratory Reports
March 2013 Semiannual Monitoring
ANALYTICAL REPORT
Job Number 280-39772-1
SDG Number 13025120
Job Description PINELLAS MONITORING
ForSM Stoller Corporation
2597 Legacy WayGrand Junction CO 81503
Attention Mr Steve Donivan
_____________________________________________
Approved for releaseKae E YoderProject Manager II3222013 256 PM
Kae E YoderProject Manager II
kaeyodertestamericainccom03222013
The test results in this report relate only to the samples in this report and meet all requirements of NELAC with anyexceptions noted Pursuant to NELAP this report shall not be reproduced except in full without the written approval ofthe laboratory All questions regarding this report should be directed to the TestAmerica Denver Project Manager
The Lab Certification ID is E87667
Reporting limits are adjusted for sample size used dilutions and moisture content if applicable
TestAmerica Laboratories Inc
TestAmerica Denver 4955 Yarrow Street Arvada CO 80002
Tel (303) 736-0100 Fax (303) 431-7171 wwwtestamericainccom
Page 1 of 962
Pages have been deleted from this laboratory report file to reduce file size The deleted pages contain raw data and instrument calibrations If the full laboratory report is needed contact ScottSurovchaklmdoegov
Table of ContentsCover Title Page 1
Data Summaries 4
Report Narrative 4
Data Qualifiers 5
Sample Summary 6
Executive Summary 7
Method Summary 9
Method Analyst Summary 10
Sample Datasheets 11
Surrogate Summary 71
QC Data Summary 75
QC Association Summary 101
Lab Chronicle 103
Manual Integration Summary 110
Organic Sample Data 132
GCMS VOA 132
Method 8260B 132Method 8260B QC Summary 133Method 8260B Sample Data 157Standards Data 306
Method 8260B ICAL Data 306Method 8260B CCAL Data 429
Raw QC Data 493Method 8260B Tune Data 493Method 8260B Blank Data 514Method 8260B LCSLCSD Data 535
Page 2 of 962
Table of ContentsMethod 8260B MSMSD Data 553
Method 8260B Run Logs 595
Method 8260B SIM 685Method 8260B SIM QC Summary 686Method 8260B SIM Sample Data 713Standards Data 778
Method 8260B SIM ICAL Data 778Method 8260B SIM CCAL Data 836
Raw QC Data 854Method 8260B SIM Tune Data 854Method 8260B SIM Blank Data 869Method 8260B SIM LCSLCSD Data 881Method 8260B SIM MSMSD Data 909
Method 8260B SIM Run Logs 930
Shipping and Receiving Documents 957
Client Chain of Custody 958
Sample Receipt Checklist 960
Page 3 of 962
CASE NARRATIVE
Client SM Stoller Corporation
Project PINELLAS MONITORING - 13025120
Report Number 280-39772-1
With exceptions noted as flags or footnotes standard analytical protocols were followed in the analysis of the samples and no problems
were encountered or anomalies observed All laboratory quality control samples analyzed in conjunction with the samples in this project
were within established control limits with any exceptions noted Calculations are performed before rounding to avoid round-off errors in
calculated results
This report includes reporting limits (RLs) less than TestAmerica Denvers practical quantitation limits These reporting limits are being
used specifically at the clients request to meet the needs of this project Please note that data are not normally reported to these levels
without qualification since they are inherently less reliable and potentially less defensible than required by the current NELAC standards
Results between the method detection limit (MDL) and reporting limit (RL) are flagged with a J qualifier to indicate an estimated value
These results are statistically less reliable than results greater than or equal to the RL and should be considered a qualitative value
All holding times were met and proper preservation noted for the methods performed on these samples unless otherwise detailed in the
individual sections below
RECEIPT
The samples were received on 392013 930 AM the samples arrived in good condition properly preserved and where required on ice
The temperatures of the 2 coolers at receipt time were 26ordm C and 31ordm C
GCMS VOLATILES - SW846 8260B
Due to the nature of the sample matrix (foamy) a reduced aliquot size had to be used for the analysis of several samples The reporting
limits have been elevated accordingly
Due to high constituent concentration reduced aliquot sizes had to be used for the analysis of Vinyl chloride in samples PIN12-0580-2
(LDU 874) PIN12-2450 (LDU 956) PIN12-S67B (LDU 904) and PIN12-S67C (LDU 905) The reporting limits have been elevated
accordingly
Surrogates 12-Dichloroethane-d4 and Dibromofluoromethane were recovered outside the control limits biased low in the 5 mL initial
volume analysis of sample PIN12-0580-2 (LDU 874) The sample was reanalyzed with similar results indicating matrix interference as
the cause for the surrogate recovery outliers
No other anomalies were encountered
GCMS VOLATILES - SW846 8260B SIM - 14-Dioxane
Due to the nature of the sample matrix (foamy) a reduced aliquot size had to be used for the analysis of sample PIN12-S67C (LDU 905)
The reporting limit haS been elevated accordingly
In some cases due to high constituent concentration samples had to be analyzed using reduced aliquot sizes The reporting limits have
been elevated accordingly
Internal standard 14-Dichlorobenzene-d4 failed to meet acceptance criteria for sample PIN12-S67C (LDU 905) As this internal standard
is not associated with the analyte of interest (14-Dioxane) data are reported as is
The MSD aliquot of the MSMSD associated with batch 280-164929 exhibited the percent recovery outside the control limits The LCS
and LCSD were within control limits
MSMSD data is not available for batch 280-164670 due to a QC failure associated with the parent sample requiring reanalysis Method
precision and accuracy have been verified by the acceptable LCSLCSD analysis data
No other anomalies were encountered
Page 4 of 962
DATA REPORTING QUALIFIERS
Client SM Stoller Corporation Job Number 280-39772-1
Lab Section Qualifier Description
Sdg Number 13025120
GCMS VOA
Indicates the analyte was analyzed for but not detectedU
MS or MSD exceeds the control limitsF
Result is less than the RL but greater than or equal to the MDL and the
concentration is an approximate value
J
Surrogate is outside control limitsX
TestAmerica Denver Page 5 of 962
SAMPLE SUMMARY
Client SM Stoller Corporation Job Number 280-39772-1
Sdg Number 13025120
Client Sample IDLab Sample ID Client Matrix Sampled Received
DateTime DateTime
280-39772-1 PIN12-0555A Water 03072013 1605 03092013 0930
280-39772-1MS PIN12-0555A Water 03072013 1605 03092013 0930
280-39772-1MSD PIN12-0555A Water 03072013 1605 03092013 0930
280-39772-2 PIN12-0555B Water 03072013 1640 03092013 0930
280-39772-2MS PIN12-0555B Water 03072013 1640 03092013 0930
280-39772-2MSD PIN12-0555B Water 03072013 1640 03092013 0930
280-39772-3 PIN12-0555C Water 03072013 1740 03092013 0930
280-39772-4 PIN12-0565-1 Water 03062013 0936 03092013 0930
280-39772-5 PIN12-0565-2 Water 03062013 1015 03092013 0930
280-39772-6 PIN12-0565-3 Water 03062013 1110 03092013 0930
280-39772-7 PIN12-0573-1 Water 03062013 1335 03092013 0930
280-39772-8 PIN12-0573-2 Water 03062013 1405 03092013 0930
280-39772-9 PIN12-0573-3 Water 03062013 1440 03092013 0930
280-39772-10 PIN12-0575-1 Water 03062013 1540 03092013 0930
280-39772-11 PIN12-0575-2 Water 03062013 1620 03092013 0930
280-39772-12 PIN12-0580-1 Water 03072013 0935 03092013 0930
280-39772-13 PIN12-0580-2 Water 03072013 1030 03092013 0930
280-39772-14 PIN12-0580-3 Water 03072013 1110 03092013 0930
280-39772-15 PIN12-2450 Water 03072013 1200 03092013 0930
280-39772-16 PIN12-S67B Water 03072013 1315 03092013 0930
280-39772-17 PIN12-S67C Water 03072013 1225 03092013 0930
280-39772-18 PIN12-S67D Water 03072013 1355 03092013 0930
280-39772-19 PIN99-2198 Water 03062013 1200 03092013 0930
TestAmerica Denver Page 6 of 962
EXECUTIVE SUMMARY - Detections
Client SM Stoller Corporation Job Number 280-39772-1
Analyte Result
Reporting
Limit Units Method
Lab Sample ID Client Sample ID
Sdg Number 13025120
Qualifier
280-39772-3 PIN12-0555C
10 ugL 8260B11cis-12-Dichloroethene
10 ugL 8260B043 Jtrans-12-Dichloroethene
280-39772-6 PIN12-0565-3
40 ugL 8260B10 JAcetone
280-39772-8 PIN12-0573-2
40 ugL 8260B18 JAcetone
280-39772-10 PIN12-0575-1
40 ugL 8260B83 JAcetone
10 ugL 8260B SIM1914-Dioxane
280-39772-12 PIN12-0580-1
10 ugL 8260B054 Jcis-12-Dichloroethene
10 ugL 8260B42Vinyl chloride
10 ugL 8260B SIM4014-Dioxane
280-39772-13 PIN12-0580-2
10 ugL 8260B6711-Dichloroethane
10 ugL 8260B18cis-12-Dichloroethene
10 ugL 8260B50trans-12-Dichloroethene
40 ugL 8260B150Vinyl chloride
20 ugL 8260B SIM16014-Dioxane
280-39772-14 PIN12-0580-3
10 ugL 8260B2311-Dichloroethane
10 ugL 8260B12cis-12-Dichloroethene
10 ugL 8260B088 Jtrans-12-Dichloroethene
10 ugL 8260B23Vinyl chloride
20 ugL 8260B SIM2814-Dioxane
280-39772-15 PIN12-2450
10 ugL 8260B6211-Dichloroethane
10 ugL 8260B16cis-12-Dichloroethene
10 ugL 8260B40trans-12-Dichloroethene
40 ugL 8260B150Vinyl chloride
20 ugL 8260B SIM19014-Dioxane
TestAmerica Denver Page 7 of 962
EXECUTIVE SUMMARY - Detections
Client SM Stoller Corporation Job Number 280-39772-1
Analyte Result
Reporting
Limit Units Method
Lab Sample ID Client Sample ID
Sdg Number 13025120
Qualifier
280-39772-16 PIN12-S67B
10 ugL 8260B3211-Dichloroethane
10 ugL 8260B13cis-12-Dichloroethene
10 ugL 8260B33trans-12-Dichloroethene
10 ugL 8260B250Vinyl chloride
10 ugL 8260B SIM9114-Dioxane
280-39772-17 PIN12-S67C
10 ugL 8260B7611-Dichloroethane
10 ugL 8260B48cis-12-Dichloroethene
10 ugL 8260B97trans-12-Dichloroethene
10 ugL 8260B064 J11-Dichloroethene
40 ugL 8260B65Vinyl chloride
280-39772-18 PIN12-S67D
10 ugL 8260B086 J11-Dichloroethane
10 ugL 8260B62cis-12-Dichloroethene
10 ugL 8260B19trans-12-Dichloroethene
10 ugL 8260B11Vinyl chloride
TestAmerica Denver Page 8 of 962
METHOD SUMMARY
Client SM Stoller Corporation Job Number 280-39772-1
Sdg Number 13025120
Preparation MethodMethodLab LocationDescription
Matrix Water
Volatile Organic Compounds (GCMS) TAL DEN SW846 8260B
Purge and Trap TAL DEN SW846 5030B
Volatile Organic Compounds (GCMS-SIM) TAL DEN SW846 8260B SIM
Purge and Trap TAL DEN SW846 5030B
Lab References
TAL DEN = TestAmerica Denver
Method References
SW846 = Test Methods For Evaluating Solid Waste PhysicalChemical Methods Third Edition November 1986 And Its Updates
TestAmerica Denver Page 9 of 962
METHOD ANALYST SUMMARY
Client SM Stoller Corporation Job Number 280-39772-1
Method Analyst Analyst ID
Sdg Number 13025120
Berger Brent BBSW846 8260B
Dobransky Michael E MDSW846 8260B
Moan Matthew R MRMSW846 8260B
Tinkham Sarah A SATSW846 8260B SIM
TestAmerica Denver
Page 10 of 962
Analytical Data
Client SM Stoller Corporation Job Number 280-39772-1
Sdg Number 13025120
Client Sample ID
Lab Sample ID
PIN12-0555A
Client Matrix
280-39772-1
Water
Date Sampled 03072013 1605
Date Received 03092013 0930
8260B Volatile Organic Compounds (GCMS)
Dilution
03142013 2211
03142013 2211
10
8260B
Final WeightVolume
Initial WeightVolume
Lab File ID
Instrument ID
RR1862D
20 mL
20 mL
5030B
VMS_R2
Analysis Date
Prep Date
Analysis Batch
Prep Batch
280-164920
NA
Analysis Method
Prep Method
Analyte Result (ugL) Qualifier MDL RL
19 U 1019Acetone
016 U 10016Benzene
017 U 10017Bromobenzene
010 U 10010Bromochloromethane
017 U 10017Bromodichloromethane
019 U 10019Bromoform
021 U 10021Bromomethane
20 U 50202-Butanone (MEK)
032 U 10032n-Butylbenzene
017 U 10017sec-Butylbenzene
016 U 10016tert-Butylbenzene
045 U 10045Carbon disulfide
019 U 10019Carbon tetrachloride
017 U 10017Chlorobenzene
017 U 10017Dibromochloromethane
041 U 10041Chloroethane
016 U 10016Chloroform
030 U 10030Chloromethane
017 U 100172-Chlorotoluene
021 U 100214-Chlorotoluene
047 U 1004712-Dibromo-3-Chloropropane
017 U 10017Dibromomethane
015 U 1001512-Dichlorobenzene
013 U 1001313-Dichlorobenzene
016 U 1001614-Dichlorobenzene
031 U 10031Dichlorodifluoromethane
022 U 1002211-Dichloroethane
013 U 1001312-Dichloroethane
015 U 10015cis-12-Dichloroethene
015 U 10015trans-12-Dichloroethene
023 U 1002311-Dichloroethene
018 U 1001812-Dichloropropane
022 U 1002213-Dichloropropane
018 U 1001822-Dichloropropane
016 U 10016cis-13-Dichloropropene
019 U 10019trans-13-Dichloropropene
019 U 1001911-Dichloropropene
016 U 10016Ethylbenzene
036 U 10036Hexachlorobutadiene
17 U 50172-Hexanone
019 U 10019Isopropylbenzene
020 U 100204-Isopropyltoluene
032 U 10032Methylene Chloride
098 U 500984-Methyl-2-pentanone
022 U 10022Naphthalene
016 U 10016n-Propylbenzene
TestAmerica Denver Page 11 of 962
Analytical Data
Client SM Stoller Corporation Job Number 280-39772-1
Sdg Number 13025120
Client Sample ID
Lab Sample ID
PIN12-0555A
Client Matrix
280-39772-1
Water
Date Sampled 03072013 1605
Date Received 03092013 0930
8260B Volatile Organic Compounds (GCMS)
Dilution
03142013 2211
03142013 2211
10
8260B
Final WeightVolume
Initial WeightVolume
Lab File ID
Instrument ID
RR1862D
20 mL
20 mL
5030B
VMS_R2
Analysis Date
Prep Date
Analysis Batch
Prep Batch
280-164920
NA
Analysis Method
Prep Method
Analyte Result (ugL) Qualifier MDL RL
017 U 10017Styrene
021 U 100211112-Tetrachloroethane
021 U 100211122-Tetrachloroethane
020 U 10020Tetrachloroethene
017 U 10017Toluene
021 U 10021123-Trichlorobenzene
021 U 10021124-Trichlorobenzene
016 U 10016111-Trichloroethane
027 U 10027112-Trichloroethane
016 U 10016Trichloroethene
029 U 10029Trichlorofluoromethane
033 U 10033123-Trichloropropane
015 U 10015124-Trimethylbenzene
016 U 10016135-Trimethylbenzene
010 U 10010Vinyl chloride
019 U 10019Xylenes Total
018 U 1001812-Dibromoethane
Surrogate Rec Acceptance LimitsQualifier
75 70 - 12712-Dichloroethane-d4 (Surr)
96 80 - 125Toluene-d8 (Surr)
90 78 - 1204-Bromofluorobenzene (Surr)
85 77 - 120Dibromofluoromethane (Surr)
TestAmerica Denver Page 12 of 962
Analytical Data
Client SM Stoller Corporation Job Number 280-39772-1
Sdg Number 13025120
Client Sample ID
Lab Sample ID
PIN12-0555B
Client Matrix
280-39772-2
Water
Date Sampled 03072013 1640
Date Received 03092013 0930
8260B Volatile Organic Compounds (GCMS)
Dilution
03142013 2234
03142013 2234
10
8260B
Final WeightVolume
Initial WeightVolume
Lab File ID
Instrument ID
RR1863D
20 mL
20 mL
5030B
VMS_R2
Analysis Date
Prep Date
Analysis Batch
Prep Batch
280-164920
NA
Analysis Method
Prep Method
Analyte Result (ugL) Qualifier MDL RL
19 U 1019Acetone
016 U 10016Benzene
017 U 10017Bromobenzene
010 U 10010Bromochloromethane
017 U 10017Bromodichloromethane
019 U 10019Bromoform
021 U 10021Bromomethane
20 U 50202-Butanone (MEK)
032 U 10032n-Butylbenzene
017 U 10017sec-Butylbenzene
016 U 10016tert-Butylbenzene
045 U 10045Carbon disulfide
019 U 10019Carbon tetrachloride
017 U 10017Chlorobenzene
017 U 10017Dibromochloromethane
041 U 10041Chloroethane
016 U 10016Chloroform
030 U 10030Chloromethane
017 U 100172-Chlorotoluene
021 U 100214-Chlorotoluene
047 U 1004712-Dibromo-3-Chloropropane
017 U 10017Dibromomethane
015 U 1001512-Dichlorobenzene
013 U 1001313-Dichlorobenzene
016 U 1001614-Dichlorobenzene
031 U 10031Dichlorodifluoromethane
022 U 1002211-Dichloroethane
013 U 1001312-Dichloroethane
015 U 10015cis-12-Dichloroethene
015 U 10015trans-12-Dichloroethene
023 U 1002311-Dichloroethene
018 U 1001812-Dichloropropane
022 U 1002213-Dichloropropane
018 U 1001822-Dichloropropane
016 U 10016cis-13-Dichloropropene
019 U 10019trans-13-Dichloropropene
019 U 1001911-Dichloropropene
016 U 10016Ethylbenzene
036 U 10036Hexachlorobutadiene
17 U 50172-Hexanone
019 U 10019Isopropylbenzene
020 U 100204-Isopropyltoluene
032 U 10032Methylene Chloride
098 U 500984-Methyl-2-pentanone
022 U 10022Naphthalene
016 U 10016n-Propylbenzene
TestAmerica Denver Page 13 of 962
Analytical Data
Client SM Stoller Corporation Job Number 280-39772-1
Sdg Number 13025120
Client Sample ID
Lab Sample ID
PIN12-0555B
Client Matrix
280-39772-2
Water
Date Sampled 03072013 1640
Date Received 03092013 0930
8260B Volatile Organic Compounds (GCMS)
Dilution
03142013 2234
03142013 2234
10
8260B
Final WeightVolume
Initial WeightVolume
Lab File ID
Instrument ID
RR1863D
20 mL
20 mL
5030B
VMS_R2
Analysis Date
Prep Date
Analysis Batch
Prep Batch
280-164920
NA
Analysis Method
Prep Method
Analyte Result (ugL) Qualifier MDL RL
017 U 10017Styrene
021 U 100211112-Tetrachloroethane
021 U 100211122-Tetrachloroethane
020 U 10020Tetrachloroethene
017 U 10017Toluene
021 U 10021123-Trichlorobenzene
021 U 10021124-Trichlorobenzene
016 U 10016111-Trichloroethane
027 U 10027112-Trichloroethane
016 U 10016Trichloroethene
029 U 10029Trichlorofluoromethane
033 U 10033123-Trichloropropane
015 U 10015124-Trimethylbenzene
016 U 10016135-Trimethylbenzene
010 U 10010Vinyl chloride
019 U 10019Xylenes Total
018 U 1001812-Dibromoethane
Surrogate Rec Acceptance LimitsQualifier
84 70 - 12712-Dichloroethane-d4 (Surr)
92 80 - 125Toluene-d8 (Surr)
89 78 - 1204-Bromofluorobenzene (Surr)
89 77 - 120Dibromofluoromethane (Surr)
TestAmerica Denver Page 14 of 962
Analytical Data
Client SM Stoller Corporation Job Number 280-39772-1
Sdg Number 13025120
Client Sample ID
Lab Sample ID
PIN12-0555C
Client Matrix
280-39772-3
Water
Date Sampled 03072013 1740
Date Received 03092013 0930
8260B Volatile Organic Compounds (GCMS)
Dilution
03152013 0116
03152013 0116
10
8260B
Final WeightVolume
Initial WeightVolume
Lab File ID
Instrument ID
RR1870D
20 mL
20 mL
5030B
VMS_R2
Analysis Date
Prep Date
Analysis Batch
Prep Batch
280-164920
NA
Analysis Method
Prep Method
Analyte Result (ugL) Qualifier MDL RL
19 U 1019Acetone
016 U 10016Benzene
017 U 10017Bromobenzene
010 U 10010Bromochloromethane
017 U 10017Bromodichloromethane
019 U 10019Bromoform
021 U 10021Bromomethane
20 U 50202-Butanone (MEK)
032 U 10032n-Butylbenzene
017 U 10017sec-Butylbenzene
016 U 10016tert-Butylbenzene
045 U 10045Carbon disulfide
019 U 10019Carbon tetrachloride
017 U 10017Chlorobenzene
017 U 10017Dibromochloromethane
041 U 10041Chloroethane
016 U 10016Chloroform
030 U 10030Chloromethane
017 U 100172-Chlorotoluene
021 U 100214-Chlorotoluene
047 U 1004712-Dibromo-3-Chloropropane
017 U 10017Dibromomethane
015 U 1001512-Dichlorobenzene
013 U 1001313-Dichlorobenzene
016 U 1001614-Dichlorobenzene
031 U 10031Dichlorodifluoromethane
022 U 1002211-Dichloroethane
013 U 1001312-Dichloroethane
11 10015cis-12-Dichloroethene
043 J 10015trans-12-Dichloroethene
023 U 1002311-Dichloroethene
018 U 1001812-Dichloropropane
022 U 1002213-Dichloropropane
018 U 1001822-Dichloropropane
016 U 10016cis-13-Dichloropropene
019 U 10019trans-13-Dichloropropene
019 U 1001911-Dichloropropene
016 U 10016Ethylbenzene
036 U 10036Hexachlorobutadiene
17 U 50172-Hexanone
019 U 10019Isopropylbenzene
020 U 100204-Isopropyltoluene
032 U 10032Methylene Chloride
098 U 500984-Methyl-2-pentanone
022 U 10022Naphthalene
016 U 10016n-Propylbenzene
TestAmerica Denver Page 15 of 962
Analytical Data
Client SM Stoller Corporation Job Number 280-39772-1
Sdg Number 13025120
Client Sample ID
Lab Sample ID
PIN12-0555C
Client Matrix
280-39772-3
Water
Date Sampled 03072013 1740
Date Received 03092013 0930
8260B Volatile Organic Compounds (GCMS)
Dilution
03152013 0116
03152013 0116
10
8260B
Final WeightVolume
Initial WeightVolume
Lab File ID
Instrument ID
RR1870D
20 mL
20 mL
5030B
VMS_R2
Analysis Date
Prep Date
Analysis Batch
Prep Batch
280-164920
NA
Analysis Method
Prep Method
Analyte Result (ugL) Qualifier MDL RL
017 U 10017Styrene
021 U 100211112-Tetrachloroethane
021 U 100211122-Tetrachloroethane
020 U 10020Tetrachloroethene
017 U 10017Toluene
021 U 10021123-Trichlorobenzene
021 U 10021124-Trichlorobenzene
016 U 10016111-Trichloroethane
027 U 10027112-Trichloroethane
016 U 10016Trichloroethene
029 U 10029Trichlorofluoromethane
033 U 10033123-Trichloropropane
015 U 10015124-Trimethylbenzene
016 U 10016135-Trimethylbenzene
010 U 10010Vinyl chloride
019 U 10019Xylenes Total
018 U 1001812-Dibromoethane
Surrogate Rec Acceptance LimitsQualifier
101 70 - 12712-Dichloroethane-d4 (Surr)
105 80 - 125Toluene-d8 (Surr)
103 78 - 1204-Bromofluorobenzene (Surr)
106 77 - 120Dibromofluoromethane (Surr)
TestAmerica Denver Page 16 of 962
Analytical Data
Client SM Stoller Corporation Job Number 280-39772-1
Sdg Number 13025120
Client Sample ID
Lab Sample ID
PIN12-0565-1
Client Matrix
280-39772-4
Water
Date Sampled 03062013 0936
Date Received 03092013 0930
8260B Volatile Organic Compounds (GCMS)
Dilution
03152013 1426
03152013 1426
10
8260B
Final WeightVolume
Initial WeightVolume
Lab File ID
Instrument ID
g2_6154D
5 mL
20 mL
5030B
VMS_G2
Analysis Date
Prep Date
Analysis Batch
Prep Batch
280-164934
NA
Analysis Method
Prep Method
Analyte Result (ugL) Qualifier MDL RL
76 U 4076Acetone
064 U 40064Benzene
068 U 40068Bromobenzene
040 U 40040Bromochloromethane
068 U 40068Bromodichloromethane
076 U 40076Bromoform
084 U 40084Bromomethane
80 U 20802-Butanone (MEK)
13 U 4013n-Butylbenzene
068 U 40068sec-Butylbenzene
064 U 40064tert-Butylbenzene
18 U 4018Carbon disulfide
076 U 40076Carbon tetrachloride
068 U 40068Chlorobenzene
068 U 40068Dibromochloromethane
16 U 4016Chloroethane
064 U 40064Chloroform
12 U 4012Chloromethane
068 U 400682-Chlorotoluene
084 U 400844-Chlorotoluene
19 U 401912-Dibromo-3-Chloropropane
068 U 40068Dibromomethane
060 U 4006012-Dichlorobenzene
052 U 4005213-Dichlorobenzene
064 U 4006414-Dichlorobenzene
12 U 4012Dichlorodifluoromethane
088 U 4008811-Dichloroethane
052 U 4005212-Dichloroethane
060 U 40060cis-12-Dichloroethene
060 U 40060trans-12-Dichloroethene
092 U 4009211-Dichloroethene
072 U 4007212-Dichloropropane
088 U 4008813-Dichloropropane
072 U 4007222-Dichloropropane
064 U 40064cis-13-Dichloropropene
076 U 40076trans-13-Dichloropropene
076 U 4007611-Dichloropropene
064 U 40064Ethylbenzene
14 U 4014Hexachlorobutadiene
68 U 20682-Hexanone
076 U 40076Isopropylbenzene
080 U 400804-Isopropyltoluene
13 U 4013Methylene Chloride
39 U 20394-Methyl-2-pentanone
088 U 40088Naphthalene
064 U 40064n-Propylbenzene
TestAmerica Denver Page 17 of 962
Analytical Data
Client SM Stoller Corporation Job Number 280-39772-1
Sdg Number 13025120
Client Sample ID
Lab Sample ID
PIN12-0565-1
Client Matrix
280-39772-4
Water
Date Sampled 03062013 0936
Date Received 03092013 0930
8260B Volatile Organic Compounds (GCMS)
Dilution
03152013 1426
03152013 1426
10
8260B
Final WeightVolume
Initial WeightVolume
Lab File ID
Instrument ID
g2_6154D
5 mL
20 mL
5030B
VMS_G2
Analysis Date
Prep Date
Analysis Batch
Prep Batch
280-164934
NA
Analysis Method
Prep Method
Analyte Result (ugL) Qualifier MDL RL
068 U 40068Styrene
084 U 400841112-Tetrachloroethane
084 U 400841122-Tetrachloroethane
080 U 40080Tetrachloroethene
068 U 40068Toluene
084 U 40084123-Trichlorobenzene
084 U 40084124-Trichlorobenzene
064 U 40064111-Trichloroethane
11 U 4011112-Trichloroethane
064 U 40064Trichloroethene
12 U 4012Trichlorofluoromethane
13 U 4013123-Trichloropropane
060 U 40060124-Trimethylbenzene
064 U 40064135-Trimethylbenzene
040 U 40040Vinyl chloride
076 U 40076Xylenes Total
072 U 4007212-Dibromoethane
Surrogate Rec Acceptance LimitsQualifier
87 70 - 12712-Dichloroethane-d4 (Surr)
94 80 - 125Toluene-d8 (Surr)
88 78 - 1204-Bromofluorobenzene (Surr)
94 77 - 120Dibromofluoromethane (Surr)
TestAmerica Denver Page 18 of 962
Analytical Data
Client SM Stoller Corporation Job Number 280-39772-1
Sdg Number 13025120
Client Sample ID
Lab Sample ID
PIN12-0565-2
Client Matrix
280-39772-5
Water
Date Sampled 03062013 1015
Date Received 03092013 0930
8260B Volatile Organic Compounds (GCMS)
Dilution
03152013 1445
03152013 1445
10
8260B
Final WeightVolume
Initial WeightVolume
Lab File ID
Instrument ID
g2_6155D
5 mL
20 mL
5030B
VMS_G2
Analysis Date
Prep Date
Analysis Batch
Prep Batch
280-164934
NA
Analysis Method
Prep Method
Analyte Result (ugL) Qualifier MDL RL
76 U 4076Acetone
064 U 40064Benzene
068 U 40068Bromobenzene
040 U 40040Bromochloromethane
068 U 40068Bromodichloromethane
076 U 40076Bromoform
084 U 40084Bromomethane
80 U 20802-Butanone (MEK)
13 U 4013n-Butylbenzene
068 U 40068sec-Butylbenzene
064 U 40064tert-Butylbenzene
18 U 4018Carbon disulfide
076 U 40076Carbon tetrachloride
068 U 40068Chlorobenzene
068 U 40068Dibromochloromethane
16 U 4016Chloroethane
064 U 40064Chloroform
12 U 4012Chloromethane
068 U 400682-Chlorotoluene
084 U 400844-Chlorotoluene
19 U 401912-Dibromo-3-Chloropropane
068 U 40068Dibromomethane
060 U 4006012-Dichlorobenzene
052 U 4005213-Dichlorobenzene
064 U 4006414-Dichlorobenzene
12 U 4012Dichlorodifluoromethane
088 U 4008811-Dichloroethane
052 U 4005212-Dichloroethane
060 U 40060cis-12-Dichloroethene
060 U 40060trans-12-Dichloroethene
092 U 4009211-Dichloroethene
072 U 4007212-Dichloropropane
088 U 4008813-Dichloropropane
072 U 4007222-Dichloropropane
064 U 40064cis-13-Dichloropropene
076 U 40076trans-13-Dichloropropene
076 U 4007611-Dichloropropene
064 U 40064Ethylbenzene
14 U 4014Hexachlorobutadiene
68 U 20682-Hexanone
076 U 40076Isopropylbenzene
080 U 400804-Isopropyltoluene
13 U 4013Methylene Chloride
39 U 20394-Methyl-2-pentanone
088 U 40088Naphthalene
064 U 40064n-Propylbenzene
TestAmerica Denver Page 19 of 962
Analytical Data
Client SM Stoller Corporation Job Number 280-39772-1
Sdg Number 13025120
Client Sample ID
Lab Sample ID
PIN12-0565-2
Client Matrix
280-39772-5
Water
Date Sampled 03062013 1015
Date Received 03092013 0930
8260B Volatile Organic Compounds (GCMS)
Dilution
03152013 1445
03152013 1445
10
8260B
Final WeightVolume
Initial WeightVolume
Lab File ID
Instrument ID
g2_6155D
5 mL
20 mL
5030B
VMS_G2
Analysis Date
Prep Date
Analysis Batch
Prep Batch
280-164934
NA
Analysis Method
Prep Method
Analyte Result (ugL) Qualifier MDL RL
068 U 40068Styrene
084 U 400841112-Tetrachloroethane
084 U 400841122-Tetrachloroethane
080 U 40080Tetrachloroethene
068 U 40068Toluene
084 U 40084123-Trichlorobenzene
084 U 40084124-Trichlorobenzene
064 U 40064111-Trichloroethane
11 U 4011112-Trichloroethane
064 U 40064Trichloroethene
12 U 4012Trichlorofluoromethane
13 U 4013123-Trichloropropane
060 U 40060124-Trimethylbenzene
064 U 40064135-Trimethylbenzene
040 U 40040Vinyl chloride
076 U 40076Xylenes Total
072 U 4007212-Dibromoethane
Surrogate Rec Acceptance LimitsQualifier
87 70 - 12712-Dichloroethane-d4 (Surr)
91 80 - 125Toluene-d8 (Surr)
90 78 - 1204-Bromofluorobenzene (Surr)
90 77 - 120Dibromofluoromethane (Surr)
TestAmerica Denver Page 20 of 962
Analytical Data
Client SM Stoller Corporation Job Number 280-39772-1
Sdg Number 13025120
Client Sample ID
Lab Sample ID
PIN12-0565-3
Client Matrix
280-39772-6
Water
Date Sampled 03062013 1110
Date Received 03092013 0930
8260B Volatile Organic Compounds (GCMS)
Dilution
03152013 1504
03152013 1504
10
8260B
Final WeightVolume
Initial WeightVolume
Lab File ID
Instrument ID
g2_6156D
5 mL
20 mL
5030B
VMS_G2
Analysis Date
Prep Date
Analysis Batch
Prep Batch
280-164934
NA
Analysis Method
Prep Method
Analyte Result (ugL) Qualifier MDL RL
10 J 4076Acetone
064 U 40064Benzene
068 U 40068Bromobenzene
040 U 40040Bromochloromethane
068 U 40068Bromodichloromethane
076 U 40076Bromoform
084 U 40084Bromomethane
80 U 20802-Butanone (MEK)
13 U 4013n-Butylbenzene
068 U 40068sec-Butylbenzene
064 U 40064tert-Butylbenzene
18 U 4018Carbon disulfide
076 U 40076Carbon tetrachloride
068 U 40068Chlorobenzene
068 U 40068Dibromochloromethane
16 U 4016Chloroethane
064 U 40064Chloroform
12 U 4012Chloromethane
068 U 400682-Chlorotoluene
084 U 400844-Chlorotoluene
19 U 401912-Dibromo-3-Chloropropane
068 U 40068Dibromomethane
060 U 4006012-Dichlorobenzene
052 U 4005213-Dichlorobenzene
064 U 4006414-Dichlorobenzene
12 U 4012Dichlorodifluoromethane
088 U 4008811-Dichloroethane
052 U 4005212-Dichloroethane
060 U 40060cis-12-Dichloroethene
060 U 40060trans-12-Dichloroethene
092 U 4009211-Dichloroethene
072 U 4007212-Dichloropropane
088 U 4008813-Dichloropropane
072 U 4007222-Dichloropropane
064 U 40064cis-13-Dichloropropene
076 U 40076trans-13-Dichloropropene
076 U 4007611-Dichloropropene
064 U 40064Ethylbenzene
14 U 4014Hexachlorobutadiene
68 U 20682-Hexanone
076 U 40076Isopropylbenzene
080 U 400804-Isopropyltoluene
13 U 4013Methylene Chloride
39 U 20394-Methyl-2-pentanone
088 U 40088Naphthalene
064 U 40064n-Propylbenzene
TestAmerica Denver Page 21 of 962
Analytical Data
Client SM Stoller Corporation Job Number 280-39772-1
Sdg Number 13025120
Client Sample ID
Lab Sample ID
PIN12-0565-3
Client Matrix
280-39772-6
Water
Date Sampled 03062013 1110
Date Received 03092013 0930
8260B Volatile Organic Compounds (GCMS)
Dilution
03152013 1504
03152013 1504
10
8260B
Final WeightVolume
Initial WeightVolume
Lab File ID
Instrument ID
g2_6156D
5 mL
20 mL
5030B
VMS_G2
Analysis Date
Prep Date
Analysis Batch
Prep Batch
280-164934
NA
Analysis Method
Prep Method
Analyte Result (ugL) Qualifier MDL RL
068 U 40068Styrene
084 U 400841112-Tetrachloroethane
084 U 400841122-Tetrachloroethane
080 U 40080Tetrachloroethene
068 U 40068Toluene
084 U 40084123-Trichlorobenzene
084 U 40084124-Trichlorobenzene
064 U 40064111-Trichloroethane
11 U 4011112-Trichloroethane
064 U 40064Trichloroethene
12 U 4012Trichlorofluoromethane
13 U 4013123-Trichloropropane
060 U 40060124-Trimethylbenzene
064 U 40064135-Trimethylbenzene
040 U 40040Vinyl chloride
076 U 40076Xylenes Total
072 U 4007212-Dibromoethane
Surrogate Rec Acceptance LimitsQualifier
87 70 - 12712-Dichloroethane-d4 (Surr)
94 80 - 125Toluene-d8 (Surr)
90 78 - 1204-Bromofluorobenzene (Surr)
94 77 - 120Dibromofluoromethane (Surr)
TestAmerica Denver Page 22 of 962
Analytical Data
Client SM Stoller Corporation Job Number 280-39772-1
Sdg Number 13025120
Client Sample ID
Lab Sample ID
PIN12-0573-1
Client Matrix
280-39772-7
Water
Date Sampled 03062013 1335
Date Received 03092013 0930
8260B Volatile Organic Compounds (GCMS)
Dilution
03152013 1232
03152013 1232
10
8260B
Final WeightVolume
Initial WeightVolume
Lab File ID
Instrument ID
g2_6148D
5 mL
20 mL
5030B
VMS_G2
Analysis Date
Prep Date
Analysis Batch
Prep Batch
280-164934
NA
Analysis Method
Prep Method
Analyte Result (ugL) Qualifier MDL RL
76 U 4076Acetone
064 U 40064Benzene
068 U 40068Bromobenzene
040 U 40040Bromochloromethane
068 U 40068Bromodichloromethane
076 U 40076Bromoform
084 U 40084Bromomethane
80 U 20802-Butanone (MEK)
13 U 4013n-Butylbenzene
068 U 40068sec-Butylbenzene
064 U 40064tert-Butylbenzene
18 U 4018Carbon disulfide
076 U 40076Carbon tetrachloride
068 U 40068Chlorobenzene
068 U 40068Dibromochloromethane
16 U 4016Chloroethane
064 U 40064Chloroform
12 U 4012Chloromethane
068 U 400682-Chlorotoluene
084 U 400844-Chlorotoluene
19 U 401912-Dibromo-3-Chloropropane
068 U 40068Dibromomethane
060 U 4006012-Dichlorobenzene
052 U 4005213-Dichlorobenzene
064 U 4006414-Dichlorobenzene
12 U 4012Dichlorodifluoromethane
088 U 4008811-Dichloroethane
052 U 4005212-Dichloroethane
060 U 40060cis-12-Dichloroethene
060 U 40060trans-12-Dichloroethene
092 U 4009211-Dichloroethene
072 U 4007212-Dichloropropane
088 U 4008813-Dichloropropane
072 U 4007222-Dichloropropane
064 U 40064cis-13-Dichloropropene
076 U 40076trans-13-Dichloropropene
076 U 4007611-Dichloropropene
064 U 40064Ethylbenzene
14 U 4014Hexachlorobutadiene
68 U 20682-Hexanone
076 U 40076Isopropylbenzene
080 U 400804-Isopropyltoluene
13 U 4013Methylene Chloride
39 U 20394-Methyl-2-pentanone
088 U 40088Naphthalene
064 U 40064n-Propylbenzene
TestAmerica Denver Page 23 of 962
Analytical Data
Client SM Stoller Corporation Job Number 280-39772-1
Sdg Number 13025120
Client Sample ID
Lab Sample ID
PIN12-0573-1
Client Matrix
280-39772-7
Water
Date Sampled 03062013 1335
Date Received 03092013 0930
8260B Volatile Organic Compounds (GCMS)
Dilution
03152013 1232
03152013 1232
10
8260B
Final WeightVolume
Initial WeightVolume
Lab File ID
Instrument ID
g2_6148D
5 mL
20 mL
5030B
VMS_G2
Analysis Date
Prep Date
Analysis Batch
Prep Batch
280-164934
NA
Analysis Method
Prep Method
Analyte Result (ugL) Qualifier MDL RL
068 U 40068Styrene
084 U 400841112-Tetrachloroethane
084 U 400841122-Tetrachloroethane
080 U 40080Tetrachloroethene
068 U 40068Toluene
084 U 40084123-Trichlorobenzene
084 U 40084124-Trichlorobenzene
064 U 40064111-Trichloroethane
11 U 4011112-Trichloroethane
064 U 40064Trichloroethene
12 U 4012Trichlorofluoromethane
13 U 4013123-Trichloropropane
060 U 40060124-Trimethylbenzene
064 U 40064135-Trimethylbenzene
040 U 40040Vinyl chloride
076 U 40076Xylenes Total
072 U 4007212-Dibromoethane
Surrogate Rec Acceptance LimitsQualifier
85 70 - 12712-Dichloroethane-d4 (Surr)
93 80 - 125Toluene-d8 (Surr)
90 78 - 1204-Bromofluorobenzene (Surr)
90 77 - 120Dibromofluoromethane (Surr)
TestAmerica Denver Page 24 of 962
Analytical Data
Client SM Stoller Corporation Job Number 280-39772-1
Sdg Number 13025120
Client Sample ID
Lab Sample ID
PIN12-0573-2
Client Matrix
280-39772-8
Water
Date Sampled 03062013 1405
Date Received 03092013 0930
8260B Volatile Organic Compounds (GCMS)
Dilution
03152013 1251
03152013 1251
10
8260B
Final WeightVolume
Initial WeightVolume
Lab File ID
Instrument ID
g2_6149D
5 mL
20 mL
5030B
VMS_G2
Analysis Date
Prep Date
Analysis Batch
Prep Batch
280-164934
NA
Analysis Method
Prep Method
Analyte Result (ugL) Qualifier MDL RL
18 J 4076Acetone
064 U 40064Benzene
068 U 40068Bromobenzene
040 U 40040Bromochloromethane
068 U 40068Bromodichloromethane
076 U 40076Bromoform
084 U 40084Bromomethane
80 U 20802-Butanone (MEK)
13 U 4013n-Butylbenzene
068 U 40068sec-Butylbenzene
064 U 40064tert-Butylbenzene
18 U 4018Carbon disulfide
076 U 40076Carbon tetrachloride
068 U 40068Chlorobenzene
068 U 40068Dibromochloromethane
16 U 4016Chloroethane
064 U 40064Chloroform
12 U 4012Chloromethane
068 U 400682-Chlorotoluene
084 U 400844-Chlorotoluene
19 U 401912-Dibromo-3-Chloropropane
068 U 40068Dibromomethane
060 U 4006012-Dichlorobenzene
052 U 4005213-Dichlorobenzene
064 U 4006414-Dichlorobenzene
12 U 4012Dichlorodifluoromethane
088 U 4008811-Dichloroethane
052 U 4005212-Dichloroethane
060 U 40060cis-12-Dichloroethene
060 U 40060trans-12-Dichloroethene
092 U 4009211-Dichloroethene
072 U 4007212-Dichloropropane
088 U 4008813-Dichloropropane
072 U 4007222-Dichloropropane
064 U 40064cis-13-Dichloropropene
076 U 40076trans-13-Dichloropropene
076 U 4007611-Dichloropropene
064 U 40064Ethylbenzene
14 U 4014Hexachlorobutadiene
68 U 20682-Hexanone
076 U 40076Isopropylbenzene
080 U 400804-Isopropyltoluene
13 U 4013Methylene Chloride
39 U 20394-Methyl-2-pentanone
088 U 40088Naphthalene
064 U 40064n-Propylbenzene
TestAmerica Denver Page 25 of 962
Analytical Data
Client SM Stoller Corporation Job Number 280-39772-1
Sdg Number 13025120
Client Sample ID
Lab Sample ID
PIN12-0573-2
Client Matrix
280-39772-8
Water
Date Sampled 03062013 1405
Date Received 03092013 0930
8260B Volatile Organic Compounds (GCMS)
Dilution
03152013 1251
03152013 1251
10
8260B
Final WeightVolume
Initial WeightVolume
Lab File ID
Instrument ID
g2_6149D
5 mL
20 mL
5030B
VMS_G2
Analysis Date
Prep Date
Analysis Batch
Prep Batch
280-164934
NA
Analysis Method
Prep Method
Analyte Result (ugL) Qualifier MDL RL
068 U 40068Styrene
084 U 400841112-Tetrachloroethane
084 U 400841122-Tetrachloroethane
080 U 40080Tetrachloroethene
068 U 40068Toluene
084 U 40084123-Trichlorobenzene
084 U 40084124-Trichlorobenzene
064 U 40064111-Trichloroethane
11 U 4011112-Trichloroethane
064 U 40064Trichloroethene
12 U 4012Trichlorofluoromethane
13 U 4013123-Trichloropropane
060 U 40060124-Trimethylbenzene
064 U 40064135-Trimethylbenzene
040 U 40040Vinyl chloride
076 U 40076Xylenes Total
072 U 4007212-Dibromoethane
Surrogate Rec Acceptance LimitsQualifier
85 70 - 12712-Dichloroethane-d4 (Surr)
95 80 - 125Toluene-d8 (Surr)
91 78 - 1204-Bromofluorobenzene (Surr)
91 77 - 120Dibromofluoromethane (Surr)
TestAmerica Denver Page 26 of 962
Analytical Data
Client SM Stoller Corporation Job Number 280-39772-1
Sdg Number 13025120
Client Sample ID
Lab Sample ID
PIN12-0573-3
Client Matrix
280-39772-9
Water
Date Sampled 03062013 1440
Date Received 03092013 0930
8260B Volatile Organic Compounds (GCMS)
Dilution
03152013 1310
03152013 1310
10
8260B
Final WeightVolume
Initial WeightVolume
Lab File ID
Instrument ID
g2_6150D
5 mL
20 mL
5030B
VMS_G2
Analysis Date
Prep Date
Analysis Batch
Prep Batch
280-164934
NA
Analysis Method
Prep Method
Analyte Result (ugL) Qualifier MDL RL
76 U 4076Acetone
064 U 40064Benzene
068 U 40068Bromobenzene
040 U 40040Bromochloromethane
068 U 40068Bromodichloromethane
076 U 40076Bromoform
084 U 40084Bromomethane
80 U 20802-Butanone (MEK)
13 U 4013n-Butylbenzene
068 U 40068sec-Butylbenzene
064 U 40064tert-Butylbenzene
18 U 4018Carbon disulfide
076 U 40076Carbon tetrachloride
068 U 40068Chlorobenzene
068 U 40068Dibromochloromethane
16 U 4016Chloroethane
064 U 40064Chloroform
12 U 4012Chloromethane
068 U 400682-Chlorotoluene
084 U 400844-Chlorotoluene
19 U 401912-Dibromo-3-Chloropropane
068 U 40068Dibromomethane
060 U 4006012-Dichlorobenzene
052 U 4005213-Dichlorobenzene
064 U 4006414-Dichlorobenzene
12 U 4012Dichlorodifluoromethane
088 U 4008811-Dichloroethane
052 U 4005212-Dichloroethane
060 U 40060cis-12-Dichloroethene
060 U 40060trans-12-Dichloroethene
092 U 4009211-Dichloroethene
072 U 4007212-Dichloropropane
088 U 4008813-Dichloropropane
072 U 4007222-Dichloropropane
064 U 40064cis-13-Dichloropropene
076 U 40076trans-13-Dichloropropene
076 U 4007611-Dichloropropene
064 U 40064Ethylbenzene
14 U 4014Hexachlorobutadiene
68 U 20682-Hexanone
076 U 40076Isopropylbenzene
080 U 400804-Isopropyltoluene
13 U 4013Methylene Chloride
39 U 20394-Methyl-2-pentanone
088 U 40088Naphthalene
064 U 40064n-Propylbenzene
TestAmerica Denver Page 27 of 962
Analytical Data
Client SM Stoller Corporation Job Number 280-39772-1
Sdg Number 13025120
Client Sample ID
Lab Sample ID
PIN12-0573-3
Client Matrix
280-39772-9
Water
Date Sampled 03062013 1440
Date Received 03092013 0930
8260B Volatile Organic Compounds (GCMS)
Dilution
03152013 1310
03152013 1310
10
8260B
Final WeightVolume
Initial WeightVolume
Lab File ID
Instrument ID
g2_6150D
5 mL
20 mL
5030B
VMS_G2
Analysis Date
Prep Date
Analysis Batch
Prep Batch
280-164934
NA
Analysis Method
Prep Method
Analyte Result (ugL) Qualifier MDL RL
068 U 40068Styrene
084 U 400841112-Tetrachloroethane
084 U 400841122-Tetrachloroethane
080 U 40080Tetrachloroethene
068 U 40068Toluene
084 U 40084123-Trichlorobenzene
084 U 40084124-Trichlorobenzene
064 U 40064111-Trichloroethane
11 U 4011112-Trichloroethane
064 U 40064Trichloroethene
12 U 4012Trichlorofluoromethane
13 U 4013123-Trichloropropane
060 U 40060124-Trimethylbenzene
064 U 40064135-Trimethylbenzene
040 U 40040Vinyl chloride
076 U 40076Xylenes Total
072 U 4007212-Dibromoethane
Surrogate Rec Acceptance LimitsQualifier
87 70 - 12712-Dichloroethane-d4 (Surr)
93 80 - 125Toluene-d8 (Surr)
89 78 - 1204-Bromofluorobenzene (Surr)
92 77 - 120Dibromofluoromethane (Surr)
TestAmerica Denver Page 28 of 962
Analytical Data
Client SM Stoller Corporation Job Number 280-39772-1
Sdg Number 13025120
Client Sample ID
Lab Sample ID
PIN12-0575-1
Client Matrix
280-39772-10
Water
Date Sampled 03062013 1540
Date Received 03092013 0930
8260B Volatile Organic Compounds (GCMS)
Dilution
03152013 1329
03152013 1329
10
8260B
Final WeightVolume
Initial WeightVolume
Lab File ID
Instrument ID
g2_6151D
5 mL
20 mL
5030B
VMS_G2
Analysis Date
Prep Date
Analysis Batch
Prep Batch
280-164934
NA
Analysis Method
Prep Method
Analyte Result (ugL) Qualifier MDL RL
83 J 4076Acetone
064 U 40064Benzene
068 U 40068Bromobenzene
040 U 40040Bromochloromethane
068 U 40068Bromodichloromethane
076 U 40076Bromoform
084 U 40084Bromomethane
80 U 20802-Butanone (MEK)
13 U 4013n-Butylbenzene
068 U 40068sec-Butylbenzene
064 U 40064tert-Butylbenzene
18 U 4018Carbon disulfide
076 U 40076Carbon tetrachloride
068 U 40068Chlorobenzene
068 U 40068Dibromochloromethane
16 U 4016Chloroethane
064 U 40064Chloroform
12 U 4012Chloromethane
068 U 400682-Chlorotoluene
084 U 400844-Chlorotoluene
19 U 401912-Dibromo-3-Chloropropane
068 U 40068Dibromomethane
060 U 4006012-Dichlorobenzene
052 U 4005213-Dichlorobenzene
064 U 4006414-Dichlorobenzene
12 U 4012Dichlorodifluoromethane
088 U 4008811-Dichloroethane
052 U 4005212-Dichloroethane
060 U 40060cis-12-Dichloroethene
060 U 40060trans-12-Dichloroethene
092 U 4009211-Dichloroethene
072 U 4007212-Dichloropropane
088 U 4008813-Dichloropropane
072 U 4007222-Dichloropropane
064 U 40064cis-13-Dichloropropene
076 U 40076trans-13-Dichloropropene
076 U 4007611-Dichloropropene
064 U 40064Ethylbenzene
14 U 4014Hexachlorobutadiene
68 U 20682-Hexanone
076 U 40076Isopropylbenzene
080 U 400804-Isopropyltoluene
13 U 4013Methylene Chloride
39 U 20394-Methyl-2-pentanone
088 U 40088Naphthalene
064 U 40064n-Propylbenzene
TestAmerica Denver Page 29 of 962
Analytical Data
Client SM Stoller Corporation Job Number 280-39772-1
Sdg Number 13025120
Client Sample ID
Lab Sample ID
PIN12-0575-1
Client Matrix
280-39772-10
Water
Date Sampled 03062013 1540
Date Received 03092013 0930
8260B Volatile Organic Compounds (GCMS)
Dilution
03152013 1329
03152013 1329
10
8260B
Final WeightVolume
Initial WeightVolume
Lab File ID
Instrument ID
g2_6151D
5 mL
20 mL
5030B
VMS_G2
Analysis Date
Prep Date
Analysis Batch
Prep Batch
280-164934
NA
Analysis Method
Prep Method
Analyte Result (ugL) Qualifier MDL RL
068 U 40068Styrene
084 U 400841112-Tetrachloroethane
084 U 400841122-Tetrachloroethane
080 U 40080Tetrachloroethene
068 U 40068Toluene
084 U 40084123-Trichlorobenzene
084 U 40084124-Trichlorobenzene
064 U 40064111-Trichloroethane
11 U 4011112-Trichloroethane
064 U 40064Trichloroethene
12 U 4012Trichlorofluoromethane
13 U 4013123-Trichloropropane
060 U 40060124-Trimethylbenzene
064 U 40064135-Trimethylbenzene
040 U 40040Vinyl chloride
076 U 40076Xylenes Total
072 U 4007212-Dibromoethane
Surrogate Rec Acceptance LimitsQualifier
87 70 - 12712-Dichloroethane-d4 (Surr)
95 80 - 125Toluene-d8 (Surr)
88 78 - 1204-Bromofluorobenzene (Surr)
92 77 - 120Dibromofluoromethane (Surr)
TestAmerica Denver Page 30 of 962
Analytical Data
Client SM Stoller Corporation Job Number 280-39772-1
Sdg Number 13025120
Client Sample ID
Lab Sample ID
PIN12-0575-2
Client Matrix
280-39772-11
Water
Date Sampled 03062013 1620
Date Received 03092013 0930
8260B Volatile Organic Compounds (GCMS)
Dilution
03152013 1348
03152013 1348
10
8260B
Final WeightVolume
Initial WeightVolume
Lab File ID
Instrument ID
g2_6152D
5 mL
20 mL
5030B
VMS_G2
Analysis Date
Prep Date
Analysis Batch
Prep Batch
280-164934
NA
Analysis Method
Prep Method
Analyte Result (ugL) Qualifier MDL RL
76 U 4076Acetone
064 U 40064Benzene
068 U 40068Bromobenzene
040 U 40040Bromochloromethane
068 U 40068Bromodichloromethane
076 U 40076Bromoform
084 U 40084Bromomethane
80 U 20802-Butanone (MEK)
13 U 4013n-Butylbenzene
068 U 40068sec-Butylbenzene
064 U 40064tert-Butylbenzene
18 U 4018Carbon disulfide
076 U 40076Carbon tetrachloride
068 U 40068Chlorobenzene
068 U 40068Dibromochloromethane
16 U 4016Chloroethane
064 U 40064Chloroform
12 U 4012Chloromethane
068 U 400682-Chlorotoluene
084 U 400844-Chlorotoluene
19 U 401912-Dibromo-3-Chloropropane
068 U 40068Dibromomethane
060 U 4006012-Dichlorobenzene
052 U 4005213-Dichlorobenzene
064 U 4006414-Dichlorobenzene
12 U 4012Dichlorodifluoromethane
088 U 4008811-Dichloroethane
052 U 4005212-Dichloroethane
060 U 40060cis-12-Dichloroethene
060 U 40060trans-12-Dichloroethene
092 U 4009211-Dichloroethene
072 U 4007212-Dichloropropane
088 U 4008813-Dichloropropane
072 U 4007222-Dichloropropane
064 U 40064cis-13-Dichloropropene
076 U 40076trans-13-Dichloropropene
076 U 4007611-Dichloropropene
064 U 40064Ethylbenzene
14 U 4014Hexachlorobutadiene
68 U 20682-Hexanone
076 U 40076Isopropylbenzene
080 U 400804-Isopropyltoluene
13 U 4013Methylene Chloride
39 U 20394-Methyl-2-pentanone
088 U 40088Naphthalene
064 U 40064n-Propylbenzene
TestAmerica Denver Page 31 of 962
Analytical Data
Client SM Stoller Corporation Job Number 280-39772-1
Sdg Number 13025120
Client Sample ID
Lab Sample ID
PIN12-0575-2
Client Matrix
280-39772-11
Water
Date Sampled 03062013 1620
Date Received 03092013 0930
8260B Volatile Organic Compounds (GCMS)
Dilution
03152013 1348
03152013 1348
10
8260B
Final WeightVolume
Initial WeightVolume
Lab File ID
Instrument ID
g2_6152D
5 mL
20 mL
5030B
VMS_G2
Analysis Date
Prep Date
Analysis Batch
Prep Batch
280-164934
NA
Analysis Method
Prep Method
Analyte Result (ugL) Qualifier MDL RL
068 U 40068Styrene
084 U 400841112-Tetrachloroethane
084 U 400841122-Tetrachloroethane
080 U 40080Tetrachloroethene
068 U 40068Toluene
084 U 40084123-Trichlorobenzene
084 U 40084124-Trichlorobenzene
064 U 40064111-Trichloroethane
11 U 4011112-Trichloroethane
064 U 40064Trichloroethene
12 U 4012Trichlorofluoromethane
13 U 4013123-Trichloropropane
060 U 40060124-Trimethylbenzene
064 U 40064135-Trimethylbenzene
040 U 40040Vinyl chloride
076 U 40076Xylenes Total
072 U 4007212-Dibromoethane
Surrogate Rec Acceptance LimitsQualifier
88 70 - 12712-Dichloroethane-d4 (Surr)
94 80 - 125Toluene-d8 (Surr)
90 78 - 1204-Bromofluorobenzene (Surr)
92 77 - 120Dibromofluoromethane (Surr)
TestAmerica Denver Page 32 of 962
Analytical Data
Client SM Stoller Corporation Job Number 280-39772-1
Sdg Number 13025120
Client Sample ID
Lab Sample ID
PIN12-0580-1
Client Matrix
280-39772-12
Water
Date Sampled 03072013 0935
Date Received 03092013 0930
8260B Volatile Organic Compounds (GCMS)
Dilution
03152013 0139
03152013 0139
10
8260B
Final WeightVolume
Initial WeightVolume
Lab File ID
Instrument ID
RR1871D
20 mL
20 mL
5030B
VMS_R2
Analysis Date
Prep Date
Analysis Batch
Prep Batch
280-164920
NA
Analysis Method
Prep Method
Analyte Result (ugL) Qualifier MDL RL
19 U 1019Acetone
016 U 10016Benzene
017 U 10017Bromobenzene
010 U 10010Bromochloromethane
017 U 10017Bromodichloromethane
019 U 10019Bromoform
021 U 10021Bromomethane
20 U 50202-Butanone (MEK)
032 U 10032n-Butylbenzene
017 U 10017sec-Butylbenzene
016 U 10016tert-Butylbenzene
045 U 10045Carbon disulfide
019 U 10019Carbon tetrachloride
017 U 10017Chlorobenzene
017 U 10017Dibromochloromethane
041 U 10041Chloroethane
016 U 10016Chloroform
030 U 10030Chloromethane
017 U 100172-Chlorotoluene
021 U 100214-Chlorotoluene
047 U 1004712-Dibromo-3-Chloropropane
017 U 10017Dibromomethane
015 U 1001512-Dichlorobenzene
013 U 1001313-Dichlorobenzene
016 U 1001614-Dichlorobenzene
031 U 10031Dichlorodifluoromethane
022 U 1002211-Dichloroethane
013 U 1001312-Dichloroethane
054 J 10015cis-12-Dichloroethene
015 U 10015trans-12-Dichloroethene
023 U 1002311-Dichloroethene
018 U 1001812-Dichloropropane
022 U 1002213-Dichloropropane
018 U 1001822-Dichloropropane
016 U 10016cis-13-Dichloropropene
019 U 10019trans-13-Dichloropropene
019 U 1001911-Dichloropropene
016 U 10016Ethylbenzene
036 U 10036Hexachlorobutadiene
17 U 50172-Hexanone
019 U 10019Isopropylbenzene
020 U 100204-Isopropyltoluene
032 U 10032Methylene Chloride
098 U 500984-Methyl-2-pentanone
022 U 10022Naphthalene
016 U 10016n-Propylbenzene
TestAmerica Denver Page 33 of 962
Analytical Data
Client SM Stoller Corporation Job Number 280-39772-1
Sdg Number 13025120
Client Sample ID
Lab Sample ID
PIN12-0580-1
Client Matrix
280-39772-12
Water
Date Sampled 03072013 0935
Date Received 03092013 0930
8260B Volatile Organic Compounds (GCMS)
Dilution
03152013 0139
03152013 0139
10
8260B
Final WeightVolume
Initial WeightVolume
Lab File ID
Instrument ID
RR1871D
20 mL
20 mL
5030B
VMS_R2
Analysis Date
Prep Date
Analysis Batch
Prep Batch
280-164920
NA
Analysis Method
Prep Method
Analyte Result (ugL) Qualifier MDL RL
017 U 10017Styrene
021 U 100211112-Tetrachloroethane
021 U 100211122-Tetrachloroethane
020 U 10020Tetrachloroethene
017 U 10017Toluene
021 U 10021123-Trichlorobenzene
021 U 10021124-Trichlorobenzene
016 U 10016111-Trichloroethane
027 U 10027112-Trichloroethane
016 U 10016Trichloroethene
029 U 10029Trichlorofluoromethane
033 U 10033123-Trichloropropane
015 U 10015124-Trimethylbenzene
016 U 10016135-Trimethylbenzene
42 10010Vinyl chloride
019 U 10019Xylenes Total
018 U 1001812-Dibromoethane
Surrogate Rec Acceptance LimitsQualifier
89 70 - 12712-Dichloroethane-d4 (Surr)
88 80 - 125Toluene-d8 (Surr)
84 78 - 1204-Bromofluorobenzene (Surr)
92 77 - 120Dibromofluoromethane (Surr)
TestAmerica Denver Page 34 of 962
Analytical Data
Client SM Stoller Corporation Job Number 280-39772-1
Sdg Number 13025120
Client Sample ID
Lab Sample ID
PIN12-0580-2
Client Matrix
280-39772-13
Water
Date Sampled 03072013 1030
Date Received 03092013 0930
8260B Volatile Organic Compounds (GCMS)
Dilution
03152013 0202
03152013 0202
10
8260B
Final WeightVolume
Initial WeightVolume
Lab File ID
Instrument ID
RR1872D
20 mL
20 mL
5030B
VMS_R2
Analysis Date
Prep Date
Analysis Batch
Prep Batch
280-164920
NA
Analysis Method
Prep Method
Analyte Result (ugL) Qualifier MDL RL
19 U 1019Acetone
016 U 10016Benzene
017 U 10017Bromobenzene
010 U 10010Bromochloromethane
017 U 10017Bromodichloromethane
019 U 10019Bromoform
021 U 10021Bromomethane
20 U 50202-Butanone (MEK)
032 U 10032n-Butylbenzene
017 U 10017sec-Butylbenzene
016 U 10016tert-Butylbenzene
045 U 10045Carbon disulfide
019 U 10019Carbon tetrachloride
017 U 10017Chlorobenzene
017 U 10017Dibromochloromethane
041 U 10041Chloroethane
016 U 10016Chloroform
030 U 10030Chloromethane
017 U 100172-Chlorotoluene
021 U 100214-Chlorotoluene
047 U 1004712-Dibromo-3-Chloropropane
017 U 10017Dibromomethane
015 U 1001512-Dichlorobenzene
013 U 1001313-Dichlorobenzene
016 U 1001614-Dichlorobenzene
031 U 10031Dichlorodifluoromethane
67 1002211-Dichloroethane
013 U 1001312-Dichloroethane
18 10015cis-12-Dichloroethene
50 10015trans-12-Dichloroethene
023 U 1002311-Dichloroethene
018 U 1001812-Dichloropropane
022 U 1002213-Dichloropropane
018 U 1001822-Dichloropropane
016 U 10016cis-13-Dichloropropene
019 U 10019trans-13-Dichloropropene
019 U 1001911-Dichloropropene
016 U 10016Ethylbenzene
036 U 10036Hexachlorobutadiene
17 U 50172-Hexanone
019 U 10019Isopropylbenzene
020 U 100204-Isopropyltoluene
032 U 10032Methylene Chloride
098 U 500984-Methyl-2-pentanone
022 U 10022Naphthalene
016 U 10016n-Propylbenzene
TestAmerica Denver Page 35 of 962
Analytical Data
Client SM Stoller Corporation Job Number 280-39772-1
Sdg Number 13025120
Client Sample ID
Lab Sample ID
PIN12-0580-2
Client Matrix
280-39772-13
Water
Date Sampled 03072013 1030
Date Received 03092013 0930
8260B Volatile Organic Compounds (GCMS)
Dilution
03152013 0202
03152013 0202
10
8260B
Final WeightVolume
Initial WeightVolume
Lab File ID
Instrument ID
RR1872D
20 mL
20 mL
5030B
VMS_R2
Analysis Date
Prep Date
Analysis Batch
Prep Batch
280-164920
NA
Analysis Method
Prep Method
Analyte Result (ugL) Qualifier MDL RL
017 U 10017Styrene
021 U 100211112-Tetrachloroethane
021 U 100211122-Tetrachloroethane
020 U 10020Tetrachloroethene
017 U 10017Toluene
021 U 10021123-Trichlorobenzene
021 U 10021124-Trichlorobenzene
016 U 10016111-Trichloroethane
027 U 10027112-Trichloroethane
016 U 10016Trichloroethene
029 U 10029Trichlorofluoromethane
033 U 10033123-Trichloropropane
015 U 10015124-Trimethylbenzene
016 U 10016135-Trimethylbenzene
019 U 10019Xylenes Total
018 U 1001812-Dibromoethane
Surrogate Rec Acceptance LimitsQualifier
94 70 - 12712-Dichloroethane-d4 (Surr)
89 80 - 125Toluene-d8 (Surr)
88 78 - 1204-Bromofluorobenzene (Surr)
94 77 - 120Dibromofluoromethane (Surr)
TestAmerica Denver Page 36 of 962
Analytical Data
Client SM Stoller Corporation Job Number 280-39772-1
Sdg Number 13025120
Client Sample ID
Lab Sample ID
PIN12-0580-2
Client Matrix
280-39772-13
Water
Date Sampled 03072013 1030
Date Received 03092013 0930
8260B Volatile Organic Compounds (GCMS)
Dilution
03152013 2140
03152013 2140
10
8260B
Final WeightVolume
Initial WeightVolume
Lab File ID
Instrument ID
RR1919D
5 mL
20 mLRun Type DL
5030B
VMS_R2
Analysis Date
Prep Date
Analysis Batch
Prep Batch
280-165112
NA
Analysis Method
Prep Method
Analyte Result (ugL) Qualifier MDL RL
150 40040Vinyl chloride
Surrogate Rec Acceptance LimitsQualifier
67 70 - 127X12-Dichloroethane-d4 (Surr)
88 80 - 125Toluene-d8 (Surr)
85 78 - 1204-Bromofluorobenzene (Surr)
76 77 - 120XDibromofluoromethane (Surr)
TestAmerica Denver Page 37 of 962
Analytical Data
Client SM Stoller Corporation Job Number 280-39772-1
Sdg Number 13025120
Client Sample ID
Lab Sample ID
PIN12-0580-3
Client Matrix
280-39772-14
Water
Date Sampled 03072013 1110
Date Received 03092013 0930
8260B Volatile Organic Compounds (GCMS)
Dilution
03152013 0225
03152013 0225
10
8260B
Final WeightVolume
Initial WeightVolume
Lab File ID
Instrument ID
RR1873D
20 mL
20 mL
5030B
VMS_R2
Analysis Date
Prep Date
Analysis Batch
Prep Batch
280-164920
NA
Analysis Method
Prep Method
Analyte Result (ugL) Qualifier MDL RL
19 U 1019Acetone
016 U 10016Benzene
017 U 10017Bromobenzene
010 U 10010Bromochloromethane
017 U 10017Bromodichloromethane
019 U 10019Bromoform
021 U 10021Bromomethane
20 U 50202-Butanone (MEK)
032 U 10032n-Butylbenzene
017 U 10017sec-Butylbenzene
016 U 10016tert-Butylbenzene
045 U 10045Carbon disulfide
019 U 10019Carbon tetrachloride
017 U 10017Chlorobenzene
017 U 10017Dibromochloromethane
041 U 10041Chloroethane
016 U 10016Chloroform
030 U 10030Chloromethane
017 U 100172-Chlorotoluene
021 U 100214-Chlorotoluene
047 U 1004712-Dibromo-3-Chloropropane
017 U 10017Dibromomethane
015 U 1001512-Dichlorobenzene
013 U 1001313-Dichlorobenzene
016 U 1001614-Dichlorobenzene
031 U 10031Dichlorodifluoromethane
23 1002211-Dichloroethane
013 U 1001312-Dichloroethane
12 10015cis-12-Dichloroethene
088 J 10015trans-12-Dichloroethene
023 U 1002311-Dichloroethene
018 U 1001812-Dichloropropane
022 U 1002213-Dichloropropane
018 U 1001822-Dichloropropane
016 U 10016cis-13-Dichloropropene
019 U 10019trans-13-Dichloropropene
019 U 1001911-Dichloropropene
016 U 10016Ethylbenzene
036 U 10036Hexachlorobutadiene
17 U 50172-Hexanone
019 U 10019Isopropylbenzene
020 U 100204-Isopropyltoluene
032 U 10032Methylene Chloride
098 U 500984-Methyl-2-pentanone
022 U 10022Naphthalene
016 U 10016n-Propylbenzene
TestAmerica Denver Page 38 of 962
Analytical Data
Client SM Stoller Corporation Job Number 280-39772-1
Sdg Number 13025120
Client Sample ID
Lab Sample ID
PIN12-0580-3
Client Matrix
280-39772-14
Water
Date Sampled 03072013 1110
Date Received 03092013 0930
8260B Volatile Organic Compounds (GCMS)
Dilution
03152013 0225
03152013 0225
10
8260B
Final WeightVolume
Initial WeightVolume
Lab File ID
Instrument ID
RR1873D
20 mL
20 mL
5030B
VMS_R2
Analysis Date
Prep Date
Analysis Batch
Prep Batch
280-164920
NA
Analysis Method
Prep Method
Analyte Result (ugL) Qualifier MDL RL
017 U 10017Styrene
021 U 100211112-Tetrachloroethane
021 U 100211122-Tetrachloroethane
020 U 10020Tetrachloroethene
017 U 10017Toluene
021 U 10021123-Trichlorobenzene
021 U 10021124-Trichlorobenzene
016 U 10016111-Trichloroethane
027 U 10027112-Trichloroethane
016 U 10016Trichloroethene
029 U 10029Trichlorofluoromethane
033 U 10033123-Trichloropropane
015 U 10015124-Trimethylbenzene
016 U 10016135-Trimethylbenzene
23 10010Vinyl chloride
019 U 10019Xylenes Total
018 U 1001812-Dibromoethane
Surrogate Rec Acceptance LimitsQualifier
97 70 - 12712-Dichloroethane-d4 (Surr)
99 80 - 125Toluene-d8 (Surr)
97 78 - 1204-Bromofluorobenzene (Surr)
100 77 - 120Dibromofluoromethane (Surr)
TestAmerica Denver Page 39 of 962
Analytical Data
Client SM Stoller Corporation Job Number 280-39772-1
Sdg Number 13025120
Client Sample ID
Lab Sample ID
PIN12-2450
Client Matrix
280-39772-15
Water
Date Sampled 03072013 1200
Date Received 03092013 0930
8260B Volatile Organic Compounds (GCMS)
Dilution
03152013 0248
03152013 0248
10
8260B
Final WeightVolume
Initial WeightVolume
Lab File ID
Instrument ID
RR1874D
20 mL
20 mL
5030B
VMS_R2
Analysis Date
Prep Date
Analysis Batch
Prep Batch
280-164920
NA
Analysis Method
Prep Method
Analyte Result (ugL) Qualifier MDL RL
19 U 1019Acetone
016 U 10016Benzene
017 U 10017Bromobenzene
010 U 10010Bromochloromethane
017 U 10017Bromodichloromethane
019 U 10019Bromoform
021 U 10021Bromomethane
20 U 50202-Butanone (MEK)
032 U 10032n-Butylbenzene
017 U 10017sec-Butylbenzene
016 U 10016tert-Butylbenzene
045 U 10045Carbon disulfide
019 U 10019Carbon tetrachloride
017 U 10017Chlorobenzene
017 U 10017Dibromochloromethane
041 U 10041Chloroethane
016 U 10016Chloroform
030 U 10030Chloromethane
017 U 100172-Chlorotoluene
021 U 100214-Chlorotoluene
047 U 1004712-Dibromo-3-Chloropropane
017 U 10017Dibromomethane
015 U 1001512-Dichlorobenzene
013 U 1001313-Dichlorobenzene
016 U 1001614-Dichlorobenzene
031 U 10031Dichlorodifluoromethane
62 1002211-Dichloroethane
013 U 1001312-Dichloroethane
16 10015cis-12-Dichloroethene
40 10015trans-12-Dichloroethene
023 U 1002311-Dichloroethene
018 U 1001812-Dichloropropane
022 U 1002213-Dichloropropane
018 U 1001822-Dichloropropane
016 U 10016cis-13-Dichloropropene
019 U 10019trans-13-Dichloropropene
019 U 1001911-Dichloropropene
016 U 10016Ethylbenzene
036 U 10036Hexachlorobutadiene
17 U 50172-Hexanone
019 U 10019Isopropylbenzene
020 U 100204-Isopropyltoluene
032 U 10032Methylene Chloride
098 U 500984-Methyl-2-pentanone
022 U 10022Naphthalene
016 U 10016n-Propylbenzene
TestAmerica Denver Page 40 of 962
Analytical Data
Client SM Stoller Corporation Job Number 280-39772-1
Sdg Number 13025120
Client Sample ID
Lab Sample ID
PIN12-2450
Client Matrix
280-39772-15
Water
Date Sampled 03072013 1200
Date Received 03092013 0930
8260B Volatile Organic Compounds (GCMS)
Dilution
03152013 0248
03152013 0248
10
8260B
Final WeightVolume
Initial WeightVolume
Lab File ID
Instrument ID
RR1874D
20 mL
20 mL
5030B
VMS_R2
Analysis Date
Prep Date
Analysis Batch
Prep Batch
280-164920
NA
Analysis Method
Prep Method
Analyte Result (ugL) Qualifier MDL RL
017 U 10017Styrene
021 U 100211112-Tetrachloroethane
021 U 100211122-Tetrachloroethane
020 U 10020Tetrachloroethene
017 U 10017Toluene
021 U 10021123-Trichlorobenzene
021 U 10021124-Trichlorobenzene
016 U 10016111-Trichloroethane
027 U 10027112-Trichloroethane
016 U 10016Trichloroethene
029 U 10029Trichlorofluoromethane
033 U 10033123-Trichloropropane
015 U 10015124-Trimethylbenzene
016 U 10016135-Trimethylbenzene
019 U 10019Xylenes Total
018 U 1001812-Dibromoethane
Surrogate Rec Acceptance LimitsQualifier
98 70 - 12712-Dichloroethane-d4 (Surr)
94 80 - 125Toluene-d8 (Surr)
91 78 - 1204-Bromofluorobenzene (Surr)
96 77 - 120Dibromofluoromethane (Surr)
TestAmerica Denver Page 41 of 962
Analytical Data
Client SM Stoller Corporation Job Number 280-39772-1
Sdg Number 13025120
Client Sample ID
Lab Sample ID
PIN12-2450
Client Matrix
280-39772-15
Water
Date Sampled 03072013 1200
Date Received 03092013 0930
8260B Volatile Organic Compounds (GCMS)
Dilution
03152013 2203
03152013 2203
10
8260B
Final WeightVolume
Initial WeightVolume
Lab File ID
Instrument ID
RR1920D
5 mL
20 mLRun Type DL
5030B
VMS_R2
Analysis Date
Prep Date
Analysis Batch
Prep Batch
280-165112
NA
Analysis Method
Prep Method
Analyte Result (ugL) Qualifier MDL RL
150 40040Vinyl chloride
Surrogate Rec Acceptance LimitsQualifier
72 70 - 12712-Dichloroethane-d4 (Surr)
96 80 - 125Toluene-d8 (Surr)
89 78 - 1204-Bromofluorobenzene (Surr)
83 77 - 120Dibromofluoromethane (Surr)
TestAmerica Denver Page 42 of 962
Analytical Data
Client SM Stoller Corporation Job Number 280-39772-1
Sdg Number 13025120
Client Sample ID
Lab Sample ID
PIN12-S67B
Client Matrix
280-39772-16
Water
Date Sampled 03072013 1315
Date Received 03092013 0930
8260B Volatile Organic Compounds (GCMS)
Dilution
03152013 0311
03152013 0311
10
8260B
Final WeightVolume
Initial WeightVolume
Lab File ID
Instrument ID
RR1875D
20 mL
20 mL
5030B
VMS_R2
Analysis Date
Prep Date
Analysis Batch
Prep Batch
280-164920
NA
Analysis Method
Prep Method
Analyte Result (ugL) Qualifier MDL RL
19 U 1019Acetone
016 U 10016Benzene
017 U 10017Bromobenzene
010 U 10010Bromochloromethane
017 U 10017Bromodichloromethane
019 U 10019Bromoform
021 U 10021Bromomethane
20 U 50202-Butanone (MEK)
032 U 10032n-Butylbenzene
017 U 10017sec-Butylbenzene
016 U 10016tert-Butylbenzene
045 U 10045Carbon disulfide
019 U 10019Carbon tetrachloride
017 U 10017Chlorobenzene
017 U 10017Dibromochloromethane
041 U 10041Chloroethane
016 U 10016Chloroform
030 U 10030Chloromethane
017 U 100172-Chlorotoluene
021 U 100214-Chlorotoluene
047 U 1004712-Dibromo-3-Chloropropane
017 U 10017Dibromomethane
015 U 1001512-Dichlorobenzene
013 U 1001313-Dichlorobenzene
016 U 1001614-Dichlorobenzene
031 U 10031Dichlorodifluoromethane
32 1002211-Dichloroethane
013 U 1001312-Dichloroethane
13 10015cis-12-Dichloroethene
33 10015trans-12-Dichloroethene
023 U 1002311-Dichloroethene
018 U 1001812-Dichloropropane
022 U 1002213-Dichloropropane
018 U 1001822-Dichloropropane
016 U 10016cis-13-Dichloropropene
019 U 10019trans-13-Dichloropropene
019 U 1001911-Dichloropropene
016 U 10016Ethylbenzene
036 U 10036Hexachlorobutadiene
17 U 50172-Hexanone
019 U 10019Isopropylbenzene
020 U 100204-Isopropyltoluene
032 U 10032Methylene Chloride
098 U 500984-Methyl-2-pentanone
022 U 10022Naphthalene
016 U 10016n-Propylbenzene
TestAmerica Denver Page 43 of 962
Analytical Data
Client SM Stoller Corporation Job Number 280-39772-1
Sdg Number 13025120
Client Sample ID
Lab Sample ID
PIN12-S67B
Client Matrix
280-39772-16
Water
Date Sampled 03072013 1315
Date Received 03092013 0930
8260B Volatile Organic Compounds (GCMS)
Dilution
03152013 0311
03152013 0311
10
8260B
Final WeightVolume
Initial WeightVolume
Lab File ID
Instrument ID
RR1875D
20 mL
20 mL
5030B
VMS_R2
Analysis Date
Prep Date
Analysis Batch
Prep Batch
280-164920
NA
Analysis Method
Prep Method
Analyte Result (ugL) Qualifier MDL RL
017 U 10017Styrene
021 U 100211112-Tetrachloroethane
021 U 100211122-Tetrachloroethane
020 U 10020Tetrachloroethene
017 U 10017Toluene
021 U 10021123-Trichlorobenzene
021 U 10021124-Trichlorobenzene
016 U 10016111-Trichloroethane
027 U 10027112-Trichloroethane
016 U 10016Trichloroethene
029 U 10029Trichlorofluoromethane
033 U 10033123-Trichloropropane
015 U 10015124-Trimethylbenzene
016 U 10016135-Trimethylbenzene
019 U 10019Xylenes Total
018 U 1001812-Dibromoethane
Surrogate Rec Acceptance LimitsQualifier
86 70 - 12712-Dichloroethane-d4 (Surr)
88 80 - 125Toluene-d8 (Surr)
84 78 - 1204-Bromofluorobenzene (Surr)
89 77 - 120Dibromofluoromethane (Surr)
TestAmerica Denver Page 44 of 962
Analytical Data
Client SM Stoller Corporation Job Number 280-39772-1
Sdg Number 13025120
Client Sample ID
Lab Sample ID
PIN12-S67B
Client Matrix
280-39772-16
Water
Date Sampled 03072013 1315
Date Received 03092013 0930
8260B Volatile Organic Compounds (GCMS)
Dilution
03152013 2226
03152013 2226
10
8260B
Final WeightVolume
Initial WeightVolume
Lab File ID
Instrument ID
RR1921D
2 mL
20 mLRun Type DL
5030B
VMS_R2
Analysis Date
Prep Date
Analysis Batch
Prep Batch
280-165112
NA
Analysis Method
Prep Method
Analyte Result (ugL) Qualifier MDL RL
250 1010Vinyl chloride
Surrogate Rec Acceptance LimitsQualifier
70 70 - 12712-Dichloroethane-d4 (Surr)
91 80 - 125Toluene-d8 (Surr)
83 78 - 1204-Bromofluorobenzene (Surr)
80 77 - 120Dibromofluoromethane (Surr)
TestAmerica Denver Page 45 of 962
Analytical Data
Client SM Stoller Corporation Job Number 280-39772-1
Sdg Number 13025120
Client Sample ID
Lab Sample ID
PIN12-S67C
Client Matrix
280-39772-17
Water
Date Sampled 03072013 1225
Date Received 03092013 0930
8260B Volatile Organic Compounds (GCMS)
Dilution
03152013 0333
03152013 0333
10
8260B
Final WeightVolume
Initial WeightVolume
Lab File ID
Instrument ID
RR1876D
20 mL
20 mL
5030B
VMS_R2
Analysis Date
Prep Date
Analysis Batch
Prep Batch
280-164920
NA
Analysis Method
Prep Method
Analyte Result (ugL) Qualifier MDL RL
19 U 1019Acetone
016 U 10016Benzene
017 U 10017Bromobenzene
010 U 10010Bromochloromethane
017 U 10017Bromodichloromethane
019 U 10019Bromoform
021 U 10021Bromomethane
20 U 50202-Butanone (MEK)
032 U 10032n-Butylbenzene
017 U 10017sec-Butylbenzene
016 U 10016tert-Butylbenzene
045 U 10045Carbon disulfide
019 U 10019Carbon tetrachloride
017 U 10017Chlorobenzene
017 U 10017Dibromochloromethane
041 U 10041Chloroethane
016 U 10016Chloroform
030 U 10030Chloromethane
017 U 100172-Chlorotoluene
021 U 100214-Chlorotoluene
047 U 1004712-Dibromo-3-Chloropropane
017 U 10017Dibromomethane
015 U 1001512-Dichlorobenzene
013 U 1001313-Dichlorobenzene
016 U 1001614-Dichlorobenzene
031 U 10031Dichlorodifluoromethane
76 1002211-Dichloroethane
013 U 1001312-Dichloroethane
48 10015cis-12-Dichloroethene
97 10015trans-12-Dichloroethene
064 J 1002311-Dichloroethene
018 U 1001812-Dichloropropane
022 U 1002213-Dichloropropane
018 U 1001822-Dichloropropane
016 U 10016cis-13-Dichloropropene
019 U 10019trans-13-Dichloropropene
019 U 1001911-Dichloropropene
016 U 10016Ethylbenzene
036 U 10036Hexachlorobutadiene
17 U 50172-Hexanone
019 U 10019Isopropylbenzene
020 U 100204-Isopropyltoluene
032 U 10032Methylene Chloride
098 U 500984-Methyl-2-pentanone
022 U 10022Naphthalene
016 U 10016n-Propylbenzene
TestAmerica Denver Page 46 of 962
Analytical Data
Client SM Stoller Corporation Job Number 280-39772-1
Sdg Number 13025120
Client Sample ID
Lab Sample ID
PIN12-S67C
Client Matrix
280-39772-17
Water
Date Sampled 03072013 1225
Date Received 03092013 0930
8260B Volatile Organic Compounds (GCMS)
Dilution
03152013 0333
03152013 0333
10
8260B
Final WeightVolume
Initial WeightVolume
Lab File ID
Instrument ID
RR1876D
20 mL
20 mL
5030B
VMS_R2
Analysis Date
Prep Date
Analysis Batch
Prep Batch
280-164920
NA
Analysis Method
Prep Method
Analyte Result (ugL) Qualifier MDL RL
017 U 10017Styrene
021 U 100211112-Tetrachloroethane
021 U 100211122-Tetrachloroethane
020 U 10020Tetrachloroethene
017 U 10017Toluene
021 U 10021123-Trichlorobenzene
021 U 10021124-Trichlorobenzene
016 U 10016111-Trichloroethane
027 U 10027112-Trichloroethane
016 U 10016Trichloroethene
029 U 10029Trichlorofluoromethane
033 U 10033123-Trichloropropane
015 U 10015124-Trimethylbenzene
016 U 10016135-Trimethylbenzene
019 U 10019Xylenes Total
018 U 1001812-Dibromoethane
Surrogate Rec Acceptance LimitsQualifier
97 70 - 12712-Dichloroethane-d4 (Surr)
100 80 - 125Toluene-d8 (Surr)
98 78 - 1204-Bromofluorobenzene (Surr)
100 77 - 120Dibromofluoromethane (Surr)
TestAmerica Denver Page 47 of 962
Analytical Data
Client SM Stoller Corporation Job Number 280-39772-1
Sdg Number 13025120
Client Sample ID
Lab Sample ID
PIN12-S67C
Client Matrix
280-39772-17
Water
Date Sampled 03072013 1225
Date Received 03092013 0930
8260B Volatile Organic Compounds (GCMS)
Dilution
03162013 0524
03162013 0524
10
8260B
Final WeightVolume
Initial WeightVolume
Lab File ID
Instrument ID
RR1939D
5 mL
20 mLRun Type DL
5030B
VMS_R2
Analysis Date
Prep Date
Analysis Batch
Prep Batch
280-165112
NA
Analysis Method
Prep Method
Analyte Result (ugL) Qualifier MDL RL
65 40040Vinyl chloride
Surrogate Rec Acceptance LimitsQualifier
80 70 - 12712-Dichloroethane-d4 (Surr)
100 80 - 125Toluene-d8 (Surr)
90 78 - 1204-Bromofluorobenzene (Surr)
95 77 - 120Dibromofluoromethane (Surr)
TestAmerica Denver Page 48 of 962
Analytical Data
Client SM Stoller Corporation Job Number 280-39772-1
Sdg Number 13025120
Client Sample ID
Lab Sample ID
PIN12-S67D
Client Matrix
280-39772-18
Water
Date Sampled 03072013 1355
Date Received 03092013 0930
8260B Volatile Organic Compounds (GCMS)
Dilution
03152013 0356
03152013 0356
10
8260B
Final WeightVolume
Initial WeightVolume
Lab File ID
Instrument ID
RR1877D
20 mL
20 mL
5030B
VMS_R2
Analysis Date
Prep Date
Analysis Batch
Prep Batch
280-164920
NA
Analysis Method
Prep Method
Analyte Result (ugL) Qualifier MDL RL
19 U 1019Acetone
016 U 10016Benzene
017 U 10017Bromobenzene
010 U 10010Bromochloromethane
017 U 10017Bromodichloromethane
019 U 10019Bromoform
021 U 10021Bromomethane
20 U 50202-Butanone (MEK)
032 U 10032n-Butylbenzene
017 U 10017sec-Butylbenzene
016 U 10016tert-Butylbenzene
045 U 10045Carbon disulfide
019 U 10019Carbon tetrachloride
017 U 10017Chlorobenzene
017 U 10017Dibromochloromethane
041 U 10041Chloroethane
016 U 10016Chloroform
030 U 10030Chloromethane
017 U 100172-Chlorotoluene
021 U 100214-Chlorotoluene
047 U 1004712-Dibromo-3-Chloropropane
017 U 10017Dibromomethane
015 U 1001512-Dichlorobenzene
013 U 1001313-Dichlorobenzene
016 U 1001614-Dichlorobenzene
031 U 10031Dichlorodifluoromethane
086 J 1002211-Dichloroethane
013 U 1001312-Dichloroethane
62 10015cis-12-Dichloroethene
19 10015trans-12-Dichloroethene
023 U 1002311-Dichloroethene
018 U 1001812-Dichloropropane
022 U 1002213-Dichloropropane
018 U 1001822-Dichloropropane
016 U 10016cis-13-Dichloropropene
019 U 10019trans-13-Dichloropropene
019 U 1001911-Dichloropropene
016 U 10016Ethylbenzene
036 U 10036Hexachlorobutadiene
17 U 50172-Hexanone
019 U 10019Isopropylbenzene
020 U 100204-Isopropyltoluene
032 U 10032Methylene Chloride
098 U 500984-Methyl-2-pentanone
022 U 10022Naphthalene
016 U 10016n-Propylbenzene
TestAmerica Denver Page 49 of 962
Analytical Data
Client SM Stoller Corporation Job Number 280-39772-1
Sdg Number 13025120
Client Sample ID
Lab Sample ID
PIN12-S67D
Client Matrix
280-39772-18
Water
Date Sampled 03072013 1355
Date Received 03092013 0930
8260B Volatile Organic Compounds (GCMS)
Dilution
03152013 0356
03152013 0356
10
8260B
Final WeightVolume
Initial WeightVolume
Lab File ID
Instrument ID
RR1877D
20 mL
20 mL
5030B
VMS_R2
Analysis Date
Prep Date
Analysis Batch
Prep Batch
280-164920
NA
Analysis Method
Prep Method
Analyte Result (ugL) Qualifier MDL RL
017 U 10017Styrene
021 U 100211112-Tetrachloroethane
021 U 100211122-Tetrachloroethane
020 U 10020Tetrachloroethene
017 U 10017Toluene
021 U 10021123-Trichlorobenzene
021 U 10021124-Trichlorobenzene
016 U 10016111-Trichloroethane
027 U 10027112-Trichloroethane
016 U 10016Trichloroethene
029 U 10029Trichlorofluoromethane
033 U 10033123-Trichloropropane
015 U 10015124-Trimethylbenzene
016 U 10016135-Trimethylbenzene
11 10010Vinyl chloride
019 U 10019Xylenes Total
018 U 1001812-Dibromoethane
Surrogate Rec Acceptance LimitsQualifier
87 70 - 12712-Dichloroethane-d4 (Surr)
92 80 - 125Toluene-d8 (Surr)
89 78 - 1204-Bromofluorobenzene (Surr)
93 77 - 120Dibromofluoromethane (Surr)
TestAmerica Denver Page 50 of 962
Analytical Data
Client SM Stoller Corporation Job Number 280-39772-1
Sdg Number 13025120
Client Sample ID
Lab Sample ID
PIN99-2198
Client Matrix
280-39772-19
Water
Date Sampled 03062013 1200
Date Received 03092013 0930
8260B Volatile Organic Compounds (GCMS)
Dilution
03152013 1407
03152013 1407
10
8260B
Final WeightVolume
Initial WeightVolume
Lab File ID
Instrument ID
g2_6153D
20 mL
20 mL
5030B
VMS_G2
Analysis Date
Prep Date
Analysis Batch
Prep Batch
280-164934
NA
Analysis Method
Prep Method
Analyte Result (ugL) Qualifier MDL RL
19 U 1019Acetone
016 U 10016Benzene
017 U 10017Bromobenzene
010 U 10010Bromochloromethane
017 U 10017Bromodichloromethane
019 U 10019Bromoform
021 U 10021Bromomethane
20 U 50202-Butanone (MEK)
032 U 10032n-Butylbenzene
017 U 10017sec-Butylbenzene
016 U 10016tert-Butylbenzene
045 U 10045Carbon disulfide
019 U 10019Carbon tetrachloride
017 U 10017Chlorobenzene
017 U 10017Dibromochloromethane
041 U 10041Chloroethane
016 U 10016Chloroform
030 U 10030Chloromethane
017 U 100172-Chlorotoluene
021 U 100214-Chlorotoluene
047 U 1004712-Dibromo-3-Chloropropane
017 U 10017Dibromomethane
015 U 1001512-Dichlorobenzene
013 U 1001313-Dichlorobenzene
016 U 1001614-Dichlorobenzene
031 U 10031Dichlorodifluoromethane
022 U 1002211-Dichloroethane
013 U 1001312-Dichloroethane
015 U 10015cis-12-Dichloroethene
015 U 10015trans-12-Dichloroethene
023 U 1002311-Dichloroethene
018 U 1001812-Dichloropropane
022 U 1002213-Dichloropropane
018 U 1001822-Dichloropropane
016 U 10016cis-13-Dichloropropene
019 U 10019trans-13-Dichloropropene
019 U 1001911-Dichloropropene
016 U 10016Ethylbenzene
036 U 10036Hexachlorobutadiene
17 U 50172-Hexanone
019 U 10019Isopropylbenzene
020 U 100204-Isopropyltoluene
032 U 10032Methylene Chloride
098 U 500984-Methyl-2-pentanone
022 U 10022Naphthalene
016 U 10016n-Propylbenzene
TestAmerica Denver Page 51 of 962
Analytical Data
Client SM Stoller Corporation Job Number 280-39772-1
Sdg Number 13025120
Client Sample ID
Lab Sample ID
PIN99-2198
Client Matrix
280-39772-19
Water
Date Sampled 03062013 1200
Date Received 03092013 0930
8260B Volatile Organic Compounds (GCMS)
Dilution
03152013 1407
03152013 1407
10
8260B
Final WeightVolume
Initial WeightVolume
Lab File ID
Instrument ID
g2_6153D
20 mL
20 mL
5030B
VMS_G2
Analysis Date
Prep Date
Analysis Batch
Prep Batch
280-164934
NA
Analysis Method
Prep Method
Analyte Result (ugL) Qualifier MDL RL
017 U 10017Styrene
021 U 100211112-Tetrachloroethane
021 U 100211122-Tetrachloroethane
020 U 10020Tetrachloroethene
017 U 10017Toluene
021 U 10021123-Trichlorobenzene
021 U 10021124-Trichlorobenzene
016 U 10016111-Trichloroethane
027 U 10027112-Trichloroethane
016 U 10016Trichloroethene
029 U 10029Trichlorofluoromethane
033 U 10033123-Trichloropropane
015 U 10015124-Trimethylbenzene
016 U 10016135-Trimethylbenzene
010 U 10010Vinyl chloride
019 U 10019Xylenes Total
018 U 1001812-Dibromoethane
Surrogate Rec Acceptance LimitsQualifier
85 70 - 12712-Dichloroethane-d4 (Surr)
95 80 - 125Toluene-d8 (Surr)
86 78 - 1204-Bromofluorobenzene (Surr)
94 77 - 120Dibromofluoromethane (Surr)
TestAmerica Denver Page 52 of 962
Analytical Data
Client SM Stoller Corporation Job Number 280-39772-1
Sdg Number 13025120
Client Sample ID
Lab Sample ID
PIN12-0555A
Client Matrix
280-39772-1
Water
Date Sampled 03072013 1605
Date Received 03092013 0930
8260B SIM Volatile Organic Compounds (GCMS-SIM)
Dilution
03122013 2146
03122013 2146
10
8260B SIM
Final WeightVolume
Initial WeightVolume
Lab File ID
Instrument ID
E3715D
20 mL
20 mL
5030B
VMS_E
Analysis Date
Prep Date
Analysis Batch
Prep Batch
280-164432
NA
Analysis Method
Prep Method
Analyte Result (ugL) Qualifier MDL RL
022 U 1002214-Dioxane
Surrogate Rec Acceptance LimitsQualifier
99 70 - 12712-Dichloroethane-d4 (Surr)
TestAmerica Denver Page 53 of 962
Analytical Data
Client SM Stoller Corporation Job Number 280-39772-1
Sdg Number 13025120
Client Sample ID
Lab Sample ID
PIN12-0555B
Client Matrix
280-39772-2
Water
Date Sampled 03072013 1640
Date Received 03092013 0930
8260B SIM Volatile Organic Compounds (GCMS-SIM)
Dilution
03122013 2204
03122013 2204
10
8260B SIM
Final WeightVolume
Initial WeightVolume
Lab File ID
Instrument ID
E3716D
20 mL
20 mL
5030B
VMS_E
Analysis Date
Prep Date
Analysis Batch
Prep Batch
280-164432
NA
Analysis Method
Prep Method
Analyte Result (ugL) Qualifier MDL RL
022 U 1002214-Dioxane
Surrogate Rec Acceptance LimitsQualifier
96 70 - 12712-Dichloroethane-d4 (Surr)
TestAmerica Denver Page 54 of 962
Analytical Data
Client SM Stoller Corporation Job Number 280-39772-1
Sdg Number 13025120
Client Sample ID
Lab Sample ID
PIN12-0555C
Client Matrix
280-39772-3
Water
Date Sampled 03072013 1740
Date Received 03092013 0930
8260B SIM Volatile Organic Compounds (GCMS-SIM)
Dilution
03122013 2256
03122013 2256
10
8260B SIM
Final WeightVolume
Initial WeightVolume
Lab File ID
Instrument ID
E3719D
20 mL
20 mL
5030B
VMS_E
Analysis Date
Prep Date
Analysis Batch
Prep Batch
280-164432
NA
Analysis Method
Prep Method
Analyte Result (ugL) Qualifier MDL RL
022 U 1002214-Dioxane
Surrogate Rec Acceptance LimitsQualifier
94 70 - 12712-Dichloroethane-d4 (Surr)
TestAmerica Denver Page 55 of 962
Analytical Data
Client SM Stoller Corporation Job Number 280-39772-1
Sdg Number 13025120
Client Sample ID
Lab Sample ID
PIN12-0565-1
Client Matrix
280-39772-4
Water
Date Sampled 03062013 0936
Date Received 03092013 0930
8260B SIM Volatile Organic Compounds (GCMS-SIM)
Dilution
03122013 2314
03122013 2314
10
8260B SIM
Final WeightVolume
Initial WeightVolume
Lab File ID
Instrument ID
E3720D
20 mL
20 mL
5030B
VMS_E
Analysis Date
Prep Date
Analysis Batch
Prep Batch
280-164432
NA
Analysis Method
Prep Method
Analyte Result (ugL) Qualifier MDL RL
022 U 1002214-Dioxane
Surrogate Rec Acceptance LimitsQualifier
96 70 - 12712-Dichloroethane-d4 (Surr)
TestAmerica Denver Page 56 of 962
Analytical Data
Client SM Stoller Corporation Job Number 280-39772-1
Sdg Number 13025120
Client Sample ID
Lab Sample ID
PIN12-0565-2
Client Matrix
280-39772-5
Water
Date Sampled 03062013 1015
Date Received 03092013 0930
8260B SIM Volatile Organic Compounds (GCMS-SIM)
Dilution
03122013 2331
03122013 2331
10
8260B SIM
Final WeightVolume
Initial WeightVolume
Lab File ID
Instrument ID
E3721D
20 mL
20 mL
5030B
VMS_E
Analysis Date
Prep Date
Analysis Batch
Prep Batch
280-164432
NA
Analysis Method
Prep Method
Analyte Result (ugL) Qualifier MDL RL
022 U 1002214-Dioxane
Surrogate Rec Acceptance LimitsQualifier
97 70 - 12712-Dichloroethane-d4 (Surr)
TestAmerica Denver Page 57 of 962
Analytical Data
Client SM Stoller Corporation Job Number 280-39772-1
Sdg Number 13025120
Client Sample ID
Lab Sample ID
PIN12-0565-3
Client Matrix
280-39772-6
Water
Date Sampled 03062013 1110
Date Received 03092013 0930
8260B SIM Volatile Organic Compounds (GCMS-SIM)
Dilution
03122013 2349
03122013 2349
10
8260B SIM
Final WeightVolume
Initial WeightVolume
Lab File ID
Instrument ID
E3722D
20 mL
20 mL
5030B
VMS_E
Analysis Date
Prep Date
Analysis Batch
Prep Batch
280-164432
NA
Analysis Method
Prep Method
Analyte Result (ugL) Qualifier MDL RL
022 U 1002214-Dioxane
Surrogate Rec Acceptance LimitsQualifier
102 70 - 12712-Dichloroethane-d4 (Surr)
TestAmerica Denver Page 58 of 962
Analytical Data
Client SM Stoller Corporation Job Number 280-39772-1
Sdg Number 13025120
Client Sample ID
Lab Sample ID
PIN12-0573-1
Client Matrix
280-39772-7
Water
Date Sampled 03062013 1335
Date Received 03092013 0930
8260B SIM Volatile Organic Compounds (GCMS-SIM)
Dilution
03132013 0006
03132013 0006
10
8260B SIM
Final WeightVolume
Initial WeightVolume
Lab File ID
Instrument ID
E3723D
20 mL
20 mL
5030B
VMS_E
Analysis Date
Prep Date
Analysis Batch
Prep Batch
280-164432
NA
Analysis Method
Prep Method
Analyte Result (ugL) Qualifier MDL RL
022 U 1002214-Dioxane
Surrogate Rec Acceptance LimitsQualifier
100 70 - 12712-Dichloroethane-d4 (Surr)
TestAmerica Denver Page 59 of 962
Analytical Data
Client SM Stoller Corporation Job Number 280-39772-1
Sdg Number 13025120
Client Sample ID
Lab Sample ID
PIN12-0573-2
Client Matrix
280-39772-8
Water
Date Sampled 03062013 1405
Date Received 03092013 0930
8260B SIM Volatile Organic Compounds (GCMS-SIM)
Dilution
03132013 0024
03132013 0024
10
8260B SIM
Final WeightVolume
Initial WeightVolume
Lab File ID
Instrument ID
E3724D
20 mL
20 mL
5030B
VMS_E
Analysis Date
Prep Date
Analysis Batch
Prep Batch
280-164432
NA
Analysis Method
Prep Method
Analyte Result (ugL) Qualifier MDL RL
022 U 1002214-Dioxane
Surrogate Rec Acceptance LimitsQualifier
103 70 - 12712-Dichloroethane-d4 (Surr)
TestAmerica Denver Page 60 of 962
Analytical Data
Client SM Stoller Corporation Job Number 280-39772-1
Sdg Number 13025120
Client Sample ID
Lab Sample ID
PIN12-0573-3
Client Matrix
280-39772-9
Water
Date Sampled 03062013 1440
Date Received 03092013 0930
8260B SIM Volatile Organic Compounds (GCMS-SIM)
Dilution
03132013 0041
03132013 0041
10
8260B SIM
Final WeightVolume
Initial WeightVolume
Lab File ID
Instrument ID
E3725D
20 mL
20 mL
5030B
VMS_E
Analysis Date
Prep Date
Analysis Batch
Prep Batch
280-164432
NA
Analysis Method
Prep Method
Analyte Result (ugL) Qualifier MDL RL
022 U 1002214-Dioxane
Surrogate Rec Acceptance LimitsQualifier
101 70 - 12712-Dichloroethane-d4 (Surr)
TestAmerica Denver Page 61 of 962
Analytical Data
Client SM Stoller Corporation Job Number 280-39772-1
Sdg Number 13025120
Client Sample ID
Lab Sample ID
PIN12-0575-1
Client Matrix
280-39772-10
Water
Date Sampled 03062013 1540
Date Received 03092013 0930
8260B SIM Volatile Organic Compounds (GCMS-SIM)
Dilution
03132013 0059
03132013 0059
10
8260B SIM
Final WeightVolume
Initial WeightVolume
Lab File ID
Instrument ID
E3726D
20 mL
20 mL
5030B
VMS_E
Analysis Date
Prep Date
Analysis Batch
Prep Batch
280-164432
NA
Analysis Method
Prep Method
Analyte Result (ugL) Qualifier MDL RL
19 1002214-Dioxane
Surrogate Rec Acceptance LimitsQualifier
103 70 - 12712-Dichloroethane-d4 (Surr)
TestAmerica Denver Page 62 of 962
Analytical Data
Client SM Stoller Corporation Job Number 280-39772-1
Sdg Number 13025120
Client Sample ID
Lab Sample ID
PIN12-0575-2
Client Matrix
280-39772-11
Water
Date Sampled 03062013 1620
Date Received 03092013 0930
8260B SIM Volatile Organic Compounds (GCMS-SIM)
Dilution
03132013 0116
03132013 0116
10
8260B SIM
Final WeightVolume
Initial WeightVolume
Lab File ID
Instrument ID
E3727D
20 mL
20 mL
5030B
VMS_E
Analysis Date
Prep Date
Analysis Batch
Prep Batch
280-164432
NA
Analysis Method
Prep Method
Analyte Result (ugL) Qualifier MDL RL
022 U 1002214-Dioxane
Surrogate Rec Acceptance LimitsQualifier
102 70 - 12712-Dichloroethane-d4 (Surr)
TestAmerica Denver Page 63 of 962
Analytical Data
Client SM Stoller Corporation Job Number 280-39772-1
Sdg Number 13025120
Client Sample ID
Lab Sample ID
PIN12-0580-1
Client Matrix
280-39772-12
Water
Date Sampled 03072013 0935
Date Received 03092013 0930
8260B SIM Volatile Organic Compounds (GCMS-SIM)
Dilution
03132013 0134
03132013 0134
10
8260B SIM
Final WeightVolume
Initial WeightVolume
Lab File ID
Instrument ID
E3728D
20 mL
20 mL
5030B
VMS_E
Analysis Date
Prep Date
Analysis Batch
Prep Batch
280-164432
NA
Analysis Method
Prep Method
Analyte Result (ugL) Qualifier MDL RL
40 1002214-Dioxane
Surrogate Rec Acceptance LimitsQualifier
102 70 - 12712-Dichloroethane-d4 (Surr)
TestAmerica Denver Page 64 of 962
Analytical Data
Client SM Stoller Corporation Job Number 280-39772-1
Sdg Number 13025120
Client Sample ID
Lab Sample ID
PIN12-0580-2
Client Matrix
280-39772-13
Water
Date Sampled 03072013 1030
Date Received 03092013 0930
8260B SIM Volatile Organic Compounds (GCMS-SIM)
Dilution
03132013 2100
03132013 2100
10
8260B SIM
Final WeightVolume
Initial WeightVolume
Lab File ID
Instrument ID
E3741D
1 mL
20 mL
5030B
VMS_E
Analysis Date
Prep Date
Analysis Batch
Prep Batch
280-164670
NA
Analysis Method
Prep Method
Analyte Result (ugL) Qualifier MDL RL
160 204414-Dioxane
Surrogate Rec Acceptance LimitsQualifier
108 70 - 12712-Dichloroethane-d4 (Surr)
TestAmerica Denver Page 65 of 962
Analytical Data
Client SM Stoller Corporation Job Number 280-39772-1
Sdg Number 13025120
Client Sample ID
Lab Sample ID
PIN12-0580-3
Client Matrix
280-39772-14
Water
Date Sampled 03072013 1110
Date Received 03092013 0930
8260B SIM Volatile Organic Compounds (GCMS-SIM)
Dilution
03152013 0323
03152013 0323
10
8260B SIM
Final WeightVolume
Initial WeightVolume
Lab File ID
Instrument ID
E3795D
10 mL
20 mL
5030B
VMS_E
Analysis Date
Prep Date
Analysis Batch
Prep Batch
280-164929
NA
Analysis Method
Prep Method
Analyte Result (ugL) Qualifier MDL RL
28 2004414-Dioxane
Surrogate Rec Acceptance LimitsQualifier
103 70 - 12712-Dichloroethane-d4 (Surr)
TestAmerica Denver Page 66 of 962
Analytical Data
Client SM Stoller Corporation Job Number 280-39772-1
Sdg Number 13025120
Client Sample ID
Lab Sample ID
PIN12-2450
Client Matrix
280-39772-15
Water
Date Sampled 03072013 1200
Date Received 03092013 0930
8260B SIM Volatile Organic Compounds (GCMS-SIM)
Dilution
03152013 0341
03152013 0341
10
8260B SIM
Final WeightVolume
Initial WeightVolume
Lab File ID
Instrument ID
E3796D
1 mL
20 mL
5030B
VMS_E
Analysis Date
Prep Date
Analysis Batch
Prep Batch
280-164929
NA
Analysis Method
Prep Method
Analyte Result (ugL) Qualifier MDL RL
190 204414-Dioxane
Surrogate Rec Acceptance LimitsQualifier
108 70 - 12712-Dichloroethane-d4 (Surr)
TestAmerica Denver Page 67 of 962
Analytical Data
Client SM Stoller Corporation Job Number 280-39772-1
Sdg Number 13025120
Client Sample ID
Lab Sample ID
PIN12-S67B
Client Matrix
280-39772-16
Water
Date Sampled 03072013 1315
Date Received 03092013 0930
8260B SIM Volatile Organic Compounds (GCMS-SIM)
Dilution
03132013 2153
03132013 2153
10
8260B SIM
Final WeightVolume
Initial WeightVolume
Lab File ID
Instrument ID
E3744D
2 mL
20 mL
5030B
VMS_E
Analysis Date
Prep Date
Analysis Batch
Prep Batch
280-164670
NA
Analysis Method
Prep Method
Analyte Result (ugL) Qualifier MDL RL
91 102214-Dioxane
Surrogate Rec Acceptance LimitsQualifier
99 70 - 12712-Dichloroethane-d4 (Surr)
TestAmerica Denver Page 68 of 962
Analytical Data
Client SM Stoller Corporation Job Number 280-39772-1
Sdg Number 13025120
Client Sample ID
Lab Sample ID
PIN12-S67C
Client Matrix
280-39772-17
Water
Date Sampled 03072013 1225
Date Received 03092013 0930
8260B SIM Volatile Organic Compounds (GCMS-SIM)
Dilution
03162013 0420
03162013 0420
10
8260B SIM
Final WeightVolume
Initial WeightVolume
Lab File ID
Instrument ID
E3844D
5 mL
20 mL
5030B
VMS_E
Analysis Date
Prep Date
Analysis Batch
Prep Batch
280-165111
NA
Analysis Method
Prep Method
Analyte Result (ugL) Qualifier MDL RL
088 U 4008814-Dioxane
Surrogate Rec Acceptance LimitsQualifier
120 70 - 12712-Dichloroethane-d4 (Surr)
TestAmerica Denver Page 69 of 962
Analytical Data
Client SM Stoller Corporation Job Number 280-39772-1
Sdg Number 13025120
Client Sample ID
Lab Sample ID
PIN12-S67D
Client Matrix
280-39772-18
Water
Date Sampled 03072013 1355
Date Received 03092013 0930
8260B SIM Volatile Organic Compounds (GCMS-SIM)
Dilution
03142013 0434
03142013 0434
10
8260B SIM
Final WeightVolume
Initial WeightVolume
Lab File ID
Instrument ID
E3767D
20 mL
20 mL
5030B
VMS_E
Analysis Date
Prep Date
Analysis Batch
Prep Batch
280-164670
NA
Analysis Method
Prep Method
Analyte Result (ugL) Qualifier MDL RL
022 U 1002214-Dioxane
Surrogate Rec Acceptance LimitsQualifier
114 70 - 12712-Dichloroethane-d4 (Surr)
TestAmerica Denver Page 70 of 962
Quality Control Results
Job Number 280-39772-1
Sdg Number 13025120
Client SM Stoller Corporation
Surrogate Recovery Report
8260B Volatile Organic Compounds (GCMS)
Client Matrix Water
Lab Sample ID Client Sample ID
DBFM DCA TOL BFB
Rec Rec Rec Rec
280-39772-1 PIN12-0555A 85 75 96 90
280-39772-2 PIN12-0555B 89 84 92 89
280-39772-3 PIN12-0555C 106 101 105 103
280-39772-4 PIN12-0565-1 94 87 94 88
280-39772-5 PIN12-0565-2 90 87 91 90
280-39772-6 PIN12-0565-3 94 87 94 90
280-39772-7 PIN12-0573-1 90 85 93 90
280-39772-8 PIN12-0573-2 91 85 95 91
280-39772-9 PIN12-0573-3 92 87 93 89
280-39772-10 PIN12-0575-1 92 87 95 88
280-39772-11 PIN12-0575-2 92 88 94 90
280-39772-12 PIN12-0580-1 92 89 88 84
280-39772-13 PIN12-0580-2 94 94 89 88
280-39772-13 DL PIN12-0580-2 DL 76X 67X 88 85
280-39772-14 PIN12-0580-3 100 97 99 97
280-39772-15 PIN12-2450 96 98 94 91
280-39772-15 DL PIN12-2450 DL 83 72 96 89
280-39772-16 PIN12-S67B 89 86 88 84
280-39772-16 DL PIN12-S67B DL 80 70 91 83
280-39772-17 PIN12-S67C 100 97 100 98
280-39772-17 DL PIN12-S67C DL 95 80 100 90
280-39772-18 PIN12-S67D 93 87 92 89
280-39772-19 PIN99-2198 94 85 95 86
MB 280-1649205 93 89 94 90
MB 280-1649347 86 83 95 88
MB 280-1651125 82 73 92 84
LCS 280-1649204 93 92 92 92
LCS 280-1649346 88 83 95 88
LCS 280-1651124 84 82 94 86
Surrogate Acceptance Limits
DBFM = Dibromofluoromethane (Surr) 77-120
DCA = 12-Dichloroethane-d4 (Surr) 70-127
TOL = Toluene-d8 (Surr) 80-125
BFB = 4-Bromofluorobenzene (Surr) 78-120
TestAmerica Denver
Page 71 of 962
Quality Control Results
Job Number 280-39772-1
Sdg Number 13025120
Client SM Stoller Corporation
Surrogate Recovery Report
8260B Volatile Organic Compounds (GCMS)
Client Matrix Water
Lab Sample ID Client Sample ID
DBFM DCA TOL BFB
Rec Rec Rec Rec
280-39772-1 MS PIN12-0555A MS 89 84 92 88
280-39751-I-1 MS 91 87 99 86
280-39756-O-16 MS 89 83 90 87
280-39772-1 MSD PIN12-0555A MSD 89 85 90 88
280-39751-I-1 MSD 93 87 98 86
280-39756-O-16 MSD 91 89 91 89
Surrogate Acceptance Limits
DBFM = Dibromofluoromethane (Surr) 77-120
DCA = 12-Dichloroethane-d4 (Surr) 70-127
TOL = Toluene-d8 (Surr) 80-125
BFB = 4-Bromofluorobenzene (Surr) 78-120
TestAmerica Denver
Page 72 of 962
Quality Control Results
Job Number 280-39772-1
Sdg Number 13025120
Client SM Stoller Corporation
Surrogate Recovery Report
8260B SIM Volatile Organic Compounds (GCMS-SIM)
Client Matrix Water
Lab Sample ID Client Sample ID
DCA
Rec
280-39772-1 PIN12-0555A 99
280-39772-2 PIN12-0555B 96
280-39772-3 PIN12-0555C 94
280-39772-4 PIN12-0565-1 96
280-39772-5 PIN12-0565-2 97
280-39772-6 PIN12-0565-3 102
280-39772-7 PIN12-0573-1 100
280-39772-8 PIN12-0573-2 103
280-39772-9 PIN12-0573-3 101
280-39772-10 PIN12-0575-1 103
280-39772-11 PIN12-0575-2 102
280-39772-12 PIN12-0580-1 102
280-39772-13 PIN12-0580-2 108
280-39772-14 PIN12-0580-3 103
280-39772-15 PIN12-2450 108
280-39772-16 PIN12-S67B 99
280-39772-17 PIN12-S67C 120
280-39772-18 PIN12-S67D 114
MB 280-1644325 95
MB 280-1646705 105
MB 280-16492917 99
MB 280-1651115 99
LCS 280-1644323 92
LCS 280-1646703 106
LCS 280-16492915 102
LCS 280-1651113 103
LCSD 280-1644324 94
LCSD 280-1646704 103
LCSD 280-16492916 97
Surrogate Acceptance Limits
DCA = 12-Dichloroethane-d4 (Surr) 70-127
TestAmerica Denver
Page 73 of 962
Quality Control Results
Job Number 280-39772-1
Sdg Number 13025120
Client SM Stoller Corporation
Surrogate Recovery Report
8260B SIM Volatile Organic Compounds (GCMS-SIM)
Client Matrix Water
Lab Sample ID Client Sample ID
DCA
Rec
LCSD 280-1651114 105
280-39772-2 MS PIN12-0555B MS 96
280-39873-C-4 MS 97
280-39873-A-2 MS 98
280-39772-2 MSD PIN12-0555B MSD 98
280-39873-C-4 MSD 100
280-39873-A-2 MSD 102
Surrogate Acceptance Limits
DCA = 12-Dichloroethane-d4 (Surr) 70-127
TestAmerica Denver
Page 74 of 962
Quality Control Results
Job Number 280-39772-1Client SM Stoller Corporation
Sdg Number 13025120
WaterClient Matrix
10Dilution
Lab Sample ID
Method Blank - Batch 280-164920
Instrument ID
Lab File ID
Initial WeightVolume
Final WeightVolume
RR1859D
20 mL
20 mLUnits ugL
Method 8260B
Preparation 5030B
VMS_R2MB 280-1649205
Analysis Date 03142013 2102
Analysis Batch
Prep Batch
Leach Batch
NA
NA
280-164920
Prep Date
Leach Date
03142013 2102
NA
Analyte RLMDLQualResult
19 U 1019Acetone
016 U 10016Benzene
017 U 10017Bromobenzene
010 U 10010Bromochloromethane
017 U 10017Bromodichloromethane
019 U 10019Bromoform
021 U 10021Bromomethane
20 U 50202-Butanone (MEK)
032 U 10032n-Butylbenzene
017 U 10017sec-Butylbenzene
016 U 10016tert-Butylbenzene
045 U 10045Carbon disulfide
019 U 10019Carbon tetrachloride
017 U 10017Chlorobenzene
017 U 10017Dibromochloromethane
041 U 10041Chloroethane
016 U 10016Chloroform
030 U 10030Chloromethane
017 U 100172-Chlorotoluene
021 U 100214-Chlorotoluene
047 U 1004712-Dibromo-3-Chloropropane
017 U 10017Dibromomethane
015 U 1001512-Dichlorobenzene
013 U 1001313-Dichlorobenzene
016 U 1001614-Dichlorobenzene
031 U 10031Dichlorodifluoromethane
022 U 1002211-Dichloroethane
013 U 1001312-Dichloroethane
015 U 10015cis-12-Dichloroethene
015 U 10015trans-12-Dichloroethene
023 U 1002311-Dichloroethene
018 U 1001812-Dichloropropane
022 U 1002213-Dichloropropane
018 U 1001822-Dichloropropane
016 U 10016cis-13-Dichloropropene
019 U 10019trans-13-Dichloropropene
019 U 1001911-Dichloropropene
016 U 10016Ethylbenzene
036 U 10036Hexachlorobutadiene
17 U 50172-Hexanone
019 U 10019Isopropylbenzene
020 U 100204-Isopropyltoluene
032 U 10032Methylene Chloride
098 U 500984-Methyl-2-pentanone
022 U 10022Naphthalene
TestAmerica Denver Page 75 of 962
Quality Control Results
Job Number 280-39772-1Client SM Stoller Corporation
Sdg Number 13025120
WaterClient Matrix
10Dilution
Lab Sample ID
Method Blank - Batch 280-164920
Instrument ID
Lab File ID
Initial WeightVolume
Final WeightVolume
RR1859D
20 mL
20 mLUnits ugL
Method 8260B
Preparation 5030B
VMS_R2MB 280-1649205
Analysis Date 03142013 2102
Analysis Batch
Prep Batch
Leach Batch
NA
NA
280-164920
Prep Date
Leach Date
03142013 2102
NA
Analyte RLMDLQualResult
016 U 10016n-Propylbenzene
017 U 10017Styrene
021 U 100211112-Tetrachloroethane
021 U 100211122-Tetrachloroethane
020 U 10020Tetrachloroethene
017 U 10017Toluene
021 U 10021123-Trichlorobenzene
021 U 10021124-Trichlorobenzene
016 U 10016111-Trichloroethane
027 U 10027112-Trichloroethane
016 U 10016Trichloroethene
029 U 10029Trichlorofluoromethane
033 U 10033123-Trichloropropane
015 U 10015124-Trimethylbenzene
016 U 10016135-Trimethylbenzene
010 U 10010Vinyl chloride
019 U 10019Xylenes Total
018 U 1001812-Dibromoethane
Surrogate Rec Acceptance Limits
12-Dichloroethane-d4 (Surr) 89 70 - 127
Toluene-d8 (Surr) 94 80 - 125
4-Bromofluorobenzene (Surr) 90 78 - 120
Dibromofluoromethane (Surr) 93 77 - 120
TestAmerica Denver Page 76 of 962
Quality Control Results
Job Number 280-39772-1Client SM Stoller Corporation
Sdg Number 13025120
Water
10
Lab Control Sample - Batch 280-164920
Client Matrix
Lab Sample ID
Dilution
Instrument ID
Lab File ID
Initial WeightVolume
Final WeightVolume
RR1858D
20 mL
20 mLUnits ugL
Method 8260B
Preparation 5030B
VMS_R2LCS 280-1649204
Analysis Date 03142013 2039
Analysis Batch
Prep Batch
Leach Batch
280-164920
NA
NA
Prep Date
Leach Date
03142013 2039
NA
Analyte QualLimit RecResultSpike Amount
500 450 90 74 - 135Benzene
500 518 104 73 - 135Bromodichloromethane
500 543 109 67 - 135Carbon tetrachloride
500 435 87 76 - 135Chlorobenzene
500 509 102 76 - 120Chloroform
500 457 91 74 - 13513-Dichlorobenzene
500 456 91 75 - 13511-Dichloroethane
500 461 92 75 - 135trans-12-Dichloroethene
500 515 103 71 - 13611-Dichloroethene
500 458 92 71 - 12012-Dichloropropane
500 457 91 72 - 120Ethylbenzene
500 429 86 54 - 141Methylene Chloride
500 450 90 70 - 135Tetrachloroethene
500 459 92 73 - 120Toluene
500 542 108 70 - 135111-Trichloroethane
500 476 95 73 - 135Trichloroethene
Surrogate Rec Acceptance Limits
12-Dichloroethane-d4 (Surr) 92 70 - 127
Toluene-d8 (Surr) 92 80 - 125
4-Bromofluorobenzene (Surr) 92 78 - 120
Dibromofluoromethane (Surr) 93 77 - 120
TestAmerica Denver Page 77 of 962
Quality Control Results
Job Number 280-39772-1Client SM Stoller Corporation
Sdg Number 13025120
Dilution
Dilution
Water
10
10
Client Matrix
Instrument ID
Lab File ID
Initial WeightVolume
Final WeightVolume
Instrument ID
Lab File ID
Initial WeightVolume
Final WeightVolume
Client Matrix Water
RR1864D
20 mL
20 mL
RR1865D
20 mL
20 mL
Method 8260B
Preparation 5030B
VMS_R2
VMS_R2
280-39772-1
280-39772-1
MS Lab Sample ID
MSD Lab Sample ID
Matrix Spike
Matrix Spike Duplicate Recovery Report - Batch 280-164920
03142013 2258
NA
Analysis Date
Prep Date
Leach Date
Analysis Batch
Prep Batch
Leach Batch
280-164920
NA
NA
Analysis Date
Prep Date
Leach Date
03142013 2321
03142013 2321
NA
Analysis Batch
Prep Batch
Leach Batch
280-164920
NA
NA
03142013 2258
Analyte RPD LimitRPDLimit
Rec
MS MSD MS Qual MSD Qual
96 87 74 - 135 10 20Benzene
101 95 73 - 135 6 20Bromodichloromethane
120 104 67 - 135 14 21Carbon tetrachloride
95 85 76 - 135 11 20Chlorobenzene
107 97 76 - 120 10 20Chloroform
102 91 74 - 135 11 2013-Dichlorobenzene
95 86 75 - 135 10 2111-Dichloroethane
101 92 75 - 135 9 24trans-12-Dichloroethene
111 99 71 - 136 11 2011-Dichloroethene
90 81 71 - 120 11 2012-Dichloropropane
103 92 72 - 120 11 26Ethylbenzene
76 70 54 - 141 8 20Methylene Chloride
103 93 70 - 135 10 20Tetrachloroethene
100 91 73 - 120 10 20Toluene
120 106 70 - 135 12 20111-Trichloroethane
106 96 73 - 135 10 20Trichloroethene
Surrogate Acceptance LimitsMS Rec MSD Rec
12-Dichloroethane-d4 (Surr) 84 85 70 - 127
Toluene-d8 (Surr) 92 90 80 - 125
4-Bromofluorobenzene (Surr) 88 88 78 - 120
Dibromofluoromethane (Surr) 89 89 77 - 120
TestAmerica Denver Page 78 of 962
Quality Control Results
Job Number 280-39772-1Client SM Stoller Corporation
Sdg Number 13025120
Water
03142013 2258 03142013 2321
Dilution Dilution10 10
Client Matrix Client Matrix Water
Method 8260B
Preparation 5030B
Units ugL280-39772-1 280-39772-1MS Lab Sample ID MSD Lab Sample ID
Matrix Spike
Matrix Spike Duplicate Recovery Report - Batch 280-164920
Analysis Date
Prep Date
Leach Date
03142013 2258
NA
Analysis Date
Prep Date
Leach Date
03142013 2321
NA
Amount
Sample
Analyte ResultQual Amount ResultQual ResultQual
MS MSDMS Spike MSD Spike
016 U 500 500 479 433Benzene
017 U 500 500 506 476Bromodichloromethane
019 U 500 500 598 518Carbon tetrachloride
017 U 500 500 476 425Chlorobenzene
016 U 500 500 533 484Chloroform
013 U 500 500 509 45613-Dichlorobenzene
022 U 500 500 475 43011-Dichloroethane
015 U 500 500 504 460trans-12-Dichloroethene
023 U 500 500 556 49511-Dichloroethene
018 U 500 500 450 40412-Dichloropropane
016 U 500 500 513 461Ethylbenzene
032 U 500 500 379 350Methylene Chloride
020 U 500 500 514 466Tetrachloroethene
017 U 500 500 502 454Toluene
016 U 500 500 599 531111-Trichloroethane
016 U 500 500 528 478Trichloroethene
TestAmerica Denver Page 79 of 962
Quality Control Results
Job Number 280-39772-1Client SM Stoller Corporation
Sdg Number 13025120
WaterClient Matrix
10Dilution
Lab Sample ID
Method Blank - Batch 280-164934
Instrument ID
Lab File ID
Initial WeightVolume
Final WeightVolume
g2_6134D
20 mL
20 mLUnits ugL
Method 8260B
Preparation 5030B
VMS_G2MB 280-1649347
Analysis Date 03152013 0716
Analysis Batch
Prep Batch
Leach Batch
NA
NA
280-164934
Prep Date
Leach Date
03152013 0716
NA
Analyte RLMDLQualResult
19 U 1019Acetone
016 U 10016Benzene
017 U 10017Bromobenzene
010 U 10010Bromochloromethane
017 U 10017Bromodichloromethane
019 U 10019Bromoform
021 U 10021Bromomethane
20 U 50202-Butanone (MEK)
032 U 10032n-Butylbenzene
017 U 10017sec-Butylbenzene
016 U 10016tert-Butylbenzene
045 U 10045Carbon disulfide
019 U 10019Carbon tetrachloride
017 U 10017Chlorobenzene
017 U 10017Dibromochloromethane
041 U 10041Chloroethane
016 U 10016Chloroform
030 U 10030Chloromethane
017 U 100172-Chlorotoluene
021 U 100214-Chlorotoluene
047 U 1004712-Dibromo-3-Chloropropane
017 U 10017Dibromomethane
015 U 1001512-Dichlorobenzene
013 U 1001313-Dichlorobenzene
016 U 1001614-Dichlorobenzene
031 U 10031Dichlorodifluoromethane
022 U 1002211-Dichloroethane
013 U 1001312-Dichloroethane
015 U 10015cis-12-Dichloroethene
015 U 10015trans-12-Dichloroethene
023 U 1002311-Dichloroethene
018 U 1001812-Dichloropropane
022 U 1002213-Dichloropropane
018 U 1001822-Dichloropropane
016 U 10016cis-13-Dichloropropene
019 U 10019trans-13-Dichloropropene
019 U 1001911-Dichloropropene
016 U 10016Ethylbenzene
036 U 10036Hexachlorobutadiene
17 U 50172-Hexanone
019 U 10019Isopropylbenzene
020 U 100204-Isopropyltoluene
032 U 10032Methylene Chloride
098 U 500984-Methyl-2-pentanone
022 U 10022Naphthalene
TestAmerica Denver Page 80 of 962
Quality Control Results
Job Number 280-39772-1Client SM Stoller Corporation
Sdg Number 13025120
WaterClient Matrix
10Dilution
Lab Sample ID
Method Blank - Batch 280-164934
Instrument ID
Lab File ID
Initial WeightVolume
Final WeightVolume
g2_6134D
20 mL
20 mLUnits ugL
Method 8260B
Preparation 5030B
VMS_G2MB 280-1649347
Analysis Date 03152013 0716
Analysis Batch
Prep Batch
Leach Batch
NA
NA
280-164934
Prep Date
Leach Date
03152013 0716
NA
Analyte RLMDLQualResult
016 U 10016n-Propylbenzene
017 U 10017Styrene
021 U 100211112-Tetrachloroethane
021 U 100211122-Tetrachloroethane
020 U 10020Tetrachloroethene
017 U 10017Toluene
021 U 10021123-Trichlorobenzene
021 U 10021124-Trichlorobenzene
016 U 10016111-Trichloroethane
027 U 10027112-Trichloroethane
016 U 10016Trichloroethene
029 U 10029Trichlorofluoromethane
033 U 10033123-Trichloropropane
015 U 10015124-Trimethylbenzene
016 U 10016135-Trimethylbenzene
010 U 10010Vinyl chloride
019 U 10019Xylenes Total
018 U 1001812-Dibromoethane
Surrogate Rec Acceptance Limits
12-Dichloroethane-d4 (Surr) 83 70 - 127
Toluene-d8 (Surr) 95 80 - 125
4-Bromofluorobenzene (Surr) 88 78 - 120
Dibromofluoromethane (Surr) 86 77 - 120
TestAmerica Denver Page 81 of 962
Quality Control Results
Job Number 280-39772-1Client SM Stoller Corporation
Sdg Number 13025120
Water
10
Lab Control Sample - Batch 280-164934
Client Matrix
Lab Sample ID
Dilution
Instrument ID
Lab File ID
Initial WeightVolume
Final WeightVolume
g2_6133D
20 mL
20 mLUnits ugL
Method 8260B
Preparation 5030B
VMS_G2LCS 280-1649346
Analysis Date 03152013 0650
Analysis Batch
Prep Batch
Leach Batch
280-164934
NA
NA
Prep Date
Leach Date
03152013 0650
NA
Analyte QualLimit RecResultSpike Amount
500 406 81 74 - 135Benzene
500 379 76 73 - 135Bromodichloromethane
500 379 76 67 - 135Carbon tetrachloride
500 413 83 76 - 135Chlorobenzene
500 396 79 76 - 120Chloroform
500 427 85 74 - 13513-Dichlorobenzene
500 408 82 75 - 13511-Dichloroethane
500 419 84 75 - 135trans-12-Dichloroethene
500 447 89 71 - 13611-Dichloroethene
500 416 83 71 - 12012-Dichloropropane
500 425 85 72 - 120Ethylbenzene
500 275 55 54 - 141Methylene Chloride
500 425 85 70 - 135Tetrachloroethene
500 423 85 73 - 120Toluene
500 392 78 70 - 135111-Trichloroethane
500 400 80 73 - 135Trichloroethene
Surrogate Rec Acceptance Limits
12-Dichloroethane-d4 (Surr) 83 70 - 127
Toluene-d8 (Surr) 95 80 - 125
4-Bromofluorobenzene (Surr) 88 78 - 120
Dibromofluoromethane (Surr) 88 77 - 120
TestAmerica Denver Page 82 of 962
Quality Control Results
Job Number 280-39772-1Client SM Stoller Corporation
Sdg Number 13025120
Dilution
Dilution
Water
10
10
Client Matrix
Instrument ID
Lab File ID
Initial WeightVolume
Final WeightVolume
Instrument ID
Lab File ID
Initial WeightVolume
Final WeightVolume
Client Matrix Water
g2_6139D
20 mL
20 mL
g2_6140D
20 mL
20 mL
Method 8260B
Preparation 5030B
VMS_G2
VMS_G2
280-39751-I-1 MS
280-39751-I-1 MSD
MS Lab Sample ID
MSD Lab Sample ID
Matrix Spike
Matrix Spike Duplicate Recovery Report - Batch 280-164934
03152013 0940
NA
Analysis Date
Prep Date
Leach Date
Analysis Batch
Prep Batch
Leach Batch
280-164934
NA
NA
Analysis Date
Prep Date
Leach Date
03152013 0959
03152013 0959
NA
Analysis Batch
Prep Batch
Leach Batch
280-164934
NA
NA
03152013 0940
Analyte RPD LimitRPDLimit
Rec
MS MSD MS Qual MSD Qual
86 84 74 - 135 2 20Benzene
84 83 73 - 135 2 20Bromodichloromethane
77 77 67 - 135 0 21Carbon tetrachloride
89 85 76 - 135 5 20Chlorobenzene
86 84 76 - 120 3 20Chloroform
86 87 74 - 135 1 2013-Dichlorobenzene
90 87 75 - 135 3 2111-Dichloroethane
85 82 75 - 135 3 24trans-12-Dichloroethene
97 95 71 - 136 2 2011-Dichloroethene
88 87 71 - 120 1 2012-Dichloropropane
90 89 72 - 120 1 26Ethylbenzene
56 56 54 - 141 1 20Methylene Chloride
90 89 70 - 135 2 20Tetrachloroethene
87 86 73 - 120 2 20Toluene
81 79 70 - 135 1 20111-Trichloroethane
84 84 73 - 135 1 20Trichloroethene
Surrogate Acceptance LimitsMS Rec MSD Rec
12-Dichloroethane-d4 (Surr) 87 87 70 - 127
Toluene-d8 (Surr) 99 98 80 - 125
4-Bromofluorobenzene (Surr) 86 86 78 - 120
Dibromofluoromethane (Surr) 91 93 77 - 120
TestAmerica Denver Page 83 of 962
Quality Control Results
Job Number 280-39772-1Client SM Stoller Corporation
Sdg Number 13025120
Water
03152013 0940 03152013 0959
Dilution Dilution10 10
Client Matrix Client Matrix Water
Method 8260B
Preparation 5030B
Units ugL280-39751-I-1 MS 280-39751-I-1 MSDMS Lab Sample ID MSD Lab Sample ID
Matrix Spike
Matrix Spike Duplicate Recovery Report - Batch 280-164934
Analysis Date
Prep Date
Leach Date
03152013 0940
NA
Analysis Date
Prep Date
Leach Date
03152013 0959
NA
Amount
Sample
Analyte ResultQual Amount ResultQual ResultQual
MS MSDMS Spike MSD Spike
016 U 500 500 432 422Benzene
017 U 500 500 422 413Bromodichloromethane
019 U 500 500 387 385Carbon tetrachloride
017 U 500 500 447 427Chlorobenzene
016 U 500 500 428 418Chloroform
013 U 500 500 432 43613-Dichlorobenzene
022 U 500 500 448 43411-Dichloroethane
015 U 500 500 424 409trans-12-Dichloroethene
023 U 500 500 487 47611-Dichloroethene
018 U 500 500 439 43712-Dichloropropane
016 U 500 500 448 443Ethylbenzene
032 U 500 500 281 278Methylene Chloride
020 U 500 500 451 444Tetrachloroethene
017 U 500 500 437 429Toluene
016 U 500 500 403 397111-Trichloroethane
016 U 500 500 420 418Trichloroethene
TestAmerica Denver Page 84 of 962
Quality Control Results
Job Number 280-39772-1Client SM Stoller Corporation
Sdg Number 13025120
WaterClient Matrix
10Dilution
Lab Sample ID
Method Blank - Batch 280-165112
Instrument ID
Lab File ID
Initial WeightVolume
Final WeightVolume
RR1914D
20 mL
20 mLUnits ugL
Method 8260B
Preparation 5030B
VMS_R2MB 280-1651125
Analysis Date 03152013 1939
Analysis Batch
Prep Batch
Leach Batch
NA
NA
280-165112
Prep Date
Leach Date
03152013 1939
NA
Analyte RLMDLQualResult
19 U 1019Acetone
016 U 10016Benzene
017 U 10017Bromobenzene
010 U 10010Bromochloromethane
017 U 10017Bromodichloromethane
019 U 10019Bromoform
021 U 10021Bromomethane
20 U 50202-Butanone (MEK)
032 U 10032n-Butylbenzene
017 U 10017sec-Butylbenzene
016 U 10016tert-Butylbenzene
045 U 10045Carbon disulfide
019 U 10019Carbon tetrachloride
017 U 10017Chlorobenzene
017 U 10017Dibromochloromethane
041 U 10041Chloroethane
016 U 10016Chloroform
030 U 10030Chloromethane
017 U 100172-Chlorotoluene
021 U 100214-Chlorotoluene
047 U 1004712-Dibromo-3-Chloropropane
017 U 10017Dibromomethane
015 U 1001512-Dichlorobenzene
013 U 1001313-Dichlorobenzene
016 U 1001614-Dichlorobenzene
031 U 10031Dichlorodifluoromethane
022 U 1002211-Dichloroethane
013 U 1001312-Dichloroethane
015 U 10015cis-12-Dichloroethene
015 U 10015trans-12-Dichloroethene
023 U 1002311-Dichloroethene
018 U 1001812-Dichloropropane
022 U 1002213-Dichloropropane
018 U 1001822-Dichloropropane
016 U 10016cis-13-Dichloropropene
019 U 10019trans-13-Dichloropropene
019 U 1001911-Dichloropropene
016 U 10016Ethylbenzene
036 U 10036Hexachlorobutadiene
17 U 50172-Hexanone
019 U 10019Isopropylbenzene
020 U 100204-Isopropyltoluene
032 U 10032Methylene Chloride
098 U 500984-Methyl-2-pentanone
022 U 10022Naphthalene
TestAmerica Denver Page 85 of 962
Quality Control Results
Job Number 280-39772-1Client SM Stoller Corporation
Sdg Number 13025120
WaterClient Matrix
10Dilution
Lab Sample ID
Method Blank - Batch 280-165112
Instrument ID
Lab File ID
Initial WeightVolume
Final WeightVolume
RR1914D
20 mL
20 mLUnits ugL
Method 8260B
Preparation 5030B
VMS_R2MB 280-1651125
Analysis Date 03152013 1939
Analysis Batch
Prep Batch
Leach Batch
NA
NA
280-165112
Prep Date
Leach Date
03152013 1939
NA
Analyte RLMDLQualResult
016 U 10016n-Propylbenzene
017 U 10017Styrene
021 U 100211112-Tetrachloroethane
021 U 100211122-Tetrachloroethane
020 U 10020Tetrachloroethene
017 U 10017Toluene
021 U 10021123-Trichlorobenzene
021 U 10021124-Trichlorobenzene
016 U 10016111-Trichloroethane
027 U 10027112-Trichloroethane
016 U 10016Trichloroethene
029 U 10029Trichlorofluoromethane
033 U 10033123-Trichloropropane
015 U 10015124-Trimethylbenzene
016 U 10016135-Trimethylbenzene
010 U 10010Vinyl chloride
019 U 10019Xylenes Total
018 U 1001812-Dibromoethane
Surrogate Rec Acceptance Limits
12-Dichloroethane-d4 (Surr) 73 70 - 127
Toluene-d8 (Surr) 92 80 - 125
4-Bromofluorobenzene (Surr) 84 78 - 120
Dibromofluoromethane (Surr) 82 77 - 120
TestAmerica Denver Page 86 of 962
Quality Control Results
Job Number 280-39772-1Client SM Stoller Corporation
Sdg Number 13025120
Water
10
Lab Control Sample - Batch 280-165112
Client Matrix
Lab Sample ID
Dilution
Instrument ID
Lab File ID
Initial WeightVolume
Final WeightVolume
RR1913D
20 mL
20 mLUnits ugL
Method 8260B
Preparation 5030B
VMS_R2LCS 280-1651124
Analysis Date 03152013 1916
Analysis Batch
Prep Batch
Leach Batch
280-165112
NA
NA
Prep Date
Leach Date
03152013 1916
NA
Analyte QualLimit RecResultSpike Amount
500 525 105 74 - 135Benzene
500 495 99 73 - 135Bromodichloromethane
500 466 93 67 - 135Carbon tetrachloride
500 490 98 76 - 135Chlorobenzene
500 481 96 76 - 120Chloroform
500 492 98 74 - 13513-Dichlorobenzene
500 477 95 75 - 13511-Dichloroethane
500 514 103 75 - 135trans-12-Dichloroethene
500 569 114 71 - 13611-Dichloroethene
500 516 103 71 - 12012-Dichloropropane
500 523 105 72 - 120Ethylbenzene
500 476 95 54 - 141Methylene Chloride
500 490 98 70 - 135Tetrachloroethene
500 513 103 73 - 120Toluene
500 477 95 70 - 135111-Trichloroethane
500 498 100 73 - 135Trichloroethene
Surrogate Rec Acceptance Limits
12-Dichloroethane-d4 (Surr) 82 70 - 127
Toluene-d8 (Surr) 94 80 - 125
4-Bromofluorobenzene (Surr) 86 78 - 120
Dibromofluoromethane (Surr) 84 77 - 120
TestAmerica Denver Page 87 of 962
Quality Control Results
Job Number 280-39772-1Client SM Stoller Corporation
Sdg Number 13025120
Dilution
Dilution
Water
10
10
Client Matrix
Instrument ID
Lab File ID
Initial WeightVolume
Final WeightVolume
Instrument ID
Lab File ID
Initial WeightVolume
Final WeightVolume
Client Matrix Water
RR1916D
20 mL
20 mL
RR1917D
20 mL
20 mL
Method 8260B
Preparation 5030B
VMS_R2
VMS_R2
280-39756-O-16 MS
280-39756-O-16 MSD
MS Lab Sample ID
MSD Lab Sample ID
Matrix Spike
Matrix Spike Duplicate Recovery Report - Batch 280-165112
03152013 2030
NA
Analysis Date
Prep Date
Leach Date
Analysis Batch
Prep Batch
Leach Batch
280-165112
NA
NA
Analysis Date
Prep Date
Leach Date
03152013 2053
03152013 2053
NA
Analysis Batch
Prep Batch
Leach Batch
280-165112
NA
NA
03152013 2030
Analyte RPD LimitRPDLimit
Rec
MS MSD MS Qual MSD Qual
99 92 74 - 135 7 20Benzene
102 99 73 - 135 2 20Bromodichloromethane
90 83 67 - 135 9 21Carbon tetrachloride
92 89 76 - 135 4 20Chlorobenzene
96 92 76 - 120 4 20Chloroform
95 90 74 - 135 5 2013-Dichlorobenzene
92 84 75 - 135 9 2111-Dichloroethane
96 88 75 - 135 8 24trans-12-Dichloroethene
110 99 71 - 136 11 2011-Dichloroethene
101 97 71 - 120 4 2012-Dichloropropane
95 89 72 - 120 6 26Ethylbenzene
84 85 54 - 141 2 20Methylene Chloride
88 81 70 - 135 9 20Tetrachloroethene
98 94 73 - 120 4 20Toluene
93 86 70 - 135 8 20111-Trichloroethane
95 88 73 - 135 8 20Trichloroethene
Surrogate Acceptance LimitsMS Rec MSD Rec
12-Dichloroethane-d4 (Surr) 83 89 70 - 127
Toluene-d8 (Surr) 90 91 80 - 125
4-Bromofluorobenzene (Surr) 87 89 78 - 120
Dibromofluoromethane (Surr) 89 91 77 - 120
TestAmerica Denver Page 88 of 962
Quality Control Results
Job Number 280-39772-1Client SM Stoller Corporation
Sdg Number 13025120
Water
03152013 2030 03152013 2053
Dilution Dilution10 10
Client Matrix Client Matrix Water
Method 8260B
Preparation 5030B
Units ugL280-39756-O-16 MS 280-39756-O-16 MSDMS Lab Sample ID MSD Lab Sample ID
Matrix Spike
Matrix Spike Duplicate Recovery Report - Batch 280-165112
Analysis Date
Prep Date
Leach Date
03152013 2030
NA
Analysis Date
Prep Date
Leach Date
03152013 2053
NA
Amount
Sample
Analyte ResultQual Amount ResultQual ResultQual
MS MSDMS Spike MSD Spike
016 U 500 500 493 460Benzene
017 U 500 500 509 497Bromodichloromethane
019 U 500 500 450 413Carbon tetrachloride
017 U 500 500 460 443Chlorobenzene
016 U 500 500 482 462Chloroform
013 U 500 500 474 44913-Dichlorobenzene
022 U 500 500 460 41911-Dichloroethane
015 U 500 500 478 439trans-12-Dichloroethene
023 U 500 500 551 49611-Dichloroethene
018 U 500 500 506 48612-Dichloropropane
016 U 500 500 474 446Ethylbenzene
032 U 500 500 418 427Methylene Chloride
020 U 500 500 440 404Tetrachloroethene
017 U 500 500 492 472Toluene
016 U 500 500 467 430111-Trichloroethane
016 U 500 500 476 440Trichloroethene
TestAmerica Denver Page 89 of 962
Quality Control Results
Job Number 280-39772-1Client SM Stoller Corporation
Sdg Number 13025120
WaterClient Matrix
10Dilution
Lab Sample ID
Method Blank - Batch 280-164432
Instrument ID
Lab File ID
Initial WeightVolume
Final WeightVolume
E3709D
20 mL
20 mLUnits ugL
Method 8260B SIM
Preparation 5030B
VMS_EMB 280-1644325
Analysis Date 03122013 1959
Analysis Batch
Prep Batch
Leach Batch
NA
NA
280-164432
Prep Date
Leach Date
03122013 1959
NA
Analyte RLMDLQualResult
022 U 1002214-Dioxane
Surrogate Rec Acceptance Limits
12-Dichloroethane-d4 (Surr) 95 70 - 127
Dilution
Dilution
Lab Control Sample
Lab Control Sample Duplicate Recovery Report - Batch 280-164432
10
10
Water
LCS Lab Sample ID
LCSD Lab Sample ID
Client Matrix
Units
Instrument ID
Lab File ID
Initial WeightVolume
Final WeightVolume
Client Matrix Water
Units
Instrument ID
Lab File ID
Initial WeightVolume
Final WeightVolume
ugL
E3707D
20 mL
20 mL
E3708D
20 mL
20 mLugL
Method 8260B SIM
Preparation 5030B
VMS_E
VMS_E
LCS 280-1644323
LCSD 280-1644324
Analysis Date
Prep Date
Leach Date
03122013 1924
03122013 1924
NA
Analysis Batch
Prep Batch
Leach Batch
280-164432
NA
NA
Analysis Date
Prep Date
Leach Date
03122013 1942
03122013 1942
NA
Analysis Batch
Prep Batch
Leach Batch
280-164432
NA
NA
Analyte LCSD QualLCS QualRPD LimitRPDLimitLCSDLCS
Rec
8985 25 - 141 4 2014-Dioxane
Surrogate LCS Rec LCSD Rec Acceptance Limits
12-Dichloroethane-d4 (Surr) 92 94 70 - 127
TestAmerica Denver Page 90 of 962
Quality Control Results
Job Number 280-39772-1Client SM Stoller Corporation
Sdg Number 13025120
Water
03122013 1924
Dilution Dilution10 10
Client Matrix
LCSD Lab Sample ID
Client Matrix Water
Laboratory Control
Laboratory Duplicate Data Report - Batch 280-164432
Method 8260B SIM
Preparation 5030B
Units ugLLCS 280-1644323 LCSD 280-1644324LCS Lab Sample ID
Analysis Date
Prep Date
Leach Date
03122013 1924
Analysis Date
Prep Date
Leach Date
03122013 1942
03122013 1942
NANA
LCSD
ResultQual
LCS
ResultQual
LCSD Spike
Amount
LCS Spike
AmountAnalyte
443426500 50014-Dioxane
Dilution
Dilution
Water
10
10
Client Matrix
Instrument ID
Lab File ID
Initial WeightVolume
Final WeightVolume
Instrument ID
Lab File ID
Initial WeightVolume
Final WeightVolume
Client Matrix Water
E3717D
20 mL
20 mL
E3718D
20 mL
20 mL
Method 8260B SIM
Preparation 5030B
VMS_E
VMS_E
280-39772-2
280-39772-2
MS Lab Sample ID
MSD Lab Sample ID
Matrix Spike
Matrix Spike Duplicate Recovery Report - Batch 280-164432
03122013 2221
NA
Analysis Date
Prep Date
Leach Date
Analysis Batch
Prep Batch
Leach Batch
280-164432
NA
NA
Analysis Date
Prep Date
Leach Date
03122013 2239
03122013 2239
NA
Analysis Batch
Prep Batch
Leach Batch
280-164432
NA
NA
03122013 2221
Analyte RPD LimitRPDLimit
Rec
MS MSD MS Qual MSD Qual
94 97 25 - 141 3 2014-Dioxane
Surrogate Acceptance LimitsMS Rec MSD Rec
12-Dichloroethane-d4 (Surr) 96 98 70 - 127
TestAmerica Denver Page 91 of 962
Quality Control Results
Job Number 280-39772-1Client SM Stoller Corporation
Sdg Number 13025120
Water
03122013 2221 03122013 2239
Dilution Dilution10 10
Client Matrix Client Matrix Water
Method 8260B SIM
Preparation 5030B
Units ugL280-39772-2 280-39772-2MS Lab Sample ID MSD Lab Sample ID
Matrix Spike
Matrix Spike Duplicate Recovery Report - Batch 280-164432
Analysis Date
Prep Date
Leach Date
03122013 2221
NA
Analysis Date
Prep Date
Leach Date
03122013 2239
NA
Amount
Sample
Analyte ResultQual Amount ResultQual ResultQual
MS MSDMS Spike MSD Spike
022 U 500 500 470 48314-Dioxane
TestAmerica Denver Page 92 of 962
Quality Control Results
Job Number 280-39772-1Client SM Stoller Corporation
Sdg Number 13025120
WaterClient Matrix
10Dilution
Lab Sample ID
Method Blank - Batch 280-164670
Instrument ID
Lab File ID
Initial WeightVolume
Final WeightVolume
E3740D
20 mL
20 mLUnits ugL
Method 8260B SIM
Preparation 5030B
VMS_EMB 280-1646705
Analysis Date 03132013 2042
Analysis Batch
Prep Batch
Leach Batch
NA
NA
280-164670
Prep Date
Leach Date
03132013 2042
NA
Analyte RLMDLQualResult
022 U 1002214-Dioxane
Surrogate Rec Acceptance Limits
12-Dichloroethane-d4 (Surr) 105 70 - 127
Dilution
Dilution
Lab Control Sample
Lab Control Sample Duplicate Recovery Report - Batch 280-164670
10
10
Water
LCS Lab Sample ID
LCSD Lab Sample ID
Client Matrix
Units
Instrument ID
Lab File ID
Initial WeightVolume
Final WeightVolume
Client Matrix Water
Units
Instrument ID
Lab File ID
Initial WeightVolume
Final WeightVolume
ugL
E3738D
20 mL
20 mL
E3739D
20 mL
20 mLugL
Method 8260B SIM
Preparation 5030B
VMS_E
VMS_E
LCS 280-1646703
LCSD 280-1646704
Analysis Date
Prep Date
Leach Date
03132013 2007
03132013 2007
NA
Analysis Batch
Prep Batch
Leach Batch
280-164670
NA
NA
Analysis Date
Prep Date
Leach Date
03132013 2025
03132013 2025
NA
Analysis Batch
Prep Batch
Leach Batch
280-164670
NA
NA
Analyte LCSD QualLCS QualRPD LimitRPDLimitLCSDLCS
Rec
7883 25 - 141 7 2014-Dioxane
Surrogate LCS Rec LCSD Rec Acceptance Limits
12-Dichloroethane-d4 (Surr) 106 103 70 - 127
TestAmerica Denver Page 93 of 962
Quality Control Results
Job Number 280-39772-1Client SM Stoller Corporation
Sdg Number 13025120
Water
03132013 2007
Dilution Dilution10 10
Client Matrix
LCSD Lab Sample ID
Client Matrix Water
Laboratory Control
Laboratory Duplicate Data Report - Batch 280-164670
Method 8260B SIM
Preparation 5030B
Units ugLLCS 280-1646703 LCSD 280-1646704LCS Lab Sample ID
Analysis Date
Prep Date
Leach Date
03132013 2007
Analysis Date
Prep Date
Leach Date
03132013 2025
03132013 2025
NANA
LCSD
ResultQual
LCS
ResultQual
LCSD Spike
Amount
LCS Spike
AmountAnalyte
390417500 50014-Dioxane
TestAmerica Denver Page 94 of 962
Quality Control Results
Job Number 280-39772-1Client SM Stoller Corporation
Sdg Number 13025120
WaterClient Matrix
10Dilution
Lab Sample ID
Method Blank - Batch 280-164929
Instrument ID
Lab File ID
Initial WeightVolume
Final WeightVolume
E3783D
20 mL
20 mLUnits ugL
Method 8260B SIM
Preparation 5030B
VMS_EMB 280-16492917
Analysis Date 03142013 2354
Analysis Batch
Prep Batch
Leach Batch
NA
NA
280-164929
Prep Date
Leach Date
03142013 2354
NA
Analyte RLMDLQualResult
022 U 1002214-Dioxane
Surrogate Rec Acceptance Limits
12-Dichloroethane-d4 (Surr) 99 70 - 127
Dilution
Dilution
Lab Control Sample
Lab Control Sample Duplicate Recovery Report - Batch 280-164929
10
10
Water
LCS Lab Sample ID
LCSD Lab Sample ID
Client Matrix
Units
Instrument ID
Lab File ID
Initial WeightVolume
Final WeightVolume
Client Matrix Water
Units
Instrument ID
Lab File ID
Initial WeightVolume
Final WeightVolume
ugL
E3781D
20 mL
20 mL
E3782D
20 mL
20 mLugL
Method 8260B SIM
Preparation 5030B
VMS_E
VMS_E
LCS 280-16492915
LCSD 280-16492916
Analysis Date
Prep Date
Leach Date
03142013 2319
03142013 2319
NA
Analysis Batch
Prep Batch
Leach Batch
280-164929
NA
NA
Analysis Date
Prep Date
Leach Date
03142013 2336
03142013 2336
NA
Analysis Batch
Prep Batch
Leach Batch
280-164929
NA
NA
Analyte LCSD QualLCS QualRPD LimitRPDLimitLCSDLCS
Rec
8980 25 - 141 10 2014-Dioxane
Surrogate LCS Rec LCSD Rec Acceptance Limits
12-Dichloroethane-d4 (Surr) 102 97 70 - 127
TestAmerica Denver Page 95 of 962
Quality Control Results
Job Number 280-39772-1Client SM Stoller Corporation
Sdg Number 13025120
Water
03142013 2319
Dilution Dilution10 10
Client Matrix
LCSD Lab Sample ID
Client Matrix Water
Laboratory Control
Laboratory Duplicate Data Report - Batch 280-164929
Method 8260B SIM
Preparation 5030B
Units ugLLCS 280-16492915 LCSD 280-16492916LCS Lab Sample ID
Analysis Date
Prep Date
Leach Date
03142013 2319
Analysis Date
Prep Date
Leach Date
03142013 2336
03142013 2336
NANA
LCSD
ResultQual
LCS
ResultQual
LCSD Spike
Amount
LCS Spike
AmountAnalyte
443400500 50014-Dioxane
Dilution
Dilution
Water
10
10
Client Matrix
Instrument ID
Lab File ID
Initial WeightVolume
Final WeightVolume
Instrument ID
Lab File ID
Initial WeightVolume
Final WeightVolume
Client Matrix Water
E3787D
1 mL
20 mL
E3788D
1 mL
20 mL
Method 8260B SIM
Preparation 5030B
VMS_E
VMS_E
280-39873-C-4 MS
280-39873-C-4 MSD
MS Lab Sample ID
MSD Lab Sample ID
Matrix Spike
Matrix Spike Duplicate Recovery Report - Batch 280-164929
03152013 0104
NA
Analysis Date
Prep Date
Leach Date
Analysis Batch
Prep Batch
Leach Batch
280-164929
NA
NA
Analysis Date
Prep Date
Leach Date
03152013 0121
03152013 0121
NA
Analysis Batch
Prep Batch
Leach Batch
280-164929
NA
NA
03152013 0104
Analyte RPD LimitRPDLimit
Rec
MS MSD MS Qual MSD Qual
125 154 25 - 141 10 20 F14-Dioxane
Surrogate Acceptance LimitsMS Rec MSD Rec
12-Dichloroethane-d4 (Surr) 97 100 70 - 127
TestAmerica Denver Page 96 of 962
Quality Control Results
Job Number 280-39772-1Client SM Stoller Corporation
Sdg Number 13025120
Water
03152013 0104 03152013 0121
Dilution Dilution10 10
Client Matrix Client Matrix Water
Method 8260B SIM
Preparation 5030B
Units ugL280-39873-C-4 MS 280-39873-C-4 MSDMS Lab Sample ID MSD Lab Sample ID
Matrix Spike
Matrix Spike Duplicate Recovery Report - Batch 280-164929
Analysis Date
Prep Date
Leach Date
03152013 0104
NA
Analysis Date
Prep Date
Leach Date
03152013 0121
NA
Amount
Sample
Analyte ResultQual Amount ResultQual ResultQual
MS MSDMS Spike MSD Spike
170 100 100 292 322 F14-Dioxane
TestAmerica Denver Page 97 of 962
Quality Control Results
Job Number 280-39772-1Client SM Stoller Corporation
Sdg Number 13025120
WaterClient Matrix
10Dilution
Lab Sample ID
Method Blank - Batch 280-165111
Instrument ID
Lab File ID
Initial WeightVolume
Final WeightVolume
E3822D
20 mL
20 mLUnits ugL
Method 8260B SIM
Preparation 5030B
VMS_EMB 280-1651115
Analysis Date 03152013 1916
Analysis Batch
Prep Batch
Leach Batch
NA
NA
280-165111
Prep Date
Leach Date
03152013 1916
NA
Analyte RLMDLQualResult
022 U 1002214-Dioxane
Surrogate Rec Acceptance Limits
12-Dichloroethane-d4 (Surr) 99 70 - 127
Dilution
Dilution
Lab Control Sample
Lab Control Sample Duplicate Recovery Report - Batch 280-165111
10
10
Water
LCS Lab Sample ID
LCSD Lab Sample ID
Client Matrix
Units
Instrument ID
Lab File ID
Initial WeightVolume
Final WeightVolume
Client Matrix Water
Units
Instrument ID
Lab File ID
Initial WeightVolume
Final WeightVolume
ugL
E3820D
20 mL
20 mL
E3821D
20 mL
20 mLugL
Method 8260B SIM
Preparation 5030B
VMS_E
VMS_E
LCS 280-1651113
LCSD 280-1651114
Analysis Date
Prep Date
Leach Date
03152013 1841
03152013 1841
NA
Analysis Batch
Prep Batch
Leach Batch
280-165111
NA
NA
Analysis Date
Prep Date
Leach Date
03152013 1859
03152013 1859
NA
Analysis Batch
Prep Batch
Leach Batch
280-165111
NA
NA
Analyte LCSD QualLCS QualRPD LimitRPDLimitLCSDLCS
Rec
8278 25 - 141 5 2014-Dioxane
Surrogate LCS Rec LCSD Rec Acceptance Limits
12-Dichloroethane-d4 (Surr) 103 105 70 - 127
TestAmerica Denver Page 98 of 962
Quality Control Results
Job Number 280-39772-1Client SM Stoller Corporation
Sdg Number 13025120
Water
03152013 1841
Dilution Dilution10 10
Client Matrix
LCSD Lab Sample ID
Client Matrix Water
Laboratory Control
Laboratory Duplicate Data Report - Batch 280-165111
Method 8260B SIM
Preparation 5030B
Units ugLLCS 280-1651113 LCSD 280-1651114LCS Lab Sample ID
Analysis Date
Prep Date
Leach Date
03152013 1841
Analysis Date
Prep Date
Leach Date
03152013 1859
03152013 1859
NANA
LCSD
ResultQual
LCS
ResultQual
LCSD Spike
Amount
LCS Spike
AmountAnalyte
409391500 50014-Dioxane
Dilution
Dilution
Water
10
10
Client Matrix
Instrument ID
Lab File ID
Initial WeightVolume
Final WeightVolume
Instrument ID
Lab File ID
Initial WeightVolume
Final WeightVolume
Client Matrix Water
E3824D
10 mL
20 mL
E3825D
10 mL
20 mL
Method 8260B SIM
Preparation 5030B
VMS_E
VMS_E
280-39873-A-2 MS
280-39873-A-2 MSD
MS Lab Sample ID
MSD Lab Sample ID
Matrix Spike
Matrix Spike Duplicate Recovery Report - Batch 280-165111
03152013 1951
NA
Analysis Date
Prep Date
Leach Date
Analysis Batch
Prep Batch
Leach Batch
280-165111
NA
NA
Analysis Date
Prep Date
Leach Date
03152013 2009
03152013 2009
NA
Analysis Batch
Prep Batch
Leach Batch
280-165111
NA
NA
03152013 1951
Analyte RPD LimitRPDLimit
Rec
MS MSD MS Qual MSD Qual
89 94 25 - 141 5 2014-Dioxane
Surrogate Acceptance LimitsMS Rec MSD Rec
12-Dichloroethane-d4 (Surr) 98 102 70 - 127
TestAmerica Denver Page 99 of 962
Quality Control Results
Job Number 280-39772-1Client SM Stoller Corporation
Sdg Number 13025120
Water
03152013 1951 03152013 2009
Dilution Dilution10 10
Client Matrix Client Matrix Water
Method 8260B SIM
Preparation 5030B
Units ugL280-39873-A-2 MS 280-39873-A-2 MSDMS Lab Sample ID MSD Lab Sample ID
Matrix Spike
Matrix Spike Duplicate Recovery Report - Batch 280-165111
Analysis Date
Prep Date
Leach Date
03152013 1951
NA
Analysis Date
Prep Date
Leach Date
03152013 2009
NA
Amount
Sample
Analyte ResultQual Amount ResultQual ResultQual
MS MSDMS Spike MSD Spike
044 U 100 100 895 94414-Dioxane
TestAmerica Denver Page 100 of 962
Quality Control Results
Client SM Stoller Corporation Job Number 280-39772-1
QC Association Summary
Lab Sample ID Client Sample ID Client Matrix Method Prep Batch
Sdg Number 13025120
Report
Basis
GCMS VOA
Analysis Batch280-164432
Lab Control Sample Water 8260B SIMLCS 280-1644323 T
Lab Control Sample Duplicate Water 8260B SIMLCSD 280-1644324 T
Method Blank Water 8260B SIMMB 280-1644325 T
WaterPIN12-0555A 8260B SIM280-39772-1 T
WaterPIN12-0555B 8260B SIM280-39772-2 T
Matrix Spike Water 8260B SIM280-39772-2MS T
Matrix Spike Duplicate Water 8260B SIM280-39772-2MSD T
WaterPIN12-0555C 8260B SIM280-39772-3 T
WaterPIN12-0565-1 8260B SIM280-39772-4 T
WaterPIN12-0565-2 8260B SIM280-39772-5 T
WaterPIN12-0565-3 8260B SIM280-39772-6 T
WaterPIN12-0573-1 8260B SIM280-39772-7 T
WaterPIN12-0573-2 8260B SIM280-39772-8 T
WaterPIN12-0573-3 8260B SIM280-39772-9 T
WaterPIN12-0575-1 8260B SIM280-39772-10 T
WaterPIN12-0575-2 8260B SIM280-39772-11 T
WaterPIN12-0580-1 8260B SIM280-39772-12 T
Analysis Batch280-164670
Lab Control Sample Water 8260B SIMLCS 280-1646703 T
Lab Control Sample Duplicate Water 8260B SIMLCSD 280-1646704 T
Method Blank Water 8260B SIMMB 280-1646705 T
WaterPIN12-0580-2 8260B SIM280-39772-13 T
WaterPIN12-S67B 8260B SIM280-39772-16 T
WaterPIN12-S67D 8260B SIM280-39772-18 T
Analysis Batch280-164920
Lab Control Sample Water 8260BLCS 280-1649204 T
Method Blank Water 8260BMB 280-1649205 T
WaterPIN12-0555A 8260B280-39772-1 T
Matrix Spike Water 8260B280-39772-1MS T
Matrix Spike Duplicate Water 8260B280-39772-1MSD T
WaterPIN12-0555B 8260B280-39772-2 T
WaterPIN12-0555C 8260B280-39772-3 T
WaterPIN12-0580-1 8260B280-39772-12 T
WaterPIN12-0580-2 8260B280-39772-13 T
WaterPIN12-0580-3 8260B280-39772-14 T
WaterPIN12-2450 8260B280-39772-15 T
WaterPIN12-S67B 8260B280-39772-16 T
WaterPIN12-S67C 8260B280-39772-17 T
WaterPIN12-S67D 8260B280-39772-18 T
TestAmerica Denver
Page 101 of 962
Quality Control Results
Client SM Stoller Corporation Job Number 280-39772-1
QC Association Summary
Lab Sample ID Client Sample ID Client Matrix Method Prep Batch
Sdg Number 13025120
Report
Basis
GCMS VOA
Analysis Batch280-164929
Lab Control Sample Water 8260B SIMLCS 280-16492915 T
Lab Control Sample Duplicate Water 8260B SIMLCSD 280-16492916 T
Method Blank Water 8260B SIMMB 280-16492917 T
WaterPIN12-0580-3 8260B SIM280-39772-14 T
WaterPIN12-2450 8260B SIM280-39772-15 T
Matrix Spike Water 8260B SIM280-39873-C-4 MS T
Matrix Spike Duplicate Water 8260B SIM280-39873-C-4 MSD T
Analysis Batch280-164934
Lab Control Sample Water 8260BLCS 280-1649346 T
Method Blank Water 8260BMB 280-1649347 T
Matrix Spike Water 8260B280-39751-I-1 MS T
Matrix Spike Duplicate Water 8260B280-39751-I-1 MSD T
WaterPIN12-0565-1 8260B280-39772-4 T
WaterPIN12-0565-2 8260B280-39772-5 T
WaterPIN12-0565-3 8260B280-39772-6 T
WaterPIN12-0573-1 8260B280-39772-7 T
WaterPIN12-0573-2 8260B280-39772-8 T
WaterPIN12-0573-3 8260B280-39772-9 T
WaterPIN12-0575-1 8260B280-39772-10 T
WaterPIN12-0575-2 8260B280-39772-11 T
WaterPIN99-2198 8260B280-39772-19 T
Analysis Batch280-165111
Lab Control Sample Water 8260B SIMLCS 280-1651113 T
Lab Control Sample Duplicate Water 8260B SIMLCSD 280-1651114 T
Method Blank Water 8260B SIMMB 280-1651115 T
WaterPIN12-S67C 8260B SIM280-39772-17 T
Matrix Spike Water 8260B SIM280-39873-A-2 MS T
Matrix Spike Duplicate Water 8260B SIM280-39873-A-2 MSD T
Analysis Batch280-165112
Lab Control Sample Water 8260BLCS 280-1651124 T
Method Blank Water 8260BMB 280-1651125 T
Matrix Spike Water 8260B280-39756-O-16 MS T
Matrix Spike Duplicate Water 8260B280-39756-O-16 MSD T
WaterPIN12-0580-2 8260B280-39772-13DL T
WaterPIN12-2450 8260B280-39772-15DL T
WaterPIN12-S67B 8260B280-39772-16DL T
WaterPIN12-S67C 8260B280-39772-17DL T
Report Basis
T = Total
TestAmerica Denver
Page 102 of 962
ANALYTICAL REPORT
Job Number 280-39873-1
SDG Number 13025120
Job Description PINELLAS MONITORING
ForSM Stoller Corporation
2597 Legacy WayGrand Junction CO 81503
Attention Mr Steve Donivan
_____________________________________________
Approved for releaseKae E YoderProject Manager II3272013 1213 PM
Kae E YoderProject Manager II
kaeyodertestamericainccom03272013
The test results in this report relate only to the samples in this report and meet all requirements of NELAC with anyexceptions noted Pursuant to NELAP this report shall not be reproduced except in full without the written approval ofthe laboratory All questions regarding this report should be directed to the TestAmerica Denver Project Manager
The Lab Certification ID is E87667
Reporting limits are adjusted for sample size used dilutions and moisture content if applicable
TestAmerica Laboratories Inc
TestAmerica Denver 4955 Yarrow Street Arvada CO 80002
Tel (303) 736-0100 Fax (303) 431-7171 wwwtestamericainccom
Page 1 of 1510
Pages have been deleted from this laboratory report file to reduce file size The deleted pages contain raw data and instrument calibrations If the full laboratory report is needed contact ScottSurovchaklmdoegov
Table of ContentsCover Title Page 1
Data Summaries 4
Report Narrative 4
Data Qualifiers 6
Sample Summary 7
Executive Summary 8
Method Summary 12
Method Analyst Summary 13
Sample Datasheets 14
Surrogate Summary 99
QC Data Summary 103
QC Association Summary 137
Lab Chronicle 140
Manual Integration Summary 150
Organic Sample Data 196
GCMS VOA 196
Method 8260B 196Method 8260B QC Summary 197Method 8260B Sample Data 229Standards Data 500
Method 8260B ICAL Data 500Method 8260B CCAL Data 763
Raw QC Data 877Method 8260B Tune Data 877Method 8260B Blank Data 907Method 8260B LCSLCSD Data 935
Page 2 of 1510
Table of ContentsMethod 8260B MSMSD Data 960
Method 8260B Run Logs 1020
Method 8260B SIM 1153Method 8260B SIM QC Summary 1154Method 8260B SIM Sample Data 1188Standards Data 1273
Method 8260B SIM ICAL Data 1273Method 8260B SIM CCAL Data 1359
Raw QC Data 1379Method 8260B SIM Tune Data 1379Method 8260B SIM Blank Data 1397Method 8260B SIM LCSLCSD Data 1412Method 8260B SIM MSMSD Data 1447
Method 8260B SIM Run Logs 1476
Shipping and Receiving Documents 1506
Client Chain of Custody 1507
Sample Receipt Checklist 1509
Page 3 of 1510
CASE NARRATIVE
Client SM Stoller Corporation
Project PINELLAS MONITORING - 13025120
Report Number 280-39873-1
With exceptions noted as flags or footnotes standard analytical protocols were followed in the analysis of the samples and no problems
were encountered or anomalies observed All laboratory quality control samples analyzed in conjunction with the samples in this project
were within established control limits with any exceptions noted Calculations are performed before rounding to avoid round-off errors in
calculated results
This report includes reporting limits (RLs) less than TestAmerica Denvers practical quantitation limits These reporting limits are being
used specifically at the clients request to meet the needs of this project Please note that data are not normally reported to these levels
without qualification since they are inherently less reliable and potentially less defensible than required by the current NELAC standards
Results between the method detection limit (MDL) and reporting limit (RL) are flagged with a J qualifier to indicate an estimated value
These results are statistically less reliable than results greater than or equal to the RL and should be considered a qualitative value
All holding times were met and proper preservation noted for the methods performed on these samples unless otherwise detailed in the
individual sections below
RECEIPT
The samples were received on 3132013 900 AM the samples arrived in good condition properly preserved and where required on
ice The temperature of the cooler at receipt was 17ordm C
GCMS VOLATILES - SW846 8260B
In some cases due to high concentrations of target analytes andor the nature of the sample matrix (foamy) reduced aliquot sizes had to
be used for the analysis of samples The reporting limits have been elevated accordingly To provide the lowest possible detection limits
multiple runs are reported where available
Sample PIN12-0539 (LDU 854) was received at the laboratory with insufficient preservation measuring a pH of 7 If samples are not
preserved to a pH of 20 and analyses are performed outside a 7 day holding time experimental evidence suggests that some aromatic
compounds in wastewater samples notably benzene toluene and ethylbenzene are susceptible to biological degradation The sample
was analyzed within the normal 14 day holding time but outside a 7 day holding time
The MSD aliquot of the MSMSD performed on sample PIN12-0524 (LDU 852) in batch 280-165236 exhibited spike compound recoveries
outside the control limits biased high The LCS was within control limits
The accuracy and precision of the MSMSD associated with batch 280-165434 could not be reliably evaluated for some compounds as
the concentrations present in the parent sample are 4 times greater than the matrix spike concentrations In addition MS andor MSD
concentrations are present above the instrument calibration range for some compounds The LCS and LCSD were within control limits
The MSMSD associated with batch 280-165627 exhibited percent recoveries outside the control limits biased high for
11-Dichloroethane The LCS was within control limits
No other anomalies were encountered
GCMS VOLATILES - SW846 8260B SIM - 14-Dioxane
In some cases due to the nature of the sample matrix (foamy) andor due to high constituent concentration samples had to be analyzed
using reduced aliquot sizes The reporting limits have been elevated accordingly
Surrogate 12-Dichloroethane-d4 was recovered outside the control limits biased high in samples PIN12-0581-1 (LDU-876)
PIN12-0581-2 (LDU 877) and PIN12-0582-1 (LDU 879) As no detectable concentrations are present in the sampleS data are reported
as is
In some cases the internal standard response for 14-Dichlorobenzene-d4 was outside acceptance criteria for samples in batch
280-165111 As this internal standard is not associated with the analyte of interest (14-Dioxane) data are reported as is
MSMSD data is not available for batch 280-164670 due to a QC failure associated with the parent sample requiring reanalysis Method
precision and accuracy have been verified by the acceptable LCSLCSD analysis data
The MSD aliquot of the MSMSD performed on sample PIN12-0540 (LDU 855) in batch 280-164929 exhibited the percent recovery
outside the control limits biased high The LCS and LCSD were within control limits
Page 4 of 1510
The RPD limit was exceeded in the MSMSD associated with batch 280-165812 Method precision and accuracy have been verified by
the acceptable LCSLCSD analysis data
The MSMSD associated with batch 280-166279 exhibited percent recoveries outside the control limits biased high It can be noted that
the MS and MSD concentrations were present above the instrument calibration range The LCS and LCSD were within control limits
No other anomalies were encountered
Page 5 of 1510
DATA REPORTING QUALIFIERS
Client SM Stoller Corporation Job Number 280-39873-1
Lab Section Qualifier Description
Sdg Number 13025120
GCMS VOA
Indicates the analyte was analyzed for but not detectedU
MS or MSD exceeds the control limitsF
MS MSD The analyte present in the original sample is 4 times greater
than the matrix spike concentration therefore control limits are not
applicable
4
Result exceeded calibration rangeE
Result is less than the RL but greater than or equal to the MDL and the
concentration is an approximate value
J
RPD of the MS and MSD exceeds the control limitsF
Surrogate is outside control limitsX
TestAmerica Denver Page 6 of 1510
SAMPLE SUMMARY
Client SM Stoller Corporation Job Number 280-39873-1
Sdg Number 13025120
Client Sample IDLab Sample ID Client Matrix Sampled Received
DateTime DateTime
280-39873-1 PIN12-0524 Water 03092013 0748 03132013 0900
280-39873-1MS PIN12-0524 Water 03092013 0748 03132013 0900
280-39873-1MSD PIN12-0524 Water 03092013 0748 03132013 0900
280-39873-2 PIN12-0525 Water 03092013 0826 03132013 0900
280-39873-2MS PIN12-0525 Water 03092013 0826 03132013 0900
280-39873-2MSD PIN12-0525 Water 03092013 0826 03132013 0900
280-39873-3 PIN12-0539 Water 03082013 1635 03132013 0900
280-39873-4 PIN12-0540 Water 03082013 1548 03132013 0900
280-39873-5 PIN12-0541 Water 03082013 1241 03132013 0900
280-39873-6 PIN12-0542 Water 03082013 1310 03132013 0900
280-39873-7 PIN12-0549 Water 03082013 1413 03132013 0900
280-39873-8 PIN12-0554A Water 03082013 0919 03132013 0900
280-39873-9 PIN12-0554B Water 03082013 1005 03132013 0900
280-39873-10 PIN12-0554C Water 03082013 1110 03132013 0900
280-39873-11 PIN12-0581-1 Water 03112013 0851 03132013 0900
280-39873-12 PIN12-0581-2 Water 03112013 0923 03132013 0900
280-39873-13 PIN12-0581-3 Water 03112013 1025 03132013 0900
280-39873-14 PIN12-0582-1 Water 03112013 1147 03132013 0900
280-39873-15 PIN12-0582-2 Water 03112013 1218 03132013 0900
280-39873-16 PIN12-0582-3 Water 03112013 1253 03132013 0900
280-39873-17 PIN12-0585-3 Water 03092013 1133 03132013 0900
280-39873-18 PIN12-2451 Water 03112013 1200 03132013 0900
280-39873-19 PIN12-2452 Water 03112013 1210 03132013 0900
280-39873-20 PIN12-S71B Water 03092013 0908 03132013 0900
280-39873-21 PIN12-S71C Water 03092013 0936 03132013 0900
280-39873-22 PIN12-S71D Water 03092013 1026 03132013 0900
280-39873-23 PIN12-S73B Water 03112013 1430 03132013 0900
280-39873-24 PIN12-S73C Water 03112013 1603 03132013 0900
280-39873-25 PIN12-S73D Water 03112013 1648 03132013 0900
280-39873-26 PIN99-2448 Water 03082013 0900 03132013 0900
TestAmerica Denver Page 7 of 1510
EXECUTIVE SUMMARY - Detections
Client SM Stoller Corporation Job Number 280-39873-1
Analyte Result
Reporting
Limit Units Method
Lab Sample ID Client Sample ID
Sdg Number 13025120
Qualifier
280-39873-1 PIN12-0524
20 ugL 8260B19 JBenzene
20 ugL 8260B570cis-12-Dichloroethene
20 ugL 8260B71trans-12-Dichloroethene
20 ugL 8260B1611-Dichloroethene
20 ugL 8260B600Vinyl chloride
280-39873-2 PIN12-0525
10 ugL 8260B13cis-12-Dichloroethene
280-39873-3 PIN12-0539
10 ugL 8260B47 JAcetone
10 ugL 8260B4811-Dichloroethane
10 ugL 8260B16cis-12-Dichloroethene
10 ugL 8260B13trans-12-Dichloroethene
40 ugL 8260B53Vinyl chloride
40 ugL 8260B SIM3814-Dioxane
280-39873-4 PIN12-0540
10 ugL 8260B57 JAcetone
10 ugL 8260B2011-Dichloroethane
10 ugL 8260B12cis-12-Dichloroethene
10 ugL 8260B68trans-12-Dichloroethene
10 ugL 8260B230Vinyl chloride
20 ugL 8260B SIM17014-Dioxane
280-39873-5 PIN12-0541
10 ugL 8260B10Acetone
10 ugL 8260B020 Jcis-12-Dichloroethene
280-39873-6 PIN12-0542
40 ugL 8260B44Methylene Chloride
280-39873-7 PIN12-0549
10 ugL 8260B14Acetone
10 ugL 8260B024 J11-Dichloroethane
10 ugL 8260B017 Jcis-12-Dichloroethene
TestAmerica Denver Page 8 of 1510
EXECUTIVE SUMMARY - Detections
Client SM Stoller Corporation Job Number 280-39873-1
Analyte Result
Reporting
Limit Units Method
Lab Sample ID Client Sample ID
Sdg Number 13025120
Qualifier
280-39873-8 PIN12-0554A
10 ugL 8260B98 JAcetone
280-39873-10 PIN12-0554C
10 ugL 8260B67 JAcetone
20 ugL 8260B6411-Dichloroethane
10 ugL 8260B16cis-12-Dichloroethene
10 ugL 8260B55trans-12-Dichloroethene
10 ugL 8260B1011-Dichloroethene
20 ugL 8260B88Vinyl chloride
50 ugL 8260B SIM7614-Dioxane
280-39873-11 PIN12-0581-1
10 ugL 8260B87 JAcetone
10 ugL 8260B089 J11-Dichloroethane
10 ugL 8260B026 Jcis-12-Dichloroethene
10 ugL 8260B050 JVinyl chloride
280-39873-12 PIN12-0581-2
10 ugL 8260B94 J11-Dichloroethane
10 ugL 8260B29 Jcis-12-Dichloroethene
10 ugL 8260B37 JMethylene Chloride
280-39873-13 PIN12-0581-3
20 ugL 8260B93 JAcetone
280-39873-14 PIN12-0582-1
10 ugL 8260B73 JAcetone
10 ugL 8260B043 J11-Dichloroethane
10 ugL 8260B12Vinyl chloride
280-39873-15 PIN12-0582-2
20 ugL 8260B73 JAcetone
20 ugL 8260B4911-Dichloroethane
20 ugL 8260B13cis-12-Dichloroethene
20 ugL 8260B23trans-12-Dichloroethene
20 ugL 8260B063 J11-Dichloroethene
10 ugL 8260B74Vinyl chloride
TestAmerica Denver Page 9 of 1510
EXECUTIVE SUMMARY - Detections
Client SM Stoller Corporation Job Number 280-39873-1
Analyte Result
Reporting
Limit Units Method
Lab Sample ID Client Sample ID
Sdg Number 13025120
Qualifier
280-39873-16 PIN12-0582-3
10 ugL 8260B020 Jcis-12-Dichloroethene
10 ugL 8260B12Vinyl chloride
280-39873-17 PIN12-0585-3
10 ugL 8260B41Carbon disulfide
50 ugL 8260B140cis-12-Dichloroethene
10 ugL 8260B11trans-12-Dichloroethene
10 ugL 8260B4011-Dichloroethene
50 ugL 8260B39 J2-Hexanone
10 ugL 8260B071 JTrichloroethene
50 ugL 8260B200Vinyl chloride
280-39873-18 PIN12-2451
10 ugL 8260B1211-Dichloroethane
10 ugL 8260B36cis-12-Dichloroethene
10 ugL 8260B047 J11-Dichloroethene
10 ugL 8260B73Vinyl chloride
280-39873-19 PIN12-2452
10 ugL 8260B4611-Dichloroethane
10 ugL 8260B13cis-12-Dichloroethene
10 ugL 8260B25trans-12-Dichloroethene
10 ugL 8260B072 J11-Dichloroethene
10 ugL 8260B023 JNaphthalene
40 ugL 8260B130Vinyl chloride
40 ugL 8260B SIM17014-Dioxane
280-39873-21 PIN12-S71C
10 ugL 8260B2911-Dichloroethane
10 ugL 8260B18cis-12-Dichloroethene
10 ugL 8260B10trans-12-Dichloroethene
10 ugL 8260B029 J11-Dichloroethene
10 ugL 8260B44Vinyl chloride
20 ugL 8260B SIM3414-Dioxane
TestAmerica Denver Page 10 of 1510
EXECUTIVE SUMMARY - Detections
Client SM Stoller Corporation Job Number 280-39873-1
Analyte Result
Reporting
Limit Units Method
Lab Sample ID Client Sample ID
Sdg Number 13025120
Qualifier
280-39873-22 PIN12-S71D
10 ugL 8260B2811-Dichloroethane
10 ugL 8260B29cis-12-Dichloroethene
10 ugL 8260B17trans-12-Dichloroethene
10 ugL 8260B060 J11-Dichloroethene
10 ugL 8260B60Vinyl chloride
280-39873-23 PIN12-S73B
10 ugL 8260B036 J11-Dichloroethane
10 ugL 8260B14cis-12-Dichloroethene
10 ugL 8260B050 Jtrans-12-Dichloroethene
10 ugL 8260B11Vinyl chloride
280-39873-24 PIN12-S73C
10 ugL 8260B1111-Dichloroethane
10 ugL 8260B18cis-12-Dichloroethene
10 ugL 8260B17trans-12-Dichloroethene
10 ugL 8260B047 J11-Dichloroethene
50 ugL 8260B230Vinyl chloride
10 ugL 8260B SIM13014-Dioxane
280-39873-25 PIN12-S73D
10 ugL 8260B021 Jcis-12-Dichloroethene
10 ugL 8260B047 JVinyl chloride
TestAmerica Denver Page 11 of 1510
METHOD SUMMARY
Client SM Stoller Corporation Job Number 280-39873-1
Sdg Number 13025120
Preparation MethodMethodLab LocationDescription
Matrix Water
Volatile Organic Compounds (GCMS) TAL DEN SW846 8260B
Purge and Trap TAL DEN SW846 5030B
Volatile Organic Compounds (GCMS-SIM) TAL DEN SW846 8260B SIM
Purge and Trap TAL DEN SW846 5030B
Lab References
TAL DEN = TestAmerica Denver
Method References
SW846 = Test Methods For Evaluating Solid Waste PhysicalChemical Methods Third Edition November 1986 And Its Updates
TestAmerica Denver Page 12 of 1510
METHOD ANALYST SUMMARY
Client SM Stoller Corporation Job Number 280-39873-1
Method Analyst Analyst ID
Sdg Number 13025120
Dobransky Michael E MDSW846 8260B
Meier Greg P GPMSW846 8260B
Wickham Tom TWSW846 8260B
Tinkham Sarah A SATSW846 8260B SIM
TestAmerica Denver
Page 13 of 1510
Analytical Data
Client SM Stoller Corporation Job Number 280-39873-1
Sdg Number 13025120
Client Sample ID
Lab Sample ID
PIN12-0524
Client Matrix
280-39873-1
Water
Date Sampled 03092013 0748
Date Received 03132013 0900
8260B Volatile Organic Compounds (GCMS)
Dilution
03182013 1142
03182013 1142
10
8260B
Final WeightVolume
Initial WeightVolume
Lab File ID
Instrument ID
C5339D
10 mL
20 mL
5030B
VMS_C
Analysis Date
Prep Date
Analysis Batch
Prep Batch
280-165236
NA
Analysis Method
Prep Method
Analyte Result (ugL) Qualifier MDL RL
38 U 2038Acetone
19 J 20032Benzene
034 U 20034Bromobenzene
020 U 20020Bromochloromethane
034 U 20034Bromodichloromethane
038 U 20038Bromoform
042 U 20042Bromomethane
40 U 10402-Butanone (MEK)
064 U 20064n-Butylbenzene
034 U 20034sec-Butylbenzene
032 U 20032tert-Butylbenzene
090 U 20090Carbon disulfide
038 U 20038Carbon tetrachloride
034 U 20034Chlorobenzene
034 U 20034Dibromochloromethane
082 U 20082Chloroethane
032 U 20032Chloroform
060 U 20060Chloromethane
034 U 200342-Chlorotoluene
042 U 200424-Chlorotoluene
094 U 2009412-Dibromo-3-Chloropropane
034 U 20034Dibromomethane
030 U 2003012-Dichlorobenzene
026 U 2002613-Dichlorobenzene
032 U 2003214-Dichlorobenzene
062 U 20062Dichlorodifluoromethane
044 U 2004411-Dichloroethane
026 U 2002612-Dichloroethane
71 20030trans-12-Dichloroethene
16 2004611-Dichloroethene
036 U 2003612-Dichloropropane
044 U 2004413-Dichloropropane
036 U 2003622-Dichloropropane
032 U 20032cis-13-Dichloropropene
038 U 20038trans-13-Dichloropropene
038 U 2003811-Dichloropropene
032 U 20032Ethylbenzene
072 U 20072Hexachlorobutadiene
34 U 10342-Hexanone
038 U 20038Isopropylbenzene
040 U 200404-Isopropyltoluene
064 U 20064Methylene Chloride
20 U 10204-Methyl-2-pentanone
044 U 20044Naphthalene
032 U 20032n-Propylbenzene
034 U 20034Styrene
TestAmerica Denver Page 14 of 1510
Analytical Data
Client SM Stoller Corporation Job Number 280-39873-1
Sdg Number 13025120
Client Sample ID
Lab Sample ID
PIN12-0524
Client Matrix
280-39873-1
Water
Date Sampled 03092013 0748
Date Received 03132013 0900
8260B Volatile Organic Compounds (GCMS)
Dilution
03182013 1142
03182013 1142
10
8260B
Final WeightVolume
Initial WeightVolume
Lab File ID
Instrument ID
C5339D
10 mL
20 mL
5030B
VMS_C
Analysis Date
Prep Date
Analysis Batch
Prep Batch
280-165236
NA
Analysis Method
Prep Method
Analyte Result (ugL) Qualifier MDL RL
042 U 200421112-Tetrachloroethane
042 U 200421122-Tetrachloroethane
040 U 20040Tetrachloroethene
034 U 20034Toluene
042 U 20042123-Trichlorobenzene
042 U 20042124-Trichlorobenzene
032 U 20032111-Trichloroethane
054 U 20054112-Trichloroethane
032 U 20032Trichloroethene
058 U 20058Trichlorofluoromethane
066 U 20066123-Trichloropropane
030 U 20030124-Trimethylbenzene
032 U 20032135-Trimethylbenzene
038 U 20038Xylenes Total
036 U 2003612-Dibromoethane
Surrogate Rec Acceptance LimitsQualifier
109 70 - 12712-Dichloroethane-d4 (Surr)
97 80 - 125Toluene-d8 (Surr)
101 78 - 1204-Bromofluorobenzene (Surr)
105 77 - 120Dibromofluoromethane (Surr)
TestAmerica Denver Page 15 of 1510
Analytical Data
Client SM Stoller Corporation Job Number 280-39873-1
Sdg Number 13025120
Client Sample ID
Lab Sample ID
PIN12-0524
Client Matrix
280-39873-1
Water
Date Sampled 03092013 0748
Date Received 03132013 0900
8260B Volatile Organic Compounds (GCMS)
Dilution
03182013 1202
03182013 1202
10
8260B
Final WeightVolume
Initial WeightVolume
Lab File ID
Instrument ID
C5340D
1 mL
20 mLRun Type DL
5030B
VMS_C
Analysis Date
Prep Date
Analysis Batch
Prep Batch
280-165236
NA
Analysis Method
Prep Method
Analyte Result (ugL) Qualifier MDL RL
570 2030cis-12-Dichloroethene
600 2020Vinyl chloride
Surrogate Rec Acceptance LimitsQualifier
121 70 - 12712-Dichloroethane-d4 (Surr)
101 80 - 125Toluene-d8 (Surr)
101 78 - 1204-Bromofluorobenzene (Surr)
114 77 - 120Dibromofluoromethane (Surr)
TestAmerica Denver Page 16 of 1510
Analytical Data
Client SM Stoller Corporation Job Number 280-39873-1
Sdg Number 13025120
Client Sample ID
Lab Sample ID
PIN12-0525
Client Matrix
280-39873-2
Water
Date Sampled 03092013 0826
Date Received 03132013 0900
8260B Volatile Organic Compounds (GCMS)
Dilution
03182013 1304
03182013 1304
10
8260B
Final WeightVolume
Initial WeightVolume
Lab File ID
Instrument ID
C5343D
20 mL
20 mL
5030B
VMS_C
Analysis Date
Prep Date
Analysis Batch
Prep Batch
280-165236
NA
Analysis Method
Prep Method
Analyte Result (ugL) Qualifier MDL RL
19 U 1019Acetone
016 U 10016Benzene
017 U 10017Bromobenzene
010 U 10010Bromochloromethane
017 U 10017Bromodichloromethane
019 U 10019Bromoform
021 U 10021Bromomethane
20 U 50202-Butanone (MEK)
032 U 10032n-Butylbenzene
017 U 10017sec-Butylbenzene
016 U 10016tert-Butylbenzene
045 U 10045Carbon disulfide
019 U 10019Carbon tetrachloride
017 U 10017Chlorobenzene
017 U 10017Dibromochloromethane
041 U 10041Chloroethane
016 U 10016Chloroform
030 U 10030Chloromethane
017 U 100172-Chlorotoluene
021 U 100214-Chlorotoluene
047 U 1004712-Dibromo-3-Chloropropane
017 U 10017Dibromomethane
015 U 1001512-Dichlorobenzene
013 U 1001313-Dichlorobenzene
016 U 1001614-Dichlorobenzene
031 U 10031Dichlorodifluoromethane
022 U 1002211-Dichloroethane
013 U 1001312-Dichloroethane
13 10015cis-12-Dichloroethene
015 U 10015trans-12-Dichloroethene
023 U 1002311-Dichloroethene
018 U 1001812-Dichloropropane
022 U 1002213-Dichloropropane
018 U 1001822-Dichloropropane
016 U 10016cis-13-Dichloropropene
019 U 10019trans-13-Dichloropropene
019 U 1001911-Dichloropropene
016 U 10016Ethylbenzene
036 U 10036Hexachlorobutadiene
17 U 50172-Hexanone
019 U 10019Isopropylbenzene
020 U 100204-Isopropyltoluene
032 U 10032Methylene Chloride
098 U 500984-Methyl-2-pentanone
022 U 10022Naphthalene
016 U 10016n-Propylbenzene
TestAmerica Denver Page 17 of 1510
Analytical Data
Client SM Stoller Corporation Job Number 280-39873-1
Sdg Number 13025120
Client Sample ID
Lab Sample ID
PIN12-0525
Client Matrix
280-39873-2
Water
Date Sampled 03092013 0826
Date Received 03132013 0900
8260B Volatile Organic Compounds (GCMS)
Dilution
03182013 1304
03182013 1304
10
8260B
Final WeightVolume
Initial WeightVolume
Lab File ID
Instrument ID
C5343D
20 mL
20 mL
5030B
VMS_C
Analysis Date
Prep Date
Analysis Batch
Prep Batch
280-165236
NA
Analysis Method
Prep Method
Analyte Result (ugL) Qualifier MDL RL
017 U 10017Styrene
021 U 100211112-Tetrachloroethane
021 U 100211122-Tetrachloroethane
020 U 10020Tetrachloroethene
017 U 10017Toluene
021 U 10021123-Trichlorobenzene
021 U 10021124-Trichlorobenzene
016 U 10016111-Trichloroethane
027 U 10027112-Trichloroethane
016 U 10016Trichloroethene
029 U 10029Trichlorofluoromethane
033 U 10033123-Trichloropropane
015 U 10015124-Trimethylbenzene
016 U 10016135-Trimethylbenzene
010 U 10010Vinyl chloride
019 U 10019Xylenes Total
018 U 1001812-Dibromoethane
Surrogate Rec Acceptance LimitsQualifier
126 70 - 12712-Dichloroethane-d4 (Surr)
98 80 - 125Toluene-d8 (Surr)
109 78 - 1204-Bromofluorobenzene (Surr)
112 77 - 120Dibromofluoromethane (Surr)
TestAmerica Denver Page 18 of 1510
Analytical Data
Client SM Stoller Corporation Job Number 280-39873-1
Sdg Number 13025120
Client Sample ID
Lab Sample ID
PIN12-0539
Client Matrix
280-39873-3
Water
Date Sampled 03082013 1635
Date Received 03132013 0900
8260B Volatile Organic Compounds (GCMS)
Dilution
03182013 1324
03182013 1324
10
8260B
Final WeightVolume
Initial WeightVolume
Lab File ID
Instrument ID
C5344D
20 mL
20 mL
5030B
VMS_C
Analysis Date
Prep Date
Analysis Batch
Prep Batch
280-165236
NA
Analysis Method
Prep Method
Analyte Result (ugL) Qualifier MDL RL
47 J 1019Acetone
016 U 10016Benzene
017 U 10017Bromobenzene
010 U 10010Bromochloromethane
017 U 10017Bromodichloromethane
019 U 10019Bromoform
021 U 10021Bromomethane
20 U 50202-Butanone (MEK)
032 U 10032n-Butylbenzene
017 U 10017sec-Butylbenzene
016 U 10016tert-Butylbenzene
045 U 10045Carbon disulfide
019 U 10019Carbon tetrachloride
017 U 10017Chlorobenzene
017 U 10017Dibromochloromethane
041 U 10041Chloroethane
016 U 10016Chloroform
030 U 10030Chloromethane
017 U 100172-Chlorotoluene
021 U 100214-Chlorotoluene
047 U 1004712-Dibromo-3-Chloropropane
017 U 10017Dibromomethane
015 U 1001512-Dichlorobenzene
013 U 1001313-Dichlorobenzene
016 U 1001614-Dichlorobenzene
031 U 10031Dichlorodifluoromethane
48 1002211-Dichloroethane
013 U 1001312-Dichloroethane
16 10015cis-12-Dichloroethene
13 10015trans-12-Dichloroethene
023 U 1002311-Dichloroethene
018 U 1001812-Dichloropropane
022 U 1002213-Dichloropropane
018 U 1001822-Dichloropropane
016 U 10016cis-13-Dichloropropene
019 U 10019trans-13-Dichloropropene
019 U 1001911-Dichloropropene
016 U 10016Ethylbenzene
036 U 10036Hexachlorobutadiene
17 U 50172-Hexanone
019 U 10019Isopropylbenzene
020 U 100204-Isopropyltoluene
032 U 10032Methylene Chloride
098 U 500984-Methyl-2-pentanone
022 U 10022Naphthalene
016 U 10016n-Propylbenzene
TestAmerica Denver Page 19 of 1510
Analytical Data
Client SM Stoller Corporation Job Number 280-39873-1
Sdg Number 13025120
Client Sample ID
Lab Sample ID
PIN12-0539
Client Matrix
280-39873-3
Water
Date Sampled 03082013 1635
Date Received 03132013 0900
8260B Volatile Organic Compounds (GCMS)
Dilution
03182013 1324
03182013 1324
10
8260B
Final WeightVolume
Initial WeightVolume
Lab File ID
Instrument ID
C5344D
20 mL
20 mL
5030B
VMS_C
Analysis Date
Prep Date
Analysis Batch
Prep Batch
280-165236
NA
Analysis Method
Prep Method
Analyte Result (ugL) Qualifier MDL RL
017 U 10017Styrene
021 U 100211112-Tetrachloroethane
021 U 100211122-Tetrachloroethane
020 U 10020Tetrachloroethene
017 U 10017Toluene
021 U 10021123-Trichlorobenzene
021 U 10021124-Trichlorobenzene
016 U 10016111-Trichloroethane
027 U 10027112-Trichloroethane
016 U 10016Trichloroethene
029 U 10029Trichlorofluoromethane
033 U 10033123-Trichloropropane
015 U 10015124-Trimethylbenzene
016 U 10016135-Trimethylbenzene
019 U 10019Xylenes Total
018 U 1001812-Dibromoethane
Surrogate Rec Acceptance LimitsQualifier
113 70 - 12712-Dichloroethane-d4 (Surr)
90 80 - 125Toluene-d8 (Surr)
95 78 - 1204-Bromofluorobenzene (Surr)
103 77 - 120Dibromofluoromethane (Surr)
TestAmerica Denver Page 20 of 1510
Analytical Data
Client SM Stoller Corporation Job Number 280-39873-1
Sdg Number 13025120
Client Sample ID
Lab Sample ID
PIN12-0539
Client Matrix
280-39873-3
Water
Date Sampled 03082013 1635
Date Received 03132013 0900
8260B Volatile Organic Compounds (GCMS)
Dilution
03192013 1338
03192013 1338
10
8260B
Final WeightVolume
Initial WeightVolume
Lab File ID
Instrument ID
RR2023D
5 mL
20 mLRun Type DL
5030B
VMS_R2
Analysis Date
Prep Date
Analysis Batch
Prep Batch
280-165451
NA
Analysis Method
Prep Method
Analyte Result (ugL) Qualifier MDL RL
53 40040Vinyl chloride
Surrogate Rec Acceptance LimitsQualifier
74 70 - 12712-Dichloroethane-d4 (Surr)
90 80 - 125Toluene-d8 (Surr)
87 78 - 1204-Bromofluorobenzene (Surr)
82 77 - 120Dibromofluoromethane (Surr)
TestAmerica Denver Page 21 of 1510
Analytical Data
Client SM Stoller Corporation Job Number 280-39873-1
Sdg Number 13025120
Client Sample ID
Lab Sample ID
PIN12-0540
Client Matrix
280-39873-4
Water
Date Sampled 03082013 1548
Date Received 03132013 0900
8260B Volatile Organic Compounds (GCMS)
Dilution
03182013 1345
03182013 1345
10
8260B
Final WeightVolume
Initial WeightVolume
Lab File ID
Instrument ID
C5345D
20 mL
20 mL
5030B
VMS_C
Analysis Date
Prep Date
Analysis Batch
Prep Batch
280-165236
NA
Analysis Method
Prep Method
Analyte Result (ugL) Qualifier MDL RL
57 J 1019Acetone
016 U 10016Benzene
017 U 10017Bromobenzene
010 U 10010Bromochloromethane
017 U 10017Bromodichloromethane
019 U 10019Bromoform
021 U 10021Bromomethane
20 U 50202-Butanone (MEK)
032 U 10032n-Butylbenzene
017 U 10017sec-Butylbenzene
016 U 10016tert-Butylbenzene
045 U 10045Carbon disulfide
019 U 10019Carbon tetrachloride
017 U 10017Chlorobenzene
017 U 10017Dibromochloromethane
041 U 10041Chloroethane
016 U 10016Chloroform
030 U 10030Chloromethane
017 U 100172-Chlorotoluene
021 U 100214-Chlorotoluene
047 U 1004712-Dibromo-3-Chloropropane
017 U 10017Dibromomethane
015 U 1001512-Dichlorobenzene
013 U 1001313-Dichlorobenzene
016 U 1001614-Dichlorobenzene
031 U 10031Dichlorodifluoromethane
20 1002211-Dichloroethane
013 U 1001312-Dichloroethane
12 10015cis-12-Dichloroethene
68 10015trans-12-Dichloroethene
023 U 1002311-Dichloroethene
018 U 1001812-Dichloropropane
022 U 1002213-Dichloropropane
018 U 1001822-Dichloropropane
016 U 10016cis-13-Dichloropropene
019 U 10019trans-13-Dichloropropene
019 U 1001911-Dichloropropene
016 U 10016Ethylbenzene
036 U 10036Hexachlorobutadiene
17 U 50172-Hexanone
019 U 10019Isopropylbenzene
020 U 100204-Isopropyltoluene
032 U 10032Methylene Chloride
098 U 500984-Methyl-2-pentanone
022 U 10022Naphthalene
016 U 10016n-Propylbenzene
TestAmerica Denver Page 22 of 1510
Analytical Data
Client SM Stoller Corporation Job Number 280-39873-1
Sdg Number 13025120
Client Sample ID
Lab Sample ID
PIN12-0540
Client Matrix
280-39873-4
Water
Date Sampled 03082013 1548
Date Received 03132013 0900
8260B Volatile Organic Compounds (GCMS)
Dilution
03182013 1345
03182013 1345
10
8260B
Final WeightVolume
Initial WeightVolume
Lab File ID
Instrument ID
C5345D
20 mL
20 mL
5030B
VMS_C
Analysis Date
Prep Date
Analysis Batch
Prep Batch
280-165236
NA
Analysis Method
Prep Method
Analyte Result (ugL) Qualifier MDL RL
017 U 10017Styrene
021 U 100211112-Tetrachloroethane
021 U 100211122-Tetrachloroethane
020 U 10020Tetrachloroethene
017 U 10017Toluene
021 U 10021123-Trichlorobenzene
021 U 10021124-Trichlorobenzene
016 U 10016111-Trichloroethane
027 U 10027112-Trichloroethane
016 U 10016Trichloroethene
029 U 10029Trichlorofluoromethane
033 U 10033123-Trichloropropane
015 U 10015124-Trimethylbenzene
016 U 10016135-Trimethylbenzene
019 U 10019Xylenes Total
018 U 1001812-Dibromoethane
Surrogate Rec Acceptance LimitsQualifier
113 70 - 12712-Dichloroethane-d4 (Surr)
91 80 - 125Toluene-d8 (Surr)
94 78 - 1204-Bromofluorobenzene (Surr)
105 77 - 120Dibromofluoromethane (Surr)
TestAmerica Denver Page 23 of 1510
Analytical Data
Client SM Stoller Corporation Job Number 280-39873-1
Sdg Number 13025120
Client Sample ID
Lab Sample ID
PIN12-0540
Client Matrix
280-39873-4
Water
Date Sampled 03082013 1548
Date Received 03132013 0900
8260B Volatile Organic Compounds (GCMS)
Dilution
03192013 1203
03192013 1203
10
8260B
Final WeightVolume
Initial WeightVolume
Lab File ID
Instrument ID
RR2019D
2 mL
20 mLRun Type DL
5030B
VMS_R2
Analysis Date
Prep Date
Analysis Batch
Prep Batch
280-165451
NA
Analysis Method
Prep Method
Analyte Result (ugL) Qualifier MDL RL
230 1010Vinyl chloride
Surrogate Rec Acceptance LimitsQualifier
75 70 - 12712-Dichloroethane-d4 (Surr)
95 80 - 125Toluene-d8 (Surr)
93 78 - 1204-Bromofluorobenzene (Surr)
85 77 - 120Dibromofluoromethane (Surr)
TestAmerica Denver Page 24 of 1510
Analytical Data
Client SM Stoller Corporation Job Number 280-39873-1
Sdg Number 13025120
Client Sample ID
Lab Sample ID
PIN12-0541
Client Matrix
280-39873-5
Water
Date Sampled 03082013 1241
Date Received 03132013 0900
8260B Volatile Organic Compounds (GCMS)
Dilution
03182013 1426
03182013 1426
10
8260B
Final WeightVolume
Initial WeightVolume
Lab File ID
Instrument ID
C5347D
20 mL
20 mL
5030B
VMS_C
Analysis Date
Prep Date
Analysis Batch
Prep Batch
280-165236
NA
Analysis Method
Prep Method
Analyte Result (ugL) Qualifier MDL RL
10 1019Acetone
016 U 10016Benzene
017 U 10017Bromobenzene
010 U 10010Bromochloromethane
017 U 10017Bromodichloromethane
019 U 10019Bromoform
021 U 10021Bromomethane
20 U 50202-Butanone (MEK)
032 U 10032n-Butylbenzene
017 U 10017sec-Butylbenzene
016 U 10016tert-Butylbenzene
045 U 10045Carbon disulfide
019 U 10019Carbon tetrachloride
017 U 10017Chlorobenzene
017 U 10017Dibromochloromethane
041 U 10041Chloroethane
016 U 10016Chloroform
030 U 10030Chloromethane
017 U 100172-Chlorotoluene
021 U 100214-Chlorotoluene
047 U 1004712-Dibromo-3-Chloropropane
017 U 10017Dibromomethane
015 U 1001512-Dichlorobenzene
013 U 1001313-Dichlorobenzene
016 U 1001614-Dichlorobenzene
031 U 10031Dichlorodifluoromethane
022 U 1002211-Dichloroethane
013 U 1001312-Dichloroethane
020 J 10015cis-12-Dichloroethene
015 U 10015trans-12-Dichloroethene
023 U 1002311-Dichloroethene
018 U 1001812-Dichloropropane
022 U 1002213-Dichloropropane
018 U 1001822-Dichloropropane
016 U 10016cis-13-Dichloropropene
019 U 10019trans-13-Dichloropropene
019 U 1001911-Dichloropropene
016 U 10016Ethylbenzene
036 U 10036Hexachlorobutadiene
17 U 50172-Hexanone
019 U 10019Isopropylbenzene
020 U 100204-Isopropyltoluene
032 U 10032Methylene Chloride
098 U 500984-Methyl-2-pentanone
022 U 10022Naphthalene
016 U 10016n-Propylbenzene
TestAmerica Denver Page 25 of 1510
Analytical Data
Client SM Stoller Corporation Job Number 280-39873-1
Sdg Number 13025120
Client Sample ID
Lab Sample ID
PIN12-0541
Client Matrix
280-39873-5
Water
Date Sampled 03082013 1241
Date Received 03132013 0900
8260B Volatile Organic Compounds (GCMS)
Dilution
03182013 1426
03182013 1426
10
8260B
Final WeightVolume
Initial WeightVolume
Lab File ID
Instrument ID
C5347D
20 mL
20 mL
5030B
VMS_C
Analysis Date
Prep Date
Analysis Batch
Prep Batch
280-165236
NA
Analysis Method
Prep Method
Analyte Result (ugL) Qualifier MDL RL
017 U 10017Styrene
021 U 100211112-Tetrachloroethane
021 U 100211122-Tetrachloroethane
020 U 10020Tetrachloroethene
017 U 10017Toluene
021 U 10021123-Trichlorobenzene
021 U 10021124-Trichlorobenzene
016 U 10016111-Trichloroethane
027 U 10027112-Trichloroethane
016 U 10016Trichloroethene
029 U 10029Trichlorofluoromethane
033 U 10033123-Trichloropropane
015 U 10015124-Trimethylbenzene
016 U 10016135-Trimethylbenzene
010 U 10010Vinyl chloride
019 U 10019Xylenes Total
018 U 1001812-Dibromoethane
Surrogate Rec Acceptance LimitsQualifier
117 70 - 12712-Dichloroethane-d4 (Surr)
87 80 - 125Toluene-d8 (Surr)
94 78 - 1204-Bromofluorobenzene (Surr)
103 77 - 120Dibromofluoromethane (Surr)
TestAmerica Denver Page 26 of 1510
Analytical Data
Client SM Stoller Corporation Job Number 280-39873-1
Sdg Number 13025120
Client Sample ID
Lab Sample ID
PIN12-0542
Client Matrix
280-39873-6
Water
Date Sampled 03082013 1310
Date Received 03132013 0900
8260B Volatile Organic Compounds (GCMS)
Dilution
03192013 1536
03192013 1536
10
8260B
Final WeightVolume
Initial WeightVolume
Lab File ID
Instrument ID
RR2028D
5 mL
20 mL
5030B
VMS_R2
Analysis Date
Prep Date
Analysis Batch
Prep Batch
280-165451
NA
Analysis Method
Prep Method
Analyte Result (ugL) Qualifier MDL RL
76 U 4076Acetone
064 U 40064Benzene
068 U 40068Bromobenzene
040 U 40040Bromochloromethane
068 U 40068Bromodichloromethane
076 U 40076Bromoform
084 U 40084Bromomethane
80 U 20802-Butanone (MEK)
13 U 4013n-Butylbenzene
068 U 40068sec-Butylbenzene
064 U 40064tert-Butylbenzene
18 U 4018Carbon disulfide
076 U 40076Carbon tetrachloride
068 U 40068Chlorobenzene
068 U 40068Dibromochloromethane
16 U 4016Chloroethane
064 U 40064Chloroform
12 U 4012Chloromethane
068 U 400682-Chlorotoluene
084 U 400844-Chlorotoluene
19 U 401912-Dibromo-3-Chloropropane
068 U 40068Dibromomethane
060 U 4006012-Dichlorobenzene
052 U 4005213-Dichlorobenzene
064 U 4006414-Dichlorobenzene
12 U 4012Dichlorodifluoromethane
088 U 4008811-Dichloroethane
052 U 4005212-Dichloroethane
060 U 40060cis-12-Dichloroethene
060 U 40060trans-12-Dichloroethene
092 U 4009211-Dichloroethene
072 U 4007212-Dichloropropane
088 U 4008813-Dichloropropane
072 U 4007222-Dichloropropane
064 U 40064cis-13-Dichloropropene
076 U 40076trans-13-Dichloropropene
076 U 4007611-Dichloropropene
064 U 40064Ethylbenzene
14 U 4014Hexachlorobutadiene
68 U 20682-Hexanone
076 U 40076Isopropylbenzene
080 U 400804-Isopropyltoluene
44 4013Methylene Chloride
39 U 20394-Methyl-2-pentanone
088 U 40088Naphthalene
064 U 40064n-Propylbenzene
TestAmerica Denver Page 27 of 1510
Analytical Data
Client SM Stoller Corporation Job Number 280-39873-1
Sdg Number 13025120
Client Sample ID
Lab Sample ID
PIN12-0542
Client Matrix
280-39873-6
Water
Date Sampled 03082013 1310
Date Received 03132013 0900
8260B Volatile Organic Compounds (GCMS)
Dilution
03192013 1536
03192013 1536
10
8260B
Final WeightVolume
Initial WeightVolume
Lab File ID
Instrument ID
RR2028D
5 mL
20 mL
5030B
VMS_R2
Analysis Date
Prep Date
Analysis Batch
Prep Batch
280-165451
NA
Analysis Method
Prep Method
Analyte Result (ugL) Qualifier MDL RL
068 U 40068Styrene
084 U 400841112-Tetrachloroethane
084 U 400841122-Tetrachloroethane
080 U 40080Tetrachloroethene
068 U 40068Toluene
084 U 40084123-Trichlorobenzene
084 U 40084124-Trichlorobenzene
064 U 40064111-Trichloroethane
11 U 4011112-Trichloroethane
064 U 40064Trichloroethene
12 U 4012Trichlorofluoromethane
13 U 4013123-Trichloropropane
060 U 40060124-Trimethylbenzene
064 U 40064135-Trimethylbenzene
040 U 40040Vinyl chloride
076 U 40076Xylenes Total
072 U 4007212-Dibromoethane
Surrogate Rec Acceptance LimitsQualifier
75 70 - 12712-Dichloroethane-d4 (Surr)
94 80 - 125Toluene-d8 (Surr)
87 78 - 1204-Bromofluorobenzene (Surr)
84 77 - 120Dibromofluoromethane (Surr)
TestAmerica Denver Page 28 of 1510
Analytical Data
Client SM Stoller Corporation Job Number 280-39873-1
Sdg Number 13025120
Client Sample ID
Lab Sample ID
PIN12-0549
Client Matrix
280-39873-7
Water
Date Sampled 03082013 1413
Date Received 03132013 0900
8260B Volatile Organic Compounds (GCMS)
Dilution
03182013 1507
03182013 1507
10
8260B
Final WeightVolume
Initial WeightVolume
Lab File ID
Instrument ID
C5349D
20 mL
20 mL
5030B
VMS_C
Analysis Date
Prep Date
Analysis Batch
Prep Batch
280-165236
NA
Analysis Method
Prep Method
Analyte Result (ugL) Qualifier MDL RL
14 1019Acetone
016 U 10016Benzene
017 U 10017Bromobenzene
010 U 10010Bromochloromethane
017 U 10017Bromodichloromethane
019 U 10019Bromoform
021 U 10021Bromomethane
20 U 50202-Butanone (MEK)
032 U 10032n-Butylbenzene
017 U 10017sec-Butylbenzene
016 U 10016tert-Butylbenzene
045 U 10045Carbon disulfide
019 U 10019Carbon tetrachloride
017 U 10017Chlorobenzene
017 U 10017Dibromochloromethane
041 U 10041Chloroethane
016 U 10016Chloroform
030 U 10030Chloromethane
017 U 100172-Chlorotoluene
021 U 100214-Chlorotoluene
047 U 1004712-Dibromo-3-Chloropropane
017 U 10017Dibromomethane
015 U 1001512-Dichlorobenzene
013 U 1001313-Dichlorobenzene
016 U 1001614-Dichlorobenzene
031 U 10031Dichlorodifluoromethane
024 J 1002211-Dichloroethane
013 U 1001312-Dichloroethane
017 J 10015cis-12-Dichloroethene
015 U 10015trans-12-Dichloroethene
023 U 1002311-Dichloroethene
018 U 1001812-Dichloropropane
022 U 1002213-Dichloropropane
018 U 1001822-Dichloropropane
016 U 10016cis-13-Dichloropropene
019 U 10019trans-13-Dichloropropene
019 U 1001911-Dichloropropene
016 U 10016Ethylbenzene
036 U 10036Hexachlorobutadiene
17 U 50172-Hexanone
019 U 10019Isopropylbenzene
020 U 100204-Isopropyltoluene
032 U 10032Methylene Chloride
098 U 500984-Methyl-2-pentanone
022 U 10022Naphthalene
016 U 10016n-Propylbenzene
TestAmerica Denver Page 29 of 1510
Analytical Data
Client SM Stoller Corporation Job Number 280-39873-1
Sdg Number 13025120
Client Sample ID
Lab Sample ID
PIN12-0549
Client Matrix
280-39873-7
Water
Date Sampled 03082013 1413
Date Received 03132013 0900
8260B Volatile Organic Compounds (GCMS)
Dilution
03182013 1507
03182013 1507
10
8260B
Final WeightVolume
Initial WeightVolume
Lab File ID
Instrument ID
C5349D
20 mL
20 mL
5030B
VMS_C
Analysis Date
Prep Date
Analysis Batch
Prep Batch
280-165236
NA
Analysis Method
Prep Method
Analyte Result (ugL) Qualifier MDL RL
017 U 10017Styrene
021 U 100211112-Tetrachloroethane
021 U 100211122-Tetrachloroethane
020 U 10020Tetrachloroethene
017 U 10017Toluene
021 U 10021123-Trichlorobenzene
021 U 10021124-Trichlorobenzene
016 U 10016111-Trichloroethane
027 U 10027112-Trichloroethane
016 U 10016Trichloroethene
029 U 10029Trichlorofluoromethane
033 U 10033123-Trichloropropane
015 U 10015124-Trimethylbenzene
016 U 10016135-Trimethylbenzene
010 U 10010Vinyl chloride
019 U 10019Xylenes Total
018 U 1001812-Dibromoethane
Surrogate Rec Acceptance LimitsQualifier
124 70 - 12712-Dichloroethane-d4 (Surr)
95 80 - 125Toluene-d8 (Surr)
96 78 - 1204-Bromofluorobenzene (Surr)
109 77 - 120Dibromofluoromethane (Surr)
TestAmerica Denver Page 30 of 1510
Analytical Data
Client SM Stoller Corporation Job Number 280-39873-1
Sdg Number 13025120
Client Sample ID
Lab Sample ID
PIN12-0554A
Client Matrix
280-39873-8
Water
Date Sampled 03082013 0919
Date Received 03132013 0900
8260B Volatile Organic Compounds (GCMS)
Dilution
03182013 1527
03182013 1527
10
8260B
Final WeightVolume
Initial WeightVolume
Lab File ID
Instrument ID
C5350D
20 mL
20 mL
5030B
VMS_C
Analysis Date
Prep Date
Analysis Batch
Prep Batch
280-165236
NA
Analysis Method
Prep Method
Analyte Result (ugL) Qualifier MDL RL
98 J 1019Acetone
016 U 10016Benzene
017 U 10017Bromobenzene
010 U 10010Bromochloromethane
017 U 10017Bromodichloromethane
019 U 10019Bromoform
021 U 10021Bromomethane
20 U 50202-Butanone (MEK)
032 U 10032n-Butylbenzene
017 U 10017sec-Butylbenzene
016 U 10016tert-Butylbenzene
045 U 10045Carbon disulfide
019 U 10019Carbon tetrachloride
017 U 10017Chlorobenzene
017 U 10017Dibromochloromethane
041 U 10041Chloroethane
016 U 10016Chloroform
030 U 10030Chloromethane
017 U 100172-Chlorotoluene
021 U 100214-Chlorotoluene
047 U 1004712-Dibromo-3-Chloropropane
017 U 10017Dibromomethane
015 U 1001512-Dichlorobenzene
013 U 1001313-Dichlorobenzene
016 U 1001614-Dichlorobenzene
031 U 10031Dichlorodifluoromethane
022 U 1002211-Dichloroethane
013 U 1001312-Dichloroethane
015 U 10015cis-12-Dichloroethene
015 U 10015trans-12-Dichloroethene
023 U 1002311-Dichloroethene
018 U 1001812-Dichloropropane
022 U 1002213-Dichloropropane
018 U 1001822-Dichloropropane
016 U 10016cis-13-Dichloropropene
019 U 10019trans-13-Dichloropropene
019 U 1001911-Dichloropropene
016 U 10016Ethylbenzene
036 U 10036Hexachlorobutadiene
17 U 50172-Hexanone
019 U 10019Isopropylbenzene
020 U 100204-Isopropyltoluene
032 U 10032Methylene Chloride
098 U 500984-Methyl-2-pentanone
022 U 10022Naphthalene
016 U 10016n-Propylbenzene
TestAmerica Denver Page 31 of 1510
Analytical Data
Client SM Stoller Corporation Job Number 280-39873-1
Sdg Number 13025120
Client Sample ID
Lab Sample ID
PIN12-0554A
Client Matrix
280-39873-8
Water
Date Sampled 03082013 0919
Date Received 03132013 0900
8260B Volatile Organic Compounds (GCMS)
Dilution
03182013 1527
03182013 1527
10
8260B
Final WeightVolume
Initial WeightVolume
Lab File ID
Instrument ID
C5350D
20 mL
20 mL
5030B
VMS_C
Analysis Date
Prep Date
Analysis Batch
Prep Batch
280-165236
NA
Analysis Method
Prep Method
Analyte Result (ugL) Qualifier MDL RL
017 U 10017Styrene
021 U 100211112-Tetrachloroethane
021 U 100211122-Tetrachloroethane
020 U 10020Tetrachloroethene
017 U 10017Toluene
021 U 10021123-Trichlorobenzene
021 U 10021124-Trichlorobenzene
016 U 10016111-Trichloroethane
027 U 10027112-Trichloroethane
016 U 10016Trichloroethene
029 U 10029Trichlorofluoromethane
033 U 10033123-Trichloropropane
015 U 10015124-Trimethylbenzene
016 U 10016135-Trimethylbenzene
010 U 10010Vinyl chloride
019 U 10019Xylenes Total
018 U 1001812-Dibromoethane
Surrogate Rec Acceptance LimitsQualifier
127 70 - 12712-Dichloroethane-d4 (Surr)
92 80 - 125Toluene-d8 (Surr)
99 78 - 1204-Bromofluorobenzene (Surr)
115 77 - 120Dibromofluoromethane (Surr)
TestAmerica Denver Page 32 of 1510
Analytical Data
Client SM Stoller Corporation Job Number 280-39873-1
Sdg Number 13025120
Client Sample ID
Lab Sample ID
PIN12-0554B
Client Matrix
280-39873-9
Water
Date Sampled 03082013 1005
Date Received 03132013 0900
8260B Volatile Organic Compounds (GCMS)
Dilution
03192013 1600
03192013 1600
10
8260B
Final WeightVolume
Initial WeightVolume
Lab File ID
Instrument ID
RR2029D
20 mL
20 mL
5030B
VMS_R2
Analysis Date
Prep Date
Analysis Batch
Prep Batch
280-165451
NA
Analysis Method
Prep Method
Analyte Result (ugL) Qualifier MDL RL
19 U 1019Acetone
016 U 10016Benzene
017 U 10017Bromobenzene
010 U 10010Bromochloromethane
017 U 10017Bromodichloromethane
019 U 10019Bromoform
021 U 10021Bromomethane
20 U 50202-Butanone (MEK)
032 U 10032n-Butylbenzene
017 U 10017sec-Butylbenzene
016 U 10016tert-Butylbenzene
045 U 10045Carbon disulfide
019 U 10019Carbon tetrachloride
017 U 10017Chlorobenzene
017 U 10017Dibromochloromethane
041 U 10041Chloroethane
016 U 10016Chloroform
030 U 10030Chloromethane
017 U 100172-Chlorotoluene
021 U 100214-Chlorotoluene
047 U 1004712-Dibromo-3-Chloropropane
017 U 10017Dibromomethane
015 U 1001512-Dichlorobenzene
013 U 1001313-Dichlorobenzene
016 U 1001614-Dichlorobenzene
031 U 10031Dichlorodifluoromethane
022 U 1002211-Dichloroethane
013 U 1001312-Dichloroethane
015 U 10015cis-12-Dichloroethene
015 U 10015trans-12-Dichloroethene
023 U 1002311-Dichloroethene
018 U 1001812-Dichloropropane
022 U 1002213-Dichloropropane
018 U 1001822-Dichloropropane
016 U 10016cis-13-Dichloropropene
019 U 10019trans-13-Dichloropropene
019 U 1001911-Dichloropropene
016 U 10016Ethylbenzene
036 U 10036Hexachlorobutadiene
17 U 50172-Hexanone
019 U 10019Isopropylbenzene
020 U 100204-Isopropyltoluene
032 U 10032Methylene Chloride
098 U 500984-Methyl-2-pentanone
022 U 10022Naphthalene
016 U 10016n-Propylbenzene
TestAmerica Denver Page 33 of 1510
Analytical Data
Client SM Stoller Corporation Job Number 280-39873-1
Sdg Number 13025120
Client Sample ID
Lab Sample ID
PIN12-0554B
Client Matrix
280-39873-9
Water
Date Sampled 03082013 1005
Date Received 03132013 0900
8260B Volatile Organic Compounds (GCMS)
Dilution
03192013 1600
03192013 1600
10
8260B
Final WeightVolume
Initial WeightVolume
Lab File ID
Instrument ID
RR2029D
20 mL
20 mL
5030B
VMS_R2
Analysis Date
Prep Date
Analysis Batch
Prep Batch
280-165451
NA
Analysis Method
Prep Method
Analyte Result (ugL) Qualifier MDL RL
017 U 10017Styrene
021 U 100211112-Tetrachloroethane
021 U 100211122-Tetrachloroethane
020 U 10020Tetrachloroethene
017 U 10017Toluene
021 U 10021123-Trichlorobenzene
021 U 10021124-Trichlorobenzene
016 U 10016111-Trichloroethane
027 U 10027112-Trichloroethane
016 U 10016Trichloroethene
029 U 10029Trichlorofluoromethane
033 U 10033123-Trichloropropane
015 U 10015124-Trimethylbenzene
016 U 10016135-Trimethylbenzene
010 U 10010Vinyl chloride
019 U 10019Xylenes Total
018 U 1001812-Dibromoethane
Surrogate Rec Acceptance LimitsQualifier
76 70 - 12712-Dichloroethane-d4 (Surr)
90 80 - 125Toluene-d8 (Surr)
88 78 - 1204-Bromofluorobenzene (Surr)
85 77 - 120Dibromofluoromethane (Surr)
TestAmerica Denver Page 34 of 1510
Analytical Data
Client SM Stoller Corporation Job Number 280-39873-1
Sdg Number 13025120
Client Sample ID
Lab Sample ID
PIN12-0554C
Client Matrix
280-39873-10
Water
Date Sampled 03082013 1110
Date Received 03132013 0900
8260B Volatile Organic Compounds (GCMS)
Dilution
03182013 1607
03182013 1607
10
8260B
Final WeightVolume
Initial WeightVolume
Lab File ID
Instrument ID
C5352D
20 mL
20 mL
5030B
VMS_C
Analysis Date
Prep Date
Analysis Batch
Prep Batch
280-165236
NA
Analysis Method
Prep Method
Analyte Result (ugL) Qualifier MDL RL
67 J 1019Acetone
016 U 10016Benzene
017 U 10017Bromobenzene
010 U 10010Bromochloromethane
017 U 10017Bromodichloromethane
019 U 10019Bromoform
021 U 10021Bromomethane
20 U 50202-Butanone (MEK)
032 U 10032n-Butylbenzene
017 U 10017sec-Butylbenzene
016 U 10016tert-Butylbenzene
045 U 10045Carbon disulfide
019 U 10019Carbon tetrachloride
017 U 10017Chlorobenzene
017 U 10017Dibromochloromethane
041 U 10041Chloroethane
016 U 10016Chloroform
030 U 10030Chloromethane
017 U 100172-Chlorotoluene
021 U 100214-Chlorotoluene
047 U 1004712-Dibromo-3-Chloropropane
017 U 10017Dibromomethane
015 U 1001512-Dichlorobenzene
013 U 1001313-Dichlorobenzene
016 U 1001614-Dichlorobenzene
031 U 10031Dichlorodifluoromethane
013 U 1001312-Dichloroethane
16 10015cis-12-Dichloroethene
55 10015trans-12-Dichloroethene
10 1002311-Dichloroethene
018 U 1001812-Dichloropropane
022 U 1002213-Dichloropropane
018 U 1001822-Dichloropropane
016 U 10016cis-13-Dichloropropene
019 U 10019trans-13-Dichloropropene
019 U 1001911-Dichloropropene
016 U 10016Ethylbenzene
036 U 10036Hexachlorobutadiene
17 U 50172-Hexanone
019 U 10019Isopropylbenzene
020 U 100204-Isopropyltoluene
032 U 10032Methylene Chloride
098 U 500984-Methyl-2-pentanone
022 U 10022Naphthalene
016 U 10016n-Propylbenzene
017 U 10017Styrene
TestAmerica Denver Page 35 of 1510
Analytical Data
Client SM Stoller Corporation Job Number 280-39873-1
Sdg Number 13025120
Client Sample ID
Lab Sample ID
PIN12-0554C
Client Matrix
280-39873-10
Water
Date Sampled 03082013 1110
Date Received 03132013 0900
8260B Volatile Organic Compounds (GCMS)
Dilution
03182013 1607
03182013 1607
10
8260B
Final WeightVolume
Initial WeightVolume
Lab File ID
Instrument ID
C5352D
20 mL
20 mL
5030B
VMS_C
Analysis Date
Prep Date
Analysis Batch
Prep Batch
280-165236
NA
Analysis Method
Prep Method
Analyte Result (ugL) Qualifier MDL RL
021 U 100211112-Tetrachloroethane
021 U 100211122-Tetrachloroethane
020 U 10020Tetrachloroethene
017 U 10017Toluene
021 U 10021123-Trichlorobenzene
021 U 10021124-Trichlorobenzene
016 U 10016111-Trichloroethane
027 U 10027112-Trichloroethane
016 U 10016Trichloroethene
029 U 10029Trichlorofluoromethane
033 U 10033123-Trichloropropane
015 U 10015124-Trimethylbenzene
016 U 10016135-Trimethylbenzene
019 U 10019Xylenes Total
018 U 1001812-Dibromoethane
Surrogate Rec Acceptance LimitsQualifier
123 70 - 12712-Dichloroethane-d4 (Surr)
95 80 - 125Toluene-d8 (Surr)
95 78 - 1204-Bromofluorobenzene (Surr)
111 77 - 120Dibromofluoromethane (Surr)
TestAmerica Denver Page 36 of 1510
Analytical Data
Client SM Stoller Corporation Job Number 280-39873-1
Sdg Number 13025120
Client Sample ID
Lab Sample ID
PIN12-0554C
Client Matrix
280-39873-10
Water
Date Sampled 03082013 1110
Date Received 03132013 0900
8260B Volatile Organic Compounds (GCMS)
Dilution
03182013 1627
03182013 1627
10
8260B
Final WeightVolume
Initial WeightVolume
Lab File ID
Instrument ID
C5353D
10 mL
20 mLRun Type DL
5030B
VMS_C
Analysis Date
Prep Date
Analysis Batch
Prep Batch
280-165236
NA
Analysis Method
Prep Method
Analyte Result (ugL) Qualifier MDL RL
64 2004411-Dichloroethane
88 20020Vinyl chloride
Surrogate Rec Acceptance LimitsQualifier
120 70 - 12712-Dichloroethane-d4 (Surr)
92 80 - 125Toluene-d8 (Surr)
93 78 - 1204-Bromofluorobenzene (Surr)
108 77 - 120Dibromofluoromethane (Surr)
TestAmerica Denver Page 37 of 1510
Analytical Data
Client SM Stoller Corporation Job Number 280-39873-1
Sdg Number 13025120
Client Sample ID
Lab Sample ID
PIN12-0581-1
Client Matrix
280-39873-11
Water
Date Sampled 03112013 0851
Date Received 03132013 0900
8260B Volatile Organic Compounds (GCMS)
Dilution
03182013 1648
03182013 1648
10
8260B
Final WeightVolume
Initial WeightVolume
Lab File ID
Instrument ID
C5354D
20 mL
20 mL
5030B
VMS_C
Analysis Date
Prep Date
Analysis Batch
Prep Batch
280-165236
NA
Analysis Method
Prep Method
Analyte Result (ugL) Qualifier MDL RL
87 J 1019Acetone
016 U 10016Benzene
017 U 10017Bromobenzene
010 U 10010Bromochloromethane
017 U 10017Bromodichloromethane
019 U 10019Bromoform
021 U 10021Bromomethane
20 U 50202-Butanone (MEK)
032 U 10032n-Butylbenzene
017 U 10017sec-Butylbenzene
016 U 10016tert-Butylbenzene
045 U 10045Carbon disulfide
019 U 10019Carbon tetrachloride
017 U 10017Chlorobenzene
017 U 10017Dibromochloromethane
041 U 10041Chloroethane
016 U 10016Chloroform
030 U 10030Chloromethane
017 U 100172-Chlorotoluene
021 U 100214-Chlorotoluene
047 U 1004712-Dibromo-3-Chloropropane
017 U 10017Dibromomethane
015 U 1001512-Dichlorobenzene
013 U 1001313-Dichlorobenzene
016 U 1001614-Dichlorobenzene
031 U 10031Dichlorodifluoromethane
089 J 1002211-Dichloroethane
013 U 1001312-Dichloroethane
026 J 10015cis-12-Dichloroethene
015 U 10015trans-12-Dichloroethene
023 U 1002311-Dichloroethene
018 U 1001812-Dichloropropane
022 U 1002213-Dichloropropane
018 U 1001822-Dichloropropane
016 U 10016cis-13-Dichloropropene
019 U 10019trans-13-Dichloropropene
019 U 1001911-Dichloropropene
016 U 10016Ethylbenzene
036 U 10036Hexachlorobutadiene
17 U 50172-Hexanone
019 U 10019Isopropylbenzene
020 U 100204-Isopropyltoluene
032 U 10032Methylene Chloride
098 U 500984-Methyl-2-pentanone
022 U 10022Naphthalene
016 U 10016n-Propylbenzene
TestAmerica Denver Page 38 of 1510
Analytical Data
Client SM Stoller Corporation Job Number 280-39873-1
Sdg Number 13025120
Client Sample ID
Lab Sample ID
PIN12-0581-1
Client Matrix
280-39873-11
Water
Date Sampled 03112013 0851
Date Received 03132013 0900
8260B Volatile Organic Compounds (GCMS)
Dilution
03182013 1648
03182013 1648
10
8260B
Final WeightVolume
Initial WeightVolume
Lab File ID
Instrument ID
C5354D
20 mL
20 mL
5030B
VMS_C
Analysis Date
Prep Date
Analysis Batch
Prep Batch
280-165236
NA
Analysis Method
Prep Method
Analyte Result (ugL) Qualifier MDL RL
017 U 10017Styrene
021 U 100211112-Tetrachloroethane
021 U 100211122-Tetrachloroethane
020 U 10020Tetrachloroethene
017 U 10017Toluene
021 U 10021123-Trichlorobenzene
021 U 10021124-Trichlorobenzene
016 U 10016111-Trichloroethane
027 U 10027112-Trichloroethane
016 U 10016Trichloroethene
029 U 10029Trichlorofluoromethane
033 U 10033123-Trichloropropane
015 U 10015124-Trimethylbenzene
016 U 10016135-Trimethylbenzene
050 J 10010Vinyl chloride
019 U 10019Xylenes Total
018 U 1001812-Dibromoethane
Surrogate Rec Acceptance LimitsQualifier
110 70 - 12712-Dichloroethane-d4 (Surr)
82 80 - 125Toluene-d8 (Surr)
82 78 - 1204-Bromofluorobenzene (Surr)
95 77 - 120Dibromofluoromethane (Surr)
TestAmerica Denver Page 39 of 1510
Analytical Data
Client SM Stoller Corporation Job Number 280-39873-1
Sdg Number 13025120
Client Sample ID
Lab Sample ID
PIN12-0581-2
Client Matrix
280-39873-12
Water
Date Sampled 03112013 0923
Date Received 03132013 0900
8260B Volatile Organic Compounds (GCMS)
Dilution
03192013 1250
03192013 1250
10
8260B
Final WeightVolume
Initial WeightVolume
Lab File ID
Instrument ID
RR2021D
2 mL
20 mL
5030B
VMS_R2
Analysis Date
Prep Date
Analysis Batch
Prep Batch
280-165451
NA
Analysis Method
Prep Method
Analyte Result (ugL) Qualifier MDL RL
19 U 10019Acetone
16 U 1016Benzene
17 U 1017Bromobenzene
10 U 1010Bromochloromethane
17 U 1017Bromodichloromethane
19 U 1019Bromoform
21 U 1021Bromomethane
20 U 50202-Butanone (MEK)
32 U 1032n-Butylbenzene
17 U 1017sec-Butylbenzene
16 U 1016tert-Butylbenzene
45 U 1045Carbon disulfide
19 U 1019Carbon tetrachloride
17 U 1017Chlorobenzene
17 U 1017Dibromochloromethane
41 U 1041Chloroethane
16 U 1016Chloroform
30 U 1030Chloromethane
17 U 10172-Chlorotoluene
21 U 10214-Chlorotoluene
47 U 104712-Dibromo-3-Chloropropane
17 U 1017Dibromomethane
15 U 101512-Dichlorobenzene
13 U 101313-Dichlorobenzene
16 U 101614-Dichlorobenzene
31 U 1031Dichlorodifluoromethane
94 J 102211-Dichloroethane
13 U 101312-Dichloroethane
29 J 1015cis-12-Dichloroethene
15 U 1015trans-12-Dichloroethene
23 U 102311-Dichloroethene
18 U 101812-Dichloropropane
22 U 102213-Dichloropropane
18 U 101822-Dichloropropane
16 U 1016cis-13-Dichloropropene
19 U 1019trans-13-Dichloropropene
19 U 101911-Dichloropropene
16 U 1016Ethylbenzene
36 U 1036Hexachlorobutadiene
17 U 50172-Hexanone
19 U 1019Isopropylbenzene
20 U 10204-Isopropyltoluene
37 J 1032Methylene Chloride
98 U 50984-Methyl-2-pentanone
22 U 1022Naphthalene
16 U 1016n-Propylbenzene
TestAmerica Denver Page 40 of 1510
Analytical Data
Client SM Stoller Corporation Job Number 280-39873-1
Sdg Number 13025120
Client Sample ID
Lab Sample ID
PIN12-0581-2
Client Matrix
280-39873-12
Water
Date Sampled 03112013 0923
Date Received 03132013 0900
8260B Volatile Organic Compounds (GCMS)
Dilution
03192013 1250
03192013 1250
10
8260B
Final WeightVolume
Initial WeightVolume
Lab File ID
Instrument ID
RR2021D
2 mL
20 mL
5030B
VMS_R2
Analysis Date
Prep Date
Analysis Batch
Prep Batch
280-165451
NA
Analysis Method
Prep Method
Analyte Result (ugL) Qualifier MDL RL
17 U 1017Styrene
21 U 10211112-Tetrachloroethane
21 U 10211122-Tetrachloroethane
20 U 1020Tetrachloroethene
17 U 1017Toluene
21 U 1021123-Trichlorobenzene
21 U 1021124-Trichlorobenzene
16 U 1016111-Trichloroethane
27 U 1027112-Trichloroethane
16 U 1016Trichloroethene
29 U 1029Trichlorofluoromethane
33 U 1033123-Trichloropropane
15 U 1015124-Trimethylbenzene
16 U 1016135-Trimethylbenzene
10 U 1010Vinyl chloride
19 U 1019Xylenes Total
18 U 101812-Dibromoethane
Surrogate Rec Acceptance LimitsQualifier
75 70 - 12712-Dichloroethane-d4 (Surr)
92 80 - 125Toluene-d8 (Surr)
85 78 - 1204-Bromofluorobenzene (Surr)
82 77 - 120Dibromofluoromethane (Surr)
TestAmerica Denver Page 41 of 1510
Analytical Data
Client SM Stoller Corporation Job Number 280-39873-1
Sdg Number 13025120
Client Sample ID
Lab Sample ID
PIN12-0581-3
Client Matrix
280-39873-13
Water
Date Sampled 03112013 1025
Date Received 03132013 0900
8260B Volatile Organic Compounds (GCMS)
Dilution
03182013 1728
03182013 1728
10
8260B
Final WeightVolume
Initial WeightVolume
Lab File ID
Instrument ID
C5356D
10 mL
20 mL
5030B
VMS_C
Analysis Date
Prep Date
Analysis Batch
Prep Batch
280-165236
NA
Analysis Method
Prep Method
Analyte Result (ugL) Qualifier MDL RL
93 J 2038Acetone
032 U 20032Benzene
034 U 20034Bromobenzene
020 U 20020Bromochloromethane
034 U 20034Bromodichloromethane
038 U 20038Bromoform
042 U 20042Bromomethane
40 U 10402-Butanone (MEK)
064 U 20064n-Butylbenzene
034 U 20034sec-Butylbenzene
032 U 20032tert-Butylbenzene
090 U 20090Carbon disulfide
038 U 20038Carbon tetrachloride
034 U 20034Chlorobenzene
034 U 20034Dibromochloromethane
082 U 20082Chloroethane
032 U 20032Chloroform
060 U 20060Chloromethane
034 U 200342-Chlorotoluene
042 U 200424-Chlorotoluene
094 U 2009412-Dibromo-3-Chloropropane
034 U 20034Dibromomethane
030 U 2003012-Dichlorobenzene
026 U 2002613-Dichlorobenzene
032 U 2003214-Dichlorobenzene
062 U 20062Dichlorodifluoromethane
044 U 2004411-Dichloroethane
026 U 2002612-Dichloroethane
030 U 20030cis-12-Dichloroethene
030 U 20030trans-12-Dichloroethene
046 U 2004611-Dichloroethene
036 U 2003612-Dichloropropane
044 U 2004413-Dichloropropane
036 U 2003622-Dichloropropane
032 U 20032cis-13-Dichloropropene
038 U 20038trans-13-Dichloropropene
038 U 2003811-Dichloropropene
032 U 20032Ethylbenzene
072 U 20072Hexachlorobutadiene
34 U 10342-Hexanone
038 U 20038Isopropylbenzene
040 U 200404-Isopropyltoluene
064 U 20064Methylene Chloride
20 U 10204-Methyl-2-pentanone
044 U 20044Naphthalene
032 U 20032n-Propylbenzene
TestAmerica Denver Page 42 of 1510
Analytical Data
Client SM Stoller Corporation Job Number 280-39873-1
Sdg Number 13025120
Client Sample ID
Lab Sample ID
PIN12-0581-3
Client Matrix
280-39873-13
Water
Date Sampled 03112013 1025
Date Received 03132013 0900
8260B Volatile Organic Compounds (GCMS)
Dilution
03182013 1728
03182013 1728
10
8260B
Final WeightVolume
Initial WeightVolume
Lab File ID
Instrument ID
C5356D
10 mL
20 mL
5030B
VMS_C
Analysis Date
Prep Date
Analysis Batch
Prep Batch
280-165236
NA
Analysis Method
Prep Method
Analyte Result (ugL) Qualifier MDL RL
034 U 20034Styrene
042 U 200421112-Tetrachloroethane
042 U 200421122-Tetrachloroethane
040 U 20040Tetrachloroethene
034 U 20034Toluene
042 U 20042123-Trichlorobenzene
042 U 20042124-Trichlorobenzene
032 U 20032111-Trichloroethane
054 U 20054112-Trichloroethane
032 U 20032Trichloroethene
058 U 20058Trichlorofluoromethane
066 U 20066123-Trichloropropane
030 U 20030124-Trimethylbenzene
032 U 20032135-Trimethylbenzene
020 U 20020Vinyl chloride
038 U 20038Xylenes Total
036 U 2003612-Dibromoethane
Surrogate Rec Acceptance LimitsQualifier
125 70 - 12712-Dichloroethane-d4 (Surr)
94 80 - 125Toluene-d8 (Surr)
97 78 - 1204-Bromofluorobenzene (Surr)
112 77 - 120Dibromofluoromethane (Surr)
TestAmerica Denver Page 43 of 1510
Analytical Data
Client SM Stoller Corporation Job Number 280-39873-1
Sdg Number 13025120
Client Sample ID
Lab Sample ID
PIN12-0582-1
Client Matrix
280-39873-14
Water
Date Sampled 03112013 1147
Date Received 03132013 0900
8260B Volatile Organic Compounds (GCMS)
Dilution
03182013 1748
03182013 1748
10
8260B
Final WeightVolume
Initial WeightVolume
Lab File ID
Instrument ID
C5357D
20 mL
20 mL
5030B
VMS_C
Analysis Date
Prep Date
Analysis Batch
Prep Batch
280-165236
NA
Analysis Method
Prep Method
Analyte Result (ugL) Qualifier MDL RL
73 J 1019Acetone
016 U 10016Benzene
017 U 10017Bromobenzene
010 U 10010Bromochloromethane
017 U 10017Bromodichloromethane
019 U 10019Bromoform
021 U 10021Bromomethane
20 U 50202-Butanone (MEK)
032 U 10032n-Butylbenzene
017 U 10017sec-Butylbenzene
016 U 10016tert-Butylbenzene
045 U 10045Carbon disulfide
019 U 10019Carbon tetrachloride
017 U 10017Chlorobenzene
017 U 10017Dibromochloromethane
041 U 10041Chloroethane
016 U 10016Chloroform
030 U 10030Chloromethane
017 U 100172-Chlorotoluene
021 U 100214-Chlorotoluene
047 U 1004712-Dibromo-3-Chloropropane
017 U 10017Dibromomethane
015 U 1001512-Dichlorobenzene
013 U 1001313-Dichlorobenzene
016 U 1001614-Dichlorobenzene
031 U 10031Dichlorodifluoromethane
043 J 1002211-Dichloroethane
013 U 1001312-Dichloroethane
015 U 10015cis-12-Dichloroethene
015 U 10015trans-12-Dichloroethene
023 U 1002311-Dichloroethene
018 U 1001812-Dichloropropane
022 U 1002213-Dichloropropane
018 U 1001822-Dichloropropane
016 U 10016cis-13-Dichloropropene
019 U 10019trans-13-Dichloropropene
019 U 1001911-Dichloropropene
016 U 10016Ethylbenzene
036 U 10036Hexachlorobutadiene
17 U 50172-Hexanone
019 U 10019Isopropylbenzene
020 U 100204-Isopropyltoluene
032 U 10032Methylene Chloride
098 U 500984-Methyl-2-pentanone
022 U 10022Naphthalene
016 U 10016n-Propylbenzene
TestAmerica Denver Page 44 of 1510
Analytical Data
Client SM Stoller Corporation Job Number 280-39873-1
Sdg Number 13025120
Client Sample ID
Lab Sample ID
PIN12-0582-1
Client Matrix
280-39873-14
Water
Date Sampled 03112013 1147
Date Received 03132013 0900
8260B Volatile Organic Compounds (GCMS)
Dilution
03182013 1748
03182013 1748
10
8260B
Final WeightVolume
Initial WeightVolume
Lab File ID
Instrument ID
C5357D
20 mL
20 mL
5030B
VMS_C
Analysis Date
Prep Date
Analysis Batch
Prep Batch
280-165236
NA
Analysis Method
Prep Method
Analyte Result (ugL) Qualifier MDL RL
017 U 10017Styrene
021 U 100211112-Tetrachloroethane
021 U 100211122-Tetrachloroethane
020 U 10020Tetrachloroethene
017 U 10017Toluene
021 U 10021123-Trichlorobenzene
021 U 10021124-Trichlorobenzene
016 U 10016111-Trichloroethane
027 U 10027112-Trichloroethane
016 U 10016Trichloroethene
029 U 10029Trichlorofluoromethane
033 U 10033123-Trichloropropane
015 U 10015124-Trimethylbenzene
016 U 10016135-Trimethylbenzene
12 10010Vinyl chloride
019 U 10019Xylenes Total
018 U 1001812-Dibromoethane
Surrogate Rec Acceptance LimitsQualifier
121 70 - 12712-Dichloroethane-d4 (Surr)
89 80 - 125Toluene-d8 (Surr)
89 78 - 1204-Bromofluorobenzene (Surr)
107 77 - 120Dibromofluoromethane (Surr)
TestAmerica Denver Page 45 of 1510
Analytical Data
Client SM Stoller Corporation Job Number 280-39873-1
Sdg Number 13025120
Client Sample ID
Lab Sample ID
PIN12-0582-2
Client Matrix
280-39873-15
Water
Date Sampled 03112013 1218
Date Received 03132013 0900
8260B Volatile Organic Compounds (GCMS)
Dilution
03182013 1808
03182013 1808
10
8260B
Final WeightVolume
Initial WeightVolume
Lab File ID
Instrument ID
C5358D
10 mL
20 mL
5030B
VMS_C
Analysis Date
Prep Date
Analysis Batch
Prep Batch
280-165236
NA
Analysis Method
Prep Method
Analyte Result (ugL) Qualifier MDL RL
73 J 2038Acetone
032 U 20032Benzene
034 U 20034Bromobenzene
020 U 20020Bromochloromethane
034 U 20034Bromodichloromethane
038 U 20038Bromoform
042 U 20042Bromomethane
40 U 10402-Butanone (MEK)
064 U 20064n-Butylbenzene
034 U 20034sec-Butylbenzene
032 U 20032tert-Butylbenzene
090 U 20090Carbon disulfide
038 U 20038Carbon tetrachloride
034 U 20034Chlorobenzene
034 U 20034Dibromochloromethane
082 U 20082Chloroethane
032 U 20032Chloroform
060 U 20060Chloromethane
034 U 200342-Chlorotoluene
042 U 200424-Chlorotoluene
094 U 2009412-Dibromo-3-Chloropropane
034 U 20034Dibromomethane
030 U 2003012-Dichlorobenzene
026 U 2002613-Dichlorobenzene
032 U 2003214-Dichlorobenzene
062 U 20062Dichlorodifluoromethane
49 2004411-Dichloroethane
026 U 2002612-Dichloroethane
13 20030cis-12-Dichloroethene
23 20030trans-12-Dichloroethene
063 J 2004611-Dichloroethene
036 U 2003612-Dichloropropane
044 U 2004413-Dichloropropane
036 U 2003622-Dichloropropane
032 U 20032cis-13-Dichloropropene
038 U 20038trans-13-Dichloropropene
038 U 2003811-Dichloropropene
032 U 20032Ethylbenzene
072 U 20072Hexachlorobutadiene
34 U 10342-Hexanone
038 U 20038Isopropylbenzene
040 U 200404-Isopropyltoluene
064 U 20064Methylene Chloride
20 U 10204-Methyl-2-pentanone
044 U 20044Naphthalene
032 U 20032n-Propylbenzene
TestAmerica Denver Page 46 of 1510
Analytical Data
Client SM Stoller Corporation Job Number 280-39873-1
Sdg Number 13025120
Client Sample ID
Lab Sample ID
PIN12-0582-2
Client Matrix
280-39873-15
Water
Date Sampled 03112013 1218
Date Received 03132013 0900
8260B Volatile Organic Compounds (GCMS)
Dilution
03182013 1808
03182013 1808
10
8260B
Final WeightVolume
Initial WeightVolume
Lab File ID
Instrument ID
C5358D
10 mL
20 mL
5030B
VMS_C
Analysis Date
Prep Date
Analysis Batch
Prep Batch
280-165236
NA
Analysis Method
Prep Method
Analyte Result (ugL) Qualifier MDL RL
034 U 20034Styrene
042 U 200421112-Tetrachloroethane
042 U 200421122-Tetrachloroethane
040 U 20040Tetrachloroethene
034 U 20034Toluene
042 U 20042123-Trichlorobenzene
042 U 20042124-Trichlorobenzene
032 U 20032111-Trichloroethane
054 U 20054112-Trichloroethane
032 U 20032Trichloroethene
058 U 20058Trichlorofluoromethane
066 U 20066123-Trichloropropane
030 U 20030124-Trimethylbenzene
032 U 20032135-Trimethylbenzene
038 U 20038Xylenes Total
036 U 2003612-Dibromoethane
Surrogate Rec Acceptance LimitsQualifier
119 70 - 12712-Dichloroethane-d4 (Surr)
92 80 - 125Toluene-d8 (Surr)
90 78 - 1204-Bromofluorobenzene (Surr)
110 77 - 120Dibromofluoromethane (Surr)
TestAmerica Denver Page 47 of 1510
Analytical Data
Client SM Stoller Corporation Job Number 280-39873-1
Sdg Number 13025120
Client Sample ID
Lab Sample ID
PIN12-0582-2
Client Matrix
280-39873-15
Water
Date Sampled 03112013 1218
Date Received 03132013 0900
8260B Volatile Organic Compounds (GCMS)
Dilution
03192013 1314
03192013 1314
10
8260B
Final WeightVolume
Initial WeightVolume
Lab File ID
Instrument ID
RR2022D
2 mL
20 mLRun Type DL
5030B
VMS_R2
Analysis Date
Prep Date
Analysis Batch
Prep Batch
280-165451
NA
Analysis Method
Prep Method
Analyte Result (ugL) Qualifier MDL RL
74 1010Vinyl chloride
Surrogate Rec Acceptance LimitsQualifier
77 70 - 12712-Dichloroethane-d4 (Surr)
95 80 - 125Toluene-d8 (Surr)
89 78 - 1204-Bromofluorobenzene (Surr)
87 77 - 120Dibromofluoromethane (Surr)
TestAmerica Denver Page 48 of 1510
Analytical Data
Client SM Stoller Corporation Job Number 280-39873-1
Sdg Number 13025120
Client Sample ID
Lab Sample ID
PIN12-0582-3
Client Matrix
280-39873-16
Water
Date Sampled 03112013 1253
Date Received 03132013 0900
8260B Volatile Organic Compounds (GCMS)
Dilution
03192013 1042
03192013 1042
10
8260B
Final WeightVolume
Initial WeightVolume
Lab File ID
Instrument ID
H0948D
20 mL
20 mL
5030B
VMS_H
Analysis Date
Prep Date
Analysis Batch
Prep Batch
280-165434
NA
Analysis Method
Prep Method
Analyte Result (ugL) Qualifier MDL RL
19 U 1019Acetone
016 U 10016Benzene
017 U 10017Bromobenzene
010 U 10010Bromochloromethane
017 U 10017Bromodichloromethane
019 U 10019Bromoform
021 U 10021Bromomethane
20 U 50202-Butanone (MEK)
032 U 10032n-Butylbenzene
017 U 10017sec-Butylbenzene
016 U 10016tert-Butylbenzene
045 U 10045Carbon disulfide
019 U 10019Carbon tetrachloride
017 U 10017Chlorobenzene
017 U 10017Dibromochloromethane
041 U 10041Chloroethane
016 U 10016Chloroform
030 U 10030Chloromethane
017 U 100172-Chlorotoluene
021 U 100214-Chlorotoluene
047 U 1004712-Dibromo-3-Chloropropane
017 U 10017Dibromomethane
015 U 1001512-Dichlorobenzene
013 U 1001313-Dichlorobenzene
016 U 1001614-Dichlorobenzene
031 U 10031Dichlorodifluoromethane
022 U 1002211-Dichloroethane
013 U 1001312-Dichloroethane
020 J 10015cis-12-Dichloroethene
015 U 10015trans-12-Dichloroethene
023 U 1002311-Dichloroethene
018 U 1001812-Dichloropropane
022 U 1002213-Dichloropropane
018 U 1001822-Dichloropropane
016 U 10016cis-13-Dichloropropene
019 U 10019trans-13-Dichloropropene
019 U 1001911-Dichloropropene
016 U 10016Ethylbenzene
036 U 10036Hexachlorobutadiene
17 U 50172-Hexanone
019 U 10019Isopropylbenzene
020 U 100204-Isopropyltoluene
032 U 10032Methylene Chloride
098 U 500984-Methyl-2-pentanone
022 U 10022Naphthalene
016 U 10016n-Propylbenzene
TestAmerica Denver Page 49 of 1510
Analytical Data
Client SM Stoller Corporation Job Number 280-39873-1
Sdg Number 13025120
Client Sample ID
Lab Sample ID
PIN12-0582-3
Client Matrix
280-39873-16
Water
Date Sampled 03112013 1253
Date Received 03132013 0900
8260B Volatile Organic Compounds (GCMS)
Dilution
03192013 1042
03192013 1042
10
8260B
Final WeightVolume
Initial WeightVolume
Lab File ID
Instrument ID
H0948D
20 mL
20 mL
5030B
VMS_H
Analysis Date
Prep Date
Analysis Batch
Prep Batch
280-165434
NA
Analysis Method
Prep Method
Analyte Result (ugL) Qualifier MDL RL
017 U 10017Styrene
021 U 100211112-Tetrachloroethane
021 U 100211122-Tetrachloroethane
020 U 10020Tetrachloroethene
017 U 10017Toluene
021 U 10021123-Trichlorobenzene
021 U 10021124-Trichlorobenzene
016 U 10016111-Trichloroethane
027 U 10027112-Trichloroethane
016 U 10016Trichloroethene
029 U 10029Trichlorofluoromethane
033 U 10033123-Trichloropropane
015 U 10015124-Trimethylbenzene
016 U 10016135-Trimethylbenzene
12 10010Vinyl chloride
019 U 10019Xylenes Total
018 U 1001812-Dibromoethane
Surrogate Rec Acceptance LimitsQualifier
127 70 - 12712-Dichloroethane-d4 (Surr)
101 80 - 125Toluene-d8 (Surr)
102 78 - 1204-Bromofluorobenzene (Surr)
111 77 - 120Dibromofluoromethane (Surr)
TestAmerica Denver Page 50 of 1510
Analytical Data
Client SM Stoller Corporation Job Number 280-39873-1
Sdg Number 13025120
Client Sample ID
Lab Sample ID
PIN12-0585-3
Client Matrix
280-39873-17
Water
Date Sampled 03092013 1133
Date Received 03132013 0900
8260B Volatile Organic Compounds (GCMS)
Dilution
03192013 1127
03192013 1127
10
8260B
Final WeightVolume
Initial WeightVolume
Lab File ID
Instrument ID
H0950D
4 mL
20 mLRun Type DL
5030B
VMS_H
Analysis Date
Prep Date
Analysis Batch
Prep Batch
280-165434
NA
Analysis Method
Prep Method
Analyte Result (ugL) Qualifier MDL RL
140 50075cis-12-Dichloroethene
200 50050Vinyl chloride
Surrogate Rec Acceptance LimitsQualifier
117 70 - 12712-Dichloroethane-d4 (Surr)
95 80 - 125Toluene-d8 (Surr)
97 78 - 1204-Bromofluorobenzene (Surr)
107 77 - 120Dibromofluoromethane (Surr)
TestAmerica Denver Page 51 of 1510
Analytical Data
Client SM Stoller Corporation Job Number 280-39873-1
Sdg Number 13025120
Client Sample ID
Lab Sample ID
PIN12-0585-3
Client Matrix
280-39873-17
Water
Date Sampled 03092013 1133
Date Received 03132013 0900
8260B Volatile Organic Compounds (GCMS)
Dilution
03202013 0810
03202013 0810
10
8260B
Final WeightVolume
Initial WeightVolume
Lab File ID
Instrument ID
Z2931D
20 mL
20 mL
5030B
VMS_Z
Analysis Date
Prep Date
Analysis Batch
Prep Batch
280-165627
NA
Analysis Method
Prep Method
Analyte Result (ugL) Qualifier MDL RL
19 U 1019Acetone
016 U 10016Benzene
017 U 10017Bromobenzene
010 U 10010Bromochloromethane
017 U 10017Bromodichloromethane
019 U 10019Bromoform
021 U 10021Bromomethane
20 U 50202-Butanone (MEK)
032 U 10032n-Butylbenzene
017 U 10017sec-Butylbenzene
016 U 10016tert-Butylbenzene
41 10045Carbon disulfide
019 U 10019Carbon tetrachloride
017 U 10017Chlorobenzene
017 U 10017Dibromochloromethane
041 U 10041Chloroethane
016 U 10016Chloroform
030 U 10030Chloromethane
017 U 100172-Chlorotoluene
021 U 100214-Chlorotoluene
047 U 1004712-Dibromo-3-Chloropropane
017 U 10017Dibromomethane
015 U 1001512-Dichlorobenzene
013 U 1001313-Dichlorobenzene
016 U 1001614-Dichlorobenzene
031 U 10031Dichlorodifluoromethane
022 U 1002211-Dichloroethane
013 U 1001312-Dichloroethane
11 10015trans-12-Dichloroethene
40 1002311-Dichloroethene
018 U 1001812-Dichloropropane
022 U 1002213-Dichloropropane
018 U 1001822-Dichloropropane
016 U 10016cis-13-Dichloropropene
019 U 10019trans-13-Dichloropropene
019 U 1001911-Dichloropropene
016 U 10016Ethylbenzene
036 U 10036Hexachlorobutadiene
39 J 50172-Hexanone
019 U 10019Isopropylbenzene
020 U 100204-Isopropyltoluene
032 U 10032Methylene Chloride
098 U 500984-Methyl-2-pentanone
022 U 10022Naphthalene
016 U 10016n-Propylbenzene
017 U 10017Styrene
TestAmerica Denver Page 52 of 1510
Analytical Data
Client SM Stoller Corporation Job Number 280-39873-1
Sdg Number 13025120
Client Sample ID
Lab Sample ID
PIN12-0585-3
Client Matrix
280-39873-17
Water
Date Sampled 03092013 1133
Date Received 03132013 0900
8260B Volatile Organic Compounds (GCMS)
Dilution
03202013 0810
03202013 0810
10
8260B
Final WeightVolume
Initial WeightVolume
Lab File ID
Instrument ID
Z2931D
20 mL
20 mL
5030B
VMS_Z
Analysis Date
Prep Date
Analysis Batch
Prep Batch
280-165627
NA
Analysis Method
Prep Method
Analyte Result (ugL) Qualifier MDL RL
021 U 100211112-Tetrachloroethane
021 U 100211122-Tetrachloroethane
020 U 10020Tetrachloroethene
017 U 10017Toluene
021 U 10021123-Trichlorobenzene
021 U 10021124-Trichlorobenzene
016 U 10016111-Trichloroethane
027 U 10027112-Trichloroethane
071 J 10016Trichloroethene
029 U 10029Trichlorofluoromethane
033 U 10033123-Trichloropropane
015 U 10015124-Trimethylbenzene
016 U 10016135-Trimethylbenzene
019 U 10019Xylenes Total
018 U 1001812-Dibromoethane
Surrogate Rec Acceptance LimitsQualifier
101 70 - 12712-Dichloroethane-d4 (Surr)
119 80 - 125Toluene-d8 (Surr)
96 78 - 1204-Bromofluorobenzene (Surr)
99 77 - 120Dibromofluoromethane (Surr)
TestAmerica Denver Page 53 of 1510
Analytical Data
Client SM Stoller Corporation Job Number 280-39873-1
Sdg Number 13025120
Client Sample ID
Lab Sample ID
PIN12-2451
Client Matrix
280-39873-18
Water
Date Sampled 03112013 1200
Date Received 03132013 0900
8260B Volatile Organic Compounds (GCMS)
Dilution
03192013 1448
03192013 1448
10
8260B
Final WeightVolume
Initial WeightVolume
Lab File ID
Instrument ID
H0959D
20 mL
20 mL
5030B
VMS_H
Analysis Date
Prep Date
Analysis Batch
Prep Batch
280-165434
NA
Analysis Method
Prep Method
Analyte Result (ugL) Qualifier MDL RL
19 U 1019Acetone
016 U 10016Benzene
017 U 10017Bromobenzene
010 U 10010Bromochloromethane
017 U 10017Bromodichloromethane
019 U 10019Bromoform
021 U 10021Bromomethane
20 U 50202-Butanone (MEK)
032 U 10032n-Butylbenzene
017 U 10017sec-Butylbenzene
016 U 10016tert-Butylbenzene
045 U 10045Carbon disulfide
019 U 10019Carbon tetrachloride
017 U 10017Chlorobenzene
017 U 10017Dibromochloromethane
041 U 10041Chloroethane
016 U 10016Chloroform
030 U 10030Chloromethane
017 U 100172-Chlorotoluene
021 U 100214-Chlorotoluene
047 U 1004712-Dibromo-3-Chloropropane
017 U 10017Dibromomethane
015 U 1001512-Dichlorobenzene
013 U 1001313-Dichlorobenzene
016 U 1001614-Dichlorobenzene
031 U 10031Dichlorodifluoromethane
12 1002211-Dichloroethane
013 U 1001312-Dichloroethane
36 10015cis-12-Dichloroethene
015 U 10015trans-12-Dichloroethene
047 J 1002311-Dichloroethene
018 U 1001812-Dichloropropane
022 U 1002213-Dichloropropane
018 U 1001822-Dichloropropane
016 U 10016cis-13-Dichloropropene
019 U 10019trans-13-Dichloropropene
019 U 1001911-Dichloropropene
016 U 10016Ethylbenzene
036 U 10036Hexachlorobutadiene
17 U 50172-Hexanone
019 U 10019Isopropylbenzene
020 U 100204-Isopropyltoluene
032 U 10032Methylene Chloride
098 U 500984-Methyl-2-pentanone
022 U 10022Naphthalene
016 U 10016n-Propylbenzene
TestAmerica Denver Page 54 of 1510
Analytical Data
Client SM Stoller Corporation Job Number 280-39873-1
Sdg Number 13025120
Client Sample ID
Lab Sample ID
PIN12-2451
Client Matrix
280-39873-18
Water
Date Sampled 03112013 1200
Date Received 03132013 0900
8260B Volatile Organic Compounds (GCMS)
Dilution
03192013 1448
03192013 1448
10
8260B
Final WeightVolume
Initial WeightVolume
Lab File ID
Instrument ID
H0959D
20 mL
20 mL
5030B
VMS_H
Analysis Date
Prep Date
Analysis Batch
Prep Batch
280-165434
NA
Analysis Method
Prep Method
Analyte Result (ugL) Qualifier MDL RL
017 U 10017Styrene
021 U 100211112-Tetrachloroethane
021 U 100211122-Tetrachloroethane
020 U 10020Tetrachloroethene
017 U 10017Toluene
021 U 10021123-Trichlorobenzene
021 U 10021124-Trichlorobenzene
016 U 10016111-Trichloroethane
027 U 10027112-Trichloroethane
016 U 10016Trichloroethene
029 U 10029Trichlorofluoromethane
033 U 10033123-Trichloropropane
015 U 10015124-Trimethylbenzene
016 U 10016135-Trimethylbenzene
73 10010Vinyl chloride
019 U 10019Xylenes Total
018 U 1001812-Dibromoethane
Surrogate Rec Acceptance LimitsQualifier
127 70 - 12712-Dichloroethane-d4 (Surr)
106 80 - 125Toluene-d8 (Surr)
101 78 - 1204-Bromofluorobenzene (Surr)
110 77 - 120Dibromofluoromethane (Surr)
TestAmerica Denver Page 55 of 1510
Analytical Data
Client SM Stoller Corporation Job Number 280-39873-1
Sdg Number 13025120
Client Sample ID
Lab Sample ID
PIN12-2452
Client Matrix
280-39873-19
Water
Date Sampled 03112013 1210
Date Received 03132013 0900
8260B Volatile Organic Compounds (GCMS)
Dilution
03192013 1510
03192013 1510
10
8260B
Final WeightVolume
Initial WeightVolume
Lab File ID
Instrument ID
H0960D
20 mL
20 mL
5030B
VMS_H
Analysis Date
Prep Date
Analysis Batch
Prep Batch
280-165434
NA
Analysis Method
Prep Method
Analyte Result (ugL) Qualifier MDL RL
19 U 1019Acetone
016 U 10016Benzene
017 U 10017Bromobenzene
010 U 10010Bromochloromethane
017 U 10017Bromodichloromethane
019 U 10019Bromoform
021 U 10021Bromomethane
20 U 50202-Butanone (MEK)
032 U 10032n-Butylbenzene
017 U 10017sec-Butylbenzene
016 U 10016tert-Butylbenzene
045 U 10045Carbon disulfide
019 U 10019Carbon tetrachloride
017 U 10017Chlorobenzene
017 U 10017Dibromochloromethane
041 U 10041Chloroethane
016 U 10016Chloroform
030 U 10030Chloromethane
017 U 100172-Chlorotoluene
021 U 100214-Chlorotoluene
047 U 1004712-Dibromo-3-Chloropropane
017 U 10017Dibromomethane
015 U 1001512-Dichlorobenzene
013 U 1001313-Dichlorobenzene
016 U 1001614-Dichlorobenzene
031 U 10031Dichlorodifluoromethane
46 1002211-Dichloroethane
013 U 1001312-Dichloroethane
13 10015cis-12-Dichloroethene
25 10015trans-12-Dichloroethene
072 J 1002311-Dichloroethene
018 U 1001812-Dichloropropane
022 U 1002213-Dichloropropane
018 U 1001822-Dichloropropane
016 U 10016cis-13-Dichloropropene
019 U 10019trans-13-Dichloropropene
019 U 1001911-Dichloropropene
016 U 10016Ethylbenzene
036 U 10036Hexachlorobutadiene
17 U 50172-Hexanone
019 U 10019Isopropylbenzene
020 U 100204-Isopropyltoluene
032 U 10032Methylene Chloride
098 U 500984-Methyl-2-pentanone
023 J 10022Naphthalene
016 U 10016n-Propylbenzene
TestAmerica Denver Page 56 of 1510
Analytical Data
Client SM Stoller Corporation Job Number 280-39873-1
Sdg Number 13025120
Client Sample ID
Lab Sample ID
PIN12-2452
Client Matrix
280-39873-19
Water
Date Sampled 03112013 1210
Date Received 03132013 0900
8260B Volatile Organic Compounds (GCMS)
Dilution
03192013 1510
03192013 1510
10
8260B
Final WeightVolume
Initial WeightVolume
Lab File ID
Instrument ID
H0960D
20 mL
20 mL
5030B
VMS_H
Analysis Date
Prep Date
Analysis Batch
Prep Batch
280-165434
NA
Analysis Method
Prep Method
Analyte Result (ugL) Qualifier MDL RL
017 U 10017Styrene
021 U 100211112-Tetrachloroethane
021 U 100211122-Tetrachloroethane
020 U 10020Tetrachloroethene
017 U 10017Toluene
021 U 10021123-Trichlorobenzene
021 U 10021124-Trichlorobenzene
016 U 10016111-Trichloroethane
027 U 10027112-Trichloroethane
016 U 10016Trichloroethene
029 U 10029Trichlorofluoromethane
033 U 10033123-Trichloropropane
015 U 10015124-Trimethylbenzene
016 U 10016135-Trimethylbenzene
019 U 10019Xylenes Total
018 U 1001812-Dibromoethane
Surrogate Rec Acceptance LimitsQualifier
123 70 - 12712-Dichloroethane-d4 (Surr)
94 80 - 125Toluene-d8 (Surr)
96 78 - 1204-Bromofluorobenzene (Surr)
106 77 - 120Dibromofluoromethane (Surr)
TestAmerica Denver Page 57 of 1510
Analytical Data
Client SM Stoller Corporation Job Number 280-39873-1
Sdg Number 13025120
Client Sample ID
Lab Sample ID
PIN12-2452
Client Matrix
280-39873-19
Water
Date Sampled 03112013 1210
Date Received 03132013 0900
8260B Volatile Organic Compounds (GCMS)
Dilution
03202013 0833
03202013 0833
10
8260B
Final WeightVolume
Initial WeightVolume
Lab File ID
Instrument ID
Z2932D
5 mL
20 mLRun Type DL
5030B
VMS_Z
Analysis Date
Prep Date
Analysis Batch
Prep Batch
280-165627
NA
Analysis Method
Prep Method
Analyte Result (ugL) Qualifier MDL RL
130 40040Vinyl chloride
Surrogate Rec Acceptance LimitsQualifier
101 70 - 12712-Dichloroethane-d4 (Surr)
98 80 - 125Toluene-d8 (Surr)
98 78 - 1204-Bromofluorobenzene (Surr)
101 77 - 120Dibromofluoromethane (Surr)
TestAmerica Denver Page 58 of 1510
Analytical Data
Client SM Stoller Corporation Job Number 280-39873-1
Sdg Number 13025120
Client Sample ID
Lab Sample ID
PIN12-S71B
Client Matrix
280-39873-20
Water
Date Sampled 03092013 0908
Date Received 03132013 0900
8260B Volatile Organic Compounds (GCMS)
Dilution
03192013 1554
03192013 1554
10
8260B
Final WeightVolume
Initial WeightVolume
Lab File ID
Instrument ID
H0962D
20 mL
20 mL
5030B
VMS_H
Analysis Date
Prep Date
Analysis Batch
Prep Batch
280-165434
NA
Analysis Method
Prep Method
Analyte Result (ugL) Qualifier MDL RL
19 U 1019Acetone
016 U 10016Benzene
017 U 10017Bromobenzene
010 U 10010Bromochloromethane
017 U 10017Bromodichloromethane
019 U 10019Bromoform
021 U 10021Bromomethane
20 U 50202-Butanone (MEK)
032 U 10032n-Butylbenzene
017 U 10017sec-Butylbenzene
016 U 10016tert-Butylbenzene
045 U 10045Carbon disulfide
019 U 10019Carbon tetrachloride
017 U 10017Chlorobenzene
017 U 10017Dibromochloromethane
041 U 10041Chloroethane
016 U 10016Chloroform
030 U 10030Chloromethane
017 U 100172-Chlorotoluene
021 U 100214-Chlorotoluene
047 U 1004712-Dibromo-3-Chloropropane
017 U 10017Dibromomethane
015 U 1001512-Dichlorobenzene
013 U 1001313-Dichlorobenzene
016 U 1001614-Dichlorobenzene
031 U 10031Dichlorodifluoromethane
022 U 1002211-Dichloroethane
013 U 1001312-Dichloroethane
015 U 10015cis-12-Dichloroethene
015 U 10015trans-12-Dichloroethene
023 U 1002311-Dichloroethene
018 U 1001812-Dichloropropane
022 U 1002213-Dichloropropane
018 U 1001822-Dichloropropane
016 U 10016cis-13-Dichloropropene
019 U 10019trans-13-Dichloropropene
019 U 1001911-Dichloropropene
016 U 10016Ethylbenzene
036 U 10036Hexachlorobutadiene
17 U 50172-Hexanone
019 U 10019Isopropylbenzene
020 U 100204-Isopropyltoluene
032 U 10032Methylene Chloride
098 U 500984-Methyl-2-pentanone
022 U 10022Naphthalene
016 U 10016n-Propylbenzene
TestAmerica Denver Page 59 of 1510
Analytical Data
Client SM Stoller Corporation Job Number 280-39873-1
Sdg Number 13025120
Client Sample ID
Lab Sample ID
PIN12-S71B
Client Matrix
280-39873-20
Water
Date Sampled 03092013 0908
Date Received 03132013 0900
8260B Volatile Organic Compounds (GCMS)
Dilution
03192013 1554
03192013 1554
10
8260B
Final WeightVolume
Initial WeightVolume
Lab File ID
Instrument ID
H0962D
20 mL
20 mL
5030B
VMS_H
Analysis Date
Prep Date
Analysis Batch
Prep Batch
280-165434
NA
Analysis Method
Prep Method
Analyte Result (ugL) Qualifier MDL RL
017 U 10017Styrene
021 U 100211112-Tetrachloroethane
021 U 100211122-Tetrachloroethane
020 U 10020Tetrachloroethene
017 U 10017Toluene
021 U 10021123-Trichlorobenzene
021 U 10021124-Trichlorobenzene
016 U 10016111-Trichloroethane
027 U 10027112-Trichloroethane
016 U 10016Trichloroethene
029 U 10029Trichlorofluoromethane
033 U 10033123-Trichloropropane
015 U 10015124-Trimethylbenzene
016 U 10016135-Trimethylbenzene
010 U 10010Vinyl chloride
019 U 10019Xylenes Total
018 U 1001812-Dibromoethane
Surrogate Rec Acceptance LimitsQualifier
120 70 - 12712-Dichloroethane-d4 (Surr)
94 80 - 125Toluene-d8 (Surr)
99 78 - 1204-Bromofluorobenzene (Surr)
105 77 - 120Dibromofluoromethane (Surr)
TestAmerica Denver Page 60 of 1510
Analytical Data
Client SM Stoller Corporation Job Number 280-39873-1
Sdg Number 13025120
Client Sample ID
Lab Sample ID
PIN12-S71C
Client Matrix
280-39873-21
Water
Date Sampled 03092013 0936
Date Received 03132013 0900
8260B Volatile Organic Compounds (GCMS)
Dilution
03192013 1617
03192013 1617
10
8260B
Final WeightVolume
Initial WeightVolume
Lab File ID
Instrument ID
H0963D
20 mL
20 mL
5030B
VMS_H
Analysis Date
Prep Date
Analysis Batch
Prep Batch
280-165434
NA
Analysis Method
Prep Method
Analyte Result (ugL) Qualifier MDL RL
19 U 1019Acetone
016 U 10016Benzene
017 U 10017Bromobenzene
010 U 10010Bromochloromethane
017 U 10017Bromodichloromethane
019 U 10019Bromoform
021 U 10021Bromomethane
20 U 50202-Butanone (MEK)
032 U 10032n-Butylbenzene
017 U 10017sec-Butylbenzene
016 U 10016tert-Butylbenzene
045 U 10045Carbon disulfide
019 U 10019Carbon tetrachloride
017 U 10017Chlorobenzene
017 U 10017Dibromochloromethane
041 U 10041Chloroethane
016 U 10016Chloroform
030 U 10030Chloromethane
017 U 100172-Chlorotoluene
021 U 100214-Chlorotoluene
047 U 1004712-Dibromo-3-Chloropropane
017 U 10017Dibromomethane
015 U 1001512-Dichlorobenzene
013 U 1001313-Dichlorobenzene
016 U 1001614-Dichlorobenzene
031 U 10031Dichlorodifluoromethane
29 1002211-Dichloroethane
013 U 1001312-Dichloroethane
18 10015cis-12-Dichloroethene
10 10015trans-12-Dichloroethene
029 J 1002311-Dichloroethene
018 U 1001812-Dichloropropane
022 U 1002213-Dichloropropane
018 U 1001822-Dichloropropane
016 U 10016cis-13-Dichloropropene
019 U 10019trans-13-Dichloropropene
019 U 1001911-Dichloropropene
016 U 10016Ethylbenzene
036 U 10036Hexachlorobutadiene
17 U 50172-Hexanone
019 U 10019Isopropylbenzene
020 U 100204-Isopropyltoluene
032 U 10032Methylene Chloride
098 U 500984-Methyl-2-pentanone
022 U 10022Naphthalene
016 U 10016n-Propylbenzene
TestAmerica Denver Page 61 of 1510
Analytical Data
Client SM Stoller Corporation Job Number 280-39873-1
Sdg Number 13025120
Client Sample ID
Lab Sample ID
PIN12-S71C
Client Matrix
280-39873-21
Water
Date Sampled 03092013 0936
Date Received 03132013 0900
8260B Volatile Organic Compounds (GCMS)
Dilution
03192013 1617
03192013 1617
10
8260B
Final WeightVolume
Initial WeightVolume
Lab File ID
Instrument ID
H0963D
20 mL
20 mL
5030B
VMS_H
Analysis Date
Prep Date
Analysis Batch
Prep Batch
280-165434
NA
Analysis Method
Prep Method
Analyte Result (ugL) Qualifier MDL RL
017 U 10017Styrene
021 U 100211112-Tetrachloroethane
021 U 100211122-Tetrachloroethane
020 U 10020Tetrachloroethene
017 U 10017Toluene
021 U 10021123-Trichlorobenzene
021 U 10021124-Trichlorobenzene
016 U 10016111-Trichloroethane
027 U 10027112-Trichloroethane
016 U 10016Trichloroethene
029 U 10029Trichlorofluoromethane
033 U 10033123-Trichloropropane
015 U 10015124-Trimethylbenzene
016 U 10016135-Trimethylbenzene
44 10010Vinyl chloride
019 U 10019Xylenes Total
018 U 1001812-Dibromoethane
Surrogate Rec Acceptance LimitsQualifier
126 70 - 12712-Dichloroethane-d4 (Surr)
99 80 - 125Toluene-d8 (Surr)
99 78 - 1204-Bromofluorobenzene (Surr)
109 77 - 120Dibromofluoromethane (Surr)
TestAmerica Denver Page 62 of 1510
Analytical Data
Client SM Stoller Corporation Job Number 280-39873-1
Sdg Number 13025120
Client Sample ID
Lab Sample ID
PIN12-S71D
Client Matrix
280-39873-22
Water
Date Sampled 03092013 1026
Date Received 03132013 0900
8260B Volatile Organic Compounds (GCMS)
Dilution
03202013 0857
03202013 0857
10
8260B
Final WeightVolume
Initial WeightVolume
Lab File ID
Instrument ID
Z2933D
20 mL
20 mL
5030B
VMS_Z
Analysis Date
Prep Date
Analysis Batch
Prep Batch
280-165627
NA
Analysis Method
Prep Method
Analyte Result (ugL) Qualifier MDL RL
19 U 1019Acetone
016 U 10016Benzene
017 U 10017Bromobenzene
010 U 10010Bromochloromethane
017 U 10017Bromodichloromethane
019 U 10019Bromoform
021 U 10021Bromomethane
20 U 50202-Butanone (MEK)
032 U 10032n-Butylbenzene
017 U 10017sec-Butylbenzene
016 U 10016tert-Butylbenzene
045 U 10045Carbon disulfide
019 U 10019Carbon tetrachloride
017 U 10017Chlorobenzene
017 U 10017Dibromochloromethane
041 U 10041Chloroethane
016 U 10016Chloroform
030 U 10030Chloromethane
017 U 100172-Chlorotoluene
021 U 100214-Chlorotoluene
047 U 1004712-Dibromo-3-Chloropropane
017 U 10017Dibromomethane
015 U 1001512-Dichlorobenzene
013 U 1001313-Dichlorobenzene
016 U 1001614-Dichlorobenzene
031 U 10031Dichlorodifluoromethane
28 1002211-Dichloroethane
013 U 1001312-Dichloroethane
29 10015cis-12-Dichloroethene
17 10015trans-12-Dichloroethene
060 J 1002311-Dichloroethene
018 U 1001812-Dichloropropane
022 U 1002213-Dichloropropane
018 U 1001822-Dichloropropane
016 U 10016cis-13-Dichloropropene
019 U 10019trans-13-Dichloropropene
019 U 1001911-Dichloropropene
016 U 10016Ethylbenzene
036 U 10036Hexachlorobutadiene
17 U 50172-Hexanone
019 U 10019Isopropylbenzene
020 U 100204-Isopropyltoluene
032 U 10032Methylene Chloride
098 U 500984-Methyl-2-pentanone
022 U 10022Naphthalene
016 U 10016n-Propylbenzene
TestAmerica Denver Page 63 of 1510
Analytical Data
Client SM Stoller Corporation Job Number 280-39873-1
Sdg Number 13025120
Client Sample ID
Lab Sample ID
PIN12-S71D
Client Matrix
280-39873-22
Water
Date Sampled 03092013 1026
Date Received 03132013 0900
8260B Volatile Organic Compounds (GCMS)
Dilution
03202013 0857
03202013 0857
10
8260B
Final WeightVolume
Initial WeightVolume
Lab File ID
Instrument ID
Z2933D
20 mL
20 mL
5030B
VMS_Z
Analysis Date
Prep Date
Analysis Batch
Prep Batch
280-165627
NA
Analysis Method
Prep Method
Analyte Result (ugL) Qualifier MDL RL
017 U 10017Styrene
021 U 100211112-Tetrachloroethane
021 U 100211122-Tetrachloroethane
020 U 10020Tetrachloroethene
017 U 10017Toluene
021 U 10021123-Trichlorobenzene
021 U 10021124-Trichlorobenzene
016 U 10016111-Trichloroethane
027 U 10027112-Trichloroethane
016 U 10016Trichloroethene
029 U 10029Trichlorofluoromethane
033 U 10033123-Trichloropropane
015 U 10015124-Trimethylbenzene
016 U 10016135-Trimethylbenzene
60 10010Vinyl chloride
019 U 10019Xylenes Total
018 U 1001812-Dibromoethane
Surrogate Rec Acceptance LimitsQualifier
119 70 - 12712-Dichloroethane-d4 (Surr)
92 80 - 125Toluene-d8 (Surr)
92 78 - 1204-Bromofluorobenzene (Surr)
116 77 - 120Dibromofluoromethane (Surr)
TestAmerica Denver Page 64 of 1510
Analytical Data
Client SM Stoller Corporation Job Number 280-39873-1
Sdg Number 13025120
Client Sample ID
Lab Sample ID
PIN12-S73B
Client Matrix
280-39873-23
Water
Date Sampled 03112013 1430
Date Received 03132013 0900
8260B Volatile Organic Compounds (GCMS)
Dilution
03192013 1701
03192013 1701
10
8260B
Final WeightVolume
Initial WeightVolume
Lab File ID
Instrument ID
H0965D
20 mL
20 mL
5030B
VMS_H
Analysis Date
Prep Date
Analysis Batch
Prep Batch
280-165434
NA
Analysis Method
Prep Method
Analyte Result (ugL) Qualifier MDL RL
19 U 1019Acetone
016 U 10016Benzene
017 U 10017Bromobenzene
010 U 10010Bromochloromethane
017 U 10017Bromodichloromethane
019 U 10019Bromoform
021 U 10021Bromomethane
20 U 50202-Butanone (MEK)
032 U 10032n-Butylbenzene
017 U 10017sec-Butylbenzene
016 U 10016tert-Butylbenzene
045 U 10045Carbon disulfide
019 U 10019Carbon tetrachloride
017 U 10017Chlorobenzene
017 U 10017Dibromochloromethane
041 U 10041Chloroethane
016 U 10016Chloroform
030 U 10030Chloromethane
017 U 100172-Chlorotoluene
021 U 100214-Chlorotoluene
047 U 1004712-Dibromo-3-Chloropropane
017 U 10017Dibromomethane
015 U 1001512-Dichlorobenzene
013 U 1001313-Dichlorobenzene
016 U 1001614-Dichlorobenzene
031 U 10031Dichlorodifluoromethane
036 J 1002211-Dichloroethane
013 U 1001312-Dichloroethane
14 10015cis-12-Dichloroethene
050 J 10015trans-12-Dichloroethene
023 U 1002311-Dichloroethene
018 U 1001812-Dichloropropane
022 U 1002213-Dichloropropane
018 U 1001822-Dichloropropane
016 U 10016cis-13-Dichloropropene
019 U 10019trans-13-Dichloropropene
019 U 1001911-Dichloropropene
016 U 10016Ethylbenzene
036 U 10036Hexachlorobutadiene
17 U 50172-Hexanone
019 U 10019Isopropylbenzene
020 U 100204-Isopropyltoluene
032 U 10032Methylene Chloride
098 U 500984-Methyl-2-pentanone
022 U 10022Naphthalene
016 U 10016n-Propylbenzene
TestAmerica Denver Page 65 of 1510
Analytical Data
Client SM Stoller Corporation Job Number 280-39873-1
Sdg Number 13025120
Client Sample ID
Lab Sample ID
PIN12-S73B
Client Matrix
280-39873-23
Water
Date Sampled 03112013 1430
Date Received 03132013 0900
8260B Volatile Organic Compounds (GCMS)
Dilution
03192013 1701
03192013 1701
10
8260B
Final WeightVolume
Initial WeightVolume
Lab File ID
Instrument ID
H0965D
20 mL
20 mL
5030B
VMS_H
Analysis Date
Prep Date
Analysis Batch
Prep Batch
280-165434
NA
Analysis Method
Prep Method
Analyte Result (ugL) Qualifier MDL RL
017 U 10017Styrene
021 U 100211112-Tetrachloroethane
021 U 100211122-Tetrachloroethane
020 U 10020Tetrachloroethene
017 U 10017Toluene
021 U 10021123-Trichlorobenzene
021 U 10021124-Trichlorobenzene
016 U 10016111-Trichloroethane
027 U 10027112-Trichloroethane
016 U 10016Trichloroethene
029 U 10029Trichlorofluoromethane
033 U 10033123-Trichloropropane
015 U 10015124-Trimethylbenzene
016 U 10016135-Trimethylbenzene
11 10010Vinyl chloride
019 U 10019Xylenes Total
018 U 1001812-Dibromoethane
Surrogate Rec Acceptance LimitsQualifier
121 70 - 12712-Dichloroethane-d4 (Surr)
95 80 - 125Toluene-d8 (Surr)
98 78 - 1204-Bromofluorobenzene (Surr)
108 77 - 120Dibromofluoromethane (Surr)
TestAmerica Denver Page 66 of 1510
Analytical Data
Client SM Stoller Corporation Job Number 280-39873-1
Sdg Number 13025120
Client Sample ID
Lab Sample ID
PIN12-S73C
Client Matrix
280-39873-24
Water
Date Sampled 03112013 1603
Date Received 03132013 0900
8260B Volatile Organic Compounds (GCMS)
Dilution
03202013 0919
03202013 0919
10
8260B
Final WeightVolume
Initial WeightVolume
Lab File ID
Instrument ID
Z2934D
20 mL
20 mL
5030B
VMS_Z
Analysis Date
Prep Date
Analysis Batch
Prep Batch
280-165627
NA
Analysis Method
Prep Method
Analyte Result (ugL) Qualifier MDL RL
19 U 1019Acetone
016 U 10016Benzene
017 U 10017Bromobenzene
010 U 10010Bromochloromethane
017 U 10017Bromodichloromethane
019 U 10019Bromoform
021 U 10021Bromomethane
20 U 50202-Butanone (MEK)
032 U 10032n-Butylbenzene
017 U 10017sec-Butylbenzene
016 U 10016tert-Butylbenzene
045 U 10045Carbon disulfide
019 U 10019Carbon tetrachloride
017 U 10017Chlorobenzene
017 U 10017Dibromochloromethane
041 U 10041Chloroethane
016 U 10016Chloroform
030 U 10030Chloromethane
017 U 100172-Chlorotoluene
021 U 100214-Chlorotoluene
047 U 1004712-Dibromo-3-Chloropropane
017 U 10017Dibromomethane
015 U 1001512-Dichlorobenzene
013 U 1001313-Dichlorobenzene
016 U 1001614-Dichlorobenzene
031 U 10031Dichlorodifluoromethane
11 1002211-Dichloroethane
013 U 1001312-Dichloroethane
18 10015cis-12-Dichloroethene
17 10015trans-12-Dichloroethene
047 J 1002311-Dichloroethene
018 U 1001812-Dichloropropane
022 U 1002213-Dichloropropane
018 U 1001822-Dichloropropane
016 U 10016cis-13-Dichloropropene
019 U 10019trans-13-Dichloropropene
019 U 1001911-Dichloropropene
016 U 10016Ethylbenzene
036 U 10036Hexachlorobutadiene
17 U 50172-Hexanone
019 U 10019Isopropylbenzene
020 U 100204-Isopropyltoluene
032 U 10032Methylene Chloride
098 U 500984-Methyl-2-pentanone
022 U 10022Naphthalene
016 U 10016n-Propylbenzene
TestAmerica Denver Page 67 of 1510
Analytical Data
Client SM Stoller Corporation Job Number 280-39873-1
Sdg Number 13025120
Client Sample ID
Lab Sample ID
PIN12-S73C
Client Matrix
280-39873-24
Water
Date Sampled 03112013 1603
Date Received 03132013 0900
8260B Volatile Organic Compounds (GCMS)
Dilution
03202013 0919
03202013 0919
10
8260B
Final WeightVolume
Initial WeightVolume
Lab File ID
Instrument ID
Z2934D
20 mL
20 mL
5030B
VMS_Z
Analysis Date
Prep Date
Analysis Batch
Prep Batch
280-165627
NA
Analysis Method
Prep Method
Analyte Result (ugL) Qualifier MDL RL
017 U 10017Styrene
021 U 100211112-Tetrachloroethane
021 U 100211122-Tetrachloroethane
020 U 10020Tetrachloroethene
017 U 10017Toluene
021 U 10021123-Trichlorobenzene
021 U 10021124-Trichlorobenzene
016 U 10016111-Trichloroethane
027 U 10027112-Trichloroethane
016 U 10016Trichloroethene
029 U 10029Trichlorofluoromethane
033 U 10033123-Trichloropropane
015 U 10015124-Trimethylbenzene
016 U 10016135-Trimethylbenzene
019 U 10019Xylenes Total
018 U 1001812-Dibromoethane
Surrogate Rec Acceptance LimitsQualifier
99 70 - 12712-Dichloroethane-d4 (Surr)
91 80 - 125Toluene-d8 (Surr)
92 78 - 1204-Bromofluorobenzene (Surr)
97 77 - 120Dibromofluoromethane (Surr)
TestAmerica Denver Page 68 of 1510
Analytical Data
Client SM Stoller Corporation Job Number 280-39873-1
Sdg Number 13025120
Client Sample ID
Lab Sample ID
PIN12-S73C
Client Matrix
280-39873-24
Water
Date Sampled 03112013 1603
Date Received 03132013 0900
8260B Volatile Organic Compounds (GCMS)
Dilution
03202013 0942
03202013 0942
10
8260B
Final WeightVolume
Initial WeightVolume
Lab File ID
Instrument ID
Z2935D
4 mL
20 mLRun Type DL
5030B
VMS_Z
Analysis Date
Prep Date
Analysis Batch
Prep Batch
280-165627
NA
Analysis Method
Prep Method
Analyte Result (ugL) Qualifier MDL RL
230 50050Vinyl chloride
Surrogate Rec Acceptance LimitsQualifier
94 70 - 12712-Dichloroethane-d4 (Surr)
92 80 - 125Toluene-d8 (Surr)
92 78 - 1204-Bromofluorobenzene (Surr)
95 77 - 120Dibromofluoromethane (Surr)
TestAmerica Denver Page 69 of 1510
Analytical Data
Client SM Stoller Corporation Job Number 280-39873-1
Sdg Number 13025120
Client Sample ID
Lab Sample ID
PIN12-S73D
Client Matrix
280-39873-25
Water
Date Sampled 03112013 1648
Date Received 03132013 0900
8260B Volatile Organic Compounds (GCMS)
Dilution
03192013 1745
03192013 1745
10
8260B
Final WeightVolume
Initial WeightVolume
Lab File ID
Instrument ID
H0967D
20 mL
20 mL
5030B
VMS_H
Analysis Date
Prep Date
Analysis Batch
Prep Batch
280-165434
NA
Analysis Method
Prep Method
Analyte Result (ugL) Qualifier MDL RL
19 U 1019Acetone
016 U 10016Benzene
017 U 10017Bromobenzene
010 U 10010Bromochloromethane
017 U 10017Bromodichloromethane
019 U 10019Bromoform
021 U 10021Bromomethane
20 U 50202-Butanone (MEK)
032 U 10032n-Butylbenzene
017 U 10017sec-Butylbenzene
016 U 10016tert-Butylbenzene
045 U 10045Carbon disulfide
019 U 10019Carbon tetrachloride
017 U 10017Chlorobenzene
017 U 10017Dibromochloromethane
041 U 10041Chloroethane
016 U 10016Chloroform
030 U 10030Chloromethane
017 U 100172-Chlorotoluene
021 U 100214-Chlorotoluene
047 U 1004712-Dibromo-3-Chloropropane
017 U 10017Dibromomethane
015 U 1001512-Dichlorobenzene
013 U 1001313-Dichlorobenzene
016 U 1001614-Dichlorobenzene
031 U 10031Dichlorodifluoromethane
022 U 1002211-Dichloroethane
013 U 1001312-Dichloroethane
021 J 10015cis-12-Dichloroethene
015 U 10015trans-12-Dichloroethene
023 U 1002311-Dichloroethene
018 U 1001812-Dichloropropane
022 U 1002213-Dichloropropane
018 U 1001822-Dichloropropane
016 U 10016cis-13-Dichloropropene
019 U 10019trans-13-Dichloropropene
019 U 1001911-Dichloropropene
016 U 10016Ethylbenzene
036 U 10036Hexachlorobutadiene
17 U 50172-Hexanone
019 U 10019Isopropylbenzene
020 U 100204-Isopropyltoluene
032 U 10032Methylene Chloride
098 U 500984-Methyl-2-pentanone
022 U 10022Naphthalene
016 U 10016n-Propylbenzene
TestAmerica Denver Page 70 of 1510
Analytical Data
Client SM Stoller Corporation Job Number 280-39873-1
Sdg Number 13025120
Client Sample ID
Lab Sample ID
PIN12-S73D
Client Matrix
280-39873-25
Water
Date Sampled 03112013 1648
Date Received 03132013 0900
8260B Volatile Organic Compounds (GCMS)
Dilution
03192013 1745
03192013 1745
10
8260B
Final WeightVolume
Initial WeightVolume
Lab File ID
Instrument ID
H0967D
20 mL
20 mL
5030B
VMS_H
Analysis Date
Prep Date
Analysis Batch
Prep Batch
280-165434
NA
Analysis Method
Prep Method
Analyte Result (ugL) Qualifier MDL RL
017 U 10017Styrene
021 U 100211112-Tetrachloroethane
021 U 100211122-Tetrachloroethane
020 U 10020Tetrachloroethene
017 U 10017Toluene
021 U 10021123-Trichlorobenzene
021 U 10021124-Trichlorobenzene
016 U 10016111-Trichloroethane
027 U 10027112-Trichloroethane
016 U 10016Trichloroethene
029 U 10029Trichlorofluoromethane
033 U 10033123-Trichloropropane
015 U 10015124-Trimethylbenzene
016 U 10016135-Trimethylbenzene
047 J 10010Vinyl chloride
019 U 10019Xylenes Total
018 U 1001812-Dibromoethane
Surrogate Rec Acceptance LimitsQualifier
122 70 - 12712-Dichloroethane-d4 (Surr)
98 80 - 125Toluene-d8 (Surr)
95 78 - 1204-Bromofluorobenzene (Surr)
108 77 - 120Dibromofluoromethane (Surr)
TestAmerica Denver Page 71 of 1510
Analytical Data
Client SM Stoller Corporation Job Number 280-39873-1
Sdg Number 13025120
Client Sample ID
Lab Sample ID
PIN99-2448
Client Matrix
280-39873-26
Water
Date Sampled 03082013 0900
Date Received 03132013 0900
8260B Volatile Organic Compounds (GCMS)
Dilution
03192013 1149
03192013 1149
10
8260B
Final WeightVolume
Initial WeightVolume
Lab File ID
Instrument ID
H0951D
20 mL
20 mL
5030B
VMS_H
Analysis Date
Prep Date
Analysis Batch
Prep Batch
280-165434
NA
Analysis Method
Prep Method
Analyte Result (ugL) Qualifier MDL RL
19 U 1019Acetone
016 U 10016Benzene
017 U 10017Bromobenzene
010 U 10010Bromochloromethane
017 U 10017Bromodichloromethane
019 U 10019Bromoform
021 U 10021Bromomethane
20 U 50202-Butanone (MEK)
032 U 10032n-Butylbenzene
017 U 10017sec-Butylbenzene
016 U 10016tert-Butylbenzene
045 U 10045Carbon disulfide
019 U 10019Carbon tetrachloride
017 U 10017Chlorobenzene
017 U 10017Dibromochloromethane
041 U 10041Chloroethane
016 U 10016Chloroform
030 U 10030Chloromethane
017 U 100172-Chlorotoluene
021 U 100214-Chlorotoluene
047 U 1004712-Dibromo-3-Chloropropane
017 U 10017Dibromomethane
015 U 1001512-Dichlorobenzene
013 U 1001313-Dichlorobenzene
016 U 1001614-Dichlorobenzene
031 U 10031Dichlorodifluoromethane
022 U 1002211-Dichloroethane
013 U 1001312-Dichloroethane
015 U 10015cis-12-Dichloroethene
015 U 10015trans-12-Dichloroethene
023 U 1002311-Dichloroethene
018 U 1001812-Dichloropropane
022 U 1002213-Dichloropropane
018 U 1001822-Dichloropropane
016 U 10016cis-13-Dichloropropene
019 U 10019trans-13-Dichloropropene
019 U 1001911-Dichloropropene
016 U 10016Ethylbenzene
036 U 10036Hexachlorobutadiene
17 U 50172-Hexanone
019 U 10019Isopropylbenzene
020 U 100204-Isopropyltoluene
032 U 10032Methylene Chloride
098 U 500984-Methyl-2-pentanone
022 U 10022Naphthalene
016 U 10016n-Propylbenzene
TestAmerica Denver Page 72 of 1510
Analytical Data
Client SM Stoller Corporation Job Number 280-39873-1
Sdg Number 13025120
Client Sample ID
Lab Sample ID
PIN99-2448
Client Matrix
280-39873-26
Water
Date Sampled 03082013 0900
Date Received 03132013 0900
8260B Volatile Organic Compounds (GCMS)
Dilution
03192013 1149
03192013 1149
10
8260B
Final WeightVolume
Initial WeightVolume
Lab File ID
Instrument ID
H0951D
20 mL
20 mL
5030B
VMS_H
Analysis Date
Prep Date
Analysis Batch
Prep Batch
280-165434
NA
Analysis Method
Prep Method
Analyte Result (ugL) Qualifier MDL RL
017 U 10017Styrene
021 U 100211112-Tetrachloroethane
021 U 100211122-Tetrachloroethane
020 U 10020Tetrachloroethene
017 U 10017Toluene
021 U 10021123-Trichlorobenzene
021 U 10021124-Trichlorobenzene
016 U 10016111-Trichloroethane
027 U 10027112-Trichloroethane
016 U 10016Trichloroethene
029 U 10029Trichlorofluoromethane
033 U 10033123-Trichloropropane
015 U 10015124-Trimethylbenzene
016 U 10016135-Trimethylbenzene
010 U 10010Vinyl chloride
019 U 10019Xylenes Total
018 U 1001812-Dibromoethane
Surrogate Rec Acceptance LimitsQualifier
125 70 - 12712-Dichloroethane-d4 (Surr)
102 80 - 125Toluene-d8 (Surr)
102 78 - 1204-Bromofluorobenzene (Surr)
112 77 - 120Dibromofluoromethane (Surr)
TestAmerica Denver Page 73 of 1510
Analytical Data
Client SM Stoller Corporation Job Number 280-39873-1
Sdg Number 13025120
Client Sample ID
Lab Sample ID
PIN12-0524
Client Matrix
280-39873-1
Water
Date Sampled 03092013 0748
Date Received 03132013 0900
8260B SIM Volatile Organic Compounds (GCMS-SIM)
Dilution
03222013 2012
03222013 2012
10
8260B SIM
Final WeightVolume
Initial WeightVolume
Lab File ID
Instrument ID
E4018D
5 mL
20 mL
5030B
VMS_E
Analysis Date
Prep Date
Analysis Batch
Prep Batch
280-166279
NA
Analysis Method
Prep Method
Analyte Result (ugL) Qualifier MDL RL
088 U 4008814-Dioxane
Surrogate Rec Acceptance LimitsQualifier
93 70 - 12712-Dichloroethane-d4 (Surr)
TestAmerica Denver Page 74 of 1510
Analytical Data
Client SM Stoller Corporation Job Number 280-39873-1
Sdg Number 13025120
Client Sample ID
Lab Sample ID
PIN12-0525
Client Matrix
280-39873-2
Water
Date Sampled 03092013 0826
Date Received 03132013 0900
8260B SIM Volatile Organic Compounds (GCMS-SIM)
Dilution
03152013 1934
03152013 1934
10
8260B SIM
Final WeightVolume
Initial WeightVolume
Lab File ID
Instrument ID
E3823D
10 mL
20 mL
5030B
VMS_E
Analysis Date
Prep Date
Analysis Batch
Prep Batch
280-165111
NA
Analysis Method
Prep Method
Analyte Result (ugL) Qualifier MDL RL
044 U 2004414-Dioxane
Surrogate Rec Acceptance LimitsQualifier
99 70 - 12712-Dichloroethane-d4 (Surr)
TestAmerica Denver Page 75 of 1510
Analytical Data
Client SM Stoller Corporation Job Number 280-39873-1
Sdg Number 13025120
Client Sample ID
Lab Sample ID
PIN12-0539
Client Matrix
280-39873-3
Water
Date Sampled 03082013 1635
Date Received 03132013 0900
8260B SIM Volatile Organic Compounds (GCMS-SIM)
Dilution
03152013 0029
03152013 0029
10
8260B SIM
Final WeightVolume
Initial WeightVolume
Lab File ID
Instrument ID
E3785D
5 mL
20 mL
5030B
VMS_E
Analysis Date
Prep Date
Analysis Batch
Prep Batch
280-164929
NA
Analysis Method
Prep Method
Analyte Result (ugL) Qualifier MDL RL
38 4008814-Dioxane
Surrogate Rec Acceptance LimitsQualifier
98 70 - 12712-Dichloroethane-d4 (Surr)
TestAmerica Denver Page 76 of 1510
Analytical Data
Client SM Stoller Corporation Job Number 280-39873-1
Sdg Number 13025120
Client Sample ID
Lab Sample ID
PIN12-0540
Client Matrix
280-39873-4
Water
Date Sampled 03082013 1548
Date Received 03132013 0900
8260B SIM Volatile Organic Compounds (GCMS-SIM)
Dilution
03152013 0046
03152013 0046
10
8260B SIM
Final WeightVolume
Initial WeightVolume
Lab File ID
Instrument ID
E3786D
1 mL
20 mL
5030B
VMS_E
Analysis Date
Prep Date
Analysis Batch
Prep Batch
280-164929
NA
Analysis Method
Prep Method
Analyte Result (ugL) Qualifier MDL RL
170 204414-Dioxane
Surrogate Rec Acceptance LimitsQualifier
100 70 - 12712-Dichloroethane-d4 (Surr)
TestAmerica Denver Page 77 of 1510
Analytical Data
Client SM Stoller Corporation Job Number 280-39873-1
Sdg Number 13025120
Client Sample ID
Lab Sample ID
PIN12-0541
Client Matrix
280-39873-5
Water
Date Sampled 03082013 1241
Date Received 03132013 0900
8260B SIM Volatile Organic Compounds (GCMS-SIM)
Dilution
03142013 0030
03142013 0030
10
8260B SIM
Final WeightVolume
Initial WeightVolume
Lab File ID
Instrument ID
E3753D
20 mL
20 mL
5030B
VMS_E
Analysis Date
Prep Date
Analysis Batch
Prep Batch
280-164670
NA
Analysis Method
Prep Method
Analyte Result (ugL) Qualifier MDL RL
022 U 1002214-Dioxane
Surrogate Rec Acceptance LimitsQualifier
108 70 - 12712-Dichloroethane-d4 (Surr)
TestAmerica Denver Page 78 of 1510
Analytical Data
Client SM Stoller Corporation Job Number 280-39873-1
Sdg Number 13025120
Client Sample ID
Lab Sample ID
PIN12-0542
Client Matrix
280-39873-6
Water
Date Sampled 03082013 1310
Date Received 03132013 0900
8260B SIM Volatile Organic Compounds (GCMS-SIM)
Dilution
03152013 0139
03152013 0139
10
8260B SIM
Final WeightVolume
Initial WeightVolume
Lab File ID
Instrument ID
E3789D
10 mL
20 mL
5030B
VMS_E
Analysis Date
Prep Date
Analysis Batch
Prep Batch
280-164929
NA
Analysis Method
Prep Method
Analyte Result (ugL) Qualifier MDL RL
044 U 2004414-Dioxane
Surrogate Rec Acceptance LimitsQualifier
103 70 - 12712-Dichloroethane-d4 (Surr)
TestAmerica Denver Page 79 of 1510
Analytical Data
Client SM Stoller Corporation Job Number 280-39873-1
Sdg Number 13025120
Client Sample ID
Lab Sample ID
PIN12-0549
Client Matrix
280-39873-7
Water
Date Sampled 03082013 1413
Date Received 03132013 0900
8260B SIM Volatile Organic Compounds (GCMS-SIM)
Dilution
03152013 0156
03152013 0156
10
8260B SIM
Final WeightVolume
Initial WeightVolume
Lab File ID
Instrument ID
E3790D
10 mL
20 mL
5030B
VMS_E
Analysis Date
Prep Date
Analysis Batch
Prep Batch
280-164929
NA
Analysis Method
Prep Method
Analyte Result (ugL) Qualifier MDL RL
044 U 2004414-Dioxane
Surrogate Rec Acceptance LimitsQualifier
108 70 - 12712-Dichloroethane-d4 (Surr)
TestAmerica Denver Page 80 of 1510
Analytical Data
Client SM Stoller Corporation Job Number 280-39873-1
Sdg Number 13025120
Client Sample ID
Lab Sample ID
PIN12-0554A
Client Matrix
280-39873-8
Water
Date Sampled 03082013 0919
Date Received 03132013 0900
8260B SIM Volatile Organic Compounds (GCMS-SIM)
Dilution
03142013 0122
03142013 0122
10
8260B SIM
Final WeightVolume
Initial WeightVolume
Lab File ID
Instrument ID
E3756D
20 mL
20 mL
5030B
VMS_E
Analysis Date
Prep Date
Analysis Batch
Prep Batch
280-164670
NA
Analysis Method
Prep Method
Analyte Result (ugL) Qualifier MDL RL
022 U 1002214-Dioxane
Surrogate Rec Acceptance LimitsQualifier
114 70 - 12712-Dichloroethane-d4 (Surr)
TestAmerica Denver Page 81 of 1510
Analytical Data
Client SM Stoller Corporation Job Number 280-39873-1
Sdg Number 13025120
Client Sample ID
Lab Sample ID
PIN12-0554B
Client Matrix
280-39873-9
Water
Date Sampled 03082013 1005
Date Received 03132013 0900
8260B SIM Volatile Organic Compounds (GCMS-SIM)
Dilution
03152013 0214
03152013 0214
10
8260B SIM
Final WeightVolume
Initial WeightVolume
Lab File ID
Instrument ID
E3791D
10 mL
20 mL
5030B
VMS_E
Analysis Date
Prep Date
Analysis Batch
Prep Batch
280-164929
NA
Analysis Method
Prep Method
Analyte Result (ugL) Qualifier MDL RL
044 U 2004414-Dioxane
Surrogate Rec Acceptance LimitsQualifier
102 70 - 12712-Dichloroethane-d4 (Surr)
TestAmerica Denver Page 82 of 1510
Analytical Data
Client SM Stoller Corporation Job Number 280-39873-1
Sdg Number 13025120
Client Sample ID
Lab Sample ID
PIN12-0554C
Client Matrix
280-39873-10
Water
Date Sampled 03082013 1110
Date Received 03132013 0900
8260B SIM Volatile Organic Compounds (GCMS-SIM)
Dilution
03152013 0231
03152013 0231
10
8260B SIM
Final WeightVolume
Initial WeightVolume
Lab File ID
Instrument ID
E3792D
4 mL
20 mL
5030B
VMS_E
Analysis Date
Prep Date
Analysis Batch
Prep Batch
280-164929
NA
Analysis Method
Prep Method
Analyte Result (ugL) Qualifier MDL RL
76 501114-Dioxane
Surrogate Rec Acceptance LimitsQualifier
100 70 - 12712-Dichloroethane-d4 (Surr)
TestAmerica Denver Page 83 of 1510
Analytical Data
Client SM Stoller Corporation Job Number 280-39873-1
Sdg Number 13025120
Client Sample ID
Lab Sample ID
PIN12-0581-1
Client Matrix
280-39873-11
Water
Date Sampled 03112013 0851
Date Received 03132013 0900
8260B SIM Volatile Organic Compounds (GCMS-SIM)
Dilution
03152013 2028
03152013 2028
10
8260B SIM
Final WeightVolume
Initial WeightVolume
Lab File ID
Instrument ID
E3826D
10 mL
20 mL
5030B
VMS_E
Analysis Date
Prep Date
Analysis Batch
Prep Batch
280-165111
NA
Analysis Method
Prep Method
Analyte Result (ugL) Qualifier MDL RL
044 U 2004414-Dioxane
Surrogate Rec Acceptance LimitsQualifier
132 70 - 127X12-Dichloroethane-d4 (Surr)
TestAmerica Denver Page 84 of 1510
Analytical Data
Client SM Stoller Corporation Job Number 280-39873-1
Sdg Number 13025120
Client Sample ID
Lab Sample ID
PIN12-0581-2
Client Matrix
280-39873-12
Water
Date Sampled 03112013 0923
Date Received 03132013 0900
8260B SIM Volatile Organic Compounds (GCMS-SIM)
Dilution
03152013 2323
03152013 2323
10
8260B SIM
Final WeightVolume
Initial WeightVolume
Lab File ID
Instrument ID
E3827D
10 mL
20 mL
5030B
VMS_E
Analysis Date
Prep Date
Analysis Batch
Prep Batch
280-165111
NA
Analysis Method
Prep Method
Analyte Result (ugL) Qualifier MDL RL
044 U 2004414-Dioxane
Surrogate Rec Acceptance LimitsQualifier
134 70 - 127X12-Dichloroethane-d4 (Surr)
TestAmerica Denver Page 85 of 1510