short-term measures proposal, newell street site · company (ge) and the massachusetts department...

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CONTENTS

INTRODUCTION . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . 1

STM FOR QUALITY PRINTING PROPERTY ........................ . 2

STM FOR MARCHETTO PROPERTY ............................. . 4

Soil Quality . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . 4

Proposed Actions . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . 5

SCHEDULE . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . 7

REFERENCES . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . 8

FIGURES

A. Proposed Short-Term Measures, Newell Street Marchetta Property, December 1990.

B. Replication Soil Sampling Location East Street Area 2 Southeast Corner of Property.

APPENDICES

A. Results of the October/November 1990 Surficial Soil Sampling Program Marchetta Property, Newell Street, Pittsfield, Massachusetts.

SHORT TERM MEASURES PROPOSAL NEWELL STREET SITE

PITTSFIELD, MASSACHUSETTS

INTRODUCTION

In accordance with Paragraph 6.1 of Administrative Consent Order

(ACO) No. SA 1-0147 and 1-0151 entered into by General Electric

Company (GE) and the Massachusetts Department of Environmental

Protection (DEP). Geraghty & Miller, Inc. has developed this

proposal for short-term measures (STMs} at the Newell Street

site in Pittsfield, Massachusetts. While GE does not believe

that existing conditions at Newell Street constitute an

"imminent hazard" to human health or the environmental within

the meaning of the Massachusetts Contingency Plan {MCP) , this .. proposal is being submitted for DEP review and approval pursuant

to the above-referenced order.

After reviewing the June 1990 Supplemental Phase II Scope of

Work (SOW) for the Newell Street site, prepared on behalf of GE

by Blasland and Bouck Engineers of Syracuse, New York, the DEP

submitted a conditional letter of approval to GE, dated August

14, 1990. One of the conditions of that letter was to submit an

STM proposal to address PCBs ~n surfic l soil through removal

or treatment at the Anthony Marchetta Contractors' property and

at a former printing facility, Quality Printing, located 500

feet west of the Marchetta property. GE responded to this

letter on September

would not necessari

surficial soil but

institutional

letter of

indicated that the

treatment of

12, 1990 and

provide

might propose

DEP

l 1 .J.. t

STM

al 1

indicated that the STM proposal

removal or treatment of the

need not

the STMs

such as

GE another

24, 1990, wh

removal or

the

2

elimination of hazards posed by surficial contamination.

Hydrogeologic studies, including surficial soil investigations,

began in 1987 at the Newell Street site. These studies have

shown the presence of elevated PCB concentrations in the

surficial soils of two properties, the Quality Printing and

Marchetta properties. The DEP has concluded that these

concentrations constitute an "imminent hazard" and require

implementation of STMs under the MCP (310 CMR 40.542) to abate

such hazard. While, as noted above, GE does not agree with the

DEP's conclusion as to the existence of an "imminent hazard,"

this proposal is being submitted for the implementation of STMs

to address the DEP's immediate concerns. As such, this proposal

is intended to comply with the MCP requirements for STMs. It is

not intended to represent final remedial action for these

portions of the Newell Street site. The ultimate cleanup level

for soils at this site and the ultimate remedial actions (if

any) will be considered and determined in connection with the

performance of activities in Phase II and Phase III of the MCP

process in accordance with Article VIII of the above-referenced

consent order.

STM FOR QUALITY PRINTING PROPERTY

GE purchased the Quality Printing property in November 1984.

Activity no longer occurs at this location the area of the

elevated PCB concentrations. A portion of the lity Printing

property which rema

of the site total

in use has been paved

fenced with warning s

completely restricted. In these c

for property will cons of institut

the remainder

Access

the proposed STM

controls.

3

Specifically, GE will maintain the fence and warning signs and

will monitor the site to ensure that the access continues to be

totally restricted.

These institutional controls should adequately protect against

any short-term hazards posed by PCBs in the surficial soils

during the interim period prior to the evaluation and

determination of final remedial action. They will do so by

preventing any direct contact of individuals with such soils.

Thus, the only potential risks are via inhalation of volatilized

PCBs or exposure to windblown fugitive dust from such soils.

A preliminary risk assessment prepared for the Newell Street

site by Geraghty & Miller, Inc. in 1989 specifically addressed

the risk from PCBs in the surficial soil at the Quality Printing

property. It is recognized that a new risk assessment for the

Newell Street site must be performed as part of the Phase II

activities, as provided in GE's supplemental Phase II Scope of

Work for the Newell Street site. Nevertheless, the preliminary

risk assessment is useful for STM purposes in that it provides

data indicating that the lifetime risk from PCBs associated with

exposure to fugitive dust from surficial soil is insignificant

(estimated to be 1.4 x 10-8 even using a potency factor of

7.7). Although this risk assessment did not address the

potential risk for volatilized PCBs, it seems clear due to

climatic conditions in the area and the inherent low

volatility of PCBs to air, that the overall risk due to

inhalation of volatilized PCBs would s be very low.

Thus, based on current ion, it appears that the overall

site risk would be less than 1 x 10-6 . demonstrates that

proposed STM 11 be suff to

concerns regarding environmental hazards associated

surficial PCB contamination on the site.

iate

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STM FOR ~~RCHETTO PROPERTY

Surficial soil sampling programs have been carried out at the

Marchetta property on several occasions as part of the Newell

Street site investigation. The 1988 and 1989 sampling events

showed elevated levels of PCBs in the surficial soil at

locations M0-3, M0-45, M0-5, M0-6, and M0-7. In order to

determine the areal extent of surficial soil with a PCB content

grater than 22 parts per million (ppm), additional sampling

programs were conducted on October 5 and 23, and November 15,

1990. The results of this sampling are presented in the

attached Appendix, entitled "Results of the October/November

Street soil Sampling Program Marchetta Property, Newell Street,

Pittsfield, Massachusetts." The sampling locations are shown on

Figures 1, 2, and 3 of that report. A summary of the

Photoionization Detector (PID) results for surficial soil

samples collected in october/November 1990 are presented in

Table 1 of the report. PCB analytical results for the May 1988,

March 1989, and October 5 and 23, and November 15, 1990 samples

are presented in Table 2 of the report. Surficial soil sampling

locations exceeding 22 ppm are shown in Figure 4 of the report.

For purposes of is STM

as concentrations

of soil.

PCB concentrat

excess of 22 the

are

four

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In accordance with the requirements for STMs {310 CMR 40.542)

proposed for the Marchetta Property, the objective of the STM

to prevent direct contact with surficial soil which contains

PCBs above 22 ppm. Three areas have been identified that

require STMs: (1) the area in the northern portion of the

property containing sampling locations M0-5, M0-6, and M0-7;

(2) the area extending from around M0-4 to the stormwater

drainage ditch on the eastern side of the property; and (3) the

area around M0-3. These areas are shown on Figure A. The

proposed STMs for these areas are as follows (subject to

obtaining permission from the property owner) :

1. A fence posted with proper warnings allowing no access

will be installed as shown in Figure A to prevent access

to the northern portion of the Marchetta property.

Additional surficial samples will be collected in the

stormwater drainage ditch south of sample DD-S to define

the southern extent of PCB contamination greater than 22

ppm in the ditch and the fence will be extended to

enclose the area. The fence will connect with the

existing fence on the eastern boundary of the property.

By installing this fence and restricting access to the

drainage ditch and northern portion of the property, the

only potential for this area is through

inhalation. Since the average concentrations PCBs in

that on

risk

Qual

soil on the Marchetta property is less than

Printing property, potential

would be even than on

7

SCHEDULE

1 Upon receiving DEP approval of the proposed STMs for the Marchetto property, GE will

contact the Massachusetts Conservation Department (MCD) to obtain approval to conduct the

proposed actions. The STMs proposed for the Marchetto property will be implemented within

60 days of receiving MCD approval, with the proviso that grading and paving can only be

conducted during appropriate weather conditions.

Sincerely,

GERAGHTY & MILLER, INC.

~~d.~_, flvZc?-7-7 W1lham J. Gray / !

Project Scientist

l b~-v~~-Dennis Colton Senior Project Advisor

DC:WJG/smh

) GERAGHTY !Y1ILLEK INC

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- -- _.-.... - _ ....... - .......---- - _..._. - -LASORATDR1EB. INC.

Laboratory Report

cuENT BLASLAND & BOUCK ENGINEERS. P.C. ~BNO. 2887.026.517

OESCRIPTION _,s.st St. Area II ·Soil Sampling Pittsfieldt MUS. B&B Job No. 101.75.12

MATRIX: Soil

Date Analyzed: 10-9-90 OAT! COLLECTED 10-8-90 DATE RI!CEtVEO 10-9-90

EA-512-Cl

EA-ST2-C2

EA-ST2-C3

EA-ST2-C4

EA-ST:Z-CS

EA-ST2-C6

EA-ST2-C7

EA-ST2-C8

1 Sample t

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L1177

Lll78

Ll179

1.1180

L118l

Lll82

Lll83

Lll84

OSG laboralonll!. inc, sn O'Brien & Gere 1.1miled Company 5000 Brittonfie!d Parkway I Suite 300, Box 4!142/ Syracus&. NY 132211 (3i5) 4.37·0200

PCB

<0.6

Unlb:

Date:

PERCENT TOTAL SOLIDS

92.

94.

94.

89. 95.

95.

91.

92.

NY034

mgjkg dry wgt.

October 24, 19Jw.

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REFERENCES

Geraghty & Miller, Inc. May 1989. Risk Assessment for the Newell Street Site, Pittsfield, Massachusetts.

GERAGHTY MILLER, INC

M0-4

• •

EXPLANATION

PREVIOUS SOIL SAMPLE LOCATION AND DESIGNATION M0-3,4 It 5 MAY,1988 MQ..&, 7, 8, 9, 10 AND 11 MARCH, 1989

SOIL SAMPLE LOCATION

IIi

I V/04 PROPOSED PAVEMENT

PROPOSED FENCE LINE

ANTHONY MARCHETTO

CONTRACTORS

SHOWN 0~----------------~ • ~ .GERAGHTY !! lfr & MU.I.ER, INC. ~ 41 ~~ s..,.,..

U0-8.&

A M0-9

SPEED SHOP

A M0-10

SCALE 0 50

FEET

PROPOSED SHORT TERM MEASURES, NEWELL STREET MARCHETTO PROPERTY

Pittsfield, Massachusetts

DD-N

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FIGURE

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GENERAL ELECTRIC COMPANY PITTSFIELD MASSACHUSETTS

EAST STREET AREA 2

FIGURE

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CONTENTS

INTRODUCTION . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . 1

SAMPLINGMETHODOLOGY .................................. . 2

ANALYTICAL RESULTS ..................................... . 3

TABLES

1. Summary of Photoionization Detector Results for Soil Samples Collected at the Marchetto Property, Newell Street, October 5 and 23, and November 15, 1990, Pittsfield, Massachusetts.

2.

3.

1.

Summary of PCB Concentrations in Surficial Soil, Marchetto Property, Newell Street, Pittsfield, Massachusetts.

Sample Collection Report for Marchetto Property, Newell Street, Pittsfield, Massachusetts.

FIGURES

Surficial Soil Sampling Locations, Marchetto Property, Newell Street, October 5 and 23, 1990, Pittsfield, Massachusetts.

2. Surficial Soil Sampling Locations Adjacent to M0-4, M0-5, M0-6, and M0-7, October 5 and 23, 1990, Marchetto Property, Newell Street, Pittsfield, Massachusetts.

3.

4.

Surficial Soil Sampling Locations Adjacent to M0-3, October 5 and 23, 1990, Marchetto Property, Newell Street, Pittsfield, Massachusetts.

Surficial Soil Locations with PCB Concentrations > 22 ppm, October 5, 1990, Marchetto Property, Newell Street, Pittsfield, Massachusetts.

APPEl'!TUICES

A. Geologic Logs

B. Analytical Laboratory Reports.

GERAGHTY MILLER.INC.

RFSULTS OF TilE OCTOBER/NOVE.\ffiER 1990 SURFICIAL SOIL SMIPLING PROGRAM-MARCHETTO PROPERTY

NEWELL STREET, PITTSFIELD, MASSACHUSETTS

INTRODUCTION

The General Electric Company (GE) and the Massachusetts Department of Environmental

Protection (DEP) have entered into an Administrative Consent Order on May 10, 1990 pursuant

to the Massachusetts Contingency Plan (MCP) for the investigation of contamination on the

Newell Street properties in Pittsfield, Massachusetts. Section 6.1 of this order contains a

provision for the implementation of Short-Term Measures (STMs) should they be required.

Geraghty & Miller, Inc. conducted a supplemental surficial soil sampling program on one

of the Newell Street properties (Marchetto Property) during October/November 1990 on behalf

of GE Company in Pittsfield, Massachusetts. The objective of the program was to collect

additional data at the Marchetto site pertaining to surficial soil quality for the determination of

a STM as required by the DEP in their letter dated August 24, 1990.

During this program surficial soil samples were collected at 55 locations on the Marchetto

property (Figure 1). In addition, two soil samples were collected from each soil stockpile (Soil

No. 1 and Soil Pile No. identit1ed on Figure 2. sampling methodology

analytical results are presented herein.

GERAGHTY MILLER.

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SAIVIPLING 1\IETHODOLOGY

The October/November 1990 surficial soil sampling program included the collection of

surficial soil samples in a radial pattern around locations M0-3, M0-4, M0-5, M0-6 and M0-

7, previously identified as containing PCBs at concentrations greater than 22 milligrams per

kilogram (mg/kg) or parts per million (ppm) (Figure 1). The samples were collected in the

north, south, east, and west directions away from each of these five locations at 5-foot

increments to 15 feet to determine the areal extent of PCB concentrations in surficial soil greater

than 22 mg/kg. The sampling locations are shown in Figures 2 and 3. Two duplicate samples

(DP-1 and DP-2) were collected from locations M0-4W3 and M0-5Wl, respectively. In

addition, two surficial soil samples were collected from a drainage ditch which is located along

the eastern property line of the Marchetto property (DD-N and DD-S). These sample locations

are shown in Figure 2.

Each sample was obtained by compositing the surficial soil from a one-foot by one-foot

by four-inch deep area. All samples were field screened for volatile organic compounds (VOCs)

using a photoionization detector (PID). The background level for VOCs at this site was

determined to be zero. Samples M0-4Nl, M0-6Wl and M0-7N3 produced PID readings of

10.3, 2.2 and 8.1 respectively (Table 1). These samples were submitted for VOC analysis

(EPA Method 8240) as required by the DEP. Soil sampling equipment was Otx:onl:am

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a laboratory-grade detergent solution and rinsed with distilled water between each location to

prevent cross-contamination of samples. The decontamination water was containerized and

transported to GE for proper disposal.

Surficial soils within the sampling area consist of a silty sand matrix with small amounts

of gravel. The nature of the soil samples are described in the soil description presented in

Appendix A.

ANALYTICAL RESULTS

The results of the surficial soil sampling program conducted on the Marchetta property

indicate that PCBs were found at concentrations above 22 mg/kg in 18 of the 41 new sampling

locations analyzed (Table 2). The laboratory was instructed to analyze the samples for PCBs

(EPA Method 8080) in sequence, at progressively farther distances away from locations M0-3,

M0-4, M0-5, M0-6 and M0-7 until a result of less than 22 mg/kg was detected (Figures

2 and 3). Therefore, the PCB data in Table 2 does not include all sampling locations identified

on Figures 2 and 3, because these figures include all sampling locations whether the soil was

analyzed or not. Based on these results, small areas adjacent to locations M0-3, M0-4, M0-6,

and M0-7 have been identified to contain PCBs greater than 22 mg/kg, as shown on Figure 4.

The soil pile samples showed PCB concentrations well below 22 mg/kg. However, DD-

and DD-S, located within the property drainage ditch, contained PCB concentrations of 91

mg/kg and 83 mg/kg, respectively. Volatile organic analyses (EPA Method 8240) were

GERAGHTY MILLER. I~C

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performed on samples M0-4Nl, M0-6Wl and M0-7N3 due to PID readings above background.

Methylene chloride, a common laboratory artifact, was detected at low concentrations in all three

samples. Toluene was detected in samples M0-4Nl and M0-7N3 at 80 micrograms per

kilogram (ug/kg) or parts per billion (ppb) and 39 ug/kg, respectively. No other volatile organic

compounds were reported above the method detection limits. A sample collection repon

describing all pertinent sampling information is presented in Table 3. Laboratory data for all

PCB and VOC results are presented in Appendix B.

If you have any questions or comments regarding the sampling program, please do not

hesitate to contact us.

Respectfully submitted,

GERAGHTY & .MILLER, INC.

w!~/ Project Scientist

b~~~ Dennis Colton Senior Project Advisor

DC:WJG/smh

GERAGHTY VHLLFR.

Table 1.

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Summary of Photoionization Detector (PID) Results for Soil Samples Collected at the Marchetto Property, Newell Street, October 5 and 23, and November 15, 1990, Pittsfield, .Massachusetts.

Depth (Inches) and Correlating Sample Designation PID Results (ppm)"

(0-4)

M0-3Nl 0.0 M0-3N2 0.0 M0-3N3 0.0 M0-3N4 0.0 M0-3Sl 0.0 M0-3S2 0.0

M0-3S3 0.0 M0-3El 0.0 M0-3E2 0.0 M0-3E3 0.0 M0-3Wl 0.0 M0-3W2 0.0

M0-4Nl 10.3 ,....

M0-4N2 0.0 M0-4N3 0.0 M0-4Sl 0.0 M0-4S2 0.0 M0-4S3 0.0

M0-4El 0.0 M0-4E2 0.0 M0-4E3 0.0 M0-4E4 0.0 M0-4Wl 0.0 M0-4W2 0.0 M0-4W3(l)P·!) 0.0

These results are qualitative only and do not represent the absolute of any volatile compound soil whether the compound is natural or man-made.

GERAGHTY MILLER,

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Table 1.

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Summary of Photoionization Detector (PID) Results for Soil Samples Collected at the Marchetta Property, Newell Street, October 5 and 23, and November 15, 1990, Pittsfield, .Massachusetts.

Sample Designation

M0-5Nl M0-5N2 M0-5Sl M0-5S2 M0-5S3 M0-5El M0-5Wl (DP-2)

M0-5W2

M0-6Nl M0-6N2 M0-6N3 M0-6Sl M0-6El

M0-6E2 M0-6E3 M0-6Wl M0-6W2

M0-7Nl M0-7N2 M0-7N3 M0-7S1 M0-7S2 M0-7S3

Depth (Inches) and Correlating PID Results (ppmt

(0-4)

0.0 0.0 0.0 0.0 0.0 0.0 0.0 0.0

0.0 0.0 0.0 0.0 0.0

0.0 0.0 2.2 ~

0.0

0.0 0.0 8.1 -0.0 0.0 0.0

a> These are qualitative and do not the any volatile organic compound in the man-made.

GERAGHTY MILLER.!

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Table 1. Summary of Photoionization Detector (PID) Results for Soil Samples Collected at the Marchetto Property, Newell Street, October 5 and 23, and November 15, 1990, Pittsfield, Massachusetts.

Soil Pile No. 1

Soil Pile No.2

Sample Designation

M0-7El M0-7E2 M0-7E3 M0-7Wl M0-7W2

DD-N DD-S

SP-1 (N&W) SP-2 (E&S)

SP-3 (N&W) SP-4 (E&S)

a) These are qualitative only any volatile organic compound man-made.

Depth (Inches) and Correlating PID Results (ppmt

do not the core, whether

(0-4)

0.0 0.0 0.0 0.0 0.0

0.0 0.0

0.0 0.0

0.0 0.0

absolute concentrations compound is or

GERAGHTY \HLLER,

Table 2.

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Summary of PCB Concentrations in Surficial Soil, Marchetto Property, Newell Street, Pittsfield, Massachusetts

Sampling Location No.

M0-3 M0-4 M0-5

M0-6 M0-7 M0-8 M0-9 M0-10 MO-ll

M0-3N1 M0-3N2 M0-3N3 M0-3N4 M0-3S1 M0-3E1 M0-3W1 M0-3W2

M0-4N1 M0-4S1 M0-4E1 M0-4E2 M0-4E3 M0-4E4 M0-4Wl

Date Collected

5-10-88 5-10-88 5-10-88

3-16-89 3-16-89 3-16-89 3-16-89 3-16-89 3-16-89

10-5-90 10-5-90 10-5-90 11-15-90 10-5-90 10-5-90 10-23-90 10-23-90

10-5-90 10-5-90 10-5-90 10-5-90 10-5-90 11-15-90 10-5-90

GERAGHTY MlLLER, INC

Total PCBs (mg/kg)

91 23 65

44 27

3.6 14 7.4

12

42.3 22.8 19.4 0.93 7.3

12.1 16.6 0.11

14.4 5.2

39.2 80.5

145.2 52.1

3.7

Table 2.

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Soil Pile No. 1

Soil Pile No. 2

Page 2 of 2

Summary of PCB Concentrations in Surficial Soil, l\1archetto Property, Newell Street, Pittsfield, Massachusetts

Sampling Location No.

M0-5Nl M0-5N2 M0-5Sl MO-SEl M0-5Wl

Date Collected

10-5-90 10-5-90 10-5-90 10-23-90 10-5-90

DP-2 ""o 5 ~ l 10-5-90

M0-6N1 10-5-90 M0-6N2 10-5-90 M0-6N3 10-23-90 M0-6S1 10-5-90 M0-6E1 10-5-90 M0-6E2 10-5-90 M0-6E3 10-5-90 M0-6W1 10-5-90 M0-6W2 10-5-90

M0-7Nl 10-5-90 M0-7N2 10-5-90 M0-7N3 10-5-90 M0-7S1 10-5-90 M0-7E1 10-5-90 M0-7W1 10-5-90 DD-N 11-15-90 DD-S 11-15-90

SP-l(N&W) 11-15-90 SP-2(E&S) 11-15-90

SP-3(N&W) 11-15-90 SP-4(E&S) 11-15-90

GERAGHTY MILLER. INC

Total PCBs (mg/kg)

7.4 42.6

3.1 3.4

13.4 20.0

43.5 56.2

207.7 27 32.2 47.3 19.4 65.6 19.2

96 27.7 14.8 10.7 15.6 18.7 91 83

3.3 5.7

0.4 0.56

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Table 3. Sample Collection Report for Newell Street Marchetto Property, Pittsfield, Massachusetts

Field Laboratory Sample Sample Sampling Sampling Sample Field Sample Samplers Sample ID Sample ID Matrix Date Container Filtration Preservation Initials

M0-3Nl 901008A 46 PCBs (EPA 8080) Soil 10-5-90 Hand-trowel 250 ml glass N/A Cool, 4°C ATL M0-3N2 901008A 47 PCBs (EPA 8080) Soil 10-5-90 Hand-trowel 250 ml glass N/A Cool, 4°C ATL M0-3N3 901008A 48 PCBs (EPA 8080) Soil 10-5-90 Hand-trowel 250 ml glass N/A Cool, 4°C ATL M0-3N4 901115T 08 PCBs (EPA 8080) Soil 11-15-90 Hand-trowel 250 ml glass N/A Cool, 4°C ATL M0-3Sl 901008A 44 PCBs (EPA 8080) Soil 10-5-90 Hand-trowel 250 ml glass N/A Cool, 4°C ATL M0-3S2 901008A 45 PCBs (EPA 8080) Soil 10-5-90 Hand-trowel 250 ml glass N/A Cool, 4°C ATL

M0-3S3 901008A 49 PCBs (EPA 8080) Soil 10-5-90 Hand-trowel 250 ml glass N/A Cool, 4°C ATL M0-3El 901008A 41 PCBs (EPA 8080) Soil 10-5-90 Hand-trowel 250 ml glass N/A Cool, 4°C ATL M0-3E2 901008A 42 PCBs (EPA 8080) Soil 10-5-90 Hand-trowel 250 ml glass N/A Cool, 4°C ATL M0-3E3 901008A 43 PCBs (EPA 8080) Soil 10-5-90 Hand-trowel 250 ml glass N/A Cool, 4°C ATL M0-3Wl 901024H 01 PCBs (EPA 8080) Soil 10-23-90 Hand-trowel 250 ml glass N/A Cool, 4°C WJG M0-3W2 901024H 02 PCBs (EPA 8080) Soil 10-23-90 Hand-trowel 250 ml glass N/A Cool, 4°C WJG

M0-4Nl 901008A 13 PCBs (EPA 8080) Soil 10-5-90 Hand-trowel 250 ml glass N/A Cool, 4°C ATL M0-4Nl 901024H 03 VOCs (EPA 8240) Soil 10-23-90 Hand-trowel 125 ml glass N/A Cool, 4°C WJG M0-4N2 901008A 14 PCBs (EPA 8080) Soil 10-5-90 Hand-trowel 250 ml glass N/A Cool, 4°C ATL M0-4N3 901008A 15 PCBs (EPA 8080) Soil 10-5-90 Hand-trowel 250 ml glass N/A Cool, 4°C ATL M0-4Sl 901008A PCBs (EPA 8080) Soil 10-5-90 Hand-trowel 250 ml glass N/A Cool, 4°C ATL M0-4S2 901008A PCBs (EPA 8080) Soil 10-5-90 Hand-trowel 250 ml glass N/A Cool, 4°C ATL

\J.I A: Field filtration not applicable to soil samples.

GERAGHTY MILLER, INC.

-Page 2 of 4


Field Laboratory Sample Sample Sampling Sampling Sample Field Sample Samplers Sample ID Sample ID Analysis Matrix Date Equipment Container Filtration Preservation Initials

M0-4S3 901008A 24 PCBs (EPA 8080) Soil 10-5-90 Hand-trowel 250 ml glass N/A Cool, 4°C ATL M0-4El 901008A 16 PCBs (EPA 8080) Soil 10-5-90 Hand-trowel 250 ml glass N/A Cool, 4°C ATL M0-4E2 901008A 17 PCBs (EPA 8080) Soil 10-5-90 Hand-trowel 250 ml glass N/A Cool, 4°C ATL M0-4E3 901008A 18 PCBs (EPA 8080) Soil 10-5-90 Hand-trowel 250 ml glass N/A Cool, 4°C ATL M0-4E4 901115T 07 PCBs (EPA 8080) Soil 11-15-90 Hand-trowel 250 ml glass N/A Cool, 4°C ATL M0-4Wl 90l008A 19 PCBs (EPA 8080) Soil 10-5-90 Hand-trowel 250 ml glass N/A Cool, 4°C ATL M0-4W2 90l008A 20 PCBs (EPA 8080) Soil 10-5-90 Hand-trowel 250 ml glass N/A Cool, 4°C ATL

M0-4W3 901008A 21 PCBs (EPA 8080) Soil 10-5-90 Hand-trowel 250 ml glass N/A Cool, 4°C ATL DP-1 901008A 09 PCBs (EPA 8080) Soil 10-5-90 Hand-trowel 250 ml glass N/A Cool, 4°C ATL M0-5Nl 901008A 31 PCBs (EPA 8080) Soil 10-5-90 Hand-trowel 250 ml glass N/A Cool, 4°C ATL M0-5N2 901008A 32 PCBs (EPA 8080) Soil 10-5-90 Hand-trowel 250 ml glass N/A Cool, 4°C ATL M0-5Sl 901008A PCBs (EPA 8080) Soil 10-5-90 Hand-trowel 250 ml glass N/A Cool, 4°C ATL M0-5S2 901008A 26 PCBs (EPA 8080) Soil 10-5-90 Hand-trowel 250 ml glass N/A Cool, 4°C ATL

M0-5S3 901008A 27 PCBs (EPA 8080) Soil 10-5-90 Hand-trowel 250 ml glass N/A Cool, 4°C ATL MO-SEl 901024H 04 PCBs (EPA 8080) Soil 10-23-90 Hand-trowel 250 ml glass N/A Cool, 4°C WJG M0-5Wl 901008A 28 PCBs (EPA 8080) Soil 10-5-90 Hand-trowel 250 ml glass N/A Cool, 4°C ATL DP-2 90 1 008A 30 PCBs (EPA 8080) Soil 10-5-90 Hand-trowel 250 ml glass N/A Cool, 4°C ATL M0-5W2 901008A 29 PCBs (EPA 8080) Soil 10-5-90 Hand-trowel 250 ml glass N/A Cool, 4°C ATL

II A: Field filtration not applicable to soil samples.


of 4



M0-6Nl 901008A 39 PCBs (EPA 8080) Soil 10-5-90 Hand-trowel 250 ml glass N/A Cool, 4°C ATL M0-6N2 901008A 40 PCBs (EPA 8080) Soil 10-5-90 Hand-trowel 250 ml glass NIA Cool, 4<>C ATL M0-6N3 901024H 05 PCBs (EPA 8080) Soil 10-23-90 Hand-trowel 250 ml glass N/A Cool, 4°C WJG M0-6Sl 901008A 33 PCBs (EPA 8080) Soil 10-5-90 Hand-trowel 250 ml glass N/A Cool, 4°C ATL M0-6El 901008A 37 PCBs (EPA 8080) Soil 10-5-90 Hand-trowel 250 ml glass N/A Cool, 4°C ATL

M0-6E2 901008A 38 PCBs (EPA 8080) Soil 10-5-90 Hand-trowel 250 ml glass N/A Cool, 4°C ATL M0-6E3 901008A 36 PCBs (EPA 8080) Soil 10-5-90 Hand-trowel 250 ml glass N/A Cool, 4°C ATL M0-6Wl 901008A 34 PCBs (EPA 8080) Soil 10-5-90 Hand-trowel 250 ml glass N/A Cool, 4°C ATL M0-6Wl 901024H 06 VOCs (EPA 8240) Soil 10-23-90 Hand-trowel 125 ml glass NIA Cool, 4°C WJG M0-6W2 901008A 35 PCBs (EPA 8080) Soil 10-5-90 Hand-trowel 250 ml glass N/A Cool, 4°C ATL

M0-7Nl 901008A 01 PCBs (EPA 8080) Soil 10-5-90 Hand-trowel 250 ml glass N/A Cool, 4°C ATL M0-7N2 901008A 02 PCBs (EPA 8080) Soil 10-5-90 Hand-trowel 250 ml glass N/A Cool, 4°C ATL M0-7N3 901008A 03 VOCs (EPA 8240) Soil 10-23-90 Hand-trowel 125 ml glass NIA Cool, 4°C WJG M0-7N3 901024H 07 PCBs (EPA 8080) Soil 10-5-90 Hand-trowel 250 ml glass NIA Cool, 4°C ATL

M0-7Sl 901008A 04 PCBs (EPA 8080) Soil 10-5-90 Hand-trowel 250 ml glass N/A Cool, 4°C ATL M0-7S2 901008A 05 PCBs (EPA 8080) Soil 10-5-90 Hand-trowel 250 ml glass NIA Cool, 4°C ATL M0-7S3 901008A 06 PCBs (EPA 8080) Soil 10-5-90 Hand-trowel 250 ml glass NIA Cool, 4°C ATL M0-7El 901008A 10 PCBs (EPA 8080) Soil 10-5-90 Hand-trowel 250 ml glass N/A Cool, 4°C ATL

N/ A: Field filtration not applicable to soil samples.


-Page 4 of 4



M0-7E2 901008A 11 PCBs (EPA 8080) Soil 10-5-90 Hand-trowel 250 ml glass N/A Cool, 4°C ATL M0-7E3 901008A 12 PCBs (EPA 8080) Soil 10-5-90 Hand-trowel 250 ml glass N/A Cool, 4°C ATL M0-7Wl 901008A 07 PCBs (EPA 8080) Soil 10-5-90 Hand-trowel 250 ml glass N/A Cool, 4°C ATL M0-7W2 901008A 08 PCBs (EPA 8080) Soil 10-5-90 Hand-trowel 250 ml glass N/A Cool, 4°C ATL

DD-N 901115T 01 PCBs (EPA 8080) Soil 11-15-90 Hand-trowel 250 ml glass N/A Cool, 4°C ATL DD-S 901115T 02 PCBs (EPA 8080) Soil 11-15-90 Hand-trowel 250 ml glass N/A Cool, 4°C ATL SP-1 (N&W) 901115T 03 PCBs (EPA 8080) Soil 11-15-90 Hand-trowel 250 ml glass N/A Cool, 4°C ATL SP-2 (E&S) 901115T 04 PCBs (EPA 8080) Soil 11-15-90 Hand-trowel 250 ml glass N/A Cool, 4°C ATL SP-3 (N&W) 901115T 05 PCBs (EPA 8080) Soil 11-15-90 Hand-trowel 250 ml glass N/A Cool, 4°C ATL SP-4 (E&S) 901115T 06 PCBs (EPA 8080) Soil 11-15-90 Hand-trowel 250 ml glass N/A Cool, 4°C ATL

'J/ A: Field filtration not applicable to soil samples.


J

I

UJ C!l a: <( a:l <( ...J

~ c..> I

5 z

15!1764

M0-4 ...

•

EXPLANATION

< -z () m z _,

c...

C/)

-1 ::n )> () c: N N

PREVIOUS SOIL SAMPLE LOCATION AND DESIGNATION M0-3,4 & 5 MAY .1988 M0-6, 7, 8, 9, 10 AND 11 MARCH, 1989

SOIL SAMPLE LOCATION

SCALE

0 50

FEET

!CU

SHOWN

SOIL PILE • • •M0-4 ......... • • • A M0-8

TRAILER

DD-S

~, 0 .,

., 1::0 ____ ,,~

m ::0 .... < r-% m

AM0-9

~. • • • ••••

/ :M0-3

/. /

l

SPEED SHOP

m ::0 -1 < r-% m

_,

... M0-10

I

\ g~----------------------4 SURFICIAL SOIL SAMPLING LOCATIONS,

NEWEll STREET MARCHETTO PROPERTY,

October 5 and 23, 1990, Pittsfield, Massachusetts

FIGURE

1

',(Y 'f) :;~

~

l

' I I I

]

151171>4

MARCHETTO PROPERTY LINE

M0-6N3.

M0·6N2.

M0-6N1.

-w 10

0 :E

N w 10

0 :E

M w 'ol? 0 :E

M0-6 --+--- ••• • • • "" -~ ~ 10 'ol? 6 0 :E :E

M0-5 • • N -~ ~ It) It)

6 6 ~

:E :E

a: CJ a:)

~ :::1

w CJ a: c( Ill c( ...J

< §

a: ::t ,; () UJ 1-....I 0 ...J

>' 4:: uJ 1-

a: ~ a: w 1- % c.

;;( 0 a: a: 0 c.

a: ~ MO._..N3.

M0-4N2. - N M ..,. w w w w .., .., .., ..,. ' 6 ' '

M0-4N1. 0 0 0

\ :E :E :E :s M0-4-- •• •• • • • • DD-S •

~N ... • M0-4S1 ~~ ~ .... "!

66 0 • M0-4S2 :E:E :E

.• M0-4S3

d EXPLANATION z

~ M0-4 ... PREVIOUS SOIL SAMPLE lOCATION AND DESIGNATION M0-3,4 & 5 MAY .1988

SCALE

0 20

M0-6 & 7 MARCH, 1989

SOil SAMPLE lOCATION

SOil PILE

leAU:

SHOWN :t-------------f ~ I A., GERAGHTY ~ ~I' & MU.I.ER, INC. ~ ~ ,..,.. l'ftfl'l,~ s~.

FEET

( SPEED SHOP 1 \ SURFICIAL SOIL SAMPLING LOCATIONS

ADJACENT TO M0-4, M0-5, M0-6 AND M0-7,

NEWELL STREET MARCHETTO PROPERTY, October 5 and 23, 1990, Pittsfield, Maasactusetts

FIGURE

2

~ jJ '

.

I I I I I I I .

I

> < a: 1.!1

a:i

~ :t

iJJ 1.!1 a: < Cl)

< ...,j

< § 0:: ~ ()

~ ()

l

5 :;:

0

N

3: C")

' 0 ::E

M0-3- e

• M0-3N4

- • M0-3N3

~ • M0-3N2

i • M0-3N1

••••• M0-3S1.

- N M w w w '1 t? (") 0 0 0

/. ,M0-3S2. I .

/I;/ I M0-3S3 • lj /I '' /1, . / I

//;/I / / ' I .

w ~ ...J

> ..... a: w a. 0 a: a.

::E ::E ::E

EXPLANATION

M0-3 PREVIOUS SOIL SAMPLE .A. LOCATION AND DESIGNATION

M0-3.4 & 5 MAY .1988 M0-6 & 7 MARCH, 1989

e SOIL SAMPLE LOCATION

LOG PILE LOCATION

ANTHONY MARCHETTO CONTRACTORS

SCALE

20

FEET

i I

~~:AU:

=~------------~S~HO~W~N~------------~ -. ~ , A., GERAGHTY

SURFICIAL SOIL SAMPLING LOCATION

ADJACENT TO M0-3,

• -w % :i > ..... a: w a. 0 a: a.

I

'

f.r & MilLER, INC. A"n.w~s~.

NEWELL STREET MARCHETTO PROPERTY, October 5 and 23, 1990, Pittsfield, Massachusetts

-..,

-1

'

FIGURE

3

(<1

i.!l >]

~ (.)

I z 0 z

l5l!7l!c

M0-4 ... EXPLANATION

PREVIOUS SOIL SAMPLE

< -z (") m z -1

c...

(/) -1 ::rJ )> (") c N N

LOCATION AND DESIGNATION M0-3,4 & 5 MAY .1988 M0-6, 7, 8, 9, 10 ANO 11 MARCH, 1989

SOIL PILE

~I 0 , m ::c ..... -< ,... % m

• • eM0-4

·~ • • A M0-8

-.A M0-9

SPEED SHOP

TRAILER

1-----\

t

I I

.A I M0-10

e SOIL SAMPLE LOCATION

0

0

AREA WITH SURFICIAL SOIL PCB CONCENTRATIONS >22ppm

SCALE

FEET

liiCML

SHOWN

50

SURFICIAL SOIL LOCATIONS

WITH PCB CONCENTRATIONS >22ppm

NEWELL STREET MARCHETTO PROPERTY,

October 5, 1990, Pittsfield, Massachusetts

FIGURE

4

1 .J

APPENDIX A


]

I I

J

l

~.,GERAGHTY AI'& MILLER, INC.

Je!Environmental Services M0-3

SAMPLE/CORE LOG AY03402/GE Company

Site Newell Street Marchetto Property 10-5-90 Drilling 10-5-90 Location------------------ '"''-'-------Completed _____ _

0.3 12 Total Depth Drilled ____ teet Hole Diameter----"

Type of Sample/ Hand-Trowel Coring Device ----------

Length and Diameter of Coring Device --------------------Sampling Interval _______ ,,...,,_,,

land-Surface ........... _____ ,, ..... , 0 Surveyed 0 Estimated

Drilling Fluid Used ___________________ Drilling Memc)a __ Ha_nd_s_~....:_l_ed ___ _

Drilling Contractor--------------------Prepared A. LaBarge Hammer Hammer By------------------------ ____ Drop

Sample/Core Oeplh (feet below land surface) Core

Recovery From To (feet)

0 0.3

I J I

nme/Hydraulic Pressure or Blows per 6

inches Sample/Core Description

Sand (70%) medium-grain, dark-brown; Gravel (20%) small, rounded;

Silt (10%) fine-grain, dark-brown

Soil from all s~le locations in the M0-3 grid appears as above.

I

] I

I

I I I I

• .I

.A., GERAGHTY Alf& l\11LLER, INC.

Je!Environmenral Services SAMPLE/CORE LOG H0-4 AY03402/GE Company

•c•'----- Project/No. ------------------

Site Hewell Street Marchetto Property Location ------------------

10-5-90 Drilling 10-5·90 lt::U ______ Completed _ ___;_..:;___ __ _

Type of Sample/ Coring Device ____ H_and_-_T_ro.:.:.w:..::e.:..l __ _ 0.3

Total Depth Drilled ____ feet Hole Diameter __ 1_2 __ inches

Length and Diameter of Coring Device --------------------Sampling Interval -------'

Land-Surface Elev. ____ feet 0 Surveyed 0 Estimated

Drilling Fluid Used ___________________ Drilling Method Hand sanpled

Drilling Contractor---------------------

Hammer Hammer Prepared A. LaBarge By _______ ~------------------------------ ____ Drop ____ inches

Sample/Core Oeplh (feet below land surface) Core


0 0.3

!

I

I

I

I

Time/Hydraulic Pressure or Blows per 6

inches

I :

Sample/Core Description

Sand (50%) medium-grain, dark-brown; Gravel (30%) small-size, rounded;

Silt (20%) fine-grain, dark-brown

H0·4W1 and M0-4W2: Soil as described above to 3 inches. Abrupt change to a

fine, light-brown sand (100%) at 3 to 4 inches.

M0-4W3: Soil as described above, stained black with strong chemical

(petroleum) odor. Appears as a localized soil contamination, probably from

1changing automobile oil or automobile leaks.

lcoupt sanpl taken at H0-4W3)

I

l

1m II

I

I I

~.,GERAGHTY All'& MILLER, INC.

A/Environmental Services

Site

SAMPLE/CORE LOG

Ux3tion ___ N_ew_e_l_l_s_t_re_e_t_M_a_rc_h_e_tt_o __ ~--~---------Drilling

10•5-9° Completed __;_;:._::_...::...::... __ _

Total Depth Drilled __ 0_·3--"""'" Length and Diameter

Type of Sample/ Hole Diameter __ , __ 2_inches Coring Device __ __:_=.:.:::......:..:...=.::..:.. ___ _

of Coring Device -------------------Sampling Interval -------'"'""'

Land-Surface '-'"'v·-----'"'"'' 0 Surveyed Estimated

Drilling Fluid Used ____________________ Drilling Method Hand sa!Jllled

Drilling Contractor--------------------Prepared Hammer Hammer By ___ ...!!.:_!:_!:~~-----------------Weight _____ Drop ___ inches

Sample/Core Depth (feet below land surfacej Core

From To

0 0.3

I

I

I

I I

Recovery (feet)

I

i I


inches

I I

I


Sand C80X) medium-grain, dark-brown; Gravel C20X) small-size, rounded;

M0-5S1 and M0-5S2, M0·5S3 and H0-5N1: Soil appears as described above to

0 to 1 inch.Abrupt change to a fine light-brown sandC100X) from 1 to 4 inche

Duplicate sample <DP-2) taken at M0-5~1.

i

I

I

J ]

· .• ~.~. ) ;~

I .

I I I

I '

_,.,GERAGHTY Alf& tvllLLER, INC.

Je,fEnvironmental Services SAMPLE/CORE LOG

Site Location __ N_e_we_L_L_s_t_r_ee_t_M_a_r_ch_e_t_to _ __:__.:__ ____ _

Drilling ,cu __ ,_o_-5_·_9o ___ Completed _1_._0--=-5---9-=o __ _

Total Depth Drilled __ 0_·3 __ feet

Length and

Hole Type of Sample/ Coring Device ___ _.:.;H;:;.and---· T_,.r...:o.:.:.we:.:L:__ __

of Coring Device --------------------Sampling Interval _______ ,<A;;,

land-Surface '-'"'v·-----""'"'' 0 Surveyed 0 Estimated

Drilling Fluid Used -------------------Drilling Method._---!!lHaatnd~s""aoo~l.£:]ed,;__ __ _

Drilling Contractor-------------------Prepared Hammer Hammer BY-----~~~~--------------------------- ____ Drop ____ inches

Sample/Core Depth (feet below land surface) Core


0 0.3

I

I

I

I


inches Sample/Core Description

Sand (80%) medium-grain, dark-brown; Gravel (20%) samll·size; rounded.

M0·6Y1 and M0·6W2: Soil as described above (50%) with sheetrock and tree bar

fragments (50%) mixed in.

M0·6E1: Soil as described above, with grayer color.

M0·6N2: Soil as described above from 0 to 3 inches; Abrupt change to

l ight·brown, fine-grained sand (100%) from 3 to 4 inches.

J

J

I

l

. I I

.A.,GERAGHTY All'& MILLER. INC.

J81£nvironmenral Services

H0-7

Site

SAMPLE/CORE LOG

Location _N_e_w_el_L_s_t_r_ee_t_Ma_r_c_he_t_to _ __:_ _ _;;__ ____ _ Drilling

10·5·90 Completed _1_0--'-5--9'--'-o ___ _

Total Depth Drilled _o_._3 --'"'""'

Length and Diameter

Type of Sample/ Hole Diameter __ ,_2 __ inches Coring Device _ __:.:.::.:.:;::_;_:...=.;c.;;_ ____ _

of Coring Device -------------------- Sampling Interval -------'"'"''

Land-Surface ,_,,.,.v. _____ , Surveyed D Estimated

Drilling Fluid Used ___________________ Drilling Method Hand s~led

Drilling Contractor-------------------Prepared Hammer Hammer By ---~~==~~--------------------------- ____ Drop ____ ,

Sample/Core Depth (feet below land surface) Core


0 0.3

'

I

l

I I


inches

I


Sand (70%) medium-grain, dark-brown; Gravel (20%) small-size· rounded.

Silt {10%) medium-grain, dark-brown.

M0-7S1: Soil as described above, stained black from 3 to 4 inches

petroleum odor.

M0-7E2: Soil as described above from 0 to 2 inches. Abrupt change to

light-brown, fine-grained sand (100%) from 2 to 4 inches.

M0·7N3: Soil as described above {70%) with cardboard pieces (30%l mixed in.

Petroleum odor.

I

i I I ~

1 I I I J

I I J~

I I I ]

J ~1

APPENDIX B

GERAGHTY MILLER, INC.

EXTRACTION FOR PCB

j PCB1016 PCB1221 ,, PCB1232

] PCB1242 PCB1248 PCB1254 PCB1260

J %SOLIDS

CTtt ANAl VTICPL LABS, LTD Laboratory Analysis Report

09tfN

EPA 5W-B46 11E'llllD 8080 sw-846 HETHJD 8080 SN-846 11E'llllD 8080 SN-846 11E'llllD 8080 5W-846 t£TKJD 8080 SN-846 11E'llllD 8080 5W-846 11E'llllD 8080 5W-846 11ET!{)D 8080 STD. I'£TH. 15TH ED. 209A

PAGE 1

EXTRACTED PC 10/10 <4,480 t£6/1<6 6C 3A: 120 10/16 <4,480 MC6/K6 6C 3A: 120 10/16 <4,480 MCS/1<6 6C 3A: 120 10/16 <4,480 11:6/1<6 6C 3A: 120 10/16 <4,480 11:6/1<6 6C 3A: 120 10/16 24,700 11:6/1<6 6C 3A: 120 10/16 71,300 MC6/K6 6C 3A: 120 10/16

90 % BT 10/19

J

J

CTI1 AtW..YTlcrt. LABS, LTD Laboratory Analysis Report

Para.eters and Standard 11ethodology Used

EXTRACTION FOR PCB EP1\ Slt-846 I£TlllD BOOO PCB1016 Slt-846 11E1IDD BOBO PCB1221 Slt-846 I£TlllD BOBO PCB1232 SN-846 t£T}(JD aoao PCB1242 sw-846 I£THOD aoao PCB1248 Slt-846 t£00D BOOO PCB1254 sw-846 I£THOD aoao PCB1260 Slt-846 I£TlllD BOBO k SOLIDS STD. I'ETH. 15TH ED.209A

PASE 2

Results Anal st Reference

EXTRACTED PC/RK 10118 <918 1£6/KG 6C3 A: 130 10/23 <918 l'tG/KS 6C3 A: 130 10/23 <918 l'tG/KG 6C3 A: 130 10123 <918 l'tG/KG 6C3 A: 130 10123 <918 KCG/KS 6C3 A:130 10/23

4,700 1£6/KG 6C3 A: 130 10/23 22,900 1£6/KS 6C3 A: 130 10123

89 k BT 10/19

_J PCB1242

] PCB1248 it PCB1254 ',}c

PCB1260

I '4 SOLIDS

Cnt AtW.. YTicrt. LABS, LTD Laboratory Analysis Report

EPA 5W-B40 f£00D 8080 5W-B40 I£THOD 8080 5W-B40 i'IETl{ll) 8080 SIH46 I£THOD 8080 5W-B40 HEOOD 8080 5W-B40 I£THOD 8080 5W-B40 I£TKJD 8080 5W-B40 I£THOD 8080 STD. METH. 15TH ED.209A

PAGE 3


EXTRACTED PC 10/25 <917 1'£6/KG 6C 3A:150 11/6 <917 1'£6/KS 6C 3A: 150 11/6 <917 1'£6/KS 6C 3A: 150 11/6 <917 1'£6/KS 6C 3A: 150 11/6 <917 1'£6/KS 6C 3A: 150 11/6

5,070 1£6/KG 6C 3A: 150 1116 9,700 1'£6/KG 6C 3A:150 11/6

sa I a: 11/1

CTI1 ANAI..YTICft. LABS, LID Laboratory lflalysis Report

PAGE 4

~··~ ~~~t=ha=~~~~~=-~===~~=~A~V=~~2~--------------------------------~C=TI1~~~~le~~~:~W=t~~==~M~---------Date Salpled: 10/05/90 Tiae: 00:00 Date Received: 10/05/90 Saalpled By : A. LABAR6E Collection Method: 6RAB

Para~~et~s and Standard Methodology Used Results Anal st Ref~ence

EXTRACTION FOR PCB EPA SN-946 l£llllD 8080 EXTRACTED PC 10/10

PCB1260 SN-846 1£11{)0 8080 B,SW MCG/KG 6C 3A: 118 10/16 .JJ-___!.I~SOL~l~DS~---------___;S!:!.!ID.!!!•wi£TH~.!!..· ...!1.l:!.!5TH!..!.!...!:ED:!!.!•!.:209!!.!!!.A ___________ 92u._ _ _a'L.___ __ J;I_BTI..-l..lo10r.L/1Liol8 ________ _

EXTRACTION FOR PCB PCB1016 PCB1221 PCB1232 PCB1242

] PCB124B PCB1254 PCB1260

J 4 SCUDS

Cnt ANAI..YTICfL LABS, LTD Laboratory Analysis Report

EPA 5W-846 1£000 0080 sw-846 1£000 0080 sw-846 1£000 0080 5W-846 I1E1H3D 0080 5W-846 1£000 0080 sw-846 1£000 0080 sw-846 I1E1H3D 0080 5W-846 l'fET}{)O 0080 STD. I£TH. 15TH ED.209A

PAGE 5


EXTRACTED PC 10/10 (890 1£6/KS 6C 3A: 118 10/16 <890 1£6/KS 6C 3A: 118 10/16 (890 HCG/KS 6C 3A: 118 10/16 <890 1£6/KS 6C 3A: 118 10/16 <890 1£6/KS 6C 3A: 118 10/16

4,580 tf:S/KS 6C 3A: 118 10/16 14,100 1£6/KS 6C 3A: 118 10/16

90 4 BT 10/18

CTI1 ANAL YTICfL. LABS, LTD Laboratory Analysis Report

Results

PAGE 6

Anal st Reference

EXTRACTION FeR PCB EPA SN-B% t£000 8080 EXTRACTED PC 10/10 PCB1016 SN-B% t£nllD 8080 <908 tt:S/KS 6C 3A: 119 10/16 PCB1221 5W-B4b t£000 8080 <908 tt:S/KG GC 3A: 119 10/16 PCB1232 SN-B% t£000 8080 <908 tt:S/KG 6C 3A: 119 10/16 PCB1242 SN-B% t£000 8080 <908 tt:S/KG 6C 3A: 119 10/16

-J~~PC~B~1~2~~------------~5W-~B4b~t£00~~0~8080~------------------~<~908~--~~~/K~G~~6C~3A~:1~19~10~/1~6 ______ __ PCB1254 5W-B4b t£000 8080 3,390 tt:S/KG 6C 3A: 119 10/16 PCB1260 SN-B% 1£000 8080 12,200 IG/KG 6C 3A: 119 10/16

EXTRACTION FOR PCB PCB1016 PCB1221 PCB1232 PCB1242 PCB1248 PCB1254 PCB1260

-J % SCUDS

Cnt ANAL YTICill LABS, LTD Laboratory Analysis Report

EPA Sti-846 t£000 80SO sw-846 l£lll)l) eoeo sw-846 I£THlD eoeo sw-846 l£lll)l) eoeo sw-846 I£Tll)D aoao sw-846 IEOOD BOOO sw-846 I£THlD eoeo sw-846 t£OOD aoao STD. I'ETH. 15TH ED. 209A

PAGE 7


EXTRACTED PC 10/10 <865 1'1:6/KS 6C 3A: 119 10/16 <865 HCS/KS 6C 3A: 119 10/16 <865 1'1:6/KS 6C 3A: 119 10/16 <865 I'ICG/KS 6C 3A: 119 10/16 <865 1£6/KS 6C 3A: 119 10/16

5,220 1£6/KG 6C 3A: 119 10/16 9,130 1£6/KS 6C 3A: 119 10/16

91 % BT 10/18

-J

CTM ANAl.YTicrt. LABS, LID Laboratory Analysis Report

Paraaeters and Standard l'lethodol . Used

EXTRACTION FOR PCB EPA Sli-846 I£TJIID 8000 PCB1016 Sli-846 I£TJIID 8000 PCB1221 Sli-846 t£000 8000 PCB1232 Sli-846 1£000 8000 PCB1242 Sli-846 PETOOD 8000 PCB1248 Sli-846 t1ETHOD 8000 PCB1254 Sli-846 1£000 8000 PCB1260 Sli-846 1£001) 8000 X Sfl..IDS SID. HETH. 15TH ED.209A

PAGE 8


EXTRACTED PC 10/10 <4,460 l'tS/KG GC 3A: 122 10/16 <4 460 l'tS/KG GC 3A: 122 10/16 <4,460 l'tS/KG GC 3A: 122 10/16 <4 460 11:6/KG GC 3A: 122 10/16 <4 460 11:6/KG GC 3A: 122 10/16 8,830 11:6/KS sc 3A: 122 10/16 30,400 l'tS/KG GC 3A: 122 10/16

91 X BT 10/18

CTI'I ANAI..YTicrt. LABS, LTD Laboratory Analysis Report

09 NOV 1990

PAGE 9

EXTRACTION FOR PCB EPA Sit-846 I£THOD 8080 EXTRACTED PC/Rl< 10118 PCB1016 5W-846 HEOOD 8080 <9,003 11:6/KG 6C3 A:130 10/23

1 1 sw-840 I£THOD 8080 <9,003 IG/K6 6C3 A: 130 10123 Sit-846 HETI{)I) 8080 <9,003 11:6/KG 6C3 A: 130 10/23 5W-846 I£THOD 8080 <9,000 IG/KG 6C3 A: 130 10/23

CTI1 ANAL YTICfi.. LABS, LTD laboratory Analysis Report

PAGE 10

J Purchase Order t.kllber: AV03402 CTM Saaple No: 901000A 18 c~~D~a~~~~~~~.~le~d~:~10~/~re~/90~~T~i~~:~OO~:OO~--------·----------------------~D~a~~~R~K~e~iv~~~:~10~/re=/~90~----------

j Saliple Id: H0-4£3 l'latrix: SOIL Sallpled By : A. LABARGE Collection Method: 6RAB

Location : GE, PITTSFIELD, I1A

Par~ters and Standard t1ethodol . Used Results Anal st Reference

EXTRACTION FOO PCB EPA SN-846 I£THOD 0080 EXTRACTED PC 10125

PCB1232 SN-846 I£THOD 8080 <4,570 lt:S/KS 6C 3A: 149 11/6 PCB1242 SN-846 I£THOD 8080 <4:570 lt:S/1<5 SC 3A: 149 11/6

PCB1260 SN-846 I£THOD 0080 127,000 HCG/KS 6C 3A:149 11/6

CTH ANALYTICfi. LABS, LTD Laboratory Analysis Report

09 oov 1990

PA6E 11

].1-_S<liP;::.::::;::...;:I.:;:_e ...::.Id:.::_:liF;.;_41i1~1 =~~=--------------------=11a=tr..:.:ix:.:.::.....:SO=IL::.__ _______ _ d Location : SE, PITTSFIELD, t1A

saiiPled BY : A. LABMSE Collection Hethod: GRAB

thodology Used Results Anal st Reference

EPA sw-840 I£THlD 8080 EXTRACTED PC 10/10 sw-840 l£1liJD 8080 <901 lt:G/KS 6C 3A: 119 10/16

<901 lt:G/KS 6C 3A: 119 10/16 <901 lt:G/KS 6C 3A:119 10/16 <901 ID3/K6 6C 3A: 119 10/16 <901 lt:G/KS 6C 3A: 119 10/16

3,060 ID3/K6 6C 3A: 119 10/16 641 tt::G/KS 6C 3A: 119 10/16

90 % BT 10118

D ~ f~;

-J

CTM IYW..VTICfL LABS, LTD laboratory Analysis Report

Para.eters and Standard Methodology Used

EXTRACTION FOR PCB EPA 5W-846 11Ell1JD 8000 PCB1016 5W-846 t£00D 0080 PCB1221 5W-846 t£THOD 8080 PCB1232 sw-846 I£1KID 8000 PCB1242 5W-846 tETOOD 0080 PCB1248 sw-846 t£00D 0080 PCB1254 5W-846 I£THOD 0080 PCB1260 5W-846 I£THOD 8080 % stl..IDS STD. t£TH. 15TH ED. 209A

PAGE 12


EXTRACTED PC 10/10 <448 1'1:6/KS 6C 3A: 120 10/16 <448 1'1:6/KS 6C 3A: 120 10/16 <448 tu:S/KS 6C 3A: 120 10/16 <448 1'1:6/KS 6C 3A: 120 10/16 <448 1'1:6/KS 6C 3A:120 10/16

92.7 tu:S/1<6 GC 3A: 120 10/16 4,260 1'1:6/KS 6C 3A: 120 10/16

92 % BT 10/19

I ,;~:,

PCB1254 PCB1260 t SOLIDS

Cllt ANALYTICtt. LABS, LTD Labtratory r:Vlalysis Report

w lllV 1990

EPA SM-846 I£THOD BOaO sw-846 t£THOD eoao sw-846 t£THOD eoao sw-846 MET!IlD eoeo sw-846 t£1HJD eoeo sw-846 t£THOD eoeo SN-846 HETHOD BOBO sw-846 MET!IlD eoeo STD. t£TH. 15TH ED.209A

PAGE 13


EXTRACTED PC 10/10 <474 HCS/KS 5C 3A: 120 10/16 <474 1£6/KS 5C 3A:120 10/16 <474 1£6/KS 5C 3A: 120 10/16 (474 HCS/KS 5C 3A: 120 10/16 <474 HCS/KS 5C 3A: 120 10/16 920 1£6/KS 5C 3A: 120 10/16

2,190 HCS/KS 5C 3A: 120 10/16 Bb % BT 10118

~) t';:, ~

-·v

~J

-J

Cnt ANALYTICft. LABS, LTD Laboratory Analysis Report

Parc1111eters and Standard Methodology Used

EXTRACTION FOR PCB EPA 5W-846 I£00D 8080 PCB1016 5W-846 t£00D 8080 PCB1221 5W-846 1£00D 8080 PCB1232 5W-846 t£001) 8080 PCB1242 Slrl-846 t£JliJD 8080 PCB1248 Slrl-846 I£00D 8080 PCB1254 5W-846 I£00D 8080 PCB1260 Slrl-846 11ETJilD 8080 % SOLIDS STD. METH. 15TH ED.209A

PAGE 14

Results Anal st Re-ference

EXTRACTED PC 10/10 <925 1'1::6/KS 6C 3A: 120 10/16 <925 1'1:6/KS 6C :sA: 120 10/16 <925 1'1:6/KS 6C 3A: 120 10/16 <925 1'1:6/KS 6C :sA: 120 10/16 <925 1'1:6/KS 6C 3A: 120 10/16

4,550 1'1:6/KS 6C 3A: 120 10/16 8,850 1'1:6/KG 6C 3A: 120 10/16

90 z BT 10/19

Cnt ANAL.VTicrt. LABS, LTD Laboratory Analysis Report

PAGE 15

Cnt Saaple No: 901ooeA 30

EPA SN-846 tEOOD 8000 EXTRACTED PC 10/10 sw-846 t£nllD 8080 <917 tt::s/1<6 6C 3A: 116 10/16 SN-846 I£00D 8080 <917 tt::s/KS 6C 3A: 116 10/16

j'~--~~~------------~~~~~~~D~0000~~----------------~~<9~17~--~tt::s;/~~~~6C~3A~:~1~16~1~07./176 ______ __ -ll 5W-846 HEOOD 8000 6,390 tt::s/KS 6C 3A: 116 10/16 SN-846 l£1lllD 8000 13,900 tt::s/KS 6C 3A: 116 10/16

~ ""F~ ';>

J

Cnt AtW... VTICAL LABS, LTD Laboratory Analysis Report

Parc111eters and Standard l'lethodology Used

EXTRACTION FOR PCB EPA sw-846 t£00D 0080 PCB1016 SN-846 t£00D 0080 PCB1221 SN-846 tETHOD 0080 PCB1232 SN-846 t£OOD 8080 PCB1242 SN-846 HETIIlll 8080 PCB1248 SN-846 I£TIIlD 8080 PCB1254 sw-846 I'IETHOD 8080 PCB1260 SN-846 11E1HJD 8080 %SCUDS STD. 11ETH. 15TH ED.209A

PAGE 16


EXTRACTED PC 10/10 <SOB 11C6/K6 6C 3A: 116 10/16 <SOB ti:6/K6 6C 3A: 116 10/16 <SOB 11:6/KS 6C 3A: 116 10/16 <SOB 1'1:6/KS 6C 3A: 116 10/16 <SOB 1'[6/KS 6C 3A: 116 10/16

2,290 11C6/K6 6C 3A: 116 10/16 5,090 11:6/KG 6C 3A: 116 10/16

82 % BT 10/18

Para.~~eters and Standard MethOdOlogy lJSed

CTI1 PIW..YTICAL LABS, LTD Laboratory tllalysis Report

PAGE 17

CTI1 Sallple No: 901008A 32 Date Received: 10105190

Results Analyst Reference

EXTRACTION FOR PCB EPA SH% 1£00D 8080 EXTRfLTED PCIRK 10118 PCB1016 SN-846 I'IETOOD 8000 <989 IDl/KS 6C3 A: 130 10123 PCB1221 SH% 1£000 8000 <989 !DilKS 6C3 A: 130 10123

1232 SN-846 I£TJ{JD 8000 <989 !DilKS 6C3 A: 130 10123 PCB1242 5W-846 I£THOD 8000 <989 MCSIKS 6C3 A: 130 10123

B1248 SN-846 I'EOOD 8080 <989 !DilKS 6C3 A: 130 10123 PCB1254 SN-846 I£THOD 8080 24,700 !DilKS 6C3 A: 130 10123 PCB1260 SN-846 I'ETKlD 8000 17,900 11CSIKS 6C3 A: 130 10/23

LE6END: < = LESS THAN, > = GREATER THAN 116/KG=PPH, IDi/KG=PPB, 11SIL=PPH, I'£GIL=PPB, HCGIS=PPI't

ru "'Q<

·I \~~

J

CTH AtW.. YTicrt. LABS, LTD Labt:ratory Analysis Report

Para.~eters and Standard l"ethodology Used

EXTRACTION FOR PCB EPA sw-846 HEllllD 8000 PCB1016 SM-846 HEllllD 8000 PCB1221 sw-846 I£THOD 8000 PCB1232 SM-846 t£001) 8080 PCB1242 SM-846 I£THOD 8080 PCB1248 SM-846 t£00D 8080 PCB1254 SM-846 1£00D 8000 PCB1260 SN-846 METHOD 8000 % SOLIDS STD. I£TH. 15TH ED.209A

PAGE 18


EXTRACTED PC 10/10 (958 11:6/KS 6C 3A: 116 10/16 <958 lt.:G/KS 6C 3A: 116 10/16 <958 lt.:G/KS 6C 3A: 116 10/16 (958 lt.:G/KS 6C 3A: 116 10/16 <958 11:6/KG 6C 3A: 116 10/16

9,760 11:6/KS 6C 3A: 116 10/16 17,300 11:6/KS 6C 3A: 116 10/16

Bb % BT 10/18

;~ Purchase Order Nwlber: AY03402 Date Salpled: 10/05/90 Time: 00:00

,HA

CTI1 AtW..YTlett. LABS, LTD Laboratory Analysis Report

PAGE 19

Cnt Salple No: 901008A 34 Date Received: 10/05/90 Collection Method: GRAB Katrix: SOIL

-~~~P~~~~~t=~~s~~~d~S~t~=~~d~~~th=o=oo=l~~~Y~~==d--------------------------~==~------~~~~~~------d

EXTRACTION FOR PCB EPA Sil-846 METHOD 8000 Sil-846 HETHOD 8000 SN-840 METHOD 8000 SN-846 I'IETHOD 8000 SN-846 HETOOD 8000 SN-846 HETHOD 8000

-J

CTI'I ANALYTIC&l. LABS, LTD Laboratory Analysis Report

Pari.llt!teM and Standard 11ethodol . Used

EXTRACTION FOR PCB EPA stt-846 I£OOD OOSO PCB1016 5W-846 t£00D 8080 PCB1221 5W-846 t£00D OOSO PCB1232 stt-846 t£00D OOSO PCB1242 5W-8% METHOD OOSO PCB124B SN-846 t£00D OOSO PCB1254 SN-846 HETHOD OOSO PCB1260 SN-846 t£00D OOSO X SOLIDS STD. METH. 15TH ED.209A

PAGE 20


EXTRACTED PCIRK 10118 <940 tt::S/KS SC3 A: 130 10/23 <940 11:6/KS SC3 A: 130 10/23 <940 tt::S/KS SC3 A: 130 10/23 (940 lf:S/KS SC3 A: 130 10/23 (940 tt::S/KG SC3 A: 130 10/23

8,960 tt::S/KS SC3 A: 130 10/23 10,200 lf:S/KS SC3 A: 130 10/23

87 X BT 10/18

LEGEND: < = lESS THAN, > = GREATER THAN

CTI1 AtW..YTicrt. LABS, LTD Laba-atory fNlysis Report

09 trN 1990

EXTRACTION FOR PCB EPA SW::846 t£:m:ID 8000 EXTRACTED PC 10/25

PAGE 21

PCB1016 stiFim t£T00D 80BO <993 l't5/K6 6C 3A: 150 11/6

;I' PCB1248 Slrl-846 I£00D 8080 (993 1'[5/KS 6C 3A: 150 11/6 t~--~~~------------~~~~~~--------------------~~--~~~~~~~~~-------

5'' PCB1254 SN-846 l£1lllD 8080 6,970 l't5/K6 6C 3A:150 11/6

PCB1242 Slrl-846 I£Tli)D 8080 <993 l't5/K6 6C 3A: 150 11/6

PCB1260 SN-846 HEOOD 8080 12,400 l't5/K6 6C 3A:150 11/6 4 SOC.IDS STD. I'ETH. 15TH ED.209A 84 4 CC 11/1

Cnt ANAl YTICAI.. LABS, LTD Laboratory fmlysis Report

EXTRACT!~ FOR PCB EPA 5W-846 t£00D SOSO EXTRACTED PC 10/10

PAGE 22

"~~~PC~B~122~1 ____________ ~5W-846~~~~~D7SOS0~------------------~<4~,~~--~~~/K~6~-=0C~~~:1~17~10~/1~6 ______ _ PCB1232 5W-846 I1EllllD SOSO <4,~ IG/KS OC ~: 117 10/16

PCB1016 5W-846 I1EllllD SOSO <4,~ IG/K6 OC ~: 117 10/16

PCB1260 SN-846 I1EllllD SOSO 24,200 HCS/KS OC ~:117 10/16 J % Stl..IDS STD. t£TH. 15TH ED.209A 85 % BT 10/18

] :00

andard 11ethodo ogy Used

Cll'l ANALYTICAL LABS, LTD Laboratory IV'!alysis Report

09 t()V

PAGE 23

C1l1 Sallp le No: 901 008A 3B Date Received: 10/05/90 Collection l'lethod: GRAB l'latrix: SOIL

Results Mal st Reference

EXTRACTED PC/RK 10118 <976 11:6/1(6 6C3 A: 130 10/23 <976 11:6/1(6 6C3 A: 130 10/23 <976 11:6/1(6 6C3 A: 130 10/23 <976 11:6/1<6 6C3 A: 130 10/23 (976 1'[6/1(6 6C3 A: 130 10/23

6,860 t1C6/J(6 6C3 A: 130 10/23 40,400 t1C6/K6 6C3 A:130 10/23

84 I BT 10/18

·J

CTM ANPL.YTICti.. LABS, LTD Laboratory Analysis Report

Paraaeters and Standard HethodolO!]Y Used

EXTRACTION FOR PCB EPA SN-846 I£1HOO 8000 PCB1016 SN-846 I£1HOO 8000 PCB1221 Slrl-846 I£1HOO 8000 PCB1232 5W-84b t£000 8000 PCB1242 SN-846 t£000 8000 PCB124B SN-846 I£1HOO 8000 PCB1254 SN-846 t£000 8000 PCB1260 SN-846 I£1HOO 8000 X SOLIDS STD. I'£TH. 15TH ED. 209A

PAGE 24


EXTRACTED PC 10/10 <4,930 lt:S/KS 6C 3A: 117 10/16 <4 930 lt:G/KS 6C 3A: 117 10/16 <4,930 lt:S/KS 6C 3A: 117 10/16 <4 930 lt:S/KS 6C 3A: 117 10/16 <4 930 I'ICG/KS 6C 3A: 117 10/16 29,100 HCG/KS 6C 3A: 117 10/16 14,400 lt:S/KG 6C 3A: 117 10/16

84 X BT 10/18

¢] ·j ~',~

] .,

J

Cnt ANALYTICAL LABS, LTD Laboratory fvlalysis Report

()qt«)V

Paraseters and Standard Methodology Used

EXTRACTION FOR PCB EPA sw-846 I£TI{)D 0000 PCB1016 sw-846 f£niJD 0000

~:g~~ sw-846 t£TOOD 0000 SIF846 t£00D 0000

PCB1242 5w:e46 t£OOD aoso

~:i~~ SH46 I£TRJD 0080 S»-846 I'1EOOD 0000

PCB1260 S»-846 I£TIIlD 0000 % SOCJDS STD. I£TH. 15TH ED.2011A

PAGE 25

Cnt Sa.lple No: 90100SA 40 Date Received: 10/05/90


EXTRr£TED PC/RK 10/18 <9,405 IG/KG 6C3 A: 130 10/23 <9,405 ti:G/KG 6C3 A: 130 10/23 <9,405 ti:G/KG 6C3 A: 130 10/23 <9,405 ti:G/KG 6C3 A: 130 10/23 <9,405 ti:G/KG 6C3 A: 130 10/23 20,700 ti:G/KG 6C3 A: 130 10/23 35,500 11C6/K6 6C3 A: 130 10/23

86 % BT 10/19

CTI1 ANit. YTICfi. LABS, LTD Laboratory lflalysis Report

EXTRACTION FOR PCB EPA sw-846 I£TlllD 8080 EXTRACTED PC 10/10

PAGE 26

I; .. ,:L~PC~B~10~1~6------------~~~~~~~~808()~~------------------~<~~7--~~~/K=6--~~~~~:~1~17~10~/1~6--------;,: PCB1221 SIH346 I£T1IlD 8080 <~7 ~/KG ~ ~: 117 10/16 PCB1232 ~~ I£TlllD 8080 <~7 ~/KG ~ ~:117 10/16 PCB1242 ~846 I£TlllD 8000 <~7 ~/K6 ~ ~:117 10/16

PCB1260 5W-~ 1£T11lD 8000 2,240 HCS/KS ~ ~:117 10/16 ;~ '% SCUDS STD. I'ETH. 15TH ED.209A 91 '% BT 10/19

J '',

~

CTI1 ANAlYTICit. LABS, lTD Llboratory Analysis Report

Paraaeters and Standard MethodOlogy used

EXTRACTION FOR PCB EPA SN-846 1£000 8080 PCB1016 SN-846 t£000 8080

B1221 SN-846 1£000 8080 sw-846 1£000 8000 SN-846 1£000 8000 SN-846 t£000 8000 SN-846 1£000 8000 sw-846 t£00D BOBO STD. I£TH. 15TH ED.209A

PAGE 27

CTI1 Sallple No: 90100BA 44 Date Received: 10/05/90


EXTRACTED PC 10/10 <412 1£6/KG 6C 3A: 118 10/16 <412 1£6/KG 6C 3A: 118 10/16 <412 11CS/KG 6C 3A: 118 10/16 <412 11CS/KG 6C 3A: 118 10/16 <412 1£6/KG 6C 3A: 118 10/16

5,850 11CS/K6 6C 3A: 118 10/16 1,450 11CG/KG 6C 3A: 118 10/16

92 I BT 10/18

-~J -~~-:

=J

-J

CTI1 ANALYTICAL LABS, L m Laboratory Analysis Report

Purchase Order ti.tlber: AY03402 Date Saapled: 10/05/90 Tiae: 00:00 Saapled By : A. LABARGE Saaple Id: H0-3Nl Location : SE, PITISFIELD, !'lA

Paraaeters and Standard Methodology Used

EXTRACTION FOR PCB EPA SIHI46 t£00D 8080 PCB1016 SN-946 IEOOD 8080 PCB1221 SIHI46 HETHOD 8080 PCB1232 SN-946 I1EOOD 8080 PCB1242 SIHI46 IEOOD 8080 PCB124B SN-946 I£00D 8080 PCB1254 SN-946 IEOOD 8080 PCB1260 SN-946 IEOOD 8080 4 SOLIDS sm. tETH. 15TH ED. 209A

PAGE 28

CTI1 Saaple No: 90100SA 46 Date Received: 10/05/90 Collection Hethod: GRAB !'latrix: SOIL


EXTRACTED PC 10/10 <4,520 HCS/KG GC 3A: 118 10/16 <4 520 11:6/KG GC 3A: 118 10/16 <4,520 11:6/KG GC 3A: 118 10/16 (4 520 11:6/KG GC 3A: 118 10/16 (4 520 11:6/KG GC 3A: 118 10/16 34,600 11:6/KG GC 3A: 118 10/16 7,720 HCS/K6 GC 3A: 118 10/16

91 4 BT 10/19

CTM ANALYTICAL LABS, LTD Laboratory Analysis Report

EXTRACTION FOR PCB EPA SN-846 t1EllKJD BOSO

PCB1260 5W-B46 t1EllKJD BOSO

PAGE 29

Cnt ANAI..YTic;t. LABS, LTD Laboratory Malysis Report

PAGE 30

Para~~eters and Standard 11ethodol . Used Results Mal st Reference

EXTRACTION FOR PCB EPA 5W-B4b I£00D 8000 EXTRACTED PC 10125

:;1.' PCB1248 5111-846 I£TKlD 8000 <884 11CS/KG 6C 3A: 150 11/b ~·~-PC~B1~~~4------------~5W-~846~1£00~~D~B000~------------------~1~4,~~~--11CS~/~KG~~SC~3A~:~150~11~/~b--------

PCB1242 5W-846 HETIIlD 8000 <884 11CS/K6 6C 3A: 150 11/ b

PCB12b0 5111-846 I£TKlD 8000 5 450 11CS/K6 6C 3A: 150 11/b I SOLIDS STD. I'ETH. 1511f ED.209A 91 4 CC 11/1

I AUTHORizED FOR RELEASE: \ _ ;i\i"" \cc;SJ? I E6END: < = l£55 rnAN, > = GREATER THAN I'IJ/K6=PPI'I, 11CS/K6=PPB, 113/L=PPI'f, HCG/L=PPB, 11C6/6=PPI'f

CTM ANALYTICAL LABS, LTD PAGE 1 LaboratOI'Y Report

EXTRACTION FOR PCB EPA Sl.rl-846 METHOD 8000 EXTRACTED PC 10/26 PCB1016 SW=-846 METHOD SQSQ PCB1221 SW=84b HETHOD 8080 PCB1232 SW-846 METHOD BQSQ <"859 t1C6/K6 GC :iA: 1:10 11/6

t1 PCB1242 sw-a% :T:D g: ~:: ~)~~ ~ ~~::~ ;;~: PCB1248 sw-e D , -11~ PCB1254 SW=-846 METHOD 8080 11, .';00 MCG/KG GC 1'.A • 1 '10 1116 PCB1260 SW-846 MeTHOD 8080 4,970 t-tr.SJKG sc <:~:150 1116

J ;~ SOL IDS sm f-l.ETH 15TH ED 'i09A 87 '! cc 1111 '

CTl1 ~~LYTICAL LABS. LTD Report

EXTRACTION FOR PCB EPA SWo-846 METHOD 8000 EXTRACTED PC 10/26 PCB1016 SWo-846 METHOD 8080 PCB1221 SW-846 METHOD 8080 PCB1232 SWo-846 METHOD 8000 PCB1242 SW-846 METHOD 8000 PCB1248 SW-846 METHOD 8080 {

PCB1254 SW-846 METHOD 8080 36 MCG/KG !3C 3A: 151 i i I L 1dU

PCB1260 SWo-846 MErriOD 8080 76 MCS/1::"6 RC :'\A:l:=il 11/6

J I. SOLIDS STD. METH. 15TH EP.209A 90 'I rr 11/l ,, ld·

CTM AtW.YTICAL LABS, LTD Laboratory Analysis Report

PAGE 3

CTM A~JAL YTICAL LABS, LTD Laboratory Analysis

PASE 4

CTM ANAlYTICAL LABS, lTD Laboratory Analysis Report

PCB1260 SW=846 METHOD 8080

<921

;:;; 11 QRO . .,, ~~0

MrB/KG

;c·;'c :a~~~ MrG/KG MCG/KG

PAGE 5

11 fb f ~ I l.

sr: \A:! 51 11/6 cr

~!~;~; ;;;: ;;: Sf \A•I"il 11/h

6C "':A·l"il 11if.. -;~~--~7.ws~o~t~ro~sL_ ______________ ~sm~.w~~:rrn~.~15ru~~~~·~.7~·0a9~A--------------------~ll---~------~~~----------------90 'I r-r 1111 ,.

CTI1 ANALYTICAl LABS, LTD Laborator·y Analysis RepOt't

PCB1242 8111-846 METHOli 8080 PCB1248 Sl!l-846 METtlOli 8080 PCB1254 SW-846 METHOD 8080

PAGE 6

FtB1260 SW:846 METHOD 8080 Gr. ~A:1~1 11/A 157.000 MCG/KG

~---7._s_o_t_ro_·s _______________ s_m_·. __ Mrru __ . __ 1~ ___ rn_._z_o9_e _____________________ Rz _____ r. _______ r_r __ 1t_t_t ____________ __

CTM ANALYTICAL LABS, LTD Laboratory Anaiysis Report

PAGE 7

CTM ANALYTICAL LABS, LTD Laboratory Analysis Report

PAGE 8

CTM ANALYTICAL LABS. LTD PAGE 9 Laboratory Repm't

PAGE W

.r~----------------------------------------------------------------------------------------------------

CTM ANAliTICAL LABS. LTD

C:! :"·:(i(j :1CG/Ki1 i:;c \B• -rc-, . . rro I

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CTM ANAUTIUil LrlBS, LTD Laboratory Report

SW-846 METtiOD 8080 SW-846 METHOD 8080 SW-846 METHOD 8080 SW-846 METt!OD 1\130 SPI-846 METtiOD 8080 SW-846 METHOD 8080 STD. MEIH. :STH ED.2Q9A 93 'I

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Report PAGE 6

CTM ANAL'HICAL LABS, liD labor·atory Analysis Report

PAGE 7

GTM ArJALYTICAL LABS, LTD laboratory Anaiys1s

FAGE 8

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CTM Analytical Laboratories, Ltd. .~ 6!S~

NY 518-786-7100 FAX Si8-786-7139

GHTY & MillER. 11vC. AlBANY NY OFFICE

GERAGHTY & MILLER INC.

QA/QC Report

Project: Newell St.

Bill Gray

Taskno: 901024H

11/20/90

GC/MS GC I CAP Samp!1ng Serv1ces

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CTM Analytical Laboratories, Ltd.

CASE NARRAT:IVE

CTM Analytical Laboratories, Ltd. performed analyses on the following samples:

CTM LAB ID

901024H-Ol

901024H-02

901024H-03

901024H-04

901024H-OS

901024H-06

901024H-07

CLIENT ID

M0-3Wl

M0-3W2

M0-4Nl

MO-SEl

M0-6N3

M0-6Wl

M0-7N3

MATR:IX

SOIL

SOIL

SOIL

SOIL

SOIL

SOIL

SOIL

No problems were encountered during analyses with the following exception:

DATE SAMPLED

10/23/90

10/23/90

10/23/90

10/23/90

10/23/90

10/23/90

10/23/90

The spike recovery on sample MO-SEl 901024H-04 was out of quality control limits. The spiked sample contained Ar 12S4 and Ar 1260, which resulted in peak overlap with the spike compound. As a result, the spike recovery was high.

Please contact us, if you have any questions.

Thomas Mikulka, Ph.D. Laboratory Director

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Client Name: CTM Sample ID's:

Data Package Inspection

Geraghty & Miller, Inc. 901024H01-7

This data package received an inspection for completeness by the CTM Analytical Quality Assurance Officer. Any deficiencies found are included in the case Narrative of the report.

Inspected By: r~~ 3. 3~~ Date: ttt;._opo

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CTM ANALYTICAL LABORATORIES, LTD. VOLATILE ORGANICS

EPA METHOD 8240 GERAGHTY & MILLER, INC. 24 MADISON AVENUE EXT. ALBANY, NEW YORK 12203 ATTENTION: MR. BILL GRAY

Date Sampled sampled By: customer Id:

X XXX X xxxxx XX XXX

COMPOUND

CHLOROME'l'HANE VINYL CHLORIDE BROMOMETHANE CHLOROETHANE ACETONE 1,1-DICHLOROE'l'HANE METHYLENE CHLORIDE 'l'RANS-1,2-DICHLOROETHENE 1,1-DICHLOROETHENE M'l'BE CHLOROFORM 1,1,1-'l'RICHLOROE'l'HANE CARBON TETRACHLORIDE BENZENE 1,2-DICHLOROE'l'HANE TRICHLOROETHENE 1,2-DICHLOROPROPANE BROMODICHLOROMETHANE CARBON DISULFIDE 'l'RANS-1,3-DICHLOROPROPENE 'l'OLUENE CIS-1,3-DICHLOROPROPENE 1,1,2-'l'RICHLOROETHANE TE'l'RACHLOROETHENE DIBROMOCHLOROME'l'HANE CHLOROBENZENE ETHYL BENZENE BROMOFORM 1,1,2,2-'l'E'l'RACHLOROE'l'HANE METHYL ISO BUTYL KE'l'ONE VINYL ACETATE METHYL E'l'HYL KETONE 2-HEXANONE S'l'YRENE 0-XYLENES M&P-XYLENES 2-CHLOBOETHYLVINYLETHER P.Q.L. : PRACTICAL QUANTITATION ND=NO'l' DETECTED

RESULT

ND ND ND ND ND ND ND ND ND ND ND ND ND ND ND ND ND ND ND ND ND ND ND ND ND ND ND ND ND ND ND ND ND ND ND ND ND

LIMIT

CTM PROJECT f: CTM Task t:

CTM Sample No: Date Received: Date Run: Matrix:

P.Q.L. UNITS

10 MCG/L 10 MCG/L 10 MCG/L 10 MCG/L 10 MCG/L 10 MCG/L 5 MCG/L 5 MCG/L 5 MCG/L 5 MCG/L 5 MCG/L 5 MCG/L 5 MCG/L 5 MCG/L 5 MCG/L 5 MCG/L 5 MCG/L 5 MCG/L 5 MCG/L 5 MCG/L 5 MCG/L 5 MCG/L 5 MCG/L 5 MCG/L 5 5 MCG/L 5 MCG/L 5 MCG/L 5 MCG/L

10 MCG/L 10 MCG/L I 10 MCG/L 10 MCG/L 5 MCG/L 5 MCG/L 5 MCG/L 5 MCG/L

90.0426 90102411

BLANK XXX XX

11/5/90 DI WATER

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:

Date Run 11/5/90


CONTROL EPA METHOD 8240

COMPOUND SPIKE CONTROL CONTROL QUALITY ADDEO CONC. % CONTROL MCG/L MCG/L REC. LIMITS

CHLOROMETHANE so 56 112 0-273 VINYL CHLORIDE so 49 98 0-251 BROMO METHANE so 18 36 0-242 CHLOROETHAHE so 37 74 14-230 ACETONE so 16 32 * 1,1-0ICHLOROETBANE so 47 94 59-155 METHYLENE CHLORIDE so 63 126 0-221 TRAHS-1,2-0ICHLOROETHENE so 48 96 54-156 1,1-DICHLOROETHENE so 44 88 0-234 MTBE so 53 106 CHLOROFORM so 46 92 51-138 1,1,1-TRICHLOROETBANE so 44 88 52-162 CARBON TETRACHLORIDE so 45 90 70-140 BENZENE so 48 96 37-151 1,2-0ICHLOROETBANE so 44 88 49-155 TRICHLOROETHENE so 54 108 71-157 1,2-0ICHLOROPROPAHE so 49 98 0-210 BROMOOICHLOROMETHANE so 45 90 35-155 CARBON DISULFIDE so 43 86 * TRAHS-1,3-0ICHLOROPROPENE so 51 102 17-183 TOLUENE so 47 94 47-150 CIS-1,3-DICBLOROPROPENE so 47 94 0-227 1,1,2-TRICBLOROETBANE so 52 104 52-150 TETRACHLOROETHENE so 54 108 64-148 OIBROMOCHLOROMETBAHE so 55 110 53-149 CHLOROBENZENE so 48 96 37-160 ETHYL BENZENE so 47 94 37-162 BROMOFORM so 67 134 45-169 1 1 1 1 2 1 2-TETRACHLOROETBAHE so 54 108 46-157 METHYL ISO BUTYL KETONE so 73 146 * VINYL ACETATE so 59 118 * METHYL ETHYL KETONE so 66 132 * 2-HEXANONE so 64 128 * STYRENE so 44 88 * M&P-XYLEHES so 85 85 80-120 0-XYLEHES so 46 92 80-120 2-CHLOROETHYLVINYLETHER so 72 144 0-305 * NO LIMITS ARE LISTED UNDER METHOD. LIMITS ARE CURRENTLY

BEING ESTABLISHED iN THE LABORATORY. I NO=NOT DETECTED

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MATRIX SPIKE/MATRIX SPIKE DUPLICATE RECOVERY EPA ME'l'ltOD 82 4 0

SPIKED SAMPLE ID. DATE RUN

1029A-09 11/5/90

COMPOUND SPIKE ADDED

SAMPLE MS CONC. CONC.

MS %

MCG/lCG MCG/lCG MCG/lCG REC. 1,1-DICBLOROETHENE so ND 48 96 TRICBLOROETHENE so ND 53 106 BENZENE so ND so 100 TOLUENE so ND 49 98 CBLOROBENZENE so ND so 100

t

COMPOUND MSD MSD CONTROL CONC. % %

MCG/lCG REC. f RPD f RPD 1,1-DICBLOROETBENE 45 90 6 14 TRICBLOROETHENE 52 104 2 14 BENZENE 48 96 4 11 TOLUENE 49 98 0 13 CBLOROBENZENE 47 94 6 13

QC LIMITS

REC. 59-172 62-137 66-142 59-139 60-133

LIMITS

REC. 59-172 62-137 66-142 59-139 60-133

f COLUMN TO BE USED TO FLAG RECOVERY AND RPD VALUES WITH ASTERISJC

* VALUES OUTSIDE OF QC LIMITS

D=SPIKE COMPOUNDS DILUTED OUT

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CTM ANALYTICAL LABORATORIES, LTD.

Date Run 11/5/90

COST. ID

XXX XX xxxxx

M0-6W1 M0-7N3 SPIKE

SPIKE DOP

S1 (TOL) = S2 (BFB) = S3 (DCE) =

LAB ID

BLANK CONTROL

102411-06 102411-07

1029A-09MS 1029A-09MSD

TOLOENE-d8

VOLATILE ORGANICS SURROGATE RECOVERY

EPA METHOD 8240

S1 S2 S3 (TOL) f (BFB) f (DCE)

92 94 100 90 92 88 82 82 96 84 92 88 90 96 100 88 96 94

WATER

I

(88-110) BROMOFLOOROBENZENB (86-115) 1,2-DICHLOROETHANE-d4 (76-114)

I COLUMN TO BE USED TO FLAG RECOVERY VALUES

* VALUES OUTSIDE OF REQUIRED QC LIMITS

D SURROGATES DILUTED OUT

OTHER

QC LIMITS

TOTAL OUT

SOIL (81-117) (74-121) (70-121)

I

C'l'M ANALYTICAL LABORATORIES 1 LTD. VOLATILE ORGANICS

EPA METHOD 8240 GERAGHTY & MILLER, INC. 24 MADISON AVENUE EXT. ALBANY, NEW YORK 12203 ATTEH'l'ION: MR. BILL GRAY

Date sampled Sampled By: customer Id:

xxxxx XX XXX xxxxx

COMPOUND

CHLOROMETHANE VINYL CHLORIDE BROMOMBTHANE CHLOROE'l'HANE ACETONE 1,1-DICHLOROETHANE MB'l'HYLENE CHLORIDE TRAHS-1 1 2-DICHLOROE'l'HENE 1 1 1-DICHLOROE'l'HENE MTBE CHLOROFORM 1 1 1 1 1-TRICHLOROE'l'HANE CARBON TETRACHLORIDE BENZENE 1 1 2-DICHLOROETHANE TRICHLOROETHENE 1,2-DICHLOROPROPAHE BROMODICHLOROMETHAHE CARBON DISULFIDE TRANS-1 1 3-DICHLOROPROPENE TOLUENE CIS-1,3-DICHLOROPROPENE 1 1 1 1 2-TRICHLOROE'l'HANE TETRACHLOROETHEHE DIBROMOCHLOROME'l'HANE CHLOROBENZENE ETHYL BENZENE BROMOFORM 1 1 1,2,2-TETRACHLOROE'l'HANE ME'l'HYL ISO BUTYL KETONE VINYL ACETATE ME'l'HYL ETHYL KETONE 2-HEXANONE STYRENE 0-XYLENES M&P-XYLENES 2-CHLOROETHYLVINYLE'l'HER P.Q.L. = PRACTICAL QUAH'l'ITATION ND=NOT DETECTED

RESULT

ND ND ND ND

<P.Q.L. ND

<P.Q.L. ND ND ND ND ND ND ND ND ND ND ND ND ND ND ND ND ND ND ND ND ND ND ND ND ND ND ND ND ND ND

LIMIT

C'l'M PROJECT t : C'l'M Task t:

C'l'M Sample No: Date Received: Date Run: Matrix:

P.Q.L. UNITS

10 MCG/L 10 MCG/L 10 MCG/L 10 MCG/L 10 MCG/L 10 MCG/L 5 MCG/L 5 MCG/L 5 MCG/L 5 MCG/L 5 MCG/L 5 MCG/L 5 MCG/L 5 MCG/L< 5 MCG/L 5 MCG/L 5 MCG/L 5 MCG/L 5 MCG/L 5 MCG/L 5 MCG/L 5 MCG/L 5 MCG/L 5 MCG/L 5 MCG/L 5 MCG/L 5 MCG/L 5 MCG/L 5 MCG/L

10 MCG/L 10 MCG/L 10 tMCG/L 10 MCG/L 5 MCG/L 5 MCG/L 5 MCG/L 5 MCG/L

90.0426 901024H

BLANK xxxxx

11/6/90 DI WATER

I I I


Date Run 11/6/90

CU8T. ID

XXX XX M0-451

Sl (TOL) = S2 (BFB) = S3 (DCE) =

LAB ID

BLANK 1024H-03

TOLUEHE-d8

VOLATILE ORGANICS SURROGATE RECOVERY

EPA METKOD 8240

81 82 83 (TOL) I (BFB) I (DCE)

102 94 104 100 86 110

WATER

I

(88-110) BROMOFLUOROBEHZEHE (86-115) 1,2-DICBLOROETKANE-d4 (76-114)

f COLUMN TO BE USED TO FLAG RECOVERY VALUES

* VALUES OUTSIDE OF REQUIRED QC LIMITS

D SURROGATES DILUTED OUT

OTHER

QC LIMITS

TOTAL OUT

SOIL (81-117) (74-121) (70-121)


GERAGHTY & MILLER, INC. 24 MADISON AVENUE EXT. ALBANY, NY 12203 ATTENTION: MR. BILL GRAY

.• 1

Date Sampled: Sampled By: customer Id:

XX XXX xxxxx xxxxx

.1

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COMPOUND

AROCLOR-1016 AROCLOR-1221 AROCLOR-1232 AROCLOR-1242 AROCLOR-1248 AROCLOR-1254 AROCLOR-1260 P.Q.L. = PRACTICAL ND= NOT DETECTED

PCB'S EPA METHOD 8080

RESULT

ND ND ND ND ND ND ND

QUANTITATION LIMIT

CTM PROJECT #: CTM Task t:

CTM Sample No: Date Received: Date Ext. Date Run: ~atrix:

P.Q.L. UNITS

10 MCG/KG 10 MCG/KG 10 MCG/KG 10 MCG/KG 10 MCG/KG 10 MCG/KG 10 MCG/KG

90.0426 901024H

BLANK XX XXX

10/25/90 11/5/90

SOIL

, 11



Date sampled: xxxxx Sampled By: xxxxx customer Id: xxxxx

COMPOUND

AROCLOR-1016 AROCLOR-1221 AROCLOR-1232 AROCLOR-1242 AROCLOR-1248 AROCLOR-1254 AROCLOR-1260


RESULT


P.Q.L. = PRACTICAL QUANTITATION LIMIT ND= NOT DETECTED

CTM PROJECT t: CTM Task t:

CTM Sample No: Date Received: Date Ext. Date Run: Matrix:

P.Q.L. UNITS


90.0426 901024H

BLANK XX XXX

10/25/90 11/5/90

SOIL

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DATE RUN 11/9/90

COMPOUND


PCB'S CONTROL

EPA METHOD 8080

RESULT CONC.

MCG/ML 0.5 0.5 0.5 0.5 0.5 0.5 0.5

CONTROL CONC.

MCG/ML 0.50031 0.62401 0.47899 0.42698 0.38325 0.20052 0.3296

CONTROL EPA-608 % CONTROL

REC. LIMITS 100 50-114 125 15-178 96 10-215 85 39-150 77 38-158 40 29-131 66 8-128

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SPIKED SAMPLE ID. DATE RUN: DILUTION FACTOR:

PCB-1242

PCB-1242

CTM ANALYTICAL LABORATORIES, LTD. MATRIX SPIKE/ SPIKE DUPLICATE

PCB'S

COMPOUND

EPA METHOD 8080

1024H-04 11/7/90

1:100

SPIKE SAMPLE MS ADDED CONC. CONC.

MCG/ML MCG/ML MCG/ML 0.5195 0 13.8

COMPOUND MSD MSD CONC. % %

MCG/ML REC. t RPD t 12 2310 * 14

MS QC % LIMITS

REC. t REC. 2660 * 39-150

CONTROL LIMITS

RPD REC. 25 39-150

#COLUMN TO BE USED TO FLAG RECOVERY AND RPD VALUES WITH AN ASTERISK

* VALUES OUTSIDE OF QC LIMITS, SEE CASE NARRATIVE

D= SPIKE COMPOUNDS DILUTED OUT

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CASE NARRATIVE

CTM Analytical Laboratories, Ltd. performed analyses on the following samples:

CTM LAB ID

901008A-01

901008A-02

901008A-03

901008A-04

901008A-07

901008A-10

901008A-13

901008A-16

901008A-17

901008A-l.8

901008A-19

901.008A-22

901008A-25

901.008A-28

901.008A-30

901008A-31

CLIENT ID

M0-7N1

M0-7N2

M0-7N3

M0-7S1

M0-7W1

M0-7E1

M0-4N1

M0-4E1

M0-4E2

M0-4E3

M0-4W1

M0-4Sl.

M0-5S1

M0-5Wl

DP-2

MO-SNl

MATRIX

SOIL

SOIL

SOIL

SOIL

SOIL

SOIL

SOIL

SOIL

SOIL

SOIL

SOIL

SOIL

SOIL

SOIL

SOIL

SOIL

DATE SAMPLED

10/5/90

10/5/90

10/5/90

10/5/90

10/5/90

10/5/90

10/5/90

10/5/90

10/5/90

1.0/5/90

1.0/5/90

10/5/90

1.0/5/90

1.0/5/90

10/5/90

10/5/90

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901.008A-32 M0-5N2 SOIL 1.0/5/90

901.008A-33 M0-6Sl. SOIL 10/5/90

901008A-34 M0-6W1 SOIL 1.0/5/90

901.008A-35 M0-6W2 SOIL 1.0/5/90

901.008A-36 M0-6E3 SOIL 1.0/5/90

901008A-37 M0-6El. SOIL 1.0/5/90

901.008A-38 M0-6E2 SOIL 10/5/90

901008A-39 M0-6Nl. SOIL 1.0/5/90

901008A-40 M0-6N2 SOIL 10/5/90

901008A-41. M0-3E1 SOIL 10/5/90

901008A-44 M0-3S1 SOIL 1.0/5/90

901008A-46 M0-3Nl. SOIL 10/5/90

901008A-47 M0-3N2 SOIL 1.0/5/90

901.008A-48 M0-3N3 SOIL 1.0/5/90

No problems were encountered during analyses.

Due to the presence of Aroclors 1.254 and 1260, spiked samples M0-4Nl. (901024H-04), M0-7Nl. (901.008A-01), M0-4S1 (901.008A-022), M0-3N1 (90l.OOSA-46) and M0-3N2 (901008A-47) required dilutions for analysis. As a result, the Aroclor 1242 spike was diluted out resulting in neglegible recoveries. Since the spiking compound (Aroclor 1.242) was diluted out of the matrix spike duplicates, the concentrations of Aroclor 1254 attributed to the sample, are included in the QC package to show extraction precision.

Please contact us, if you have any questions.

Thomas Mikulka, Ph.D. Laboratory Director

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GERAGHTY & MILLER, INC. 24 MADISON AVENUE EXTENTION ALBANY, NY 12203 ATTENTION: MR. BILL GRAY


xxxxx xxxxx xxxxx

COMPOUND


ND= NOT DETECTED


RESULT


CTM PROJECT f: CTM Task f:


DET. UNITS LIMIT


90.0426 901008A

BLANK xxxxx

10/10/90 10/14/90

SOIL


15 PO Box Latham, New 12110

785·1805 785·0370

-GEAAGHTT & MllU:.r:;r · . .::. AlBi\NY. NY OFH"t

GERAGHTY & MILLER INC.

QA/QC Report

Project: GE Pittsfield, MA

Bill Gray

Taskno: 901008A

11/30/90

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GCIMS GC I CAP Samp!lng Serv1ces

J J J

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Client Name: CTM Sample ID's:

Data Package Inspection

Geraghty & Miller, Inc. 901008A01-4,7,10,13,16,17-l9,22,25,28,30-4l,

44,46-48

This data package received an inspection for completeness by the CTM Analytical Quality Assurance Officer. Any deficiencies found are included in the Case Narrative of the report.

Inspected By: 1? -.-..-L\.. B, B~J..rr-Date: ttl;.., II" '

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XXX XX xxxxx xxxxx

COMPOUND


ND: NOT DETECTED


RESULT




DET. LIMIT

10 10 10 10 10 10

UNITS

MCG/KG MCG/KG MCG/KG MCG/KG MCG/KG MCG/KG

10 MCG/KG

90.0426 901008A

BLANK xxxxx

10/10/90 10/14/90

SOIL



Date Sampled: XXX XX Sampled By: xxxxx customer Id: xxxxx

COMPOUND


ND= NOT DETECTED


RESULT


CTM PROJECT #: CTM Task #:


DET. UNITS LIMIT


90.0426 901008A

BLANK xxxxx

10/10/90 10/14/90

SOIL

I



Date Sampled: xxxxx Sampled By: xxxxx customer Id: xxxxx

COMPOUND


ND= NOT DETECTED


RESULT


CTM PROJECT f: C'l'M Task f :


DET. UNITS LIMIT


90.0426 901008A

BLANK xxxxx

10/11/90 10/14/90

SOIL

'l

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GERAGHTY & MILLER, INC. 2 4 MADISON AVENUE EXTENTION ALBANY, NY 12203 ATTENTION: MR. BILL GRAY


xxxxx xxxxx xxxxx

COMPOUND


NO: NOT DETECTED


RESULT

NO

NO NO NO NO NO NO



DET. UNITS LIMIT

10 MCG/KG 10 MCG~il 10 MCG/ 10 MCG/K 10 MCG/KG 10 MCG/KG 10 MCG/KG

90.0426 901008A

BLANK xxxxx

10/18/90 10/22/90

SOIL

J J



Date Sampled: xxxxx Sampled By: XX XXX customer Id: xxxxx

COMPOUND

AROCLOR-1016 AROCLOR-1221 AROCLOR-1232 AROCLOR-1242 AROCLOR-1248 AROCLOR-1254 AROCLOR-1260 P.Q.L. = PRACTICAL NO:NOT DETECTED


RESULT

NO NO NO NO NO NO NO

QUANTITATION LIMIT



P.Q.L. UNITS


90.0426 901108A

BLANK X XXX X

10/25/90 11/5/90

SOIL



Date Sampled: xxxxx Sampled By: xxxxx customer Id: xxxxx

COMPOUND

AROCLOR-1016 AROCLOR-1221 AROCLOR-1232 AROCLOR-1242 AROCLOR-1248 AROCLOR-1254 AROCLOR-12 6 0 P.Q.L. = PRACTICAL ND=NOT DETECTED

PCB'S EPA METHOD 808 0

RESULT


QUANTITATION LIMIT



P.Q.L. UNITS


90.0426 901108A

BLANK XXX XX

10/25/90 11/5/90

SOIL

J ]


DATE RUN 10/13/90

COMPOUND

AROCLOR-1016 AROCLOR-122l. AROCLOR-l.232 AROCLOR-3.242 AROCLOR-1248 AROCLOR-l.254 AROCLOR-1260

PCB'S CONTROL

EPA METHOD 8080

CONTROL CONC.

MCG/ML 0.5 0.5 0.5 0.5 0.5 0.5 0.5

RESULT CONC.

MCG/ML 0.56674 0.65521 0.55155 0.50943. 0.4281 0.5632 0.4836


REC. LIMITS 113 50-114 131 15-178 1l.O 10-215 102 39-150 86 38-158

113 29-131 97 8-128

I


DATE RUN 10/16/90

COMPOUND


PCB'S CONTROL

EPA METHOD 8090

CONTROL CONC.

MCG/ML 0.5 0.5 0.5 0.5 0.5 0.5 0.5

RESULT CONC.

MCG/ML 0.5716 0.6146 0.5119 0.6194 0.5299 0.5929 0.3395


REC. LIMITS 114 50-114 123 15-179 102 10-215 124 39-150 106 39-159 119 29-131 69 9-129

1

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DATE RUN 11/9/90

COMPOUND


PCB'S CONTROL

EPA ME'l'B:OD 8 0 8 0

CONTROL CONC.

MCG/ML 0.5 0.5 0.5 0.5 0.5 0.5 0.5

RESULT CONC.

MCG/ML 0.50031 0.62401 0.47899 0.42698 0.38325 0.20052 0.3296


REC. LIMITS 100 50-114 125 15-178 96 10-215 85 39-150 77 38-158 40 29-131 66 8-128

J ]


Latham. New 785·1805

785·0370


AROCLOR 1254 CONCENTRATIONS IN MATRIX SPIKE/MATRIX SPIKE DUPLICATE

CTM SAMPLE

ID

901008A-01 MS

901008A-01 MSD

901008A-22 MS

901008A-22 MSD

901008A-46 MS

901008A-46 MSD

901008A-47 MS

901008A-47 MSD

9010248-04 MS

9010248-04 MSD

DILUTION

1:500

1:500

1:50

1:50

1:500

1:500

1:100

1:100

1:100

1:100

CONC. OF

Ar1254

27,000 MCG/KG

19,000 MCG/KG

1,400 MCG/KG

1,200 MCG/KG

38,000 MCG/KG

41,000 MCG/KG

16,000 MCG/KG

21,000 MCG/KG

1,700 MCG/KG

1,800 MCG/KG

1

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PCB-1242

PCB-1242



1008A-01 10/22/90

1:500

COMPOUND SPIKE SAMPLE MS ADDED CONC. CONC.

MCG/KG MCG/KG MCG/KG 0.519 0 D


MCG/KG REC. i RPD i D D D

MS QC % LIMITS

REC. t REC. D 39-150

CONTROL LIMITS

RPD REC. 25 39-150





PCB-1242

PCB-1242


PCB'S

COMPOUND

EPA METHOD 8080

1008A-22 10/22/90

1:50




MCG/KG REC. f RPD f D D D

MS QC % LIMITS


CONTROL LIMITS

RPD REC. 25 39-150




l

1

I .

J


PCB-1242

PCB-1242


PCB'S

COMPOUND

EPA ME'l'HOD 8080

1008A-46 10/22/90

1:500




MCG/KG REC. t# RPD t# D D D

MS QC % LIMITS

REC. :f REC. D 39-150

CONTROL LIMITS

RPD REC. 25 39-150



D: SPIKE COMPOUNDS DILUTED OUT

1

1

]

1

J J

SPIKED SAMPLE ID. DATE RON: DILUTION FACTOR:

PCB-1242

PCB-1242


PCB'S

COMPOUND

EPA METHOD 8080

1008A-47 10/22/90

1:100




MCG/KG REC. # RPD # D D D

MS QC % LIMITS

REC. # REC. D 39-150

CONTROL LIMITS

RPD REC. 25 39-150





PCB-1242

PCB-1242


PCB'S

COMPOUND

EPA METHOD 8080

1024H-04 11/7/90

1:100




MCG/KG REC. # RPD # 12 D D

MS QC % LIMITS


CONTROL LIMITS

RPD REC. 25 39-150




short-term measures proposal, newell street site · company (ge) and the massachusetts department...

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