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PERFORMANCE EVALUATION 03-31-2016 49445626 WS16-1 Page 1 of 87 Scheduled Study WS16-1 49445626 27-Jan-2016 Through 17-Mar-2016 RTC Labcode WY00002 EPA Labcode Participating Laboratory: Energy Laboratories-Casper Donny Juarez PO Box 247 Casper WY 82602-0247 US Thank you for participating in study WS16-1. Additional information about this study may be found online at www.sigmaaldrich.com/pt. Sigma-Aldrich RTC Inc. 2931 Soldier Springs Road Laramie, WY 82070 USA 1-307-742-5452 www.sigmaaldrich.com This report shall not be reproduced except in full, without written approval of the laboratory. The data and results reported in this document are the property of the participating laboratory and are confidential. If you wish to appeal an evaluation listed in this report, please call our QA Supervisor at (307) 742-5452 or email [email protected] Sincerely, Jennifer Duhon Proficiency Testing Supervisor

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PERFORMANCE EVALUATION

03-31-2016 49445626 WS16-1 Page 1 of 87

Scheduled StudyWS16-1 4944562627-Jan-2016 Through 17-Mar-2016 RTC Labcode

WY00002EPA Labcode

Participating Laboratory:Energy Laboratories-CasperDonny JuarezPO Box 247Casper WY 82602-0247 US

Thank you for participating in study WS16-1. Additional information about this study may be found online atwww.sigmaaldrich.com/pt.

Sigma-Aldrich RTC Inc.2931 Soldier Springs RoadLaramie, WY 82070 USA1-307-742-5452www.sigmaaldrich.com

This report shall not be reproduced except in full, without written approval of the laboratory. The data andresults reported in this document are the property of the participating laboratory and are confidential. If youwish to appeal an evaluation listed in this report, please call our QA Supervisor at (307) 742-5452 or [email protected]

Sincerely,

Jennifer DuhonProficiency Testing Supervisor

WS16-1

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AccreditorsEvaluations of this dataset will be sent to the accreditor(s) listed below using your laboratory's labcode listed above eachaccrediting agency. If any of the information listed below is incorrect, please contact RTC immediately.

Accredating LabcodeFlorida Department of Health

Vanessa SotoActing Program AdministratorPO Box 2101217 Pearl StreetJacksonville FL 32231 US

Accredating LabcodeIdaho Bureau of Laboratories

Robert VoermansMicro Program2220 Old Penitentiary RoadBoise ID 83712 US

Accredating LabcodeNorth Dakota DOH

Cindy Auen2220 Old Penitentiary RoadBoise ID 83712 US

Accredating LabcodeNorth Dakota DOH

Marty HaroldsonDMR-QA Coordinator2220 Old Penitentiary RoadBoise ID 83712 US

Accredating LabcodeNebraska DEQ

Reuel AndersonDMR-QA Coordinator/Lab CertificationPO Box 98922Lincoln NE 68509-8922 US

Accredating LabcodeNew Mexico Environmental Department

Oneva PenaLaboratory Certification Coordinator - WSPO Box 98922Lincoln NE 68509-8922 US

Accredating LabcodeNevada DEP

Don LafaraDMRQA Coordinator

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901 S. Stewart StreetSte. 4001Carson City NV 89701 US

Accredating LabcodeOregon State Public Health Laboratory

Gary WardORELAP Administrator3150 NW 229th Ave.Ste. 100Hillsboro OR 97124-6536 US

Accredating LabcodeSouth Dakota DENR

Barbara FriedemanDrinking Water Acc.3150 NW 229th Ave.Ste. 100Hillsboro OR 97124-6536 US

Accredating LabcodeSouth Dakota DENR

Stacy EllwangerHealth Lab3150 NW 229th Ave.Ste. 100Hillsboro OR 97124-6536 US

Accredating LabcodeTexas CEQ

Susan SimonetDMR-QA CoordinatorQuality Assurance/Laboratory AccreditationPO Box 13087 (MC-176)Austin TX 78711-3087 US

Accredating LabcodeTexas CEQ

Frank JamisonPROGRAM MANAGERQuality Assurance/Laboratory AccreditationPO Box 13087 (MC-176)Austin TX 78711-3087 US

Accredating LabcodeUtah Bureau of Laboratory Improvement

Jill JonesLaboratory Certification Program4431 South 2700 WestTaylorsville UT 84119 US

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Accredating LabcodeWyoming DEQ

Steve VienLaboratory Supervisor208 South College DriveCheyenne WY 82002 US

Accredating LabcodeEPA Region 8

Monia Ben-KhaledDMR-QA Coordinator1595 Wynkoop StreetDenver CO 80202-1129 US

Accredating LabcodeNew Mexico Environmental Department

Barbara CooneyDMR-QA Coordinator1595 Wynkoop StreetDenver CO 80202-1129 US

Accredating LabcodeColorado DPHE

Eric MinkDMR-QA Coordinator4300 S Cherry Creek Drive South(WQCD-CADM B2)Denver CO 80246 US

Accredating LabcodeSouth Dakota DENR

Tim FlorSurface Water Acc.4300 S Cherry Creek Drive South(WQCD-CADM B2)Denver CO 80246 US

Accredating LabcodeColorado DPHE

Ben ChouafCertifcation Officer4300 S Cherry Creek Drive South(WQCD-CADM B2)Denver CO 80246 US

Accredating LabcodeEPA Region 8

Marcie TiddWaste Water/Drinking Water Certification1595 Wynkoop Street

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Denver CO 80202-1129 US

Accredating LabcodeMontana Dept. of Public Health & Human Services

Russell LeuPO Box 4369Helena MT 59604-4369 US

Accredating LabcodeWashington State Dept. of Ecology

Alan RueLab Accreditation Unit SupervisorPO Box 488Manchester WA 98353 US

Accredating LabcodeNevada DEP

Michelle NenzelLaboratory Certification Officer901 S. Stewart StreetSte. 4001Carson City NV 89701 US

Accredating LabcodeIdaho Bureau of Laboratories

Ernie BaderChemistry Program2220 Old Penitentiary RoadBoise ID 83712 US

Accredating LabcodeNebraska Health and Human Services System

Laurie WietingAssistant Lab Manager3701 S. 14th StreetLincoln NE 68502 US

RTC is accrediated to perform PT programs for the scope of accredation to ISO/IEC 17043under ACLASS certificate AP-1469

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Herbicides

Method:EPA 547 (1990) [10092009]

Analyte ResultUnits

AssignedValue

Accept.Window Z Evaluation

Glyphosate 1,2 383 ug/L 423 338 to 508 -0.95 Acceptable9411 / PE1435-2ML - Lot LRAB0399/Analyst:AA/ Analysis Date: 2016-03-06

Evaluation Criteria - 8Voluntary Evaluation Parameter - a:1, b:0, c:0.10, d:0

Method:EPA 549.2 1 (1997) [10093400]

Analyte ResultUnits

AssignedValue

Accept.Window Z Evaluation

Diquat 1,2 533 ug/L 28 14 to 42 72.14 Not Acceptable9390 / PE1435-2ML - Lot LRAB0399/Analyst:AA/ Analysis Date: 2016-03-08

Evaluation Criteria - 8Voluntary Evaluation Parameter - a:1, b:0, c:0.25, d:0

WS16-1

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Inorganic Disinfection By-Products

Method:EPA 300.0 2.1 (1993) [10053200]

Analyte ResultUnits

AssignedValue

Accept.Window Z Evaluation

Bromide 1,2 300 ug/L 325 276 to 374 -1.02 Acceptable1540 / PE3306-500ML - Lot LRAA8416/Analyst:AA/ Analysis Date: 2016-02-29

Evaluation Criteria - 8Voluntary Evaluation Parameter - a:1, b:0, c:0.075, d:0

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Microbiology

Method:SimPlate® (2000) [60032602]

Analyte ResultUnits

AssignedValue

Accept.Window Z Evaluation

Heterotrophic Plate Count, MPN 1,2 23.1 MPN 59.1 0 to 197 -0.52 Acceptable2555 / MIC002-2EA - Lot LRAB0419/Analyst:AA/ Analysis Date: 2016-03-02

Evaluation Criteria - 5Voluntary Evaluation Parameter - deviations:2

Method:SM 9223 B (Colilert® Quanti-Tray®) 21st ED (1997) [20211409]

Analyte Result Units AssignedValue

Accept.Window Z Evaluation

Coliforms, total - Sample 01 1,2 <1MPN/100mL 0 0 to 0 0 Acceptable

2500 / MIC001-MPN - Lot LRAB0424/Analyst:AA/ Analysis Date: 2016-03-02

Evaluation Criteria - 6Voluntary Evaluation Parameter - span:2

Coliforms, total - Sample 02 1,2 261.3MPN/100mL 340 10.6 to

669 -0.48 Acceptable

2500 / MIC001-MPN - Lot LRAB0424/Analyst:AA/ Analysis Date: 2016-03-02

Evaluation Criteria - 8Voluntary Evaluation Parameter - a:1, b:0, c:0, d:164.68

Coliforms, total - Sample 04 1,2 <1MPN/100mL 0 0 to 0 0 Acceptable

2500 / MIC001-MPN - Lot LRAB0424/Analyst:AA/ Analysis Date: 2016-03-02

Evaluation Criteria - 6Voluntary Evaluation Parameter - span:2

Coliforms, total - Sample 03 1,2 65.0MPN/100mL 69.7 23.9 to

116 -0.21 Acceptable

2500 / MIC001-MPN - Lot LRAB0424/Analyst:AA/ Analysis Date: 2016-03-02

Evaluation Criteria - 8Voluntary

Evaluation Parameter - a:0, b:69.7, c:0,d:22.9

Coliforms, total - Sample 05 1,2 72.7MPN/100mL 69.7 23.9 to

116 0.13 Acceptable

2500 / MIC001-MPN - Lot LRAB0424/Analyst:AA/ Analysis Date: 2016-03-02

Evaluation Criteria - 8Voluntary

Evaluation Parameter - a:0, b:69.7, c:0,d:22.9

Coliforms, total - Sample 06 1,2 307.6MPN/100mL 340 10.6 to

669 -0.2 Acceptable

2500 / MIC001-MPN - Lot LRAB0424/Analyst:AA/ Analysis Date: 2016-03-02

Evaluation Criteria - 8Voluntary Evaluation Parameter - a:1, b:0, c:0, d:164.68

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Coliforms, total - Sample 07 1,2 260.3MPN/100mL 340 10.6 to

669 -0.48 Acceptable

2500 / MIC001-MPN - Lot LRAB0424/Analyst:AA/ Analysis Date: 2016-03-02

Evaluation Criteria - 8Voluntary Evaluation Parameter - a:1, b:0, c:0, d:164.68

Coliforms, total - Sample 08 1,2 <1MPN/100mL 0 0 to 0 0 Acceptable

2500 / MIC001-MPN - Lot LRAB0424/Analyst:AA/ Analysis Date: 2016-03-02

Evaluation Criteria - 6Voluntary Evaluation Parameter - span:2

Coliforms, total - Sample 09 1,2 75.4MPN/100mL 69.7 23.9 to

116 0.25 Acceptable

2500 / MIC001-MPN - Lot LRAB0424/Analyst:AA/ Analysis Date: 2016-03-02

Evaluation Criteria - 8Voluntary

Evaluation Parameter - a:0, b:69.7, c:0,d:22.9

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Method:SM 9223 B (Colilert® Quanti-Tray®) 21st ED (1997) (Continued)

Analyte Result Units AssignedValue

Accept.Window Z Evaluation

Coliforms, total - Sample 10 1,2 <1MPN/100mL 0 0 to 0 0 Acceptable

2500 / MIC001-MPN - Lot LRAB0424/Analyst:AA/ Analysis Date: 2016-03-02

Evaluation Criteria - 6Voluntary Evaluation Parameter - span:2

E. Coli - Sample 01 1,2 <1MPN/100mL 0 0 to 0 0 Acceptable

2525 / MIC001-MPN - Lot LRAB0424/Analyst:AA/ Analysis Date: 2016-03-02

Evaluation Criteria - 6Voluntary Evaluation Parameter - span:2

E. Coli - Sample 02 1,2 <1MPN/100mL 0 0 to 0 0 Acceptable

2525 / MIC001-MPN - Lot LRAB0424/Analyst:AA/ Analysis Date: 2016-03-02

Evaluation Criteria - 6Voluntary Evaluation Parameter - span:2

E. Coli - Sample 03 1,2 59.1MPN/100mL 69.7 23.9 to

116 -0.46 Acceptable

2525 / MIC001-MPN - Lot LRAB0424/Analyst:AA/ Analysis Date: 2016-03-02

Evaluation Criteria - 8Voluntary

Evaluation Parameter - a:0, b:69.7, c:0,d:22.9

E. Coli - Sample 04 1,2 <1MPN/100mL 0 0 to 0 0 Acceptable

2525 / MIC001-MPN - Lot LRAB0424/Analyst:AA/ Analysis Date: 2016-03-02

Evaluation Criteria - 6Voluntary Evaluation Parameter - span:2

E. Coli - Sample 05 1,2 72.7MPN/100mL 69.7 23.9 to

116 0.13 Acceptable

2525 / MIC001-MPN - Lot LRAB0424/Analyst:AA/ Analysis Date: 2016-03-02

Evaluation Criteria - 8Voluntary

Evaluation Parameter - a:0, b:69.7, c:0,d:22.9

E. Coli - Sample 06 1,2 <1MPN/100mL 0 0 to 0 0 Acceptable

2525 / MIC001-MPN - Lot LRAB0424/Analyst:AA/ Analysis Date: 2016-03-02

Evaluation Criteria - 6Voluntary Evaluation Parameter - span:2

E. Coli - Sample 07 1,2 <1MPN/100mL 0 0 to 0 0 Acceptable

2525 / MIC001-MPN - Lot LRAB0424/Analyst:AA/ Analysis Date: 2016-03-02

Evaluation Criteria - 6Voluntary Evaluation Parameter - span:2

E. Coli - Sample 08 1,2 <1MPN/100mL 0 0 to 0 0 Acceptable

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2525 / MIC001-MPN - Lot LRAB0424/Analyst:AA/ Analysis Date: 2016-03-02

Evaluation Criteria - 6Voluntary Evaluation Parameter - span:2

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Method:SM 9223 B (Colilert® Quanti-Tray®) 21st ED (1997) (Continued)

Analyte Result Units AssignedValue

Accept.Window Z Evaluation

E. Coli - Sample 09 1,2 75.4MPN/100mL 69.7 23.9 to

116 0.25 Acceptable

2525 / MIC001-MPN - Lot LRAB0424/Analyst:AA/ Analysis Date: 2016-03-02

Evaluation Criteria - 8Voluntary

Evaluation Parameter - a:0, b:69.7, c:0,d:22.9

E. Coli - Sample 10 1,2 <1MPN/100mL 0 0 to 0 0 Acceptable

2525 / MIC001-MPN - Lot LRAB0424/Analyst:AA/ Analysis Date: 2016-03-02

Evaluation Criteria - 6Voluntary Evaluation Parameter - span:2

Method:SM 9223 B (Colilert®) 21st ED (1997) [20212402]

Analyte ResultUnits

AssignedValue

Accept.Window Z Evaluation

Coliforms, total - Sample 01 1,2 0 Units 0 0 to 0 0 Acceptable2500 / MIC001-PA - Lot LRAB0424/Analyst:AA/ Analysis Date: 2016-03-02

Evaluation Criteria - 8Voluntary Evaluation Parameter - a:1, b:0, c:0, d:0

Coliforms, total - Sample 02 1,2 1 Units 1 1 to 1 0 Acceptable2500 / MIC001-PA - Lot LRAB0424/Analyst:AA/ Analysis Date: 2016-03-02

Evaluation Criteria - 8Voluntary Evaluation Parameter - a:1, b:0, c:0, d:0

Coliforms, total - Sample 04 1,2 0 Units 0 0 to 0 0 Acceptable2500 / MIC001-PA - Lot LRAB0424/Analyst:AA/ Analysis Date: 2016-03-02

Evaluation Criteria - 8Voluntary Evaluation Parameter - a:1, b:0, c:0, d:0

Coliforms, total - Sample 03 1,2 1 Units 1 1 to 1 0 Acceptable2500 / MIC001-PA - Lot LRAB0424/Analyst:AA/ Analysis Date: 2016-03-02

Evaluation Criteria - 8Voluntary Evaluation Parameter - a:1, b:0, c:0, d:0

Coliforms, total - Sample 05 1,2 1 Units 1 1 to 1 0 Acceptable2500 / MIC001-PA - Lot LRAB0424/Analyst:AA/ Analysis Date: 2016-03-02

Evaluation Criteria - 8Voluntary Evaluation Parameter - a:1, b:0, c:0, d:0

Coliforms, total - Sample 06 1,2 1 Units 1 1 to 1 0 Acceptable2500 / MIC001-PA - Lot LRAB0424/Analyst:AA/ Analysis Date: 2016-03-02

Evaluation Criteria - 8Voluntary Evaluation Parameter - a:1, b:0, c:0, d:0

Coliforms, total - Sample 07 1,2 1 Units 1 1 to 1 0 Acceptable

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2500 / MIC001-PA - Lot LRAB0424/Analyst:AA/ Analysis Date: 2016-03-02

Evaluation Criteria - 8Voluntary Evaluation Parameter - a:1, b:0, c:0, d:0

Coliforms, total - Sample 08 1,2 0 Units 0 0 to 0 0 Acceptable2500 / MIC001-PA - Lot LRAB0424/Analyst:AA/ Analysis Date: 2016-03-02

Evaluation Criteria - 8Voluntary Evaluation Parameter - a:1, b:0, c:0, d:0

Coliforms, total - Sample 09 1,2 1 Units 1 1 to 1 0 Acceptable2500 / MIC001-PA - Lot LRAB0424/Analyst:AA/ Analysis Date: 2016-03-02

Evaluation Criteria - 8Voluntary Evaluation Parameter - a:1, b:0, c:0, d:0

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Method:SM 9223 B (Colilert®) 21st ED (1997) (Continued)

Analyte ResultUnits

AssignedValue

Accept.Window Z Evaluation

Coliforms, total - Sample 10 1,2 0 Units 0 0 to 0 0 Acceptable2500 / MIC001-PA - Lot LRAB0424/Analyst:AA/ Analysis Date: 2016-03-02

Evaluation Criteria - 8Voluntary Evaluation Parameter - a:1, b:0, c:0, d:0

E. Coli - Sample 01 1,2 0 Units 0 0 to 0 0 Acceptable2525 / MIC001-PA - Lot LRAB0424/Analyst:AA/ Analysis Date: 2016-03-02

Evaluation Criteria - 8Voluntary Evaluation Parameter - a:1, b:0, c:0, d:0

E. Coli - Sample 02 1,2 0 Units 0 0 to 0 0 Acceptable2525 / MIC001-PA - Lot LRAB0424/Analyst:AA/ Analysis Date: 2016-03-02

Evaluation Criteria - 8Voluntary Evaluation Parameter - a:1, b:0, c:0, d:0

E. Coli - Sample 03 1,2 1 Units 1 1 to 1 0 Acceptable2525 / MIC001-PA - Lot LRAB0424/Analyst:AA/ Analysis Date: 2016-03-02

Evaluation Criteria - 8Voluntary Evaluation Parameter - a:1, b:0, c:0, d:0

E. Coli - Sample 04 1,2 0 Units 0 0 to 0 0 Acceptable2525 / MIC001-PA - Lot LRAB0424/Analyst:AA/ Analysis Date: 2016-03-02

Evaluation Criteria - 8Voluntary Evaluation Parameter - a:1, b:0, c:0, d:0

E. Coli - Sample 05 1,2 1 Units 1 1 to 1 0 Acceptable2525 / MIC001-PA - Lot LRAB0424/Analyst:AA/ Analysis Date: 2016-03-02

Evaluation Criteria - 8Voluntary Evaluation Parameter - a:1, b:0, c:0, d:0

E. Coli - Sample 06 1,2 0 Units 0 0 to 0 0 Acceptable2525 / MIC001-PA - Lot LRAB0424/Analyst:AA/ Analysis Date: 2016-03-02

Evaluation Criteria - 8Voluntary Evaluation Parameter - a:1, b:0, c:0, d:0

E. Coli - Sample 07 1,2 0 Units 0 0 to 0 0 Acceptable2525 / MIC001-PA - Lot LRAB0424/Analyst:AA/ Analysis Date: 2016-03-02

Evaluation Criteria - 8Voluntary Evaluation Parameter - a:1, b:0, c:0, d:0

E. Coli - Sample 08 1,2 0 Units 0 0 to 0 0 Acceptable2525 / MIC001-PA - Lot LRAB0424/Analyst:AA/ Analysis Date: 2016-03-02

Evaluation Criteria - 8Voluntary Evaluation Parameter - a:1, b:0, c:0, d:0

WS16-1

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Method:SM 9223 B (Colilert®) 21st ED (1997) (Continued)

Analyte ResultUnits

AssignedValue

Accept.Window Z Evaluation

E. Coli - Sample 09 1,2 1 Units 1 1 to 1 0 Acceptable2525 / MIC001-PA - Lot LRAB0424/Analyst:AA/ Analysis Date: 2016-03-02

Evaluation Criteria - 8Voluntary Evaluation Parameter - a:1, b:0, c:0, d:0

E. Coli - Sample 10 1,2 0 Units 0 0 to 0 0 Acceptable2525 / MIC001-PA - Lot LRAB0424/Analyst:AA/ Analysis Date: 2016-03-02

Evaluation Criteria - 8Voluntary Evaluation Parameter - a:1, b:0, c:0, d:0

WS16-1

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Minerals

Method:EPA 200.7 4.4 (1994) [10013806]

Analyte ResultUnits

AssignedValue

Accept.Window Z Evaluation

Calcium, Ca 1,2 63.8 mg/L 62.2 52.9 to71.6 0.34 Acceptable

1035 / PE1304-1KT - Lot LRAA7326/Analyst:AA/ Analysis Date: 2016-02-12

Evaluation Criteria - 8Voluntary Evaluation Parameter - a:1, b:0, c:0.075, d:0

Magnesium, Mg 1,2 13.2 mg/L 13.2 11.2 to15.1 0 Acceptable

1085 / PE1304-1KT - Lot LRAA7326/Analyst:AA/ Analysis Date: 2016-02-12

Evaluation Criteria - 8Voluntary Evaluation Parameter - a:1, b:0, c:0.075, d:0

Potassium, K 1,2 16 mg/L 14.5 12.3 to16.6 1.39 Acceptable

1125 / PE1304-1KT - Lot LRAA7326/Analyst:AA/ Analysis Date: 2016-02-12

Evaluation Criteria - 8Voluntary Evaluation Parameter - a:1, b:0, c:0.075, d:0

Sodium, Na 1,2 16.7 mg/L 15.3 13 to 17.6 1.22 Acceptable1155 / PE1304-1KT - Lot LRAA7326/Analyst:AA/ Analysis Date: 2016-02-12

Evaluation Criteria - 8Voluntary Evaluation Parameter - a:1, b:0, c:0.075, d:0

Method:EPA 300.0 2.1 (1993) [10053200]

Analyte ResultUnits

AssignedValue

Accept.Window Z Evaluation

Chloride 1,2 113 mg/L 111 94.4 to 128 0.24 Acceptable1575 / PE1364-20ML - Lot LRAA9636/Analyst:AA/ Analysis Date: 2016-03-04

Evaluation Criteria - 8Voluntary Evaluation Parameter - a:1, b:0, c:0.075, d:0

Fluoride 1,2 1.76 mg/L 1.86 1.67 to2.05 -1.08 Acceptable

1730 / PE1364-20ML - Lot LRAA9636/Analyst:AA/ Analysis Date: 2016-03-04

Evaluation Criteria - 8Voluntary Evaluation Parameter - a:1, b:0, c:0.05, d:0

Sulfate 1,2 127 mg/L 126 107 to 145 0.11 Acceptable2000 / PE1364-20ML - Lot LRAA9636/Analyst:AA/ Analysis Date: 2016-03-04

Evaluation Criteria - 8Voluntary Evaluation Parameter - a:1, b:0, c:0.075, d:0

Method:SM 2340 B 21st ED (1997) [20046406]

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Analyte ResultUnits

AssignedValue

Accept.Window Z Evaluation

Calcium hardness as CaCO3 1,2 159 mg/L 155 132 to 179 0.34 Acceptable1550 / PE1304-1KT - Lot LRAA7326/Analyst:AA/ Analysis Date: 2016-02-16

Evaluation Criteria - 8Voluntary Evaluation Parameter - a:1, b:0, c:0.075, d:0

Hardness, total as CaCO3 1,2 214 mg/L 210 178 to 241 0.25 Acceptable

1755 / PE1304-1KT - Lot LRAA7326/Analyst:AA/ Analysis Date: 2016-02-16

Evaluation Criteria - 8Voluntary Evaluation Parameter - a:1, b:0, c:0.075, d:0

Method:SM 4500-F¯ C 22nd ED (2011) [20102210]

Analyte ResultUnits

AssignedValue

Accept.Window Z Evaluation

Fluoride 1,2 1.67 mg/L 1.86 1.67 to 2.05 -2.04 Acceptable1730 / PE1364-20ML - Lot LRAA9636/Analyst:AA/ Analysis Date: 2016-03-04

Evaluation Criteria - 8Voluntary Evaluation Parameter - a:1, b:0, c:0.05, d:0

Method:SM 4500-SO4¯ E 21st ED (1997) [20132825]

Analyte ResultUnits

AssignedValue

Accept.Window Z Evaluation

Sulfate 1,2 125 mg/L 126 107 to 145 -0.11 Acceptable2000 / PE1364-20ML - Lot LRAA9636/Analyst:AA/ Analysis Date: 2016-02-19

Evaluation Criteria - 8Voluntary Evaluation Parameter - a:1, b:0, c:0.075, d:0

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Miscellaneous Analytes

Method:EPA 200.7 4.4 (1994) [10013806]

Analyte ResultUnits

AssignedValue

Accept.Window Z Evaluation

Silica as SiO2 1,2 13.4 mg/L 13.6 11.6 to 15.6 -0.2 Acceptable

1990 / PE1350-20ML - Lot LRAA7196/Analyst:AA/ Analysis Date: 2016-02-12

Evaluation Criteria - 8Voluntary Evaluation Parameter - a:1, b:0, c:0.075, d:0

Method:EPA 200.8 5.4 (1994) [10014605]

Analyte ResultUnits

AssignedValue

Accept.Window Z Evaluation

Silica as SiO2 1,2 12.5 mg/L 13.6 11.6 to

15.6 -1.08 Acceptable

1990 / PE1350-20ML - Lot LRAA7196/Analyst:AA/ Analysis Date: 2016-02-12

Evaluation Criteria - 8Voluntary Evaluation Parameter - a:1, b:0, c:0.075, d:0

Uranium, U 1,2 22.7 ug/L 22.3 18.5 to26.2 0.21 Acceptable

3055 / PE1548-20ML - Lot LRAA4551/Analyst:AA/ Analysis Date: 2016-02-12

Evaluation Criteria - 8Voluntary

Evaluation Parameter - a:.9568, b:.1153,c:.0668, d:.3716

Method:EPA 245.7 2 (2005) [10038105]

Analyte ResultUnits

AssignedValue

Accept.Window Z Evaluation

Low Level Mercury 1,2 47.8 ng/L 50.5 35.4 to 65.7 -0.36 Acceptable1095 / PE1432-20ML - Lot LRAB0398/Analyst:AA/ Analysis Date: 2016-02-22

Evaluation Criteria - 8Voluntary Evaluation Parameter - a:1, b:0, c:0.15, d:0

Method:HACH 8021 [60003501]

Analyte ResultUnits

AssignedValue

Accept.Window Z Evaluation

Total residual chlorine 1,2 1.3 mg/L 1.05 0.88 to 1.21 3.03 Not Acceptable1940 / PE1450-2ML - Lot LRAA9443/Analyst:AA/ Analysis Date: 2016-03-10

Evaluation Criteria - 8Voluntary

Evaluation Parameter - a:1.0000, b:-0.0048,c:0.0723, d:0.0065

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Residual free chlorine 1,2 1 mg/L 1 0.8 to 1.2 0 Acceptable1945 / PE1450-2ML - Lot LRAA9443/Analyst:AA/ Analysis Date: 2016-03-10

Evaluation Criteria - 8Voluntary

Evaluation Parameter - a:1.0000, b:0.0004,c:0.0776, d:0.0246

Method:SM 2120 B 21st ED (2001) [20039003]

Analyte ResultUnits

AssignedValue

Accept.Window Z Evaluation

Color 1,2 30 Pt-CoUnits 30 20 to 40 0 Acceptable

1605 / PE1401-20ML - Lot LRAB0396/Analyst:AA/ Analysis Date: 2016-03-10

Evaluation Criteria - 8Voluntary Evaluation Parameter - a:1, b:0, c:0, d:5.0

Method:SM 2130 B 21st ED (2001) [20042608]

Analyte ResultUnits

AssignedValue

Accept.Window Z Evaluation

Turbidity 1,2 1.3 NTU 1.4 1.11 to 1.68 -0.69 Acceptable2055 / PE1342-2ML - Lot LRAA9244/Analyst:AA/ Analysis Date: 2016-03-10

Evaluation Criteria - 8Voluntary

Evaluation Parameter - a:0.9755, b:0.0593,c:0.0565, d:0.0661

Method:SM 2320 B 21st ED (1997) [20045403]

Analyte ResultUnits

AssignedValue

Accept.Window Z Evaluation

Alkalinity as CaCO3 1,2 38.3 mg/L 33.1 29.8 to 36.4 3.15 Not Acceptable

1505 / PE1304-1KT - Lot LRAA7326/Analyst:AA/ Analysis Date: 2016-03-09

Evaluation Criteria - 8Voluntary Evaluation Parameter - a:1, b:0, c:0.05, d:0

Method:SM 2330 B 21st ED (2000) [20003354]

Analyte ResultUnits

AssignedValue

Accept.Window Z Evaluation

Corrosivity 1,2 -0.165 SIUnits -0.24 -0.64 to

0.16 0.39 Acceptable

1620 / PE1304-1KT - Lot LRAA7326/Analyst:AA/ Analysis Date: 2016-03-11

Evaluation Criteria - 8Voluntary Evaluation Parameter - a:1, b:0, c:0, d:0.200

Method:SM 2510 B 21st ED (1997) [20048402]

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Analyte Result Units AssignedValue

Accept.Window Z Evaluation

Specific conductance, Conductivity (25ºC) 1,2 600umhos/cm 614 553 to 675 -0.46 Acceptable

1610 / PE1304-1KT - Lot LRAA7326/Analyst:AA/ Analysis Date: 2016-03-04

Evaluation Criteria - 8Voluntary Evaluation Parameter - a:1, b:0, c:0.05, d:0

Method:SM 2540 C 21st ED (1997) [20050208]

Analyte ResultUnits

AssignedValue

Accept.Window Z Evaluation

Total Dissolved Solids at 180ºC (TDS) 1,2 383 mg/L 424 339 to 509 -0.97 Acceptable1955 / PE1304-1KT - Lot LRAA7326/Analyst:AA/ Analysis Date: 2016-03-09

Evaluation Criteria - 8Voluntary Evaluation Parameter - a:1, b:0, c:0.10, d:0

Method:SM 3112 B 21st ED (1999) [20057801]

Analyte ResultUnits

AssignedValue

Accept.Window Z Evaluation

Low Level Mercury 1,2 0.0369ng/L 50.5 35.4 to

65.7 -6.66 Not Acceptable

1095 / PE1432-20ML - Lot LRAB0398/Analyst:AA/ Analysis Date: 2016-02-22

Evaluation Criteria - 8Voluntary Evaluation Parameter - a:1, b:0, c:0.15, d:0

Method:SM 4500-H+ B 22nd ED (2011) [20105015]

Analyte ResultUnits

AssignedValue

Accept.Window Z Evaluation

pH 1,2 4.18 Units 5.23 5.03 to 5.43 -10.5 Not Acceptable1900 / PE1368-20ML - Lot LRAB0390/Analyst:AA/ Analysis Date: 2016-03-04

Evaluation Criteria - 8Voluntary Evaluation Parameter - a:1, b:0, c:0, d:0.10

Method:SM 5310 C 21st ED (2000) [20138607]

Analyte ResultUnits

AssignedValue

Accept.Window Z Evaluation

Dissolved organic carbon (DOC) 1,2 11.2 mg/L 11.1 10 to 12.1 0.19 Acceptable1710 / PE1308-20ML - Lot LRAA7524/Analyst:AA/ Analysis Date: 2016-03-09

Evaluation Criteria - 8Voluntary

Evaluation Parameter - a:0.9744, b:0.0960,c:0.0402, d:0.0700

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Total organic carbon (TOC) 1,2 11.3 mg/L 11.3 9.01 to13.5 0 Acceptable

2040 / PE1308-20ML - Lot LRAA7524/Analyst:AA/ Analysis Date: 2016-03-09

Evaluation Criteria - 8Voluntary Evaluation Parameter - a:1, b:0, c:0.10, d:0

Method:SM 5540 C 22nd ED (2011) [20144814]

Analyte ResultUnits

AssignedValue

Accept.Window Z Evaluation

Surfactants - MBAS 1,2 0.322mg/L 0.28 0.17 to 0.39 0.82 Acceptable

2025 / PE1337-20ML - Lot LRAB0383/Analyst:AA/ Analysis Date: 2016-03-04

Evaluation Criteria - 8Voluntary

Evaluation Parameter - a:0.9804, b:0.0054,c:0.0673, d:0.0348

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Nutrients

Method:EPA 300.0 2.1 (1993) [10053200]

Analyte ResultUnits

AssignedValue

Accept.Window Z Evaluation

Nitrate as N 1,2 5.21 mg/L 5.25 4.73 to5.78 -0.15 Acceptable

1810 / PE1364-20ML - Lot LRAA9636/Analyst:AA/ Analysis Date: 2016-03-04

Evaluation Criteria - 8Voluntary Evaluation Parameter - a:1, b:0, c:0.05, d:0

Nitrate+nitrite as N 1,2 6.36 mg/L 6.42 5.46 to7.38 -0.12 Acceptable

1820 / PE1364-20ML - Lot LRAA9636/Analyst:AA/ Analysis Date: 2016-03-04

Evaluation Criteria - 8Voluntary Evaluation Parameter - a:1, b:0, c:0.075, d:0

Nitrite as N 1,2 1.15 mg/L 1.17 1 to 1.35 -0.23 Acceptable1840 / PE1364-20ML - Lot LRAA9636/Analyst:AA/ Analysis Date: 2016-03-04

Evaluation Criteria - 8Voluntary Evaluation Parameter - a:1, b:0, c:0.075, d:0

Orthophosphate as P 1,2 2.84 mg/L 2.8 2.38 to3.22 0.19 Acceptable

1870 / PE1364-20ML - Lot LRAA9636/Analyst:AA/ Analysis Date: 2016-03-04

Evaluation Criteria - 8Voluntary Evaluation Parameter - a:1, b:0, c:0.075, d:0

Method:EPA 353.2 (calc) [10238809]

Analyte ResultUnits

AssignedValue

Accept.Window Z Evaluation

Nitrate+nitrite as N 1,2 6.39 mg/L 6.42 5.46 to 7.38 -0.06 Acceptable1820 / PE1364-20ML - Lot LRAA9636/Analyst:AA/ Analysis Date: 2016-02-22

Evaluation Criteria - 8Voluntary Evaluation Parameter - a:1, b:0, c:0.075, d:0

Method:SM 4500-NO2¯ B 21st ED (2000) [20112805]

Analyte ResultUnits

AssignedValue

Accept.Window Z Evaluation

Nitrite as N 1,2 1.14 mg/L 1.17 1 to 1.35 -0.34 Acceptable1840 / PE1364-20ML - Lot LRAA9636/Analyst:AA/ Analysis Date: 2016-02-19

Evaluation Criteria - 8Voluntary Evaluation Parameter - a:1, b:0, c:0.075, d:0

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Organic Disinfection By-Products

Method:SM 2150 B 21st ED (1997) [20043601]

Analyte ResultUnits

AssignedValue

Accept.Window Z Evaluation

Odor 1,2 140 TON 105 0 to 225 0.88 Acceptable1855 / PE1133-500ML - Lot LRAB0561/Analyst:AA/ Analysis Date: 2016-03-10

Evaluation Criteria - 2Voluntary Evaluation Parameter - c:0, d:40

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Trace Metals - Drinking Water

Method:EPA 200.7 4.4 (1994) [10013806]

Analyte ResultUnits

AssignedValue

Accept.Window Z Evaluation

Antimony, Sb 1,2 <39.8 ug/L 18.8 13.2 to24.4 -6.67 Acceptable

1005 / PE1458-20ML - Lot LRAB0426/Analyst:AA/ Analysis Date: 2016-02-12

Evaluation Criteria - 8Voluntary Evaluation Parameter - a:1, b:0, c:0.15, d:0

Arsenic, As 1,2 <39.2 ug/L 28.6 20 to 37.2 -14.59 Acceptable1010 / PE1488-20ML - Lot LRAB0432/Analyst:AA/ Analysis Date: 2016-02-22

Evaluation Criteria - 3Voluntary Evaluation Parameter - percentage:0.30

Barium, Ba 1,2 1340 ug/L 1310 1110 to1510 0.31 Acceptable

1015 / PE1458-20ML - Lot LRAB0426/Analyst:AA/ Analysis Date: 2016-02-12

Evaluation Criteria - 8Voluntary Evaluation Parameter - a:1, b:0, c:0.075, d:0

Beryllium, Be 1,2 5.2 ug/L 5.11 4.34 to5.88 0.23 Acceptable

1020 / PE1488-20ML - Lot LRAB0432/Analyst:AA/ Analysis Date: 2016-02-12

Evaluation Criteria - 8Voluntary Evaluation Parameter - a:1, b:0, c:0.075, d:0

Boron, B 1,2 1570 ug/L 1540 1310 to1770 0.26 Acceptable

1025 / PE1458-20ML - Lot LRAB0426/Analyst:AA/ Analysis Date: 2016-02-12

Evaluation Criteria - 8Voluntary Evaluation Parameter - a:1, b:0, c:0.075, d:0

Cadmium, Cd 1,2 42.2 ug/L 39.6 31.7 to47.5 1.55 Acceptable

1030 / PE1488-20ML - Lot LRAB0432/Analyst:AA/ Analysis Date: 2016-02-12

Evaluation Criteria - 3Voluntary Evaluation Parameter - percentage:0.20

Chromium, Cr (total) 1,2 174 ug/L 169 144 to 194 0.58 Acceptable1040 / PE1488-20ML - Lot LRAB0432/Analyst:AA/ Analysis Date: 2016-02-12

Evaluation Criteria - 3Voluntary Evaluation Parameter - percentage:0.15

Cobalt, Co 1,2 167 ug/L 168 134 to 202 -0.06 Acceptable1050 / PE1448-20ML - Lot LRAA8373/Analyst:AA/ Analysis Date: 2016-02-12

Evaluation Criteria - 8Voluntary Evaluation Parameter - a:1, b:0, c:0.1, d:0

Copper, Cu 1,2 1160 ug/L 1150 1040 to1270 0.17 Acceptable

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1055 / PE1488-20ML - Lot LRAB0432/Analyst:AA/ Analysis Date: 2016-02-12

Evaluation Criteria - 8Voluntary Evaluation Parameter - a:1, b:0, c:0.05, d:0

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Method:EPA 200.7 4.4 (1994) (Continued)

Analyte ResultUnits

AssignedValue

Accept.Window Z Evaluation

Iron, Fe 1,2 1100 ug/L 1040 884 to1200 1.05 Acceptable

1070 / PE1488-20ML - Lot LRAB0432/Analyst:AA/ Analysis Date: 2016-02-12

Evaluation Criteria - 4Voluntary

Evaluation Parameter - break:250,highPercentage:0.15, lowPercentage:0.20

Lead, Pb 1,2 120 ug/L 81.4 57 to 106 9.51 Not Acceptable1075 / PE1488-20ML - Lot LRAB0432/Analyst:AA/ Analysis Date: 2016-02-18

Evaluation Criteria - 3Voluntary Evaluation Parameter - percentage:0.30

Manganese, Mn 1,2 643 ug/L 638 542 to 734 0.1 Acceptable1090 / PE1488-20ML - Lot LRAB0432/Analyst:AA/ Analysis Date: 2016-02-12

Evaluation Criteria - 8Voluntary Evaluation Parameter - a:1, b:0, c:0.075, d:0

Molybdenum, Mo 1,2 116 ug/L 116 98.6 to 133 0 Acceptable1100 / PE1458-20ML - Lot LRAB0426/Analyst:AA/ Analysis Date: 2016-02-12

Evaluation Criteria - 8Voluntary Evaluation Parameter - a:1, b:0, c:0.075, d:0

Nickel, Ni 1,2 355 ug/L 346 294 to 398 0.35 Acceptable1105 / PE1488-20ML - Lot LRAB0432/Analyst:AA/ Analysis Date: 2016-02-12

Evaluation Criteria - 8Voluntary Evaluation Parameter - a:1, b:0, c:0.075, d:0

Selenium, Se 1,2 71.5 ug/L 80 64 to 96 -1.06 Acceptable1140 / PE1488-20ML - Lot LRAB0432/Analyst:AA/ Analysis Date: 2016-02-12

Evaluation Criteria - 8Voluntary Evaluation Parameter - a:1, b:0, c:0.1, d:0

Silver, Ag 1,2 251 ug/L 239 167 to 311 0.33 Acceptable1150 / PE1458-20ML - Lot LRAB0426/Analyst:AA/ Analysis Date: 2016-02-18

Evaluation Criteria - 8Voluntary Evaluation Parameter - a:1, b:0, c:0.15, d:0

Strontium, Sr 1,2 171 ug/L 166 133 to 199 0.3 Acceptable1160 / PE1448-20ML - Lot LRAA8373/Analyst:AA/ Analysis Date: 2016-02-12

Evaluation Criteria - 8Voluntary Evaluation Parameter - a:1, b:0, c:0.1, d:0

Tin, Sn 1,2 541 ug/L 958 766 to1150 -4.35 Not Acceptable

1175 / PE1448-20ML - Lot LRAA8373/Analyst:AA/ Analysis Date: 2016-02-12

Evaluation Criteria - 8Voluntary Evaluation Parameter - a:1, b:0, c:0.1, d:0

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Method:EPA 200.7 4.4 (1994) (Continued)

Analyte ResultUnits

AssignedValue

Accept.Window Z Evaluation

Titanium, Ti 1,2 86 ug/L 90.9 72.7 to 109 -0.54 Acceptable1180 / PE1448-20ML - Lot LRAA8373/Analyst:AA/ Analysis Date: 2016-02-12

Evaluation Criteria - 8Voluntary Evaluation Parameter - a:1, b:0, c:0.1, d:0

Vanadium, V 1,2 2060 ug/L 2050 1740 to2360 0.06 Acceptable

1185 / PE1458-20ML - Lot LRAB0426/Analyst:AA/ Analysis Date: 2016-02-12

Evaluation Criteria - 8Voluntary Evaluation Parameter - a:1, b:0, c:0.075, d:0

Zinc, Zn 1,2 1320 ug/L 1300 1110 to1500 0.21 Acceptable

1190 / PE1488-20ML - Lot LRAB0432/Analyst:AA/ Analysis Date: 2016-02-12

Evaluation Criteria - 8Voluntary Evaluation Parameter - a:1, b:0, c:0.075, d:0

Aluminum, Al 1,2 726 ug/L 679 509 to 849 1 Acceptable1000 / PE1488-20ML - Lot LRAB0432/Analyst:AA/ Analysis Date: 2016-02-12

Evaluation Criteria - 4Voluntary

Evaluation Parameter - break:40,highPercentage:0.25, lowPercentage:0.30

Method:EPA 200.8 5.4 (1994) [10014605]

Analyte ResultUnits

AssignedValue

Accept.Window Z Evaluation

Antimony, Sb 1,2 19 ug/L 18.8 13.2 to24.4 0.07 Acceptable

1005 / PE1458-20ML - Lot LRAB0426/Analyst:AA/ Analysis Date: 2016-02-12

Evaluation Criteria - 8Voluntary Evaluation Parameter - a:1, b:0, c:0.15, d:0

Arsenic, As 1,2 31.1 ug/L 28.6 20 to 37.2 1.28 Acceptable1010 / PE1488-20ML - Lot LRAB0432/Analyst:AA/ Analysis Date: 2016-02-12

Evaluation Criteria - 3Voluntary Evaluation Parameter - percentage:0.30

Barium, Ba 1,2 1430 ug/L 1310 1110 to1510 1.22 Acceptable

1015 / PE1458-20ML - Lot LRAB0426/Analyst:AA/ Analysis Date: 2016-02-12

Evaluation Criteria - 8Voluntary Evaluation Parameter - a:1, b:0, c:0.075, d:0

Beryllium, Be 1,2 5.04 ug/L 5.11 4.34 to5.88 -0.18 Acceptable

1020 / PE1488-20ML - Lot LRAB0432/Analyst:AA/ Analysis Date: 2016-02-18

Evaluation Criteria - 8Voluntary Evaluation Parameter - a:1, b:0, c:0.075, d:0

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Boron, B 1,2 1580 ug/L 1540 1310 to1770 0.34 Acceptable

1025 / PE1458-20ML - Lot LRAB0426/Analyst:AA/ Analysis Date: 2016-02-12

Evaluation Criteria - 8Voluntary Evaluation Parameter - a:1, b:0, c:0.075, d:0

Cadmium, Cd 1,2 39.7 ug/L 39.6 31.7 to47.5 0.06 Acceptable

1030 / PE1488-20ML - Lot LRAB0432/Analyst:AA/ Analysis Date: 2016-02-12

Evaluation Criteria - 3Voluntary Evaluation Parameter - percentage:0.20

Chromium, Cr (total) 1,2 180 ug/L 169 144 to 194 1.29 Acceptable1040 / PE1488-20ML - Lot LRAB0432/Analyst:AA/ Analysis Date: 2016-02-12

Evaluation Criteria - 3Voluntary Evaluation Parameter - percentage:0.15

Cobalt, Co 1,2 172 ug/L 168 134 to 202 0.24 Acceptable1050 / PE1448-20ML - Lot LRAA8373/Analyst:AA/ Analysis Date: 2016-02-12

Evaluation Criteria - 8Voluntary Evaluation Parameter - a:1, b:0, c:0.1, d:0

Copper, Cu 1,2 1320 ug/L 1150 1040 to1270 2.96 Not Acceptable

1055 / PE1488-20ML - Lot LRAB0432/Analyst:AA/ Analysis Date: 2016-02-12

Evaluation Criteria - 8Voluntary Evaluation Parameter - a:1, b:0, c:0.05, d:0

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Method:EPA 200.8 5.4 (1994) (Continued)

Analyte ResultUnits

AssignedValue

Accept.Window Z Evaluation

Iron, Fe 1,2 1030 ug/L 1040 884 to1200 -0.18 Acceptable

1070 / PE1488-20ML - Lot LRAB0432/Analyst:AA/ Analysis Date: 2016-02-12

Evaluation Criteria - 4Voluntary

Evaluation Parameter - break:250,highPercentage:0.15, lowPercentage:0.20

Lead, Pb 1,2 83.2 ug/L 81.4 57 to 106 0.44 Acceptable1075 / PE1488-20ML - Lot LRAB0432/Analyst:AA/ Analysis Date: 2016-02-12

Evaluation Criteria - 3Voluntary Evaluation Parameter - percentage:0.30

Manganese, Mn 1,2 636 ug/L 638 542 to 734 -0.04 Acceptable1090 / PE1488-20ML - Lot LRAB0432/Analyst:AA/ Analysis Date: 2016-02-12

Evaluation Criteria - 8Voluntary Evaluation Parameter - a:1, b:0, c:0.075, d:0

Mercury, Hg 1,2 1.63 ug/L 1.58 1.11 to2.05 0.21 Acceptable

1095 / PE1488-20ML - Lot LRAB0432/Analyst:AA/ Analysis Date: 2016-02-12

Evaluation Criteria - 8Voluntary Evaluation Parameter - a:1, b:0, c:0.15, d:0

Molybdenum, Mo 1,2 110 ug/L 116 98.6 to 133 -0.69 Acceptable1100 / PE1458-20ML - Lot LRAB0426/Analyst:AA/ Analysis Date: 2016-02-12

Evaluation Criteria - 8Voluntary Evaluation Parameter - a:1, b:0, c:0.075, d:0

Nickel, Ni 1,2 370 ug/L 346 294 to 398 0.92 Acceptable1105 / PE1488-20ML - Lot LRAB0432/Analyst:AA/ Analysis Date: 2016-02-12

Evaluation Criteria - 8Voluntary Evaluation Parameter - a:1, b:0, c:0.075, d:0

Selenium, Se 1,2 81.8 ug/L 80 64 to 96 0.23 Acceptable1140 / PE1488-20ML - Lot LRAB0432/Analyst:AA/ Analysis Date: 2016-02-12

Evaluation Criteria - 8Voluntary Evaluation Parameter - a:1, b:0, c:0.1, d:0

Silver, Ag 1,2 176 ug/L 239 167 to 311 -1.75 Acceptable1150 / PE1458-20ML - Lot LRAB0426/Analyst:AA/ Analysis Date: 2016-02-18

Evaluation Criteria - 8Voluntary Evaluation Parameter - a:1, b:0, c:0.15, d:0

Strontium, Sr 1,2 178 ug/L 166 133 to 199 0.72 Acceptable1160 / PE1448-20ML - Lot LRAA8373/Analyst:AA/ Analysis Date: 2016-02-12

Evaluation Criteria - 8Voluntary Evaluation Parameter - a:1, b:0, c:0.1, d:0

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Method:EPA 200.8 5.4 (1994) (Continued)

Analyte ResultUnits

AssignedValue

Accept.Window Z Evaluation

Thallium, Tl 1,2 6.62 ug/L 8.01 5.61 to10.4 -1.16 Acceptable

1165 / PE1458-20ML - Lot LRAB0426/Analyst:AA/ Analysis Date: 2016-02-12

Evaluation Criteria - 8Voluntary Evaluation Parameter - a:1, b:0, c:0.15, d:0

Tin, Sn 1,2 560 ug/L 958 766 to1150 -4.15 Not Acceptable

1175 / PE1448-20ML - Lot LRAA8373/Analyst:AA/ Analysis Date: 2016-02-12

Evaluation Criteria - 8Voluntary Evaluation Parameter - a:1, b:0, c:0.1, d:0

Titanium, Ti 1,2 76.7 ug/L 90.9 72.7 to 109 -1.56 Acceptable1180 / PE1448-20ML - Lot LRAA8373/Analyst:AA/ Analysis Date: 2016-02-18

Evaluation Criteria - 8Voluntary Evaluation Parameter - a:1, b:0, c:0.1, d:0

Vanadium, V 1,2 2080 ug/L 2050 1740 to2360 0.19 Acceptable

1185 / PE1458-20ML - Lot LRAB0426/Analyst:AA/ Analysis Date: 2016-02-12

Evaluation Criteria - 8Voluntary Evaluation Parameter - a:1, b:0, c:0.075, d:0

Zinc, Zn 1,2 1390 ug/L 1300 1110 to1500 0.92 Acceptable

1190 / PE1488-20ML - Lot LRAB0432/Analyst:AA/ Analysis Date: 2016-02-12

Evaluation Criteria - 8Voluntary Evaluation Parameter - a:1, b:0, c:0.075, d:0

Aluminum, Al 1,2 663 ug/L 679 509 to 849 -0.34 Acceptable1000 / PE1488-20ML - Lot LRAB0432/Analyst:AA/ Analysis Date: 2016-02-18

Evaluation Criteria - 4Voluntary

Evaluation Parameter - break:40,highPercentage:0.25, lowPercentage:0.30

Method:EPA 245.1 3 (1994) [10036609]

Analyte ResultUnits

AssignedValue

Accept.Window Z Evaluation

Mercury, Hg 1,2 1.49 ug/L 1.58 1.11 to 2.05 -0.38 Acceptable1095 / PE1488-20ML - Lot LRAB0432/Analyst:AA/ Analysis Date: 2016-02-12

Evaluation Criteria - 8Voluntary Evaluation Parameter - a:1, b:0, c:0.15, d:0

Method:SM 3114 B 21st ED (1997) [20059807]

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Analyte ResultUnits

AssignedValue

Accept.Window Z Evaluation

Arsenic, As 1,2 33.6 ug/L 28.6 20 to 37.2 2.55 Acceptable1010 / PE1488-20ML - Lot LRAB0432/Analyst:AA/ Analysis Date: 2016-02-25

Evaluation Criteria - 3Voluntary Evaluation Parameter - percentage:0.30

Selenium, Se 1,2 81 ug/L 80 64 to 96 0.13 Acceptable1140 / PE1488-20ML - Lot LRAB0432/Analyst:AA/ Analysis Date: 2016-02-24

Evaluation Criteria - 8Voluntary Evaluation Parameter - a:1, b:0, c:0.1, d:0

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Trihalomethanes

Method:EPA 524.2 4.1 (1995) [10088809]

Analyte ResultUnits

AssignedValue

Accept.Window Z Evaluation

Total trihalomethanes 1,2 85.9 ug/L 91.1 54.7 to 128 -0.29 Acceptable5205 / PE1456-2ML - Lot LRAA0922/Analyst:AA/ Analysis Date: 2016-02-23

Evaluation Criteria - 8Voluntary Evaluation Parameter - a:1, b:0, c:0.20, d:0

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Volatile Organic Compounds(VOCs)

Method:EPA 504.1 1.1 (1995) [10082801]

Analyte ResultUnits

AssignedValue

Accept.Window Z Evaluation

1,2-Dibromo-3-chloropropane (DBCP) 1,2 1.17 ug/L 1.17 0.7 to 1.64 0 Acceptable4570 / PE1484-2ML - Lot LRAA9565/Analyst:AA/ Analysis Date: 2016-03-07

Evaluation Criteria - 8Voluntary Evaluation Parameter - a:1, b:0, c:0.20, d:0

1,2-Dibromoethane (EDB, Ethylene dibromide) 1,2 1.47 ug/L 1.22 0.73 to1.71 1.02 Acceptable

4585 / PE1484-2ML - Lot LRAA9565/Analyst:AA/ Analysis Date: 2016-03-07

Evaluation Criteria - 8Voluntary Evaluation Parameter - a:1, b:0, c:0.20, d:0

Method:EPA 524.2 4.1 (1995) [10088809]

Analyte ResultUnits

AssignedValue

Accept.Window Z Evaluation

Benzene 1,2 9.96 ug/L 10 8 to 12 -0.04 Acceptable4375 / PE1358-1KT - Lot LRAA7981/Analyst:AA/ Analysis Date: 2016-02-22

Evaluation Criteria - 4Voluntary

Evaluation Parameter - break:10,highPercentage:0.20, lowPercentage:0.40

Bromobenzene 1,2 19 ug/L 18 14.4 to21.6 0.69 Acceptable

4385 / PE1358-1KT - Lot LRAA7981/Analyst:AA/ Analysis Date: 2016-02-22

Evaluation Criteria - 4Voluntary

Evaluation Parameter - break:10,highPercentage:0.20, lowPercentage:0.40

Bromochloromethane 1,2 14.6 ug/L 14.1 11.2 to16.9 0.24 Acceptable

4390 / PE1358-1KT - Lot LRAA7981/Analyst:AA/ Analysis Date: 2016-02-22

Evaluation Criteria - 4Voluntary

Evaluation Parameter - break:10,highPercentage:0.20, lowPercentage:0.40

n-Butylbenzene 1,2 5.6 ug/L 5.33 3.2 to 7.46 0.56 Acceptable4435 / PE1358-1KT - Lot LRAA7981/Analyst:AA/ Analysis Date: 2016-02-22

Evaluation Criteria - 4Voluntary

Evaluation Parameter - break:10,highPercentage:0.20, lowPercentage:0.40

sec-Butylbenzene 1,2 8.4 ug/L 8.28 4.97 to11.6 0.17 Acceptable

4440 / PE1358-1KT - Lot LRAA7981/Analyst:AA/ Analysis Date: 2016-02-22

Evaluation Criteria - 4Voluntary

Evaluation Parameter - break:10,highPercentage:0.20, lowPercentage:0.40

tert-Butylbenzene 1,2 16.3 ug/L 17.6 14.1 to21.1 -0.88 Acceptable

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4445 / PE1358-1KT - Lot LRAA7981/Analyst:AA/ Analysis Date: 2016-02-22

Evaluation Criteria - 4Voluntary

Evaluation Parameter - break:10,highPercentage:0.20, lowPercentage:0.40

Carbon tetrachloride 1,2 8.28 ug/L 8.28 4.97 to11.6 0 Acceptable

4455 / PE1358-1KT - Lot LRAA7981/Analyst:AA/ Analysis Date: 2016-02-22

Evaluation Criteria - 4Voluntary

Evaluation Parameter - break:10,highPercentage:0.20, lowPercentage:0.40

Chlorobenzene 1,2 5.72 ug/L 5.85 3.51 to8.19 -0.24 Acceptable

4475 / PE1358-1KT - Lot LRAA7981/Analyst:AA/ Analysis Date: 2016-02-22

Evaluation Criteria - 4Voluntary

Evaluation Parameter - break:10,highPercentage:0.20, lowPercentage:0.40

Chloroethane 1,2 15.3 ug/L 12.7 7.64 to17.8 1.02 Acceptable

4485 / PE1358-1KT - Lot LRAA7981/Analyst:AA/ Analysis Date: 2016-02-22

Evaluation Criteria - 8Voluntary Evaluation Parameter - a:1, b:0, c:0.20, d:0

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Method:EPA 524.2 4.1 (1995) (Continued)

Analyte ResultUnits

AssignedValue

Accept.Window Z Evaluation

2-Chlorotoluene 1,2 10.5 ug/L 10.8 8.66 to 13 -0.24 Acceptable4535 / PE1358-1KT - Lot LRAA7981/Analyst:AA/ Analysis Date: 2016-02-22

Evaluation Criteria - 4Voluntary

Evaluation Parameter - break:10,highPercentage:0.20, lowPercentage:0.40

4-Chlorotoluene 1,2 12.3 ug/L 12.5 10 to 15 -0.16 Acceptable4540 / PE1358-1KT - Lot LRAA7981/Analyst:AA/ Analysis Date: 2016-02-22

Evaluation Criteria - 4Voluntary

Evaluation Parameter - break:10,highPercentage:0.20, lowPercentage:0.40

Dibromomethane 1,2 17.6 ug/L 16.3 13 to 19.5 0.92 Acceptable4595 / PE1358-1KT - Lot LRAA7981/Analyst:AA/ Analysis Date: 2016-02-22

Evaluation Criteria - 4Voluntary

Evaluation Parameter - break:10,highPercentage:0.20, lowPercentage:0.40

1,2-Dichlorobenzene 1,2 16.6 ug/L 16.2 13 to 19.5 0.28 Acceptable4610 / PE1358-1KT - Lot LRAA7981/Analyst:AA/ Analysis Date: 2016-02-22

Evaluation Criteria - 4Voluntary

Evaluation Parameter - break:10,highPercentage:0.20, lowPercentage:0.40

1,3-Dichlorobenzene 1,2 12.6 ug/L 13.1 10.5 to15.7 -0.51 Acceptable

4615 / PE1358-1KT - Lot LRAA7981/Analyst:AA/ Analysis Date: 2016-02-22

Evaluation Criteria - 4Voluntary

Evaluation Parameter - break:10,highPercentage:0.20, lowPercentage:0.40

1,4-Dichlorobenzene 1,2 13.8 ug/L 14.6 11.6 to17.5 -0.59 Acceptable

4620 / PE1358-1KT - Lot LRAA7981/Analyst:AA/ Analysis Date: 2016-02-22

Evaluation Criteria - 4Voluntary

Evaluation Parameter - break:10,highPercentage:0.20, lowPercentage:0.40

Dichlorodifluoromethane 1,2 8.88 ug/L 8.94 5.36 to12.5 -0.03 Acceptable

4625 / PE1358-1KT - Lot LRAA7981/Analyst:AA/ Analysis Date: 2016-02-22

Evaluation Criteria - 8Voluntary Evaluation Parameter - a:1, b:0, c:0.20, d:0

1,1-Dichloroethane 1,2 5.24 ug/L 5.3 3.18 to7.42 -0.07 Acceptable

4630 / PE1358-1KT - Lot LRAA7981/Analyst:AA/ Analysis Date: 2016-02-22

Evaluation Criteria - 4Voluntary

Evaluation Parameter - break:10,highPercentage:0.20, lowPercentage:0.40

1,2-Dichloroethane 1,2 4.2 ug/L 4.15 2.49 to5.81 0.09 Acceptable

4635 / PE1358-1KT - Lot LRAA7981/Analyst:AA/ Analysis Date: 2016-02-22

Evaluation Criteria - 4Voluntary

Evaluation Parameter - break:10,highPercentage:0.20, lowPercentage:0.40

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Method:EPA 524.2 4.1 (1995) (Continued)

Analyte ResultUnits

AssignedValue

Accept.Window Z Evaluation

1,1-Dichloroethylene 1,2 4.88 ug/L 6.12 3.67 to8.57 -1.56 Acceptable

4640 / PE1358-1KT - Lot LRAA7981/Analyst:AA/ Analysis Date: 2016-02-22

Evaluation Criteria - 4Voluntary

Evaluation Parameter - break:10,highPercentage:0.20, lowPercentage:0.40

cis-1,2-Dichloroethylene 1,2 14.8 ug/L 15.9 12.7 to19.1 -0.71 Acceptable

4645 / PE1358-1KT - Lot LRAA7981/Analyst:AA/ Analysis Date: 2016-02-22

Evaluation Criteria - 4Voluntary

Evaluation Parameter - break:10,highPercentage:0.20, lowPercentage:0.40

1,2-Dichloropropane 1,2 15.4 ug/L 14.6 11.7 to17.5 0.61 Acceptable

4655 / PE1358-1KT - Lot LRAA7981/Analyst:AA/ Analysis Date: 2016-02-22

Evaluation Criteria - 4Voluntary

Evaluation Parameter - break:10,highPercentage:0.20, lowPercentage:0.40

1,3-Dichloropropane 1,2 10.5 ug/L 9.95 5.97 to13.9 0.7 Acceptable

4660 / PE1358-1KT - Lot LRAA7981/Analyst:AA/ Analysis Date: 2016-02-22

Evaluation Criteria - 4Voluntary

Evaluation Parameter - break:10,highPercentage:0.20, lowPercentage:0.40

2,2-Dichloropropane 1,2 10.8 ug/L 10.9 8.69 to 13 -0.06 Acceptable4665 / PE1358-1KT - Lot LRAA7981/Analyst:AA/ Analysis Date: 2016-02-22

Evaluation Criteria - 4Voluntary

Evaluation Parameter - break:10,highPercentage:0.20, lowPercentage:0.40

1,1-Dichloropropene 1,2 14.6 ug/L 14.7 11.8 to17.7 -0.04 Acceptable

4670 / PE1358-1KT - Lot LRAA7981/Analyst:AA/ Analysis Date: 2016-02-22

Evaluation Criteria - 4Voluntary

Evaluation Parameter - break:10,highPercentage:0.20, lowPercentage:0.40

cis-1,3-Dichloropropene 1,2 13 ug/L 13.7 10.9 to16.4 -0.53 Acceptable

4680 / PE1358-1KT - Lot LRAA7981/Analyst:AA/ Analysis Date: 2016-02-22

Evaluation Criteria - 4Voluntary

Evaluation Parameter - break:10,highPercentage:0.20, lowPercentage:0.40

trans-1,3-Dichloropropene 1,2 14.6 ug/L 14.1 11.3 to 17 0.36 Acceptable4685 / PE1358-1KT - Lot LRAA7981/Analyst:AA/ Analysis Date: 2016-02-22

Evaluation Criteria - 4Voluntary

Evaluation Parameter - break:10,highPercentage:0.20, lowPercentage:0.40

trans-1,2-Dichloroethylene 1,2 6.96 ug/L 8.08 4.85 to11.3 -1.03 Acceptable

4700 / PE1358-1KT - Lot LRAA7981/Analyst:AA/ Analysis Date: 2016-02-22

Evaluation Criteria - 4Voluntary

Evaluation Parameter - break:10,highPercentage:0.20, lowPercentage:0.40

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Method:EPA 524.2 4.1 (1995) (Continued)

Analyte ResultUnits

AssignedValue

Accept.Window Z Evaluation

Ethylbenzene 1,2 7.72 ug/L 7.45 4.47 to10.4 0.4 Acceptable

4765 / PE1358-1KT - Lot LRAA7981/Analyst:AA/ Analysis Date: 2016-02-22

Evaluation Criteria - 4Voluntary

Evaluation Parameter - break:10,highPercentage:0.20, lowPercentage:0.40

Hexachlorobutadiene 1,2 15.9 ug/L 16.5 13.2 to19.8 -0.36 Acceptable

4835 / PE1358-1KT - Lot LRAA7981/Analyst:AA/ Analysis Date: 2016-02-22

Evaluation Criteria - 4Voluntary

Evaluation Parameter - break:10,highPercentage:0.20, lowPercentage:0.40

Isopropylbenzene 1,2 15 ug/L 15.5 12.4 to18.6 -0.31 Acceptable

4900 / PE1358-1KT - Lot LRAA7981/Analyst:AA/ Analysis Date: 2016-02-22

Evaluation Criteria - 4Voluntary

Evaluation Parameter - break:10,highPercentage:0.20, lowPercentage:0.40

4-Isopropyltoluene 1,2 18.4 ug/L 18.2 14.6 to21.9 0.18 Acceptable

4910 / PE1358-1KT - Lot LRAA7981/Analyst:AA/ Analysis Date: 2016-02-22

Evaluation Criteria - 4Voluntary

Evaluation Parameter - break:10,highPercentage:0.20, lowPercentage:0.40

Methyl bromide (Bromomethane) 1,2 18.4 ug/L 22.9 13.7 to 32 -0.98 Acceptable4950 / PE1358-1KT - Lot LRAA7981/Analyst:AA/ Analysis Date: 2016-02-22

Evaluation Criteria - 8Voluntary Evaluation Parameter - a:1, b:0, c:0.20, d:0

Methyl chloride (Chloromethane) 1,2 16.7 ug/L 21.4 12.8 to 30 -1.1 Acceptable4960 / PE1358-1KT - Lot LRAA7981/Analyst:AA/ Analysis Date: 2016-02-22

Evaluation Criteria - 8Voluntary Evaluation Parameter - a:1, b:0, c:0.20, d:0

Methylene chloride (Dichloromethane) 1,2 16.8 ug/L 17.8 14.2 to21.3 -0.44 Acceptable

4975 / PE1358-1KT - Lot LRAA7981/Analyst:AA/ Analysis Date: 2016-02-22

Evaluation Criteria - 4Voluntary

Evaluation Parameter - break:10,highPercentage:0.20, lowPercentage:0.40

Methyl tert-butyl ether (MTBE) 1,2 23.2 ug/L 16.9 13.5 to20.3 1.97 Not Acceptable

5000 / PE1358-1KT - Lot LRAA7981/Analyst:AA/ Analysis Date: 2016-02-22

Evaluation Criteria - 4Voluntary

Evaluation Parameter - break:10,highPercentage:0.20, lowPercentage:0.40

Naphthalene 1,2 28.3 ug/L 28.5 19.9 to 37 -0.06 Acceptable5005 / PE1358-1KT - Lot LRAA7981/Analyst:AA/ Analysis Date: 2016-02-22

Evaluation Criteria - 4Voluntary

Evaluation Parameter - break:10,highPercentage:0.30, lowPercentage:0.40

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Method:EPA 524.2 4.1 (1995) (Continued)

Analyte ResultUnits

AssignedValue

Accept.Window Z Evaluation

n-Propylbenzene (1-Phenylpropane) 1,2 9.12 ug/L 9.7 5.82 to13.6 -0.5 Acceptable

5090 / PE1358-1KT - Lot LRAA7981/Analyst:AA/ Analysis Date: 2016-02-22

Evaluation Criteria - 4Voluntary

Evaluation Parameter - break:10,highPercentage:0.20, lowPercentage:0.40

Styrene 1,2 8 ug/L 7.97 4.78 to11.2 0.06 Acceptable

5100 / PE1358-1KT - Lot LRAA7981/Analyst:AA/ Analysis Date: 2016-02-22

Evaluation Criteria - 4Voluntary

Evaluation Parameter - break:10,highPercentage:0.20, lowPercentage:0.40

1,1,1,2-Tetrachloroethane 1,2 6.8 ug/L 6.7 4.02 to9.38 0.14 Acceptable

5105 / PE1358-1KT - Lot LRAA7981/Analyst:AA/ Analysis Date: 2016-02-22

Evaluation Criteria - 4Voluntary

Evaluation Parameter - break:10,highPercentage:0.20, lowPercentage:0.40

1,1,2,2-Tetrachloroethane 1,2 11.4 ug/L 12.9 10.3 to15.5 -1.23 Acceptable

5110 / PE1358-1KT - Lot LRAA7981/Analyst:AA/ Analysis Date: 2016-02-22

Evaluation Criteria - 4Voluntary

Evaluation Parameter - break:10,highPercentage:0.20, lowPercentage:0.40

Tetrachloroethylene (Perchloroethylene) 1,2 17 ug/L 16.4 13.2 to19.7 0.4 Acceptable

5115 / PE1358-1KT - Lot LRAA7981/Analyst:AA/ Analysis Date: 2016-02-22

Evaluation Criteria - 4Voluntary

Evaluation Parameter - break:10,highPercentage:0.20, lowPercentage:0.40

Toluene 1,2 13.8 ug/L 13 10.4 to15.6 1.02 Acceptable

5140 / PE1358-1KT - Lot LRAA7981/Analyst:AA/ Analysis Date: 2016-02-22

Evaluation Criteria - 4Voluntary

Evaluation Parameter - break:10,highPercentage:0.20, lowPercentage:0.40

1,2,3-Trichlorobenzene 1,2 32.3 ug/L 32.5 26 to 39 -0.05 Acceptable5150 / PE1358-1KT - Lot LRAA7981/Analyst:AA/ Analysis Date: 2016-02-22

Evaluation Criteria - 4Voluntary

Evaluation Parameter - break:10,highPercentage:0.20, lowPercentage:0.40

1,2,4-Trichlorobenzene 1,2 9.32 ug/L 9.61 5.77 to13.5 -0.4 Acceptable

5155 / PE1358-1KT - Lot LRAA7981/Analyst:AA/ Analysis Date: 2016-02-22

Evaluation Criteria - 4Voluntary

Evaluation Parameter - break:10,highPercentage:0.20, lowPercentage:0.40

1,1,1-Trichloroethane 1,2 7.36 ug/L 7.61 4.57 to10.7 -0.2 Acceptable

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5160 / PE1358-1KT - Lot LRAA7981/Analyst:AA/ Analysis Date: 2016-02-22

Evaluation Criteria - 4Voluntary

Evaluation Parameter - break:10,highPercentage:0.20, lowPercentage:0.40

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Method:EPA 524.2 4.1 (1995) (Continued)

Analyte ResultUnits

AssignedValue

Accept.Window Z Evaluation

1,1,2-Trichloroethane 1,2 11 ug/L 10.3 8.21 to12.3 0.79 Acceptable

5165 / PE1358-1KT - Lot LRAA7981/Analyst:AA/ Analysis Date: 2016-02-22

Evaluation Criteria - 4Voluntary

Evaluation Parameter - break:10,highPercentage:0.20, lowPercentage:0.40

Trichloroethene (Trichloroethylene) 1,2 14.8 ug/L 14.7 11.7 to17.6 0.06 Acceptable

5170 / PE1358-1KT - Lot LRAA7981/Analyst:AA/ Analysis Date: 2016-02-22

Evaluation Criteria - 4Voluntary

Evaluation Parameter - break:10,highPercentage:0.20, lowPercentage:0.40

Trichlorofluoromethane 1,2 20.2 ug/L 24.5 14.7 to34.3 -0.88 Acceptable

5175 / PE1358-1KT - Lot LRAA7981/Analyst:AA/ Analysis Date: 2016-02-22

Evaluation Criteria - 8Voluntary Evaluation Parameter - a:1, b:0, c:0.20, d:0

1,2,3-Trichloropropane 1,2 16.9 ug/L 17.3 13.8 to20.7 -0.19 Acceptable

5180 / PE1358-1KT - Lot LRAA7981/Analyst:AA/ Analysis Date: 2016-02-22

Evaluation Criteria - 4Voluntary

Evaluation Parameter - break:10,highPercentage:0.20, lowPercentage:0.40

1,2,4-Trimethylbenzene 1,2 17.1 ug/L 16.9 13.5 to20.2 0.22 Acceptable

5210 / PE1358-1KT - Lot LRAA7981/Analyst:AA/ Analysis Date: 2016-02-22

Evaluation Criteria - 4Voluntary

Evaluation Parameter - break:10,highPercentage:0.20, lowPercentage:0.40

1,3,5-Trimethylbenzene 1,2 15.1 ug/L 15 12 to 18 0.06 Acceptable5215 / PE1358-1KT - Lot LRAA7981/Analyst:AA/ Analysis Date: 2016-02-22

Evaluation Criteria - 4Voluntary

Evaluation Parameter - break:10,highPercentage:0.20, lowPercentage:0.40

Vinyl chloride 1,2 5.2 ug/L 5.1 3.06 to7.14 0.1 Acceptable

5235 / PE1358-1KT - Lot LRAA7981/Analyst:AA/ Analysis Date: 2016-02-22

Evaluation Criteria - 8Voluntary Evaluation Parameter - a:1, b:0, c:0.20, d:0

m+p-Xylene 1,2 13.3 ug/L 13 10.3 to15.6 0.23 Acceptable

5240 / PE1358-1KT - Lot LRAA7981/Analyst:AA/ Analysis Date: 2016-02-22

Evaluation Criteria - 5Voluntary Evaluation Parameter - deviations:2

o-Xylene 1,2 19 ug/L 18.1 15.7 to20.4 0.76 Acceptable

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5250 / PE1358-1KT - Lot LRAA7981/Analyst:AA/ Analysis Date: 2016-02-22

Evaluation Criteria - 5Voluntary Evaluation Parameter - deviations:2

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Method:EPA 524.2 4.1 (1995) (Continued)

Analyte ResultUnits

AssignedValue

Accept.Window Z Evaluation

Xylene, total 1,2 32.3 ug/L 30 24 to 36 1.39 Acceptable5260 / PE1358-1KT - Lot LRAA7981/Analyst:AA/ Analysis Date: 2016-02-22

Evaluation Criteria - 4Voluntary

Evaluation Parameter - break:10,highPercentage:0.20, lowPercentage:0.40

Group Analysis SummaryAcceptable : 56 / 57Score : 98.25% - (Acceptable)

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Volatile Organic Compounds(VOCs)

Method:EPA 504.1 1.1 (1995) [10082801]

Analyte ResultUnits

AssignedValue

Accept.Window Z Evaluation

1,2,3-Trichloropropane 1,2 2.47 ug/L 1.42 0.85 to 1.99 3.7 Not Acceptable5180 / PE1484-2ML - Lot LRAA9565/Analyst:AA/ Analysis Date: 2016-03-07

Evaluation Criteria - 8Voluntary Evaluation Parameter - a:1, b:0, c:0.2, d:0

Method:EPA 524.2 4.1 (1995) [10088809]

Analyte ResultUnits

AssignedValue

Accept.Window Z Evaluation

Bromodichloromethane 1,2 28.1 ug/L 32 25.6 to38.4 -1.22 Acceptable

4395 / PE1456-2ML - Lot LRAA0922/Analyst:AA/ Analysis Date: 2016-02-23

Evaluation Criteria - 8Voluntary Evaluation Parameter - a:1, b:0, c:0.10, d:0

Bromoform 1,2 19.3 ug/L 18.2 14.6 to21.8 0.6 Acceptable

4400 / PE1456-2ML - Lot LRAA0922/Analyst:AA/ Analysis Date: 2016-02-23

Evaluation Criteria - 8Voluntary Evaluation Parameter - a:1, b:0, c:0.10, d:0

Chloroform 1,2 22.7 ug/L 25.6 20.5 to30.7 -1.13 Acceptable

4505 / PE1456-2ML - Lot LRAA0922/Analyst:AA/ Analysis Date: 2016-02-23

Evaluation Criteria - 8Voluntary Evaluation Parameter - a:1, b:0, c:0.10, d:0

Dibromochloromethane 1,2 15.8 ug/L 15.2 12.2 to18.2 0.39 Acceptable

4575 / PE1456-2ML - Lot LRAA0922/Analyst:AA/ Analysis Date: 2016-02-23

Evaluation Criteria - 8Voluntary Evaluation Parameter - a:1, b:0, c:0.10, d:0

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Sample Information

ANIONIC SURFACTANT - MBAS - WS

PE1337-20ML / Lot LRAB0383

Analytes Units GravimetricValue Study Mean Study Std. Dev.

Surfactants - MBAS 1,2

2025 Miscellaneous Analytes mg/L 0.278±0.001 0 0

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CARBAMATE PESTICIDES - WS

PE1507-2ML / Lot LRAB0434

Analytes Units GravimetricValue Study Mean Study Std. Dev.

Aldicarb (Temik) 1,2

7010 ug/L 30.9±0.300 30.4 2.55

Aldicarb sulfone 1,2

7015 ug/L 34.6±0.336 33.3 2.95

Aldicarb sulfoxide 1,2

7020 ug/L 39.5±0.383 35.1 0.53

Carbaryl (Sevin) 1,2

7195 ug/L 49.9±0.484 46.3 3.52

Carbofuran (Furaden) 1,2

7205 ug/L 65.7±0.638 60 5.9

3-Hydroxycarbofuran 1,2

7710 ug/L 60.6±0.588 53.2 11.4

Methiocarb (Mesurol) 2

7800 ug/L 71.1±0.689 0 0

Methomyl (Lannate) 1,2

7805 ug/L 79.5±0.771 75.6 9.98

Oxamyl 1,2

7940 ug/L 38.2±0.370 37.1 3.51

Propoxur (Baygon) 2

8080 ug/L 57.8±0.560 0 0

Aldicarb (Temik) 1,2

7010 Carbamates & Vydate ug/L 30.9±0.300 30.4 2.55

Aldicarb sulfone 1,2

7015 Carbamates & Vydate ug/L 34.6±0.336 33.3 2.95

Aldicarb sulfoxide 1,2

7020 Carbamates & Vydate ug/L 39.5±0.383 35.1 0.53

Carbaryl (Sevin) 1,2

7195 Carbamates & Vydate ug/L 49.9±0.484 46.3 3.52

Carbofuran (Furaden) 1,2

7205 Carbamates & Vydate ug/L 65.7±0.638 60 5.9

Diuron 2

7505 Carbamates & Vydate ug/L 91.3±0.886 0 0

3-Hydroxycarbofuran 1,2

7710 Carbamates & Vydate ug/L 60.6±0.588 53.2 11.4

Methiocarb (Mesurol) 2

7800 Carbamates & Vydate ug/L 71.1±0.689 0 0

Methomyl (Lannate) 1,2

7805 Carbamates & Vydate ug/L 79.5±0.771 75.6 9.98

Oxamyl 1,2

7940 Carbamates & Vydate ug/L 38.2±0.370 37.1 3.51

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Propham 2

8075 Carbamates & Vydate ug/L 89.5±0.868 0 0

Propoxur (Baygon) 2

8080 Carbamates & Vydate ug/L 57.8±0.560 0 0

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TRIHALOMETHANES - WS

PE1456-2ML / Lot LRAA0922

Analytes Units GravimetricValue Study Mean Study Std. Dev.

Bromodichloromethane 1,2

4395 Trihalomethanes ug/L 32.0±0.311 0 0

Bromoform 1,2

4400 Trihalomethanes ug/L 18.2±0.177 0 0

Chloroform 1,2

4505 Trihalomethanes ug/L 25.6±0.248 0 0

Dibromochloromethane 1,2

4575 Trihalomethanes ug/L 15.2±0.148 0 0

Total trihalomethanes 1,2

5205 Trihalomethanes ug/L 91.1±0.884 0 0

Bromodichloromethane 1,2

4395 Volatile Organic Compounds(VOCs) ug/L 32.0±0.311 0 0

Bromoform 1,2

4400 Volatile Organic Compounds(VOCs) ug/L 18.2±0.177 0 0

Chloroform 1,2

4505 Volatile Organic Compounds(VOCs) ug/L 25.6±0.248 0 0

Dibromochloromethane 1,2

4575 Volatile Organic Compounds(VOCs) ug/L 15.2±0.148 0 0

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EDB/DBCP - WS

PE1484-2ML / Lot LRAA9565

Analytes Units GravimetricValue Study Mean Study Std. Dev.

1,2-Dibromo-3-chloropropane (DBCP) 1,2

4570 Volatile Organic Compounds(VOCs) ug/L 1.17±0.011 0.96 0.15

1,2-Dibromoethane (EDB, Ethylene dibromide) 1,2

4585 Volatile Organic Compounds(VOCs) ug/L 1.22±0.012 1.02 0.2

1,2,3-Trichloropropane 1,2

5180 Volatile Organic Compounds(VOCs) ug/L 1.42±0.015 1.35 0.32

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PH - WS - 20ML

PE1368-20ML / Lot LRAB0390

Analytes Units GravimetricValue Study Mean Study Std. Dev.

pH 1,2

1900 Miscellaneous Analytes Units 5.23±0.267 5.21 0.03

pH 1,2

1900 Units 5.23±0.267 5.21 0.03

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ANIONS - WS

PE1364-20ML / Lot LRAA9636

Analytes Units GravimetricValue Study Mean Study Std. Dev.

Orthophosphate as PO4 2

11870 mg/L 8.59±0.044 8.46 0.61

Chloride 1,2

1575 mg/L 111±0.565 109 5.17

Fluoride 1,2

1730 mg/L 1.86±0.010 1.82 0.13

Nitrate as NO3 1,2

1805 mg/L 23.2±0.119 0 0

Nitrate as N 1,2

1810 mg/L 5.25±0.027 5.25 0.24

Nitrate+nitrite as N 1,2

1820 mg/L 6.42±0.033 6.41 0.25

Nitrite as NO2 1,2

1835 mg/L 3.84±0.020 3.67 0.01

Nitrite as N 1,2

1840 mg/L 1.17±0.006 1.17 0.08

Orthophosphate as P 1,2

1870 mg/L 2.80±0.014 2.77 0.14

Sulfate 1,2

2000 mg/L 126±0.642 126 6

Orthophosphate as PO4 2

11870 Minerals mg/L 8.59±0.044 8.46 0.61

Chloride 1,2

1575 Minerals mg/L 111±0.565 109 5.17

Fluoride 1,2

1730 Minerals mg/L 1.86±0.010 1.82 0.13

Nitrate as NO3 1,2

1805 Minerals mg/L 23.2±0.119 0 0

Nitrate as N 1,2

1810 Nutrients mg/L 5.25±0.027 5.25 0.24

Nitrate+nitrite as N 1,2

1820 Nutrients mg/L 6.42±0.033 6.41 0.25

Nitrite as NO2 1,2

1835 Minerals mg/L 3.84±0.020 3.67 0.01

Nitrite as N 1,2

1840 Nutrients mg/L 1.17±0.006 1.17 0.08

Orthophosphate as P 1,2

1870 Nutrients mg/L 2.80±0.014 2.77 0.14

Phosphorus as P, total 1,2

1910 Miscellaneous Analytes mg/L 2.80 2.92 0.1

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Sulfate 1,2

2000 Minerals mg/L 126±0.642 126 6

Nitrate as N 1,2

1810 Minerals mg/L 5.25±0.027 5.25 0.24

Nitrate+nitrite as N 1,2

1820 Minerals mg/L 6.42±0.033 6.41 0.25

Nitrite as N 1,2

1840 Minerals mg/L 1.17±0.006 1.17 0.08

Orthophosphate as P 1,2

1870 Minerals mg/L 2.80±0.014 2.77 0.14

Sulfate 1,2

2000 Miscellaneous Analytes mg/L 126±0.642 126 6

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RESIDUAL FREE CHLORINE (RFC) - WS

PE1450-2ML / Lot LRAA9443

Analytes Units GravimetricValue Study Mean Study Std. Dev.

Residual free chlorine 1,2

1945 Miscellaneous Analytes mg/L 1.00±0.0064 0.96 0.12

Total residual chlorine 1,2

1940 Miscellaneous Analytes mg/L 1.05±0.0064 1.03 0.06

Combined Chlorine 2

111 Miscellaneous Analytes mg/L 0.1±0.0064 0 0

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TOTAL ORGANIC CARBON (TOC) - WS

PE1308-20ML / Lot LRAA7524

Analytes Units GravimetricValue Study Mean Study Std. Dev.

Dissolved organic carbon (DOC) 1,2

1710 Miscellaneous Analytes mg/L 11.26±0.057445 11.5 1.14

Total organic carbon (TOC) 1,2

2040 Miscellaneous Analytes mg/L 11.26±0.057445 11.3 0.6

Sulfate 1,2

2000 Miscellaneous Analytes mg/L 0±0 0 0

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TURBIDITY - WS

PE1342-2ML / Lot LRAA9244

Analytes Units GravimetricValue Study Mean Study Std. Dev.

Turbidity 1,2

2055 Miscellaneous Analytes NTU 1.37 1.38 0.15

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TRACE METALS 1 - WS

PE1488-20ML / Lot LRAB0432

Analytes Units GravimetricValue Study Mean Study Std. Dev.

Arsenic, As 1,2

1010 ug/L 28.6±0.146 29.4 1.96

Beryllium, Be 1,2

1020 ug/L 5.11±0.0261 5.18 0.28

Cadmium, Cd 1,2

1030 ug/L 39.6±0.202 39.6 1.68

Chromium, Cr (total) 1,2

1040 ug/L 169±0.861 167 8.55

Copper, Cu 1,2

1055 ug/L 1150±5.89 1140 64

Iron, Fe 1,2

1070 ug/L 1040±5.32 1030 56.9

Lead, Pb 1,2

1075 ug/L 81.4±0.415 80.9 4.06

Lithium, Li 2

1080 ug/L 382±1.95 385 18

Manganese, Mn 1,2

1090 ug/L 638±3.26 638 33

Mercury, Hg 1,2

1095 ug/L 1.58±0.008 1.5 0.15

Nickel, Ni 1,2

1105 ug/L 346±1.77 345 17.6

Selenium, Se 1,2

1140 ug/L 80.0±0.408 79 5.68

Zinc, Zn 1,2

1190 ug/L 1300±6.65 1290 65.3

Aluminum, Al 1,2

1000 ug/L 679±3.46 686 47.2

Arsenic, As 1,2

1010 Trace Metals - Drinking Water ug/L 28.6±0.146 29.4 1.96

Beryllium, Be 1,2

1020 Trace Metals - Drinking Water ug/L 5.11±0.0261 5.18 0.28

Cadmium, Cd 1,2

1030 Trace Metals - Drinking Water ug/L 39.6±0.202 39.6 1.68

Chromium, Cr (total) 1,2

1040 Trace Metals - Drinking Water ug/L 169±0.861 167 8.55

Copper, Cu 1,2

1055 Trace Metals - Drinking Water ug/L 1150±5.89 1140 64

Iron, Fe 1,2

1070 Trace Metals - Drinking Water ug/L 1040±5.32 1030 56.9

Lead, Pb 1,2

1075 Trace Metals - Drinking Water ug/L 81.4±0.415 80.9 4.06

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Lithium, Li 2

1080 Trace Metals - Drinking Water ug/L 382±1.95 385 18

Manganese, Mn 1,2

1090 Trace Metals - Drinking Water ug/L 638±3.26 638 33

Mercury, Hg 1,2

1095 Trace Metals - Drinking Water ug/L 1.58±0.008 1.5 0.15

Nickel, Ni 1,2

1105 Trace Metals - Drinking Water ug/L 346±1.77 345 17.6

Selenium, Se 1,2

1140 Trace Metals - Drinking Water ug/L 80.0±0.408 79 5.68

Zinc, Zn 1,2

1190 Trace Metals - Drinking Water ug/L 1300±6.65 1290 65.3

Aluminum, Al 1,2

1000 Trace Metals - Drinking Water ug/L 679±3.46 686 47.2

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TRACE METALS 2 - WS

PE1458-20ML / Lot LRAB0426

Analytes Units GravimetricValue Study Mean Study Std. Dev.

Antimony, Sb 1,2

1005 Trace Metals - Drinking Water ug/L 18.8±0.100 18.5 1.2

Barium, Ba 1,2

1015 Trace Metals - Drinking Water ug/L 1310±6.67 1310 80.1

Boron, B 1,2

1025 Trace Metals - Drinking Water ug/L 1540±7.88 1590 77.7

Molybdenum, Mo 1,2

1100 Trace Metals - Drinking Water ug/L 116±0.59 116 6.76

Silver, Ag 1,2

1150 Trace Metals - Drinking Water ug/L 239±1.24 236 18.7

Thallium, Tl 1,2

1165 Trace Metals - Drinking Water ug/L 8.01±0.04 7.66 0.58

Vanadium, V 1,2

1185 Trace Metals - Drinking Water ug/L 2050±10.4 2010 103

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SILICA - WS

PE1350-20ML / Lot LRAA7196

Analytes Units GravimetricValue Study Mean Study Std. Dev.

Silica as SiO2 1,2

1990 Miscellaneous Analytes mg/L 13.59±0.0693 13 0.46

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COLOR - WS

PE1401-20ML / Lot LRAB0396

Analytes Units GravimetricValue Study Mean Study Std. Dev.

Color 1,2

1605 Miscellaneous Analytes Pt-Co Units 30±0.153 27.4 3.59

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URANIUM - WS

PE1548-20ML / Lot LRAA4551

Analytes Units GravimetricValue Study Mean Study Std. Dev.

Uranium, U 1,2

3055 Miscellaneous Analytes ug/L 23.2±0.12 22.2 2.18

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CORROSIVITY/SODIUM - WS

PE1304-1KT / Lot LRAA7326

Analytes Units GravimetricValue Study Mean Study Std. Dev.

Calcium, Ca 1,2

1035 Minerals mg/L 62.2191±0.3173 61.3 2.49

Magnesium, Mg 1,2

1085 Minerals mg/L 13.1692±0.0672 13 0.66

Potassium, K 1,2

1125 Minerals mg/L 14.4601±0.0737 14.9 1.07

Sodium, Na 1,2

1155 Minerals mg/L 15.299±0.078 15.6 0.99

Alkalinity as CaCO3 1,2

1505 Miscellaneous Analytes mg/L 33.0752±0.1687 33.7 1.96

Calcium hardness as CaCO3 1,2

1550 Minerals mg/L 155.3612±0.7923 156 6.09

Specific conductance, Conductivity (25ºC) 1,2

1610 Miscellaneous Analytes umhos/cm 614±5.22 614 27.6

Corrosivity 1,2

1620 Miscellaneous Analytes SI Units -0.242 0 0

Corrosivity (langlier index @ 25ºC) 1,2

1620 Miscellaneous Analytes Units -0.2422 -0.53 1.08

Corrosivity (pH) 1,2

1625 Miscellaneous Analytes Units 8.0 7.97 0.27

Hardness, total as CaCO3 1,2

1755 Minerals mg/L 209.5918±1.0689 210 5.43

Hardness, total as CaCO3 (calc.) 1,2

1760 Miscellaneous Analytes mg/L 209±1.076 207 9.72

Total Solids (TS) 1,2

1950 Miscellaneous Analytes mg/L 505 425 147

Total Dissolved Solids at 180ºC (TDS) 1,2

1955 Miscellaneous Analytes mg/L 424±2.1751 424 72

Langlier @ 140ºF 1,2

1800 Miscellaneous Analytes 0 0

Langlier @ 40ºF 2

1800 Miscellaneous Analytes 0 0

Langlier @ 50ºF 2

1800 Miscellaneous Analytes -0.525 0 0

Calcium, Ca 1,2

1035 Trace Metals - Drinking Water mg/L 62.2191±0.3173 61.3 2.49

Magnesium, Mg 1,2

1085 Trace Metals - Drinking Water mg/L 13.1692±0.0672 13 0.66

Potassium, K 1,2

1125 Trace Metals - Drinking Water mg/L 14.4601±0.0737 14.9 1.07

Sodium, Na 1,2

1155 Miscellaneous Analytes mg/L 15.299±0.078 15.6 0.99

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Calcium hardness as CaCO3 1,2

1550 Miscellaneous Analytes mg/L 155.3612±0.7923 156 6.09

Hardness, total as CaCO3 1,2

1755 Miscellaneous Analytes mg/L 209.5918±1.0689 210 5.43

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Standard Plate Count - WS

MIC002-2EA / Lot LRAB0419

Analytes Units GravimetricValue Study Mean Study Std. Dev.

Heterotrophic plate count 1,2

2555 Microbiology CFU/mL 135±5 128 28.6

Heterotrophic Plate Count, MPN 1,2

2555 Microbiology MPN 171±5 59.1 68.7

Heterotrophic plate count 1,2

2555 CFU/mL 135±5 128 28.6

Heterotrophic Plate Count, MPN 1,2

2555 MPN 171±5 59.1 68.7

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Inorganic Disinfection By-Products - WS (Whole Volume)

PE3306-500ML / Lot LRAA8416

Analytes Units GravimetricValue Study Mean Study Std. Dev.

Bromate 1,2

1535 Inorganic Disinfection By-Products ug/L 45.3±0.231 0 0

Bromide 1,2

1540 Inorganic Disinfection By-Products ug/L 325±1.75 0 0

Chlorate 1,2

1570 Inorganic Disinfection By-Products ug/L 124±0.632 0 0

Chlorite 1,2

1595 Inorganic Disinfection By-Products ug/L 964±4.91 0 0

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ODOR - DRINKING WATER PT

PE1133-500ML / Lot LRAB0561

Analytes Units GravimetricValue Study Mean Study Std. Dev.

Odor 1,2

1855 Organic Disinfection By-Products TON 50 105 141

Odor 1,2

1855 TON 50 105 141

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DIQUAT/GLYPHOSATE/PARAQUAT - WS

PE1435-2ML / Lot LRAB0399

Analytes Units GravimetricValue Study Mean Study Std. Dev.

Diquat 1,2

9390 ug/L 28.0±0.272 24.7 5.86

Glyphosate 1,2

9411 ug/L 423±4.1 418 42.2

Paraquat 1,2

9528 ug/L 69.4±0.674 0 0

Diquat 1,2

9390 Herbicides ug/L 28.0±0.272 24.7 5.86

Glyphosate 1,2

9411 Herbicides ug/L 423±4.1 418 42.2

Paraquat 1,2

9528 Herbicides ug/L 69.4±0.674 0 0

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MERCURY (LOW LEVEL) - WS

PE1432-20ML / Lot LRAB0398

Analytes Units GravimetricValue Study Mean Study Std. Dev.

Low Level Mercury 1,2

1095 ng/L 50.5±0.258 0 0

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Complete Volatiles Kit - WS

PE1358-1KT / Lot LRAA7981

Analytes Units GravimetricValue Study Mean Study Std. Dev.

Benzene 1,2

4375 Volatile Organic Compounds(VOCs) ug/L 10±0.097 9.9 0.91

Bromobenzene 1,2

4385 Volatile Organic Compounds(VOCs) ug/L 18.01±0.175 18.1 1.45

Bromochloromethane 1,2

4390 Volatile Organic Compounds(VOCs) ug/L 14.05±0.136 14.3 2.09

n-Butylbenzene 1,2

4435 Volatile Organic Compounds(VOCs) ug/L 5.33±0.052 5.65 0.48

sec-Butylbenzene 1,2

4440 Volatile Organic Compounds(VOCs) ug/L 8.28±0.08 8.8 0.71

tert-Butylbenzene 1,2

4445 Volatile Organic Compounds(VOCs) ug/L 17.57±0.17 18.2 1.48

Carbon tetrachloride 1,2

4455 Volatile Organic Compounds(VOCs) ug/L 8.28±0.08 8.09 0.93

Chlorobenzene 1,2

4475 Volatile Organic Compounds(VOCs) ug/L 5.85±0.057 5.96 0.54

Chloroethane 1,2

4485 Volatile Organic Compounds(VOCs) ug/L 12.74±0.143 12.6 2.52

2-Chlorotoluene 1,2

4535 Volatile Organic Compounds(VOCs) ug/L 10.82±0.105 11 1.24

4-Chlorotoluene 1,2

4540 Volatile Organic Compounds(VOCs) ug/L 12.53±0.122 12.8 1.25

Dibromomethane 1,2

4595 Volatile Organic Compounds(VOCs) ug/L 16.29±0.158 16.4 1.42

1,2-Dichlorobenzene 1,2

4610 Volatile Organic Compounds(VOCs) ug/L 16.21±0.157 16.3 1.44

1,3-Dichlorobenzene 1,2

4615 Volatile Organic Compounds(VOCs) ug/L 13.11±0.127 13.1 0.97

1,4-Dichlorobenzene 1,2

4620 Volatile Organic Compounds(VOCs) ug/L 14.55±0.141 14.7 1.35

Dichlorodifluoromethane 1,2

4625 Volatile Organic Compounds(VOCs) ug/L 8.94±0.186 7.31 1.51

Dichlorofluoromethane 2

4627 Volatile Organic Compounds(VOCs) ug/L 0±0 0 0

1,1-Dichloroethane 1,2

4630 Volatile Organic Compounds(VOCs) ug/L 5.3±0.051 5.28 0.8

1,2-Dichloroethane 1,2

4635 Volatile Organic Compounds(VOCs) ug/L 4.15±0.04 4.24 0.55

1,1-Dichloroethylene 1,2

4640 Volatile Organic Compounds(VOCs) ug/L 6.12±0.059 4.99 0.79

cis-1,2-Dichloroethylene 1,2

4645 Volatile Organic Compounds(VOCs) ug/L 15.89±0.154 15.4 1.55

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1,2-Dichloropropane 1,2

4655 Volatile Organic Compounds(VOCs) ug/L 14.61±0.142 14.9 1.31

1,3-Dichloropropane 1,2

4660 Volatile Organic Compounds(VOCs) ug/L 9.95±0.096 9.81 0.78

2,2-Dichloropropane 1,2

4665 Volatile Organic Compounds(VOCs) ug/L 10.86±0.105 11.1 1.78

1,1-Dichloropropene 1,2

4670 Volatile Organic Compounds(VOCs) ug/L 14.74±0.143 14.9 2.53

cis-1,3-Dichloropropene 1,2

4680 Volatile Organic Compounds(VOCs) ug/L 13.67±0.133 12.4 1.33

trans-1,3-Dichloropropene 1,2

4685 Volatile Organic Compounds(VOCs) ug/L 14.14±0.137 13.3 1.4

trans-1,2-Dichloroethylene 1,2

4700 Volatile Organic Compounds(VOCs) ug/L 8.08±0.078 7.66 1.09

Ethylbenzene 1,2

4765 Volatile Organic Compounds(VOCs) ug/L 7.45±0.072 7.56 0.68

Hexachlorobutadiene 1,2

4835 Volatile Organic Compounds(VOCs) ug/L 16.47±0.16 17.2 1.66

Isopropylbenzene 1,2

4900 Volatile Organic Compounds(VOCs) ug/L 15.51±0.15 16.3 1.62

4-Isopropyltoluene 1,2

4910 Volatile Organic Compounds(VOCs) ug/L 18.21±0.167 18.4 1.1

Methyl bromide (Bromomethane) 1,2

4950 Volatile Organic Compounds(VOCs) ug/L 22.89±0.222 18 6.03

Methyl chloride (Chloromethane) 1,2

4960 Volatile Organic Compounds(VOCs) ug/L 21.4±0.208 19 4.14

Methylene chloride (Dichloromethane) 1,2

4975 Volatile Organic Compounds(VOCs) ug/L 17.78±0.172 16.7 2.25

Methyl tert-butyl ether (MTBE) 1,2

5000 Volatile Organic Compounds(VOCs) ug/L 16.88±0.164 18.2 3.19

Naphthalene 1,2

5005 Volatile Organic Compounds(VOCs) ug/L 28.47±0.276 28.6 3.48

n-Propylbenzene (1-Phenylpropane) 1,2

5090 Volatile Organic Compounds(VOCs) ug/L 9.7±0.094 10.2 1.17

Styrene 1,2

5100 Volatile Organic Compounds(VOCs) ug/L 7.97±0.077 8.23 0.49

1,1,1,2-Tetrachloroethane 1,2

5105 Volatile Organic Compounds(VOCs) ug/L 6.7±0.065 6.7 0.71

1,1,2,2-Tetrachloroethane 1,2

5110 Volatile Organic Compounds(VOCs) ug/L 12.89±0.125 12.6 1.22

Tetrachloroethylene (Perchloroethylene) 1,2

5115 Volatile Organic Compounds(VOCs) ug/L 16.44±0.159 16.7 1.5

Toluene 1,2

5140 Volatile Organic Compounds(VOCs) ug/L 12.96±0.126 13.2 0.79

1,2,3-Trichlorobenzene 1,2

5150 Volatile Organic Compounds(VOCs) ug/L 32.49±0.315 32.1 4.19

1,2,4-Trichlorobenzene 1,2

5155 Volatile Organic Compounds(VOCs) ug/L 9.61±0.093 9.44 0.73

1,1,1-Trichloroethane 1,2

5160 Volatile Organic Compounds(VOCs) ug/L 7.61±0.074 7.52 1.22

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1,1,2-Trichloroethane 1,2

5165 Volatile Organic Compounds(VOCs) ug/L 10.26±0.099 10.4 0.88

Trichloroethene (Trichloroethylene) 1,2

5170 Volatile Organic Compounds(VOCs) ug/L 14.65±0.142 14.6 1.62

Trichlorofluoromethane 1,2

5175 Volatile Organic Compounds(VOCs) ug/L 24.5±0.238 22.4 3.88

1,2,3-Trichloropropane 1,2

5180 Volatile Organic Compounds(VOCs) ug/L 17.27±0.168 16.7 2.14

1,2,4-Trimethylbenzene 1,2

5210 Volatile Organic Compounds(VOCs) ug/L 16.87±0.164 17.3 0.91

1,3,5-Trimethylbenzene 1,2

5215 Volatile Organic Compounds(VOCs) ug/L 15±0.146 15.8 1.54

Vinyl chloride 1,2

5235 Volatile Organic Compounds(VOCs) ug/L 5.1±0.08 5.29 1.18

m+p-Xylene 1,2

5240 Volatile Organic Compounds(VOCs) ug/L 12.44±0.1207 13 1.33

o-Xylene 1,2

5250 Volatile Organic Compounds(VOCs) ug/L 17.58±0.171 18.1 1.19

Xylene, total 1,2

5260 Volatile Organic Compounds(VOCs) ug/L 30.02±0.291 30.8 1.65

Benzene 1,2

4375 ug/L 10±0.097 9.9 0.91

Bromobenzene 1,2

4385 ug/L 18.01±0.175 18.1 1.45

Bromochloromethane 1,2

4390 ug/L 14.05±0.136 14.3 2.09

n-Butylbenzene 1,2

4435 ug/L 5.33±0.052 5.65 0.48

sec-Butylbenzene 1,2

4440 ug/L 8.28±0.08 8.8 0.71

tert-Butylbenzene 1,2

4445 ug/L 17.57±0.17 18.2 1.48

Carbon tetrachloride 1,2

4455 ug/L 8.28±0.08 8.09 0.93

Chlorobenzene 1,2

4475 ug/L 5.85±0.057 5.96 0.54

Chloroethane 1,2

4485 ug/L 12.74±0.143 12.6 2.52

2-Chlorotoluene 1,2

4535 ug/L 10.82±0.105 11 1.24

4-Chlorotoluene 1,2

4540 ug/L 12.53±0.122 12.8 1.25

Dibromomethane 1,2

4595 ug/L 16.29±0.158 16.4 1.42

1,2-Dichlorobenzene 1,2

4610 ug/L 16.21±0.157 16.3 1.44

1,3-Dichlorobenzene 1,2

4615 ug/L 13.11±0.127 13.1 0.97

1,4-Dichlorobenzene 1,2

4620 ug/L 14.55±0.141 14.7 1.35

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Dichlorodifluoromethane 1,2

4625 ug/L 8.94±0.186 7.31 1.51

Dichlorofluoromethane 2

4627 ug/L 0±0 0 0

1,1-Dichloroethane 1,2

4630 ug/L 5.3±0.051 5.28 0.8

1,2-Dichloroethane 1,2

4635 ug/L 4.15±0.04 4.24 0.55

1,1-Dichloroethylene 1,2

4640 ug/L 6.12±0.059 4.99 0.79

cis-1,2-Dichloroethylene 1,2

4645 ug/L 15.89±0.154 15.4 1.55

1,2-Dichloropropane 1,2

4655 ug/L 14.61±0.142 14.9 1.31

1,3-Dichloropropane 1,2

4660 ug/L 9.95±0.096 9.81 0.78

2,2-Dichloropropane 1,2

4665 ug/L 10.86±0.105 11.1 1.78

1,1-Dichloropropene 1,2

4670 ug/L 14.74±0.143 14.9 2.53

cis-1,3-Dichloropropene 1,2

4680 ug/L 13.67±0.133 12.4 1.33

trans-1,3-Dichloropropene 1,2

4685 ug/L 14.14±0.137 13.3 1.4

trans-1,2-Dichloroethylene 1,2

4700 ug/L 8.08±0.078 7.66 1.09

Ethylbenzene 1,2

4765 ug/L 7.45±0.072 7.56 0.68

Hexachlorobutadiene 1,2

4835 ug/L 16.47±0.16 17.2 1.66

Isopropylbenzene 1,2

4900 ug/L 15.51±0.15 16.3 1.62

4-Isopropyltoluene 1,2

4910 ug/L 18.21±0.167 18.4 1.1

Methyl bromide (Bromomethane) 1,2

4950 ug/L 22.89±0.222 18 6.03

Methyl chloride (Chloromethane) 1,2

4960 ug/L 21.4±0.208 19 4.14

Methylene chloride (Dichloromethane) 1,2

4975 ug/L 17.78±0.172 16.7 2.25

Methyl tert-butyl ether (MTBE) 1,2

5000 ug/L 16.88±0.164 18.2 3.19

Naphthalene 1,2

5005 ug/L 28.47±0.276 28.6 3.48

n-Propylbenzene (1-Phenylpropane) 1,2

5090 ug/L 9.7±0.094 10.2 1.17

Styrene 1,2

5100 ug/L 7.97±0.077 8.23 0.49

1,1,1,2-Tetrachloroethane 1,2

5105 ug/L 6.7±0.065 6.7 0.71

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1,1,2,2-Tetrachloroethane 1,2

5110 ug/L 12.89±0.125 12.6 1.22

Tetrachloroethylene (Perchloroethylene) 1,2

5115 ug/L 16.44±0.159 16.7 1.5

Toluene 1,2

5140 ug/L 12.96±0.126 13.2 0.79

1,2,3-Trichlorobenzene 1,2

5150 ug/L 32.49±0.315 32.1 4.19

1,2,4-Trichlorobenzene 1,2

5155 ug/L 9.61±0.093 9.44 0.73

1,1,1-Trichloroethane 1,2

5160 ug/L 7.61±0.074 7.52 1.22

1,1,2-Trichloroethane 1,2

5165 ug/L 10.26±0.099 10.4 0.88

Trichloroethene (Trichloroethylene) 1,2

5170 ug/L 14.65±0.142 14.6 1.62

Trichlorofluoromethane 1,2

5175 ug/L 24.5±0.238 22.4 3.88

1,2,3-Trichloropropane 1,2

5180 ug/L 17.27±0.168 16.7 2.14

1,2,4-Trimethylbenzene 1,2

5210 ug/L 16.87±0.164 17.3 0.91

1,3,5-Trimethylbenzene 1,2

5215 ug/L 15±0.146 15.8 1.54

Vinyl chloride 1,2

5235 ug/L 5.1±0.08 5.29 1.18

m+p-Xylene 1,2

5240 ug/L 12.44±0.1207 13 1.33

o-Xylene 1,2

5250 ug/L 17.58±0.171 18.1 1.19

Xylene, total 1,2

5260 ug/L 30.02±0.291 30.8 1.65

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TRACE METALS 3 - WS

PE1448-20ML / Lot LRAA8373

Analytes Units GravimetricValue Study Mean Study Std. Dev.

Cobalt, Co 1,2

1050 Trace Metals - Drinking Water ug/L 168±0.855 169 3.65

Strontium, Sr 1,2

1160 Trace Metals - Drinking Water ug/L 166±0.847 167 20.6

Tin, Sn 1,2

1175 Trace Metals - Drinking Water ug/L 958±4.89 773 313

Titanium, Ti 1,2

1180 Trace Metals - Drinking Water ug/L 90.9±0.464 80.5 15.5

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WS-Microbiological PT - Presence/Absence

MIC001-PA / Lot LRAB0424

Analytes Units GravimetricValue Study Mean Study Std. Dev.

Coliforms, total - Sample 01 1,2

2500 Microbiology Units 0±0 0 0

Coliforms, total - Sample 02 1,2

2500 Microbiology Units 1±0 0 0

Coliforms, total - Sample 04 1,2

2500 Microbiology Units 0±0 0 0

Coliforms, total - Sample 03 1,2

2500 Microbiology Units 1±0 0 0

Coliforms, total - Sample 05 1,2

2500 Microbiology Units 1±0 0 0

Coliforms, total - Sample 06 1,2

2500 Microbiology Units 1±0 0 0

Coliforms, total - Sample 07 1,2

2500 Microbiology Units 1±0 0 0

Coliforms, total - Sample 08 1,2

2500 Microbiology Units 0±0 0 0

Coliforms, total - Sample 09 1,2

2500 Microbiology Units 1±0 0 0

Coliforms, total - Sample 10 1,2

2500 Microbiology Units 0±0 0 0

Fecal Coliforms - Sample 01 1,2

2530 Microbiology Units 0±0 0 0

Fecal Coliforms - Sample 02 1,2

2530 Microbiology Units 0±0 0 0

Fecal Coliforms - Sample 03 1,2

2530 Microbiology Units 1±0 28.7 69.9

Fecal Coliforms - Sample 04 1,2

2530 Microbiology Units 0±0 0 0

Fecal Coliforms - Sample 05 1,2

2530 Microbiology Units 1±0 18.5 40

Fecal Coliforms - Sample 06 1,2

2530 Microbiology Units 0±0 0 0

Fecal Coliforms - Sample 07 1,2

2530 Microbiology Units 0±0 0 0

Fecal Coliforms - Sample 08 1,2

2530 Microbiology Units 0±0 0 0

Fecal Coliforms - Sample 09 1,2

2530 Microbiology Units 1±0 33.2 81.4

Fecal Coliforms - Sample 10 1,2

2530 Microbiology Units 0±0 0 0

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E. Coli - Sample 01 1,2

2525 Microbiology Units 0±0 0 0

E. Coli - Sample 02 1,2

2525 Microbiology Units 0±0 0 0

E. Coli - Sample 03 1,2

2525 Microbiology Units 1±0 0 0

E. Coli - Sample 04 1,2

2525 Microbiology Units 0±0 0 0

E. Coli - Sample 05 1,2

2525 Microbiology Units 1±0 0 0

E. Coli - Sample 06 1,2

2525 Microbiology Units 0±0 0 0

E. Coli - Sample 07 1,2

2525 Microbiology Units 0±0 0 0

E. Coli - Sample 08 1,2

2525 Microbiology Units 0±0 0 0

E. Coli - Sample 09 1,2

2525 Microbiology Units 1±0 0 0

E. Coli - Sample 10 1,2

2525 Microbiology Units 0±0 0 0

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WS-Microbiological PT - MPN

MIC001-MPN / Lot LRAB0424

Analytes Units GravimetricValue Study Mean Study Std. Dev.

Coliforms, total - Sample 01 1,2

2500 Microbiology MPN/100mL 0±0 0 0

Coliforms, total - Sample 02 1,2

2500 Microbiology MPN/100mL 340±82.34 0 0

Coliforms, total - Sample 04 1,2

2500 Microbiology MPN/100mL 0±0 0 0

Coliforms, total - Sample 03 1,2

2500 Microbiology MPN/100mL 60.2±5.8 0 0

Coliforms, total - Sample 05 1,2

2500 Microbiology MPN/100mL 60.2±5.8 0 0

Coliforms, total - Sample 06 1,2

2500 Microbiology MPN/100mL 340±82.34 0 0

Coliforms, total - Sample 07 1,2

2500 Microbiology MPN/100mL 340±82.34 0 0

Coliforms, total - Sample 08 1,2

2500 Microbiology MPN/100mL 0±0 0 0

Coliforms, total - Sample 09 1,2

2500 Microbiology MPN/100mL 60.2±5.8 0 0

Coliforms, total - Sample 10 1,2

2500 Microbiology MPN/100mL 0±0 0 0

Fecal Coliforms - Sample 01 1,2

2530 Microbiology MPN/100mL 0±0 0 0

Fecal Coliforms - Sample 02 1,2

2530 Microbiology MPN/100mL 0±0 0 0

Fecal Coliforms - Sample 03 1,2

2530 Microbiology MPN/100mL 60.2±5.8 28.7 69.9

Fecal Coliforms - Sample 04 1,2

2530 Microbiology MPN/100mL 0±0 0 0

Fecal Coliforms - Sample 05 1,2

2530 Microbiology MPN/100mL 60.2±5.8 18.5 40

Fecal Coliforms - Sample 06 1,2

2530 Microbiology MPN/100mL 0±0 0 0

Fecal Coliforms - Sample 07 1,2

2530 Microbiology MPN/100mL 0±0 0 0

Fecal Coliforms - Sample 08 1,2

2530 Microbiology MPN/100mL 0±0 0 0

Fecal Coliforms - Sample 09 1,2

2530 Microbiology MPN/100mL 60.2±5.8 33.2 81.4

Fecal Coliforms - Sample 10 1,2

2530 Microbiology MPN/100mL 0±0 0 0

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E. Coli - Sample 01 1,2

2525 Microbiology MPN/100mL 0±0 0 0

E. Coli - Sample 02 1,2

2525 Microbiology MPN/100mL 0±0 0 0

E. Coli - Sample 03 1,2

2525 Microbiology MPN/100mL 60.2±5.8 0 0

E. Coli - Sample 04 1,2

2525 Microbiology MPN/100mL 0±0 0 0

E. Coli - Sample 05 1,2

2525 Microbiology MPN/100mL 60.2±5.8 0 0

E. Coli - Sample 06 1,2

2525 Microbiology MPN/100mL 0±0 0 0

E. Coli - Sample 07 1,2

2525 Microbiology MPN/100mL 0±0 0 0

E. Coli - Sample 08 1,2

2525 Microbiology MPN/100mL 0±0 0 0

E. Coli - Sample 09 1,2

2525 Microbiology MPN/100mL 60.2±5.8 0 0

E. Coli - Sample 10 1,2

2525 Microbiology MPN/100mL 0±0 0 0

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WS-Microbiological PT - MF (CFU)

MIC001-MF / Lot LRAB0424

Analytes Units GravimetricValue Study Mean Study Std. Dev.

Coliforms, total - Sample 01 1,2

2500 Microbiology CFU/100mL 0±0 0 0

Coliforms, total - Sample 02 1,2

2500 Microbiology CFU/100mL 340±82.34 0 0

Coliforms, total - Sample 04 1,2

2500 Microbiology CFU/100mL 0±0 0 0

Coliforms, total - Sample 03 1,2

2500 Microbiology CFU/100mL 60.2±5.8 0 0

Coliforms, total - Sample 05 1,2

2500 Microbiology CFU/100mL 60.2±5.8 0 0

Coliforms, total - Sample 06 1,2

2500 Microbiology CFU/100mL 340±82.34 0 0

Coliforms, total - Sample 07 1,2

2500 Microbiology CFU/100mL 340±82.34 0 0

Coliforms, total - Sample 08 1,2

2500 Microbiology CFU/100mL 0±0 0 0

Coliforms, total - Sample 09 1,2

2500 Microbiology CFU/100mL 60.2±5.8 0 0

Coliforms, total - Sample 10 1,2

2500 Microbiology CFU/100mL 0±0 0 0

Fecal Coliforms - Sample 01 1,2

2530 Microbiology CFU/100mL 0±0 0 0

Fecal Coliforms - Sample 02 1,2

2530 Microbiology CFU/100mL 0±0 0 0

Fecal Coliforms - Sample 03 1,2

2530 Microbiology CFU/100mL 60.2±5.8 28.7 69.9

Fecal Coliforms - Sample 04 1,2

2530 Microbiology CFU/100mL 0±0 0 0

Fecal Coliforms - Sample 05 1,2

2530 Microbiology CFU/100mL 60.2±5.8 18.5 40

Fecal Coliforms - Sample 06 1,2

2530 Microbiology CFU/100mL 0±0 0 0

Fecal Coliforms - Sample 07 1,2

2530 Microbiology CFU/100mL 0±0 0 0

Fecal Coliforms - Sample 08 1,2

2530 Microbiology CFU/100mL 0±0 0 0

Fecal Coliforms - Sample 09 1,2

2530 Microbiology CFU/100mL 60.2±5.8 33.2 81.4

Fecal Coliforms - Sample 10 1,2

2530 Microbiology CFU/100mL 0±0 0 0

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E. Coli - Sample 01 1,2

2525 Microbiology CFU/100mL 0±0 0 0

E. Coli - Sample 02 1,2

2525 Microbiology CFU/100mL 0±0 0 0

E. Coli - Sample 03 1,2

2525 Microbiology CFU/100mL 60.2±5.8 0 0

E. Coli - Sample 04 1,2

2525 Microbiology CFU/100mL 0±0 0 0

E. Coli - Sample 05 1,2

2525 Microbiology CFU/100mL 60.2±5.8 0 0

E. Coli - Sample 06 1,2

2525 Microbiology CFU/100mL 0±0 0 0

E. Coli - Sample 07 1,2

2525 Microbiology CFU/100mL 0±0 0 0

E. Coli - Sample 08 1,2

2525 Microbiology CFU/100mL 0±0 0 0

E. Coli - Sample 09 1,2

2525 Microbiology CFU/100mL 60.2±5.8 0 0

E. Coli - Sample 10 1,2

2525 Microbiology CFU/100mL 0±0 0 0

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Definitions and Interpretation of Statistical Analysis:

Assigned Value: Value attributed to a particular quantity and accepted, sometimes by convention, ashaving an uncertainty appropriate for a given purpose. See ISO/IEC 17043 for additional information. Ingeneral the assigned value is the value used to assess proficiency and may or may not be the made to value(gravimetric value).

Accept. Window: The range of values that constitute acceptable performance for a laboratory participatingin this PT study.

Z: A Z-Score tells how a single data point compares to normal data. A Z-Score says not only whether a pointwas above or below average, but how unusual the measurement is. Generally, a method result with aZ-Score less than |2| is considered to be in control, a Z-Score between |2| and |3| is considered’Questionable’, but still within control and a Z greater than |3| is considered not acceptable and the methodis out of control. For WS studies, a z-score greater than |2| is unacceptable. Calculated as Z = (ReportedValue - Assigned Value) / Proficiency Std. Dev.

Proficiency Std. Dev.: Standard deviation calculated based on Evaluation Criteria.

Study Mean: Statistical study mean calculated using a robust statisitical model (RTC employs the’Biweight Program’). Robust statistical techniques to minimize the influence that extreme results can haveon estimates of the mean and standard deviation. NOTE - These techniques assign less weight to extremeresults, rather than eliminate them from a data set.

Study Std. Dev.: Standard deviation calculated from study data using robust statisicals (Biweight).

Gravimetric Value: The ’prepared to’ value, determined by gravimetric means. The uncertainty associatedto this value is standard uncertainty and based on RTC’s gravimetric tolerances.

Evaluation Criteria:

1 - Regression Equation - Acceptance windows based on TNI adopted equation of proficiency value +/- 3proficiency standard deviations and check limits of proficiency value +/- 2 proficiency standard deviations.Proficiency value and proficiency standard deviation are calculated from gravimetric variables a, b, c, & das proficiency value = a * gravimetric + b and proficiency standard deviation = c * gravimetric + d.

2 - Study Robust Mean and c,d regression - Acceptance windows based on TNI adopted equation ofproficiency value +/- 3 proficiency standard deviations and check limits of proficiency value +/- 2proficiency standard deviations. Proficiency value and proficiency standard deviation calculated from robuststudy mean and variables c & d as proficiency value = robust mean and proficiency standard deviation = c *proficiency value + d.

3 - Fixed Limits - Acceptance windows based on span of gravimetric percentage from gravimetric asgravimetric +/- gravimetric * percentage.

4 - Adjustable Fixed Limits - Acceptance windows base on a span of gravimetric percentage fromgravimetric as gravimetric +/- gravimetric * lowPercentage where gravimetric < break and gravimetric +/-

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gravimetric * highPercentage where gravimetric >= break.

5 - Study Statistics - Acceptance windows based on a number of standard deviations span from the studymean as study mean +/- (deviations * standard deviation).

6 - Log Transform Statistics - Acceptance windows based on lognormal distributed data. Acceptancewindows = mean(lognormal) +/- span * standard deviation(lognormal).

7 - Reserved

8 - Regression Equation 2SD - Acceptance windows based on EPA equation of proficiency value +/- 2proficiency standard deviations. Proficiency value and proficiency standard deviation are calculated fromgravimetric variables a, b, c, & d as proficiency value = a * gravimetric + b and proficiency standarddeviation = c * gravimetric + d. Generally reserved for drinking water studies.

Proficiency Test Item Preparation, Homogeneity and Stability Assessment - RTC uses proprietaryand published methods for the manufacture, homogeneity and stability testing of proficiency test items.RTC’s proficiency test materials meet requirements of ISO Guide 34. For more information contact RTC.Additionally RTC complies with TNI Volume 3 ’General Requirements for Environmental Proficiency TestProviders’, EL-V3-2009, 2009 for all TNI Fields of Proficiency Testing analytes.

Metrological Traceability - All preparations are made using balances calibrated annually traceable toNIST standards. Where appropriate analytical measurements are traceable through an unbroken chain toNIST standards, or a Certified Reference Material manufactured under ISO Guide 34 in conjunction withISO/IEC 17025.

Statistical Analysis - RTC uses robust statistics to calculate study means and standard deviations -Reference - Kafadar, K, A Biweight Approach to the One-Sample Problem, Journal of the AmericanStatistical Association, Vol. 77, No. 378, June, 1982, pp. 416-424.

Additional Information - Go to www.rt-corp.com/reporting for additional information on summarystatistics for specific methods, advice on the interpretation of the statistical analysis, and additionalcomments/recommendations. If you failed an analyte it may be required to perform a corrective actionand/or retest. RTC recommends that you contact your accreditation body for specific instruction.

Program analyte accrediting footnotes1 NELAC Compliant, covered by RTC’s ACLASS Proficiency Testing Provider accreditation, Cert. AP-14692 ISO 17043 Accredited, covered by RTC’s ACLASS Proficiency Testing Provider accreditation, CertAP-1469

Authorizing Officer:

Date: 3/31/2016

Patrick Brumfield, ASQ CQA

QA Manager

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This section of the report is for informational purposes only. If you are unsure aboutspecific accreditation requirements, please contact your state coordinator.

UNACCEPTABLE ANALYTES

RTC Lab Code: 49445626

PE1304-1KT

CORROSIVITY/SODIUM - WS

Analytes MethodNumber MethodName

Alkalinity as CaCO3 1,2 20045403 SM 2320 B 21st ED (1997)

PE1368-20ML

PH - WS - 20ML

Analytes MethodNumber MethodName

pH 1,2 20105015 SM 4500-H+ B 22nd ED (2011)

PE1450-2ML

RESIDUAL FREE CHLORINE (RFC) - WS

Analytes MethodNumber MethodName

Total residual chlorine 1,2 60003501 HACH 8021

PE1432-20ML

MERCURY (LOW LEVEL) - WS

Analytes MethodNumber MethodName

Low Level Mercury 1,2 20057801 SM 3112 B 21st ED (1999)

PE1488-20ML

TRACE METALS 1 - WS

Analytes MethodNumber MethodName

Copper, Cu 1,2 10014605 EPA 200.8 5.4 (1994)

Lead, Pb 1,2 10013806 EPA 200.7 4.4 (1994)

PE1448-20ML

TRACE METALS 3 - WS

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Analytes MethodNumber MethodName

Tin, Sn 1,2 10013806 EPA 200.7 4.4 (1994)

Tin, Sn 1,2 10014605 EPA 200.8 5.4 (1994)

PE1358-1KT

Complete Volatiles Kit - WS

Analytes MethodNumber MethodName

Methyl tert-butyl ether (MTBE) 1,2 10088809 EPA 524.2 4.1 (1995)

PE1484-2ML

EDB/DBCP - WS

Analytes MethodNumber MethodName

1,2,3-Trichloropropane 1,2 10082801 EPA 504.1 1.1 (1995)

PE1435-2ML

DIQUAT/GLYPHOSATE/PARAQUAT - WS

Analytes MethodNumber MethodName

Diquat 1,2 10093400 EPA 549.2 1 (1997)

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PASS RATE

Number of Reported Results: 191

Number of Passing Results: 180

Pass Rate: 94.24%

Donny JuarezEnergy LaboratoriesPO Box 247Casper, WY 82602USA

WatR™Supply Study

Open Date: 01/11/16

Close Date: 02/25/16

Report Issued Date: 02/29/16

WS-234 Final Report

Study # : WS-234

February 29, 2016

Donny JuarezEnergy LaboratoriesPO Box 247Casper, WY 82602

Enclosed is your final report for ERA's WS-234 WatR™Supply Proficiency Testing (PT) study. Your final report includes an evaluation of all results submitted by your laboratory to ERA. Data Evaluation Protocols: All analytes in ERA's WS-234 WatR™Supply Proficiency Testing (PT) study have been evaluated using the following tiered approach. If the analyte is listed in the current TNI Fields of Proficiency Testing (FoPT) tables, the evaluation was completed by comparing the reported result to the acceptance limits generated using the criteria contained in the TNI FoPT tables. If the analyte is not included in the TNI FoPT tables, the reported result has been evaluated using the procedures outlined in ERA's Standard Operating Procedure for the Generation of Performance Acceptance Limits (SOP 0260).

Corrective Action Help: As part of your accreditation(s), you may be required to identify the root cause of any "Not Acceptable" results, implement the necessary corrective actions, and then satisfy your PT requirements by participating in a Supplemental (QuiK™Response) or future ERA PT study. ERA's technical staff is available to help your laboratory resolve any technical issues that may be impairing your PT performance and possibly affecting your routine data quality. Our laboratory and technical staff have many years of collective experience in performing the full range of environmental analyses. As part of our technical support, ERA offers QC samples that can be useful in helping you work through your technical issues.

At the request of the TNI Accreditation Council, we have included a Laboratory Exception Report that includes a list of all analytes reported with less than qualifiers when the assigned value was greater than “0.” In addition, because we have received many requests from laboratories, this report also includes a list of all analytes with "Not Acceptable" evaluations.

Some states have elected not to convert to the 2009 TNI Standards at this time. If you have released your results to a state that has retained the 2003 NELAC Evaluation Criteria, your final report will include a section that evaluates the results according to the 2003 Standard in addition to the 2009 TNI Standards.

Thank you for your participation in ERA's WS-234 WatR™Supply Proficiency Testing study. If you have any questions, please contact our Proficiency Testing Department at 1-800-372-0122.

Sincerely,

Patrick LarsonQuality Officer

attachments

16341 Table Mountain Pkwy • Golden, CO 80403 • 800.372.0122 • 303.431.8454 • fax 303.421.0159 • www.eraqc.com Study # : WS-234

Report Recipient Contact/Phone Number Reporting Type Evaluation Type

EPA Region 8 Marcie Tidd / (303) 312-7764 All Analytes 2009 TNI

Florida Vanessa Soto / 904-791-1599 All Analytes 2009 TNI

Idaho Ernie Bader / 208-334-2235 x 290 All Analytes 2009 TNI

Montana Russell Leu / 406-444-5259 All Analytes 2009 TNI

Nebraska Laurie Wieting / 402-471-8407 All Analytes 2009 TNI

Nevada Don LaFara / 775-687-9491 All Analytes 2003 NELAC

New Mexico (WS) Oneva Pena / 505-476-8648 All Analytes 2009 TNI

North Dakota Cynthia Auen / 701-328-6172 All Analytes 2009 TNI

Oregon Gary Ward / 503-693-4122 All Analytes 2009 TNI

South Dakota Stacy Ellwanger / 605-773-4757 All Analytes 2009 TNI

Texas Frank Jamison / (512) 239-3754 All Analytes 2009 TNI

Utah Jill Jones / 801-965-3899 All Analytes 2009 TNI

Study # : WS-234

WS-234 Definitions & Study DiscussionStudy Dates: 01/11/16 - 02/25/16 Report Issued: 02/29/16

WS Study Definitions WS Study Discussion

The Performance Evaluation:

Acceptable

Not Acceptable

No Evaluation

Reported Value falls within the Acceptance Limits.

Reported Value falls outside the Acceptance Limits.

Reported Value cannot be evaluated.

ERA's WS-234 WatR™Supply Proficiency Testing study has been reviewed by ERA senior management and certified compliant with the requirements of the 2009 TNI PT Standards and the criteria contained in the most current TNI Fields of Proficiency Testing (FoPT) tables.

ERA's WS-234 WatR™Supply study standards were examined for any anomalies. A full review of all homogeneity, stability and accuracy verification data was completed. All analytical verification data for all analytes in the standards met the acceptance criteria contained in the 2009 TNI PT Standard and the criteria contained in the most current TNI FoPT tables.

The data submitted by participating laboratories was also examined for study anomalies. There were no anomalies observed during the statistical review of the data.

ERA's WS-234 WatR™Supply study reports shall not be reproduced except in their entirety and not without the permission of the participating laboratories. The report must not be used by the participating laboratories to claim product endorsement by any agency of the U. S. government.

The data contained herein are confidential and intended for your use only.

If you have any questions or concerns regarding your assessment in ERA's WatR™Supply Proficiency Testing program, please contact our Proficiency Testing Department at 1-800-372-0122.

The Method Description is the method the laboratory reported to ERA.

=

=

=

The Reported Value is the value that the laboratory reported to ERA.

The ERA Assigned Values are compliant with the current TNI Fields of Proficiency Testing (FoPT) tables. A parameter not added to the standard is given an Assigned Value of "< PTRL" per the guidelines contained in the 2009 TNI Standards. The assigned values are directly traceable to the commercially prepared starting materials used to manufacture the PT standards.

The Acceptance Limits are established per the criteria contained in the most current TNI FoPT tables, or ERA's SOP for the Generation of Performance Acceptance Limits™ as applicable.

Not Reported No Value reported.=

Study # : WS-234

2009 TNI Evaluation ChecksThere are no values reported with < where the assigned value was greater than 0.

2009 TNI Not Acceptable EvaluationsThere were no Not Acceptable evaluations for this study.

16341 Table Mountain Pkwy • Golden, CO 80403 • 800.372.0122 • 303.431.8454 • fax 303.421.0159 • www.eraqc.comPage 1 of 1

Study # : WS-234All analytes are included in ERA's A2LA accreditation. Lab Code: 1539-01

Donny JuarezQuality Assurance ManagerEnergy LaboratoriesPO Box 247Casper, WY 82602307-235-0515 x3244

EPA ID:ERA Customer Number:Report Issued:Study Dates:

WY00002E77282802/29/16

01/11/16 - 02/25/16

WS-234 Laboratory Exception Report

Final Report Results For Laboratory Energy Laboratories

16341 Table Mountain Pkwy • Golden, CO 80403 • 800.372.0122 • 303.431.8454 • fax 303.421.0159 • www.eraqc.comPage 1 of 3

Study # : WS-234

Study:

ERA Customer Number:

Laboratory Name:

WS-234

E772828

Energy Laboratories

Organic Results

2009 TNI Evaluation Report

16341 Table Mountain Pkwy • Golden, CO 80403 • 800.372.0122 • 303.431.8454 • fax 303.421.0159 • www.eraqc.comPage 2 of 3

Study # : WS-234

Donny JuarezQuality Assurance ManagerEnergy LaboratoriesPO Box 247Casper, WY 82602307-235-0515 x3244

EPA ID:ERA Customer Number:Report Issued:Study Dates:

WY00002E77282802/29/16

01/11/16 - 02/25/16

WS-234 2009 TNI Evaluation Final Complete Report

TNIAnalyteCode

Analyte Units Reported Value

Assigned Value

Acceptance Limits

Performance Evaluation Method Description Analysis

Date Z Score Study Mean

Study Standard Deviation

Analyst Name

WS Carbamate/Carbamoxyloxime Pesticides (cat# 846, lot# S234-707)

7010 Aldicarb µg/L 20.4 17.5 13.1 - 21.9 Acceptable EPA 531.1 3.1 1995 2/5/2016 1.84 17.3 1.66

7015 Aldicarb sulfone µg/L 27.4 23.1 17.3 - 28.9 Acceptable EPA 531.1 3.1 1995 2/5/2016 2.82 21.5 2.08

7020 Aldicarb sulfoxide µg/L 20.9 20.9 15.7 - 26.1 Acceptable EPA 531.1 3.1 1995 2/5/2016 0.0523 20.8 1.52

8080 Baygon µg/L 38.4 36.3 29.5 - 43.1 Acceptable EPA 531.1 3.1 1995 2/5/2016 1.72 34.5 2.25

7195 Carbaryl µg/L 20.7 19.6 14.7 - 24.5 Acceptable EPA 531.1 3.1 1995 2/5/2016 1.57 18.5 1.43

7205 Carbofuran µg/L 27.5 26.2 14.4 - 38.0 Acceptable EPA 531.1 3.1 1995 2/5/2016 1.27 24.5 2.39

7710 3-Hydroxycarbofuran µg/L 25.0 23.0 18.4 - 27.6 Acceptable EPA 531.1 3.1 1995 2/5/2016 1.17 22.7 1.95

7800 Methiocarb µg/L 35.8 37.4 29.2 - 44.6 Acceptable EPA 531.1 3.1 1995 2/5/2016 1.91 32.5 1.73

7805 Methomyl µg/L 26.7 23.9 19.1 - 28.7 Acceptable EPA 531.1 3.1 1995 2/5/2016 1.64 24.0 1.67

7940 Oxamyl (vydate) µg/L 41.6 37.9 28.4 - 47.4 Acceptable EPA 531.1 3.1 1995 2/5/2016 1.50 37.6 2.68

16341 Table Mountain Pkwy • Golden, CO 80403 • 800.372.0122 • 303.431.8454 • fax 303.421.0159 • www.eraqc.comPage 3 of 3

Study # : WS-234All analytes are included in ERA's A2LA accreditation. Lab Code: 1539-01

Final Report Results For Laboratory Energy Laboratories

16341 Table Mountain Pkwy • Golden, CO 80403 • 800.372.0122 • 303.431.8454 • fax 303.421.0159 • www.eraqc.comPage 1 of 3

Study # : WS-234

Study:

ERA Customer Number:

Laboratory Name:

WS-234

E772828

Energy Laboratories

Organic Results

2003 NELAC Evaluation Report

16341 Table Mountain Pkwy • Golden, CO 80403 • 800.372.0122 • 303.431.8454 • fax 303.421.0159 • www.eraqc.comPage 2 of 3

Study # : WS-234

Donny JuarezQuality Assurance ManagerEnergy LaboratoriesPO Box 247Casper, WY 82602307-235-0515 x3244

EPA ID:ERA Customer Number:Report Issued:Study Dates:

WY00002E77282802/29/16

01/11/16 - 02/25/16

WS-234 2003 NELAC Evaluation Final Complete Report

NELAC Analyte

CodeAnalyte Units Reported

ValueAssigned

ValueAcceptance

LimitsPerformance

Evaluation Method Description Analysis Date Z Score Study

Mean

Study Standard Deviation

Analyst Name

WS Carbamate/Carbamoxyloxime Pesticides (cat# 846, lot# S234-707)

7010 Aldicarb µg/L 20.4 17.5 13.1 - 21.9 Acceptable EPA 531.1 3.1 1995 2/5/2016 1.84 17.3 1.66

7015 Aldicarb sulfone µg/L 27.4 23.1 17.3 - 28.9 Acceptable EPA 531.1 3.1 1995 2/5/2016 2.82 21.5 2.08

7020 Aldicarb sulfoxide µg/L 20.9 20.9 15.7 - 26.1 Acceptable EPA 531.1 3.1 1995 2/5/2016 0.0523 20.8 1.52

8080 Baygon µg/L 38.4 36.3 29.5 - 43.1 Acceptable EPA 531.1 3.1 1995 2/5/2016 1.72 34.5 2.25

7195 Carbaryl µg/L 20.7 19.6 14.7 - 24.5 Acceptable EPA 531.1 3.1 1995 2/5/2016 1.57 18.5 1.43

7205 Carbofuran µg/L 27.5 26.2 14.4 - 38.0 Acceptable EPA 531.1 3.1 1995 2/5/2016 1.27 24.5 2.39

7710 3-Hydroxycarbofuran µg/L 25.0 23.0 18.4 - 27.6 Acceptable EPA 531.1 3.1 1995 2/5/2016 1.17 22.7 1.95

7800 Methiocarb µg/L 35.8 37.4 29.2 - 44.6 Acceptable EPA 531.1 3.1 1995 2/5/2016 1.91 32.5 1.73

7805 Methomyl µg/L 26.7 23.9 19.1 - 28.7 Acceptable EPA 531.1 3.1 1995 2/5/2016 1.64 24.0 1.67

7940 Oxamyl (vydate) µg/L 41.6 37.9 28.4 - 47.4 Acceptable EPA 531.1 3.1 1995 2/5/2016 1.50 37.6 2.68

All analytes are included in ERA's A2LA accreditation. Lab Code: 1539-0116341 Table Mountain Pkwy • Golden, CO 80403 • 800.372.0122 • 303.431.8454 • fax 303.421.0159 • www.eraqc.com

Page 3 of 3Study # : WS-234

CERTIFICATE OF EXCELLENCEIn recognition of the quality of your laboratory in proficiency testing for

WS-234Energy Laboratories

is issued this certificate of achievement by ERA. This laboratory has been recognized as a Laboratory of Excellence for achieving 100% acceptable data in this study which included 690 participating laboratories. This achievement is a

demonstration of the superior quality of the laboratory in evaluation of the standards listed below.

Carbamate/Carbamoxyloxime Pesticides

Patrick LarsonQuality Officer E772828