scanning electron microscope · the first scanning electron microscope (sem) debuted in 1938 ( von...
TRANSCRIPT
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CHARACTERISATION TOOL FOR BIOMATERIALS
SCANNING ELECTRON MICROSCOPE
GAUTAM KKS
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Electron Microscopy
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High Voltage Unit
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Online UPS
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Chillar Unit
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• mean free path of electrons v short in air
- at least 10 -5 mbar usually aimed for
• also
- tungsten filaments burn out in air
- columns must be kept dust free
• achieved by 2-fold pumping:
rotary (mechanical) pump + diffusion pump
or + turbo pump
why high vacuum ?
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Rotary Pump
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how does a diffusion pump work?
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Defusion Pump
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Sputter Unit
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Gold Plate
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the electromagnetic lens
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(SEM) and TEM
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ANT
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ANT EYE
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ANT LEG
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TEFLON TAPE
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FIBERS
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FRACTURED 1
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FRACTURED 2
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AL CU MICROSTRUCTURE
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NANOPARTICLES
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WEARED SURFACE
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WEARED SURFACE 2