sampling data documents (part 3 of 7) · tmpls ids &9918a le ids r2587 deceived s q4/07/89...

1ftVOLATILE ORGANICS ANALYSIS DATA SHEET

EPA SAMPLE NO.

b N,

V . b C<

Matri

Sampli

Level

x Moi«Columi

-

\ .

ftmea VgRSAR.INC

3de: VgRSAR

< : (soil/water)

r wt/vol:

: (low/med)

Kture: not dec.

i: (pack/cap)

CAS NO.

74-87-3 —————t. 74-83-9 —————75-01-4 —————75-00-3 —————75-09-2 —————67-64-1— ———75-15-0 —————75-35-4 —————75-35-3 —————

67-66-3 —————1O7-06-8 ————78-93-3 —————71-55-6 —————36-23-3 —————108-05-4 ————75-27-4 —————78-87-5 —————10061-01-5 ——79-01-6 —————124-48-1 ————79-00-5 —————71-43-3 —————10061-02-6 ——75-as-a ———108-10-1 ————591-78-6 ————187-18-4 ————

108-88-3 ————108-90-7 ————100-41-4 ————100-43-5 ————1330-20-7 ———107-02-fl ————107-13-1 ————

11 EDG89DL /

a. ... _ __„ Contract : _ , _ 1

Case No. : IiZ24_ S^S N°- ' 45321

WATE.R Lab S.

-SSi.2 <g/n»L) QU _ L*b Fa

L.QW __ Date F

Date t

PQQ& _ Dilut:

CONCENTRATICCOMPOUND <ug/L or ug/

—— Chloromethane. ____________—— Bromomethane ___ _______—— Vinyl Chloride _____ ___ __—— Chloroethane.. _____________—— Methylene Chloride _____ __—— Acetone ___ _ _ _____ __—— Carbon Bisulfide ___ ___ _—— 1, 1-Dichloroethene __ __ _.—— 1, 1-Dichloroethane——1. 2— Dich loroethene (total)—— Chloroform—— 1,2-Dichloroethane __ ___ _—— "a-Butanone _.__. ___ _____—— 1, 1, l-Trichloroethanew __ __

—— Vinyl Acetate ... __ ___ _

—— 1, 2— Dich lor o pro pane— — cis-l,3,-Dichloropropene ____—— Trichloroethene. __________

—— 1, 1,2-Trichloroethane—— Benzene .—— -Trans-1, 3-Diohloropropene _ , _—— Bromo form—— 4-riethyl-a-Pentanone- _—— a-Hexanon* _ .^ . _ __ _—— Tetrach loroethene _ _—— 1, l,a,a-Tetrachloroethane _ . _——Toluene—— Chlorobeniene --B _ ___ _—— Ethylbenzene.. _____ __ ___— "— Styrene—— Total Xylenes __ ____ __ . _—— Acrolein. _______________ , _—— AcrylonitTile _ _____

I _ SDO No. s EAG 37 fl&0^

impla ID: 6 9gS£

Lie ID: R3&I7 ___

Deceived: Q4/07/89

Analyzed! Q4/i9/89

ton Factor: §000

]N UNITS:'Kg) UQ/U_ Q

1380 IU210 IUS60 IU190 IU230 IU2000 IU230 IU80 IU87 !U250 IU100 IU120 IU1400 IU120 IU110 IU340 IU190 IU140 IU170 IU120 IU160 IU230 IU100 IU240 IU210 IU270 IU2300 IU38000 1 D

220 1 U120 IU120 IU130 IU210 IU200 IU6500 1 U2900 IU

FORM I VOA 1/87 Rev

IE EPA SAMPLE NO.VOLATILE ORGANICS ANALYSIS DATA SHEET __

TENTATIVELY IDENTIFIED COMPOUNDS I II EDG89DL I

b Name: Vgg§AR_iy£a. _____________ Contracts __________ I ______________ I

-- -b Codas VERSAR.. Case No. s H23i. SAS No. a 45537E _ SDG No.: £80.37

Hatrixs (soil/water) UA!gR_ Lab Sample IDs &22S3G ______

Sample wt/vol: .i3i2 <g/mL) QU _ Lab Fil« IDs

L«v»ls <low/m*d) UQy __ Data Rec«iv«d s

% Moisturas not d»c. ___ Data Analyzads Q4

Column (pack/cap) £BQ£ _ Dilution Factor: §000

CONCENTRATION UNITSaNumbar TICs found: _ 0 <ug/L or ug/Kg) Ug ^^ (

1 CAS NUMBER 1 COMPOUND NAME I RT I EST. CONC. I Q I

FORM I VOA-TIC 1/S7 Rev.

100501

1AVOLATILE QRGANICS ANALYSIS DATA SHEET

EPA SAMPLE NO.

b Names VERSAR IMQ

b Codes ygRSAR_

Matrix : (soil /water)

Sample wt/vols

Level ; (low/med)

X Moistures not dec.

Column: (pack/ cap)

CAS NO.

74-87-3 —————74-83-9 —————75— A1 —A— ——— — —

75-00-3 —————73-09-2 —————67-64-1 —————7S-1S-0 —————73-33-4 —————73-35-3 —————54O— 5Q— O— — • -— —tJ-T'tt W 7 V

67-66-3 —————107-06-3 ————78-93-3 —————

108-03-4 ————

78-87-3 —————10061-01-3 ——79-01-6 —————134-48-1 ————

71-43-3 —————10061-08-6 ——73-33-3 —————ioa-io-1 ———391-78-6 ————127-18-4 ————

108-88-3 ————108-90-7 ————100-41-4 ————100-42-3 ————1330-20-7 ———107-03-8 ————107-13-1 ————

' ^. '1 EDG9& «,' -TM».* 1

a. __ Contracts _ 1 _______ ._ _ „ _ __ 1

Case No. s i!7g4 SAS No. s 4S37E SDG No.: EAG 37

yATiR. Lab Si

-§§±.2 <g/mL) ML _ Lab Fi

L.QW __ , Date F

___ Date f

PAgK _ Diluti

CONCENTRATICCOMPOUND <ug/L OT ug/

—— Chlorometh*ne_ _ _____—— Bromomethane _ _ __ _—— Vinyl Chloride _ _ _— — Chlbroethana—— Meth/lene Chloride—— Acetone ___ _ __ _—— Carbon Disulfide _ __ _—— 1, l-Dichloroethene_ _—— 1, 1-Dichloroethane.. ______—— 1,3-Dichloroathene (total) __—— Chloroform ___ _ __ __—— 1, 3-Dichloro»thane_ __ __—— 3-Butanone_ __ ___ ______ _—— 1, 1, 1-Trichloroethane ___ _——Carbon Tetrachlor ide—— Vinyl Acetate^ __ ________

—— ci»-l , 3, -Dichloropropene __—— Trichloroethene—— Dibromochloromethane—— 1, 1, a-Trichloroethane _ ___—— Benzene _.. _ _ _—— Tran»-l, 3-Dichloropropene ___—— Bromoform . __ ___ __ ___—— 4-Methyl-a-Pentanone—— a-Hexanone__ _ _ _ __- — Tetrachloroethene _ _- — 1, 1, a,a-Tetr*chloroethane ___—— Toluene_ _—— Chlorobenzene^ _ _ __ ___—— Ethyl benzene _ „ ___—— Styrene _______ __ ____ __—— Total Xylene* _____—— Acrolein __ _ ___—— Acrylonitrile

tmpls IDs &9918A

le IDs R2587

deceived s Q4/07/89

Analyzed! Q4/17/89

.on Factors 5.0

3N UNITS:'Kg) UG/L. Q

I0.4IUo.aiu0.910.3IU0.3IU3 10.21U0.08IU0.911 I0.1IU0. 1 IU1 PU0.1IU0.1 IU0.3IU0.2IU0. 1 IU0.2IU0.710.2IU0.2IU0.310.3IU0.2IU0.3IU2 IU2 I0.2IU0.210. 1 IU0.1 IU0.2IU0.2IU7 IU3 IU

1FORM I VOA 1/87 Rev.

200001

IE EPA SAMPLE NO-VOLATILE ORGANICS ANALYSIS DATA SHEET ______________

TENTATIVELY IDENTIFIED COMPOUNDS II ED090

b Names V R S R I N Contract: I

' b Codes VER§AR_ Case No. s HZ84. SAS No.: 453?g_^ SDO No.:

Matrixs (soil/water) WAT£R_ • Lab Sample IDs

Sample wt/vol: _13i2 <g/mL> QL, _ Lab File IDs BiS§7 _____

Level: <low/med) L.QW __ Date Receiveds Q4/07/Q9

% Moistures not dec. ___ Date Analyzed s Q4/I?/g9

Column (pack/cap) PBC.£ _ Dilution Factor: 3 0 ___

CONCENTRATION UNITSsNumber TICa found: _ Q <ug/L or ug/Kg) UQ^L-^ • • B * •• • •••t «Mf « -4 ^ *B ^ « «»4 ^ ^ *» « ^ i «** ^ ^ < ^ ^ B * - »••«>«• •••H «* •* ••

I I l i l tI CAS NUMBER I COMPOUND NAME 1 RT I EST. CONC. I Q I| *mmmmmmmmmmmm*mtt \ *mn*mm**mmmmmmm*mmmmmmmmmmmma \ BHVHOMH | mmmnmmmttaaasmm | R M B K H |

!„ ____ ^ _______ I _____________________________________ I ___________ I __________________ I _______ I

FORM I VOA-TIC 1/fl? Rev.

200002

UH1TCO STATU WWOliNCWTAL FtOTtCTIOH ACEKCfv .t$3/Cefttril Regional Libornory

OATA TRACK I MC FORK FOR CONTRACT SAhPLtS

CRl Oata Set No.

SrtO Case Noman*. MiDWo 793 rot,

. ;/7^VA4S*tt37£l«tt Bat and location:

He.1.

r of. Contractor or tPA laboratory: m__________

of Stoolts: / 7 Oata Stales or Data Received:

Oata Pier; « M

-r?Havt chafn-of-custody rtcoMs bten recaNtd? TES ^ HOHave Teattic Reports or packing lists been recetvTdl" TtIf no. art T r a f f i c Report or packing lijf numbers written on the cnaio-of-custedyrecord? t£S «0__If no, which Traf f i c report er packing list ambers art Kissing?

Arc basic data foras In? T£3_

Ifumber of sauries claimed:

T Iced by: s\Jt

Mu&btr of saffiples received:

Data:17

Received by Contract ftrfeject Kan«ge«ent Section: </J//L/fL. D»te;

Started*: 5.3.5, 19__________ Reviewer Signiturt: &•S'-JQ

Total ti*e spent en

Copied (xeroxed) by:

Oate review completed: JT 33. £3

Mailed to Data User by:USERS:

Fleast f i l l 1n tht blanks beto* and rttura this fora to: SjUia Criffin. OataManagement Coordinator. Region T. SSCRL

Data received by:

Q.A. review received bj:

Inorganic Date Complete [ 'Organic Oata CompleteDiei inUata CompleteSAS Oata Complete

Cite:

fi&te:

I, Suitable for Intended Furpeics '! 1 /t 3 If acceptable.. Suftablt for Intended Furposes, Suftablt for Intended Fyrposes. Suitable for Intended Purposes

List prebJeos belo«»

* Attached 'Hissing Oata Reeuest For** [ ]JBLEMS: Flcase indicate reasans [if »ny] *hy data art not suitable for jour uses

Other problems*

Received bv Data Management Coordinate^ CRU for File: Date:.

79-7S;

\jvo-

TOTb

OFUNITED STATES ENVIRONMENTAL PROTECTION AGENCY

HEG1ON V

DA (L^^ J> I

: R*V1e« of Region V CLP Data ^ ,Receded for Review on ^- / 0 - 79

-no«. Cartls loss. Director (5SCRL)Central Regional Laboratory

User;

Ve have reviewed the data for the following case(s).

31T£ KArg; ju^^^ ^ T • $MO Case Ho, / / 7 ^ V J / ? 5 V.C3 7 £7~ " to. of D.O.Mctlvltjr /,

IPA Data Set Mo. $ Ft, 074 f_ft Samples; J.D Numbers TFA/TFA ItiJ' L -—— - .___.

CRL

Traffic Ho. Ef\LL3 ED&22 35 £2 -ft & 0- ^T 7*~ 7,f 77.^x- ' •* ' :) ' Hrs. Required

CLP Laboratory: It ts^*^ _____________________ for Review:

»re our findings; "7^^ c / ^ C e^ / ?, //

0V/

\J(JjM

.Data are acceptable for vse.Data are acceptable for vse with qualifications referenced above.See Data Qu4l1f1er sheets and Calibration Outlier forms for flags and << /-* A / <& &additional comments. ^ / s^f/ ^>JJata are preliminary - pending verification by Contractor Laboratory.See Case Sunnary above*

) Data are unacceptable.

Carla Oeiipsey.CLP Quality Assurance Officer. Analytical Operations BranchJames Petty. Chief Quality Assurance Research. EttSL. Las Vegzs

DATA QUALIFIERSMGE _Z-~flF

Contractor: // I| Case // 72^

ttlow 1s a ftuaaarj of tht out-of-control audits and tnt posslblt tfftct on thedata for tftU case:

//

r*— -Rtvltvtd by:

Oatt:

OATA QUALIFIERSM6E < OF

Contractor: case

ftlow 1s • Sumnarjr of the out*of»contro1 audits and th* postlolt tfftct on thefata for this cast:

f^TTU- isKV2> - 77

-/Jl rta^

^L

gDC-

/J

PDP.

a L,

T7

ttvlcwtd by:Phone:Oatt:

- 3 O ~

/

OAT* QUALIFIERS

Contractor: | CastI___

ttlov 1s • tumarj of tht out-of»contfol audits and tnt toulblt tfftct on*ata for this case:

/L / Lei

6L*d-A uS>-^/ ~i%~ lO//-^/- i^^Oti-j 4£zj&>/</

<psb-r-s~t~ cLJrg^u-gy^g ipp . ~t£*^<Jkn Lr^

if h r*sr£~+i.

'.ilttjlii<AJjfc* _

Mvlcved bv;">one:

UNITEO STATES ENVIRONMENTAL PROTECTION AGENCY REGION VCALIBRATION OUTLIERS

VOLATILE HSL COMPOUNDS

PAGE5 OF

CASE/SAS

Instrument * V 5d-t>oDATE/TIME: '

ChloromethaneBromomethaneVinyl ChlorideChloroethaneMethylene ChlorideAcetoneCarbon nisulfide1 tl-Dichloroethane1,1-Dichloroethene

!Trans-l f2-DichloroetheneChloroform2-Butanonel,2*Dichloroethane1 ,1,1-TrichloroethaneCarbon Tetrachloride

(Vinyl Ace ta teBromodi Chloromethane1,2-Dichloropropane

jTrans-l,3-DichloropropeneTrichloroetheneDibromochloromethanel_Il_,2-Tri ChloroethaneBenzene •cis-1.3-Dichloropropene2-Chloroethyl vinyl etherBromoform4-Methy 1-2- Pent anone2-HexanoneTetrachloroethene1.1.2.2-TetrachloroethaneTolueneChlorobenzene

JEthylbenzeneStyrenem-Xyleneo/p-Xylene

yAFFECTED /SAMPLES: ^Sj* J

^7ji&jfaJ£^

Reviewer's ^^^^fjf^Initials/Date: ^wfa.?*

/ 'f

Inv-f^RF

f/ftF)?

^7><1?

/*T>£T)FpfrQ

.. Ca5/f^JaRSD

ULf7Lb?c>i*,^ */G*r?G~SZG-ST:C^C

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lb

t .

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kl-. L«

ib

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Com

kl-

•

. Ca

tb\ .•jt

* These flags should be applied to the analytes on the sample data sheets.

CASE/SAS

UNITEO STATES ENVIRONMENTAL PROTECTION AGENCY REGION VCALIBRATION OUTLIERS

VOLATILE HSL COMPOUNDSCONTRACTOR

PAGE_£_ OF~*-

Instrument f V5-4-froDATE /TIME: /

/ChlopomethaneBromomethaneVinyl ChlorideChlOPoethaneMethylene ChlorideAcetoneCaPbon nisuifide1.1-DichloPoethane1,1-DichloroetheneTrans-l,2-DichloPoetheneChlorofopmZ-Butanone1.2-DichloPoethane1,1, 1-T ri ChlOPoethaneCaPbon TetpacnlopideVinyl AcetateBrofliodi chl oromethaneI.z-DlchlopoppopaneTpans-1 ,3-DichloropPOpeneTrichlopoetheneDibpomochlopomethanel_,l,2-Tpi chlopoethaneBenzene -cis-1 ,3-DichloPOpPOpene2-ChloroethylvinylethePBromoform4-Methyl-Z-Pentanone2-HexanoneTetrachlopoetnene1 ,1 ,2,2-TetPachloPoethaneToluene

IChloPObenzeneEthylbenzeneStyrenem-Xyleneo/p-Xylene

AFFECTED /SAMPLES: ^£.R e v 1 ewe PS ^ / *,.Initials/Date: %-& n/IMfc/

Init. Ca .W/&& 'tti/eRF

,' -• -• 0H

IRSD •

Cont. Cal .S/rfRF

, - : iJfii

ff.f^^ID

- :-.S1&1

*

1<J

lmU£-UJ4>f 06-<7A&DG- ?¥ DL£7)6-55fDcr^$M£/Jt&

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IH J f^ZfJi

lb {*

//^i*C-3O^DG- ^/

b

Cont. Cal .

RF" iu V

dont. Cal.

RF lb *

•

* These flags should be applied to the analytes on the sample data sheets.

Cr£V£7?AL'E)AyaFor reporting raeults tr **JS) UftUa, tha following contract specificqualifiers arc to b* used. The eer*n qualifier* defined b«low«eg subject to mortification by the laboratory. Up to fiv«qualifier* Bay b« reported «n Form I for each ei

The sc-ven EPA-dafinod qualifiers to ba used are aa follows:

.U - ladieataa \. \mymmA mu analyzed for but not dataetad. Thesample quantltation limit must be eorractad for dilxition. andfor pareane •oiatora. For «xavpl*( 10 U for phaaol la vatar ifCha saapla final oluaM la tha protocol-cpacifiad final valuaa.If a 1 to 10 dilution of aareract ia aaeaaaary, tha raportadlimit t» 10O 9. For • •oil MMpla, tha valua moat Alia b«adjuatad for paroanc •oisttxra. For axa la. if tha saapla had24% •oiator* jad • 1 to 10 dilation factor, tha saaplaquantitadon limit for phanol (330 0} would ba eorroetad to:

100

and df - dilution factor

at 24% moisture. 9 • 100-34 - 0.76100

f33Q Tn x 10 • 4300 U rounded to the appropriate number of.76 significant figures

* *

For soil samples subjected to C?C clean-up procedures, the CKQLIs also multiplied by 2, to account for the fact that only ha£±of tha extract is recovered.

* Indie etas aa estimated value. This flag Is used either whenestimating a concentration for tentatively identified compoundswhere a 1:1 response is assumed, or when the mass spectral dataindicate the presence of a compound chat meets theIdentification criteria but tha result is less than the samplequant!tation limit but greater than xero. For example; if thesample quantltatioa limit is 10 ug/L, but a concentration of 3ug/Z. ia calculated, report it aa 3J. The eample quantitatlon

-t*MJR «U«L 1» Miljuaead t** fcfljfo rfit»i*-frwi »~A p^fg^f •«<«!

as discussed for tha V flag, so that If a sample with 24%moisture and a 1 to 10 dilution factor has a calculatedconcentration of 300 ug/L and a sample quantltatlon limit of430 ug/kg, report the concentration as 300J en Form I.

C - This flag applies to pesticide results where the identificationbaa been confirmed by CC/US. Single component paatlcldaang/ul in the final extract shall bo confirmed by CC/MS.

1-29 2/88

- T*«- flag 1* «»*d **•» «*» analyt* is found lablank as wall as in tfa* aampl*. It Indicates posaibla/probabl*blank contamination and warns tfa* data ms*r to tafc* approprlac.Action. This flag must b* used for a TIC as well as for apositively identified TCL compound.

- T**« flM identifies compounds vhoa* concentrations oxc**d th«calibration range of tfae CC/MS instrumenC for that •pacificanalysis. This flag will aa* apply to p*sriddes/rc*a mnalyz.d^^ ,«. *^ Borfanrta If one or more compounds bare a response

"tfaan full aeale, the aample or oxcract must b*ro-aaalTXod aceordlnc to tfao •poc«uch eo-pgmidt vltb a TMp«tt*o crutor than full •**!*ldhaWS* nuucouKaH nn flat*.* with « T « th. T

for tfao OTlciaal «naly«l«. If tfao dilution of tfa« oxtract

eaiibraciaa ran«« inin th

ooc -th«-« *p .* *••»•••»•• • •— — — —— — - __of both aaalyaa* •ball b« roportod on aaparata Fornj

Tha For. I for tho dllotad aa la oiuU b-*« th. W M££ i«op«nd«d to tfaa •aa lo «-b*r. POTZ: For total xyl««. w*Srao Uo«ars ara oîantiflod aa tw p^ks. tfao calibrationTanc« of ««eH t»««lc should bo considarad aaparataly. o.f. . adllutad analT«l» ±M aflt t*<Tul«d for total xylanoa onlaas thco«s«oatlon of oltfaor p«ak •aparataiy aacooda 200 ut/I..

D . This fl*i Idontlfiaa all eoaôunda idonrdfiod in an aaalyaisaacondary dilution factor. If a aa«pla or axrraet Is

•« aacon .ro-aaalrc«d at a hlgbar dilution factor. «• to tha •£aboô. th* "W." «utti* !• «PP«n^«d to tfa* M«pl« mab.rTor» I for th* dllutad aaapla, and all concentration vala«roportad on that Tor« I ar« flau*d irirfa th* •»" flag.

A - This flaf todtcata« that a TIC Is a *u*p*ct*daldol-«ond«ns*tlon product.

X - Oth*r «p«clflc fla»s may b« r*qulr«d to proptrly d*£in* =*«r*«ults. If u«*d. th«y a«Jt b« fully d*acrib«d and auchd«crlptlon attached to th. Saapla l>ata Sunary Packaj* and -.C«a* Karr*tiv.. B*tto by usln» -XV If m»r* than on* flaj iEvquizw««» «*»w * ••-• • • -• " ——— • ———— r — r^— >.ojuallflars ar« xo«iilr*d for a Mapl* r»*ult. na* th* -X flasCo coablao a«r*ral flag*, •» n**dod. For iaatanc*. th* -Xflag might aombino tfao «A". "»-. «d "0" fl*g« for ooa« aa

Tho combination of flags "»T or-OT- I* oocproatly prohlbltad. »!..contaminants aro flagg.d •»" «i1^r whoa th«y ar. also d*e.ct*d In -aaapl*.

If analvv«« at two dlff.mt dilution f^ceora or* rooiiirodExhibit* D}, folio- th* data reporting Instructions glv«n In0 ard with th. "D- and "I" flag* abova.

1-30

APR 2 7 1550c c

CASE NUMOtll/SAS No.

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THIS FORM IS TO BE USED FOR SAMPLES SENT TO CONTRACT ONLY

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USEPA CONTRACT LABORATORY PROGRAMSAMPLE MANAGEMENT OFFICE \P.O BOX B18 ALEXANDRIA. VA 22313703'557-2490 FTS-557-2490

(TF APPLICABLE)'

ORGANIC TRAFFIC REPORT

TYPE OF ACTMTY (CIRCLE CM (J)SUPERFUNO—PA SI ESI RP& RO RA ER

NPtO O*MNON-SUPERFUNO—____ .PROGRAM

(ENTER INi. SURFACE2. GROUND WATJ*G3.LEACHAT*

•xu

REJMQN & .<P ..

SAMPLER: (NAM^

SHIP TO:

SAMPUMQ

DATE REC'D: SOG NOT"

O BY:

LABORATORY CONTRACT NO. UNIT PRICE

IIWHWRH Tft DATE REC'D: <2>

RECTO BY: CONTRACT NOJPRICE:

CLPSAMPtffNUMBER

^

k flANALY90

SPECMLHANDLING

STATIONLOCATION

SAMPLECONOfTIONON RECEIPT

PHASES(CHECK)

52.53

•:ur xV

-a^5

f k o r j-iEPA Fonn 2075-« (i-«7)

WHTTE - SUQ COPY PINK — CLIENT COPY WHITE.- LAB-COPY FQfl RETUflN.TaSUa YELLOW — LAB COPY

'~™n r°?yy

**re irret&Jf (7

Hay 3, 1989

I. NarrativeOrganic* Caae 11724 SAS* 4S37E SDG* EAL69EPA Raglan V - Curt i a Roaa

- - Verear Project 969.80 - Batch 6

Thia raport contain* the CLP analytical data for the volatilelov detection Halt organic analyaia of twenty (20) water aampleecontained in Caae 11724 SDQ EAL69. The eample* Hated belowarrived Intact at Veraar by Federal Expreaa on April 6, 1989.

LISTEAL69 * ED060EDG22 EDG61EDG39 EDG62EDGS2 EDG63EDG33 EDG64EDGS4 EDG6SEDGS9 EDQ74EDG96 EDG75EDGS7 EDG77EDG58 EDG81 •*

• - Firat aaaple in SDG. »* - Laat aaaple in SDG

*****************************************************************SAS ONLY

No Diskette DeliverableSeven day aample holding time30 day hardcopy report due dateLow Detection Limit Analyaia

•Acrolein & acrylonitrila added to volatile target compound liat*

GC/HS inatrument calibration* uaing BFB met contractrequirement* for volatile analyai*. SPCC and CCC criteria weremet for the volatile initial calibration curve* and continuingcalibration check atandardS. All GC/HS analy*** occurred duringthe twelve hour period following daily instrument calibration. Aholding time extension waa granted by the Region aince the numberof aamplea being ehipped on a weekly baai* exceeded the numberthat were acheduled.

All volatile Internal standard area abundance* and relativeretention time* were compliant for all analyee*.

Volatile aurrogata atandard recovery value* met all apecifledQC limit*. One eat of matrix *pike/matrix apike duplicateanaly*!* wa* performed in conjunction with thia SDG.

J00005

«c

Narrative - Page 2Veraar Project 963.80 Batch 6

Saaplea were acreened prior to analyala and it vaadetermined that EDG33, EDQ37, EDG38, EDG61, and EDG62 requireddilution in ord»r to quantify targvt oowpound* within th»calibration rang* of th* curv*. Dilution iaetora for »aeh aanpl*are liat»d on th* individual Fora ZA. No oth»r aaMpl»« raquiraddilution* prior to analyais.

Pleaa* contact Clay Haan«r* CLP Project Manager, ahould youhave any queationa or require additional inforaation pertainingto the low detection liait analyaia of theae water aaaplaa.

Releaae of the data contained in thia hardcopy data package haabeen authorized by the Laboratory Manager or hie deeignee, aaverified by the following aignaturet

_ May 3, 1989Linda E. BockQC/MS Data Proceaalng CoordinatorLaboratory Operationa

100006

Lab Name i

Lab Code i

anWATER VOLATILE SURROGATE RECOVERY

VERSAR Contract i____.

VERSAR Case No. 111734 SAS No. I4537E SDG No.i EAL69

I EPA1 SAMPLE NO.

011EAL6902 1 EDG2203 1 EDQ3504 1 EDG5205 1 EDG5306 1 EDG5407 1 ED35508 1 EDG5609 1 EDG57DL10IEDG58DL •1 1 I EDG6012IEDG6113IEDG6214IEDG6315IEDG6416IEDG6517IEDG7413IEDG7519IEDG77201EDGSI21IEDG55M322 1 EDG55 1*5&23 i EDG5724 1 EDG5825 1 VBLK8726 1 VBLK0227 1 VBLK3028 1 VBLK44291301 _____

81(TOL)«

10198969697969699939895959796iaa989610199100969296951019910093_

52(BFB)tt

1021031041051041041021041081061041031011049710310510110110110010396102101103100110

S3(DCE)*

100938996961019610096959693969594949610096991001001011011009696108

OTHER

iimi

.

TOTOUT

000000000000000000e000000000

/•'?.*-• "•

QC LIMITSsi (TOD - Toiu»n«-da (ae-110)32 <BFB> - Bromofluorotjenzene (36-115)S3 (DCE) - 1,2-Dichloroethane-d4 (76-114)

# Column to be used to flag recovery value*

* Value* outside of contract required QC limit*

D Surrogate* diluted out

page _1 ofFORM II VOA-1 100009

.:2c:2 :zc:s-;:2c 3Ai^ATER VOLATILE MATRIX SPIKE/MATRIX SPIKE DUPLICATE RECOVERY

Name- VFRSAR INC_____________ Contract: _________

(t Code- VERSAff Cas* No. : 11724 SAS No. : 4537E SDG No. : EALA9

< - " i x S s i V f t - EPA S a m p l a N o - : EDS55_______

COMPOUND

I .. 1-Dicn I orottntnt ____*•<• icMor oethcnt ._2 = n 2 3 n e.~ -• 1 w s n eI i-. IcTot'S-nrs-rie

SPIKEADDED( ug/L)

500300500500500

SAMPLECONCENTRATION

<ug/L)

03130

1520

MSCONCENTRATION

(ug/L)

230718MOT60351S

MS ! QCX ILlrllTS

REC #; REC.

56 *!61-14581 -171-12O81 176-12790 176-125104 175-130

i

COMPOUND

• n : ? n e1 u 9 n e

SPIKEADDED(ug/L)

500500500500500

MSDCONCENTRATION

(ug /L>«a8sas:ss=BB3aB

223725418583515

MSD%

REC #S WTVvS

45 *328HS6

103

XRPD t

sfs*a*x

22 *4I

351

QC LIMITSRPD

S2S±3B3:S

1414111313

REC.SSBSKB

61-14571-12076-12776-12575-130

n to os used to flag recov»ry «nd RPD values with an asterisk

•> .-'i2'j»i Dutaice of QC limits

--T _L out of _5_ outside limit*In-e Recovery: ^_, out of 10 outside limits

rr^MENTS: CLP, 11724, EAL69, EDG55. L. Mi 69B31A, V* 4ML/100ML, 25ML, 1/25INST V SP-1OOO 45COMIN) TO 225C SC/MIN

FORM III VQA-1 1/87 Rev.

100010

4AVOLATILE METHOD BLANK SUMMARY

Lab Nama i ____VERSAR________ Contract i _________

Lab Cod»iVERSAR C*»« No.i11724 8A8 No.i_4537E SDG No.iEAL69

Lab Fila? IDi _YS387 Lab Sampl* IDi __VBLK87

Dat« Analyzadi 04/15/89 Tim* Analyzvdi 1141

Matrixi (»oil/wat»r) WATER L»v»li<low/m«d> LOW

Iinstrument IDi Y

THIS METHOD BLANK APPLIES TO THE FOLLOWING SAMPLE, MS AND MSDt

t EPA1 SAMPLE NO.

01IEAL690£ 1 EDG7503IEDG8104 1 EDG7705 1 EDG5606 1 EDG5807 1 EDG5408 1 EDG570911011 1 1 __ __121131141151 _ ____161171181191201 _ _21 t22 1 _____ _23 1 _____ _24125 1 __ ___S6I271281291301

LABSAMPLE ID

69823A69839A69840A69841 A69832D69834D69835D69833D

__________

___

___ _ _

_ __

„ __ ____

LABFILE ID

Y5388Y5389Y5390Y5391Y5394Y5395Y5396Y5398

_________

_____ __

TIMEANALYZED

12211305134314241628170917501912

_________

_ _____

IMENTSi

pag» _1 of _FORM IV VOA 100011

r-4*m?: VEP5AR INC.

Code:


________ Contract: ______

ile ID:

Analyzed:

Ca«* No. : 11724

Y5402

04/16/8?

( soii/matfr) i>JATER

ID' Y .

SAS No. : 4S37E SDG No. : EAL69

Lab Samplt ID: VBLK02 ____

Time Analyzed: 16Q6

Level: < lou/med ) ' LQU

HIS METHOD BLANK APPLIES TO THE FOLLOWING SAMPLES. MS AND MSD:

01020304^* ~•~i .— .07OSOr

ERASAMPLE NO-

3 A£RS 3 Wtt SSfttSO

cn£22M^ fc~r>^*i*sy<* Ji^— f, m ~.^.Is'-p-je.~ n .^ • T5D-S60ED 563EDG64EDG65ED574 '

LABSAMPLE ID

698426982469828693296983069825698266982769838

LABFILE ID

YS403Y5412Y5407Y540SY9409Y3410Y5411Y5406Y5405

TIMEANALYZED

173923442019210O21412222230319381956

C-F. - - VELK02, L, W, VBLKQ2, V, , , 25ML1NST V SP-1000 45CC3MIN) TO 225C 8C/MIN

;:;> : ofFORM rv VGA 1/S7 R«v.

100012

L55 Name: VERSAR INC


________ Contract: ______

32 Code: VERSAR Cast No. : t!724 SAS No. : 4537E SDQ No. : EAL69

.at- File ID: Y3444______ Lab Sample ID: VBLK44_____

'at* Analyzed: 04/18/3? Time Analyzed: 1257

'.* cr i x ;*oil/wat*r ) UJATER Levsl: Clou/med)

>.-: rruni*r.t ID: Y_______

LQU

TrtIS MSTH3D BLANK APPLIES TC THE FOLLOWING SAMPLES* MS AND MSD:

04•*"• FL

EFASAMPLE NO.

^aaaiaaaa =EMX

E r.«^«K^r'j3w

P™ "TP-ITr-^^c ™iC.L--J JDwU

EU"»a2£r533WS£E535«S>

LABSAMPLE ID

SEEK xfammmttmmmsK

69S31A69S33C69S34C69S36A69331 A69831

LABFILE ID

Y5449Y5447Y5448Y5432Y5430Y5451

TIMEANALYZED

162315031544134817111748

CL= • .- .. V3LK44, L. W, VSLK44, V, BLANK, , , 25MLIMST Y SP-1000 45C(3MIN) TO 223C 8C/MIN

i cf 1FORM IV VOA 1/87 Rev.

100013


u*c Name: VER5AR INC._____________ Contract: ______

£.: Code: VERgAP Case No. : 11724 SAS No. : 4S37E ' SDC No. : EAL69

4v "ile ID: Y5430_____ Lab Sample ID: VBLK30____

r= Ar.slyretf: QA/17/39 Time Analyzed: 2307

*tr 1 1 . •- soil /'water ) WATER Level: (lou/med) LDU

ID: Y

Th'IS METHOD BLANK APPLIES TO THE FOLLOWING SAMPLES, MS AND MSD:

EPASAMPLE NO.

EDQfe 1

LAB.SAMPLE ID

69837

! LABi FILE ID

,' Y5437

! TIMEI ANALYZED

i 0528

: Er.T= CLF, ,, VBLKSO. L.- w, VBLKSO/ v,,, SSML1NST V SP-1000 45C<3MZN) TO 225C SC/MIN

£*•3ace 1 of 1

FORM IV VOA 1/87 Rev.

100014

" ™-i !• r*T- — R. - — HVOLATILE QR5ANICS

1AANALYSIS DATA

SPA =AHPLESHEET

J-33 Name: vERSAR INC.

Code: VS3SAR C

Contract:VSLKS:

11724 3A5 NO. : 4337E SD<3 No. : SAL6*

M5t-ix: ( soil /water ) U1ATSR Lab Samp It ID: V3LK87

,mn

wt/vol: 55. 0 (g/mL> QL__

(lou//ntd> LOU

;ur»: not dec. ___

(pack/cap) PACK

Lab Fil* ID: Y5337

Data Received: ____

Date Analyzed: 04/15/39

Dilution Factor: 3. 0____

CA3 NO. COMPOUNDCONCENTRATION UNITS:(ug/L or ug/Kg) UQ/L

74-37-3————————Ch ioromethane___________74-33-9———•———Br3tnom*than*__________75-01-4———————Vinyl Chloride__________73-00-3————————Ch lor o«thant____________75-C9-2————————M*thy l«n» Ch lor ide_______67-64-1———————Ac 3 ton*_________________73-13-0————————Carbon Di«ulfid*_________73-35-4————————I, 1-Dich loroethene_______73-33-3———————1, l-Dichloro*thane______340-39-0——————1* 2-Dich lorotthen* < total)67-66-3———————Chloroform^_________„___107-06-2——————1, 2-Dich lorotthan*______73-93-3—— •——-—2-8utanon«______________71-35-c ——————— 1. 1, 1-Trichloroethane____56-23-3———•———Carbon Tttrach lor ide_____103-03-4———•—--Vin'jl Acetat*______~____75-27-4——•——•——Sromodich lorom*than*_____73-87-3———————1. 2-Dicfilaropropane_____10061-01-3—————cis-1.3,-Dichioropropen*_79-01 -e————————Tr i c h 1 or o« t h en * _________124-43-1——————.Di&romochloromethan*^_____79-00-3————————1. I, 2-Tr ich lor oethane____71-43-2————————Ben z e n *_________________73-25-2————————Sromof orm._______________103-10-1———————4-1ethyl-2-Ptntanon«_____591-73-6———————2-H*«anon«______________127-13-4——————Tetrachlorotthene_______79-34-5—— -————1, 1,2- 2-T*trach loroethane^.1 OS-eS-3——————To I u 3 ne.________________103-irC-7——————Ch lorabanzane ____iCO-41-4——————Ethyl b*n:*n»____________100-42-3———————Styrene,________________1330-2C—7——————Total Xyl*n«*____________107-02-3———————Acr o 1 * in________________107-13-1——————Acrylonitrile___________

FORM I VQA

0000050. 2!U

0. 03 !U0. 0?0. 30. 1

. 0. 1* I0. i

u00000000000200-O.-l0. i0. HU0. 2!U0. 2!U7 iU3. :u

1

2;i;2;3!

1

i:3 '

1/97 Rev.

100518

IEVOLATILE ORGAN1CS ANALYSIS DATA SHEETTENTATIVELY IDENTIFIED COMPOUNDS

EPA SAMPLE

Lab Name: VEPSAR INCJi_ab Code: VEPSAfl Casa No. : 11724

'Matrix: ( soil/yat*r) WATER

Sample wt/vol: 23. 0 (g/mL)

Livtl: (low/mad) LOW

% Moisture: not dsc. ___

Cslumn tpack/cap) PACK

?I'iumbar TIC3 found: _Q,

VBLK37Contract:

SAS No. : 4537E SDG No. : EAL69

Lab Sampl* ID: VBLKS7

Lab Filt ID: Y3387

Datt Rtcaivtd: ______„

Data Analgzed: Q4/15/99

Dilution Factor: S. Q____

CONCENTRATION UNITS:(ug/L or ug/Kg> US/L

CAS NUMBER COMPOUND NAME RT EST. COMC.

FORM I VOA-TIC 1/87 R»v.

InCSq. 1AVOLATILE CRGANICS ANALYSIS DATA SHEET

.3D Mam*: VgPSAR INC._________- . Contract: __

EPA SAMPLE

V3LK0

J_3i Coda: VE9SAS Ca«» No. : 11724 SAS No. : 4537E SCO No. : EAL69

Matr i x ; ( soi i/wat*r > UATER Lab Sampl* ID: VSLKO2

Sampl* ut/vol: 23. 0 <g/mL> MJ.__

Ltvtl: ilow/mtd) LOW

: not d»c. ___

Lab. Flit ID:

Datt Rtctivtd

Y34Q2

Ivjmn: (pack/cap) PACK

Dat* Analyz*d: 04/16/39

Dilution Factor: 3. 0___

CA3 NO. COMPOUNDCONCENTRATION UNITS:(ug/L or ug/Kg> UQ/L

74-97-3———————Ch 1 or am*than«___________74-83-9—•—•————Br3moro*than*________.___73-01 -4———————v i n y 1 Chl or i d • _________73—00—3-—— ———Ch loroathan*^_ _____73-09-2——-———M»thy l*n« Chl or id*______67-64— I —————•—-Ac «t a n • ___r_ni______m____a__73-13-0———————Carbon Diiolfid*________73-33-4———————1, l-0ichloro«th«n*_______73-33-3———————1. 1-Dichlorotthan*______340-39-0--—————1- 2-Dichloro«th*n* (total)67-66-3————•——c h 1 o r o form , ,107-06-2——————l, 2-Dichloro*than*_______Va-93-3———————2-Butanon«_____________71-33-6———————!• 1, l-Trichloro*than«____36-23-3———————Car bon T« trach 1 or i d *_j___103-03-4———————Vinyl Ac*t*t»^____________73-27-4———————3romodichlorom»than»_____73-87-3———————1* 2-Dichloropropan*______10061-01-3—————cii-1.3.-Dichloroproptn*_79-01-6——————Trich loro*th*n*__________124-43-1——————Dibromochiorom*than*^_____79-OO-3————————1* 1. 2-Trichloro*than*____71-43-2———————73-23-2————.——103-10-1——————391-73-6——————2-H*xanon«____________127-13-4——————T*trachloTO*th*n*_______79-34-3———————l, 1, 2* 2-T*trachloro«than«.103-83-3——-——Toluan* ___103-90-7——•————C h i or ob *n i tnt__________100-41-4—————100-42-3——————1330-20-7—————Total X«Un««.107-O2-8———————Ac r o I» in107-13-1——————

;u!U!U!U

4iU2!U3JU2iUs:u;u

2;uo. os :uo. 09: uo. 3iu0. 1!U0. 1 !U100000000000020. 1 iUO. 2!U-O.-liU0. 1IU0. 1 !U0. 2!U

2!Ui:u2!U3 J UIU

o.73

!U:u:u

FORM I VOA 1/87 R«v.

100527

IE EPA SAMPLE NO.VOLATILE GR3ANIC3 ANALYSIS DATA SHEET ______________. TENTATIVELY IDENTIFIED COMPOUNDS J

{ VBLK02'_ab Name: VSRSAR INC.____________ Contract: _________ !____________.

'Lib Codt: VERSAR Cas» Mo. : 11724 SAS No. : 4337E SDG No. :

rtatrix: (soil/uattr) WATER Lab Samp It ID: VSLKQ2

Samol* ut/vol: 23. 0 (g/mL) QL_ L*b Filt ID: Y34Q2

Lsval: (low/med) LQU Datt Rtctivtd: ____

:: Moistura: not d»c. _;__ Data Analgrad: 04/16/59

Column -:pack/cap) PACK Dilution Factor: 3. Q

CONCENTRATION UNITS:>uflib»r TICi found: _0. (ug/L or ug/Kg) UQ/L

CAS NUMBER ! , COMPOUND NAME ! RT I EST. CQNC.

tji'i•*i FORM I VOA-TIC 1/87 Rtv.

100528TlJffffiWffggre.'JW.fli; W .StKSWV*F92afUK fWf. MW

1A EPA SAMPLEVOLATILE CRGANICS ANALYSIS DATA SHEET

Nam*. vgRSAR INC Contract:V3LK30

"i.£u Cod*: VEPSAR Cat* No. : 117B4 SAS NO. : 4537£_ 3DG No. :

Matrix: < *oil/uat*r) WATER

Samplt wt/vol: 23. 0 <g/fnL> ML

Lcval: (low/mtd) LQM

" Moisture: not d»c. ___

(pack/cap) PACK

CAS NO. COMPOUND

Lab Samp It ID:

Lab Filt ID: YS43Q

Datt Rtctivtd:

Datt Analyztd: Q4/17/99

Dilution Factor: 5- Q

CONCENTRATION UNITS:<ug/L or ug/Kg> UQ/L

74-97-3———————Chloromtthant___________74-93-0—————--3romomtthana___________73-01-4———————Vinyl Chloridt__________75-00-3———————Chlorotthant____________73-09-2———————fUthg Itnt Chloridt ____67-64-1————————Ac*ton*_________________73-13-0———————Carbon Diiulfidt________73-33-4—j——————1, 1-Dichlorotthtnt_______73-33-3———————I/ 1-Dichlorotthant_______340-39-0——————1. 2-Dichloro«thtnt (total)67r-66-3———————Chloro^orm^____________107-06-2—————— 1. 2-D i c h 1 or ott h an t______78-93-3————————2-3 u t anont______________71-35-6———————1. I, 1-Trichlorotthant____36-23-3———————Carbon Tetrachloridt_____108-03-4——————v i n y 1 Ac t ta 11__________73-27-4———•—-——H^nfBadiehloromathana7Q-97-5———————1. 2-Dichloropropane______10061-01-3—————ci*-l. 3» -Oichloroproptnt_79-01-6————•——Trich lorotthtnt__________124-49-1 ——————D ibromochloromtthant _79-00-3———————1. I* 2-Trichlorotthant____71-43-273-23-2loa-10-1——————4-Mtth(jl-2-Ptntanont_591-7S-6———————2-Htxartont___127-19-4——————Tetrachloroathtnt79-34-3———————1* 1, 2' 2-Tttrachlorotthant103-93-3———————Talu»nt103-90- 7——————C hlorobtnz tn t ______100-41-4———————Ethyl btnxtnt100-42-3———————S t y r t n t __„________;1330-20-7—————Total Xylant*1-07-O2-3———————Ac r o 11 i n107-13-1 ———————Ac r y 1 on i tr i 11_______

FORM i VGA

0000. 20. 270. 2

0. 080. 090. 30. 10. 110. 10. i0. 3

4iU2!U3!U2!U2iU

0. 2!UIIUZIUliU2!U2!U1 JU2!U31U

2 !Uo. i:u0. 2!U-O.-l !U0. 1 !U0. i!U0. 2IU0. 2IU7 ;u3 :u

1/87 R»v.

100533

IEVOLATILE ORGANICS ANALYSIS DATA SHEETTENTATIVELY IDENTIFIED COMPOUNDS

SPA SAMPLE NO.

Nam«: VERSAR INC. Contract:VBLK30

¥Cod*: VERSAR Ca«* No.-: 11724 SAS No. : 4937E

Matrix: (1011/uat»r> WATER

Sampl* wt/vol: 25. Q <g/mL) ML

L*v*l: (Iow/m«d) LOW

" floiitur*: not dac. ___

C 3lumn (pack/cap) PACK

SDG No. ;

Lab Sarnpl* ID: VBLK3Q

Lab Filt ID:

Datt R«ctivtd:

Data Analyztd: 04/17/89

Dilution Factor: 5. 0

TIC» found: _Q.CONCENTRATION UNITS:(ug/L or ug/Kg) UQ/L

CAS NUMBER COMPOUND NAMEi

RT ! EST. CONC.ii

ii! 0i


100534\X3$«K v:.-?AV tfJ- ^

zi^ctq. IAVOLATILE ORSANICS ANALYSIS DATA SHEET

.35 Name: VEPSAR INC._____________ Contract: _

ERA SAMPLE

VBLK44

"la-; Coda: VESS^F Ca»* No. : 11724

•Mcrix: (soil/uatar) WATER

5*iTipi» wt/vol: 25. 0 (fl/mL) HL

w«v*l: (lou/.nad) LJW

"i Moisture: not dsc. ___

: i "Lijron: •: pac */c ap i

SA3 NO'. : 4537E 3DG No. : SAL a?

Lab Sampl* ID: VSLK44

Lab Fil» ID: V3444

Data R*c*iv»d: _______

Datt Analyzed; 04/13/39

Dilution Factor: 5 0____

CA5 NO. COMPOUNDCONCENTRATION UNITS:(ug/L or ug/Kg> UQ/L

74-37-2——-•—————Ch loronuthan*________74-33-?——-———-Bromoffi*than*_________73-01-4————————Vinyl Ch I or Ida__________73-00-3—— ————Chloro*than«___________73-09-2————————M«thy lana Chlorida_______6 7-64-1———————Acatona________________73-13-0————————Carbon Oi«ul?id«________73-33-4———————1, l-Dichloro«th»n«______73-33-3———————1, I-Dichloro«than»______340-39-0———————i, 2-Dichloro«th«n» (total)67-66-3——-——•——Ch lorof orm.^___________107-06-2——————1* 2-Dich lorotthan*______78-93-3—-———•——2-5utanona __________71-53-6————————I/ It l-Trichloro«than«____36-22-3———————Carbon T*trachlorids_____103-03-4———————Vinyl Ac«t*t«____________75-27-4—-——•——granted ich laromathane_____73-37-5———————it, 2-Dichloropropan*_____10061-01-5—————•: is-1. 3* -Oichloroprop«n«_79-01-c———————Trich lor oath an*_________124-43-1———————Di&rorTiochlorom«thane_____79-OO-3———————1. 1, 2-Trichloro«than«____71-43-2———————S«nrt n*________________73-23-2———————:3romo-?orm______________103-10-1 ——————4-ri 11 h y l-2-P»n tanon e_____591 -73-6—————-2-H» x anona127-13-4——————T*trachlorotth«n*_______79-34-3————————1- l, 2- 2-T»trachloro«than*_103-BS-3———————To 1 u » nt ___________t OS-90- 7-——————C hlarobanza n *__________100-41-4——————Ethyl ban i ana____________100-42-3———————Sty ran*_________________1330-SO-7—————Total Xyl*n*»___________107-02-3———————Acrol *in_______________107-13-1——————Acrylonitril*__________

FORM I VGA

0. 03 !U0. 091 U0. 3!U0. 1 i U0. 1IU

0.0.0.0.0.0.O.0.0.0.0.0.20.0.-0,0.0.0.0.73

1 iU

2!UliU2iU11U

2!Uli U2!U3!U!U

I :u2!U

l :ui :u2iU2iU:u;u

1/37 R*v.

100542B ^ ff 'A

IEVOLATILE ORGANIC'S ANALYSIS DATA SHEET

TENTATIVELY IDENTIFIED COMPOUNDS

EPA SAMPLE NO.

VSLK44.ab Natna: VERSAR INC.. Contract:

"usb Coda: VEPSAR Cas« Mo. : 11724

rstrix: (soil/uat*r) WATSR

Sampla wt/vol. 25. 0 Cg/mL) ML

Lsvftl: (lou/mad) LOW

'I Moistur*: not dac. _^^

r:lymn (pack/cap> PACK

(Tiber TIC»

5AS No. : 4537E 5DQ No. : EALo9

Lab Samp It :D: • VBLK44

Lab Fill ID: YS444

Datt R«c»ivad: ______

Datt Analyztd: Q4/13/89

Dilution Pactor: 3. 0____

CONCENTRATION UNITS:(ug/J- or ug/Kg) UQ/L

CAS NUMSER COMPOUND NAME<•: RT11

t

: EST. CONC.11

0

FORM I VOA-TIC 1/87 R«v.

100543

•jnf'.fjtlx t WJ g*S ^

VQLftTIL£ OftGflNICS ANALYSIS DATA SHEET

Lab Names _ _ Vwrsar __ .„„.„___

'^b Cod»i.V«r«ar __ Ca*» No. a

Matrix i (moil/water) WATER

Sample wt/voli 85 _<g/»l)ML

Level* (low/med) LOW

X «oi»turei not dec.

Columns (pack/cap) _PACK

Contract i I

SA9 No. i4«7E SDO No. i

Lab Sample IDi _

Lab File IDi __

Date Received i

CAS NO. COMPOUNDCONCENTRATION UNITSi<ug/L or ug/Kfl>_UO/L.

Date Analyzedi __

Dilution Factort /

74-87-3 —————74-83-9 —————75-01-4 —————75-00-3 —————

67-64-1 —————

75-35-4 —————75-34-3 —————

67-66-3 —————107-06-8 ————78-93-3 —————

108-05-4 ————75-B7-4 —————

10061-01-5 ——79-01-6 —————

71-43-8 —————10061-02-6 ——75-35-3 —————

591-78-6 ————137-18-4 ————

108-88-3 ————108-90-7 ————100-41-4 ————100-43-5 ————1330-30-7 ————

"-•'107- 13-1

—— Ch 1 or oneth ane—— Br omometh ane——/Vinyl Chloride— - Ch 1 oroeth ane „..«,—— Methylene Chloride__ __——Acetone _ „___._... _—— Carbon Dimulfide __—— I, l~Dichloroethene_-— 1, 1-Dichloroethane—— 1, a -Dichl oroeth en* (total) _— — Ch 1 or o form—— 1,2 -Dichl oroeth ane- —— a-Butanone_________- — 1, 1, l-Trichloroethane_ __ .__-—Carbon Tetrachloride——Vinyl Acetate__ __ _ ____

—— 1,2-Dichloropropane—— ci»-l, 3-Dichloropropene—— Tr i ch loroethene___^—— D i bronoch 1 oroaethane—— 1, 1,2-Trichloroethane—— Ben z ene__ _ .__„___„___„_,, __—— tran»-l. 3-Dichloropropene___— — — Br ono f or»

n i^eviiyx— c "en i*anone—-.g^Mex anone— -Tetrachloroethene™" " "" """""— -1, 1, 2, a-Tetrachloroethane___——Toluene—— Chlorobenzene—— Ethyl benzene____ „_____..._ .— — Styrene —_«_«.„„—— Xylene (total) _____________ Acrolein ____ __ ___________

Acrylonitrile „„.._ ____ . _

0.380.210.860.190.832.0O0.23o.oa0.090.850.10.121.381.950.110.350.190.140.170.120.060.07O.O3O.O8o.oa0.080.461.750.070.050.180.130.880.26.58a. 86

IUIUIUIUIUIU -IUIUIUIUIU

IUIU1IUIUIUIUIUIUIUIUIUIUIUIUIU1IUIUIUIUIUIUIU J

100021

IEVOLATILE GRGANICS ANALYSIS DATA SHEET


ERA SAMPLE

EAL69ab Name: VERSAR INC. Contract:

L_=C Code: VEF-SAR Case No. :- 11724 SAS No. : 4537E SDG No. : EAL&9

li-rrix:. (soil.- 'water) UIATER

fc.Tip le ut/vol 25. 0 (g/mL) Ml^

.*vel: ' ( lou/med > LOW

not dec. ___

Lab Sample ID: 69823A

Lab File ID: Y53B9

1 : i L ran '.pack/cap) PACK

.Trier TIC* -Pound: 0

Date Received: Q4/O6/89

Datt Analyzed: Q4/15/S9

Dilution Factor: 5. Q___

CONCENTRATION UNITS:(ug/L or ug/Kg) UO/L

t 1I 1

C*S NUMBER J COMPOUND NAME ! RT

f i

EST. CONC. Q

FORM I VOA-TIC 1/87 Rev.

100022

VOLATILE ORGfiNICS ANALYSIS DATA SHEET

Lab Namvs V»rmar

No. s

tlatrixi <*oil/wat»r>UATER

Sampl* wt/voli 35 _<B/»1>HL

<low/m»d> LOW

Contracti

SAS No.i SDO No. s

X Moi»tur»8 not d»c.

Columni (pack/cap) _PACK

Lab Sa»pl* IDi

Lab Fil» IDi

Dat» R»c»iv»di

Dat« Analyzed i _

Dilution Faetori _ /

CAS NO. COMPOUNDCONCENTRATION UNITSi<ug/L or ug/Kg>_UO/L__

a-Chloro»thyl-vinyl-»th»r___•Chl or omwthan*.......,.,.., ___.....____•Bromomvth *"•___.._____„«.._•Vinyl Chlorid«_.__________

74-87-3------74-83-9------75-01-4------75-00-3------75-09-3------67-64-1————————Acvton*__________________75-15-0———————Carbon Di«ulfid»________;_75-35-4————————l,l-Dichloro«th»n*________75-34-3———————l,l-Dichloro«than«._______540-59-0——————l,a-»ichloro»th»n« (total)_67—66—3———————Cn loro T oriii^ ——>a- —p—,———„»»«,..,.__.107-06-3——————l,2-Diohloro»th*n«78-93-3-———— •—2-Butanon»___—___«__^_____._71-35-6———————l,l,l-TrichloTO»than»_____56-33-5———————Carbon T»traehlorid»______108-05-4———————V i ny 1 Ac»t* t»_____________75-27-4——————- BronodichloroM«th*n«._._....78-87-5—-————-lf 2-Dichloroprop*n».___._„__10061-01-3—————ci»-lf3-Dichloroprep»n»____

124-48-1—————Dibromochloro»»than»___.____79-OO-5————————1, l,3-Trichloro»than»______71-43-3———————B*nz»n»_______....________10061-03-6—————tran*-1.3-Dichloroprop«n»__73-35-3——•——-—Bro»ofonn-.____.-..-._____.^____108-10-1——————4-(1»thyl-a-P»ntanon«______591-78-6:—————a-H»xanon»-.-._-(—.__„_......137-18-4——————T»trachloro«th»n«_________79-34-5———————1,1,3, 3-T«tr«ch loro*than»__108-86-3——™—-Tolu»n«____—--B__—».————..._108-9O-7————•——Chlorobwniwn*.......__.„«__1OO-41 -4———————Eth y 1 b»nz »n»_M___________100-43-5———————Styr»n»____....... _________1330-30-7———————Xyl»n« (total)_____________JQT_^.Qi«S_______Aerol»in___________:_____• 107- 13- I Acry 1 on itfi !•_,,.,,.__.„,______ |

0.30.380.310.260.190.232.0O0.230.08J.6Z18.4O. I

381311351914

0.170.120.060.070.030.080.0808483607,05,13,13,33o.a6.52a. 66

0.0.0.0.0.0,0.0,

IUIUIUIUIUIUIUIUIUIIIUIXIUIUIUIUIUIUIUIUIUIUIUIUIUIUIUIUIUIUIUIUIUIUIUlU

100033

VOLATILE ORGANICS ANALYSES DATA SHEETTENTATIVELY IDENTIFIED COMPOUNDS

tfc Nam«; VERSAR INC

.tr C o d s : VE?5AR Case No. : 11724

' i t r ix ; <*oil/u*t»r) UIATER

limpl* uit/vol. 25. 0 <g/fflL)

• f -vt 1: f lou/ffltd ) LOW

. "1ci«tu^*: not d*c . ^^^,

ilumTi ' . p a c k / c a p ) PACK

:;-,-,£• «T TICi found: • 0

. EPA SAMPLE NO.

EDG22Contract:

SAS No. : 4537E SDC No. : EAL69

Lab Sampit ID: A9942

Lab Fil» ID: YS4Q3

Datt Rtc»iv«d: 04/QA/99

Datt Analgitd; O4/1&/B9

Dilution Factor. 5. Q____

CONCENTRATION UNITS:(ug/L or ug/Kg) UQ/L

*Ai NUMBERt>

COMPOUND NAME 1ii

• ii >RT 1 EST. CONC. ! Q

i j


100034

1AVC-ATILE ORGANICS ANALYSIS DATA SHEET

EPA SAMPLE K

Name: VSSAR INC.

C o tf f :

Contract:EDG33

Case f'Jc. : 11724

•if '• soil/water > WATER

lie wt/vol: 55. 0 fg/fnL) EJL

•el 'low/med) LOW1 J: i s t u r 5: net d 9 C. ___

•jr r, i pack /cap i

SAS No. : 4537E SDG No. : E.AL&9

Lab Sample ID: 69§ 4

Lab File ID: YS412

Date Received: 04/06/89


Dilution Factor: 5. O___

GAS NC. COMPOUNDCONCENTRATION UNITS:<ug/L or ug/Kg) UG/L

'74-57-3———————-Chloromethan* ________

75-01 —1———————V i T, y ; C h 1 or i d e__________•75-00-3———————Ch loroethane^ ________75-0^-2———————Methy lene Chloride__.____•i"-6*-;———•————Acetone ________75-15-0--—————Carbon Ditulrtde________^75-35—3————•———l, i-Dichloro»thene_______75-35-3 ————— -——-1; i-Pi eh lor o> than*343-99-0——————t, 2-Dichioro»thene (total),67-4b-3————————Chloroform^______^____

75-93-3———————2-Butanone_____________71-55-6———————1. 1, 1-Trichloroethane____36-23-f———••———Car-bon Tetrachloride_____10S-05-A——————Vinyl Acetate__________75-27-4———————73-S7-5————————1, I10061-01-5—————ci*-l> 3.-Dichloropropene.79-oi-s———————Trichloroethtne_______124-43-:——————Ditromochloromethane___79-00-5————————i —,, .— a—————-.»—7S--Z5-Z———————3remo^orm_

592-75-0——————2-Haxanont_____________127-33-4——————T*trachloro»thtne_______79-34-5———————i, !, 2» 2-Tetrachloroethane.102-82-3———————Tolu»ne _________1 OS-90-"7——————Ch lor often ztna__________100-41-A———•"——Etnu l benrene _____„_100-42-5———————Sturana : ___________1330-2C-7—————Total Xyltnt*__________

107-13-:——————Aery lonitrile__________

FORM I VOA

0. 4!U0. 2!U6 !0. 2!U0. 2!U2 !U0. 2 1 U

0. 08 IU6 :0. 3!U0. 1 !Uo. iiu1 !U

10 :o. i :uO. 3!U0. 2!Uo. i :u0. 2!U0. 4{o. 2;u0. 2!U2 :0. 2!U0. 3!U2 ;u2 :0. 2!U0. 3! '0. l :u2 :0. 2!U2 ;7 :u3 :u

1/S7 Rev.

100043

IEVOLATILE ORSAIMICS ANALYSIS DATA SHEETTENTATIVELY IDENTIFIED COMPOUNDS

ab Name: VEPSAR INC.

.*b Code: VESSAR Case No. : 11724

•»trix: <*oil/wat»r> UJATER

:*r,?lt wt/'vol: 25. 0 <g/mL>

.f»*1. (1 cut/mid) LOW

*1ci*ture: not dec. ___

: Iw-mn i pack /cap) PACK

i-.Ttb»r TIC* found: __C;

EPA SAMPLE NO.

EDG35Contract

SAS No. : 4537E SDQ No. : EAL69

Lab Sample ID: 69924

Lab File ID: Y5412

Date Rtctivtd: Q4/Q&/99

Datt Analyitd: Q4/1&/S9



1

CAS NUMBER i; ;

COMPOUND NAME ! RT 1 EST. CONC. Q

FORM I VOA-TIC 1/87 Rtv.

100043

.2qC2( 1AVOLATILE ORSANICS ANALYSIS DATA SHEET

ERA SAMPLE

= & Name: VER5AR INC._____________

_ = r Code: VEPSAff Case No. : 11724

Contract:


"itrix: (toil/water) UATER Lab Sample ID: A9S

ri.r.sle wt.'vol: 25, 0 < g / m L > fiL._. Lab File ID: Y54

_f.'*I: (low/med) LOW Date Received: Q4A

i*lciiture: not dec . ___

-\--.-mr.- ; p a c K / c » p ) PACK

r

CAS NO. COMPOUND

Date Analyzed: 04/

Dilution Factor: 5 _i

CONCENTRATION UNITS:Cug/L or ug/Kg) U&/L

74-37-3———————Ch 1 or omethane__________74-33-°——?—————Br omomethane „___75-01-4————-——Vinyl Chloride__________75-00-3———————Chloroethane.____________75-09-2———————Methy lene Chloride_______6 7-64-1 ————————Ace t o ne _____' ____75-15-0———————Carbon Dituifide________75-35-4———————1* l-Dichloroethene______75-35-3—'•—————1. 1-Dichloroethane_______540-5^-0——————1» 2-Dichloroethene (total)67-66-3———————Chloroform.^_________107-06-2——————1. 2-Dichlorotthane_______75-93-3———————2-Butanona_____________.71-55-e————————li l> i-Trichloroethane____56-23-?———————Carb on Tttrach 1 or ide_____1 OB-OS,-4————"——Viny 1 Acetate ________75-27-4———————Sromodich lor omethane_____7S-87-5———————1; 2-0ichloropropane______1C061-01-5—————cis-1' 3» -Dichloropropene^79-01-6————————Trich loroethene_________124-43-1————•—Dibromochloromethane__^^_79-00-5———————1« 1» 2-Trichloroethane____71-43-2—-———"-"Ban a ana ____75-25-2———————Bromoform______________; 03-10-1 ———•——4-Me t h y 1 -2-P en ta'none_____591-7S-6-——————2-He * anont______________127-1S-4——————Tetrach loroethene_______79-34-5————————1* li 2' 2-Tetrachloroethane_10S-S3-3—-——•—Toluene ________103-90-7——————Chlorobenztnt_________iOO-^ 1-4———•——Eth y 1 b en zene ________100-42-5——————Styrene________________1330-20-7—————Total Xylines_______'...107-02-8———————Aero 1 e in_______________107-13-1——————Acrylonitrile___________

2iU3!U2.'U2IU:u

o.o.0.0.0.20. 2!U

0. 08 iU0. 09 !U0. 7!0. 1!U0. 1!U

IU10.0.0.0.0.0.0.0.o.0.0.0.20.0,0.o.0,0,0.73

1IU

2!Ul i U2!U1!U2!U2!UliU2!U3!U!UU-UUu!U

2iU2iUIU:u

FORM i VOA 1/S7 Rev.

100081

IEVOLATILE ORGANICS ANALYSIS DATA SHEET


tb Nam«: VER5AR INC.

.*:• Cotfe: VERSAR Gas* No. : 11724

:*tTix: (*oil/w»t*r) WATER

riT.pl* Ut/VOl 2S. 0 (fl/fflL)

.*-•* 1: (low/med ) LOW

. *1ciitur»: not dec. ___

; umn (. pack/cap > PACK

..->•«'• TICs found' 0

EPA SAMPLE NO.

EDG52Contract

SAS No. : 4B37E SDO No. : EAL69

Lab Sample ID: 69B28

Lab Filt ID: V54O7

Dat* R*c*iv*d: Q4/O6/99

Dat* Analgztd: Q4/1&/B9

Dilution Factor: 5. Q____


145 NUMBER COMPOUND' NAME RT EST. CONC. Q

rFORM I VOA-TIC 1/S7 R»v.

100082

a 1AVOLATILE ORGANICS ANALYSIS DATA SHEET

EPA SAMPLE

.52 Name: VERSAR INC. Contract:

Cede- VEHSAR Case No. : 11724

ix: i soii/watsr ) WATER

SAS NO. : 4537E SDC No. : EAL69

Lab Sample ID: 6*8:

wt/vo (g/mLJ £& _

^r vf 1 ( loui'mtd > LOW

"Is i sture: net dec.

(pack/cap) PACK

CAS NO. COMPOUND

Lab File ID: Y54(

Date Received: 04/<

Date Analyied: 04/:

Dilution Factor:

CONCENTRATION UNITS:<ug/L or ug/Kg) UQ/L

74-37-3———————CM or omt thane__________74-83-9———————Eromomethane________75-01-4———————Vinyl Chloridt__________75-00-3—•—————Ch loroethane _____^««_75-Q9--————————Methy lene Chloride__i7-S4-1 —•—•——•—Ac etcne ___________75-15-0————————Carbon Di«ul*ide______'75-35-4———————1, l-Dichlorotthene_______75-35-3———————1, 1-Dichlorotthane______540-5^-0———————1. 2-Dichloroethene (total)67-66-3————————Chloroform_____________107-06-2:——————1* 2-Dichlorotthane______7S-93-3————————2-Butanone^____________71-55-6————————1. 1. 1-Trichloroethane____56-23*-;———————Carbon ' Tetrachlor ide_____105-C5—-——————Vinyl Acetate__________75-27-4————•—— Sramodich lor ome thane_____7E-S7-5———————1. 2-Dichloropropant_____1C061-01-S—————c i»-l i 3^-Dichloroprop•"«__79-0l-o———————Trich loroethene_________i24-4£-i——————Di bromochl or Odie thane_____77-00-5————————1* l> 2-Trichloroeth«ne____71-43-1—————————Banz»ne _______^__«_75-25-1————————Bromof orm ___________103-10-1———————4-Methyl-2-Pentanone_____591-7E-6——————2-Hexanone_____________127-13-4——————Tetrachlorotthene______7^-34-5———————1. 1. 2- 2-Tetrachloroethane_1C8-8S-3*——————To I uene._______________103-90-7——————Chlorobenztnt_________: 00-41-4——————Ethyl benzene_______ _100-42-5——————Styrene_______________„1320-20-7—————Total Xylene*_______^__107-02-S———————Acrol tin ________107-12-:——————Aery i onitrile_________

FORM I VOA

4iU2!U3!U2iU2IU!U

2!U0. 08 !U0. 09iU0. 7!o. i:u0. 1!Uiooo0000000002o. i :u0. 2!U0. 1!Uo. i:uo. i:uo. 2:u0. 2!U7 !U3 :u

U

3!U2iUi:u2iU1!U2iU2!U1!U2!U3!U:u

1/87 Rev.

100090

IEVOLATILE QRGANICS ANALYSIS DATA SHEETTENTATIVELY IDENTIFIED COMPOUNDS

ERA SAMPLE NO.

EDG53.as N«mt: VERSAR INC.

.-33 Coie. VERSAR Case No. : 1J724

'iSri*: (soii/uatar) WATER

Contract:

SAS No. : 4537E SDO No. : EAL69

Lab Sample ID: A9829

TipIe ut/vol: - 25. '

el: Uow/m*d) LOW

!£ isture: not doc. •

lu«»r < pack/cap)' PACK

(g/fflL) Qk_ Lab File ID:

Datt Rtctivtd

Datt Analyzed

04/06/89

04/1A/B9


r TICs found: _0_CONCENTRATION UNITS:<ug/L or ufl/Kg) UQ/L

C,AS NUMBER COMPOUND NAME RT EST. CONC.

FORM 1 VOA-TIC 1/37 R*v.

100091

:is:eo 1AVOLATILE QPOANICS ANALYSIS DATA SHEET

EPA SAMPLE P

EDC34Name: VERSAR INC. Contract:

Coda: V£P5AP Case No. : 11724 SAS No.: 4S37E SDQ No. : EAL69

trix: (toil/water) WATER

• T.gle ut-'voi 23. 0 (g/mL> £!_,__

'.si: (law/mad) LQU

":c: s tur*- not dac. ___

mn < pack/cao > PACK

CAS N COdPOUND

Lab Sample ID:

Lab File ID:

Date Received:

Date Analyzed:

Dilution Factor: 5.

CONCENTRATION UNITS:(ug/L or ug/Kg> US/L

: 7«-S7-3——————Ch loromethan*.,___________

1 75-01 -4————————Vinyl Chloridt__________; 75-00-3———•—-—Ch l a r o e t h a n e . _ _ _ _ _ _; 75-09-2————————Metfty lent Chloride_______! 67-6^-1————————Acetone ____________: 73-15-0———————Carbon Ditulfide________: 75-35-4———————i, l-Dichloro«thene______! 75-35-3—•—————1, i-Dichlofo»thane______': 540-59-0——————1* 2-Dichloro«thene (total)' 67-4i6-2———————Ch lor of orm__,_______________: iO~-Or-2——————1> 2-Dich loro»thane________: 75-93-2————————2-Butanona ________; 71-55-c———————1- I, 1-Trichloroethane____: t=-22-5———————Carbon Tttrach lor ids_____; 1C3-CS-4——————vinyl Acetate "___! 73-27---———"-——"Bramodichloromethane; 7g-a7-;—— -——T—i, E-Dichloropropan*^____; :0061-C:-5—————ci *-l» 3.-Dichloropropene_

; ; £'.2-45-1———————Dibromochlarome thane____„: 79-00-3———————1- 1. 2-Trichloroethane"____

•r- _42--——————•? t—5««,—.—~ —----- __..-.

' :CE-lv-i——————4-netfty 1-2-Pentanone^___

: 127-13-^——————Tetrachlorotthene________; 75-3^-5———————l- i, 2» S-T«tr«chloroethane,; .05-82-3'———————Toluane __________! 1 OS-90-"——————Chiorobtnitnt__________: iQ:'-4;-4——————Et.hylbtnzant^_________; 10 0-42-3———————S t y re ne ____________; ;3iC— 1--T—————Total Xyltn«s__________I 1 CT-C2-S—;——————Acrol ^in ____,^,_,: 1C-7-I3-; ——————Ac?-u i onitrile__________

FORM i

0. 4!U0. 2'!U0. 3!U0. 2!U0. 2!U2 1U0. 2!U

0. 08 !Uo. 09 :u0. 3!U0.0.10.0.0.00.0.20.00-0.o.2100.0.0.o.0.0.73

7!i:u;u

6!

2!U

2IU2!Ui :u2IU3:u:ui '"'

2IU6!i :u2!U2!U!U:u

1/37 Rev.

100099

IEVOLATILE ORGANIC3 ANALYSIS DATA SHEET


Contract

EPA SAMPLE NO.

EDC54Name; VERSAR INC,______________

Code: VER5AR Case No. : 11724 SAS No. : 4B37E SDG No. : EAL69

UATER

<fl/mL> QL, __

Lab Sampl* ID: 6983SD

Lab Fil» ID: Y5396

Dats R«ctiv*d

Data Analgztd

»pack/C)iD) PACK

04/06/89

04/15/89


;: *r TIC*CONCENTRATION UNITS:(ug/L or ug/Kg) UQ/L

'5-43-4

! COMPOUND NAME

! UNKNOWNi METHANE, DICHLORQFLUORO-lUNK ETHYLMETHYL BENZENEi

RT

7..I76. 12

Tl. 6Z

<<EST. CONC. I Q

0. 3!J0. 6iJ0. 3!J

ri

FORM I VOA-TIC 1/B7 Rtv.

100100

1AVOLATILE ORGANICS ANALYSIS DATA SHEET

EPA SAMPLE N

EDG5552 Name: VgSSAR INC. Contract:

V.. Case No. • 11724 SAS No. : 4537E SDG No. :-EAL&9

:ri * • ( soil/ water) WATER

:p le wt/vol:. 25 0 (Q/mD QL. __

*1: (lou/mtd) LOW

ture cT dec.

.?.(.' 'Tin (pa;!.- 'cap ) PACK

CAS NO COMPOUND

Lab Sample ID: 698:

Lab File ID: Y54-

Date Received: Q4/>

Date Analyzed: 04/

Dilution Factor: 13'

CONCENTRATION UNITS:(ug/L or ug/Kg> UQ/L

74-37-3————•——Chior ometlrane^______^__T--33-5———.———gr amofnethanei_75-01—t———————Vinyl Chloride__________T5-00-2-———————Ch 1 or oethane____________TJ-09-E———————Methy lene Chloride_______o~-64-l————————Acetone _______^—•75-15-0————————Carbon Di*ul*ide_________^5-35-4———————1, i-Dichlorotthene_______^5-35-3———————1. l-DichloTO»thane_______540-9^-0——————1, 2-Cichloroethene (total)s7-6fe-5————————Chloroform ___________:07-o=-2——————1- 2-Dichloroethane______73-93-5—'—————-S-Butanone _____.____"'l-SS-e———————i. :. l-Trichloroethane____56-23-5———————Carbon Tetrachloride_____103-05-4———————Vinyl Acetate ________T5-27-4———————3romodichloromethane_____.73-S7-5———————1. 2-Dichloropropan*______10061-01-5—————ci*-l> 3*-Dichloropropene_79-0:-t———————Trich loroethene_________124-45-1——————Dibromochloromethane_____79-00-5————————1. 1. 2-Trich 1 oroethane____71-43-5————- ~-- E it n T » n e ________,75-25-i———————Bromof orm______________; 03-10-1——————4-Meth«lv-2-Pentanonc_____591-73-a———————2-Hexanon»______________127-13-4——————Tetrachlorotthene_______79-34-5—— ————— 1, 1, 2* 2-Tetr*chloroethane_IOS-S3-3—————-Toluene________________1 OS-90-7——————Chlcrobenitnt__________100-41-4——————Ethyl benzene____________100-42-5——-——atii-rane ___________1330-20-7——————Total Xylene*___________107-OS-S———————Ac rol* in ___________107-13-1——•————Acryl onitrile__________

FORM I VOA

1056527506

1003503510039544

31046357573106

150335

6416072

UUUU

UUUU

U

U

UUUUU

.UUUU!U!Ut\!UiI

!U:u!Uii

!U!U

1/S7 Rev.

100127

IEVOLATILE ORSANICS ANALYSIS DATA SHEETTENTATIVELY IDENTIFIED COMPOUNDS

EPA SAMPLE NO.

.30 Name: VERSAR INC. Contract:ED355

. = = Code: VgRSAR Case No. : 11724

••str ix : (toil/Ufa t«r) UJATEff

:sr.rle wt/vol 25. 0 ig/mL) ML

.*vel: (law/mad) LOW

, >lcistur«: not dtc. __.

•: lumn < pack /cap ) PACK

;_'.T>*r TICs found: _Q,


Lab Sample ID: A9931A

Lab Fil» ID: V5449 .

Date Rectivtd: Q4/Q6/89

Datt Analyzed: 04/18/99

Dilution Factor: 13Q____

CONCENTRATION UNITS:(ug/L or ug/Kg> UG/L

•:A3 NUMBER COMPOUND NAMEii! RT

i '

EST. CONC. Qmmmam

f


100123

VOLATILE ORGANICS ANALYSIS DATA SHEET

Lab Nam»i___V»rsar.

Xab Cod»i_V»r*ar __ Ca»» No. i

Matiriai <»oil/wat»r)WATER

Sampl* wt/voli ^5

<low/m»d> LOW

Contracti

SAS No.i4.3 E SDG No. i

% Moi»tur»i not d»c.

Column i (pack/cap) .PACK

Lab Sampl* IDi

Lab Fil» IDi

Dat* R»c»iv«dt

Dat* Analyzed i _

Dilution Factor i

CAS NO. COMPOUNDCONCENTRATION UNITSs<ui/L or UQ/KB)_UO/L.

74-87-3 —— •74-63-9 —— •75-01-4 —— -75-00-3 —— -

67-64-1 —— -75-15-0 —— -75-35-4 —— •75-34-3 —— •

67-66-3 —— •

78-93-3 —— •

56-23-5 —— •106-O5-4 — •75-27-4 —— -78-87-5 —— •10061-01-5-79-01-6 —— -124-48-1 — -79-00-5 —— -71-43-2 —— -10061-02-6-75-25-2 —— •108-10-1 — -591-78-6 — •127-18-4 — •79-34-5 —— -108-66-3 — •108-9O-7 — •100-41-4 — -100-42-5 — •1330-20-7 — -

r • IO7- 13- 1

———— Uinyl Chlorid*

———— ri»thyl«n» Chlorid* _ _ .-——— -Ac-ton»___ ______———— Carbon Disulfid* __ _ ___ |——— — lt l-Dichloro»th«n» _,.——— — 1, l-Dichloro«than«—— —— i,2-Dichloro*th«n» (total) _

- ———— l,2-Dichloro»th*n*

—— —— 1, 1, l-Trichloro»th*n» _— ——Carbon T»trachlorid«————-Vinyl Acwtat •_______ _ .......

——— -~ 1, 2-Dichloroprop*n«

—— — Trichloro»th«n»___ _ __ .___. — . —— DibronochlorcMM»tha,n»____ _ _

— ——— B»nx»n»_.___-___.- ___ __ „———— trans-l.S-Dichloropropwn-,. .

• ———— 4-M«thyl-S— P»ntanon»——— """a~H«s<*non»____--._-___ ___ B--.

-- ——— 14 l,S,2-T«trachloro»th*n» __

——— -Ethylb»nx»n» _— «_.™._—— »———— Styr«n»__ .___..„___«_., ___. ———— Xyl»n» (total) __ ________ _, _ Acrolvin _™_ _ -

Aery 1 on i tr i 1 •_______.. ____

0.36 IU0.21 IU0.26 IU0.19 IU0.23 IU"Z.QO IU0.23 IU0.06 IU0.09 IU0.61 10.8*1 10.12 IU1.36 IUI.O1 10.11 IU0.35 IU0.19 IU0.14 IU0.17 IUZ.lfe 10.06 IU0.07 IU0.03 IU0.06 IU0.06 IU0.06 IU0.48 IU10. a i0.07 IU0.05 IU0.12 IU0.13 IU0.22 IU0.2 IU6.52 1U2.66 ,U

1U0157

IEVOLATILE OROANICS ANALYSIS DATA SHEETTENTATIVELY IDENTIFIED COMPOUNDS

EPA SAMPLE NO.

ED056Nam«: VERSAR INC Contract:

5 Code- VERSAR Cast No. _____

TTix: ( so'il/water ) WATER

me-i* ut/vol- 25. Q (g/mL> HL

>•«!: (low/med) LOW

^oiiturs: not dec. ____

"i'.mn ( pack /'cap) PACK

'mfrtr TICs found: __1

11724 SAS No. : 4537E SDO No. : EAL69

Lab Samplt ID: 69Q32D

Lab Fil» ID: YS394

Datt Rtceivtd: Q4/O6/89

Data Analyzed: O4/15/99

Dilution Factor: S. Q___


CAS NUMBS?

1 75-43-^

I

! COMPOUND NAME

! METHANE- DICHLOROFLUORO-ii

IRT J

6 12. :i

EST. CONC.

1

11i Q

: ji>

cFORM I VOA-TIC 1/S7 Rtv.

100158


L*b Nam* t V»r*ar Contract i

'-.lib Cod*a_M*r»ar__ Cat* No. i in*** SAS No. »4S37E SDO No. i

Matr ix i <soil/wat*r>UATER Lab Sampl* IDx _69833

Sampl* w-b/voli 35 _<g/ml>J1L Lab Fil* IDi

L*v*la <low/m*d> LOW Dat* R*e*iv*d> __

% Moi*tur*s not d*c. Dat* Analyz*di __OH/I3/S9

Columnt(pack/cap) .PACK Dilution Factori _ '0

CAS NO. COMPOUNDCONCENTRATION UNZTSi<ug/L or UQ/KQ)_UO/L__

f

74-87-3 ——74-43-9 ——73-01-4 ——7S-00-3 ——

67-64-1 ——75-15-0 ——

75-34-3 ——

67-66-3 ——

78-93-3 ——71-55-6 ——

108-05-4 —75-37-4 ——78-67-5 ——10061-01-579-01-6 ——1S4-48-1 —79-OO-5 ——71-43-2 ——10061-02-675-25-S ——108-10-1 —591-78-6 —127-18-4 —

108-88-3 —108-90-7 —100-41-4 —100-42-5 —

1330-2O-7 —-iQ.l-.QZ.i-.

IOT- 13- t

a-rhlfi-^athyl-Miimil-gth*.* __ } ———————— o-a_

————— Vinyl Chlorid*— - —— Ch 1 or o«th an»^-w-_.

—— — -Acvton* __ .... _————— Carbon Di *ul f id»__ ______ \ _————— 1, 1-Dichlorotfthvn*.,, _______—— •- —— 1, l-Dichloro«than» .__. _— • — • — 1, 2-Dichloro«th«n« <total)__-- —— -Ch lorof or»_^__.---—— -— l,2-Dichloro«than»

————— 1, 1, l-Trichloro»than»__- ———— Carbon Tvtraehlorid*— ——— V i ny 1 Acwtatw.. . .... __ ....

— • ——— lf 2-Dichioropropan»__ __ ._——— — ei»-l, 3-Dichloroprop«n»—— .. — Trichlorowthwnw.....^..— ——— DibroKoehloronvthan*.....————— 1,1,2-Trichlorovthan* _____ -_—— —— B»nz»n» .... _————— tran»-1.3-Dich lore pro p»n»___

————— 4-rt»thyl-2-P»ntanon»____ ____—— — -2-H»x «non»_ -— _ _ _ _

——— """ChlorobBTizwnw...... _ ..... ___- ———— Ethyl b»ni«n»_--__-____. _ ....— ._ ... styr»n» _ .___._.__. —————— Xyl»n» <total> _____________ ... .AcrolMin ........... __ ......

Aery 1 oni tr i 1 •_..___ __ ... ___

0.360.210.260.190.235<W0.233.TI0.09157.3.82.11.38

3.<Th0.350.190.140.17

0.060.0729. 1O.O80.08^(,2.0.48

0.07

0.12I9.M0.22

11106.522.86

-U).I UI UI UI UI U ^JK'I U1I U111I UIE1I UI UI UI UI EI UI U1I UI U1I UIEI U1CI UtI U1I U|U

100181

IE EPA SAMPLE NO.v. VOLATILE OR3ANICS ANALYSIS DATA SHEET _

TENTATIVELY IDENTIFIED COMPOUNDS I " |IED857 I

Lab Name i __VERSAR___________ Contract s ________ I ___________._ I

Lab Codei.VERSAR__ Ca»e No. 111784 SAS No. I4537E SDS No. IEAL&9

MatriMs (soil/water>WATER Lab Sample IDi .69833D

Lab File IDi _Y5398i

Date Received! __04/08/89

Date Analyzedi __04/15/89

Dilution Factori _ 10

Sample wt/voli 8.5 _<g/ml)ML

Leveli Uow/med) LOW

% Moimturei not dec. __.__,_

Columns(pack/cap) .PACK

Number TIC» foundi _CONCENTRATION UNITSi<UQ/L or UQ/K8)_US/L

CAS NUMBER

1 . ___8. ___3. _ _ ___4.5. ____6. ______7. ____8. ___9. __10. __1 1 . ______ __18. ___13. _________14. ___15. __16. ______ ___17.18. ___19. _ _80. _________81. ______ ___88. _____83. _____ __84. ___85. ____ __86.

• 87. ___?8..£9.30.

COMPOUND NAME

_, ___ ,„. ^ ____ _ ^ ____ _1

ta

RT

____ _

__________

____ _ ________

________ _-

_____

________ ___

_

__ __

____________ .

EST. CONC.

_______ __

_______ __

_ -

________ _

______ _________

________

__ __ ___

___ _ ____________

_______________________

Q

_

_ _

_

_

FORM I VOA-TIC100182

ra'irT^r3W' BWK?c^


ERA SAMPLE

EDG57DLtb Name: VE5SAR INC. Contract:

V.."i.£3 Code. VEPSA* Case No. : 11724

rstri*: (toil/water) U1ATER

3*-r.pie wt/vol' 25 0 <9/mL) QL.__

_*v*i: (low/med) LOW

\ *si *ture- not dec. ___

(pack/cap) PACK


Lab Samp It ID: 69833C

Lab File ID: Y5447

Data Received: Q4/Q6/89

Data Analyzed: Q4/1B/89

Dilution Factor: 25O____

CAS NO. COMPOUNDCONCENTRATION UNITS:(ug/L or ug/Kg) UQ/L

1 74-S7-3————-——Ch I or omethane: 74-83-9---———-Bramomethane____________.: 75-01-4———————Vinyl Chloride__________; 75-00-3———————Chloroethane.___________I 75-09-2————————Methy lene Chloride.______' 67-64-1 ————————Ac *tone _____________: 75-15-0———————Carbon Di*ulfide________: 75-35-4———————l, 1-Dichlorotthene_______! 75-35-3———————1> 1-Dichlorotthane_______! 540-59-0——————1, 2-Dichloro»thene (total); 67-66-3- ——————Ch 1 or of orm-^________.____„i 1C7-06-2——————1> 2-Dichlorotthane_______

i • 7S-93-3————————g-Sutanona __________: 71-55-=———————\> 1> 1-Trichloroethane____: 56-23-5———————Carbon Tttrachloride_____; i OS-05-4——————Vinyl Acetate___________.75-27-4-——————-Bromodichloromethane^^^__

; 7S-S7-5———————li 2-Dichloropropan*._____.; 10061-01-5————-cii-1'3*-Dichloropropene_: 70-01-^———————Trlchloroethene_________; 124-43-1——————Dibromochl or ome thane_____i 7C-00-5————————1. 1» 2-Trichloroethane____: 71-43-ft——-———— Ba: 75-25-2———————Sromo103-10-1-————— 4-Methyl-2-Pentanone____

; 591-73-6——————2-He xanon«_B: 127-13-4——————Tetrachlorotthtne; 79-34-5———————i, i, a, 2-Tetrachloroethanei 1OS-S3-3———————To 1 u «nai i OS-90-7———---- Ch 1 or ob tn z tne _____! : 00-41 -4——————E t h y 1 b en i tna! 100-42-5———————Styrene___! 1330-20-7—————Total XylentfI I07-02-S———————Acrolein

r" ' I 107-13-1——————Aery lonitrile

FORM I VOA

191113104310012441356694706171079

15003

115

1014

1101600

111900

67

1110

.330140

iU:uiUIUII:u:u;u!U:uIU:u;u;D:u:u:u:utuID:u:u:u!U:u:u:D:uID:u;utututu!U

1/87 Rev.

100220



EPA SAMPLE NO.

I IIEDG57DL I

Lab Nam*»__VERSAR___________ Cont ract s ________ I ____________ I

Lab Cod* i .VERSAR__ Ca»« No, 111784 8AS No.*4537E SDG No.i£AL69

Matrixi <»oil/wat»r>WATER Lab Sampl* IDi .69833C

Lab File ID: _Y5447

Dat* R»c«iv»di __84/06/89

Date Analyzvdi __04/18/89

Dilution Factors _ 50

Sample wt/voli 25.0 _<g/ml)ML

L»v»li (low/m«d) LOW

% Mo i mt ur« s not d*c. ____•

Number TIC» foundiCONCENTRATION UNITSi<US/L or UO/KQ)_UQ/L

CAS NUMBER

1.2.3. _ _ _ _*•5.6.7.8.9.10.11. _12. _13.14.15. _ _16.17. _____ _____18.19. _ _ ___20. _ ___21.22. _ __ __23. ___ _24.25. ___________26. ____________

\~ 27.*8.:9.

1 30.1 _ ______

COMPOUND NAME

UNK TRIMETHYLBENZCNC

..._.. _..._... ._._._._ ,_„„„.„,-,- - ...

_____ _ __ _____

RT

29.2166

___ _

__ __

_____

_______

__ _

_______

_________________ ____

___ .

_________________ _____

EST. CONC.

330_______ .

______ __

__

_ _ _ __ _ _ _

___________

___ _______ _ ___

________ ______ _________ ______

__ _ _

________________

_ _______

Q

J

________

__

__

FORM I VOA-TIC 100221

IS cone SAMPLE tt EDB57DL

PKtt

12345&7891011IS131415167.8192021228384858687888930

RET.TIME

89. 220.000.000.000.000.000.000.000.000.000.000.000.000.000.000.000.000.000.000.000.000.000.000.000.00

" 0.000.000.000.000.00

TIC RIC

56384

IS RICtmwM*mmmmm»

178800

172800

B

50

50

CONC(ug/1) or(ug/Kg)

386.8962

0

c

ISftl13*8IStt3

RETENTIONTIME RIC

85.34 I85.34 I85.34 I

178880 I178800 I178800 I

85.3435. 34

100222


Lab Nam* a _.._V»T-»ar___.—™™_- Contract i I __,

•-*b Cod»»_V«rsar__. Cas* No. t I112H SAS No. »4k 3*E SDO No.

Matrixi (soil/watwr)WATER Lab Sampl* IDi ..

Sampl* wt/voli 25 _(g/»l>HL Lab Fil* XDi

(low/m»d) LOW Dat« R«c»iv*da _.

Date Analyzed* _

Dilution Factori

CONCENTRATION UNITSiCAS NO. COMPOUND <Ufl/L or ug/Ka)HUG/L__

% doi»tuT«8 not dvc.

Columni(pack/cap) _PACK

74-87-3 —————74-63-9 —————75-01-4 —————75-00-3 —————75-09-2 —————67-64-1 —————75-15-0 —————73-33-4 —————73-34-3 —————

107-06-2 ————78-93-3 —————

36-23-5 —————106-05-4 ————75-27-4 —————76-67-3 —————10061-01-5 ——79-01-6 —————124-48-1 ————79-OO-3 —————71-43-2 —————10O61-02-6 ——73-25-2 —————108-10-1 ————391-78-6 ————127-16-4 ————

108-68-3 ————1O6-9O-7 ————100-41-4 ————1OO-42-5 ————1330-20-7 ————

*-.!07- 13- 1

— — — BT ononvth an*—— Vinyl Chlorid* _—— 'Chloro*than«_ _— — m»thyl»n» Cnlorid* _— « Acetone ___ _ _ __—— Carbon Disulfidv— -- 1, l-Dichloro«tha>n« _ __ mtm— -1, l-Dichloro«than* ________—— 1, 2-Dichloro«th*n« (total) _ „— — Chloroform—— 1, a-Dichloro«than»—— '3-Butanon*—— 1, 1, l-Trichloro»than»——Carbon TvtrachloTid*——Vinyl Ac»t*t» _ .

—— 1,2-Dichloro propa «•____„__ _

—— Trichloro»th»n» _ __— — — Di bromochloromvthan*—— 1, l,2-Trichloro«th*n»_-..____

—— tran«-1.3-Dichloroprop»n» __—— BronoforM—— 4-M»thyl-2-P»ntanon» _ ,_»__—— 2-H»xanon»___- „„____ _____——— T**brAehloro*1shMnA

— — Tolu»n«-*•- Ch 1 orob»nz»n* «.«__.._. . __ ,— — Eth y 1 b»n z »n»__w--.___ __ . ___— — — Styr»n»—— Xyl»n» (total) __________ __

Acrolvin „___ „._.___ __ , ___ ,Acrylonitril* «.^^__«__ ___

0.360.210.260.190.232.000.230.08O.foW2.87O.foS0.121.369.1**0.110.350.190.140.17

0.060.070.530.060.060.060.46

0.0751.70.12O.A70.22

6.52I 2.66

IUIUIUIUIU-"IUIUIU111IUIU1IUIUIUIUIU

IUIU1IUIUIUIUItIU1IU

IU1IU|U

100244



EPA SAMPLE NO.

I IIEDG3B II______ _____ILab Name i __VERSAR___.________ Contract s ________ ________

Lab Cod»:_VERSAR__ Ca»« No.si1784 SAS No.I4527E SDG No.*EAL£9

Matrixi <soi1/wat»r>WATER Lab Sampl* IDi _69834D

Sampl* wt/voli 25 _(g/ml)ML

L>v*li Uow/m«d> LOW

% Mo i mt ur« i not d»c. ____.

Columni(pack/cap) _PACK

Lab Fil* IDi _Y5395

Dat» R»c»iv«di __04/96/89

Dat» Analyzed! __04/15/89

Dilution Factori 1

Numb«r TIC« foundi _ 0CONCENTRATION UNITSi<UQ/L or UG/KS)_UQ/L

CAS NUMBER

1.2.3.4.5. _6.7.8. _ ________9.10.11.12.13.14.15.16.17.18.19.20.21.22.S3. _ _ ____24.25.26.-27.>e.9.30.

COMPOUND NAME

__________ _ _ __________ . __ __

_

_ _____ ___ _ ___ ____ _

__________ _ ______ _

______ ____ _____

________________ _______ ___ ____ _ _______

,

RT

______

_

____

_______

_

EST. CONC.

__ __

__ _ _ _

_____ _____ _____

__ ___

___ ______

______________ ___

_________

__ ____

Q

____

___

____

FORM I VOA-TIC 100245

Sq • 1AVOLATILE ORGANICS ANALYSIS DATA SHEET

Narn*: VEP5AR INC,______________

EPA- SAMPLE

EDG60

•-od«; VERSA? Cas* No. : VI724

•rix. (soil/water) WATER

Pie ut/vol: 25 0 (g/mL)

-c-1 <low/mad ) LOW

i•:-1»tur *: not d * c. ___

i. fjsn fpack/cap) PACK

Contract: ____

SAS No.: 4537E SDC No. EAL69

Lab Samp la ID:

Lab Fila ID:

Date Rtctivad:

Data Analyzed:

69S3Q

V5AQ9

O4/O&/99

Q4/1A/89


CA3 NO. COMPOUNDCdNCENTRATION UNITS:< u g / L or ug/Kg) UO/L

-?4 — 37— "* — ~74-83-®™

7«_nr— *—75-09-2 —67-64-1 —7*— 1 5—' — -

340-39-0—67-66-3 —

yc-p-^— 2—

56-23-5 —

73-27-A —— •

— — - — —Ch lor oma than*—————— Br amamtthana _————— Vini^l Chlorida————— Ch 1 or o*thana.r—— —— .-Mtthijltn* Chlorida _—————— Ac*tona IIMI— - —— — Carbon Di«ulfiri* _——— - — 1, l-Dichloroath»n»————— i, i-Dichloroathan» mn __,.,.—— -—— i, 2-Dichloro*th»n* (total > __———— . — Ch lor of orm ._ _—————— l, 2-Dichloro»than*

—————— l, i, i-Tricftloro»than»—————— Car-hon Tatrach 1 or i d*-- — —— v i n y 1 Ac a tat a———— —— 3ramodichlorom*th«n«—— —— «— 1 . r-nich 1 or oOT-ooan*

10061-01-5 ————— c i*-l' 3» -Dichloroprop tnt ____ .70-0 1 -s —— ' ————— Tr ichlorotthtna1 94— AP— •* —

71-43-; —-?«_.?*.— r —1 03-10- 1 -«(^l_7P-B-

—————— nihTomoehlorom«th«n* „—— — — i . i . 2-TriehlOT»o»th«n»—————— B*nz»na ,„„_,_ ,,,„.——————— E-ramof orm_,__ii——————— 4-!*!»thyl-2-Pantanon» ,————— -2-H»i»nont

127-13-4 ——————— T»trachloroathan»79-34-5 —103-33-3-105—90-7-100-41-4-1 GO-42- 9-

107-03-e-107-13-1-

————— 1, i, 2' 2-Tatrachloroathana ___————— Toi "•«*'..„,«————— Ch lorobantana————— Etnylbani*na_—————— Styrsna „.„„....„_—————— Total Xultnt*

—————— Aery 1 oni tr'i 1 •

i0. 4!U0. 2!U0. 3!U0. 2IU0. 2 ! U --2 !U0. 2!U

0. 081Uo. 09 : u0. 3!U0. 1 !Uo. i :ui :u3 :o. i :u0. 3!U0. 21U0. 1IU0. 2!U3 :0. 2!U0. 2!Uo. i:u0. 2!U0. 3!U2 :u17 : -0. 2!U0. 1 !U0. 1!UO. 4!o. 2 : u0. 9!7 !U3 :uii

FORM 1 VQA 1/87 R*v.

100286


EPA SAMPLE NO,

• b Nama: VEPSAR INC Contract:EDG60

3 Code: VE'SAP Case No. : 1J724

t-ix: (soil'uattr) UATER

,Tslt wt/voi. 25. 0 (g/nL> ML

^-c-i: <lou/mtd> LOW

x*cis turft- nor dtc. ____

lumn -^pack/cap) PACK

"•frsr TICs round: __£[_

SAS NO. : 4537E SDG No. : EAL^9

Lab Samplt ID: A983Q

Lab Filt ID: Y54Q9

Datt Rtctivtd: 04/Q6/S9

Data Analyzed: Q4/1A/89



COMPOUND NAME RT EST. CONC.

r

FORM i VOA-TIC 1/S7 R»v.

100287

1AVOLATILE OROANICS ANALYSIS DATA SHEET

EfA SAMPLE

EDG61act Name: VERSAR INC

Code: VERSAR Case No. : 11724

r x » : (soil/water) WATER

Contract:



p_ Cg/niL) HL Lab File ID:

Date Received

Y3437,

O4/O6/99

r

not d*c

pack/cap) PACK

Date Analyzed. Q4/1B/89

Dilution Factor: 10

CA5 NO. COMPOUNDCONCENTRATION UNITS:(ug/L or ug/Kg) UG/L

74-37-3———————Ch 1 oromethane_______74-S3-9———————Erofnomethane_ ________75-01 -4————————V inyl Chlorid e___________75-00-3———————Chloroethane____________73-Oe-2———————Methy lene Chloride_______67-64-1————————Acetone________________73-15-0———————Carbon Di«ulfide________75-35-4———————l, l-Dichloro»thene_______75-35-3———————1. 1-Dich lor Of thane_______540-59-0——————1< 2-Dichlorotthene (total)67-6e-3—— -—————-Chlorof orm __________107-06-2———•———1, 2-Dichlorotthane_______7S-93-3————————2-Sutanone __________71-55-6--—————li 1. 1-Trichlor oethane____56-23-5———————Carbon Tetrachloride_____1 OS-05-4———————Vinyl Acetate___________75-27-4—————»—Bromodichloromethane_____78-87-3———————l, 2-Dichloropropane_I____lOOil-01-3—————cii-1*3/-Dichloropropene_79-C1-6———————Tr ich loroethene_________i 24-43-i———————Dibromochloro(n«thane_^___79-00-5 ——————— 1. 1, 2-Trichloroethane____7:-43-£———————Benzene________________75-2J-2————•——Bromoform _____________l OS-1C— i———————4-Msthyl-2-Pentanone_____S91-73-6——————2-He x nont...___________127-18-4——————Tetrachlororthene_______79-34-5———————1, I. 2. 2-Tetrachloroethane_103-S3-3———————Toluene,________________1 OS-90-7——————Chiorobenient__________100-41-4——————Etftylbenzene^__________100-42-5——————Styrene_______________1320-20-7——————Total Xylentl___________10~-02-e———————Aero le in,_______________1C7-12-:——————Acryionitrile__________

0.0.0.0.0.40.0.0,

340.0.30.0.0.0.0.0.70.o.0,0.0.5

100.0.0.0.0.0.

136

SiU4IU5!U4!Us:u-

1USIU2iU2!U

2!U7!U4!U3!U3!U

4!U2!U2!U3!U4!U4!U

!U;u


100310

IE'VOLATILE ORCANICS ANALYSIS DATA SHEET

TENTATIVELY IDENTIFIED COMPOUNDSERA SAMPLE NO.

EDG613D Namt: VgSSAR INC.

.IS Cod*: VB

Contract:

Case No. : 11724 SAS No. : 4337E SDG No. : EAL69

sr-ix: (soil/water) WATER

.*;?-& le ut/voi. 25. 0 (g/mD.QL_

.«• -'5 I. i lou/mtd ) LOW

9: not d»c. ___

(pack/cap) PACK

_<:-.: er TICt ^

Lab Sample ID:

Lab Flit ID: Y5437

Date FUctivad: 04/06/89

Datt Analyzed: 04/18/69

Dilution Factor: 10

CONCENTRATION UNITS:(ug/L or ug/Kg) UG/L

C«.S NUMBER ! COMPOUND NAME*

RT ! EST. CONC.•: G

FORM I VOA-TIC 1/87 R*v.

100311


EPA SAMPLE

v..b Nama: VER5AR- INC

i r Code; VERSAR

Contract:EDG62

Case No. : 11724 SAS No. : 4337E SDG No. : EAL69

T T - i x : i s o i l /water ) WATER Lab Sample ID:

.r.c le ut/vol 25, <

% *!: (lou/mad ) LQUJ

venture: not dec. '

iuffln: Cpack/cap) PACK

<g/mL>

Date Received: Q4/Q6/89


Dilution Factor: 13Q___

CAS NO. COMPOUNDCONCENTRATION UNITS:<u g / L or ug/Kg> UQ/L

74-37-3———————Ch laromethane7i-32-c————.-———Rrnmnm«than»75-01-4———————Vinyl Chloride__________75-00-2———————Chloroethana.___________73-09-Z————•——Methy lene Chloride__.17-64-1————————Acatane __________75-15-0————————Carbon Di«ul*ide________75-35-4——————1, 1-Dichloroathtne______75-35-3———————1, 1-Dichlorotthane_____540-59-0——————li 2-Dichlorotthene (total),c7-6o-3————————Chloroform..._^___________.:C7-C*-2——————1, 2-Dichlorotthan*______78-93-3———————2-Dutanona_____________71-55-s———————1. 1- 1-Trichloroethane____Sc-23-3———————Carbon Tetrachloride^.____103-05-4——————Viny 1 Acetate__________75-27-4————-——-Br.3<nodichlorom»thane^___7S-S7-5———•——•—1* 2-DichIoropropane_____10061-01-5——-—-cis-1' 3/ -Dichlo.roprop»ne__79-Ol-e————————Tr ich loroethene_________124-43-1——————Dibromochlororaethane^____79-00-1———————!• 1. 2-Trichloroethene____7: -43 -t—————•——B c n i *ne ______«___75-25-2————————Bromoform______________lOS-lC—1————•——4-M*thy 1-2-Ptntanon*^^^__591-73-c———-——2-Hexanone_^______127-13-4———————Tetrachloroathene ____79-34-5———————1, 1, 2- 2-Tatr«chloroethane_103-S3-3——————Toluene____„___________105-90-T——————C h 1 or ob »n x tnt___________100-41-4———————Ethyl ben ten*.___________100-42-5———————Stur«n« ____________1330-20-7—————Total Xylenei__________107-02-6———————Aeralain ____________1C?-12-1———••——Aery lonitriln _________

10563630622

2803333339544504633737120693333

16072

:u!U:u!U!U-:u:uJU!U

!UIU!U!U;u:u:u!Uii!U!UIU:uiU!UI1!Ui --iU!UiUiU!U!U

FORM i VOA 1/87 Rev.

100325

IEVOLATILE ORQANICS ANALYSIS DATA SHEETTENTATIVELY IDENTIFIED COMPOUNDS

EPA SAMPLE NO.

EDC62sb Nam«: VEPSAR INC Contract:

V.- = c Code; VEPSAP Case No. : 11724

'•'•*T"i x : (aoil/uattr ) U1ATER

:s;7!?-l* wt/vol: 25. Q (g/fflL) ML

-sv»l: (low/mtd) LOW

-* *lti*tuTt: not dec. a__m

Itlvmn (pack/c«p> PACK

'-.-•m&er TICs found: __2.

SAS NO. : 4937E SDC No. ; EAL69

Lab Sample ID: A983AA

Lab Fill ID: Y5493

Datt Rtctivtd: Q4/Q6/B9

Data Analyzed: O4/1B/89

Dilution Factor. 13O____

CONCENTRATION UNITS:(ug/L or ug/Kfl? UQ/l,

I1

CAS NUMSER ! COMPOUND NAME

t

RT EST. CONC. Q

FORM I VQA-TIC 1/S7 R«v.

10032C


ERA SAMPLE

EDQ63Na.-ne: VERSAR INC.

- Q i e : VEPSAP Case No. : 11724

,r j x : ( soi 1/uater J UiATER

Contract:


Lab Sample ID: A9B25

• Is ut-'vo <g/mL> QL,_

(law/mad) LOW

fr- not dec. ___

(pack/cap) PACK

COMPOUND

Lab Filt ID:

Date Received

Date Analyzed

Y3410

Q4/Q6/B9

04/16/99

Dilution Factor: 5. O____

GAS N3CONCENTRATION UNITS:(ug/L or ug/Kg) UQ/L

74-37-3-Ti-ST-O-7«-n 1 — 4-75-00-3-75-09-2-67-64-1-75-15-0-

•73-3*—''—540-59—067-66-3-107-06-27S-93-3—

«.-.-c>3-B-1 OS -05- 4

7S-67-3-10061-0179-01-6-1ZS-4S-179-or,-;-•r* _ yt^ _ ™J_/ i— *t J— *75-25-2-i os- 10-13 ? I -73-6127-13-479-34-3-103-83-3I OS-90-?100- 41-4100-42-51333-20-:07-CI-3107-13-1

—————— Chl or ome thane————— —— Eramom* than*——————— Vinql Chloride——————— Chloroethane .——————— Msthylene Chlorid*—————— -Acetone M| , ,—————— "Carbon Dieulfida , , .„..,,.., .——————— 1, l-Dichloroeth»n*—————— 1, 1-Dichloroethane—————— t, 2-Dichloroethene (total )———— - —— Chloroform,.—————— I, 2-D ich lor oe than*- ———— • — 2-5utandna- —————— 1. 1. l-Trichlopo«thane——————— Carbon Tetrachlor ide——————— Vinij 1 Acetate— • —— - —— Bromodichloromethane——————— 1, 2-Dich lorapropane-3 —— • —— cis-1 - 3» -Dichloropropene ____——————— Trich loroathan*———— • — Dibromoch lor oine thane———— - —— 1, i, 2-Trichloro«th*n*——————— g . n T • n • mit >m t 1 1

————— . — 4-«»thu l-2-P»ntanon*

—————— Tstrachloroethan* , „ .,„,——— — —— 1, 1, 2' 2-Tetrachloroethane ___

——— • —— ch lorobenzen*——————— Eihy lb«nzene,,,;——————— Sti/r*na M7 ————— Tctal Xylanei——————— Arr-ol »iniiii— __, (—————— Acrij lonitrile

1

0. 4!U0. 2!U0.3IUO. 2iU0. 2!U-2 !U0. 2!U

0. 08 !U0. 09 !U0. 3!U0. 1 !U0. 1 !Ui :uo. i :u0. 1 J U .0. 3!U0. 2!U0. 1 !U0. 2!Uo. i:u0. 2!U0. 2IU0. 1IU0. 2!U0. 3!U2 !U0. 1!U-0. 2 i U0. 1 i Uo. i :u0. 1 !U0. 2!U0. 2IU7 :u3 IU

1


100343

IE ERA SAMPLE NO.VOLATILE ORQANICS ANALYSIS DATA SHEET _________TENTATIVELY IDENTIFIED COMPOUNDS !

1 EDG63*b Name: VERSAR INC.____________ Contract: _________ !______

.52 Code: VEPSAff ' Case No. : 11724 SAS No. : 4S37E SDG No. : EAL69

strix: (soil/water) WATER ' Lab Sample ID:

;*.T-.ple 'ut/val: 25. Q (g/fflL) QL._ Lab File ID: Y541Q

(low/mad) LOU Date Received: Q4/Q&/99

: not dec. ___ Date Analgred: Q4/1A/S9

umn '.pack/cap) PACK Dilution Factor: 5. Q

CONCENTRATION UNITS:.-.r.ttr TICt found: _0. (uj/L or ug/Kg > UQ/L

•:-*S NUMBER COMPOUND NAME I RT EST. CONC.


100344


ERA SAMPLE

HE Name: V^S^AR IN$

?r Coae: VEPSAR

"•*-.* i » • c soil/water )

~ x ~- : I 9 w t / v o i

_?- ••* I : ( iQw/mt d )

*, '-c : s T or e • not dec.

". : ". .-mr,. \ pac k ''cap )

CA5 NO.

J 74-67-3 —————i 74-S3-9 —————! 75-01-4 —————! 75-OC-3 —————; 7*-rvc— 2—— —— —

1 75-15-0 ——————: r^-^5-4— — «—; T^-'JS— "*——————•. "-rO — r-5?— w— — • ——

; ic~-06-2 ————i 73-<V3-3 ——— - —

! 5a-Z3-3 —————' IOS-C5-4 ————

J TS-.7--*—— «— _

: TC— -•;. i — e— — —— —

1 79-00-5 ——————

EDG64mi, ,., - Contract:

Cas* No. : \\7^( SAB No. : 45 7 , SDG No. : ?AL 9.

WATER Lab Samol* ID: 69826

25 Q (g/mL> E1U __ L*b Fl

[.flW ' Date F

le ID: Y54H ,

eceived: O4/Q&/99

D*t» Analyzed: 04/;6/ ^

PACIl Dilution Factor: J. 0 ,

CONCENTRATION UNITS:COMPOUND (ug/L or ug/Kg) UQ/L Q

—— Chl or ome thane—— Ercmom»thane_—— Vinyl Chloride—— Cn loraethana—— M»thylene Chloride „„ ,,.

—— C*rban Di«ulfid»—— l, l-Dichloroeth»n» , ..—— 1, I-Dichloroethane , „ . , , ,—— 1- 2-Dichloroethene (total) __— — Ch iflpof orm—— i, 2-Dichloroethane , , ,—— 2-Butanone—— 1, 1, 1 -Trichloro*thane—— Carbon Tetrachloride—— vmy 1 Acetate— — Bromod ieh 1 or atnm thane—— l, ?-DichloroDrooane—— r !*-! , 3i -Dichlorooronene— -Tr • ml or oath en*—— rsihromochlQromsthan* , __.„,..,.,„——— 1 , -j . r--Tr ichlflf o»th*ne

• -c_^r._-. ___ _ CT-itno-fcrm

; «?ci -T£--a—— ««.! 117-18-4 ————

.' IC£-8S-Z ————

I lCv-41-4 ————! 1 CO-42- 5 —————

; 1C7-13-1 ————

—— 4-~!«tnul-2— Pentanone—— 3-H«*anane : :—— T«>frrachloroath*n* „„ .—— 1* 1.2- 2-Tetraqhl or oe thane—— To I LIB ne_iH umi -—— Chiorob tnztn*

__ StuT-»ne—— Tc-tiii Xylenet

—— A,-rij lonitrile

10. 4!U0. 2!U0. 3!U0. 2!U0. 2!U-2 !U0. 2iU

0. OSiUo. 09 :u0. 3!U0. 1 !U—o. i:u1 !U0. 1 !U0. liUO. 3JU0. 2!U0. liU0. 2!Uo. i :uo. 2;u0. 2!U0. 1 JU0. 2IUO. 3!U2 :u0. liU--0. 2iU0. I !U-0. liU0. 1 I U0. 2!U0. 2!U7 !U3 !U

ii

FORM I VGA 1/S7 Rev.

100349

IEVOLATILE ,QROANICS ANALYSIS DATA SHEET


-D Name: VERSAR INC.

= Cad*: VERSAR Case No. : 11724

tr ix . (so i l /water ) UJATEP.

mpl« wt/vol: 55. Q < g / m L >

.-*1: <low/mtd) LOW

*lc iitur*: not d*c. ___

(pacti/cap) PACK

TICs *ound' _C:

ERA SAMPLE NO.

ED064Contract:

SAS No. : 4537E SDG No. :

Lab Sample ID:

Lab File ID: Y5411

Date Received: 04/Q6/S9

Date Analyzed: O4/1A/89



COMPOUND NAME RT EST. CONC.

PORM I VOA-TIC 1/37 Rev.

J00350

1AVOLATILE ORGANXCS ANALYSIS DATA SHEET

ERA SAMPLE

EDQ63,\& Name: VEPSAR INC. Contract:

Coie: VE35AP Case No. : 1 1 724 SA5 No. : 4537E SDG No. : EAL69

'.s tr i *: isci1/uat*r) WATER

*r::-it ut'vol- 23. .Q <g/mL)

fv»l. (lou/med) LOW

«ct d&c. ___

jnn pack/cap) PACK

Lab Sample ID: A9S37

Lab File ID: YS4OA

Date Received: 04/Q6/B9

Date Analyzed: O4/1A/B9

Dilution Factor: 5, Q___

GAS NO. COMPOUNDCONCENTRATION UNITS:(og/L or ug/Kg) UQ/L Q

74-S7-3———————Ch iorometh*ne_______74-S2-9—•—————Sromomethane^ _________75-01—3———————Viny 1 Chloride__________75-00-3———————Ch loroethane____________75-09-2———————methyItne Chloride______c7-64-1———————AC e t one _________7?-: 5-0———————Carbon Di«ul*ide________75-35—a———————1- l-Dichloro»thene______75-35-3———————1, l-Dichloro«thane______540-59-0——————i, 2-Dichloroethene (total)67-66-3———————Ch lorof orm ______„__iC7-Oa-2——————i. 2-D ichl or oe thane______7«-?3-3—— ————g-Sutanona _________7i-55-fl————— ——1» 1. l-Trichloroethane_____5a-23-5———————Carbon Tetrach 1 oride_____105-C9-4——————vinyl Acetate^__________75-Z7-^——————— Sromod ich loromethane_____7S-27-5———————i, 2-Dichloropropane_____100ft1-01-5—————cit-I-3.-Dichloropropene_79-0i-r————————Trich loroethene__________1*4-^3-1 ——————Dibromoch loromethar.g_ J n^^7«-00-5 ———————1» I* 2-Trichloroethane____7: --42-2———————Benzene________________75-25-*———————Bramof orm ________.___iCS-10-1——————59 l-7S-ft——————S-He x127-18-4——————Tetrachlorotthene79-34-5———————i. 1, 2. 2-Tetraehloroethane103-8S-3———•———To 1 u«ne _________i 05-90-7——————Chlorobanztnt100-41-4——————Ethyl bentene100-42-5——————Styrene1330-2C—7—————Total XyleneslO^-02-S———————Acfoiein _______I07-i3-l————•—Aery Ion itrile______

FORM 1 VGA

O000020

0. 080. 090. 3001000000O. 10. 20. 20. 10. 202000000073

4!U2!U3!U2!U2!U-JU

2iU!U!U!UJ U -JU:u;u!U

3!U2!U

2iU1 JU2!U

U1 IU2IU3!U;uUUU

i :u2iU2JU!U!U

1/S7 Rev.

100355

IE . EPA SAMPLE NO.VOLATILE ORPANICS ANALYSIS DATA SHEET ______________


«b Namt: VERSAR INC._____________ Contract:EDQ65

_£3 Code: VERSAR Cast No. : 11724 SAS No. : 4537E SDC No. : EAL69

r'itri,. (soii/uatar) MATER Lab S*mpl* ID: 69827

€i.T:pl* ut/vol: _2S 0 Cg/fflL> QL,_ Lab Fil» ID: Y34Q6

-?v«l: (low/mad) LOW ' ' Data R«ctiv»d: Q4/QA/89

". r;ci3tura: not d*c. _^__ Datt Analyzed: Q4/1A/89

.". lurnn •; pack/cap ) PACK Dilution Factor: 5. Q

CONCENTRATION UNITS:.?>b»r TICs found: _£ (ug/L or ug/Kg) UQ/L

. . .

•AS NUriBER : COMPOUND NAME ! RT I EST. CQNC.

FORM I VQA-TIC 1/87 R«v.

10035G


ERA SAMPLE N

EDG74Nam«: VERSAR INC.______

C o d e : VE3SAP Case No

- : x . (so i1 /uatar ) -WATER

Contract:

1 1 724 SAS NO. : 4537E SDG No. : EAL&9

Lab Sampla ID: 69828

. - : I e LJ t.-' v c 1:

- •s i : ( lou»/mf d >

re i»tur*: not (iftc

25. 0 (g/fflU) C3L_

LOW

Y 5 40.5

I : I'.rnn: ' pac k ''cap ) PACK

Lab Filt ID: _______

Dat« Rtc«iv*d: 04/Q6/B9

Data Analyiad: O4/1A/99


CAS NO. COMPOUNDCONCENTRATION UNITS:<ug/L or ug/Kg) UQ/L

74-37-3————————Chloromtthant___________74-22-c———-———Bromoroathana_iM__________75-01-4———————Vi ny 1 Chlorida__________73-00-3————————Ch Ioro«th«na____________75-09-2————f——Mathy lan« Chlorid*_______67-64-1———-————Aotona________75-15-0———————Carbon 0i«ul*ide________75-25-4———————1, l-Dichloro»than«_______75-35-2———————1. l-Dichloro«thana______540-?9-o——————1, 2-Dichloroath»ne (total)67-6o-3———————Ch lorof orm._____________107-06-2——————i- 2-Dichloroathane______75-93-3———————2-3utanona_____________71-55-6———————l- I, 1-Trichloroethane____5c-23-5———————Carbon Tttrachloride_____10S-C3-4———————Viny 1 Acatata___________75-27-4————-——8rcmodichloro(nethan*_____7S-S7-3———————1. 2-Dichloropropane.______i006i-01-5—————c is-1.3*-Dichloroprop«nt_79-0!-s————————Trich loroathtn*_________124-43-1——————Dibromochloromathana.____79-OD-5————————1, 1. 2-Trichlorotthant____7:-4 3-1——-————Benztnt________________75-25-2————————Sromoform ___________iOS-lO-1—»————4-Methgl-2-Pantanont______59: -7S- =———————2-He x anont a__________.^^127-13-4——————T«trachlorotth«n»_______79-34-5————————1, 1, 2. 2-T«trachloro«thana_105-S3-3——————To I ua na______;_________1 OS-90-7——————C h 1 or o b tn z tn«__________100-41-4——————Ethyl b*nitnt.____;_______100-42-5———————Styrgna _____________1330-20-7——————Total Xyl«nt«_______;____107-02-3—•—————Acrol «in ____________107-13-1———————Acr-ylonitrila___________

0.0.0.00.20.0.20.0.0.130.0.0.0.0.0.0.0.0.0.0.2130.0.0.0.0.0.73

3!U2!Ui:u2!U612!U2!U1!U2!U3!U!U

iU:u:u:u:u!U!U!U

FORM I VOA /87 R»v.

100361


3S Name: VERSAR INC.

.« Code : VEP5AP Case No. : 11724

s^Tiy.: Csoi l /uatfD WATER

:a*;le ut/voi: 25. 0 (g/mL)

.?- -e l : ( lou/med) LOW

t tcisture: not dec. ___

ciumn • ; p a c k / c a p ) PACK

-."Tiber TICt ^ound: _0.

EPA SAMPLE NO.

EDG74Contract:

SAS No. : 4S37E SDG No. : EAL69


Lab File ID:

Date Received

Date Analyzed

04/06/89

Q4/16/89

Dilution Factor: 3. Q


CAS NUMBERi i <i i i

COMPOUND NAME ! RT ! EST. CONC. ! G

• i iI r i


loose:


Lab Nam*i__V»r»ar___________ Contracti I ___

ab Cod**_V*r»ar__ Cas* No. i I l"7lM SAS No.34S37E SDO No. i

llatrixi <*oil/wat*r>UATER Lab Sampl* IDi __I

Sampl* wt/vol* 25 _(Q/ml>ML Lab Fil* IDi __V5389

L»v»ls <low/m*d) LOW Dat* R*c*iv*di

I1oi*tur*s not d*c.

Column*(pack/cap) .PACK

Dat* Analyzedi _U

Dilution Factori _

CAS NO. COMPOUNDCONCENTRATION UNITSi<ug/L or ug/Kg)_UO/L.

74-87-3 —————74-S3-9 —————73-01-4 —————75-00-3 —————75-09-2 —————67-64-1 —————75-15-0 —————75-35-4 —————75-34-3 —————

67-66-3 —————107-06-3 ————76-93-3 —————71-55-6 —————56-23-5 —————106-05-4 ————75-27-4 —————78-87-5' —————10061-01-5 ——79-01-6 —————124-48-1 ————79-00-5 —————

— — Ch Xoromtthanv— — — Brononivth an*—— Vinyl Chloirid*...—— Chloro»than»_.___-.-. _ ___ __—— M»thyl»n» Chlorid»__.____ _^_—— Ac*ton» „-.„—__—„„ ———Carbon Disulf id*— -1, l-Dichlorowth n*....... _____—— 1, l-Dichloro«than»—— l,2-Dichloro»th»n» <total) _— — — Ch 1 oro "f orm—— 1, 2-Dich lor o»than»—— 2-Butanon»____________ __..—— 1, 1, l-T-richloro»than» _ B ..__——Carbon Twtrachlorid*—— Vinyl Acwtat*.. ___________—— Br oMod i ch 1 or omvth an*——If 2-Dich loropropan*- — -ci»-l, 3-Dichloroprop»n» ___ „_—— Tr ich 1 oro*th*n»______ _____

71-43-2—- ————— B»nz«n»10061-08-6 ——73-25-2 —————108-10-1 ————391-78-6 ————127-18-4 ————

108-88-3 ————1O8-90-7 ————100-41-4 ————100-42-5 ————1330-20-7 ————-LQl-.Q i ___107- 13-1

—— tran»-l. 3-Dichloreprop*n» __— — — Br OMO form—— 4-M»thyl-2-P»ntanon» _ „__ _ .—— 2-H»x anon*.__________M. _______—— Twtrach loro*th»n*______ ____—— 1, l,2,2-T»trachloro»than» __— -Tolu*n* _______».. _ ._ ____ ,_—— Ch 1 oro b*nz *n*-— Ethyl b*nz»n»________________— -Styr*n* ..____«_., ________—— Xyl*n* (total) ____________

Acrolvin _ ________ ______Acrylonitril*___^__-___ ____

0.360.210.260.190.23z.oo0.230.081.80.250.10.121.383.10.110.350.190.140.170.50.060.070.030.080.080.080.4813.Z0.070.050.120.130.220.26.52

1 2.86

IUIUIUiUIUIUIUIU1IUIU-IUIU1IUIUIUtuIU1(UIUIUIUIUIUIU\'-IUm--IUIUIUIUIU J|U

100382

IEVOLATILE ORQANICS ANALYSIS DATA SHEETTENTATIVELY IDENTIFIED COMPOUNDS

ERA SAMPLE NO.

= 0 Name: VESSAR INC.

'Las Code: VERSAR Case No. : 11724

resrix: (soil/water) WATER

3a.-;Dle ut/vol: 25. 0 < g / m L >

_* vel:. (low/med ) LOW

*. Moisture: not dec. ____

l:Iumn (pack/cap) PACK

r-i^nber TIC» found: _£

Contract:EDC75


Lab Sample ID: A9839A

Y5399

Datt Received: Q4/Q6/89

Date Analyzed: Q4/15/99

Dilution Factor: 5. O


11

:AS NUrtBER :>i

COMPOUND NAME RTii

EST. CONC. ! Q

!

r


300383


1 EDG-7-7Lab Name i __ Ver»ar ___________ Contract i

\b Codes_Ver*ar __ Ca»e No. i I 112*4 SAS No. 1 4537. E SDG No. i

riatrias (t»oil/water>UATER Lab Sample IDs __

Sample wt/voli 25 .<Q/ml)HL Lab File IDt __ / 5*591

Levels <low/med>. LOW Date Receiveds

Moistures not dec.

Columns (pack/cap) .PACK

Date Analyzed i _

Dilution Factors _ I

CAS NO. COMPOUNDCONCENTRATION UNITSt<UQ/L or UB/KB>_UO/L.

74-87-3 —————74-83-9 ------7S-01-4 — —— -73-00-3 —————73-09-2 —————67-64-1 —————

75-34-3 —————

78-93-3 —————

108-03-4 —— —75-27-4 —————

10061-01-3 ——79-01-6 —————

2-Chloro»thyl-vinyl-»th»r __— — Ch loromvthan*- — B romometh an»__._._______ ___—— Vinyl Chlorid* _ ; __________—— Ch 1 or o*th an**—— l*l»thyl«n» Chlorid*............ .—— Acetone _™— .««—————Carbon Disulf id*—— 1, l-Dichloro»th»n«____. __ ,. _—— • -1, l-Dichloro«than»____ _____——lf 2— Dichlorovthvne (total) __——Chloroform—— 1 , 3-D i eh 1 or o« than*———2— But anon*—— 1, 1, l-Trichloro«than* ___._«— — Carbon Tetrachlorid* ______—— Vinyl Acetate ___ . ____ ____«.gponiod i ch 1 oromethane——If 2— Dichloropropane- — cis-lfS-Dichloropropene.......- — Trichloroethene............... _—— Di broMochloroMethane—— 1, 1,2-Trichloroethane __ . _ .__——— Bvnxvn*

10061-02-6 —— — — tran»-1.3-Dichloirbpropene___

108-10-1 — ——391-78-6 ————127-18-4 — ——

ioa-aa-3 — —108-90-7 —— —100-41-4 — ——100-42-3 ————1330-20-7 — ——JOT - O2 -«107-13-1

—— 4-Meth y 1 -2-Pent«ncme__ _____-— 2-Hest anone---,.______, _____ ._—— Tetrach loroethene_____. ____—— 1 ,1,2, 2-Tetraehloroethane __———To 1 uene—— Chlorobenzene............ _ ......—— Eth y 1 benz ene_________ ____ „.-»— Styrene—— Xylene (total) ____________

Acrolein _...__...____...»..Acrylonitrile................

0.20.360.210.260.190.3fcz.oo0.230.080.090.2518.30.121.380.130.110.350.190.140.170.120.060.070.03O.O60.080.080.480. 180.07O.ftl0.120.130.22o.a6.52

1 2.86

IUIUIUIUIU1IUIUIUIUIU1IUIU1UIUIU1UIUIUIUIUIUIUIUIUIUIU1IU1IUIUIUIUIU J|U

100400

IE EPA SAMPLE NO.VOLATILE ORQANICS ANALYSIS DATA SHEET ______________

TENTATIVELY IDENTIFIED COMPOUNDS !J EDG77

ao Name: VER5AR INC._____________ Contract: _________ !______

.*3 Code: VE35AR Case No. : 11724 SAS No. : 4337E SDO No. : EAL69

r*tTia: <*oil/water> WATER Lab Sample ID: 69941A

rft.r.Die ut/vol: 25. 0 (g/fliL> Ql._ Lab File ID: Y5391

.avel: <lou/med> LOW Date Received: 04/06/89

moisture: not dac. __w Date Analyzed: Q4/15/B9

siumn (pack/cap) PACK Dilution Factor: 5. Q

CONCENTRATION UNITS:-jmoer TIC* found: _0. (ug/L or ug/Kg ) UQ/L

CA3 NUMBS?ii

COMPOUND NAME•i

tiRT I EST. CONC.

ii

Q

FORM I VQA-TIC 1/87 Rev.

100401

VOLATILE ORGANXCS ANALYSIS DATA SHEETI

L*b Names__V»r»*r

*b Cod»i_V»r»ar__ Ca«» No. i t

Matrixi <*oil/wat»r>WATER

Contracti _T__

SAS No. i4, 3 E SDO No. i

" Lab Sample IDs __

EDG-81

Sample wt/vols 25 _<Q/ml)«L Lab File IDi ___ 5390

Levels (low/med) LOW • Date Received! _y

% Moistures not dec.

Columns(pack/cap) .PACK

CAS NO. COMPOUND

Date Analyzed i _y_

Dilution Factori _

CONCENTRATION UNITSi<ua/L or ug/Kfl>_UG/L__

74-87-3 —— -74-83-9 —— -75-01-4 —— -75-00-3 —— -75-09-2 —— -67-64-1 —— -75-15-0 —— -

75-34-3 —— •

67-66-3 —— •

78-93-3———

56-23-5 —— -108-05-4 — -

10061-01-5-79-01-6 —— •124-48-1 — •79-OO-5 —— •71-43-2 —— •10061-02-6-75-25-2 —— •108-10-1 — •591-78-6 — •127-18-4——

108-88-3 — •108-90-7 — •100-41-4 — •100-42-5 — •1330-20-7 — -

&%. 107- l^-l

2-Chloroethyl-vinyl-ether __

. ———— Vinyl Chloride• —— • — -Ch 1 or oeth ane_;. ______ _ .__- ———— Hethylene Chloride _____ 'm ___•———Acetone .._____._._._._.__«.__

— — —— 1 , 1 -Dich loroethne..........

- ———— 1,2-Dichloroethane

- ———— 1, 1, 1-Trichloroethane _____———— Carbon Tetrachloride ______- ———— Vi ny 1 Acetate.; ___________

———— ci»-l, 3-Dichloropropene _ ___———— Trichloroeth •»»•___„. _ .___„..._-— — — — — Di bromochloromethane

——— —Benzene _._„___»,„.______ _ ._———— tran»-1.3-Dichloropropene__-

———— 4-Meth y 1 -2-Pen*«none ______— ——— 2-Hex anone___ „-»-»- ___ ._

———— 1, l,2,S-Tetrachloroeth*ne __———— Toluene ______..___.._ __ _„„— • —— -Chloro benzene „.„____ ____ .

____ Stvrene———— Xy 1 ene < total > _ ; __________

Acr ol e i n __.«._....___. ____ .Acrylonitrile ————————————

0.2 IU0.38 IU0.21 IU0.26 IU0.19 IU0.23 IU"Z.OO IUo.y* iOb/Z7 1ZO.9 10.25 IU0.1 IU-0.12 IU1.38 IU4.C, 10.11 IU0.35 IU0.19 IU0.14 IU0.17 IUO.M8 10.06 IU0.07 IUIO.9 10.08 IU0.08 IU0.08 IU0.48 IU23.1 \'0.07 IU

oil2 IU0.4,8 10.3M 13.29 I6.52 IU J

, 2.86 |U

100418


SPA SAMPLE NO.

EDG81*b Nam»: VERSARINC. Contract: t

ib Code: VESSAR Cast No. : 11724

.#trix: (soil/u*t«r> WATER

impl« ut/vol: 25. 0 (g/mL) ML

*vtl: (low/med) LOW

^oisturs: not d*c. ^___

tlumn <pack/cap) PACK

lymbtT- TICs found: _C;


Lab SampU ID: A984QA

Lab Fil* ID: Y539Q

Datt Rtctivtd: Q4/QA/89

Data Analyztd: O4/13/89



11

CAS NUMBER ! COMPOUND NAMEI II 1

RT ! EST. CONC. ! Q

t >

FORM I VQA-TIC 1/87 R«v.

1U0419

1^-li,,

32-33

TO

TO

To

UNITED STATES ENVIRONMENTAL WlOTECTlONAttEhMQIONV

7C_

uiCT; tevlev of Region V CLP Data•tecelved for Review on___

c""l, JX<oO /O /

moil. Cart«s tosi. Director (5SCXL)Central Regional Laboratory

_$/; 5

Vt fcave reviewed tht data for the following case(s).

sm IUHEM Oat.

CRL •o

c«t

-a?;CLP Laboratory:

7/7 -y]for Review:

rollowlng art Our findings:

^ wt#nc£s »r&r<**/

*/* f

frfr' i* sf *_I J Data art acceptable for «se. ]/(/^>

*) DUa are aceeptablt for use with qualifications referenced above.tee Data Qualifltr fthttti and Calibration Outlltr foras for flags and'ddltlonal comments*

f j Data are preliminary * pending verification by Contractor Laboratory.See Case Summary above.

( ) Data art unacceptable.

« Carla Oe-npsty.CLP Quality Assurance Officer. Analytical Operations Branchr'ames Petty. Chief Ouallti* Assurance Rescireh. f^i . i »<

DATA QUALIFIERSf AGE T- or

:ontr«tor;

Below 1s a ium*arjr of the out-of-control audits and the possible effect on thefor this ease: ^x

fefm+fte

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ATAT

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by:Phone:Date:

DATA QUALIFIERSMCE 3 or

Contractor:i

Belo* 1s • »utnT.»-jr of the out-of-eontrol audits and the possible tfftct on thefor this case:

(f)

frs #5 u^LL A* hsn^f&Ck

l-tl-Ptt#&%e&ni&i6ft 'M* fa.

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by:Phone:Date:

3l7.-363-??nSho

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CASE/SAS $ //T?l

PROTECTION AGENCT REGION VCALIBRATION OUTLIERS

TILE HSL COMPOUNDSCONTRACTOR

Instrument * VDATE/T1M£: /

dhloroffiethaneBroffioêthaneVinyl ChlorideChioroethaneWethî^ne ChlorideAcetoneCarbon nisulfioe1,1-DicMoroethaneKl-DichloroetneneTrans-3.Z-DiChloroetheneChloroform?-Butanone1 ,?-Dichioroethane1 ,1.1-TrichloroethaneCfi'bon Tetrachlorif leV»n>i Acetate

[p-oi;5i'chloroêthane1 ,?-r'Cf-ioro?"opene|Trai$-l,3-DicMoropropenfT r * c^ * o*oetheêD * t ™ o™*oc h t o r o^'C * ha nejl ,1 »?-Trichloroelhane|Ber.:fieC ^ S ™ J .3*uChioroprop^he

'2-C^lo-oet^yl vinyl etherB'DTfO'f-A-^f t^v l -2-Pentanone

:2-He»anoneTetra:*" Ic'oethene1 ,1 ^ .P-Tet racr -MC-roethaneT G ' ê eC^l o^cT'e^zeêlthjiDe".:e*ieSty'eêrr-^j'le''-ec '?->j ie"e

Jfc/totiftt''JtcZmft/fAtif

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fi/67

CASE/SAS

CALIBRATION OUTLIERSVOLATILE MSL COMPOUNDS

CONTRACTOR

bATE/tlHE:

ChiopoêthaneBroff^TifthflneVi nyl Chl OPI deChloôpthaneKetnj'lene ChlorideAcetoneCarbon nisuifide3,1-DichloPOethane1 ,1-DicMoPoetheneTpans-3 ,?-DichioPoetheneChloPOfOPm?-Butanone],?-Dlchioroethane3 ,1.1-TricMoPoethaneCe-Don TetraeMopi'deV'tn>i Ace ta tef *o^^ c i c n i o poêt h a nej ,?"r*c'"' '0"o?"0pdêTpans-l ,3-DicnloPOpPOpeneIP* cfio'oetneien •« c- 'o~'DC M o POf.et ha ne1 .1 .Z-TricnloPoetnaneBe^êneC t S - 1 ^-D^ChlOPOpPOpene2-CHo'oethyi vinjletnerp-o--:foT.4-^f:^vl-2-Pentanone2-He i s^DêTe'.ra:^ icroethene1 .1 ,? t Z-Te tPa ,c r i iCPoe tnaneTolueneChio'cre r '2e r-eft^lDe'.reieSt^reêr-^'leêo/t*>yien?

A.'î'^/A/'0Ct(YiCA/lf?m£'

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ff/87

CASE/SAS

PKUitCUONCALIBRATION OUTLIERS

HSL COMPOUNDS

REGION V

CONTRACTOR

Instrument * yDATE/T1HI: ;

CMoromethaneBroffi^TiethaneVin_yi CMorideCnloroethaneHet^ylene ChlorideAcetoneCarbon nisuifide1 ,1-DicMoroetnane1.1-DicMoroetheneTrans-1 ,?-OicMoroetheneCMoroform?-Butanone] ,7-DieMoroethane3.),J-TricMoroetnar»eCe-Doi Tetract i lor ideVSnyi Acetategro^sSicMoroêthane1 ,?-P*cMoro?-opane

JTrais-1 ,3-DicMoropropeneTricfTO'OetêneT t< "o^c-c M o ror-et na nel,3J?-TrichloroemaneBenzeneC^s-1 ^-D^cMo'opropene2-CMo-Dft^yl vinyl etherp-cr:lo-r.fl-Vfinvl-Z-Pentanone

|Z-HeianoneTet 'aiMc'oeiêne1 ,1 .Z.Z-Tet racrnc*oeth«neToi ueê|C'iio*cr'epiref;eiEt^y^5e'•.7e"leIStyreneff-^yle'"'*c'z-Jyleê

p^f-c-LC-n^^.wj^^/ifR|L£

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.-.!„• A.

CASE/SAS

CALIBRATION OUTUERSVOLATILE MSI COHPOUNPS

7 7

CONTRACTOR

Instrument • Y&AU/tlM£: ' ———————

ChlOPomethaneproffioêthaneVinjî Chlopid*C^lOPOPthaneMethjrlene ChlpPideAcetoneCapbon nisuifide, ,1-DicMopoethane, ,1-DieMopoetneneT pans- 3 ,?-DicMoPoetheneCMOPOform?-Butanone, .?-Dicnloroethane

J.l-TPicnloPO§thaneCe-Bon TelPachiOPidev>n>i AcetateB -01351 cnlopowethaneJ.Z-r^cMorop-op«neTpans-1 ,3-DicMOPOpPOpeneTpicf'io'oethenepic.'o*-o:Moponethanel.l.?-TPicnloroetnaneBep7e«eCTS-],3-0''Chlorop"Op^ne2-C^lo-oet^ylvin^yl etherB-D'-:fo"ni.a-^f;".vl-2-Pentanone2-HexeiDieTetracMopoeihene1.3 ,2,?-Tetricr i icroetf i«neTcluen*'CMo-crfêêEtn>l&e'.2e"'eStypeêff-;>lenec's- iyieê

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£? AT*For reporting results tr *he VSDA, tha following contract specificqualifiera are to bo used. The seven •qualifiers defined belov arenog subject to modification by the laboratory. Up to fivequalifiers may be reported on Form X for each compound.

tha seven ZZA-defiaod qualifier.} <!» V need are «3 follows:

.U - Indicates compound was analyzed ^or but. dot eletaeted. Thesample quantitation limit must bo corrected for dilution sadfor percent moisture. For example, 10 U for phenol ia vater ift£e sample final volume is tho protocol-specified final volume.If a 1 to 10 dilution of extract is necessary, tha reportedlimit is 100 U* For a Mil sample, tha value must illft *•adjusted for percent moisture. For example, if tho sample bad24% moisture jn4 a 1 to 10 dilution factor* the samplequantitation limit for phenol (330 U) would bo corrected to:

and df • dilution factor

at iatura. 0 -

10 - 4300 U

100

- 0.7<100

.7*roundod to tho appropriate mabor of•ignifieaat figuroa

C *

For soil samples subjected to CK clean-up procedures, the GLQLis also multiplied by 2, to account for the fact that only halfof the extract is recovered. • .

Indicates sa estimated value. This flag is used either whanestimating a concentration for tentatively identified compoundswhere a 1:1 response is assumed, or when the mass spectral dataindicate the presence of a compound chat meets theidentification criteria but tho result is leas than the aamplequantitation limit but greater than sere. For example; if theaample quantltatioa limit is 10 ug/L, but • concentration of 3ug/L la calculated, report It aa 3J. The aample quantitation

___ F** •*** p*»»*j*» «t>!ilAS discussed for the V flag, so that if a sample with 24%moisture sad a 1 to 10 dilution factor has « calculatedconcentration of 300 ug/L sad a sample quantitation limit of430 ug/kg, report the concentration as 300J on Form 1.

This flag applies to pesticide results where the Identificationhas bean confirmed by GC/HS. Single component pee tic Idea £10ag/ul in tho final extract shall bo confirmed by CC/MS.

B-29 2/88

Thl* flag 1* «ood when tfao aaalyta la found In tha "bleak M mil aa ia tfaa »aapla. It indieataa posslbU/fcrobabl*blank contamination and wns tiba data uaar to taka appropriat*action. This flag wat bo usad for « TIC a* wall aa for -politicly idonfiflod TO.ThI* flag Idamttftaa •oaawmilf who** •oneontrations oxe**d th*Mllbratiom rang* of tho CC/MS inatrtsartt ^ thatiipoaifia .

thZTfUg will B&£ apply «• poat±cld*a/?C»a «nalyz*dIf ana or aero auoTpmindi hava a racponaoallTtb. a lTSIwttaet ~-c bo dllutad

-wording to cna apoclfieationa to bblbit D.vttb * xoapoBoo groatar Cfcaa fuU aealo••!! i •«!» n*ggod with «n-T «^o for. *

for tho original analyst*. If Aa dilution of tha oxtraetidanrlfiad in tho flrit gflT***, «•

bolow tha calibration rang* in tna oocond «B*l/.i., u«« tu.of both aaalyso. .ball bo roportad_on^.aparat. Jorm*

in* f w*^ * *v* ^»^ •••• — - ——— w — — — — —— — _amondad to th* aa»la artxr. TOTX: For total «yl*noa. ntw-r

Uoaars ar* fuantifiad aa t» poaks. th* calibrationf»««V aboold bo oonald*r*d ••of ««eh f»««V aboold bo oonald*r*d ••parataly, o.g

dilutad analy«ia ia n&£ roquirad for total «ylanaa unl*ai;ontratian of oitbor poak aaparataly ozcaoda 200

D - ttia flag tdontifioa all aoormmrta idantifi*d In an «n*ly«i*« ••condarj dilution factor. If a aanplo or ox«act iaro-analTzad at a highar dilution factor, aa in tha •£' Hag•Ixrr*. th* "Dt.- auffiz la app*tidod to tfeo aaarpl* numb *r onTor. I for tba dilutad aaapl*. and jU ooncantrattion v«la«jraportad on that Form I ara £Ugg*d wish tha -0" flag-

A - thia nag iadieataa that a TIC ia a mrfpoctad«ldal-oond«naation product.

X • Othor apocific flags »ay bo r*quir*d to prop«rl? dafin* sMroaultaV If uaod. thay w-t bo fully daacribod and atachd«jeription attaebad to th* Sao?la Data St ury Package and .CM*. lUrrativ*. B*gin by uaing -XV If ~r* than on* flag i

* • * ___•uaUflars ara roqulrod for a sampla rooult, «ao tha "XiTwobl« oowrU flag*. •• aaodod. For inataneo. th* -Xflat might Mofcino tho -A". •*". and -D" flaga for aoo* aaa?l

tho oooftlnation of flags -W •r^JB- la oproasly prohibitad. 11.. 'contaninantj aro flagged •»" P«^ *oa thay ara alao d*eoct*d In i-aaaplo.

If analv**s at two dif foront dilution fwrtora at* r*quir*d Ca**Exhibit* »J. follow tho data ropoctirg instructieas given In Exh.D «pd »lth th* *!>• and •!• Hags abov*.

1-90 2/i

USEPA CONTRACT LABORATORY PPOGBAMSAMPLE MANAGEMENT OFFICEP.O. BOX 818 ALEXANDRIA. VA 22313703. b57 2490 FTS-S57-2490


TYPE OF ACTtyiTY (CmCLESUPCTRJNO—PA * ESI

- -I»ll)

0en

JiJi.B'

V

SMPTCt

ATDt .BitMTI:

DATE

DATE RCCO:, 8OQ HO:

AECt I BY: A. ..Ta.^IIT NO. UNTTPMCE

TQc DAT!

B«C*O IV: CONTRACT NOJPflCt

NUMBCfl

-r,' c:;,WQHOOMC..pKAaea

iiL

rngonor XTT^CS;

*&* RR v .* "pfOfeifii^ ^EPA FOM 2071-7 (»-nj

WHITE - SMO COPY PINK COPY WHITE - LAS COPY FOB RETUAN TO SMO YELLOW — LAB COPY1U0007

cAPR 2 7 1309

CENTRAL REGIONAL LABORATORY SAMPLE DATA REPORTORGANICS/INORGANICS

THIS FORM IS TO BE USED FOR SAMPLES SENT TO CONTRACT ONLY

0fir&

CASH NUMOEH/SAS No

SUPEItrUNO OU NUMBERAC 11VIIV NUMBER (

L?P

LABOHAIOAV.

PA RPM Of OSC |S M S VICESI NUMBER

DA1E SHIPPED

————PAGE

on LIQUIDS SEDIMENTS oc SOILS

cm. LOGNUMBER



orSAS Packing List No.

5 *

I *

ss'

P

ii F

Hg «1«,f *IRlit I I

SIS tALswSlot

btfton

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c cAPR 27 1989Ar" '

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CENTRAL REGIONAL LABORATORY SAMPLE DATA REPORTORGANICS/INORGANICS 0tt& £M&2

THIS FORM IS JO BE USED FOR SAMPLES SENT TO CONTRACT ONLYUtu F

SUrtlltUNUOU HUM

AC1IVIIY NUMBER |

CRL LOGNUMBER

2(?2.C03wSO--5>ol--^—S«f-5o?- /2/J

-5 SIJyo^/73Sfc^(01

JstfSt.^0*5ok£»*)£tqS3f5io^j ^H(/

^b&df'TFftnm^V*^. • ^ FEPA RPM or C

^75^^^

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CMSAS Packir

£frt'7S:'«'^ 4_l I*Jf Mittf\* * T 7

£I>C3V^£A-L^f>*t/fru* * *

^O^^/f^OG 31/£oJL 82-W&*ltt><£> fO££>£>*•/•/€b& V^£4-t »70£*-t 9f

/K, />7£^D^ °if2Dfe ' '€oc»4?0>0»^WEOCUV7

F/V^-i


rig List No.

)SC |S MS I/ICES i Y^T>- ^J-/Y^*HLY— -^ (**

:ERCLIS NUMBERWATER OR LIQUIDS

AC

B4A

SI

NfUT

HALC

FOS

UG

'L

TOX

1TI7

* 1ii1

3

14

!1:2iis

VC

ULS

Unoa

OU

VM

HffllO

Ml

sh

» ii!

f

§ s

Ml1

ri

i ii

iii•

H|(1: MU

ttU

t NO

N-*H

.T

TSS

MO

'L

MM

7TT7

1)Cj(^^^X-Kj^X^jj'KkItX^£fcK.

Ai ft PAGf V_ OF JL..

SEDIMENTS or SOILS

AOO.

MSI N

iunu

i ens

OHO

4NIC

SCAN

Mfi/

KO

T

OK

IinS

ij1

§i

i SEO

IMtN

TS P

OvT

CMLW

IWAT

tO«m

iNns

MG

/KO

K

S31

M23 a oI

3 !

a

i -

CP TO

MOTT

MKT

«UM

O/K

6i!

Hay 4, 1989

I. NarrativeOrganic* Caae 11724 SAS* 4337E SDO# EAL74EPA Region V - Curti* RoaaV*r*ar Project 969.80 - Batch 4

Thia report containa the CLP analytical data for the volatilelov detection liait organic analyeia of nineteen (19) water•ample* contained in Caae 11724 SDO EAL74. The aaaplea li*tedbelov arrived intact at Veraar by Federal Expre** on April 5,1989.

SofiCLE LIST"EAL74- •OSAL73EAL7C --EDG04

^EAL80 -* ED032-EAL81 — EDQ3»

— EAL86-CAL94

—— EAL99CD001

• - Firat aaapla in SDO*• * Laat eaaple in SD6

*«**••••••***•**••*************•****•**»•**•*****•***»••»•*******SAS ONLY

No Diskette DeliverableSeven day aample holding time30 day hardoopy report due dateLow Detection Limit Analyaia

Acrolein t acrylonitrile added to volatile target compound li*t*

QC/MS in*trument calibration* u*ing BFB met contractrequirement* for volatile analyaia. SPCC and CCC criteria weremet for the volatile initial calibration curve* and continuingcalibration check atandard. All QC/HS analyae* occurred duringthe twelve hour period following daily instrument calibration.

All volatile internal standard area abundance* and relative ::retention time* were compliant for all analyae*. .•

Volatile aurrogat* standard recovery value* met all apecified ;., OC limit*. One *et of matrix apika/matrix *pike duplicateanalyaia vaa performed in conjunction with thi* SDG. '

No *ample required dilution prior to analyeie. •C ' -T S

rf

100005 ;

T

Narrative - Pag* 2 fVerear Project 965.80 Batch 2 t

iA

Pleaee contact Clay Hamner, CLP Project Manager* ehould you •have any queetione or require additional information pertaining :to the lev detection limit analyeia of theee vater eamplee. ;

Releaee of the data contained in thie hardcopy data package hae 'been authorized by the Laboratory Manager or hie deeignee, aeverified by the following elgnaturei .

May 4, 1969Linc^a E. BockGC/MS Data Proceeeing CoordinatorLaboratory Operatione

r-

100006

Lab Namvi

Lab Cod*t

SAWATER VOLATILE SURROGATE RECOVERY

VERSAR Contract I ____.

VERSAR C*»» No.t11734 8AS No.i4537E SDQ No.s _ EAL74

1 EPA1 SAMPLE NO.

01IEAL7402 1 EAL7503 1 EAL7604 1 EAL8005IEAL8106 1 EAL8S07 1 EAL8608 1 EAL9409 1 EAL9510IEDG011 1 1 ED30212IEDG0313IEDG0414IEDG3215IEDG3316IEDG3617IEDG3718IEDG4319IEDG5820IEAL80-MS21IEAL80-MSD22 1 VBLK0623IVBLK2124 1 VBLK4225 1 VBLK5926127 1 __281 _ _ _ _291301

SI<TOL>#

9710210310798939797971031011011011041049910710396939410410098100

S2<BFB>#

106104103981021051021031009797989797951059610410610410398106101100

S3(DCE)tt

1049999919495959689114112111111111109101110981019797110989493

____

OTHER

.

I ___ I~

______

mni

imiimillmill__i _ ii« -

TOTOUT

0000000000000000000000000

00

QC LIMITS51 (TOD * Toluwrwda (68-110)52 (BFB) * Bromofluorob«nz»n» (86-115)53 (DCE> « 1,2-Dlchloro«than»-d4 (76-114)

41 Column to b» u»«d to flag r«cov»ry valuvm

* Valu*m outmid* of contract r«quir«d QC limit*

D SurrogatM diluted out

page _1 ofFORM II VOA-1

100003

3A^; WATER VOLATILE MATRIX SPIKE/MATRIX SPIKE DUPLICATE RECOVERY

Lab N*m«i VERSAR Contracti___________

Lab Codvi VERSAR Cam* No.i 11724 SAS No.I4537E 8DG No.iEAL74

Matrix Spike - EPA Sample No.i£ALS0 LOW

COMPOUND

1, l-Dichloro»th«n* _ _Trichloro«th»n» ______..B*nz«n» . ________ „Toluvn* _ „, __ _ .....Chlorob»nz»n« _

_ __ ___

SPIKEADDED<ug/L)

2080808020

_ ___ _

SAMPLECONCENTRATION

(UQ/L)

00000

MSCONCENTRATION

(UQ/L)

10.518.716.717.980.5

MS 1 QC 1* (LIMITS!

REC ttl REC. 1

53 *I61-145I94 171-180184 176-187190 176-125 1103 175-1301

t 1

COMPOUND

1, 1— Dichloro»th»n«___, _Tr i ch 1 oroe-t h*n»— —— .B»nz*n* _ M _ „ __Tol uwn* .. ________ ._Ch 1 or o b»n z «n« .......

SPIKEADDED(UQ/L)

8080808080

MSDCONCENTRATION

(ug/L)

IS. 580.918.219.982.9

MSD%

REC tt

6310591100115

%RPD «

17 *1191111___

IQC LIMITS 1RPD 1 REC. 1

14 161-145114 171-180111 176-127113 176-125113 175-1301

1 1

* Column to b» UM<J to flag r«cov«ry and RPD valu»» with an amt«ri«k

* Valuam outbid* of QC limit*

RPDi 1 out of 5 _ outside limit*Spik* R»cov«ryi 1 out of 10 outsid* limits

COMMENTSI

FORM III VOA-1

: VE3SAR INC

4AVOLATILE METHOD BLANK SUMMARY________ Contract: ______

.*- Code: VERSA* Case No. : 11724 SAS No. : 4537E SDC No. : EAL74

a: Filt ID: Y5306_____ Lab Sample ID: VBLK06____

04/12/89 Tim* Analyzed: QQ50

Ltvtl:(low/mtd) LOW

rstrument ID Y_______

£73 Analyzed:;iT7 -i x: (soil/water) UATER

THIS METHOD BLANK APPLIES TO THE FOLLOWING SAMPLES, MS AND MSD;

01w*l03040506Q7

EPASAMPLE NO.EDGO:SD502EDG03ED004EDv32ED533EtQ37

LABSAMPLE ID

69729697306973169732697336973469736

LABFILE ID

Y5307. YS30BYS309YS310Y5311Y53I2Y5314

TIMEANALYZED

0213025003300410045005300649

CL?. - , VBLK06, L> W, VBLK04,V, , , 25ML1N=T V SP-1000 45COMIN) TO 225C 8C/MIN

1 of 1FORM IV VOA 1/87 Rev.

100009

• fcb Name: VErSAR INC.


________ Contract: ______

;"tis Code: VE55AR Ca«e No. : 11724 SAS No. : 4S37E SDG No. : EAL74

L-?; File ID: Y5321_____ Lab Sample ID: VBLK21_____

"fcT* Analyzed: Q4/12/B9

-strix: (soii/water) U1ATER

:-itrumtnt ID: Y _

Time Analyzed:

Level: Uou/med)

1S40

LOW

THIS M=THOD BLANK APPLIES TO THE FOLLOWING SAMPLES, MS AND MSD:

01•1'-'tf.

03040306

EPASAMPLE NC.

SAL74EAL75EAL76EDC30EDS43EDG5S

LABSAMPLE ID

697396974069741697356973769738

LABFILE ID

Y5326Y5327Y5325Y3322Y5323Y5324

TIMEANALYZED

195020411907165817381826

CL&- , , VBLK21.L. W. VBLK2i> V, BLANK, , , 25MLIT45T Y SP-1000 4SCOMIN) TO 225C 8C/MIN

1 of 1FORM IV VOA 1/87 Rev.

100010

INC

4AVOLATILE METHOD BLANK SUMMARY________ Contract: ______

;14:. Code: VERSAR Ca*e No. : 11724 SAS No. : 4537E SDO No. : EAL74

_*: Fil» ID: V5342_____ L»b Samp It ID: VBLK4B____

DITS Analyzed: 04/13/99 Tim* Analgi*d: 1226

rttrix: (*oil/w«t»D UATER Ltvftl:<lou/mtd) LDU

~~.strumtnt ID: Y

THIS METHOD BLANK APPLIES TO THE FOLLOWING SAMPLES* MS AND MSD:

01020304030607

EPASAMPLE NO.

EAL80EAL31EAL35EALB6EAL94EALBOttSEAL80MSD

LABSAMPLE ID

69742697436974469745'697466974269742

LABFILE ID

Y5344Y5345Y5346YS347Y5348Y5349Y3350

TIMEANALYZED

1408145315321614165517371819

VBLK42, L* W, VBLK42, V, BLANK, , . 25MLINS7 Y SP-1000 45CC3MIN) TO 225C 8C/MIN

FORM IV VOA 1/S7 R»v.

100011

it N*mt:


________ Contract: ______

.s: Cod*: VE5SAP- Ca*» Wo. : 117S4 SAS No. : 4S37E SDC No. : EAL74

.it Fil» ID: Y5359_____ Lab Sampl* ID: VBLKB9____

iT3 Analyzed: 04/14/B9 Tim* An*lvi*d: 1112

: = Trix: (aoii/watfeT) U1ATEP Ltvvl: < lou/mtd) LOW

~. 5trum«nt ID: Y

THIS METHOD BLANK APPLIES TO THE FOLLOWING SAMPLES. MS AND MSD:

; EPA! SAMPLE NO.

01 IEAL93

LABSAMPLE ID

69747

LABFILE ID

Y5370

TIMEANALYZED

1846

C-P. , > VBLK59, L, W, VBLK59. V, BLANK, , , 25MLINST Y SP-1000 45COMIN) TO 223C 8C/MIN

;«s« 1 of 1FORM IV VOA 1/87 R*v.

100012

: i' 0 L a.' 0 1AVOLATILE ORSANICS ANALYSIS DATA SHEET

ERA SAMPLE f-

IM*fli*: VEPSAR INC Contract:VBLK06

*: Ccie: VESSAP Cas* No. : 11724 SAS No. : 4537E SDG No. : 724

= rr; > • (*eil/uat»r) WATE5 Lab Samp It ID: VBLKQ6

•*-;£• le ut/'vol'

* ,-sl: < law/mac!)

>:- is tur* r.ot dtc.

<g/mL>

LOW

Lab Filt ID: Y53Q6

Datt Rtctivtd: ____

ipack/cap) PACK

Datt Analyzed: O4/12/B9

Dilution Factor: S. Q___

CA5 NG. COMPOUNDCONCENTRATION UNITS:Cug/L or ug/Kg> UG/L

Chloromathan*___________74-S2-9————————2romQmathana_ ________,75-0 i -4———————V i n g 1 C h 1 or i d e__________71-00-3————————Chloro«than«_____________75-Oc-2————————Methy l«n« Chloride_______67-64-1———————Ace ton*________________75-1 5-0————————Carbon Di iul f i d t_________75-35-4——————.— 1. l-Dichloro«thtn«_______75-25-2———————1* 2-Dichloro«thant_______540-5^-0——————1. 2-Dichlorotthtn« (total)67-66-3———————Ch lor of orm_____________107-06-2——————1. 2-Dichlorotthant_______7S-93-3—— •————2-Butanone_____________71-55-c—— ————1. i, l-Trichioro*than*____56-23-5———————C*r b on Tttr ach 1 or i d e_____10S-O5-*———————Vinyl Ac«tat»_____________75-27-4—————• —— Eromodichlorom*than*_____7S-87-3———————l, 2-Dichloropropan*______10063-01-5—————eit-1'3.-Dichloropropant_79-01-=—————•—Trich lor oath «n»_________124-4S-I——————Dibromochlorom«thane_____79-00-5—— -————1, I, 2-Trichlorotthan«____71-43-2————————Banstna________________75-25-2—————————Bramof orm ________1 OS-10-1——————4-M*thyl-2-Ptntanone_____5* 1 -78-6——————2-H» x anona_____________127-1S-4——————Tetrachlorot thtnt_______79-34-5————————li l> 2- 2-T*tr»chloroethan»_10S-S3-3———————Tolu»na ____________1 OS-90-7——————Chlorobtnztnt_______»„__100-41-4——————Eth y 1 b tnitn*____________100-42-5———————Styrtna____„____________1330-20-7——————Total X«l«nt«___________1O7-O2-5———————Acroltin_____;__________107-13-i——————Acrylonitrilt___________

0. 4!U0. 2!U0. 3!U2!U2!U!U

21U0. 08 !Uo. 09 :u0. 3!U0.0.10.0.0.0.0.0.0.0.0.0.0.0,20.0.0.0.0.0.0.73

3!U2iU

2!U

2!U2!U

2IU

:u21U

1IU2!U2!U:u!U


100445

IE EPA SAMPLEVOLATILE ORSANtCS ANALYSIS DATA SHEET _______________TENTATIVELY IDENTIFIED COMPOUNDS I

i VBLK06*b Nam*: VERSAR INC._____________ Contract: _________ !_________'

"LiD Code: VgRSAR Case No. : 11724 SAS No. : 4937E SDC No. : EAL74

Matrix: <ioil/uat*r) UJATEfi Lab Sample ID: VBLK06______

S*rt.p3« ut/vol: 23. O (g/mL) (3U__ L*b Filt ID: Y53OA

i-5-vfl: (low/m*S) LOW Datt R»c*lv»d: ____

r, floistuT*: not d*c. ___ Dat» Analyzed: O4/12/89

Ctlumn (pack/cap) PACK Dilution Factor: 5.O

CONCENTRATION UNITS:iwnfctr TIC» found: _£ <ug/L or ug/Kg) UQ/L

i :CAS NUMBER I COMPOUND NAME 1 RT

i :

'EST. CONC. Q

FORM I VOA-TIC i n n I '£? R»v-1004

* 1AVOLATILE ORGANICS ANALYSIS DATA SHEET

EPA SAMPLE

Namr: VEHSAR INC

"..*;• Ccdt: VEffSAR Case No. : 11724

Contract: ____

SAS NO. : 4537E.

VSLK21

SDC No. : 724

r:*TTix: doil/uattr) WATES Lab Saftplt ID: VBLK21

imp It wt/vol: 25. 0 (g/mL>

fvtl: <lou/mtd) LOW

Hoitturt: not <Jtc. ___

Lab Filt ID: Y5321

D*tt Rtctivtd: ____

'„ - j, L? mn:

r

< p a c k / c a p ) PACK

Datt Analyitd: Q4/1S/99


CAS N3. COMPOUNDCONCENTRATION UNITS:(ug/L or ufl/Kg) UQ/L

74-37-3—...—————Chloromtthant____m____.74-S3-*————•——-Eramorngthana75-01-4————————Vinyl Chloridt__________75-00-3———————Chiorotthant.___________7^-09-2————————Mtthg Itnt Chloridt ____67-64-1————————Acttont____m___________75-15-0———————Carbon Ditulfidt________75-35-4———————1, l-Dichlorotthtnt______75-35-3———————1. 1-Dichlorotthant______540-59-0———————1. 2-Dichlorotthtnt (total),&7-6e-3———-———Chloroform _____^__—107-06-2——————1, 2-Dichlorotthant ____7£-?3-3-———————g-5ut*non«71-55-b———————I/ 1* 1-Trichlorotthant____56-23-5———————Carbon Tttrachlorid»_____10S-05-4——————Vinyl Acttatt.___________75-27-4—-————Brofr.odichloromtthant_.__^_7S-S7-5———————1< 2-Dichloropropant_____lOOel-01-5—————cii-1*3.-Dichloroproptnt_79-01-c————————Trich lorotthtnt ____124-4S-1——————DiSromochloromtthant^____79-00-5———————1, 1. 2-Trichlorotthant____71-43-2————————B»nt»nt ___________75-25-2————————Erpmof orm10S-1O-1——————4-Mttl-.«l-2-Ptntanont_____591-7S-6——————2-Ht x anont _____________127-1S-4———————Tttrach lorotthtnt________79-34-5————————i, i, 2, 2-Tttrachlorofthant_10B-SS-3——————Tolutnt________________1 OS-90-7——————Ch 1 or ob tn z tnt_______.^.^1OO-41-4———————Ethyl btnztnt____________100-42-5———————Styrtnt______________^1330-20-7——————Tctal Xultnts ____107-02-E———————Acroltin________________107-13-1———————Ac r ylonitril t___________

4!U2!U3!U2!U2!U

00000140. 2!U

0. OSiU0. 09 !U0. 3IU

:u0.0.10.0.0.0.0.0.0.0.o.0.0.0.20.o.0.0.0.0.0.73

1i :u;u;u;u

3iU2!Ui :u2!Ui :u2!U2iUi;u2;u3!U!U

i :u2tU

2IU2;u:u:u

FORM I 1/87 Rev.


. ERA SAMPLE NO.

b N«m«: VEffSAR INC Contract:VBLK21

Lib Cod*: VER5AR Cas« No. : 11724

N*trix: <*oil/uat*r) WATER

rx-Tiplf wt/vol: 25. O (g/mU> QU_

Lfrv*l: t low/mtd) LDU

% *tci*tur»: not d*c. ^^_.

•Irlumn (pack/cap ) _

r.^"r,fr»r TIC* found: _Q,

SAS NO. : 4537E SDS No. : EAL74

Lab Samp!• ID: VSLK21

Lab Filt ID: Y5321

Datt R*ctiv»d: ______

Datt Analgztd: 04/12/89

Dilution Factor: 5.Q____


)

CAS NUMBER ! COMPOUND NAME RT: i

EST. CONC. ! Q i* ii i


100451


EPA SAMPLE

*t NiTie: VgRSAR INC.

w Ci u • '

Contract:VSLK4S

i. -.' •i - - •— ». <t Ca»e No. : 11724 SAS NO.: 4S37E SDO No. . 724

r'3t"i x: (soil/water) UIATER

= *-iple ut/vol: 25. 0 (g/mL>

'..?vel: (low/med) LOR

Lab Sampla ID: VBLK42

Lab FiU 10: Y5342_

Datt Received: _____

c i iture not dec.

'.: •'. L:mTv (pack/cap) PACK

Datt Analyzed: Q4/13/S9


NO. COMPOUNDCONCENTRATION UNITS:(ug/U or ug / K g > UO/L

74-E7-3——•——-—Ch l o r o m e t h a n e _ _ _ _74-53-9-—————3r3mofflfthane_________^___75-Ql -i——-—-— ———W inyl Ch I or i d • _____7J-00-3--——-———Chloroethane.^______ -75-C9-2——————Methyleni Chloride______fc7-c4-1 —-—"--—Ac 11 one _________75-15-0————————Carbon Diiulfide________75-35-4———————1, 1-Dichloroethene______75-35-3———————l, l-Dichloro»thane_____540-59-0——————1. 2-Dichloroethene (total)67-6r--3——•—————Chloroform,^__________107-Oc-Z——————1^ 2-Dichlorotthane______75-93-2—————•—2-Butanone_^__________71-35-e———————I/ li 1-Trichloroethane____5^-23-5—————-—Carbon Tetrachloride_____i05-C5-4———————Vinyl Acetate______^____75-27-4————————Br-3modichloromethane_____75-S7-5———————li 2-DichIoropropan*_____10061-C 1-5—-———ci i-1- 3- -Dichloroprop»ne^79-01-e———————Tr ich loroethene.________1*4-42-1——————Difcromochloromethane_____79-00-5———————l, I/ 2-Trichloroethane____•^i-43-I———————Benz-ene____.m___________75-2 5-2————— —— EroTiO-form ______^___105-1C— 1——————4-Methy l-2-Pentanone_____I9I-7S-6——--——2-Hexanone_____________127-13-4——————Tetrachioroethtne_______79-34-5———————l, 1, 2- 2-Tetrachloroethane_1 OS-85-3——————To I ue ne._______________1 OS-90-7—"—————Ch 1 or o benzene,__________: GO-41-4——————Ethyl benzene,___________100-42-5———————Styrtne_________________1330-20-7——————Total Xylenet______^____107-02-S———————Aeralein ____________107-13-1 ——————A crylonitri 1 e__________

FORM I VOA

0. 4!U0. 2! UO. 31U0. 2!U0. 31'fl'2 i-8"0. 2IU

0. 081U0. 09 !U

0. 30.0.10.0.0.0.0.O.0.0.0.0.0.0,20.0.0.0.0.0.0.73

li3!2'i:2)i :

uuuuuuuuuuu

2!U2!Ui!U2!U3!U

!Ui:u2!Ui:ui;ui;u2!U2iU

!U:u

1/S7 Rev.100453

IEVOLATILE ORCANICS ANALYSIS DATA SHEETTENTATIVELY IDENTIFIED COMPOUNDS

EPA SAMPLE NO.

£5 Nam*: VERSAP INC

.*5 Code: VgqSAR Case No. : 11724

**r tx: ( toi l/wat*r ) WATER

«n.plt ut/vol: 25. 0 <g/mL)

*vt 1: (lou/mcd) LOUI

rcai«tur»: net d»c. ___

*lumn (pack/cap) PACK

'- .-:r«r TIC* f cund:

Contract:VBLK42

SA5 NO. : 4537E SDG No. : EAL74

Lab Samplt ID: VBLK42

Lab Fill ID: Y5342

Dat* Rtctivtd: ______

Date Analgztd: Q4/13/89



{C*iS NUMBER I COMPOUND NAME

[

RT EST. CONC. Q

rFORM I VOA-TIC

1AVOLATILE ORSANICS ANALYSIS DATA SHEET

EPA SAMPLE

VBLK59.40 Name: VERSAR INC Contract:

-s? Code: VEP5AP Case No. : 11724 SAS No. : 4537E SDQ No. : 724

i^itrix: (soil/water) U1ATER Lab Sample ID: VBLK99

Sfc.T.ple wt/vol: 25. Q <g/mL> QL._ Lab File ID: Y9359

_f-vsi: (lou/med) LOW Data Received: ______

isturt: not dec.

umn

r

(pack/cap) PACK

Data Analyzed: 04/14/B9


CAS NO. COMPOUNDCONCENTRATION UNITS:<ug/L or ug/Kg> UQ/L

74-S7-3———-———Chloromathant___________74-33-?———————Bromomethana______________7.5-01-4———————Vinyl Chlorid*__________75-00-2—— -————Ch lorotthant____________75-09-2———————M*thy lant Chloride_____;__67-64-;————————Acetone________________75-3 5-0————————Carbon Di«ul*id•_________75-35-4———————i, 1-Dichlorotthtn*______75-35-3——————-i, 1-Dichloroathana______540-59-0———————i. 2-Dichloro*th*n* (total)£7-66-2———————Chloroform _____iCT-Os-2——————1, 2-Dichlorotthan*______7S-93-3—-—————2-Butanone____________7:-55-e————————1, l, l-Trichloro*thane____56-23-5———————Carbon Tttrachloride_____1G5-05-4——————Vinyl Acatata___________75-27-4———————-Br omo d ichl or omt thane_____7S-S7-5———————i, 2-Dichloropropane_______10061-01—9™——c it-1* 3. -Dichloropropane_79-01-6————-——Trich lor oath ana__________124-43-1——————Dibromoch lor ome thane_____79-00-5———————1, I, 2-Trichloro*thane____71-43-2———————Benzena________________75-25-2————————Sromoform _____________103-10-1——————4-tt*ttiyl-2-Pentanone_____591-7S-6——————2-Hexanona_____________127-1S-4——————Tetrachloroathen*_______79-34-5————————l, l, 2» 2-T*trachloroethane_108-82-3——————Toluena________________1 OS-90-7——————c h I or ob t n rent__________100-41-4——————Ethyl banian*____________100-42-5——————S t y r trna __________1330-20-7—————Total Xyltnai___________107-02-S———————Aerolain ___________107-13-1——————Acrylonitril*___________

FORM i VOA

4IU2!U3;u2!U6;u

2!Uo. oe ;u0. 09 !U0. 30.0.10.0.0.0.0.00.0.0.0.0.0.20.0.0.0.0.0.0.73

u1IUl i U:u

i:ui:u3!U2!Ui:u2!Ui:u2!U2!U1!U2!U3;uJ U

1!U2 IUliUi;uiiu2!U2!U:uJ U

1/87 Rev.

100471

VESSAR INC,

. E C oc s; VE35AP

IAVOLATILE ORGANICS ANALYSIS DATA SHEET

Contract: _

ERA SAMPLE

EAL74

Casa No. : 11724

TTIX: (ioil/wat*r) UATER

SAS No. : 4537E- SDG No. : 724

Lab S*mpl» ID: 69739

- r -' ft

D 1 * Ut/VOl-

(low/flitd)

25. Q <g/mL> QL_

LOW

Lab Filt ID: YS326

turt: not dec.

". :•. l'_:mn: (pack/cap) PACK

Data Racaivad: O4/Q5/89

Data Analyiad: Q4/12/89

Dilution Factor: 5 Q

CAS NQ. COMPOUNDCONCENTRATION UNITS:<ug/L or ug/Kg) UG/L

74~B7-3———————Chloromethana____________74*03-9————.——-Bromom»thant____________75*01-4———————Vinyl Chlorida__________75*00-3———————Chlorot thant____________75-09-2————————Mtthy Itna Chlorid•_______67-64-1————————Act tont_________________75~lS-Q———————Carbon DitulfIda________75-25-4———————I/ 1-Dichloroathtna______75-3?-3———————li 1-Dichlorotthan*______540-P9-0———————1, 2-Dichlorotth«n» (total)o7*66-3———————C h 1 or o f orm______________l07-Oz-2———-——1. 2-Dicfilorotthant_______75.93-3————————2-Eutanona71-55-e———————1. 1- 1-Trichloroathane____5i-23-5———————Carbon Tttrachloride_____103-05-4-——————Vinyl Acatatt__________^75-27-4————•—-Br3fflodichlorom»than*_ .___7S-S7-5———————1. 2-Dichloropropan*,_____10061-01-5-—-——ci*-l» 3t-Dichloropropana_.79-01-0————•——Tr ich loroathana _______124-43-i———————DibrnmcchlarQmathang79-00-5——-————I/ li 2-Trichloro«than*____71-43-2———————Banitnt________________75-25-2—-——-——Srsmoform __________„1 OS-10-1 ————•—4-M* t h y 1 -2-P an tan o nm591 -73-s——————2-H« * anona_____________127-1S-4—•——-—Tetrach lorotthent_______m79-34-5———————1* It 2> a-Tatrachlorotthana_105-SS-3———————Toluana_________________103-90-7——————C h 1 or o b an i ana___________100-41-4——————Ethyl banztne____________100-42-5———————Styr*na_________________1370-20-7—————Total Xylantt__________1G7-02-S——————Aero 1 tin_______________107-13-1———————Acrylonitrila________;___

FORM I VOA

4!U2{U3!U2!U2.'U

0000030. 21U

o. oe :uo. 09 :u0. 30. 10. 110.0.0.0.0.O.0,0.0.0.0.0.20.0.0.0.0.0.0.7.3

uuu:u

1!U11U3IU2!UliU2!UliU2!U2!U1 I U21U3iU:u

l i U2iU1IUi:ui:u2iU2iU:u:u

1/87 Rav.

J00019



ERA SAMPLE IS

EAL74it N*m»: INC. Contract:

- s •:• C c- b « : VESSAR Case No. : 11724 SAS No. : 4537E SDC No. ; EAL74

*r?.plt ut/vol: 25.

?vg i : ( loui/mtd ) LOW

" :• 1 1 1 UT * • n c- 1 dec. ___

: i -.• r.r. (pack/c«p> PACK

WATER

55. 0 (g/mL) QL._

Lab Samplt ID: 6*»739

L*b Filt ID:

Date Rectivtd: 04 /OS/ 99

Dat« Analyztd: 04/12/69

Dilution Factor: V Q

j-.zrT TIC*CONCENTRATION UNITS:(ug/L or og/Kg) US/L

•;*£ NUMEE^ i COMPOUND NAME ! RT

i i

EST. CONC. G


100020

.C2q. . 1AVOLATILE QRGANICS ANALYSIS DATA SHEET

EPA 3KMPLE

EAL73,b Name: VER5AR INC

: Code: VE'Sa?

Contract:

Case No. : 11724 SAS No. : 4537E SDC No. : 724

<foil/uat«r> UATER

ut/vol: 25. Q (g/mL) BL

LOW


Lab Filt ID: Y5327

Date Received:

:ur*: r, o t dec.

::lumn: (pack/cap) PACK

04/03/89

Data Analyzed: 04/12/99

Dilution Factor: 5, Q____

r

CA3 NO. COMPOUNDCONCENTRATION UNITS:<u g / L or ug/Kg) UQ/L

7A~g7_3——————Ch:oromathan«____________7--B3-9—•——-——Sr omo math ant _ ________75-01-4———————Vinyl Chlriridt__________75-00-3———•———-Chloroethan»,_______________75-09-Z———————M*thyItnt Chloridt_______67-64-1—-—————Acatone __________75-15-0———————Carbon Ditulfidt________75-35-4———————i, l-Dichloro«thtn«_______75-35-3———————It 1-D1 eh lor o« thane54O-S9-Q——•————I* 2-Dichlorotth*n» (total)67-66-3—•——————ChlarBf orm ____________107-06-2——————1, 2-Dichlorotthane,______78-73-3—-——-——2-3utanon» __________71-55-6——————'-i, I, 1-Trichlorotthant____56-23-5————————Carbon T«trichloride,_____1O8-OS-4———————Viny 1 Ac»t«t«____________75-27-4—————-——Bromodiehlprofliathjn*7B-S7-5———————i, 2-Dichloropropane____^!O'561-Oi-5————e !»-!' 3* -Dichloroprop»n»_70-0:-6———————Trich lorotth«n» _____124-43-1—————— Dibroniochlorom»than*— _____70-00-5———————i, i, 2-Trichloro«than*____71-43-*75-25-21 OS-10-1———————4-M*thgl-2-^«nt*none591 -7S-c——-————2-Ht x anon t__127-1S-4——-————T«trachlorottft»n*79-34-3———•————i, i, 2* 2-Tttrachloro*thantIOS-BS-3--——-—-Tialu-n*1O8-TO-7——————Chlorab«nz»nt100-41 -a ——————E thylbtnz t n t_100-42-5———————S tyrant.1330-20-7——————Total Xyltnt*107-O2-S———————Acrol*in_________\107-13-1™————AcT-ulonitrilt

0. 40. 220. 2150. 2

0. OS130. 1

' 0. 110. 10. 10. 3G. 20. 1O. 220. 20. 20. 10. 2O. 320. ?0. 20. 10. 10. 10. 20. 2

:u:uit:u

:uJU

JU--JUJU:u:uiu:u!U;u•i:u:u:u:u;utu:u!U -!U:u!U;u,'U:u

FORM i VGA 1/87 Rev.1.00023

IEVOLATILE DR5ANICS ANALYSIS DATA SHEET


ERA SAMPLE

*? Name: VE^SAR INC. Contract:EAL75

.«: Code: VERSAF C«*e No. • 11724

r^-.rijc: <*oil/uater> UATER

Simple wt/voli 23. 0 Cg/mL)

Lt . e I : <low/metf> LOW

": Iciitur*: not dec. ___m

'::umn ipar k/c»p) PACK

•..Ti-tT TIC* found: _2

SAS No. : 4537E SDC No. : 724

Lab Sample ID: &974Q

Lab File ID: Y5327

Date Received: Q4/OS/99

Date Analyzed: 04/12/B9


CONCENTRATION UNITS<ug/L or ug/Kg)

CA= NUNBER

Z. 629-14-1

: COMPOUND NAME! UNKNOWNi ETHANE, 1, 2-DIETHOXY-t>

RT

2. 1312. 15

•iEST. CONC. ! Q

4 i J0. 8! J•i

r

FORM i VQA-TIC 1/B7 Rev.

100029

1AVOLATILE ORSANICS ANALYSIS DATA SHEET

EPA^SAMPLE

EAL76

e- M*m»: VEP.SAP INC

C a i *: VEPS-^?

Contract:

_ i .• 3.

_______ Cat* No. : 11724 SA5 No. : 4537E SDG No. : gAL74

(soil/water) WATER * Lab Samplt ID: 69741

wt/vol- 25.0 (g/mL> QL__ Lab Filt ID: Y5325

(low'mtd) LQU Data Rtctivtd: 04/05/89

__ Data Analyitdnot dac.

(pack/cap) PACK

04/12/89


CA5 N3. COMPOUNDCONCENTRATION UNITS:(ug/L or ug/Kg> UQ/L

74-S7-3————•———Ch loromtthant___________?4-83-s'—•————Bromomtthant _______75-01-4———————Vinyl Chloridt__________75-00-3—•—————Chlorotthant____________75-09-2———————Mtthy Itnt Chloridt_______67-64-1————————Ac 11 ont __________75-15-0———————Carbon Ditulfida________75-25-4———————1, 1-Dich lor oath tn*______75-35-3———————1. l-Dichlorotthant_______5AO-5°-G———————1. 2-Dich lor oath tn« (total)67-66-3————————Ch lor of or «______________•107-0&-2——————1- 2-Dichlorotthant______72-93-3————————2-Butancnt^„___________71-55-6—-————:—I, 1. l-Trichlorotthan»____5»-23-5———————Carbon Tttrachloride_____105-05-4———————Vinyl Acttatt___________75-27-4——•—•———•Brofiiodichloromtthane_______72-57-3———————i, 2-Dichloropropan«______IC061-C1-5—————cis-1'3/-Dichloroproptnt_

124-45-1—————Dibromochloromtthant^_____79-00-5———————1» l> 2-Trichlorotthant____71-43-2————————Btnztnt____m____________75-25-2——————•>—Brpmoform ___________10S-1C—1-——————4-Metriy 1-2-Ptntanone._____5? I -7S-o———————2-Ha x anont______________I £7-IS-*——————Tttrachlorotthtne______79-34-5———————1, l, 2. 2-Tttrachlorotthant_1 OS-83-3———————Toiutnt_____;__________10S-9C'-7——————Chlorobtnitnt__________100-41-4——————Ethyl btnztnt,____. ____100-42-5——•——————Sturrtn* ______________1230-20-7——————Total Xyltntt__________107-02—S—————ACT-O! *in ____________107-13-1——————-Aery 1 oni trilt___________

FORM I VOA

0000060. 2!U

0. 08 iUo. 09: u0. 3!U0. 11U

i:u!U

1!Ui :u3!U

0.10.0.0.0.0.0.0.0.0.0.0.0.20.0.0.0.0.0.0.73

1!U2!U1 !U2!U2;u1!U2!U3!U

!U4!2;ui:u1!Ui:u2!U2!U

!U

1/87 Rev.

1UOOGO

IEVOLATILE CEGANIC3 ANALYSIS DATA SHEET


EPA SAMPLE NO,

Name: VEFSAR INC

Code: V£g£AR Case No. : 11724

<«oil/uat«r> UIATER

wt/vol: 23 0 (g/mL>

<lou/mtd> LOW

not

1: lump ^pacV/c*p) PACK

. ni »T TICs found: ., _ C;

Contract:EAL76


Lab Samplt ID: A9741

Lab Filf ID: Y532S

Datt R*ctiv«d: O4/QS/B9

Datt Analyztd: O4/12/89



^-/ -S.Jrt

CA5 NUMEER " COMPOUND NAME RT EST. CONC. Q

cFORM i VOA-TIC 1/87 R»v.

1000Gi

I *: q i. •: q 1AVOLATILE ORSANICS ANALYSIS DATA SHEET

EPA SAMPLE

5& Nan.e: VEP5*R INC

'_sr Code: VESSAR

Contract:EALBO

Cas« No. :• 11724 SAS NO. : 4537E SDG No. : 724f-st.rit: (scil/uattr-) WATE*

Sine 1ft ut/vol: . 25. 0 (g/mL> ML

_**§!: Clow/mtd) LOW

** -*!5i»tur»: not dec. ____

•ipack/cap) PACK

Lab Samplt ID: 69742

Fil» ID: Y5344

c

Data Racaivad: Q4/Q5/B9

Data Analgztd: 04/13/89


CAS NO. COMPOUNDCONCENTRATION UNITS:(ufl/L or ug/Kg) UG/L

74-S7-2--——•———Ch laromathana________74-83-9——— -——EromQtnathana_ ___m75-01-4————————Vinyl Chloridt___________75-00-3——————Ch loroathana.-________75-09-2———————Methy lana Chlorida.______67-64^1———————Ac 9 ton*,________________75-15-0————————Carbon PHulfid*75-35-4———————1, I-Dichloro«thtn*^_____75-25-3——————— 1. 1 -D i c h 1 orq tthan*______540-99-0———————i. 2-Dichloroathant (total)67-66-3———————Ch i or of orm______________107-06-2——————1- 2-Dichlorotthant______7S-93-3————————2-But*non«______________71-55-6———————It I, 1-Trichlorotthan*____56-23-5———————Carbon Tetrachloridt_____1OS-C5-4————————V i ny 1 Ac a ta 11_____________75-27-4-—————Bromodich loromtthane_.___7S-S7-5———————l, 2-Dichloropropan«_____100&1-C1-5—————ci*-l. 3. -Dichloroprop ena^79-01-6———————Tr ich lorotthtne_________124-48-1——————Dibromochloromtthant^____79-00-5———————1, 1, 2-Trichlorofthan«____71-43-2-———————B • n z * na _^_____75-25-2————————Bromof orm__^___________103-10-1 ———————4-tta t h y 1 -2-Pan tan on a_____591-73-s———————2-Haxanona_____________127-1S-4———————Tetrachlorot than*________79-34-5———————1. I, 2< 2-Tatrachloro*thana_108-3S-3———————Toluana.________________1 OS-90-7———————Chiorobenztna___________100-41 -4———————Et h y 1 b an i ana___________1.00-42-5———————St^irsna _____________1330-20-7——————Total Xylana*___________107-02-8———————Ac r o 1 • i n_______________107-13-i———————Aery lonitrila___________

FORM I VOA

4IU2!U3iU2!U7

0000030. 2!U

0. 08iU0. 09 I U0. 3!U00.10.0.0.0.0.0.0.0.0.0.0.0.20.0.0.0.0.0.0.73

1 JU1!U;u

i:ul.iU3IU2!Ui:u21 Ui;u2tU2!U1!U2!U3!UIU

IIU•.1112

1/87 Rav.

100075.

IEVOLATILE ORCANICS ANALYSIS DATA SHEET


VEa5AR INC

:ci»- VE-5AR Case No. : 11754

>.: (foxl/uattr) WATER

a ut/vol: 25. 0 Cg/mL)

: (lou'/med) LOW

5 turt; not d»C. __

(pack/cap) PACK.

TICs found

ERA SAMPLE NO.

EAL80Contract:


Lab Sampl* ID: 69742

Lab Fil« ID: Y3344

Date Rtctivsd: 04/05/69

Dat* Analyzed: QA/13/89



C-5 N'JMDE^

•; 75-43-*

i

: COMPOUND NAME

i METHANE, DICHLOROFLUORO-t*

RT

6. 17

EST. CONC.

1

1

: Q; j

FORM I VOA-TIC 1/S7 R»v. i

100076


ERA SAMPLE t-

o Nc

: Cc

TT I 31

r..*le

•/ 9 1 :

*!e i 3

1 •„• T.r

**

ma- VPS SAP INC

de: VE*5iB

(soil '''uiatfi-r >

wt/vol:

( lou/mtd )

turt: not dt-c.

> : i p * c k / c a p )

CAS NG.

75-01-4 —————75-00-3 —————

67-64-1 ------75-15-0 ------75-35-4 —————

67-66-3 ------107—05—2- — —7S-93-3 —————

105-05-4 ————75-27-4 ——————7S-S7-S —————10061— Cl-3 ———79-01-6 ——————124-45-1 ————

71-43-2 ——————•? -£*-2— — —— —105-10-1 -----«.C< -7=-A—— —— —

EAL81Conti-act:

Case Nc. : 11724 SAS No. : 4537S SDC No. : 72*

WATER Lab SJ

25. 0 Cg/mL) ML Lab Fi

l pW Date F

mola ID: 69743

la ID: Y5341J

tcaivtd: 04/05/89

Dat» Analyzed: 04/13/89

PACjf. Dilution Factor: 5 0.

CONCENTRATION UNITS:COMPOUND Cug./L or ug/Kg ) UQ/L Q

—— r*.. loromcthant.^ —— Bramnfttathana,,—— Vinyl Chlorida—— Ch!oro»thant_——— Methul»n» Chlarid*—— Ac*tont , ,„„„.„„—— Carbon Diftulfid*——— 1 , i-nich lor o«th *n*—— 1. l-Dichloroath»n» . , .—— 1, 2-Dichlorotth»nt (total ) __—— Chlorof ormi-iBii—— 1, "-Dnchlorotthana . .—— r-=nt«non»—— 1. 1. l-Triehlo»*B*th*nP—— Cirhon Tatrachlorid*—— Uinyl Ac»tata_— — r-irr.mnd ich lorom»th*np—— 1, ?-Dichloropropan* .— • — c is — 1 * 3» — Dichloropr op »n» ____—— Tr ieh lorotthtna—— Di hreftiach lorom»th*n*—— l. l . Z-TriehlOTflathanB—— Banzant) ,,,,„„,„„——— Bramof orm,,, ___—— 4-M»fchi/l-2-Pant*non*— .-.2-He.xinona

1 JTT-1S-4 ———————— Tptrachloraathana79-34-5 —————10S-S3-3 —— —I OS-90-7 -----

100-42-5 —— —T S"r»-20— 7— — — —107-02-e — —107-13-1 -----

—— 1. i. 2' 2-*Tttrachlorotthan» ___—— T ° 1 u * n * - ._ -——— Chlorobtnitnt—— Fth^l btnztnt_——— StL;r*n*—— Total Xylana* __ im—— Acrol tin ,—— Aery lonitril*

i0. 4!U0. 2!U0. 3!U0. 2!U0. 6! -*2 ia">i0. 2iU

o. oe ;uo. 09 :u0. 3IU0. 1!U-0. IfUi :uo. i:uo. i:u0. 3!U0. 2!U0. 1!UO. 2!Uo. i :u0. 2!U0. 2!Uo. 1 :u0. 2!U0. 3!U2 iUo. i :u0. 2!U0. 2!0. 1 !U0. 1 !U0. 2!U0. 2tU7 :u3 ;u

!

#•«'*##

FORM I VDA 1/87 Rev.

JOOCDO


TENTATIVELY IDENTIFIED COMPOUNDSERA SAMPLE NO.

Z N*nit: VER5AR INC ContractEAL81

.si Code: VEffSAR Case No. : L1724

:i?r i x : (soil/water) WATER

a.T.cle ut/voi: 25 C <g/mL> MJ_

(10ui/m«d)

. net d*c

LOW

PACK


Lab Samp It ID: 69743

Lab Filt ID: YS345

Datt Rtctivtd: 04/05/89

Datt Analgztd. Q4/13/89


-fcundCONCENTRATION UNITS:<ug/L or ug/Kg) UG/L

i::•*;£ NUM3ES !

ir

COMPOUND<i

NAME ! RT

i

EST. CONC. Q


J00091

1AVOLATILE ORSAN1CS ANALYSIS DATA SHEET

EFA SAMPLE

z Name: VEP5AR INC

= : Cois: VEPSAP Ca«e No. ' 11754

'itr i x : < *oi 1/water.) UATEP

**ple ut/vol: . 25. 0 <g/mL>

.*.-* I: <lou/m«d) LOW

TOI*. tur«- not dec. ___

: 1 j mri. ( p «: k / cap ) PACK

Contract:EALS5

SAS NO. : 4537E SOG No. : 724

Lab' Sample ID: 69744

Lab File ID: Y5346


Date Analyzed: 04/13/S9


CA5 NO. COMPOUNDCONCENTRATION UNITS:Cug/L or ug/Kg) UQ/L

•>i-OT_T ———————————

/ 5— Qi— — —— ———75-OC-2 —————75-09-2 —————£7-64-1 —————75-15-0 ——————Te,_-?c_4___ .—«

^ • •* m f~ f

67-ftfe-3™ — —

7g-9^_2 —————

J6-S3— 3— —— -—« M ^^ ,V

7S-S7- "— — ——— —I W W / 4

I0061-01-S ——

124-4S-I— —— •

105-30-1 -----591-7S-6 ————127-15-4 ————

—— C M or ome thane---Eramome thane—— Vinyl Chlorid*—— Chloroethane , ,—— Methijlene Chlorid*—— Acetone— —Carbon Ditulfide—— 1, l-Dichloroeth»n* .,,.„.._, ,—— 1, i-Dichloroethan»—— 1» 2-Dichloroethene (total ) __—— Chloroform—— 1, 2-Dichloroethan*—— 2-Sutanone—— 1, l. l-Trichlero»th*n»—— C*T-hcn TetrachloriHp , .,— — Vinij 1 Acetate—— 2r3modichlorom«th*ne ,..,„, ,,,—— 1, 2-Dichloroorop«n»— — ci»-l * 3. -Dichloropropene ____— — Tr ich loroethene—— r. i bromochl or ome thane ,,_,.. .....,.„—— 1, 1, 2-Trichlot*o«thin» , „,. ,.„ ,— —Benzene—— Brcmof orm—— 4-M*th4l-2-Pentanon»— — 2-Hexanone—— T»trach loroethene

108-S3-3 ———————— Toluene.103-90-7 ————100-41-4 —— —100-42-5 ————1330-20-7 ———107-02-S ————107-11— i ————

—— Chlorobenitne—— Ethul benzene—— Stur»ne—— Total Xulene*—— Aerol ein _,—— AcT-y loni tri le

0. 4!U0. 2!U0. 3IU0. 2!U1 ! >r3 ^ ^0. 2!U

o. oe:u0. 09 ! U0. 3iU0. I !U-o. i ;ui :uo. i :u0. 1 IU0. 3!U0. 2IU0. I JU0. 2!U0. 1 !U0. 2!U0. 2!U0. i !U0. 2!U0. 3!U2 !U0. 1 iU0. 2!U0.6! —o, i :uo. i:uo. 2:uo, 2:u7 !U3 !U

1i

FORM i VOA 1/87 Rev.

100105

IEVOLATILE CRGANIC5 ANALYSIS DATA SHEET


EPA SAMPLE NO,

:.- Nam*: VEgSAR INC ContractEALB5

Cede: VgggAff Case No. : 11724 SA5 No. : 4537E. SDG No. : EAL74

ViTTix: (soil/water) UATER

=*T?lt wt/vol 25 0 (g/mL)

_ r - - * i - (low/mtd) L5U

** "^ciftur*: not d*c. __

::;ymr < p a c k / c * p > PACK

'..-t*^ TICi found: _ 0


Lab Fil* ID: Y534&

Datt R*ctiv»d: 04/OB/89

Date Analyitd: Q4/13/B9

Dilution Factor: S O


CAS NU^*3E^ COMPOUND NAME ; RT»

EST. CONC. Q

rFORM i VQA-TIC 1/87 Rtv.

J0010G

1AVOLATILE OR3ANICS ANALYSIS DATA SHEET

EPA SAMPLE

EC Na.it»: INC Contract:EALS6

Code: VEg5AP Case J 11724 SAS No. : 45375 5DS No. : 754

ix. <ioil/w«t*r> WATER

1» wt/vol- 25 0 < g / m L > QL._

:• (low/mad J LQUI


Lab Filt ID: Y5347

io 15 ture not dtc

(pack/cap) PACK




CAS NO. COMPOUNDCONCENTRATION UNITS:Cug/L or ug/Kg) UO/L

74-07-3 ——— — —— Ch lor omethane74-E2-c — •—— • — --Bramomethane75-01-4 ————————— Vin4l Chlorid*7*;-no-~ ————————— Chloroethane^7*-Q9-£ ———————— M*thylene Chlorid* ,,, „„67- 4-1 ——————— Acetone _ ..„..„.,7S-15-G ——————— Carbon Disulfide75-33-4 ———————— 1, l-Dichloroeth»n» , . . ,75-25-3 ———————— 1, l-Dichloroethan* ,„„ „,_..,540-59-0 ——————— 1, 2-Dichloroethene (total) __£7-Ai-2 ————————— ChloroformiS7-fii-2 —————— I, 2-Dichloroethans , ,.78-93-2 —— — • ——— 2-Butanone71-S«»-<=, ————————— 1- I, l-Trichloro«thane5£-23-5 ———————— Carbon Tetrachlar id*!£C!-rj?-4 ———————— Uiniyl Acetate"?— 2T-4 ————————— 5romodichlcrom»than*7C-S7-' ————— —— 1 , 2-Dich Iflrap-popan*.iOOtl-Cl-5 ————— c i»-l * 3. -Dichloropropene ____7=-ri i — ————————— Tr i c h 1 or oe t h en •U4-49-1 ——————— -.T-ibromochloromBthan*7e-nr,-« ————————— i. 1, P-Triehlora.th.n..? l -4^-2 ———————— Bfir,?*ne _„._„ _ im7*- TE-r ————— —— »ramof arm _,_,„,_,^r.^-i •"— 1 ———————— 4-f-!*tny l-2-P*nt*non* . __«,? i --»c-= ——————— 2-H* i an one127-is-i ——————— Tetr*chloroeth»n» -79-34-5 ——————— 1, 3/2. 2-Tetrachloroethane ___lG!P-S5-3 ———————— Tolu*neto-a-Q--— 7 ——————— Ch 1 or o benzene • ,in^-41-4 ———————— FtKyibenren* , ,. ,1 DC— 42- 5 ———————— S t u r • n e n _ _„ ., _._„1230-30-7 —————— Tctal Xulene*i G7-CS-S ——————— Aero 1 e in1 07- 1 3- 1 ——————— ACT- ylonitrile

r

0. 4!U0. 2.'U0.3!U0, 2!U0. 5ifi<>t3 J -0. 2!U

0. 08 IU0. 09 !U0. 3IUo. i :u-o. i :ui :uo. i;uo. i;u0. 3!U0. 2!U0. l.'U0. 2!U0. liU0. 2IU0. 2!U0. 1 !U0. 2IU0. 3!U2 :u0. l.'Uo. 2:u1 1 ' ;'o. i ;uo, i :uo. E:U0.2JU7 :u3 :ui

FORM I VOA 1/S7 Rev.

J00120

IEVOLATILE ORSANICS ANALYSIS DATA SHEET


ERA SAMPLE NO.

b Name: VERSAR INC

.: Code: Vg^SAR Case No. : 11724

tri x: < soil /water.) UATER

n pl» wt/vol 25. 0 ( g/mD ML

Contract: ____.

SAS No. : 4337E

EALB6

_______ 5DG No. : EAL74


Y5347

tl: <lGW/med> LDU1

Mcitturt: not d*c.

(pack/cap) PACK

Lab Fil* ID: ______

Date Rtctiv«d: 04/05/89

Datt Analyzed: O4/13/S9


.,->. e r T ] C » foundCONCENTRATION UNITS:< u g / L or ug/Kfl) UQ/L

CAS NUMBER ! COMPOUND NAME ! RT !

i i i

EST. CONC. Q

rFORM I VOA-TIC 1/87 Rtv.

J00121


ERA SAMPLE

\z N*mt:

_ ? i -DCS

INC. Contract:EAL94

Case No 11724 SA5 No. : 4337E SDG No. : 724

r"£ tr i x : doil/uattr) WATER

= = .T,pie u t / vo l : 25. 0 < g / m L >

L r x f i l : ( l ow /mtd ) LOW

', *?c ittu^*: not d *c . ___

". i-lumn: ( p a c k / c a p ) PACK '


Lab Fil* ID: Y534B

Datt Rtctived: Q4/O3/89



CA5 NO. COMPOUNDCONCENTRATION UNITS:(ug/L or ug/Kg) UG/L Q

1

74-87-3 —————————74-e3-9 ——————— > ——"? 5 -O 1-4 — — • —————75-00-2 —————————75-09-2 —————————t7-64-I —————————75-15-0 —————————75-35-4 —————————

54!"1— 5*— H— —— —— ———W ^ '— ' w • *•

67-66-3 ————————

7g-o-?-T — ^ ———— . —•* i _^*,_i-._— ..___.._«-,o-r^-* — „ ———— ———1 OS-05-4 ————————75-57-A —————————7S-87-5 —————————1 OOfe 1 -C 1- 5 —————79-01-6 —————— r ———

79-00-5 —————————71-43-2 —————————75-25-2 ————————

\-!S— 1 v— i,—— ——— — — —591-73-fc ———————127-12-4 ————————

103-S3-3 ———————1 OS-90-7 ———————1 0^-4 1-4 ———————100-42-5 ———————1330-20-7 ——————i07-or-e —————10"-13-1 ———————

rh 1 aT»om«th«n«Br Q m o m t t h a n a _ ___V i n y l C h l o r i d *Ch ! oT-o«than«M » t h y l « n a Ch lo r id* .,.,_. .... ,Ac*tont , . .C*rhen D i « u l f i d »1 , i -D ich lo roa th»n« , .. , ,,,1, l -Dich loro«than* . .,„...„_„,.„1. 2-Dichloro»thtnt ( to ta l > __C h l o T - o f a rml, ?-Dich lor o» than* . . _7-Rnftanon*1 , 1 . 1-Trichlorn»th*n»Carbon Tetrachlor idsV i n i r f l Ac»tat»Pcp.«mnd i c h lorom»%h«n* _ , „ , . , ,1 , 2-Dich loropropan* „ „. , ,„,c i f-1* 3. -Dich lo roprop tnt ____Tr irh 1 or o»th an* _„„. ,. , , ,n< h ^ n m o c h lor om« than* _ i n _1 . •« . 5-Triehloro»th«n» .__, _.B*n;«n*Bromof orfll iM_ i mii-M.thy l-2-P»nfe*non« HI IMI I ,.5-w*if»nQna i ini ,T» t rachloro«th»n* _, . ,,,_..,.,„.,I/ 1> 2f 2-Tttrachlorot thant ___Tnl i t«n«C h ! n r o b « n z » n «F ^ h y l b » n z » n *Sti;r*na-i._._iTotal X u l t n t sA e T ' o i » i nA c T - 4 I o n i t r il« _

ii0. 4!U0. 2!U0. 3!U0. 2!U^0. 6J^-*T2 itfji0. 2 ! U .

0. 08 !U0. 09!U

0. 3 J Uo. i :u-~0. 1!Ui :u0. 1 !U0. IIU0. 3,'Uo. stuo. i ;u0. 2!Uo. i:u0. 2!U0. 2!Uo. i;uo. 2:u0. 3JU2 iU0. UU0. 2IU0. 11U0. I IU0. I IU0. 2!U0. 2!U7 :u3 :u

1

FORM i VOA 1/87 Rtv.

300135



EPA SAMPLE NO.

.b Name: v"E=SAR INC

"_ s :• C s c s:

Contract:EAL94

Case No. : 11724

"!*tr i x : (toil/wa tar) WATER

Simple ut/vol: 25 L 0 (g/mD QL,__

:.vvsl: (low/mtd) LOW

", "^oiftuT*: not dec. ^ ^

'.rlwian (pack/cap) PACK

"M-.-.t*r- TIC§ found 1 _^

SAS No. : 4537E SD5 No. : EAL74

Lab Samplt ID: fe9?4A

Lab Filt ID: Y5349

Datt Received: 04/05/99

Date Analgzed: 04/13/89

Dilution Factor: 5 0____


•^ * i h'- Jf^W^E'. ^ rH\yrii3t COMPOUND NAME•

RT EST. CONC. Q


300136

i \i ;. Z'if£i'V:iHu) f.JWi&

1AVOLATILE ORSANIC3 ANALYSIS DATA SHEET

ERA SAMPLE t

Na-ne VEPSAR INC Contract:EAL95

rode: VE=SAP Case No. : 11724 SAS No. : 4537E

i x : (toil/water-) UATEE ,

le wt/vol: . 25. 0 (g/mL) ML

1: (low/med) LDUI

ifture: net dec.

SD5 No. : 724


Lab File ID: Y5370

Date Received:

•Tin; (pack/cap) PACK

GAS N3. COMPOUND

04/05/89

Date Analgztd: O4/14/99

Dilution Factor: 25QQ


7--ST-2——————•—Ch loremethane________7--52-5———————Ersmom«thane_____________7 5- D; -4- -——————v i n y 1 C h 1 or i d t__________75-OC—3—————-——Ch 1 oroathant__ ____^_75-09-2———————n«tny Itnt Chloride______* 7-64-1———————Acetont________________7S-15-0———————Carbon Diiulfid«________7«-35—*———————1. l-Dichloro«th«nt__^^_7?-3«-3———————1, 1-Dichlorotthan*______540-39-C————•——1* 2-Dichlorotth«n* (total)*7-ie-3—————•——Ch larof orm ________lCv-Cfc-2————-:-:, 2-Dichlorotthan*______7£-93-3———————:-£-gutanona __________71-55-6———————1. I. l-Trichloro*than*____5i-23-;———————Carbon Tttrachloride_____105-09-4———————Vinyl Actt«t«______^____75-27-4———————Bromodichloromethane,____7S-S7-3————————1. -DicMorQflyonAnslOOil-Cl-5—;- —— c i*-l»3»-Dichloroprop «n«__75-03-*————————Trich loroathan*i £4-4S-i——————Dibromochloromtthane^____79-OO-5———————li I, 2-Trichloro«than»____71-47-2———————Eeniena.^^.____________75-25-1————————Bromef orm ___________103-13-1——————4-n«thgl-2-Ptntanori»_____5^1-78-6———————2-Hexanont______________127-1S-4———————Tttrachlorotthtnt________79-34-5———————I/ 1* 2' 2-Tttr«chlorotthan*_ioe-ee-3————Toiu*n«_____________103-90-7———————Chlorobenztnt___________: 00-41 -4———————Et h g 1 b en z tnt___________100-42-5———————Styr«n*_________________133D-20-7——————Total Xyltn«s_ii_________1C7-C2-8————•——Ac r o 1 * i n _______________107-13-1 —————Ac r y 1 on i tr i 1 •

FORM 1 VOA

190110130962201300120404413090616906900

55170957087

1700079110360100140

110017000

11O34000

622000110740033001400

:uiu:uU

:uiuJU!U!U!U!U*i;u:u:u:u:u:u!Uiiiu!U:uii!UI

:ui*:uii!U:u

100147l/B? Rtv.

. -'OP. JJj-.

LEVOLATILE ORGANICS ANALYSIS DATA SHEET


EPA SAMPLE NO.

5 Name: VERSAR INC. Contract:EAL95

C o d e : VEPSAP Case No.

rim (soi l /uat»r) UIATER

ip lc wt /vo l : . 25. 0 Cg/mU flL.__

•e l : ( law/f f l t (J) LOUI

loistur*: not d»c. ___

umn ( p a c k / c a p ) PACK

i-rs1- TICs found: _^

11724 SAS NO. : 4537E SDG No. : EAL74


Lab Filt ID: Y327Q

Date Rtctivtd: Q4/QB/89

Date Analgzed: Q4/14/89

Dilution Factor: 23QQ


1 11 1

A5 NUMBEP ! COMPOUND NAME ! RT

t i< i

EST. CONC. a

fFORM I VOA-TIC 1/87 R»v.

J 001 4 3

-:.:2q 1AVOLATILE DRGANICS ANALYSIS DATA SHEET

ERA SAMPLE

- Name: I'ESSAR INCt;

Contract :EDG01

r

: V£?SAR Case No. : 11724 SAS No. : 4337E SDG No. : EAL74

sTTix: (aoil/wattr) UIATER Lab Samplt ID: 69729

TT,?:» wt/vol: . 23 Q <g/mL> QL,_ Lab Fil* ID: Y53O7

f--*l: (lou'ncd) LOW Date Received: 04/05/69

^sis-cure: not ds-c.

(pact'./cap) PACK

Datt Analg:*d. 04/12/89

Dilution Factor: 5. O

CAS NO. COMPOUNDCONCENTRATION UNITS:(ug/L or ug/Kg> UG/L

74-37-3-—•——•——Ch loromtthant__________74-S2-9—-———- Brcmomtth«n«——__________73-01-4———————Vinyl Chloridt__________75-OO-2———————Chlorotthant___________75-09-2———-——— Mtthg lent Chloridt______«67-64-1———————Acttont________________73-35-O———————Carbon Di«ul*idt________75-33-4———————i, l-Dichlorotthtnt_______75-33-3———————1. l-Dichlorotth«ne_-_____540-59-0———————3* 2-Dichlorotthtnt < total)t7-&s-3-——————Ch 1 orof orffi _________lC~-Oc-2——————1, 2-Dichlorotth«ne_______7S-93-3—— ———2-gutanont________71-31—c——-——-—— 1. 1< 1-Trichlorotthane____Ss-23-3———————Car b on Tttrac h I or i d t_____3 C 5-03-4———————Vinyl Acttatt___________75-27-4———————Brc.mcdichloromtthane_____7S-S7-3———————1> Z-Dichloroprop*ne______lCr = :-Cl-3—————-cis-1 • 3--Dichloroprop *nt__7P-Q:-a———————Tr ich lorotthtnt_________i2^-4S-i——————rMfcrQfliOChloromtthantv?c-£C—3———————1. l, 2-Trichlorotthant____71-43-Z—————————B«nz»nt _____________75-23-2-——-———'Bramef crm ________iC-B-ir—1———————4-M*thg l-2-Ptntanont_____5=l-7S-fc——————2-r*txanon«______________:rT-is-4——————Tetrachlorotthtn*._______7 -34-: ———————— 1, 1, 2/ 2-Tttrachlorotthant_105-65-3————"——Toluant ______»___1CS-90-7——————Chlor ob*ni*nt_________^100-41-4——————Ethyl btnztnt____________iOO-42-5———————Styrent_________________1330-20-7——————Total Xyltnt*___________107-02-S——————:Acr o 1 tin_______________1C"?-13-1———————Acrylonitrilt___________

0000. 20. 420. 2

0. OB0. 090. 30. 10. 1

uuuu^ruuuuuuuu

0.00.0.0.0.o.0.0.0.0.0.20.0.0.0.0.o.0.73

i ;u3!U2!Ui ;u2:ui :u2!U2!Ui :u2!U31U!U

2!U1!Ui :ui;u2!U2!U!UiU

FORM I VOA 1/E7 Rev.

100183



ERA SAMPLE NO.

EDGC1b Nafne: VEP5AR INC

. :• C o d e :

Contract:

Cast No. ' 11724

stris; (fcoii/water) WATER

*mpl* wt/vol: . 25 0 <fl/mL> Ml^

*.-*i: (lou/mtd) LDU

*!oi ttur*: not d*c. ___

:>lumn t pack /cap ) PACK

.-•Tp»r TICs found: __C;



Lab Filt ID: Y33Q7

Dat» Ractivtd: 04/05/89

Datt A n a l g i t d : O4/12/S9

Dilution Factor: 5 Q____


ii•:AS NUMBER : COMPOUND NAME RT EST. CONC. Q


100184

CI q C 2 q. 1AVOLATILE ORGAN1CS ANALYSIS DATA SHEET

EPA SAMPLE

t Nfifr,«: VE=£AR INC Contract:EDG02

; Cod*: VEffSAR Case NO. : 11724 SAS No. : 4537£

-r:x: <ioil/uat»r-> UATES

-DI» wt/vol: . 2?, 0 (g/mL) Mi.

v*l: (!oui/fn»rt) LOW

f^c it turt: not d»c. ___

SDG No. : 724

Lab Sampl* ID: 6.9730

Lab Fil* ID: Y33QB

li. mn; (pack/cap) PACK

CAS NO. COMPOUND

Date R*C»iyfrt: Q4./03/S9

Dat* Analyzed: 04/12/89


CONCENTRATION UNITS:(ug/L or ug/Kfl) UO/L

74-37-3—-—————Chlor om*than*____„___.74-33-°———————Brcmom*than*_Bi___________75-01-4————————Vinyl Chloridt___________75-00-3—-—•———Chloro*than« _____75-09-2——————tltthy l*n* Chloride. ___,67-64-1———-———Acston* ________m75-15-0———————Car-bon Difulfid*________75-35-4———————1, l-Dichlorotth*n«_______75-35-3———————1* l-Dichloro*th«n*_______540-5^-0———————1, 2-Dichloro*th*n* (total)o7-&6-3——————"™Ch loroform _____107-Of.-2—— -———1> 2-Dichloro*than*_______79-93-3—————-•"--2-Sutanon* ____71-55-c———————1. 1* l-Trichloro*than«____56-23-5———————Car-bon T*trachlorid*_____1 OS-05-4———————Vinyl Act tat*___________75-27-4———————Sromodicbloromtfthan*._____73-57-5———————1, 2-Dichloropropan*._____10O61-C1-5—————ci*-l.3.-Dichlaropropgn*79-01-6-———-—-Trich loro*th*n* _______124-4S-1——————Dibromochloromtthan*^____79-00-5———————1> I. 2-Trichloro*than*____71-43-2————•--—E»ni*n* _______75-25-2———————Bromof orm^______m_______106-10-1———————4-P!*thyl-2-P*ntanon«_____5s? i -75-6————•—2-H* x anon*127-1S-4——————T*tr»chloro*th*n*_______7^-34-5———————1, 5, 2/ 2-T*trachloro*than*_103-SS-2———————Tolu*n*__________________1 OS-90-7—-—————Ch 1 or ob*nz*n*100-41-4———————Ethyl btnzen*,.____________100-42-5———————Stsir*n*_________________1230-20-7——————Total Xyltntt___________107-02-8———————Ac r o 1 * in________________107-13-1——————Acrylonitri 1*___________.

FORM I VOA

4!U2iU3!U2!U2; j

O. 20. 080. 090. 3001

!U: u:u!U

1 iUi :u:u

0.0.0.0.0.o.0.0.0.0.0.0.20.0.0.0.0.0.0.73

i ;u1 !U3!U2:ui :u2!Ui:u2!U2!U1IU2:u3:u;u

2!2!UliU

2!U2!U!U

1/87 Rev.00193

'T <Vi\s £



ERA SAMPLE NO.

EDGO;5 Name: VERSAR INC. Contract:

-5: C o C e - VEP5AR

x:

Case No. : 11724

UIATER

ut/vol: . 25. Q <g/mL)

(low/mtd) LOW

: not d*c. ___

SAS NO, : 4537E SDG No. : EAL74

Lab Samp It ID: A973Q

Lab Fil« ID: Y53Q8

Irlumn (pack/cap) PACK

TICt found;

Dat* Rtctivtd: 04/OJ/89


Dilution Factor: 5. o___

CONCENTRATION UNITS:(ug/L or u g / K g > UQ/L

"AS NUnBER ! COMPOUND NAME RT EST. CONC. Q

cFORM i VOA-TIC 1/87 R*v.

100199

; - -vio i, --vii


EP.A SAMPLE

£& Warns: VE3SAR INC ContractEDG03

Code: VE^SAS Case No. : 11724 SAS No. : 4537E. SD5 No. : 724

<EO 'wat*r> UATER Lab Sampli ID: 69731

1 v wt/vol: (g/mL)

(lou/mad) LOW

Lab Fil* ID:

Data Rac*iv*d

Y5309

04/05/S9

•o i jtur *: no dr-c

(pack/cap) PACK

Dat* Analy:*d: Q4/ 12/89



74-37-3——--.————Chlor omtthant ________74-83-9———•———Brc-fnom*than*_ ...___'75-01-4———————Vinyl Chlorid*_________75-00-3———————Ch 1 oro*than*________ .75-09-2———————M*thyItn* Chlor id*_______67-64-1———————Acttont________________75-15-0———————Carbon Disulfidt________.75-35-4———————1, l-Dichlorotth«n*_______75-35-3———————1* l-Dichloro«th«n«_______540-59-0———————I, r-Dichloro*th*n* (total)£.7-66-3-————•——Chlor of orm _____—__107-06-2———————1» 2-Dichlorotthan* ____75-93-3——-—————2-Sutanont,______________71-55-6———————1* 1. 1-Trichlorotthan*____56-23-5———————Car-bon Tttrachloride_____1 OS-05-*——————-Vir.y 1 Acetata ________75-27-4———•————Br omodich lor om« than*_____78-37-5———————1. 2-Dichloropropan*______10061-01-?—————ci*-l> 3* -Dlchloroprop*n*_79-O1-6———————Trichloro*th*n*_________124-4S-1——————Dibromochlorom*than*____79-00-5———————If 1. 2-Trichloro*than*____7: -43-1———————B*n ;»n* ____________75-25-S————————Qromoform_______________•_105-1C— 1 ——————4-M* t h y 1 -2-P *n t an o n •_____59i-7S-b——————2-H*xanont_____________127-18-4———————Tttrachlorotth«n*_______79-34-5———————1» 1, 2> 2-T*trachloro*than«_10S-SS-3———————Tolu*n*________________1CS-9C—7———————Chlorob*nztn*___________10O-41-4———————Etr.ulb*ni*nt^ ________,100-42-5———————Styr*n*________________1330-20-7——————Total Xyl*n*«___________107-C2-S———————Aero 1* in________________107-13-1———————Acrylonitril*___________

4!U2!U31Uu

00000. 2!U3 !•*0. 2!U

0. 08 i U0. 09 !UO. 3IUo, i:u

uu

0.10.0.0.0.0.O.0.0.0.0.0.0.20.0.0.0.0.0.0.73

!U!U:u:u!U!U:utulu:u!U!U

i:u2iU21 --i;ui ;u2!U2!U!UIU

FORM I VOA 1/87 R*v.


ERA SAMPLE NO.

: Mam*: VEP5AR INC.

; Coda: VERSAR Case No. : 11724

Trix: (soil/uatsr) "WATER

fi.plt wt/vol: . 25 0 (g/mU)

•»!: Clow/mtd) LOW

r,c-istur»: not d*c. ^____

lumn '. pack /cap ) PACK _

Contract:EDG03

SAS No. : 4537E SDS No. : EAL74


Lab Filt ID: YS3O9

Datt Rtc«iv*d: 04/05/89

Dat« Analgztd: O4/12/S9


TIC* found: __ C;CONCENTRATION UNITS:(ug/L or ug/Kg) UQ/L

CAE NUrtEES

\ i> i1 COMPOUND NAME \ RT

> tt >

EST. CONC. Q

r~

FORM I VOA-TIC 1/87 R*v.

. -r -«.V-Sw».ij~; •,>_'£• A-l-Ui Jj £• * _ji_-»r«. ;-- i'?Oc=.Uii.1-.iiK


EPA SAMPLE

b Name; VER5AP INC. Contract:

LS= Code: VgPSAP Case No. : 11724 SAS No. : 4537E SDG No, : 724

-^ix: (toil/water) WATER

.Tiple ut/vol: 25. 0 <3/mL> QL __

-vel : ( low/mtd ) LOW

."icifture: not __ _

lumn: t pack /cap ) PACK


Lab File ID: Y3310

Data Rtctivtd: 04/03/99

Date Analyzed: O4/12/89



74-37.3—.————ch loromethane74-S2-?——-———— Bromomathant_ _______^_73-01-*———————Vinyl Chloridt__________75-OO-3————————Chloroethant^____________75-09-2—— -————Methylene Chloride_______67-64-1———————Acetone_______________73-15-0———————Carbon Di»ulfide________75-35-4———————1, 1-Dichlorotthene______75-35-3———————l, I-Dichloroethane_______540-59-0——————1. 2-Dichloroethene (total)67-66-3———————Chloroform!07-0=s-2——————1* 2-Dichloroeth*ne_______7S-73-3———————2-Eutanone______________71-55-6———————I, 1, 1-Trichloroethane____56-23-3———————Carbon Tetrachloride_____10S-03-A——————Vingl Acetate___________75-27-4-—-——-—Bromod ichlorom*than*7S-S7-3———————1. 2-Dichloropropane______10061-01-3—————ci*-l» 3. -Dichloropropene_79-01-6———————Tr ichloroethene_________124-43-1———————Dibromochloromethane_____79-00-3——————1, i, 2-Trichloroethane____71 -43-2———————Ben 2 e n e____„___________75-25-2———————Bromo-Porm ___;_______1 OS-10-1——————4-Methgl-2-Pentanone_____591-7S-6———————2-Hexanone______________127-13-4——————Tetrachloroethtne_______79-34-3———————li 1, 2- 2-Tetrachloroethane_IOB-3S-3——————Toluene________________108-90-7——— ——Ch 1 or o b e n z ene _______100-41-4———————Ethyl benzene____________100-42-3——————Styrene____________'1330-20-7——————Total Xylenes___________107-02-S———————Aero le in________________107-13-1———————Acrylonitrile___________

42322

0000038 !-0. 2!U

0. OSiUo. o?: u0. 30. 10. 110.0.0.0.00.0.0.0.0.0.0.20.0.0.0.0.0.0.73

uu-uuuuuuuuuuuuuuuuuuuuuuuu

FORM I VOA 1/87 Rev.

00224



-.5 Namt: VER5AR INC Contract

EPA SAMPLE NO.

EDC04

s: Code: VERSAR Cast No. : 11724

.»trix: (*oil/uat«r> MATEP

ample wt/vol: 25 0 <g/mL>

*v*l: Uou/fllfttf) LDUJ

^ciitur*: net d*c. ____

:• luff.n < pack/cap) PACK

jffiD tr TICi found: 1



Lab Filt ID: Y331O

Datt Rtctivtd: Q4/Q5/89

Datt Analyztd: O4/12/99



CAS NUMBER«

COMPOUND NAME i RT

UNKNOWN i 12. 12r

EST. CONC.

2

rr

: G: »*»«! Jit


- r r» 9 9 R• , * *-• ». *

1AVOLATILE OPGAN1CS ANALYSIS DATA SHEET

EPA SAMPLE

EDG3J3 Name: VERSAR INC Contract:

'!«: Code: VERSAR Case No. : 11724 SAS NO. : 4S37E SDG No. : 724

(soil/water) WATER Lab Sample ID: 69733

= *T.5le wt/vol: . 25- 0 (g/mL).

Ltvsl: (low/mtd) LOW

\ roisture: not dec. ___

Irlumn: (pack/cap) PACK

Lab File ID: Y3311




CAS NO. COMPOUNDCONCENTRATION UNITS:(ug/L or ug/Kg> UO/L

74-37-3———-—•——Chloromethane___________74-S3-9———————Sromomethane__________.75-01-4——-r————Vinyl Chloride__________75-00-3———————Ch loroethane____________75-09-2——-————Methylene Chloride_______67-64-i———————Acetone_______________75-15-0———————Carbon Di»ulfide________75-35-4———————i. i-Dichlorotthene______75-3P-3———————I, l-Dichloro«thane_______540" 59-0——————I, 2-Dichloroethene (total)67-66-3———————Chloroforffl_„___________107-06-2———— —— 1* 2-Dich lor of thane______7S-93-3——————-—5-3utanone ____71-55-6———————1. 1* 1-Tr ichloroethane____Sa-22-5———————Carbon Tetrichloride,_____105-05—4———————Vinyl Acetate___________75-27-4————•——Eromodichloromethane_____.7S-S7-3——•——•—-If 2-Dichloropropane_.____10061—01-3—————ci» —1*.3» -Dichloropropene—_79-01-6———————Trich loroethene_________124-4S-1———•——Dibroraochloromtthane____79-00-5———————1» I* 2-Trichloroethane____71-4 3-2————————B • n i e n e.________________75-25-2————————Bromoform_______________105-10-1———————4-rtethyl-2-Pentanone_____591 -73-6——————2-He x an one,_____________127-1S-4——————Tetrach loroethene_______79-34-5———————1, 1. 2^ 2-Tetrachloroethane_103-82-3——————Toluefie_______________105-90-7——————Ch 1 or ob en i ene__________100-41 -4 ——————E t r. y 1 b en z ene____________100-42-5———————Sturene ___________1330-20-7—————Total Xylenet__________lC~-02-a———————Acrol e in_______________: 07-13-1——-———Aery 1 onitrile.______.____

0. 40. 210. 20. 330. 20.080.0930. 10. 110. I0. 10. 30. 20. 10. 20. 10. 20. 20. 10. 20. 320. 10. 20. I0. i0. 10. 20 2

!U:ut•;u

;u:u:uiiJUJU;u:u;u:u:u:u:u:u:u;uJUJUJU!UIU;uJU!U:u:u,'U:u:u


JO0236

IE EPA SAMPLE NO.VOLATILE ORCANICS ANALYSIS DATA SHEET ______________


so Nam*: VERSAR INC._____________ Contract:V..-

EDQ3I

-*? Coc?: VERSAR Cast No. : 11724 SAS NO. : 4537E SDG No. : EAL74

r:r: Csoil/uat*r) MATEP. Lab Sampl* ID: 69733

as.-nplc ut/vol: 25 Q (g/mL> OL Lab Fil» ID: Y5311

.Svgl: (lou/mtd) LOW Datt Rtctivtd: Q4./OS/89

:» ^icistur*; not d»c. ___ Datt Analyztd: Q4/15/S9

Cclwmn (pack/cap) PACK Dilution Factor: 3. Q____

CONCENTRATION UNITS:7' TIC* found: _C; (ug/L or ug/Kg) UO/L

CASii

NUrlBEP i COMPOUND NAME I RT EST. CONC. Q

FORM i VOA-TIC 1/97 R*V.

J00237


Contract:

ERA SAMPLE

EDG33:. Name: VERSAR INC._____________.

'».*;. Cobs: VE?SAR Case No. : 1 1724 SAS No. : 4S37E SDC No. : 724

"£*;-:x: (scil/watsr) WATER

i?le wt/vol: . 25 0 Cg/mL> Q^__

•*1: <low/mefl? LOW

!oi »tyr»: not d*c. ___.

yT.r.: i pack/cap) PACK


Lab File ID: Y5312

Datt Received 04/03/89

Datt Analyzed: O4/12/S9

Dilution Factor: 13O____


r

74-57-2—————•——Chlor o m e t h a n e _ _ _ _ _ _ _74-53-*—-——-——Sromomtthang .. ____^__75-01-4———————Vinyl Chloridt_________75-00-5———————Chloroathant^.___________~ 5-09-2———————Mt t h y 11n a Ch 1 or i d t_______67-64-1————————Acttona ____________75-15-0———-————Carbon Di»ul*ida________75-35-4———————1, i-Dichlorotthtnt_______75-35-3———————1, l-Dichlorofth«n«_______540-5^-0——————1* S-Dichlorotthtnt (total)67-6e-3————————Chloroform ____107-06-2——————I* 2-Dichloro«than»______70-93-3—————————g-5utanona ___________71-55-? ———————1> l* l-Trichlofotthant____56-23-5———————Carbon Tttrachloridt_____10S-0:-4————————Vinyl Actt»t»_____________75-27-4———————Sromcd ichloromtthant^_____73-37-5———————1> 2-Dichloropropan*______10061-01-5—————cit-1 / 3' -Dichloropropen•_79-01-=———————Trichlorotthtna_________124-45-1——————Difcromochloromtthana^____79-00-5———————1. li 2-Trichlorotthan»____7 2 - 43-2—————————Ban 2 *n» ______________75-2S—L—————————Grams form ___________1 OS-1 C— 1 ——————4-Hff t h y 1 -2-P tn tan on • _____5? i -73-6——————2-Ha x an on»^__________•l2"I'-lS-4——————Tetrachlorotthtne_______79-34-5———————l. 1* 2' 2-Tatr«chloroethan«_1CS-SS-3——————Toluana________________1 OS-90-7——————Ch lorobtiir »na______.___100-41-4——————Etfiylbanrana._________100-42-5———————S t y r e na ____________1330-20-7——————Total Xyltnai______;_____: 07-C2-S———————AC r o 1 f i n_______________107-12-1———————Ac r i^lonitril •___________

10565650621916033353395445B463575717633355

16O

FORtl I VOA

;u;u:u:u:uiu -!U!U

iU:u!U:u!U:u!U1U;ui!U:u!U!U!U:ut<iUiUiUiUtu1U!U:u

1/87 Rav.

100254

IEVOLATILE ORQA?4ICS ANALYSIS DATA SHEET

TENTATIVELY IDENTIFIED COMPOUNDSN*m«: VE3SAR INC

Case No.

UATER

11724LSI Cod*: V_ER5AR

£*ir.pla ut/vol: 25. Q (g/fflL)

L*v«l: (low/mad) LQUI

"; M o i s t u r a : not dtc. ___

(pack/cap) PACK

TICs found: _£

EPA SAflPLE NO.

EDG33Contract:

SAS NO. : 4B37E SDG No. : EAL74

Lab Samp la ID: 69734

Lab Fila ID: Y5312

Data Racaivad: 04/05/89

Data Analyzad: 04/12/89

Dilution Factor: 130____


r

CAS NUMBER ! COMPOUND NAME RT ! EST. CONC.

i

Q

FORM I VOA-TICJ00255

1/87 Rtv.

£fe£gf':--j.£_ .V'.gta,; L ;a8: %tiiftY»'"irii5iii& ^

1AVOLATILE ORCANICS ANALYSIS DATA SHEET

EPA SAMPLE

(*-:- .Name: VESSAR INC.

r

Cede: VE3SAP . Case No. : 11724

ix: i *oil/wat*r ) WATER

le wt/vol; - 25 0 <g/mL>

i; (low/mid) LOW

isti.tr*;

Contract: ..

SAS No. : 4537E

EDG36

SDC No. : 724

Y5322

(pack /cap) PACK

Lab Sample ID:' 69735

Lab File ID:


Date Analyzed: O4/12/B9

Dilution Factor: 2SO___

CAS NS. COMPOUNDCONCENTRATION UNITS:(ug/L or ug/Kg) UG/L

- _ — — — — „ — — — o r _______74-83-?™———•—Eromom«thant . _________75-01-^———————Vir.yl Chlorid*__________75-00-3———————Cnl or ot thane.^__________7S-09-2———————M«thyltnt Chloride_______67-64-1———•—•——Acetone _______75-15-0———————Carbon Disulfide________75-35-4———————1, l-Dichloro»thtne_______75-35-3———————1, 1-Dich lor ot thane_______640-59-0——————1, 2-Dichlorotthene (total)67-66-3———————CM orof orm ____•lC7-Oc-2——————lt 2-Dichlorotthane_______7S-73-3———————2-Sut«non*_____________71-55-6———————1, i, I-Trichloro«thanr____it-22-3——————Cartsor. Tttr*chUrldt____1CS-05-4———————Vinyl Acetate^__________75-27-4-——-———»-Bromodieft 1oromethane75-87-5———————it 2-Dichloropropane______10O6I-01-5——•——c i » —1« 3* —Dich lor opr op ene ___79-01-6———————Trichloroathene_________124-4S-1-:—————Dibromochloromathane_____79-00-5—— -————i, I, 2-Trichloroethane"____71-43-2———""—Banian* _________75-25-2-————•——Bromof orm ________103-10-1———————4-Methyl-2-Ptntanone _____591-7S-6———————2-Ht x anona ___________127-15-4——————Tetrachloroethene_______79-34-5———————1, 1, 2' 2-T»trachleroethane_108-85-3—————Toluene ________.102-90-7——————Chlorobenitnt^;_________100-41 -4——————E t ft y 1 b en z ene___________100-42-5—————•—Sturena'- ____________1330-20-7——————Total Xylenti___________107-02-3———————Acrolein ______________1 C?-13-1 -————•—Ac r ylonitril t _________

19116801011

1200124

140039056

.- nat66.171079S381143010

10OO1107811

160069811

35033014O

!UIU>i!U

u

iU

UuuuU"uU

uU

FORM I VGA 1/87 Rev.

00272



ERA SAMPLE NO.

c Name: ygPSAR INC Contract:EDG36

Life Cod*: VE3SAR Case No. : 11724

v*trix: (ioil/wat*r) WATER

3*7,? It wt/vol: 23. 0 (g/mL> QU__

Lfrv*l: (low/ntrt) LDUJ

". Mciitur*: not d*c. ___m

loiumr. (pack/cap) PACK

:..-.T.frfr TIC* found' _£

SAS No. ; 4537E SDG No. : EAL74

Lab Sample ID: 6973S

Lab Filt ID: YS322

Datt Rtctivtd: 04/05/89

Date Analgztd: 04/12/89

Dilution Factor: 55Q


1

CAB NUMBER '• COMPOUND NAME

ii

i: RT11

1

: EST. CONC.11

Q

rFORM I VOA-TIC

1002731/87 Rtv.

\~&f'^ #3^'&s^-i^*4£J&?^^'tis& VL Ii ' L.

5 Name: VERSAR INC

: Cade: VE^SAR


___________ Contract: _

ERA SAMPLE

EDG37

C«s* No. 11724 SAS No.: 4537E SDG No. : 724

"s-rrix: doil/uattr) UIATER Lab Sample ID: 69736

s s - r t p l e wt/vol: 25. P (g/mL) QL.__ Lab File ID: Y5314

- ? - s l : (low/med) LOW Date Received: 04/05/89

in iture: rot dfrc.

c

(pack/cap) PACK


Dilution Factor: i_2o____


74-87-3————-—Chloramethane____74-S3-9———————Eromomethane,____75-01--——-————Vinyl- Chloride_________75-00-3——•—-——Ch Ioroethane_ ________75-09-2———————Methy lene Chloride______67-64-1———————Acetone_______________75-15-0———————Carbon Ditulfide________75-35—i———————1- 1-Dichloroethene_______"^5-35-3———————1- 1-D i ch 1 or o ethane______E4C-**—3——————i. 2-Dichloroethene (total >,67-66-2-———————Ch lorcif orm ____„:07-06-2—————— 1, 2-Dich 1 or oethane______76-93-3————— —— 2-Butanone ___,____„71-5-5-=———————1. 1. l-Trichloroethan*____56-23-5————•——Carbon Tetrachloride_____JCS-05-4——————Vinyl Acetate ________75-27-4———————Sromodichloromethane_____7S-S7-;——•————I, 2-Dich loropropane^...____lOOel-Gl-S——————cii-l* 3*-Dichloroprop en».79-01-a————— —— Tr ich loroethene________124-43-1——————DifcrofflQChl or omt thane_____79-00-5———————1. 1* 2-Trichloroethane"____71-43-2———————Benzene______«_________75-25-2————————Eromof orm _________10S-i:—:——————4-M*thyl-2-Pent»none_____5? I -73-ss———————2-Ke x anone_____________127-15-4——————Tetrachloroethene ____7**-3&-5———————li 1* 2- 2-Tetrachloroethane_lQS-BS-3——————Toluene,________________10S-9"-7——————Chlor ob en: ene________200-41-4——-————Ethyl benzene.,___________100-42-5———————Serene________________1330-20-7——————Total Xylent*___________: C7-C2-S——————Acre 1 e i n_____;__________1C 7- 33-'.————•——Acrulonitr ile ____

FORM I VQA

10512585062Z58333533954493463

57380633355

16072

;u:ui;u•i;u:u:u!U•iiUIU:u!U;u!U!U:uIU•!U:u!UJ U!U;u••!U:u!U:u;u!U!U!U

1/3" R*v.

100314

IEVCLATILE ORGANICS ANALYSIS DATA SHEETTENTATIVELY IDENTIFIED COMPOUNDS

EPA SAMPLE NO.

EDG3?Mime INC Contract:

Case No. : 117g4 SAS No. ; 4537E SDS No. : EAL7A

wt.-'vcl

U1ATER

25 0 (g/mL) QL,_

LOW

Lab Sample ID: fe973fe

Lab Fil* ID: Y»3i4

istu-e: net dec. ___

!tir. < p £ c k / c a p ) PACK

Dat* Rtc»iv«d: 04/05/8

Datt Analyzed: 04/12/B9

Dilution Factor: 130

. r r c- • T I C 5 found: __ J.CONCENTRATION UNITS:Cug/L or ug/Kg) 'JQ/L

;*.£ N'JflEE? I COMPOUND

1 i UN KNOWN-

NAME RT

27. 36

i

EST. CONC. ! G

4 ! J

FORM X VOA-TIC l/8~ Rev.

30031H

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C * *-* • X: «-» O O O O « - » H * * ( - O U J l t . » - * Q. ftp C * * >~*<• c i~ c u DI - ( - I . t- j r i - * o i - H 4 * a . c | o *> «c c: -•£ < V O < V • » O O O 6 O f t O 4 J - P ' - « O O f t r ^ U I.H ft (- ft Mft ft (,+ * £ * - * £ • - - * « - « r - t f - . f - — t c - « ^ f t * i : — * | O J C » 4 £ | C O h - C M • - • 4Jft 4J .C 4J C Q . f l . C f O . f l O f - h - l ' U . C . f - U l - (- *-« O — l t ft C 3» C -^E • O ft W ft U M U < t - U C I — < t ' « - * U O O O | — f t O H > C ^ f 4 f t A f t f t X ' * - * CO€ O •-« C C --t •-* ^ O -^ H | C \ j — « , . - « E | C M - . c : * . » . J . C O j C * C ftot- O>-« f. 7O O Q O O t- CJ 4J r-i O •-* O Q «H il ora W O4> M <9 t j ft i- •-» f t« -«r - . t~«O C 7 0 C . J A I i i o l 3 , i i 3 ' e i | u ( - . * • € « « ( - - a o j - f - t n o j --* ij ii *-•• 4' w f. -»• r-4 cj >-i r«i m >••* f. ir o r«l *" « .<^ >••* i- c> ir X -t-"* *•-• •••* •--• *^ :> ** i- t-j i * - M £ * u * * - , -*: -1 ^ »tt r» t-. . -ri (. r« , f t f _ i t • i f ~ u x : 4 - | 4 ' C t o uU CJ > (J £: *t O --i --i -« O ••• TI* r« O > ii» ••• o I-- C) -• CQ i-J *t (tf 1- w-t J- (j U U) |- *t <1 1 11 1 11 1 11 1 11 1 11 1 1I D i

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f+ .-. .1 t;t!. «'l 11 ..1

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V.

IE .VOLATILE ORGANICS ANALYSIS DATA SHEET


EPA SAMPLE NO.

--: N*ffie : VSPSAR INCV..

Coti*: VEPSAR Case No

2 x ( soil/uatar ) WATER

ut/vol

11724

(g/mL)

LDU

. :. i -.-mri

*: not dec. ___

f p a c k / C A p ) PACK

i . _ £»

EDG43Contract:

SAS No. : 4337E SDG No. : E.AL74


Lab File ID: Y5323




CONCENTRATION UNITS:<ug/L or ug/Kg) UG/L

" — — f I!_ —I i^^ COMPOUND NAME RT EST. CONC.

rI VQA-TIC 1/87 Rev.

100340

QRGANICS1A

ANALYSIS DATAEPA SAMPLE

SHEET

EDG58AR IN: Contract:

'•* o 11724 SAS NO. : 4537E SDG No. : 72£

• scil -''is*e^ ) UATgR

r=-.:-!« u/t/voi: 25. 0 (g/mL>

I ak C«*-«*i» T TVi_SS =3\UU it ii.' .

Lab Fil* ID: Y5324

_= .-si: LDUJ

•: is tur*' not ds-c.

PACM.

Dat* R*c*iv*d: 04/05/89



CAS NO. COMPOUNDCONCENTRATION UNITS:(ug/L or ug/Kg) UO/L

74-*7-% —— - ————— Ch la-rom*than*74-$ - ————— —— $r«diom*thari* .75-01 -- ——————— Vinul Chlorid*75- SO-"—— —— - ———— CnlflroBthan*^73-O9-2 ————————— Mft thy l*n* Chlarid*&7-e4- 1 ————————— Ar * t o n ft73-i*-O ————————— Carbon Di«ulfid*7S-3S-4 ————————— l. l-Dichloro*th*n* __. .75-35-3 ——————— l, i-Dichloro*than*54C— 5*— :> —————— 1, 2-Dichloro*th*n* (total ) __i-.7-ie-I- ———————— Ch 1 preform1C7-OA-2 ———————— 1, 2-nichloro*th«n*iiB m ., ., ._70-9 •*-- ————————— 2-Butanon*,,,7'-**- « ————————— i. 1. l-TrichlOTo»fchan»?»-~"f-5 ————————— Car- ban T*trach 1 or i d*1C---C5— a —————— Vir.ul Ac* tat*7S-37-4 ————————— Rr^/r.Ddichlorom»thariB7S-«i7-? ————————— 1 . -nichloroprapane _ .,.,_ „10061-C1-5 ————— ci t-1 > 3' -Dichleroprop »n*7c-C-l-c —— —————— Tr ich loro*th*n*124-45-1 ———————— DibromochlQrOffl»thar,»7Q-.-10-S ————— —— 1 . i . 2-Trichlot»a»than»71-4^-2: —————— • ——— B»nT»n*_7*-2*-2 ————————— Sramof orm _,._,_IftS-l "'-1 ———————— 4-M»thyl-2-P*nt*non» „ ,•ci-75-B ——————— ?-M9Kanon*_ _„__,..1C7-1J-4 ———————— T*f.rachlflro*th»n» ..... , , , ,70-34-j ——————— i, i, 2* 2-T*trachloro*than* ___ica-&3-3 —————— Toiu*n*M , .,i rjp_-?o-7 ————— . — Ch I or Qb*nz*n*1 GO-41 -4 ———— —— Eth4lb*nz*n*1 OCi-42-5 ————— ——— Shijran*^l^f.Q~yC-7 ——————— Total Xqltn**1 O7-O2-S ———————— Aer-ol »ini r,7- 1-^-1 — . —————— A,-n|( 1 onitril*

i•0. 4 1 U0. 2!U0. 3!U0. 2!U0. 6! 4 \rf <*0. 2!U

0. 08 iU0. 09 IU0. 3!U0. 7!^-<-o. i :ui :u0. 1 !U0. 1-!U0. 3!U0. 21U0. 1 !U0. 2!Uo. i :u0. 2!U0. 2iU0. 1 !U0. 2!U0. 3!U2 :uo. i:u0. 2!U0. 7! :0. 1 !U0. 1 !U0. 2!U0. 2!U7 !U3 iU

*

fK,y/

FORM I VQA 1/87 Rev

100354

IE.'•CLATILE ORGANICS ANALYSIS DATA SHEETTENTATIVELY IDENTIFIED COMPOUNDS

EPA SAMPLE NC.

EDG53Name INC Contract:

Case No. : 1 1724

•11 k = oi 1 /watt-r > UATER

:-:& wt/vol 2S. 0 <g/mU>

•*i. < lour/mta ) LOU

••:; = t UT- e ; not d fc c . a ___

. n >: p a c V. -••' c a p< 3' PAC*

r # r 7 T C t Found: _ 0

SAS No. : 4 337E" SDG No. : EAL74

Lab Sampl* ID: 6^733

L»b Filt ID: YS324


Dat« Analyzed: O4/12/89

Dilution Factor: ? 0


NAME RT EST. CONC

i VGA-TIC 1/S7 Rev .

100355

UKlTtO STATU tWIftOimfmi nOTCCTlON ACENCTaction vISS/Central ttgfonal laboratory

OATA TlAClttHG fQM FOft CONTRACT

C R L Oata S o t « o - - - CtlCLlS t o .S«0 Cast No. lnai\Sl M l£lito >a»t and location: UP j n/vo d fUQiLD Q. ,JU*> if. Contractor tr I?A laboratory: VJ^JLTJ^ Bata Isorj

Mo. »f SaapTts: / 7 tata Sanplts or Data ttctivtd: ^5 — S

1. Mart chatn-of-custody rtco'ds bttn rtctivtd? TEt^ — «0J. Havt Tnaltic ttports or packing lists tttn rtctlvt?T Ttl ^NOS. If no, art Traffic ttport or packlftf litfausbtrs vritton on Ihichaia-of -custody

rtcord? US MO __4* If no. which Traffic rtport or picking list avobtrs aro vissing?

basic data fores 1n? TES — toi^^/f ' jf*t

wbtr of sais^lts claimtd: f*~r Kuahtr of saoplts ractivtd: /*-/

-ktd by: P 01 /UU Oat.: S ^r-Sj

,<!vtd by Contract Frojtct HAAagtatRt Stetion: OattsStarttd: o n w I fttvitwtr Sigaaturt: ____

\-a 9 • k^f/fcA3Total ti»t sptnt on rtvit*: A :> ^^ Oatt rt*it» cocpltttd: " /'*/<>

Copt td (xtrosad) by: CrrA/TrX Cata:^ " " ^ ^ " ^ ^^^^^^^^^^™^^^^^^^^

Ma.!1td to Bata Vstr by:

*1tast fill in tht blanks btlo* and rttum this fon to: Sylvia ftrtffin. DataManagtmtnt Coordinator, Mgion f, SSCftL

Oata rtctivtd by: _ ____ P^ttt ^ ^

O.A. rtvit* rtctUtd b«i tait; _ ^ __ _ _

Inorganic Oatt Cowplttt t 1, Suitablt for Inttndtd 'urposts I 3 /[ 3 if acctptablt.Organic Oata Complttt I J. Suftablt for Inttndtd Vurposts t J List probltas btlo*.Oioxin-Oata Co«ploto L J. Suitable for Inttndtd Furposts L JSAS Oata Conpltto C 3. Suftablt for Inttndtd Purposes t J

Stt Attachtd 'Missing Oata ttoutst fona* [ \rttast jndicatt riasans (if any] «"y ^t* *rt not suitablt for yourOthtr problem*.

KecctVtd by Data Kanajtmtnt CoordinaterA CRL for Ptlt: Oatt:.

r»T7T-o a

6 i^-

f

y -

PAG? i OF bUNITED STATES ENVIRONMENTAL »*<vr6CTlON AGEWCY —

REGION V

r r -JICTS Review of Region V CLP Data

Received for Review on*/*7 "

Curt 1s toss. Director (55CRL)Central leslonal Laboratory»7ta Users

Vt have reviewed the data for the foil)

SITEData Set No..

C*L Mo.______

SHO Traffic . ST7 - 93, ?&-t7. PbJ Krs. RKrs. RequiredCLP laboratory: __________ /g.ffl-^ ___________ for Review;

Following are our findings:

^V#"5>Tr// j£f£77^Dii*y *'«'JHT&Tfcvi,,yr SesJKJIz

tfData art acceptable for vse. V£***~&£ \Oata are acceptable for use with qualifications referenced above. / • / . / 'See Data Qualifier sheets and Calibration Outlier forns for Tags and tf ,(/! W ^ ?Iddltional connents. '

C ^ Oata are preliminary - pending verification by Contractor Laboratory.See Case Sumary above. • /

i ) Data are unacceptable* \/

ec: Carla Ompsey.CLP Quality Assurance Officer, Analytical Operations BrianchJames Petty. Chief Quality Assurance Research, EKSL, Las Vegts

or oW7A QUALIFIERS

I Case

1* a ftunmirjr of the out-of-control audits and the posslblt tfftct en thttfata for this cast:

I(3

Ttif CPL

Vflff V&K

V3LK 1-3

of 1£LiiJ ft 0*/

*?rt Lr/n, r

tvltwtd by:*hont:Oatt:

OF (?DATA QUALIFIERS

C«t

trio- U t tum»v of the out*of-control audUt and the »0ss1Mt tfftct en tht««U for this case:

ft-ll

ML urtff *Z"3

AfJ

W/vP -r

tic } fr,T/?/c'//c

n II.

by:Phont:Date:

CASE/SAS

PROTECTIONCALIBRATION OUTLIERS

VOLATILE HSL COMPOUNDS

tEGlON V

CONTRACTOR\

Instrument 9 vDME/TJME:

CniOPomethaneBPomoêthaneVinyi chlorideCnlopoethaneKMnyiene ChlorideAcetonecapbon nisuifide1 ,1-OicMoroethane1 ,1-DiehioroetneneTrans-1 ,Z-DichiopoetheneCMoPOfOPmZ-ButanoneI.z-Dieniopoethane2.1 .1-TricniopoetnaneCa'bon TetPacniopideVinyl Acetate?-o-i55i cm opoêt hane] ,Z-P"CMorOP*Op|nt

|Tpais-l .3-DicMoPOpPOpeneTp^cHO*0eiheneD1; t'oôc M oponet na ne1 .1 .Z-Tpichl opoetnaneBenzeneC^S-1 .S-D^Chloropropene?-Cnlo -o«tnyl vinyl etherP'OTfO'ffa.^ft^vl-Z-Pentanone

IZ-Heê^Dê|Te* racMoPoethene1 ,] t Z.Z-Tet pacnic-poethaneToluene

[Chio*cr;ep'Zef>'eI E t hy iDe"'2C"êIStypeneir->ylefteC'5->yleneA'Ac^/A'ffftW UbrFj it-

AFFECtED$AM-fcES:

f k \ *Kevlewer's f\t^* tyl'l MM1

lnU1al$/Oaie: "I !

Invu/-f

^F

C.lff

c/;sy£Ttf3

£.i3t

;* Ca?dIR5D

'3LV

7.*?

&,1/ '

•

*

7r

rlf"

if,

Ionfu

Ml-

. i* *

M/yfu.c^7

bV if;

i«Jl* 0*P /J ^^

P* l?#Lftl£$t

.* L^yib

f!'^

Ji/'is'c.

IL1H

?^-VIf^( c-•*i?3$

ll*^11*

*^*' /^

^r

jrt

^t

Con'

RF

* t

10

il*

•

Coni

RF

a

'

.* C

ID

> 1 »

*

Con:

l

. Ci1.

r1

The&e flags should be applied tc the inalytes on the tample data sheets.

S/87

V*4 »t« *l*'C.d

CASE/SAS

FRDTECTION AGENCT REGION VCALIBRATION OUTLIERS

VOLATILE MSL COMPOUNDSCONTRACTOR

inn. Cai. Cent. CaiInstrumentbATE/TIW£:

Cent* Cai. cent. cai. com, cai.Jh -%I! 'I 'I

Kr 1U Kt IU VICnioromethane

o r e

o r ec e o n e

s u e, *piCMoroetnane_. -uicniprpetnenerms- . - c o r o e t e n e

CM or.

,1.1-Tncniproetnane

Acetate

|Trans-l,3-Dichloropropene

l l . l .?"TrlcMoroetnane

i;

7''

-'y

.«fF

InUials/Oate

rrt£L t

These flags should be applied tc the analytes on the sample data sheets.

aT/87

CASE/SAS 9

fMj4UfTO.DIAL WUUCTION AGENCT REGION VCAU8RAT10N OUTLIERS

HSt COMPOUNDSCONTRACTOR

6 7

nstrument • mn. CD. Cent. Cl Cent. CD. Cont* Cai ont. cai.D A 7 £ / T J H £ : *#//

RF RF ID u XT IU

n y n o r e

h o r d eceone

. - c o r o e t i n e- c o r o e t n e n e

- u e n o n e iwc

etr«cMorideVinyl Acetate

Trans-l

].l.?-Tricnioroeinane

*2-CMo*oet*y1 vinyl ether

AFFECTEDSAM^ES:

Revie-pr's

M

• These flags should be applied tc the analytes en the sample data sheets.

For reporting results tr -be VSSFA, tbo following contract specificqualif loro oro to bo used. Tbo sevea- cjualifiers defined below ar««pg subject to modification by tbo laboratory. Up to firequslifioro aa? bo reported on Fora I for each eiTbo seven ZPA*defined qualifiers to bo used ore aa follows:

JJ - Indicates compound was analyzed for but not detected. Tboquantitatioa l ait must bo corrected for dilution sad

for percent mcisturo. for example. 10 0 for pbonol ia voter iftbo sample fin^ volume Is tbo protocol-specified final volume.If a 1 to AO dilution of extract is accessary, tbo reportedlimit ia 100 0. For a sail sample, the value must jlia *•adjusted for percent moisture. For example, if tbo sample bad24% moisture and a 1 to 10 dilution factor, tbo samplequsatitatioa limit for phenol (330 V) would bo oorroetod to:

100

aad df - dilution tactor

at 24% iatura. 9 - iflfl-24 - 0.74100

10 - 4300 V roundad to tha aapropriato•iffaifieaat firuraa

mabor of

C •

For ooil aavploo vubjoetod to CfC eloan-up proeoduraa, tbo C&QLio olao aultipliod by 2, to account for tbo fact that only halfof tbo extract ia roooworod.Xadieataa aa ootiaotod *aluo, Thla flag ia uaod oitbar whanoatiaatlai a ooneantration for tentatively identified oovjpoundawhore a 1:1 reipoaae ia oosuaod, or when tha aaaa apoctral dataindicate the preaoaoo of a ooapound that aoeta theidentification criteria bat tbo result is less dun the oaapleojuaatltatlon liait but creator than zero. Tor eataaple; if theeaaple quaatitatiea limit io 10 ug/L, but o ooncentretion of 3

io calculated, report it as 3J. The sample quantitationf^T

aa diseuosod for tbo V flag, so that if a sample with 24%moisture and o 1 to 10 dilution footer bos a calculatedconcentration of 300 «g/L mad a sample quantitatlon limit of430 aft/kg, report tbo concentration as 300J on Form 1.

iTbis flag applies to pesticide reeults where the identificationboa been confirmed by GC/MS. Single component pesticidesnf/ul ia the final extract shall bo confirmed by CC/KS.

»-2f 2/88

This flag la wad when the •nalyta la found la the associatedblank aa well as In tha acaple. Zt Indleataa possible/probableblank eontaalnation end warns tha data naar to taka appropriateaction. This flag »ust bo naad for a TIC aa well aa for apositively Idantlflad TCL

I • This flag Irt whose concentrations exceed thecalibration range of tbe'CC/MS Instztaont for that specificanalysis. This flag will aa£ apply to pestleldaa/TCBa analyzedby GC/IC methods. If one or nore enerpnunrle have a responseCreator than full saalo, the aawple or extract oust be dilutedand ze-analyxed according to tha specifications In fcchibit D.All such finepnimrii with a response greater than full scaleahould have the eoocentratlon flagged with an •!• on the Tom Xfor tibe original analysis. If the dilution of the extract

MUEilZ£_ja*l*lis_te bebelow the calibration range*results of both analyses shall be reported on separate TomsThe Tom X for the diluted eaaple shall have the *DL" suffixappended to tha sample wisher. VOTE: Tor total xylenea, wh*•:».three laoners are quantified as two peaks, .the calibrationrange of «aeh peak should be considered separately, e.g., adiluted analytis Is fio£ required for total xylenea unless th*-•eneentratlaa of either peak separately exceeds 200 ug/L.

0 * This flag Identifies all cioefpmmdi Identified In an analysis *ra secondary dilution factor. Xf a aanple or extract Isre-analysed at a hi|ber dilution faetor. as In the "£" flagabove, the *DL* suffix la appended to the aanple number on th*Tom I for the diluted aaajple, and all concentration values *reported on that Tom t are flagged with the *D" flag.

A • This flag Indicates that a TIC la a suspectedaldol •condensation product.

X - Other specific flags my be required to properly defineresults. If used, they aust be fully described and suchdescription attached to the Sanple Data Sunnaty Tackage and *Case lUrratlve. Begin by using *X*. Xf nore than one flag *

'veajualiflers are required for a aanple result, use the "X" flaxto poehine several flags, aa needed. Tor instance, the "X*flag night onoMne the "A*. ••". and "0" flags for sone sasipl

The cosfelnatlon of flags •W or^JB* la expressly prohibited. 11..eontanlnanta are flagged *ft* e«1v when they are also detected in isaaple.

If analyses at two different dilution factors ate required CeeeExhibit 0}, follow the data reporting insrruetions given in Exh.9 ard with the *D" and *1* flag* above.

B-30

UMITEO STATE* OimOimCMTAL PROTECTION ACENCYftUIM V .

153/Central Regional LaboratoryOATA TRACKING FORM PQR CONTRACT SAt*lES

CRL Bata $tt *o._____________CtRCLtS «o.

SnO Ctso Mfl.//%?y5y£St/5"-?ar sue it** and location: l/om«t aif. Contractor or EFA Laboratory* V O"g.G i Bata Bstr:

Ho. «f *«ap1ts: _Jj__Bata Santas «r Bata Receded: V *1. Kavo eha!n-of-custody rtco'ds batn racofvod? tCS __ ItO ^^"2. Hav« T«aCUc tt ports or packing Usts batn racatvaaTTiS^ «0 ~—3. If no. aro Traffic laport or p&cUng Illf w«bars vritton on tht Tenain-of-eustody

racord? TCS HO __4. Xf no. «hieh Traffic rtport or packing list avatars aro orfssing?

Art basic data foms in? TES ^ RO

Kumber of sauries chained: / r Kuaber of samples racelYcd:

by; (jA M Cu\Sls-*^ Bate:

by Contract Prsjact Kanasanant Sactlon: J/. { Bata;

Startad: ^/ ^V^7/ Bovlaftr Sfgaaturt:

Total tliio sptnt on rtv1t«: *>/ Bato rtvltw CMplatad:

Capfod (*troxad) by: A . _________ Bata:

Ul UJJ^^ Bata: . 5 " A •U.11ed to Bata User by: ___

DATA USERS;Please fill In the blanks below and return this fora to: Sylvia Crlffla. Batalianagtffltnt Coordinator. Region V, SSCRt

Data rtcttvtd by: Batt;

O.A. rtv1t« roct1vo4 by:____ . ____

Inorganic Bato ConplttoOrganic Bata CompltttBUx1n*Oata CeaplottSAS Bata CampUtt

. Suitable for Intended Purposes I 3 /t 1 If acceptable, Suitable for Intended Purposes C J List problems bele«, SuTtible for Intended Purposes L. Suitable for Intended Purposes L

Attached 'Mfsslng Bata Request Fom* I }XOBLEMS: Pteast Indicate reasans (if «ny] why data art not suitable for your uses

Other problems*"- ' :.;-•.-.•- //- '

by Data Hanagtmint Coordinate^ CRL for File: Bate:

SaaSSi &^V^

April 21, 1989

I. HarrativeOrganic* Case 11724 SAS* 4937E SDQ* EAL62CPA Region V - Curtie RossVersar Project 969.80 - Batch 2

This report contains the CLP analytical data for the volatilelav detection limit organic analysis of nineteen <19> watersamples contained In Cas* 11724* The samples Hated below arrivedintact at Veremr by Federal Express on April 4, 1989.

SABCUC USXEAL62 * EAL96EAL83 EAL97EAL84 EDG06EAL67 EDG14EAL88 EDG19EAL89 ED616 ,EAL90 ED026EAL91 EDO27EAL92 EDG28 ••EAL93

* - First eaaple in SDQ•• - Laet eaaple in SDQ

• »*SAS OHLY

Ho Diskette DeliverableSeven day ssspls .holding time30 day hardoopy report due dateLow Detection Limit Analysis

•Aerolein I aerylonltrils addsd to volatile target compound list* ,•••••••••••A***************************************************** [

iQC/HS instrument calibrations using BFB met contract j

requirements for volatile analysis. SPCC and CCC criteria vere |met for the volatile initial calibration curves and continuing jcalibration check standard. All QC/HS analyses occurred duringthe twelve hour period following dally instrument calibration.

All volatile internal standard area abundances and relativeretention times vere eompliaat for all analyses.

Volatile surrogate standard recovery values met all specifiedQC limits. One set of matrix spike/matrix spike duplicateanalysis was performed in conjunction vith this SDQ. . All valuesmet criteria.

Samples EAL87, EAL90, EAL92, and EAL93 required dilution inorder to quantify target compounds within the calibration rangeof the curve. Dilution factors for each sample are listed on theindividual Form IA. Ho other samples required dilution prior toanalysis.

7.0C005

we.

Narrative - Pag* 2Versar Project 965.80 Batch 2

Please contact Clay Hamner, CLP Project Manager, should youhave any questions or require additional information pertainingto the low detection limit analysis of these water samples.

Release of the data contained la this hardeopy data packagebeen authorized by the Laboratory Manager or his designee,verified by the following signature.

hae

_______ April 21, 1989E. Bock

QC/HS Data Processing CoordinatorLaboratory Operations

Data Qualifier Flag*

For Target Compound*! This flag ±m uaed when MMftpeotral data indicate* the preeence of a compound butthe reault i* leM than the *pecif ied detection limitbut *till greater than aero*

For Hon Target Compound* t Thia flag indicate* that theconcentration i* an e*tiMted valu«» aaauwing a 1 to 1

vith th» Internal standard.

B Thia flag ia uaad vh«n th« analyt* ±» found in theblank aa vail mm In the Maple. It indicate*poMible/probable contamination and warn* the data uaerto take appropriate notion.

Thia flag state* that the eoapound va* analyzed for butva* not detected. The number i* the miniaua attainabledetection limit for the eavple.

X or T Thi* flag etatem that the ma** epectrum doe* not meetGPA CLP criteria for confirmation* but compoundpresence i* etrongly auapected.

C Thi* flag i* umed to indicate that the quantltation ofthe analyte i* outaide the linear calibration of thecurve and that dilution va* required in order toproperly quantltate*

D Thi* flag i* umed to indicate the value for -the targetanalyte va* calculated from a dilution (me* *C* flagabove).

Thi* flag i* ueed vhen a matrix epike compound 1* aleoconfirmed preeent in the unepiked *ampl*.

Flag* excerpted from and e*tabli*hed by theUS EPA Contract Lab Program (CLP) protocol.

10Q207

°% ,-T ';^^^£^fb^^^'^^'^ii^^^1^^f-^^-^ r-^f?-:

2AWATER VOLATILE SURROGATE RECOVERY

Lab Nam«: VERSAR INC._____________ Contract: ________

Cod«: VERSAR C*«« No.: 11724 SAS No.: 4337E SDO No. : EAL62

i EPA ! SIt SAMPLE NO. 1 <TOL>»

011EAL62 1 9302 1 EAL83 1 9903JEAL84 1 9904IEAL87 i 91O9 1 EAL88 1 94061EAL89 I 10007 ! EAL90 ! 98O8IEAL91 1 10109 1 EAL92 I 9910IEAL93 I 97111EAL96 ! 10112IEAL97 1 9713 ! ED C 06 I 97141EDG14 ! 9413IEOG19 ! 9916IEDG16 ! 99171ED026 t 97181EDG27 t 9919IEDG28 1 94201EAL83MS ! 1O421!EAL83MSD 1 9822 ! VBLK49 ! 9623 ! VBLK69 1 9724IVBLK93 I 100

I I

82(BFB)«

99989910310310O10699102104106104981021019810199100102109101101104

S3<DCE>*

8891879996949791989497969990909294999297989392100

OTHER'

'

*

TOTiOUT

O0O0O0O000O000O0000000O0

SI (TOL) - Tolutn»-dB32 (BFB) • Bromof luorobvnzan*S3 (DCE) m 1, 2-Dichloro«th«n»-d4

QC LIMITS( 88-110)( 86-115)( 76-114)

* Column to bt uttd to flag recovery valut*

* Valut* outsida of contract rtquir»d QC limits

D ;Surrogatt» diluted out

r1 of 1

FORM II VOA-1 1/87 R»v.

10C009

3aSM*2?*?*£ ^ gp-rflKT

WATER VOLATILE MATRIX SPIKE/MATRIX SPIKE DUPLICATE RECOVERY

Lab Name: VERSAR INC._____________ Contract: _________

Code: VERSAR Case No. : 11724 SAS No. : 4337E

Jatrix Spiki - EPA Sample No. : EAL83_______

SDG No. : EAL62

COMPOUND

1* 1-Dichloroethene __Triehloroathen*BenzeneTolueneChlorobenzvne , , ,,

I SPIKEI ADDED! <ug/L)

! 20.01 20. 01 20. 0t 20.0

_ 1 20.01

SAMPLECONCENTRATION

(ug/L)00000

118CONCENTRATION

<ug/L)

13.617. 519.219.3 -19.2

US%

REC tt

7888769796

! QC 1I LIMITS!1 REC. t

161-1491171-1201t 76-1271(76-1291179-13011 t

' COMPOUND

1* l-Dichloroethen*Trichloro»then«BenzeneTolueneChlorobenz»ne

SPIKEADDED(ug/L)

2O. 020.020.020.020.0

MSDCONCENTRATION

(ug/L)

14. 816. 819. 917. 919.3

MSDX

REC tt

7484789097

XRPD «

9 '9-37-1

IQC LIMITS tRPD t REC. 1

14 161-149!14 171-120111 176-127113 176-129!13 179-1301

I 1

* Column to bt u«td to flag recovery and RPD valuvs with an atttri»lt

* Values outtid* of QC limits

RPD: _2. out of _a outsid* limitsSpik* Recovery: _2. out of 10 outside limits

COMMENTS: CLP*11724.EAL62, EAL83, L, U* 69624, V. , . 29MLINST Y SP-1000 43CC3MIN) TO 229C 8C/MIN

FORM III VOA-1 1/87 Rev.

100010

^

Lab Nam»: VERSAR INC.


________ Contract: _____

Cod«: VERSAR Ca*« No. : 11724 • SAS No. : 4S37E SDO No. :

Lab Fill ID: Y5249 Lab Sampl* ID: VBLKM*.

Dat* Analyzed: 04/06/89 Tim* Analyzed: 2234

Matrix: («oil/wat»r) WATER L»v»l: (low/mod) LOW

Inttrumvnt ID: V


i EPA1 SAMPLE NO.

O1IEAL6202 ! EAL8303 ! EAL84041EDG06051EDG1406IEDG1507iEDG16OS ! EDG2609 ! EDG2710IEDG28

1

LABSAMPLE ID

69623696246962369616696206962169622696176961869619

:

LABFILE ID

Y92S7Y5298Y5259Y5250Y9294Y9299Y9296Y9291Y9292Y9293

TIMEANALYZED

091109930639602103O903470429009901410223

COMMENTS: CLP, » > VSTD20, L, W. 17S03, V* CC-020, 25MLINST R: SP1000 60/80 CARBOPACK 2Mft45C > 225Cft8C/M > 3OMt225C

,.49* 1 of 1FORM IV VOA 1/87 R»v.

10G011


EPA SAMPLE NO

Lab Name: COMPUCHEM LABS_________

Lab Cod«: COMPU Ca»« No.: OOQQ

Matrix: (soil/water) WATgR

Sample vt/vol: 20.0 (g/raL) ML

L*v«l: (low/m«d) LOW

% Moistura: not d«c. ___

Column (pack/cap) PACK

Number TICs found: _Q

EAW14Contract: SAS4231E

SAS NO.: 4231E SDG NO.: EAWQQ.

Lab Saapl* ID: 247S14____

Lab Fila ID: CMQ47S14C11

Data Racaivad: 03/01/89Data Analyzed: Q3/Q6/89

Dilution Factor:

CONCENTRATION UNITS:(ug/L or ug/Kg) uc/L

CAS NUMBER COMPOUND NAME RT EST. CONC.- Q


SBMPLE OPTO SUHHBRV


EPA SAMPLE HO.

Lab Name: CQMPUCHEM LABS_____'"

Lab Coda: COMPU Casa Mo.: OQOQ

Matrix: (soil/water) WATEBSample vt/vol: 20.Q (g/mL) ML

Level: (low/mad) LOW

% Moistura: not dac. ___

Column: (pack/cap) PACK

EAW15Contract: SAS4231S

SAS No.: 4231S SDG No.: EAWQO

CAS NO. COMPOUND

Lab Saaple ID: 2 47 Sis

Lab rila ID: CNQ47515C11


Data Analyzed: 03/06/89i.C

Dilution Factor:


74-87*3——————Chloromethane_________74-83-9——————Broaoaethane__________75-01-4——————Vinyl Chloride________75-00-3—————-Chloroethane__________75-09-2——————Methylene Chloride_____67-64-1——————Acetone_____________75-15*0——————Carbon Disulfide_______75-35-4——————1,1-Dichloroethene_____75-34-3———————1,1-Dichloroethane______540-59-0—————1,2-Dichloroethene (total),67-66-3——-——Chlorofor*___________107-06-2————-1,2-Dichloroethane_____78-93-3———————2-Butanone____________71-55-6——————1,1,1-Trichloroethane___56-23-5——————Carbon Tetrachloride____108-05-4—————Vinyl Acetate_________75-27-4——————Bromodichloromethane____78-87-5——--'——1,2-Dichloropropane_____10061-01-5———-ci*-l,3-Dichloropropene___79-01-6——————Trichloroethene________124-48-1—————-DibrQaochlorome thane79-00-5———————1,1,2-Trichloroethane____71-4 3 -2™———-Benzene_____________10061-02-6———Tran»-l,3-Dichloropropene_75-25-2——————BroBOfom____________108-10-1—————4-Methyl-2-Pentanona____591-78-6——————2-Hexanone____________127-18-4—————Tetrachloroethene______79-34-5———————l,l,2,2-Tetrachloroethane_108-88-3—————Toluene_____________108-90-7—————Chlorobenzana__________100-41-4—————-Ethylbenzene__________100-42-5—————Styrene_____________1330-20-7————Total Xylenee_________107-02-8—————Acrolein____________107-13-1—————Acrylonitrile_________

FORM I VOA

10.80.911210.90.90.90.9141111111111121110.910.91122026

1/87 Rev,

SPMPLE Off TO SUHH8RV


EPA SAMPLE NO

Lab Nan*: CQMPUCHEM L A B S _ _ _ _

Lab Coda: COMPU Ca*« No.: OQOO

Matrix: (soil/water) WATERSampla wt/vol: 2Q.Q (g/mL) ML

Laval: (low/ra«d) LOW

% Mbifltura: not dac. _^


Number TICs found: _o


SAS NO.: 4231E SDG NO.: EAWQQ


Lab Fil* ID: CKQ47S15C11

Data R«c«iv«d: 03/01/89


Dilution Factor: »- ••# 5-/


CA5 NUMBER CONFOUND NAME RT EST. CONC/ Q

FORM I VOA-TIC 1/87 Rav.

Sf9HPL£ DffTff SUHH0RY


EPA SAMPLE NO.

Lab Nama: COMPUCHgM. Lft 85 _____

Lab 7oda: COMPU Casa No.: QQQQ

Matrix: (soil/watar) WATERSampla wt/vol: 20.o (g/mL) ML

Laval: (low/m*d) LOW



EAW16Contract: SAS4231E __

SAS No.: 4231E SDG No.: EAWQO

CAS NO. COMPOUND


Lab File- ID: CN0475iSBii


Data Analyzad: Q3/QS/89Dilution Factor:


74-87-3™———-Chioromathana_________74-83-9—————-Bromomathana___________75-01-4——————Vinyl Chlorida________75-00-3——————Chloroathana__________75-09-2——————M«thyl«i« Chlorida______67-64-1——————Acatona_____________75-15-0———————Carbon Diaulfida_______75-35-4——————l,l-Dichloroath«n«_____75-34-3——————1,1-Dichloroathana_____540-59-0—————l,2-Dichloro«th*na (total),67-66-3——————Chloroform___________107-06-2——————l,2-Dichloro*thana______78-93-3———————2-Butanona____________71-55-6——————1,1,1-Trichloroathana^56-23-5——————Carbon Tatrachlorida____108-05-4—————Vinyl Acatata______'75-27-4——————BronodiehlaroMthana78-87-5—————-1,2-Dichloropropana_____10061-01-5————cia-l,3-Dichloroprop«na__79-01-6——————Trichloroathana________124-48-1——-——Dibromochloronathana____79-00-5—-————1,1,2-Trichloroathaha____71-43-2————-—Banxana_____________U)06l-02-6———Trmn«-l,3-Dichloroprop«n«_75-25-2--————Bromoforn___________108-10-1-————4-Mathyl-2-Pantanona____591-78-6———••——2-Haxanona___________12 7 -ia-4—————Tatrachloroathana______79-34-5———————l,l,2,2-Tatrachloro«thana_108-88-3—————Tolu«n«______________108-90-7—————Chlorobanzana_________100-41-4————Ethylbanzana__________100-42-5—————styr«n«_____________1330-20-7————Total Xylanaa_________107-02-8—————Acrol«in____________107-13-1—————Acrylonitril*_________

FORM I VOA

10.80.912210.90.90.90.9141111111111121110.910.91122026

1/87 Rav,

SffHPLE D0T(9 SUHHBBV


EPA SAMPLE NO,

Lab Name: COMPUCHEM LABS___________

Lab Code: COMPU Case No.: QOQQ

Matrix: (soil/water) WATER

Sample vt/vol: 20.0 (g/mL)

Level: (low/med) LOW

% Moisture: not dec. _____



EAW16Contract: SAS4231E .

SAS NO.: 4231E SDG No.t EAWQO

Lab Sample ID: 247S16______

Lab File ID: CNQ47516B11



Dilution Factor:

CONCENTRATION UNITS:(ug/L or ug/Kg) UC/L

CAS NUMBER COMPOUND NAME RT EST. CONC^ Q

FORM I VOX-TIC 1/87 Rev

SBHPLE OOT0 SUf1H0#V 29


EPA SAMPLE NO.

Lab Kama: CQMPUCHEM LABS_________

Lab Coda: COMPU Casa No.: QQOQ

Matrix: (soil/watar) WATERSampla vt/vol: 20.Q (g/mL) ML

Laval: (low/mad) LOW

% Moistura: not dac. .


GAS NO. COMPOUND


SAS NO.: 4231E SDG No.: EAWQO

Lab Sampla ID: 247517____

Lab Fila ID: CN047517CH

Data Racaivad: Q3/Q1/89

Data Analyzad: Q3/Q6/B9/-O

Dilution Factor:CONCENTRATION UNITS:(ug/L or ug/Kg) UQ/L

74-87-3——————Chloromathana_________74-83-9-—————Bromoaathana__________75-01-4——————Vinyl Chlorida________75-00-3———————Chloroathana___________75-09-2——————Mathylana Chlorida_____67-64-1——————Acatona_____________75-15-0———————Carbon Diaulfida_______75-35-4——————1,1-Dichloroathana______75-34-3——————1,1-Dichloroathana______540-59-0——————1,2-Diehloroathana (total).67-66-3———————Chloroform____________107-06-2——————1,2-Dichloroathana______78-93-3———————2-Butanona____________71-55-6———~—1,1,1-Trichloroathana___56-23-5——————Carbon Tatrachlorida____108-05-4—————-Vinyl Acatata_________75-27-4———————Bromodichloromathana____78-87-5—————1,2—Dichloropropana_____10061-01-5———-ci»-l,3-Dichloropropana__79-01-6——————Trichloroathana________124-48-1———— Dibromocnloromathana____79-00-5—-——-—1,1,2-Trichloroathana____71-4 3 -2——————Baniana_____________10061-02-6————Trmn«-l,3-Dichloropropana_75-25-2-————-Bro»oform___________108-10-1——————4-M«thyl-2-Pantanona____591-78-6——————2-Haxanona____________127-18-4—————Tatrachloroathana______79-34-5——————1,1,2,2-Tatrachloroathana_108-88-3——————Toluana_______________108-90-7—————Chlorobanzana_________100-41-4————Ethylbanzana__________100-42-5—————styrana_____________1330-20-7————Total Xylanas__________107-02-8—————Acrolain__________•107-13-1—————Acrylonitrila_________

16.80.910.9210.90.90.90.9141111111111121110.910.91122026

FORM I VOA 1/87 Rav

StMIPLE Of* TO SUHHQRY 23


EPA SAMPLE NO.

Lab Name: COMPUCHEM LABS_______Lab Cod«: CQMPU Gas* No.: QQQQ

Matrix: (soil/water) WATERSample, wt/vol: 20.0 (g/mL) IU,_

L«v«l: (low/mad) LOW

% Moi»tur«: not d«c. ___


Numb«r TICs found: _0


SAS NO.: 4231E SDG No.: EAWOO

Lab Sample ID: 247517Lab Fil« ID: CN047517C1^

Dat« R«c«iv«d: 03/01/89

Data Analyzed: Q3/Q6/89/.C

Dilution Factor:.-4*ftiO&J-/5"-


GAS NUMBER COMPOUND NAME RT EST. CONC. Q

FORM I VOA-TIC 1/87 R«v,

SAMPLE DOTB SUHH08V


EPA SAMPLE NO.

Lab Name: COMPUCHEM LABS__________

Lab Coda: COMPU Cas* No.: QQQQ

Matrix: (soil/water) WATERSample wt/vol: 20.Q (g/mL) ML

Laval: (1ow/m«d) LOW

% Moisture: not dec. ___



SAS NO.: 4231E SDG No.: EAWQQ


Lab File ID: CN047518C11

Data Received: 03/01/89

Data Analyzed: 03/06/89Dilution Factor:

CAS NO. COMPOUNDCONCENTRATION UNITS:(ug/L or ug/Kg) UC/L

74-87-3—————-Chloromethane_________74-83-9——————Bromomethane__________75-01-4——————Vinyl Chloride________75-00-3—-——— -Chloroethane__________75-09-2——————Methylene Chloride_____67-64-1——————Acetone_____________75-15-0——————Carbon Dieulfide_______75-35-4——————1,1-Dichloroethene______75-34-3——————1, 1-Dichloroethane______540-59-0—————1,2-Dichloroethene (total)67-66-3——-——--Chloroform___________107-06-2—————1,2-Dichloroethane_____78-93-3——————2-Butanone___________71-55-6——————1,1,1-Trichloroethane___56-23-5——————Carbon Tetrachloride____108-05-4——————Vinyl Acttata__________75-27-4—•————Broaodichlorom«than«____78-87-5———-——1,2-Dichloropropana_____10061-01-5™——ci«-l,3-Dichloropropana__79-01-6——————-Trichloro«th«n«_______124-48-1-———™Dibromochlorom«than«____79-00-5———-™l,l,2-Trichloro«than«___71-43-2—————Banzana_____________10061-02-6——--Tran»-l,3-Dichloropropan«_75-25-2—————Bromoform___________108-10-1—————4-H«thyl-2-P«ntanon«____591-78-6—-————2-H*xanon«_____________127-18-4—————T«tr*chloro«th«n«______79-34-5—————-l,l,2,2-T«trachloro«than«_108-88-3—————Toluana_____________108-90-7—————-Chlorob«nz«n«_________100-41-4—————Ethylbanzana_________100-42-5————StyrtiM_____________1330-20-7———-Total Xylanaa_______.__107-02-8—————Acrolain_____________107-13-1——————Acrylonitrila__________

10.80.910.8210.90.90.90.9141111111111121110.910.91122026


SQHPLE OffTff SUHH88V


EPA SAMPLE NO

Lab Nam«: COMPUCHEM LABS__________

Lab Cod«: COMPU Cast No.: QOQQ


Sampl* wt/vol: 2Q.Q (g/mL) ML

L«v«l: (low/m«d) LOW



Numb«r TICs found: _0


SAS NO.: 4231E SDG No.: EAHQO

Lab Sampl* ID: 247518 ____

Lab Fll« ID: CN047518C11

Data R«c«iv«d: 03/01/89

Data Analyzed: os/os/aa

Dilution Factor:


GAS NUMBER COMPOUND NAME RT EST. CONC.- Q

FORM I VOA-TIC I/87 R«v.

S8HPLE DffTff SUHHQBV


EPA SAMPLE NO.

Lab Nam«: COMPUCHEM LABS__________

Lab Coda: CQMPU Cas* Ho.: ooooMatrix: (soil/watar) WATERSampla wt/vol: 20.Q (g/mL) ML


% Moiatura: not d«c. ___



SAS No.: 4231B SDG NO.: EAWOQ

CAS NO. COMPOUND

Lab Saapl* ID: 247519

Lab Fil« ID: CNQ47519B11

Data R«c«iv«d: 03/01/89

Data Analyzed: Q3/QS/89

Dilution Factor:

CONCENTRATION UNITS:(ug/L or ug/Kg) PG/L

- rf''J"J

74-87-3 ———— -74-83-9 ———— -75-01-4 —— ——75-00-3 ———— •75-09-2 ———— -67-64-1 ———— -75-15-0 ———— -75-35-4 ———— -75-34-3 ———— -540-59-0 ——— -67-66-3 ———— •107-06-2 ——— -78-93-3 ———— -71-55-6 ———— •56-23-5 ———— -108-05-4 ——— -75-27-4 ———— -

. —— Vinyl Chlorid*

- — -Carbon Dimulfida

- — -l.l-Dichloro«than«.._ _u _— -1 , 2-Dichloro«th«n« ( total ) __

— -1 . 1 . l-Trichloro«than«

lOOfil-01-5-— - — ci«-1.3-Dichlorooroti«n«79-01-6 ———— -

79-00-5 ——— —71-43-2 ———— -10061-02-6 — -75-25-2 ———— -108-10-1————591-78-6 ——— -127-18-4 ——— -79-34-5 ———— -108-88-3 ————108 -9 0-7 -- — -100-41-4————100-42-5 ——— •1330-20-7 —— -107-02-8 ——— -107-13-1————

— - -1 . 1 . 2-Trichloro«than«

»»Tafcraehloroathana

. —— Chlorobanzana ,.,._.,. 1M1 ,, ,

— — Acrolain—— -Aerylonitril* .,_ . .

10.80.912210.90.90.90.9141111111111121110.910.9112

2026

UUUUUUUUUUUUUUUUUUUUUUUUUUUUUUUUUUUU


StMIPLE D8T0 SUHHOKY


EPA SAMPLE NO.

Lab Nanw: CQMPUCHEM LABS________

Lab Coda: CQMPU Cast No.: QQOQ

Matrix: (soil/wat«r) WATERSampl« wt/vol: 20.0 (g/mL) ML_

Laval: (low/m«d) LOW

% Moisture: not d«c. _____


Numbar TICs found: _0


SAS No.: 4231E SDG No.: EAWQQ

Lab Saapla ID: 247519_____

Lab Pil« ID: CNQ47519B11

Data R«c«iv«d: Q3/01/p9

Data Analyzed: oa/os/aa10

Dilution Factor: -4-«-y "\b 3-/^V

CONCENTRATION UNITS:(ug/L or ug/Kg) Uc/L

CAS NUMBER COMPOUND NAME RT EST. CONC; Q


SOMPLE DBTf) SUMMBBV


Lab Nama: CQMPUCHEM LABS ________ Contract: 5 AS 4 2 3 IE

Lab Coda: CQMPU casa No.: oooo SAS No.: 4231E SOG No EAWOO

0102030405060708091011121314151617181920212223242526272829

EPASAMPLE NO.

EAWOOEAW01EAW02EAH02REEAW03EAW04EAW05EAW06EAW07EAW08EAW09EAW09R2EAW10EAW11EAW12EAW13EAW14EAW15EAH16EAW17EAW18EAW19EAW09REMSEAW09R2MSDVBLKXGVBLKSJVBLKAOVBLKARVBUOCI

SI(TOL) #

10299103989810810810110510410099ill -*109106105103104106102104102979910296102101103

S2(BFB)*

9595999793102105100981009410110610498979799999698971009999941039998

S3(DCE)#

9394108979410310397981009810610510510410310310110210210510210410510592999899

OTHER TOTOUT

000000000000-*-0000000000000000

QC LIMITS31 (TOL) - Tolu«na-d8 ( 88-110)S3 (BFB) - Broaofluorobanzana ( 86-115)S3 (OCX) - l,2-Dichloroathana-d4 ( 76-114)

I Column to b* u»ad to flag racovary values

* ValuM outaida of contract raquirad QC limits

D Surrogate* dilutad out

pag« 1 of 1FORM II VOA-1 1/87 Rav,

SPHPLE PffTff SUHMRRY 19

3AWATER VOLATILE MATRIX SPIKE/MATRIX SPIKE DUPLICATE RECOVERY

Lab Nan*: COMPUCHEM TABS________ contract: SAS4231E

Lab Code: COMPU Case Mo.: QOQO SAS No.: 4231E SDG Mo.: EAWQQ

Matrix Spike - EPA Sample No.: EAWQ9RE_____

COMPOUND

1 , 1-Dichloroethene ___TrichloroetheneBenzeneTolueneChlorobenzene, _. M

SPIKEADDED<ug/L)

278 .278278278278

SAMPLECONCENTRATION

(ug/L)0

100016.5

11300

MSCONCENTRATION

(ug/L)28013803061500291

MS%

REC #

101137 *104133 *105

- '

QCLIMITSREC.

61-14571-12076-12776-12575-130

COMPOUND

1,1-Dichloroethene.Tr iehloroetheneBen z ene_________Toluene________Chlorobenzene.

SPIKEADDED(ug/L)MMBmn

278278278278278

MSDCONCENTRATION

(ug/L)iai»B

2731330300

1470293

QC LIMITSRPD««*1414111313

REC.

61-14571-12076-12776-12575-130

I Column to be used to flag recovery and RPD values with an asterisk* Values outside of QC limitsRPD: _fl out ofSpike Recovery: .

outside limitsout of 10 outside limits

COMMENTS: CLP ,4231,EEAWOO,-EAWO,LOW,WATER,247509,PEST, ,

FORM III VOA-1 1/87 Rev,

SOMPLE DQTff SUHHBBV i:

4AVOLATILE METHOD BLANK.SUMMARY

Lab Name: COMPUCHEM LABS________ Contract: sAS423IF

Lab Code: COMPtT Case No.: OQQO SAS No.: 4231E SDG No.: EAWQQ

Lab File ID: ggg9Q302Bii Lab Sample ID: VBLKXS____

Data Analyzed: 03/02/89 Tim* Analyzed: 2010

Matrix: (soil/water) HM2R- Level:(low/med) LOW

Instrument ID: 11

THIS METHOD BLANK APPLIES TO THE FOLLOWING SAMPLES, MS AND MSD:

0102

EPASAMPLE NO.

EAHOOEAW09

LABSAMPLE ID

247497247509

LABFILE ID

CK047497C11CN047509C11

TIMEANALYZED

04410528

COMMENTS: CLPTUNE: 0011 030289 1826

page 1 of 1FORM IV VGA 1/87 Rev

SQMPLE DffTP SUMHBRY


Lab Nam«: CQMPUCtfEM LABS ______ Contract: SAS423IE

Lab Cod*: CQMPU Cas« Mo.: QQOQ SAS Mo.: 4231E SDG Mo.: EAWQO

Lab Fil« ID: CBa9Q3Q3All Lab Sampl* ID: VBLKSJ____

Dat« Analyzed: Q3/Q3/89 Tlm« Analyzed: 0913

Matrix; (soil/wat«r) WATER I*v«l:(low/m«d) LOWInstrument ID: 11


0102

EPASAMPLE NO,tmmmm*EAW01EAW02

LABSAMPLE IDMHBvflnn247498247502

LABFILE ID

CH047498A11CN047502A11

TIMEANALYZED

tmmmm*10161117

COMMENTS: CLP , , , , , , ,PEST,BLANK,TUNE: 0011 030389 0736

pag« 1 of 1FORM IV VGA 1/87 R«v.

SQMPLE D0T0 SUMM8RV


Lab Nam«: CQMPUCHEM LABS_________ 'Contract: SAS4231E

Lab Cod«: COMPU Ca»« No.: QOQO SAS No.: 4231E SDG No.: EAWQO

Lab Fil« ID: gBagQ3Q4Ali Lab Sampl* ID: VBLKAQ____

Dat« Analyz«d: 03/04/89 Tim« Analyzed: 0942

Matrix: (soil/wat«r) HAIHL. L»v«l:'(low/m«d) LOWInstrument ID: 11


010203

EPASAMPLE NO.

EAW02REEAW03EAW04

LABSAMPLE ID

247502247303247304

LABFILE ID

C4R47302A11CN047503A11*CN047S04A11

TIMEANALYZED

154810371130

COMMENTS: CLP , , , , , , ,PEST,BLANK,TUNE: 0011 0304S9 0711

pag« 1 of 1FORM IV VGA 1/87 R«v

SBHPLE DPTff SUMHBRY


Lab Name: CQMPUCHEM LABS_________ Contract: SAS4231E

Lab Code: CQMPU case Mo.: QQOQ SAS No.: 4231E SDG No.: SAHOQ

Lab File ID: cBa9Q30SAli Lab Sample ID: VBLKAH____

Date Analyzed: 03/05/89 Tim* Analyzed: 0942

Matrix: (soil/water) WATER Level:(low/med) LOW

Instrument ID: 11


010203040506

EPASAMPLE NO.

EAW05EAW06EAW07EAW08EAW10EAW11

. LABSAMPLE ID

24750S247S06247507247508247510247511

LABFILE ID

CR047505B11CR047506A11CN047507A11CR047508B11CN047510B11CN047511B11

TIMEANALYZED

164412501121173215581811

COMMENTS: CLP , , , , , , ,PIST,BLANK,TUNE: 0011 030589 0709

page l of lFORM IV VOA 1/87 Rev.

SQHFLE DP TO SUMMBRV


Lab Nam«: COMPUCHEM IABS______ Contract: SAS4231E

Lab Cod«: CQMPU Cai* Ho.: QQQQ SAS No.: 4231E SDG No.: EAWQQLab File ID: ccaqosQSBii Lab Sanpl* ID: VBLKXI____

Data Analyzed: 03/08/89 Tim* Analyzed: 2103

Matrix: (soil/watar) WATER I*v«l:(low/a«d) LOW

Instrument ID: 11



0102030405060708091011

EPASAMPLE NO.

EAW09REEAW12EAW13EAW14EAW15EAW16EAW17EAW18EAH19EAW09REMSEAW09REMSD

LABSAMPLE ID

247509247512247513247514247515247516247517247518247519247499247500

LABFILE ID

C2R47509C11CN047512B11CR047513C11CN047514C11CN047515C11CN047516B11CN047517C11CN047518C11CN047519B11CN047499C11CN047500C11

TIMEANALYZED

04072353003501200205223202440324215204530552

page 1 of 1FORM IV VGA 1/87 R«v.

SQMPLE SUMMPRY


EPA SAMPLE MO.

Lab Name: CQMPUCHEM LABS__________

Lab Code: CQMPU Case No.: OQQQ


Sample wt/vol: 20.Q (g/mL) ML


% Moisture: not dec. __


VBLKXGContract: SAS4231E


CAS NO. COMPOUND

Lab Sample ID: VBLKXQ

Lab File ID: CC89Q302B11

Date Received:

Data Analyzed: 03/02/89i.O

Dilution Factor:


74-87-3——————Chloromethane_________74-83-9——————Bromomethane__________75-01-4——————Vinyl Chloride________75-00-3——————Chloroethane__________75-09-2———-——Methylene Chloride_____67-64-1——————Acetone_____________75-15-0———————Carbon Bisulfide75-35-4———————1,1-Dichloroethene______7 5-34-3 —————-l, l-Dichloroethane_____540-59-0——————1,2-Oichloroethene (total).67-66-3——--——Chloroform___________107-06-2—————-1,2-Dichloroe thane______78-93-3——————2-Butanpne___________71-55-6——————l, 1,1-Trichloroethane____56-23-5———————Carbon Tetrachloride____108-05-4—————Vinyl Acetate_________75-27-4—•———-Bromodichloromethane____78-87-5—————-1,2-Dichloropropane_____10061-01-5————ci»-l,3-Dichloropropene__79-01-6—————-Trichloroethene________124-48-1™———Dibromochlorome thane____79-00-5——————1,1,2-Trichloroethane___71-43-2—————-Benzene_____________10061-02-6-™—-Tr«M-l,3-Dichloropropene_75-25-2--™——Bromoform___________108-10-1—————4-Methyl-2-Pentanone____591-78-6————2-Hexanon«___;_______127-18-4————-Tetrachloroethene______79-34-5——————1,1,2,2-Tetrachloroethane__108-88-3————---Toluene_____________108-90-7——-—-Chlorobenzene_________100-41-4—————Ethylbenzene__________100-42-5—————Styrene_____________1330-20-7————Total Xylene*_________107-02-8—————Acrolein____________107-13-1—————Acrylonitrile_________

l0.80.912610.90.90.90.9141111111111121110.910.91122026


SPHPLE DO TO SUMHBKY 14

1£VOLATILE ORGANICS ANALYSIS DATA SHEETTENTATIVELY IDENTIFIED COMPOUNDS

EPA SAMPLE NO,

Lab Nam«: COMPUCHEM L A B S _ _ _ _ _

Lab Coda: CQMPU Cas* No.: OQQO

Matrix: (soil/wat«r) WATERSamplf wt/vol: 20.Q (g/mL) ML

L«v«l: (low/mad) LOW% Moi»tura: not dec. ___


Numbar TICs found: Q

VBLKXGContract: SAS4231E

SAS NO.: 4231E SDG No.: EAWOQ

Lab Saapla ID: VBLKXC

Lab Fil« ID: CC8903Q2B11

Date R«c«iv«d: ______

Data Analyzed: 03/02/89l& -Dilution Factor: A-*- -U1 3 o-

CONCENTRATION UNITS:(ug/L or ug/Kg)



SQHPLE DO TO SUHMQBV


EPA SAMPLE NO.

Lab Man*: COMPUCHEM LABS________

Lab cod«: COMPU Ca»« No.; QQQO

Matrix: (soil/watar) WATER

Sampla wt/vol: 20.Q (g/mL) ML

L*v«l: (low/mad) LOW

% Moistura: not d«c. __..Column: (pack/cap) PACK

VBLKSJContract: SAS4231E


Lab Sanpla ID: VBLKSJ

Lab Fll« ID: CB89Q3Q3A11

Data Rac«iv«d:

Dat* Analyzed: 03/03/89(,C

Dilution Factor: V-; 3-/5 j"'fl

CAS NO. COMPOUNDCONCENTRATION UNITS:(ug/L or ug/Kg) uc/L

74-87-3 —————74-83-9 —————75-01-4 —————75-00-3 —————75-09-2 —————67-64-1 —————75-15-0 —————75-35-4 —————75-34-3 —————540-59-0————67-66-3 —————107-06-2 ————78-93-3 —————71-55-6 —————56-23-5 —————108-05-4 ————75-27-4 —————

—— ChlorooMthana— - Bromoma than*——Vinyl Chloride-— Chloroathana—— Mfltbylan* Chloride—— Actton*——Carbon Di»ulfid«—— 1 f l-Dichloro*than«—— 1 , l-Dichloro«than«—— l,2-Dichloro«th«n« (total) __——Chloroform—— 1 . 2-Dichloro«than«—— 2 -But anon*—— 1 . 1 . l-Trichloro«than«—— Carbon Tatrachlorida—— Vinyl Acatata—— Bromodichlorom«than«

10061-01-5-— —— -ci«-l . 3-DichloroDroo«na79-01-6 —————124-48-1 ————79-00-5 —————71-43-2 —————10061-02-6—— -75-25-2 ————108-10-1 ————591-78-6 ————127-18-4 ————79-34-5 —————108-88-3 ————108-90-7 ————100-41-4 ————100-42-5 ——— -1330-20-7 ———107-02-8 ————107-13-1 ————

— -Trichloro«th«n«—— DlbroBochl oroinathana—— 1 P 1 t 2-Trichloro*than«

—— Trans-1, 3-Dichloroprop«n«-"BroMOforn—— 4-Mathyl-2-P«ntanon«——2 -Haxanona-— T«trachloro«th«n* "" '-— 1 ,1,2, 2-T«trachloro«than«—— Toluan*— -Chlorob«nz«n«—— Ethvlb*nz«n«—— Styran*—— Total Xvlanaa—— Acrolain—— Acrylonitriltt m

10.80.911210.90.90.90.9141

' 111111111121110.910.91122026

Uu •UUJUUUUUUUUUUUUUUUUUUUUUUUUUUUUUUU


S8MPLE OffTff SUHHPRV 11


EPA SAMPLE NO

VBLKSJLab Nam«: COMPUCHEM LASS________ Contract: SA54231E

Lab Cod«: COMPU Cas« No.: OQQQ SAS No.: A231E SDG No.: EAWOO

Matrix: (soil/wat«r) WATER

Sampl* wt/vol: 20.0 (g/mL) ML

L«vttl: (low/mad) LOW




Lab Sample ID: VBLKSJ

Lab Fila ID: CB89Q303A11

Data R«c«iv«d: ________

Dat* Analyzed: 03/03/89

Dilution Factor:


CAS NUMBER COMPOUND NAME RT EST. CONC/ Q

FORM I VOA-TIC 1/87 Rav.

SfiHPLE O8T0 SUHHQRV 10


EPA SAMPLE NO.

Lab Nam«: CQMPUCHEM LABS________

Lab Cod*: CQMPU Gas* Ho.: QQOO

Matrix: (aoil/wat*r) WATER

Sampl*. wt/vol: 20.Q (g/mL) MLL*v*l: (low/m*d) LOW

% Moi»tur«: not d*c. ___„


CAS NO. COMPOUND

VBLKAOContract: SAS4231E


Lab Sampl* ID: VBLKAQLab Fil* ID: CB890304A11

Dat* R*c*iv*d: ______

Dat* Analyzed: Q3/Q4/89

Dilution Factor :


74-87-3——————Chloromthan*_________74-83-9——————BroBomthan*__________75-01-4——————Vinyl Chlorid*________75-00-3————«-chloro«tban*_________75-09-2————«M*thyl*n« Chlorid*_____67-64-1——————Ac*ton*_____________75-15-0—————-Carbon Diaulfid*_______75-35-4——————l,l-Diehloro*th*n*_____75-34-3———————l,l-Dichloro*than*______540-59-0——————l,2-Dichloro«th*n« (total).67-66-3——————Chloroform___________107-06-2——————l,2-Dichloro«than*______78-93-3——————2-Butanon*___________71-55-6———————1,1, l-Trichloro*than*____56-23-5——————Carbon T*trachlorid*____108-05-4—————Vinyl Ac«tat*_________75-27-4—-------Bromodichlorom* than*____78-87-5——————1,2-Dichloropropan*_____10061-01-5————ci«-1.3-Dichloroprop*n*79-01-6———•—'-Trichloro*th*n*_______124-48-1—™---Dibromochlorom*than*____79-00-5———————l,l,2-TTichloro*than*____71-4 3-2 ————————B*ni*n*_________________10061-02-6———-Tran«-l,3-Dichloroprop*n*_75-25-2——————Bromoform___________108-10-1—————4-K«thyl-2-P*ntanon*____591-78-6—————2-H*xanon*___________127-18-4—————T*trmchloro*th*n*_______79-34-5——————1,1,2,2-T*trachloro*than*_108-88-3————-TolU*n*_______________108-90-7—————'Chlorob*nz*n«_________100-41-4—————Ethylb«nz«n*__________ioo-42-5—————styr*n«_____________1330-20-7————Totml Xyl*n*«_________107-02-8—————Acrol«in_______•107-13-1—————Acrylonitril*_________

i0.80.912210.90.90.90.9141111111111121110.910.91122026


SAMPLE DOTf9 SUMMQRV


EPA SAMPLE NO.

Lab Name: CQMPUCHEM L A B S _ _ _ _ _

Lab Code: COMPU Case Ho.: QQQQMatrix: (soil/water) WATERSample vt/vol: 20.Q (g/rnL) ML

Level: (low/med) LOW% Moisture: not d«c. ___



VBLKAOContract: SAS4231E


Lab Sample ID: VBLKAO

Lab File ID: CB89Q304A11

Date Received: ______

Date Analyzed: Q3/Q4/89/.C

Dilution Factor: -4-rfr- C&3-<>~


CAS NUMBER COMPOUND NAME RT EST. CONC. Q

FORM I VOA-TIC 1/87 Rev,

SOHPLE OffTff SUHHPPV


EPA SAMPLE NO.

Lab Nan*: COMPUCHEM LABS_________

Lab Coda: COMPU Casa No.: OQQQ

Matrix: (soil/wat«r) WATERSampla wt/vol: 20.Q (g/mL) ML




VBLKARContract: SAS4231E

SAS NO.: A231E SDG No.: EAWQQ

CAS NO. COMPOUND

Lab Sampla ID: VBLKAR

Lab Fil« ID: CB89Q3Q5A11

Data Racaivad: __ _


Dilution Factor:


74-87-3 ———— -74-83-9 ———— •75-01-4 ———— -75-00-3 ———— •75-09-2 —— -—67-64-1 ———— »75-15-0 ———— -75-35-4 ———— -75-34-3 ———— •540-59-0 ——— -67-66-3 ———— •107-06-2 ——— •78-93-3 ———— •71-55-6 ———— -56-23-5 ———— •108-05-4 ——— -75-27-4 ———— •78-87-5 ———— •10061-01-5 — •79-01-6 ———— •

79-00-8————71-43-2 ———— -10061-02-6 — •75-25-2 ———— -108-10-1 ——— -591-78-6 ——— -127-18-4 ——— -79-34-5 ———— -108-88-3 ——— -108-90-7 ——— -100-41-4 ——— •100-42-5 ——— •1330-20-7 —— •107-02-8 ——— -107-13-1 ——— -

- —— Vinyl Chlorida

— — Ma thy 1 ana Chlorida— -Acatona

— — 1 , 2-Dichloroathana (total) __

— — 2-Butanona— — 1 . 1 . l-Triehloroathana——— Carbon Tatrachlorida. —— Vinyl Aeatata

— — -eim-1 f 3-Diehloropropana ,

—— -Banaana

—— -Toluana—— -Chlarabanzana mm

«— Stvrana.-..Total Xylanaa—— -Acrolain—— Aerylanitrila

10.80.912210.90.90.90.9141111111111121110.910.91122026

UU "UUUUUUUUUUUUUUUUUUUUUUUUUUUUUUU .UUU

FORM I VOA 1/87 Rav,

SRHPLE DffTff SUHHOffV


EFA SAMPLE MO,

Lab Nan*: COMPUCHEM L A B S _ _ _ _ _

Lab Coda: COMTO casa No.: QOQQMatrix: (aoil/watar) WATERSample wt/vol: 20.Q (g/mL) ML


% Moiatura: not dac. __


Number TIC» found: _0

VBLKARContract: SAS4231E

SAS No.: 4231E SDG No.: EAWOO

Lab Sampla ID: VBLKAR

Lab Fila ID: CB890305A11

Data Racaivad: ______


Dilution Factor:


CAS NUMBER COMPOUND NAME RT EST. CONC-- Q

FORM I VOA-TIC 1/87 Rav,

S0HPLE DP TO SUMH0RY 4


EPA SAMPLE NO.

VBLKXILab Nama: COMPUCHEM LABS________. contract: 5AS4231E

Lab Coda: COMPU Ca«a No.: QQOO SAS No.: 4231E SDG No.: EAWOQ

Matrix: (soil/watar)' WATER

Saapla wt/vol: 20.Q (g/mL)



Lab Sampla ID: VBLKXI

Lab Fila ID: CC890305B11

Data Racaivad:


CAS NO. COMPOUND


Dilution Factor:


74-87-3——————-Chloro««than«________74-83 -9——————Bro»omathana__________75-01-4——————Vinyl Chlorida________75-00-3——————Chloroathana__________75-09-2——————M«thyl«n« Chlorida_____67-64-1——————Acaton*_____________75-15-0——————Carbon Di»ulfida_______75-35-4———————l,l-Diehloro«thana______75-34-3———————1, 1-Dichloroathana______540-59-0—————1,2-Dichloroathana (total)67-66-3—-———-Chlorofora__________107-06-2——————1,2-Dichloroathana______78-93-3———————2-Butanona____________71-5 5-6———————1,1, l-Trichloroathan«____56-23-5——————Carbon Tatrachlorida____108-05-4-—™—Vinyl Acatata_________75-27-4——————Broaodichloromathana____78-87-5—-————1,2-Dichloropropan*_____10061-01-5——-~-ci»-l,3-Dichloroprop«na__79-01-6——•———Trichloroathana_______124-48-1—————Dibroaochloronathana____79-00-5——————1,1,2-Trichloroathana___..71-43-2—————Baniana_____________10061-02-6———-Tran«-l,3-Dichloroprop«n«_75-25-2——————^Bro«ofpn«______________108-10-1——————4-M»thyl-2-P«ntanon«____591-78-6————-2-H«X«non*_____________127-18-4—————Tatrachloroathana______79-34-5———-——l,l,2,2-Tatrachloroathana_108-88-3——————Toluww_______________108-90-7 —————Chlorobanzana_________100-41-4—————Ethylbansana__________100-42-5—————StyrttMt_____________1330-20-7—————Totml Xylanaa_________.107-02-8—————Acrolain____________107-13-1—————Acrylonitrila_________

10.80.912210.90.90.90.914'1111111'111121110.910.91122026

FORM I VOA 1/87 Rav.

SffMPLE DffTff SUMM88V


EPA SAMPLE NO


Lab Code: CQMPU Case No.: QQOQ

Matrix: (soil/water) WATERSample wt/vol: 2Q.Q (g/mL) ML


% Moimture: not dec. __..


Number TICs found: _fl

VBLKXIContract: SAS4231E

SAS NO.: 4231B SDG No.: EAWQQ

Lab Sample ID: VBLKXILab File ID: CC89Q305B11


Date Analyzed: 03/QS/89/.O

Dilution Factor:


GAS NUMBER COMPOUND NAME RT EST. CONC, Q

FORM I VOA-TIC 1/87 Rev

SBMPLE OffTf) SUMMPRV


EPA SAMPLE HO.

Lab Name: CQMPUCHEM LABS________

Lab Code: CQMPU Case No.: QOQQ

Matrix: (soil/water) WATERSample wt/vol: 20.0 (g/mL) ML






CAS NO. COMPOUND

Lab Sample ID: 247504____

Lab File ID: CNQ475Q4A11



Dilution Factor:CONCENTRATION UNITS:(ug/L or ug/Kg) PG/L

74-87-3—————-Chloroaethane_________74-83-9———————BroBOBethane___________75-01-4——————Vinyl Chloride________75-00-3——————Chloroethane__________75-09-2——————Methylene chloride_____67-64-1——————Acetone_____________75-15-0——————Carbon Disulfide_______75-35-4——————-1,1-Dichloroethene______75-34-3——————-1,1-Diehloroethane______54 0-59-0—————1,2-Diehloroethene (total),67-66-3——«.«.- chloroform__________107-06-2——————Ir2-Dichloroethane______78-93-3——————2-Butanone___________71-55-6——————1,1,1-Trichloroethane___56-23-5——————Carbon Tetrachloride____108-05-4—————Vinyl Acetate_________75-27-4——————Broaodichloromethane____78-87-5-——•——1,2-Dichloropropane_____10061-01-5———-ci»-l,3-Dichloropropene__79-01-6——————Trichloroethene________124-48-1-—-——Dibroaochloromethane____79-00-5—-—-—-1,1,2-Trichloroe thane___71-43-2——————Ben»ene_____________10061-02-6———Tr«n»-l,3-Dichloropropene_75-25-2——————Bromofoni____________108-10-1—————4 tothyl-2-Pentanone____591-78-6™—-—2-Hexanone___\________127-18-4 ————Tetrachloroethene______79-34-5———————1,1,2,2-Tetrachloroethane_108-88-3—————Toluene_____________108-90-7—————Chlorobenzene_________100-41-4—————Ithylbenxene__________100-42-5—————styrene____________1330-20-7—————Total Xylenes__________107-02-8—————Acrolein____________107-13-1—————Acrylonitrile_________

10.80.912210.90.90.90.9140.71111111111211a0.910.91122026

FORM I VOA 1/87 Rev,

S0HPLE OP TO SUHH8RY


EPA SAMPLE NO.

Lab Nan*: CQMPUCHEM LABS_________

Lab Coda: CQMPU Ca«« No.: QQOQ


Sanpl* vt/vol: 2Q.Q (g/mL) ML

L«v«l: (1ow/m«d) LOW



Nuab«r TICs found: _1


SAS NO.: 4231B SDG No.: EAWQQ

Lab Sampl« ID: 2475Q4

Lab Flltt ID: CNQ475Q4A11

Dat« R«c«iv«d: Q3/Q1/89

Data Analyzed: Q3/Q4/89

Dilution Factor: 4?fri.O Qb 3

CONCENTRATION UNITS:(ug/L or ug/Kg)

CAS NUMBER

1.

COMPOUND NAME

FREON

RT

3.23

EST. CONC-

2.0i

QXf

Wip


SOHPLE M9T0


EPA SAMPLE MO.

Lab Nam«: CQMPUCHEM LABS_________

Lab cod«: CQMPU Ca*« No.: QQQQMatrix: (soil/watar) WATER



% Moiatura: not dac. ___




CAS NO. COMPOUND

Lab Sampla ID: 247SQS_____

Lab Fila ID: CRQ475QSB11



Dilution Factor: 4 rtf- i.C y? ^

CONCENTRATION UNITS:(ug/L or ug/Kg) UG/L Q

74-87-3————-Chloroaathana_________74-83-9——————Bromonathana__________75-01-4——————Vinyl Chlorida________75-00-3——————Chloroathana__________75-09-2——————Mathylana Chloride_____67-64-1———————Acatona_______________75-15-0——————Carbon Diaulfida_______75-35-4———————l,l-Dichloro«th«n«______

I 75-34-3——-——1, l-Dichloro«thari«_____j 540-59-0——————l,2-Dichloro«th«n« (total).

67-66-3——————Chloroform___________107-06-2————-l,2-Dichloro«than«_____78-93-3———————2-But*non«____________71-55-6—————-1,1, l-Trichloro«than«____56-23-5——————Carbon T«trachlorid«____'.108-05-4—————Vinyl Ac«tat«_________75-27-4——————Bromodichloron»than«____78-8 7-5 —————— 1,2-Dichloropropan«_____10061-01-5———ci«-l,3-Dichloroprop«n«__79-01-6—————Trichloro«th«n«________124-48-1————-Dlbro»ochlorom«than«____79-00-5———————1,1,2-Trichloro«than«___71-43-2—————B«n»«n«_______________10061-02-6———Tran«-l,3-Dichloroprop«n«_75-25-2-—————Bromoform____________108-10-1—————4-ltothyl-2-P«ntanon«____591-78-6-————-2-H«eanon«___________127-18-4—————T«trachloro«th«n«______79-34-5———————1,1,2,2-T«trachloro«than«_108-88-3—————Tolu«n«_____________108-90-7————-Chlorob«nz«n«_________100-41-4—™—Ethylb«nz«n«__________100-42-5—————Styr«n«_____________1330-20-7—————Total Xyl«n«»__________107-02-8—————Acrolain_____________107-13-1—-———-Acrylonitrila_________

l0.80.914210.90.90.90.9140.6111111111121170.910.91122026

FORM I VOA 1/87 Rav

SQHPLE OffTP


EPA SAMPLE NO

Lab Namft: COMPUCHEM LABS__________

Lab Coda: CQMPU Cai« No.: QQQO


Sanpla wt/vol: 20.Q (g/mL) ML

L«val: (low/m«d) LOW

% Moi»tur«: not dac. ___


Numbar TICa found: _0



Lab Saapl* ID: 247505____

Lab Fll« ID: CRQ475Q5B11

Data R«c«iv«d: 03/01/89

Data Analyzed: 03/05/89Dilution Factor:


CAS NUMBER COMPOUND NAME RT EST.


SAMPLE D0T0 SUHHfUiY


EPA SAMPLE NO

Lab Nam*: COMPUCHEM tABS Contract: SAS4231EEAH06

Lab Code: COMPU CaM No.: OQQQ SAS NO.: 4231E SDG NO.: EAWQO.


Sampl* wt/vol: 1.7 (g/mL) MLLaval: (low/mad) LOW

t Moistura: not d«c. _____


Lab Sampl* ID: 247SQ6_______

Lab Fil« ID: CRQ475Q6A11

Data R«c«iv«d: 03/01/89

Dat* Analyzed: Q3/QS/89

Dilution Factor:

W

CAS NO. COMPOUNDCONCENTRATION UNITS:(ug/L or ug/Kg) UG/L

74-87-3—-————Chlorom«than«_________74-83-9——————Broao-Mthana__________75-01-4——————Vinyl Chlorid*________75-00-3—————Chloro*than«_________75-09-2——————Mathylana chloride_____67-64-1—————ACtttOZM_________________75-15-0——————Carton DUulfid*_______75-35-4——————l,l-Dichloro«th«n«_____75-34-3——————l,l-Dichloro«than«_____540-59-0————— l,2-Dichloro«th«n« (total)67-66-3—————Chloroform____________________107-06-2——————1,2-Dichloro«than«______78-93-3—————-2-Butanon«___________71-55-6———————1,1,1-Tr ichloro«than«___56-23-5——————Carbon T»trachlorid«____108-05-4—————Vinyl Acatat*_________75-27-4—————Bro«odichlorom«than«____78-87-5———-——l,2-Dichloropropan«_____10061-01-5-———ci»-l,3-Dichloroprop«n«__79-01-6——————Trichloro«th«n«_______12 4 -4 8-1————Dibro»ochlorom«than«____79-00-5—————l,l,2-Trichloro«than«____71-4 3 -2 ———™- B*nxan*_______________10061-02-6———Tran»-l,3-Dichloroprop«n«_75—25—2————v—BfOBOfors____________108-10-1-————4-M«thyl-2-P«ntanon«____591-78-6————-2-H«xanon«___________127-18-4—————T«trachloro«th«n«______79-34-5———————l,l,2,2-T«trachloro«than«_108-88-3——————TolUWM_________________108-90-7—-———Chlorob*nz*n«_________100-41-4—————Ethylb«nz«n«__________100-42-5—————StyraiM_____________1330-20-7—————Total Xyl«n*«_________107-02-8————-Acrolain____________107-13 -i—————Acryionitr ila_________

169111216201311119011225026012141315145601413191418141642010570113512200240310

c

FORM I VOA 1/87 R«v,

SBHPLE DOT* SUt*H**V


EPA SAMPLE NO

Lab Nam«: CQMPUCHEM LABS________Lab Cod«: CQMPU Ca»« No.: QQQQ

Matrix: (soil/water) wATgg

Sampl* vt/vol: 1-7 (g/mL) ML






SAS NO.: 4231E SDG NO. : EAjfOO

Lab Samplft ID: 247506

Lab Fil« ID: CRQ47506A11

Dat« R«c«iv«d: Q3/Q1/89


Dilution Factor:

CONCENTRATION UNITS(ug/L or ug/Xg)


FORM I VOA-TIC 1/87 R«v

S0HPLE SUHH0RV


EPA SAMPLE NO.

Lab Kama: COMPUCHEM T A B S _ _ _ _

Lab Coda: CQMPU caaa Mo.: 0000Matrix: (soil/vatar) WATERSample vt/vol: 20.Q (g/mL) ML

Laval: (low/mad) LOW% Moistura: not dac. __„Column: (pack/cap) PACK

EAW07Contract: SAS4231ESAS NO.: 423IE SDG NO.: EAWOO

CAS NO. COMPOUND

Lab Sanpla ID: 247507Lab Pila ID: CN047SQ7AH


Data Analyzad: Q3/QS/89Dilution Factor: «*ra I.L Ote

CONCENTRATION UNITS:(ug/L or ug/K9) UC/L

74-87-3—————Chloromathana_________74-83-9——————Bromomathana__________75-01-4——————Vinyl Chlorida________75-00-3——————Chloroathana__________75-09-2——•———Mathylana Chlorida_____67-64-1—————-Ac«ton«______________75-15-0——————Carbon Disulfida_______75-35-4———————1,1-Dichloroathana______75-34-3——————1,1-Dichloroathana_____540-59-0—————1,2-Dichloroathana (total)67-66-3——————Chloroform___________107-06-2—————1,2-Dichloroathana_____78-93-3——————2-Butanona___________71-55-6——————1,1,1-Trichloroathana___56-23-5-—-———Carbon Tatrachlorida____108-05-4—————Vinyl Acatata_________75-27-4——————Broaodichloronathana____78-87-5—————1,2-Dlchloropropana_____10061-01-5———ci«-l,3-Dichloropropana__79-01-6—————-Triohloroathana_______124-48-1————- Dibroaochloromathana____79-00-5——————1,1,2-Trichloroathana___71-43-2—————-Banxana_____________10061-02-6———Trww-1,3-Dichloropropana_75-25-2—————Broaofon__________108-10-1—————4-M«thyl-2-Pantanona____591-78-6—————2-H«t*nona____________127-18-4—————Tatrachloroathana______79-34-5——————1,1,2,2-Tatrachloroathana_108-88-3———™Toluana_______________108-90-7—————Chlorobanzana_________100-41-4————-Ethylbanzana__________100-42-5—————Styrana_____________1330-20-7———™Totml Xylanaa_________107-02-8—————Acrolain____________107-13-1—————Acrylonitrila_________

10.80.412210.90.90.60.91411111121111211

110.910.91122026


SIMPLE D0T0 SUHH0XV


EPA SAMPLE NO,

Lab Nam«: CQMPUCHEM LASS________

Lab Cod«: CQMPU Cas* No.: 0000


Sampla wt/vol: 20.o (g/mL) MLL«v«l: (low/mad) LOW



Number TICs found: Q



Lab Sanpl* ID: 247SQ7____

Lab Fil« ID: CNQ47SQ7A11

Dat* R«c«iv«d: 03/01/89

Data Analyzed: oa/os/aa

Dilution Factor:

CONCENTRATION UNITS(ug/L or ug/Xg)

CAS NUMBER CONFOUND NAME RT EST. CONC.


SBHPLE 00 TO SUKHOKV


EPA SAMPLE HO.

Lab Name: CQMPUCHEM LABS________Lab Coda: CQMPU Ca*a Mo.: QQOQ


Sanpl* vt/voi: 19.a (g/mL) ML_Laval: (low/mad) LOW

% Moistura: not dac. ___Column: (pack/cap) PACK


SA5 Mo.: 4231E SDG No.: RAWOQ

CAS NO. COMPOUND

Lab Sanpla ID: 247508

Lab Fila ID: CR047S08B11

Data R«caiv«d: 03/01/99


Dilution Factor: A-Q. I C •-")&J/5-


74-87-3 —————74-83-9 —————75-01-4 —————75-00-3 ——— —75-09-2—————67-64-1 —————75-15-0 —————75-35-4 -----75-34-3— ———540-59-0 -----67-66-3 —————107-06-2 -----78-93-3 —————71-55-6 —— ——56-23-5 ————108-05-4 ————75-27-4—————78-87-5 — ———10061-01-5 ——79-01-6 —————124-48-1 ————79-00-5 —————71-43-2 —————10061-02-6——75-23-2 ————108-10-1 ————591-78-6 ————127-18-4 ————79-34-5 —————108-88-3 ————108-90-7- ———100-41-4 ————100-42-5 ————1330-20-7- ——107-02-8 ————107-13-1 ————

—— Chloroaathan*—— BroBOMthana— -Vinyl Chloride— -Chloroathana . ,— - M«thvl«n« Chloride—— Aeatona——Carbon Dimulfida«-l . l-Dichloro«th«n«—— 1, 1— Dichloroathana—— l,2-Dichloro*th*n« (total) __—— Chloroform—— 1 , 2— DichloroAthana—— 2-Butanona— -1- 1. l-Trichloro«than«——Carbon T«trachlorid«——Vinyl Acatata—— Broaodichl oronatHana—— 1 t 2— Dlchloropropana— -ci«-l, 3-Diehloropropana—— Trichloro«th«na— — DibftMaochl or omathan*

— - BMZUW ,—— Tran»-l, 3-Dichloroprop«n«___— - Bromofora— -4-ltathyl-2-P«ntanon«—— 2-Haxanon*—— Tatraehl oroa than*—— 1 , 1 , 2 , 2-T*trachloro*than«— -Toluana— - CBlorobanzana—— Ethy lb«nz ana—— fityrana——Total Xvl«n««—— Acrolain—— Acrylonitr i !•

10.81122110.720.914811111321 •111211470.9300.91152127

u .UUuuuuuJuuuuuuuuuuuuuuuuuuuuu


SAHPLE DBTB SUHHORV


EFA SAMPLE NO.

Lab Name: CQMPUCHEM TABS__________

Lab Cod«: CQMPU Cas« No.: QO'oo

Matrix: (soil/wat«r) WATERSample wt/vol: 19.2 (g/aL) ML

L*v«l: (low/n«d) LOW



Number TICs found: _1

EAW08Contract: 5AS4231E

SAS No.: 4231E SDG NO.: EAWQO

Lab Sample ID: 247508___Lab File ID: CRQ47S08B11

Dat* R«c*iv*d: 03/01/89


Dilution Factor:


CAS NUMBER

1. 75-43-4

COMPOUND NAME

METHANE,DICHLOROFLUORO-


SQHPLE OPT8 SUHHQRY


EPA SAMPLE NO.

Lab Nam«: CQMPUCHEM tABS_____

Lab Coda: CQMPU Gas* No.: QQQO

Matrix: (soil/watar) WATERSampla. vt/vol: 20.0 (g/mL) ML


% Moi«tur«: not d«c. ___




CAS NO. COMPOUND

Lab Sampl* ID: 247509____

Lab Fil« ID: CNQ47SQ9C11



Dilution Factor:

CONCENTRATION UNITS:(ug/L or ug/Kg) uc/r.

74-87-3 —————74-83-9 —————75-01-4 —————75-00-3 —————75-09-2—————67-64-1 —————75-15-0 —————75-35-4—————75-34-3 ———— -540-59-0— ——67-66-3—————107-06-2 ————78-93-3 — - — -71-55-6 —————56-23-5 ————— •108-05-4-——

10061-01-5 ——79-01-6 —————124-48-1 ————79-00-5 —————71-43-2 —————10061-02-6——75-25-2 ————108-10-1 ————591-78-6 ————

108-88-3 ————108-90-7————100-41-4————100-42-5 ————1330-20-7——107-02-8 ————107-13-1 ————

—— Chloromathana—— Broaonathana—— Vinyl Chlorida—— Chloroathana-« M*thyl«n« Chlorid*- — Acatona—— Carbon Dimulfida ,,,„—— 1 , l-Diehloro«th«n*—— 1, 1-Dichloroathanfl—— l,2-Dichloro«than« (total)-•—-Chloroform—— 1 t 2— Diehloro«than«—— 2-Butanon«—— 1 . 1 . l-Trichloro«than«———Carbon Tatrachlorid*—— Vinyl Acatata—— BroBOdichl oromathana—— 1 t 2-Diehloropropan*-« elm-lr3-Diehloroprop«M—— Triehl oroathanA—— Dibromochloromathan*-«1 . 1 - 2-Trichloro«than«— — — Banuna— -Trmnfl-i, s-Dichloropropana, .....— — Braoform—— 4-M«thyl-2-P«ntanon«—— 2— Itoxanon*—— Tatrachl oro*th«n*-— 1 ,1,2, 2-T«trachloro«than« __— -Chlorob«nz«n«--- Kthylb«nzan*— -Styrana im——Total Xvlanas—— Acirola in——Aerylonitrila

10.80.512

35010.92513163823051111

450112012381

3500.9

4001901

3902026

U -UJu

uJ

E

UuuuEUuuuuEUE

UEUU

FORM I VOA 1/87 Rav.

SQHPLE Off TO SUHUBBY


EPA SAMPLE MO

Lab Nama: CQMPUCHEM LABS_______Lab Coda: CQMPU Casa No.: QQQQ

Matrix: (soil/watar) WATERSampla wt/vol: 20.0 (g/mL) ML




Nunbar TICs found: _5


SAS NO.: 4231E SDG NO.: EAWOQ

Lab Saapla ID: 247509____

Lab Fll« ID: CN0475Q9C11


Data Analyzad: Q3/Q3/B9

Dilution Factor: +r*-i.C- >'J


GAS NUMBER

1. 96-37-72. 110-54-33.4.5. 103-65-1

COMPOUND NAME

CY CLOPENTANE , METHYL-HEXANEUNKNOWNUNKNOWNBENZENE ,PROPYL-

RT

4.055.235.427.429.54

EST. CONC.

2.03.02.03.09.0

Q

JJJJJ

FORM I VOA-TIC 1/87 Rav,

SPHPLE D0T0 SUHHBRY


EPA SAMPLE NO.

Lab Nam«: COMPUCHEM LABS________

Lab cod«: coMPU cas« Ko.: QQQQ


Sample wt/vol: Q.9Q (g/mL) ML




EAW09REcontract: SAS4231E

SAS NO.: 4231E SOG No.: EAWOO

GAS NO. COMPOUND


Lab Fll« ID: C2R47509C11

Data R«c«iv«d: 03/01/89

Data Analyzed: Q3/Q6/89

Dilution Factor:


74-87-3——————chlorom«than«_________74-83-9—————-Bro«om*than«__________75-01-4——————Vinyl Chlorid*________75-00-3——————Chloro«than«__________75-09-2———————ItathylciM Chlorida______67-64-1—————-Ac«ton«_____________75-15-0——————Carbon Di»ulfid«_______75-35-4——•———l,l-Dichloro*th«n«_____75-34-3-————l,l-Dichloro«than«_____540-59-0—————1,2-Dichloro«th«n« (total).67-66-3——————chloroform__________107-06-2—————l,2-Dichloro«than«______78-93-3————————2-BUt«non«______________71-55-6--———-1,1, l-Trichloro«than«___56-23-5——————Carbon T«trachlorid«____108-05-4——-—-Vinyl Ac«tat«_________75-27-4——-——Bromodichlorom«than«____78-87-5——————l,2-Dicnloropropan«_____10061-01-5———•ci«-l,3-Dichloroprop*n«__79-01-6—-———-Trichloro«th«n«_______124-48-1————-Dibro»ochlorom«than«____79-00-5———————1,1,3-Trichloro«than«____71-43-2————————MIISWM_________________10061-02-6-™--Trmn»-l,3-Dichloroprop«n«_75-25-2—————Bro»oforM___________108-10-1—————4-ltothyl-2-P«ntanon«____591-78-6—-———2-H«canon«___________127-18-4—————-T«trachloro«th«n«______79-34-5———————1,1,2,2-T«trachloro«than«_108-88-3——————Tolu«n«_______________108-90-7————-Chlorob«nz«n«_________100-41-4—————Ethylb«n2«n«__________100-42-5—————Styr«n«_____________1330-20-7—————Total Xyl«n«»_________107-02-8—————Acrolain___________107-13-1—————Acrylonitrila_________

2917212223

820242121382024944402327242926

10002624162734263079019

1100205922340440590

U .tfUUDJDUUUDUUUDUUUUUDUUDJUUUUDUDUDUDUU


S0HPLE SUHMfUtY


EPA SAMPLE NO,

Lab Nam*: COMPUCHEM LABS

Lab Cod«: COMPU cas* No.: OQQQ

Matrix: (soil/water) WATERSample wt/vol: Q.9Q (g/mL) ML

L«v«l: (low/mad) LOW

% Moisture: not d«c. __^_

Column (pack/cap)

Nuabtr TICs found: Q

EAW09REContract: SAS4231E

SAS No.: 4231E SDG No.: EAWOQ

Lab Sampl« ID: 247S09____

Lab Pil« ID: C2R47SQ9C11

Data R«c«iv«d: 03/01/89

Data Analyzed: 03/06/89Dilution Factor: 4-r<- /. C'

CONCENTRATION UNITS:(ug/L or ug/Kg) nc/L

CA5 NUMBER COMPOUND NAME RT EST. CONC/ Q


SAMPLE &OTQ SUMH8XV

1AVOLATILE ORGAKICS ANALYSIS DATA SHEET

EPA SAMPLE NO.

Lab Nam«: CQMPUCHEM LABS________

Lab Cod«: COMPU Cas« No.: 0000

Matrix: (soil/water) WATEa

Sample wt/vol: 20.o (g/mL) ML


% Moi»tur«: not d«c. _^^


CAS NO. COMPOUND



Lab Sample ID: 24751Q____

Lab Fil« ID: CNQ4751QB11

Data R«c«iv«d: 03/01/89

Dat« Analyzed: 03/05/89Dilution Factor: 4-re-l-C c&


74-87-3———————ChloroMthan*__________74-83 -9——™---BroBom«than«__________75-01-4——————Vinyl Chlorid*________73-00-3——————Chloro«than«___________75-09-2——————M*thyl«n« Chloride_____67-64-1————————Ac«tOn«_________________75-15-0——————Carbon Di«ulfid«_______7 5-3 5-4 ——————1 , l-Dichloro«th«n«______75-34-3——————l,l-Dichloro«than«_____54 0-59-0—————-1,2-Dichloro*th«n« (total),67-66-3——————ChlerofQM _________107-06-2——————l,2-Dichloro«than«______78-93-3——————2-Butanon«___________71-55-6——————l,l,i-Trichloro«than«___56-23-5—————-Carbon T«trachlorida____108-05-4—————Vinyl Ac«tat«____;_____75-27-4——————BroBOdichloroiuthan*____78-87-5———-—-l,2-Dichloropropan«_____10061-01-5————ct»-l,3-Dichloroprop«n«__79-01-6———---- Trichloro«th«n«________124-48-1——«——Dibro»ochlorom«than«____79-00-5————™l,l,2-Trichloro«than«____71-43-2——————B«ns«n«_____________10061-02-6——--TraiW-l/S-Dichloropropana.75—25-2—————-Broaoforn ...__.....0_108-10-1-:——•——4-M«thyl-2-P«ntanon«____591-78-6—————2-H«xanon«___;_______127-18-4—————T*trachloro«th«n«______79-34-5———————1,1,2,2-T«trachloro«than«_108-88-3———————TollMIM_________________108-90-7—-———Chlorob«nr«n«_________100-41-4—————Ethylb«nz«n«__________100-42-5—————styron*____________1330-20-7————Total Xyl«n«»_________107-02-8—————Acrolttin___________107-13-1—————Acrylonitril*_________

10.80.913210.90.90.90.9141111111111121110.90.70.91122026

FORM I VOA 1/87 R*v.

SAMPLE £>QT8 42


EPA SAMPLE NO

Lab Nan*: CQMPUCHEM LABS_________

Lab Coda: COMPU Ca«« No.: OQQO

Matrix: (soil/vat«r) WATER


L*v«l: (low/m«d) LOW

% Moisture: not d«c. ___





Lab Sample ID: 247S1Q____

Lab File ID: CNQ47S1QB11

Date Received: Q3/01/89


Dilution Factor: 4-rg. 1.0 -'Jfe?


GAS NUMBER COMPOUND NAME RT EST. CONC.


SPHPLE OP TO SUHHP8V 41


EPA SAMPLE NO.

Lab Nam«: COMPUCHEM tABS____f____

Lab Coda: CQMPU Ca»« No.: QQQQ

Matrix: (aoil/watar) WATERSaopl* vt/vol: 20.0 (9/mL) ML


* Hoi«tur«: not d«c. ___


EAWllContract: SAS4231E


CAS NO. COMPOUND

Lab Sanpla ID: 247S11

Lab Fila ID: CNQ47511B11


Data Analyzad: Q3/Q5/B9

Dilution Factor:


74-87-3 ———————74-83-9 ———————75-01-4 ———————75-00-3 ———————75-09-2 —————— -67-64-1 ———————75-15-0 ———————75-35-4 ———————75-34-3 ———————540-59-0 ——————67-66-3 ———————107-06-2 ————— —78-93-3 ———————71-55-6 ———————56-23-5 ———————108-05-4 ——————75-27-4 ———————78-87-5 ———————10061-01-5 ————79-01-6 ———————124-48-1 ——————79-00-5 ———————71-43-2 ————10061-02-6 ————75-25-2 ——————108-10-1 ——————591-78-6 ——————127-18-4 ——————79-34-5 ———————108-88-3 ——————108-90-7 ————— -100-41-4 ——————100-42-5 ——————1330-20-7 —————107-02-8 ——————107-13-1 ——————

— ChloroMthan*— BroBOBathana-Vinyl Chlorida-Chloro«thana-Mathylana Chlorid*-Acaton*—Carbon Disulfid*— 1 t l-Dichloro«th«na-1 , l-Dlchloroathana-l,2-Dichloro«th«n« (total) __-Chloroform-1 t 2-Dichloro«than«

-1.1. l-Trichloro«than«-Carbon Tatrachlorida-Vinvl Acatat*-BroBodichlorom*than*•1 , 2-Dichloropropana-ci»-l , 3-Dichloroprop«n«.— Trichloroathana-DibroBOchl oroaathana— 1 f 1 , 2-Trichloro«than«

-TraiM-1 , 3-Dichloroprop«n« __-Broaofors— 4 MB*fchyl— 2— Pantanona— 2 — HAituiona— Tatraehloroathttna-1 , 1 , 2 , 2-Tatrachloro«than« ___-TolllMM— ChlorolMnz ana-Ethylbonz an*-Styrmna.....•Total Xylanaa IM-Acrolain-Acrvlonitrila

10.80.912210.90.90.90.9141111111111121110.910.91122026

U -UUuuuuuuuuuuuuuuuuuuuuuuuuuuJuuuuuu


S8HPLE Off TO SUHHtUiV


EPA SAMPLE NO,

Lab Nam*: COMPUCHEM LABS________Lab Cod«: CQMPU Cas« Ho.: QQQQ


Sampl« wt/voli 20.Q (g/mL) ML

L«v«l: (low/m«d) Low


Coluan (pack/cap) PACK

Number TICs found: Q

EAWllContract: SAS4231E

SAS NO.: 4231E SDG NO.: EAWOO

Lab Sanpl* ID: 247SH

Lab Pil« ID: CN047S11B11

Dat« R«c«iv«d: 03/01/89

Dat« Analyzed: 03/05/89

Dilution Factor:

CONCENTRATION UNITS:(ug/L or ug/Kg) IIC/L

GAS NUMBER COMPOUND NAME RT EST. CONC." Q


S0MPLE DBT0 SUHHBKY


NO.

Lab Nam«: CQMPUCHEM LABS__________

Lab Cod«: COMPU Cas* No.: QOOQ


Sampl* wt/vol: 20.Q (g/mL) ML


% Moisture: not d«c. . __


EAH12Contract: SAS4231E


CAS NO. COMPOUND

Lab Sampl* ID: 247512____

Lab Fil« ID: CN047512B11

Data R«c«iv«d: 03/01/89

Data Analyzed: 03/05/89(.0

Dilution Factor:


74-87-3————*ChlorOB*thana__________74-83-9——————BroaoMthan*_________75-01-4——————vinyl Chlorida________7 5-00-3 ——————Chloro«than«___________75-09-2——————M«thyl«n« Chlorid*_____67-64-1—————-Actton*_____________75-15-0——————Carbon Di«ulfid«______75-35-4——————l,l-Dichloro«th«n«_____75-34-3——————-l,l-Dichloro«than«______540-59-0——————1,2-Oichloro«th«n« (total)67-66-3-™———Chloroform___________107-06-2-————l,2-Dichloro«than«_____78-93-3——————2-Butanon«___________71-55-6——————1,1, l-Trichlorocthan*___56-23-5——————Carbon T«trachlorid«____108-05-4—————-Vinyl Ac»tat«_________7S-27.-4——————BroBodichloron«than«____78-87-5———————l,2-Dichloropropan«_____10061-01-5™——ci»-l,3-Dichloroprop«n«__79-01-6————Trichloro«th«n«_______124-48-1——-——Dibromochloro»«than«____79-00-5-—™——1,1,2-Trichloro«than«____71-43-2™--™-B«««l«_________________10061-02-6——-•-Tr*n«-l,3-Dichloroprop«n«_75-25-2™-™——Broaofora____________108-10-1——————4-««thyl-2-P«ntanon«____591-78-6—————-2-K«eanon«___________127-18-4————-T«trachloro«th«n«______79-34-5——.———1,1,3,2-T«trachloro«than«_108-88-3———————TolttMM_________________108-90-7—————Chlorob«nz«n*_________100-41-4—————Ethylb«nzan«_________100-42-5—————Stymi*_____________1330-20-7—————Total XylwiM_________-_107-02-8—————Acrol«in___________107-13-1—————Aerylonitril*_________

10.80.912210.90.90.90.9141111111111121110.910.9112

2026

FORM I VOA 1/87 R«V

SBHPLE SUHHBBV


EPA SAMPLE NO.

Lab Nam«: COMPUCHEM LABS________

Lab Coda: COMPU Ca«« No.: QQQQ


Sampl* wt/vol: 20.Q (g/mL) ML






SAS NO.: 4231E SDG No.: BABOO


Lab Fil« ID: CN047512B11

Data R«c«iv«d: 03/01/89


Dilution Factor:


CAS NUMBER COMPOUND NAME RT EST. CONC.-


SAMPLE OPTP SUMHBRV


;AMFEPA SAMPLE NO.

Lab Nam*: COMPUCHEM LABS________

Lab Coda: CQMPU Casa No.: QQQQ

Matrix: (soil/water) HAXEB_

Sanpl* vt/vol: 20.0 (g/mL) MLLsvttl: (low/mad) LOW

% Moi»tur«: not dac. ___




GAS NO. COMPOUND


Lab Pila ID: CRQ47513C11

Data R«c«iv«d: 03/01/89

Data Analyzed: 03/06/89/.u

Dilution Factor: .

CONCENTRATION UNITS:(ug/L or ug/K$) UG/L

74-87-3——————Chlorom«than«_________74-83-9——————BromoB*than«__________75-01-4——————Vinyl Chlorida________75-00-3——————Chloroathana__________75-09-2——————Itethylm* Chlorid*_____67-64-1——————Acatona-_____________75-15-0———————Carbon Di»ulfid«_______75-35-4——————1, l-Dichloro«than«______75-34-3——————l,l-Dichloro«than«_____540-59-0—————l,2-Dichloro«th*na (total)67-66-3———-Chloroform___________107-06-2——————l,2-Dichloro«than«______78-93-3—————-2-Butanon«______________71-55-6——————l,lfl-Trichloro«than«___56-23-5——————Carbon T«trachlorid«____108-05-4——————Vinyl Acatata__________75-27-4———™Bromodichlorom«than«____,78-87-5——————l,2-Dichloropropan«_____10061-01-5————ci»-l,3-Dichloroprop«n«__79-01-6——————Trichloro«th«n«_______124-48-1-——--Dibro»ochlorom«than«____79-00-5———————l,l,2-Trichloro«thana____71-43-2————————B*ni«M__________________10061-02-6——™Tran«-l,3-Dichloroprop«na_75-25-2——————Bromofora____________108-10-1——————4-K«thyl-2-P«ntanona____591-78-6--————2-H«xanon«___________127-18-4——™T«trmchloro«th«n«______79-34-5——————l,l,2,2-T«trachloro«than«_108-88-3—————Toluana_____________108-90-7™———Chlorob«nz«n«_________100-41-4————-Ethylb*nx«na__________100-42-5—————styr«n«_____________1330-20-7————Total Xyl«n««_________107-02-8—————Acrol«in_____________107-13-1—————Acrylonitrila_________

10.80.911210.90.90.90.9141111111111121110.910.91122026


DOTP SUHHf9*Y


EPA SAMPLE NO

Lab Nanw: COMPUCHEM LABS_________

Lab Cod«: COMPU Ca«« No.: 0000


Saapl* wt/vol: 20.Q (g/mL) ML

I*v«l: (low/m«d) LOW

% Moisture: not d«c. _____


Nunb«r TICs found: _Q



Lab Sampla ID: 247513____

Lab Fil« ID: CRQ47513C11

Data R«c«iv«d: 03/01/89

Dat* Analyzed: Q3/Q6/B9/.Q . - .Dilution Factor:



FORM I VOA-TIC 1/87 R«v

oara


EPA SAMPLE HO.

Lab Nama: CQMPUCHEM LASS_________

Lab coda: CQMPU casa No.: QQQQ


Sanpla vt/vol: 20.o (g/mL) ML


% Moiatura: not dac. ___


EAW14contract: SAS423ie


CAS NO. COMPOUND

Lab Sampla ID: 247S14

Lab Fila ID: CNQ47S14C11

Data Racaivad: 03/01/89Data Analyzad: 03/06/89

I.C

Dilution Factor:


74-87-3——————Chloromathana_________74-83-9———————BroBoaathana___________75-01-4——————Vinyl Chlorida________75-00-3——————Chloroathana__________75-09-2——————Mathylana Chlorida_____67-64-1——————Acatona_____________75-15-0——————Carbon Di«ulfid«_______75-35-4——————1,1-Dicnloroathana______75-34-3————---1,1-Dichloroathana_____540-59-0—————1,2-Dichloroathana (total).67-66-3——————Chloroform___________107-06-2—————1,2-Dichloroathana_____78-93-3——-----2-Butanona____________71-55-6——————1,1,1-Trichloroathana___56-23-5——————Carbon Tatrachlorida____108-05-4—————Vinyl Acatata_________75-27-4——————BroBOdichloromathana____78-87-5——————1,2-Dichloropropana_____10061-01-5——™ci»-l,3-Dichloropropana__79-01-6————-—Trichloroathana________124-48-1-——-—-Dibrcaochloromathana____79-00-5——————1,1,2-Trichloroathana___71-43-2——-———Banxana_______________10061-02-6——™Tran»-l,3-Dichloropropana_75-25-2————--Brettofora____________108-10-1—————4-H«thyl-2-Pantanona____591-78-6—————2-H«x*nona^________127-18-4——————Tatrachloroathana^_____79-34-5——————1» If 2,2-Tatrachloroathana_108-88-3——————Toluana_______________108-90-7—————Chlorobanzana_________100-41-4—————Ethylbanzana__________100-42-5—————styr«n«_____________1330-20-7————Total Xylanaa_________107-02-8—————Acrolain____________107-13-1—————Acrylonitrila_________

FORM I VOA

10.80.912210.90.90.90.9141111111111121110.910.9112

2026

1/87 Rav

SfMPLE SUHtWBY

Lab Namt: VERSAR INC.


________ Contract: ______

J Codt: VERSAR Cast No. : 11724 SAS No. : 4537E SDO No. : EAL62

Lab Filt ID: ' Y3263 Lab SampIt ID: VBLK65____

Datt Analyztd: 04/07/89 Ti«« Analyztd: 1323

Matrix: <*oil/uattr) WATER Ltvtl:(lou/mtd) LOW

Inttrumtnt ID: ' V


• : EPA! SAMPLE NO.01IEAL8702 ! EALS803 ! EALS904IEAL91

t

: LABt SAMPLE XD

1 69626! 69627At 69628t 69629DI

LABFILE ID

Y5266YS267YS269Y9268

TIMEANALYZED

1440152016591616 i

COMMENTS: CLP, - * VSTD20,L,W, 17503.V* CC-020. 25MLINST R: SP1000 60/80 CARBOPACK 2Mt45C > 22SCtBC/M > 3OMt225C

ag* 1 of 1FORM XV VOA 1/87 R»v.

100012

2v--; -i i*

Lab Name: VERSAR INC.


_______ Contract: _____

, Cod»: VERSAR . Cas« No. : 11724 SAS No. : 4337E SDG No. : EAL62S£L«b Fil« ID: Y9293_____ Lab Sampl* ID: VBLK93

Dat* Analyzfld: 04/11/89 Ti»« Analyzed: 14Q9

Matrix: (ioil/wat«T) WATER L«v«I:(lou/m»d) LOW

Inttrum»nt ID: Y

THIS METHOD BLANK APPLIES TO THE FOLLOWING SAMPLES* MS AND MSD:

I EPAI SAMPLE NO.

011EAL90021EAL9203JEAL9304 ! EAL96OS ! EAL9706 ! EAL83MS07 ! EAL83MSD

:

LABSAMPLE ID

6963469630A69613C69632A69633A69624C69624B

LABFILE ID

Y5299Y5294Y5298Y9296Y9297Y9300Y9301

TIMEANALYZED

18221903|7401620169919141992

.MENTS: CLP, , * VBLK93* L* W,VBLK93* V.BLANK..,23MLINST Y SP-1000 49CC3MIN) TO S29C 8C/MIN

1 of 1FORM IV VOA 1/87 R»v.

100013

%tf& ^


EPA SAMPLE

' -b Nam*: VER5AR INC. ContractVBLK49

•w*D Code: VER5AR Cas* No. : 11724 SAS No. : 4S37E SDG No. : _

Matrix: <*oil/uat*r) WATER Lab Sample ID: VBLK

Sample wt/vol; 25.0 (g/mL) HL_ L'b Fil* ID: Y5249

Lavel: (low/m*d) LOW Dat* R*c*iv*d: ____

hoisture: not dtc

Ct-iumn: (pack /cap) PACK

Datt Analgz*d: 04/06/99

Dilution Factor: g. Q I


74-87-3————————Chlorom*than»______74-83-9-—————— Bromom^than*_______^75-01-4———————Vinyl Chlorid*__________75-00-3———————Chloroethant____________75-09-2———————M* th glint Chlorid•_______67-64-1———————Act ton*________________75-15-0———————Carbon Di»ulfid*________75-35-4———————1, l-Dichloro*th*n*_______75-35-3———————li l-Dichloro»than§_______540-59-0———•———1,2-Dichlorotthtnt (total),67-66-3——-————Ch lorof orm ______107-06-2——————1* 2-Dichloroathant_______78-93-3————————2-Butanont______________71-55-6———————1, 1, l-Trichloro»than«____56-23-5——————-Carbon Tttrachlorid*.____10S-05-4———————Vingl Acatat*___________75-27-4———————Bromod i ch 1 oromathana_____7S-S7-5———————li 2-Dich loropropan*______10061-01-5———---cii-1* 3* -Dichloropropen*_79-01 -6———————-Tr i c h 1 or o* th »nm124-48-1———-—Dibromoehloroaathana79-00-5—————.——1» I/ 2-Trichloro*than*____71-43-2————————B*nz*ne_________________75-25-2——————•—Bromof orm ____;____1C5-1O-1——————4-Metny l-2-P*ntanone,_____391-7S-6———————2-Hexanon*127-19-4———————T*trachloro^th*n*'79-34r5103-8S-3————•—Tolu*n*'108-90-7——————Chlorob*nztna100-41-4———————Ethylb*nz*n*100-42-5—•—————Stur*n*1330-20-7——————Total Xgl*n*f107-02-8———————Ac r o 1 * i n107-13M——————Acrglonitril*

FORM I VOA

4!U2!U3!U2!U2!U!U

2iU0'. 08 i U0. 090. 30. 10. 110. 10. 10. 30. 20. 10. 20. 10000Q

.2q.Q6oooo73

1 !U2!U2IU1 !U21 U

0. 3 U:u

1 !U

1 !U2!U2!U;u!U

1/87 Rev.

JOO-179


EPA -SAMPLE N!

VBLK49b Name: VERSAR INC. Contract:

^dfa Code: VERSAR Cat* No. : 11724

Matrix: (soil/wat«r> WATER

Sampl* ut/vol: 25. Q (g/mL) ML

Lavel: (loui/mtd) LDU _

% Moiiture: not dec. _____



SAS No. : 4537E SDC No. :

Lab Samp It ID: VBLK

Lab Filt ID: Y5249

Datt Rtctivtd: __________


Dilution Factor: ""JrS* I


CAS NUMBER ! COMPOUND NAME

1. {UNKNOWN!

*RT :34. 01 !

!

1

EST. CONC. ! Q

o. i : j11


J.00480


ERA SAMPLE NO.

Lab Name: VER5AR INC. ContractVBLK65

J Code: VERSAR Case No. : 11724 SAS No. : 4537E SDG No. : EAL62

Matrix: < *oi 1/uater) WATER Lab Sample ID: VBLK65

Sample wt/vol: 25. Q <g/mL> ML Lab File ID: Y5265

Level: (lou/med) LOW Date Received: _______

X Moiiture: not dec. , __

Column: <pack/cap > PACK

Date Analyzed: Q4/O7/89

Dilution Factor: i. Q \


74-87-3——-——-Chloromethane74-83-9————————Bromome thane75-01-4———————Vingl Chloridt75-OO-3———————Chloroethane75-09-2———————Methglene Chloride67-64-1 ———————Ac e t one75-15-0———————Carbon Dim If ide75-35-4———————1, 1-Dichloroethene75-35-3———————1. 1-Dichloroethane540-59-0———————1,2-Dichlorotthene < total)67-66-3——————Chloroform107-06-2——————1,2-Dichloroethane7S-93-3————•———2-B u tanone71-55-6—•*—————1, 1. 1-Trichloroethane56-23-5——-————Carbon Tetrachloride10S-05-4———————Vinyl Acetate75-27-4————•——Qrofnod ich loromethane_______7B-E7-5———————I, 2-Dichloropropane10061-01-5—————ci«-l» 3*-Dichloropropene79-01-6——-———Tr i c h 1 oroethene124-48-1———————DibroiaQchlornmathana79-OO-5——-——•—— 1, 1,2-Tri Chloroethane71 -43-2———-———B e n z ene75-25-2————————Bromo-form1QS-IO-1———————4-Me thy :-2-Pen tanone591-73-6———————2-Hexanone127-13-4——————Tetrachloroethene ___•79-34-3———.—----l.»..l» 2. 2-TetT\at-hloroe.th*n8108-S8-3-—v -- Tqluen»-;-:-;-''-">"'"•• -• '^<f- ['•'>•*• v •'•' !108-90-7———————Chlorobenzene_____________1OQ-41-4———————Ethyl ben 2 ene______________1OO-42-5———————Styrene__________________1330-20-7——————Total Xylene«_____________107-02-8———————Aero 1 e in__________________107-13-1 ———————Aery 1 on i t r i 1 e_____________

0. 4!o. 2;0. 3!o. 2;0. 2!2 :0. 2!0. 08!0. 09!0. 3!0010. 1000000

1321212!2!1 !2!

0. 1!O. 2-1•O-..-Ho. i:0. 1!0. 2!0. 2!


100488



EPA SAMPLE NO.

Lab Name: VER5AR INC.

.D Code: VERSAR Cat* No.,: 11724


Samp It bit/vol: 25. 0 <g/mL> MJ

Level: Uou/mttf) LOW

7. Moisture: not dec. ^___


Number TICt found: _1

ContractVBLK63


Lab Sample ID: VBLK65

Lab File ID: Y5265

Date Received: ^_____

Date Analyzed: O4/Q7/89

Dilution Factor: -i. 0 \

CONCENTRATION UNITS:(ug/L or ug/Kg> UQ/L

CAS NUMBER

- 1.

i *i iCOMPOUND NAME ! RT !

UNKNOWN ! 13. 39 fi i

EST. CONC.

0. 3

Q

J


100489


EPA SAMPLE NC

1 ~b Name: VERSAR INC._____________

S_-*b Code: VERSAR Case No. : 11724


Sample wt/vol: 25. Q (g/mL)

Level: (lou/med) LOW

;; Moisture: not dec. ____


VBLK93Contract:

SAS No. : 4537E SDG No. :

Lab Sample ID: VBLK93

Lab File ID: Y5593

Date Received: _____

CAS NO. COMPOUND


Dilution Factor: -g_ 0 \


74-87-3————•——Ch l o r o m e t h a n * _ _ _ _ _74-83-9——-———--Bromorne t h a n e _ _ _ _ _75-01-4———————Vinyl Chloride__________73-00-3———————C h 1 or o e t hane____________75-09-2———————Methy lene Ch 1 or ide_______67-64-1—————f—Acttone________________75-15-0—————'—Carbon Ditulfid•________75-35-4———————i, 1-Dichloroethene_______75-35-3———————I, 1-Dichloroethane______540-59-0———————l, 2-Dichloroethene (total >.67-66-3———-———Ch l o r o f o r m _ _ _ _ _ .107-06-2——————1» 2-D i c h 1 or o e t h an e_______78-93-3—«————2-Butanone _______71-55-6———————1, 1, 1-Trichloroethane____56-23-5———————Carbon Te tr*c h1or i de_____10S-O5-4——————Vinyl Acetate___________75-27-4————————Bromod ich loromethane73-S7-5———————1, 2-Dich loropropane______10C61-01-5—————cic-li3.-Dichloropropene_79-01 -6———————-Tr i c h 1 or o ethene _______.124-48-1—-———Dibromo.ch loromethane79-00-5———————1, lj 2-Trichloroethane____71 —6-2-2———————Ben z ene________________"5-25-2———————Bromof orm ___________I OS-1C—I——————4-Methy 1-2-Pentanone_____591-78-6———————2-Hexanone______________127-13-4———-——Tetrachloroethene.79-34-5————*:———rlV L 2, 2-Tj|tr*feliatJf oethane..10S-88-3---- - -to'iu nV''''"-' • "'••"•'••'••"• " •"•*-"r108-90-7——————Chlorobenzene ________100-41 -4——————E t h y 1 b en z ene____________100-42-5———————Styrene_________________1330-20-7——————Total Xylenet___________107-02-8———————Aero 1 e in________________107-13-1—-—————Acruloni trile _______

O000220

0.0.0001000000000000

4!U2!U3!U2!U

1!

2!U08 I U09 !U3!U1 I U

UUUUUUUUU

21U2!Ul :u2!U3! U!U

1

..'aj.y:'iru-

. 1 !U

. 2iU

. 2JU!U!U

FORM I VQA 1/87 Rev.

J00496


ERA SAMPLE NC

Name: VERSAR INC.

-*b Code: VERSAR Case No. : 11724


Sample ut/vol: 25. Q (g/mL)




Number TICs found: 0

Contract: .

SAS No. : 4B37E

VBLK93

SDG No. :

VPLK93

Y5S93

Lab Sample ID:

Lab File ID: ______



Dilution Factor: 5. 9' \


11

CAS NUMBER t COMPOUND NAME

it

iRT ! EST. CONC.

•

Q


J00497

•• -- ••-LJ--1?--*'''-- Ll'i ••' -'- '--' in"*' i "fl* '

USEPA CONTRACT LABORATORY PROGRAM

.__V<SAMPLE MANACEMF'JT OFFICEP.O BOX 313 ALEXANDRIA. VA 22313

703 r-^7 -?4tn FTS SS7 7490

APPUCABLE)


• ,

i

•WHTTC — SMO COPY PINK - CLIENT COPY WHITE - LAB COPY POR BETUWN TO SMOJOC008YELLOW-\tA8 COPYGS£O)

1AVOLATILE ORQANICS ANALYSIS DATA SHEET

ERA SAMPLE NO.

EAL96Lab Name: VERSAR INC. Contract:

.0 Code: VERSAR Cat* No. : 11724 SAS No. : 4537E SDS No. : EAL62

Matrix: (soil/water) WATER Lab Sample ID: 69632A

Sample ut/vol: 25. Q (g/mL) HL_ 1-ab Fil» ID: Y5296

Level: (lou/med) LOW Date Received: 04/04/89

y. Moisture: not dec. ___


CA5 NO. COMPOUND

Date Analyxed: 04/11/89

Dilution Factor: *9r^- \

CONCENTRATION UNITS:(ufl/L or ug/Kg) UQ/L

— — — c h 1 or ome thane—"-— Bromome thane

Vingl ChlorideC h 1 or o e t h an eMethylene ChlorideAcetbneCarbon Ditulfide1, 1-Diehloroethene1. 1-Dichloroethane1,2-DichloroetheneC h 1 or o f orm

74—87—3 — -• —74-83—9 —— -75-01-475-00-375-O9-267-64-175-15-O75-35-4- —75-35-3540-59-067-66-3- — -107-06-278-93-3 —— -71-55-656-23-5108-05-475-27-4- —————78-87-5 ————— •1OO61-01-579-0 1 -6124-48-1- —— ——79-OO-5 ———————— 1, 1, 2-Trichloroethane71-43-2- — — ———— Benzene75-25-21 08- i 0- 159 I -73-6

(total)

1, 2-Dichloroethane2-Butanone1, 1* 1-TrichloroethaneCarbon TetrachlorideVinyl Acetat«Br oirio d i c h 1 oromethane1, 2-Dichloropropanecit-1. 3» -DichloropropeneTr i ch 1 oroetheneDibromochloroeiethane

Bromoform4-Me t h y 1 -2-P en tan one2-He xanone

127-13-4 ————— •--Tetrachloroathehe79-34-5—- — — rr-lr !•* 3» 2-Tmtrachloroethane1 08-88-3 —— - ——— ^To 1 uene ' • . - . - • .108-90-7 ——————— Chlorobenzene10O-41-4 —————— Ethylbeniene10O-42-5 ——————— Styrene1330-2O-7 —————— Total Xylene*1 07-O2 8 ——————— Aero 1 e in107-13-1 Acrylonitrile

FORM I VOA

0. 4!U0. 2!U0. 3!U

3 !0.120.

u

o. os: u0. 09 !U0. 3!U

2!U1!U2!U

0011000003 i0. 2!U0. 2!U0. 1!U0. 2!UO. 3!U2 !U

10 ' !0. 2!UC. 6! 'o. iru

11U2:u2!U

;u:u

1/87 Rev,

JU0272


EPA SAMPLE NO.

Lab Name: VER5AR INC._____________

V_ ^ Code: VER5AR Case No. : 11754

Matrix: (soil/water) UATER

Sample ut/vol: 25. Q <g/mL>




Number TIC* found: 0

Contract:EAL96



Lab File ID: YB29&



Dilution Factor: '5.0 \


GAS NUMBER

(

COMPOUND NAME•

RT 1 EST. CONC.

rQ


100273


EPA SAMPLE NO.

Lab Name: VERSAR INC. ContractEAL97

^ ., Code: VERSAR Case No. ; 11724

Mdtrix: (soil/water) UATER

Sample ut/vol: 25. O <g/mL) ML

Level: <lou/med> LOW

X Moisture: not dec. ___


C

CAS NO. COMPOUND



Lab File ID: Y5297



Dilution Factor:


74-S7-3———————Chloromethane_.________74-83-9————-——Bromomethane_______75-01-4———————Vinyl Chloride__________75-OO-3———————Chloroethane____________75-09-2———————Methylene Chloride_______67-64-1———————Acetone________________75-15-0———————Carbon Ditulfide________75-35-4———————1. 1-Di c h 1 oroeth ene_______75-35-3———————1 * 1-Di c h 1 oroethane______540-59-0——————1,2-Dichloroethene (total)67-66-3—•-—————Chloroform ________107-06-2———————1, 2-Di c h 1 oroethane_______78-93-3———————2-Butanone______________71-55-6———————1, 1. 1-Trichloroethane____56-23-5———————Carbon Tetrach 1 oride_____108-05-4———————Vinyl Acetate___________75-27-4—•—————Bromodich lor one thane7S-87-5———————1, 2-Di c h 1 oropropane______10061-01-5—————ci»-l> 3»-Dichloropropene_79-01 -6————-———Tr i c h 1 o r o e t h e n e _ _ _ _ _124-4B-1———-———Dibromochloromethane79-OO-5————————\> \> 2-Trichloroethane71-43-2———————B en z ene_______\________75-25-2——————-.-Bromof orm ________105-10-1———————4-Methyl-2-Pentanone_____591 -79-6———————2-He x anone______________127-13-4—'————Tetrachloroethene______79-34-5—————;—1* I*.;?* 2-T«trachl.orpethane_i OS-SS-3-r—•? •' ""-"To 1 u-ana-'- • • • • •.'.-..- •; •*•• •" '•..•:'''.-/-..;:.'.108-90-7——————Chlorobeniene__________100-41 -4———————Et h y 1 b en z ene____________10O-42-5———————Styrene________________1330-20-7——————Total Xylertet___________107-02-8———————A c r o 1 e i n_______________107-13-1———————Acrylonitrile___________

FORM I VOA

0.0.0.0.0.20.

4!U2!U3!U2!U2!UiU

2!Uo. 08: u0. 09 !U0. 3!U

:u:uIU

0.0.140.0.O.0.0.60.0.0.0.0.226. .0.0;0.0. 1 !UO. 2!U0. 2!U73

i :u3!U2!Ui :u2!U

II2iU2!U7!2iU3!U:.ui

2iUTHJ:1 !U

!U!U

1/87 Rev

-100293

IE rVOLATILE ORGANICS ANALYSIS DATA SHEET


ERA SAMPLE NO.

EAL97Name: VER5AR INC. Contract:

11754^ --b Code: VERSAR Case No,


Sample ut/vol: 25. 0 (g/mL) QL__

Level: <1ow/med) LOW

7. Moisture: not dec. ___

Column < p a c k / c a p ) PACK

Number TICs -found: _£



Lab File ID: Y5297

Date Received: 04/04/S9

Date Analyzed: Q4/11/89

Dilution Factor: 6r-e \ >

CONCENTRATION UNITS:(ug/L or ug/Kg) UQ/

CAS NUMBER.

COMPOUND NAMEt1

RT f" EST. CONC.

i•

Q


100294


EPA SAMPLE NO.

Name: VERSAR INC. Contract:

,D Code: VERSAR Case No.


Sample ut/vol: 25. 0 <g/mL> QL_




11724 SAS No. : 4537E SDQ No. : EAL62


Lab File ID: Y5250



Di lution Factor: 5. 6 1


74-87-3—••————-C h 1 or one t h ane__________m74-63-9—————-—Bromomethane _____75-01-4———————Vinyl Chloride__________75-00-3———————Ch 1 or oe thane____________75-09-2———————-Methylene Chloride_______67-64-1———————Acetone________________75-15-0———————Carbon Ditu 1 fide________75-35-4———————i, 1-Dichloroethene_______75-35-3———————1* 1-Dich lor ot thane_______540-59-O——————l. 2-Dichloroethene (total)67-66-3———-——Chloroform _________107-06-2——————1* 2-Dichloroethane______78-93-3———————2-Butanone _____71-55-6———————1> l, 1-Trichloroethane____56-23-5———————Carbon Tetrachloride_____108-05-4——————Vinyl Acetate__________75-27-4———————Bromodichloromethane78-87-5———————1. 2-Dichloropropane______10061-01-5—-———c i*-i» 3>-Dichloropropene_79—01—6———————-"-Trichloroethene _________124-48-1——————Dibromochloromethane79-00-5———————1* l* 2-Trichlorotth»ne____71 -43-2———————-Ben i ene _______75-25-2———————Bromof orm _________1 OS-10-1——————4-Methyl-2-Pentanone_____592-73-6———————2-Hexanone______________127-19-4—-————Tetrachloroethene_______79-34-5———:———-1,1, 2.2-TetrACh1 oroethane_lOB-.Ba-3-™— --tTQ'luan.e"••'.-'•';. '.1; '.'•' .'..'...'..; ••108-90-7——————Chlorobeniene__________100-41 -4——————E t h y 1 b en * ene____________1OO-42-5———————Sty r ene_________________1330-20-7——————Total Xylene»___________107-O2-S———————Acrolein________________107-13-1 ——————Ac r y 1 on i tr i 1 e_____;______

tu:uuuu

o. 4tu0. 2!U0. 3!U0. 2!U0. 2!U20. 2

0. 080. 090. 30. 7\"0. 1!U

UUuuuuuu

2!U2!U

10.0.0.0.0.0.0.0.0.0.0.0.20.0.

!U!U:u!U.:u,

,3.1.liUi :u2IU2!U:u:u

FORM I VOA 1/87 Rev

100311

IEVOLATILE OROANICS ANALYSIS DATA SHEET


Lab Name: VERSAR INC._____________

Q Code: VERSAR Case No. : 11724

Metric: (soil/water) WATER

Sample ut/vol: 25. Q <s/mL>

Level: (lou/med.) LOU1

X Moisture: not dec. ^__


fMumbt/r TICs found: _£

Contract:

EPA SAMPLE NO.

EDG06

Y525Q


Lab Sample ID: 6961&

Lab File ID:



Dilution Factor: 5r-9- \

CONCENTRATION UNITS:(ug/L or ug/Kfl) UQ/L

GAS NUMBER COMPOUND NAME RT : EST. CONC. i Q

O- C» j Jji'L*

CFORM I VOA-TIC 1/87 Rev.

J00312


ERA SAMPLE NO.

EDG14Lab Name: VER5AR INC,_ Contract

o Code: VERSAR Case No. : 11724 SAS No. : 4537E SDC No. : EAL62

Matrix: <soil/uat*r) UATER Lab Sample ID: 69620

Sample ut/vol: 25.Q <g/mL> QL__ Lab File ID: Y5254

Level: (1ow/med) LOW



CAS NO. COMPOUND



Dilution Factor: -3. 0 \

CONCENTRATION! UNITS:<ug/L or ug/Kg) UQ/L

74-S7-3————————Chlaromethane _____74-S3-9———-————Bromomethane ________75-01-4———————Vinyl Chloride__________75-00-3————————Chloroetha.ne____________75-09-2———————-Methylene Chloride_______67-64-1———————Acetone________________75-15-0———————Carbon Ditulfidt________75-35-4—————-—1* 1-Dichloroethene _____75-35-3———-———1 * 1 -Di c h 1 ofoettt ane______540-59-0———————1. 2-Dichloroethene <total)67-66-3————————Chloroform _______107-06-2————-——1* 2-Dichlorotth«ne_______78-93-3-———————-2-Butanone _______71-55-6———————1* 1. 1-Trichloroethane____56-S3-5———————Carbon Tetrachloride_____103-05-4———————Vinyl Acetate___________75-27-4———•————"Br omod ich lor ome thane_____73-S7-5———————1» 2-Dichloropropane______10061-01-5—————cis-1* 3» -Dichloroproperie_79-01-6————————Trichloroethena_____124-48-1———————Dibromochloromethane_____79—OO-5————————!• 1* 2—Trichloroethan*____71-43-2——-—————Beniene _______75-£?-2———————Broflioform______________iOS-iO-i——————4-Methy l-2-Pentanone____591 -78-6———————2-He x anone_________127- i 8-4—————;--Te tr a c h lor o e t'h e n e_______79-34-5———-——-1» 1... 2. a-Te-trpehlproethane^1 oS-BS-3- -1- -—-To 1 u»ne": V":'"" '... ' v';'. •' •""'.' : V .1 OS-90-7————-—Ch 1 orofaenzene _______1OO-41 -4———————E t h y 1 b en i en e ____________100-42-5———————Sturene ______1330-20-7——————Total Xylents___________107-02-8———————Ac r o 1 e i n_______________107-13-1———————Aery lonitrile____________

FORM I VOA

O. 4!U0. 2!U0. 3IU0. 2<0. 220. 2

0. 080. 090. 30. 10. 110. 10. 10.0.0.0.0.0.o.0.0.0.2o;0.o:0.0.0.0.73

uuuuuuuu-u!U

1 !U1!U3;u2!Ui :u2!U612!U2!U

;ui :02!USI '.i iui :uU2

1/87 Rev.

1U032G

IEVOLATILE QRGANICS ANALYSIS DATA SHEETTENTATIVELY IDENTIFIED COMPOUNDS

EPA SAMPLE NO.

EDO 14Lab Name: VERSAR INC. Contract:

^ Code: VERSAR Case No. ___

Matrix: (soi1/uater) MATER

Sample ut/vol: 23. Q (g/mL)




Mumber TIC* found: Q

11724 SAS No. : 4337E SDC No. : EAL62


Lab File ID: Y5234

Date Received: O4/04/89


Dilution Factor: •9. 0 \


CAS NUMBER COMPOUND NAME RT<«

EST. CONC. ! Q

.i

FORM I VOA-TIC 1/87

100327

•v <.~*---j*',",-" "-r;'- T',>' I'.'-''6?---1; ;-•• /'»3â*,5^£rvtf£)atjt"-''Oc>vAiJ?l> ':t*^:-^"--r.r^SSjrJj-tii L'J_VJ_ -y ' • J.iwii " • •' ~-*'^T>i>jfrf^yyyr\fi>jy^î,.»^^fcîly-->--j?[i'j^f^^^j-i^


ERA SAMPLE NO.

EDG151 -b Name: VER5AR INC. Contract

^ ...D Code: VERSAR Case No. : 11724


Sample wt/vol: 25.0 <g/mL) Qt__


?i Moisture: not dec. .1 __


GAS NO. COMPOUND



Lab File ID: Y3255



Dilution Factor: E. 0 1

CONCENTRATION UNITS:(ufl/L or ug/Kg) UQ/L '

74-B7-3————————Chloromethane74—83-9-————————Bromomethane75-01-4———————Vinyl Chloride75-00-3———-————Chloroethane75-09-2———————Methylene Chloride67-64-1———————Acetone____;75-15-0———————Carbon Disulfid*75-35-4———————1* 1-Dichloroethene75-35-3———————1, 1-Die hi orotthan*540-59-0———————l»2-Dichloroethene (total)67-66-3—————————Chloroform _________107-06-2—————— 1. 2-D i c h 1 oro eth ane7S-93-3———————2-Butanone71-55-6———————1» 1* 1-Trichloroethane56-23-5———————Car b on Te tr a c h 1 or i d e10S-05-4———————Vinyl Acetate75-27-4-——————-Bromod ichlorpmethane78-S7-5———————1» 2-DichloropropanelOOai-03-5—————cis-1* 3*-Dichloropropene79-01 -6————————Tr i c h 1 or o •than*124-48-1——————D i br omoc h 1 or ome thane79-00-5———————1, 1,2-Trichlorot thane7 i -43-2————————B en z ene75-25—2———:————Bromof orm_____________103-1O-1———————4-Methyl-2-Pentanone591-78-6————————2-Htxanone ______- ..127-13-4-^——r-—Tetracbloroethene79-34-5————:---li -li^. 2-Tetrachloroethane1OB-S8-3-——^y-Tolueng . '-'• '•-•'.> • . •' '.. :-.•:1 OB-90-7———-——Ch 1 or ob en z ene100-41-4———————Ethylbenzene1OO-42-5-——————Sty r ene1330-20-7——————Total Xylenet107-02-8———————Aero 1* in__________i1O7-13-1———————Aery lonitr i lt_

FORM I VOA

4!U21U3!U2!U2!Utu

2iU0. 03 !U0. 09!U0. 30. I

10.10.0.0.0.0.0.0. 1 !U0. 2!U

u;u!U:u!U:u!U:u:uIU

0.0.0.0.26.0,

0.0.0.0.73

2!U

2JU3!U

uy2!U

i :ui:u2!U2!U:u;u

1/B7 Rev.

100338


ERA SAMPLE NO.

Lab Name: VERSAR INC. Contract:EDO 15

11724j Code: VERSAR Case No.


Sample ut/vol: 23. Q (g/mL) ML


7, Moitture: not dec. __


Number TIC* found: _Si



Lab File ID: Y3233



Dilution Factor: "5. Q \


CAS NUMBER COMPOUND NAME RT EST. CONC.f

Q


100339

^


ERA SAMPLE NO.

Lab Name: VERSAR INC

( , Code: VERSAR

ContractEDO 16

______ Case No. : 11724 SAS No. : 4537E SDS No. : EAL62

Matrix: (soil/water) UATER Lab Sample ID: 69622

Sample wt/vol: 25. Q <g/mU> flL,_ Lab File ID: Y5256

Level: Uou/med) LOU Date Received: 04/04/89

X Hoiiture: not dec.


Date Analgzed: Q4/07/89

Dilution Factor: -fr-6

C


74-87-3————-——Chloromethane______74-83-9-——————Bromome t h a n e _ _ _ _75-01-4———————Vinyl Chloridt__________75-00-3———————Chloroethane ________75-09-2———————Methylene Chloride_______67-64-1————————Acetone ____75-13-0———————Carbon D i * u 1 f i de________75-35-4———————1* 1-Dichloroethen-e_______75-35-3———————1, 1-Dichloroethane______540-39-0———————1* 2-Dichloroethene <total)67-66-3————————Chloroform ______107-06-2———————1,2-Dichlorotthane_______78-93-3———————2-Butanone____,_________71-55-6———————1> 1* 1-Trichlorotthane____56-23-5———————Carbon Tetrachloride_____10S-05-4———————Vinyl Acetate___________75-27-4———•————Bromod i c h 1 or omethan*______7S-E7-5———————1. 2-Dich lor o propane,._____10061-01-5—————cis-1.3i-Dichloropropene_79—01 -6———•————Tr i c h 1 or oe t h ena________124-48-1———————Dibromochlororotthane_____79-00-3———————1. 1> 2-Trichloroethane____71-42-2———-————Benzene _______^^S-SS-S————————Bromoform_______________1 OS-10-1 ——————4-Me t h y 1 -2-P ent anone_____59.1-78-6————————2-Hexanone ___________127-13-4—•-:———-Tetrachiproethene_______79-34-5———————!,-!> 2.* 2-T*trachloroethane_108-88-3——TT—r- T.oIuari'a!.-..' . .'"' '•'••.• -V. ' ' ' -.1 OS-90-7——————-Ch 1 or ob en z ene ______100-41 -4———————Et h y 1 b en z ene____________100-42-5——————Sty r ene________________1330-20-7——————Total Xylenti___________107-02-8———————Acrolein________;________107-13-1 ———————Aery 1 on i tr i 1 e____________

0. 4O. 2000

!U;u

3!U2!U2!U

20. 2

0. 080. 090. 30. 10. 110. 10. 1

:u:u:u:u;u:u!U!U

0.0.0.0.0.0.0.0.0.0..20.0.

0.0.0.0.73

1!U3!U2iU1 !U2!Ul i U2!U2iU1 !U2!U3!U:u

i'iu2iU

i :u2!U2!U:u!U

FORM 1 VGA 1/87 Rev.

100347


EPA SAMPLE NO.

EDO 16Lab Name: VERSAR INC. Contract:

j Code: VERSAR Case No. : 11724 SAS No. : 4537E

Matrix; (soil/water) UATER

Sample ut/vol: 25.0 <fl/mL> ML

Level: <lou/med) LOW

7. Moisture: not dec. ____


SDG No. : EAL62


Lab File ID: Y5236


Date Analyzed: 04/Q7/B9

Dilution Factor: -5. Q • \

Number TIC* found: OCONCENTRATION UNITS:(ug/L or ug/Kg) US/L

11CAS NUMBER ! COMPOUND NAME

1

RT EST. CONC. ! Q

i

FORM I VOA-TIC 1/B7 Rev.

100348


ERA SAMPLE NO.

EDG26Name: VER5AR INC. Contract:

11724^b Code: VERSAR Case No. _____


Sample wt/vol: 25. Q (g/mL) MJ.__


X Mo.i*ture: not dec. ____


CAS NO. COMPOUND



Lab File ID: Y5251

Date Received 04/04/89

Date Analyzed: Q4/07/B9

Dilution Factor: B. Q I


74-S7-3——-————Chloromethane . _________74-83-9—-———-——Bromomethan*_________75-01-4———————Vinyl Chlorid*__________75-00-3———————Chloroethane____________75-09-2———————Methylene Chloride_______67-64-1———————Acetone ____75-15-0———————Carbon Diiulfide________75-35-4———————1, 1-Dichloroethene_______75-35-3——————l, l-Dichloro»th«n»______540-59-O——————l, 2-Dichloroethene (total),67-66-3——-——-——Chloroform __________107-06-2——————1, 2-Dichlorotthane______78-93-3————————2-Butanone __________71-55-6———————1, 1, 1-Trichloroethane____56-23-5———————Carbon Tetrac hi bride_____108-05-4——————Vinyl Acetate___________75-27-4———————Bromodichloromethane_____7S-S7-5————————1, 2-DlchlorooroDane10061-01-5—————cis-1* 3» -Dichloropropene_79—01 -6————————Tr i c h 1 or o e t h »n»124-48-1—-————Dibromochloromethane79-00-5———————1> 1,2-Trichloroethane____71-43-2——•——•—Beniene _______75-25-2————————Bromoform _________i 08- i 0-1 ——————4-«e t h y 1 -2-Pentan one_____591-7B-6———————2-Hexanone _______.127-1.8-4———————Tetrjchloro«.thai>a79-34-5———————1/1, 2» 2-Tetrach.lorp«thane-1OB-88-3-——---——Tol-ubtf*-- *••**'• •:' • • ;•• V:- • '•••*••-•••*• ''• *'• •1OS-9O-7——————C h 1 or ob en z ene___________10O-41-4——————Ethylbenzene____________100-42-5———————Styrene_________________1330-20-7——————Total Xylenes___________107-02-8———————Ac r o 1 e in________________107-13-1 ———————Aery 1 on i tr i 1 •___________

000002029300. I120. 10. 30. 20. 1

0.o.0.0.73

4!U2!U9!2!U2!U;u

2!U

11U-1,'U:u

0. 2IUO. 7!0. 2!U

2!U1 iU2!U

J U:u

0. 2iU


1U035G



EPA SAMPLE NO.

Lab Name: VER5AR INC.

^ ..o Code: VERSAR Case No. : 11724


Sample ut/vol: 25. Q <g/mL)

Level: Uou/med) LOW

X Moisture; not dec. ____


Contract:EDG26

Number TICt found:



Lab File ID: Y5251


Date Analgied: 04/07/89

Dilution Factor: -B. O- \


iCAS NUMBER

1.

COMPOUND NAME

UNKNOWN

RT ! EST.

34. 82 !'1

CONC.

1

: Q

:V


J00357


EPA SAMPLE NO.

Lab Name: VER5AR INC. Contract:EDG27

.-o Code: VER5AR Case No. : 11724 SAS No. : 4537E SDC No. : EAL62

Matrix: (soil/yater) WATER Lab Sample ID: 696IB

Sample ut/vol: 25.O (g/mL) QL.__ Lab File ID: Y5252

Level: (lou/med) LOW Date Received: Q4/Q4/89

Moisture: not dec.


r

CAS NO. COMPOUND


Dilution Factor: Srfr 1


74-87-3——————•—Chloromethane______74-83-9————————Br omome t hane75-01-4———————Vinyl Chloridt75-00-3———————Chloroethane.^,75-09-2———————Methylene Chloride67-64-1———————Acetone.75-15-0———————Carbon Di*u 1 fidt75-35-4———————i, 1-Dichloroethene75-35-3———————1, l-Dichloroeth«ne540-59-0———————l, 2-Dich 1 oroethene (total)67-66-3———————C h 1 or o f or nt107-06-2——————1» 2-Di c h 1 oroethane78-93-3————————2-Butanone71-55-6———————l, 1* 1-Trichloroethane56-23-5———————Carbon Tetrichloride108-05-4———————Vinyl Acetate75-27-4———-———Bromodichloromethane_7S-B7-5———————1, 2-Dichloropropane____10061-01-5—————ci*-l.3*-Dichloropropene79-01 -6———————-Tr ichloroeth en»124-48-1——————Dibroroochloro*ethane____79-00-5———————1. 1, 2-Tr i c h 1 oroethane71 -43-2————————Ben z ene75-25-2———————Bromoform108-10-1——————4-«ethyl-2-Pent»none591 -73-6———————2-He x an one __________.127-13-4——————Te t r a c h 1 or o a t h tn e79-34-5———————.1, 1, 2. 2rTetr«hloroethane108-98-3--*--—i—ytttori*?1" '***:--'** *••«•+&-'-'*'f^•108-90-7———————C h 1 or ob en z ena1OO-41 -4———————Et h y 1 b en z ene100-42-5———————Sturen.e1330-20-7——————Total Xyltn»f107-02-8——————Aero 1* in____________:107-13-1———————Ac r y 1 on i tr i I e

4tU2!U3!U2!U

0. 2!U2 iU0. 2!U

0. 08 !U0. 09! U0. 3!U0. 10. 1130. 10. 30000000002

2!Ui:u2!U11U2iU2!Ui:u2!U3!U!U

o. i:uo. 2!U

i:uiiu2iU2!U;u!U

FORM 1 VOA 1/87 Rev.

300389


ERA SAMPLE NO.

Lab Name: VERSAR INC. ContractEDG27

...j Code: VERSAR Caie No. : 11724

Metrix: (soil/water) WATER

Sample ut/vol; 23. Q <g/mL) OL__


X Moisture: not dec. _^_


Number TICs found: _Q.


Lab Sample ID: 696IS

Lab File ID: Y5252

Date Received: Q4/04/B9

Date Analyzed: Q4/Q7/99

Dilution Factor:

CONCENTRATION UNITS:<ufl/L or ug/Kg) UQ/L

iiCAS NUMBER ! COMPOUND NAME RT !

!'

EST. CONC. Qatxtmt


J00390


ERA SAMPLE NO,

Lab Name: VER5AR INC. ContractEDG2S \

Code: VERSAR Cast No. : 11724 SAS No. : 4537E SDG No. : EAL62


Sample wt/vol: 25. 0 (g/mL) QL,__

Level: (lou/mtd) LQUI

% Moi«tur*e: not dec. __^_



L«b File ID: Y5253

CAS NO. COMPOUND



Dilution Factor: §. 0 V.


74-S7-3———————Chl or omt thane___________74-S3-9———————Bromome thane____,_______75-01-4———————Vinyl Chloride__________75-00-3———————Chloroethane ________75-O9-2———————Methylene Chloride_______67-64-1———————Acetone________________75-15-0———————Carbon Ditulfide________75-35-4———————i, l-Dichloroethene_______75-35-3———————1, l-Dichloroeth«ne______540-59-0———————1,2-Dichloroethene (total)67-66-3——————'—Chloroform ____107-06-2——————1, 2-Dichloroethane_______73-93-3———————2-Butanone______________71-55-6———————1, 1, 1-Trichloroethane____56-23-5———————Carbon Tetrac h1or i de____108-05-4——————Vinyl Acetate___________75-27-4————————Bromodichlpromethane73-S7-5———————1. 2-Dichloropropane^,____10061-01-5—————cis-1/3»-Dichloropropene_79-01-6———————Trichloroethene_________124-48-1——————Dibromochloromethane_____79-00-5————————1, It 2-Triehloroethane71-43-2———————Benzene____„___________75-25-2————————Brpmoform _________108-10-1———————4-Methul-2-Pentanone591-78-6———————2-Hexanone ___________127-18-4————•——Tetrachloroethene ____79-34^5————-———i, 1> 2> 2-Tetfachiaroethane^1QS-B8-3- ••*-' - -' Ttrl a*ne-' * '108-90-7——————Ch 1 or ofa rn tene.100-41-4——————Et h g 1 b en z ene_100-42-5———————Styrene_____1330-20-7—————Total Xylene*.107-02-8———•.———Aero 1 e in____107-13-1 ——————Aery 1 on i tr i 1 e.

FORM I VOA

0. 40. 20. 30. 20. 220. 2

0. OSt

0. 30. 10. 1t30. 10. 30. 20. 10. 20. 10. 20. 20. 10. 20. 32a0. 20.0. 10. 10. 20. 273

!U!Uii:u:u:u:u;u!UiUJU

!U:u!U

!U

:u;u!U!U

1/87 Rev.

-00398

IE EPA SAMPLE NO.VOLATILE ORCANICS ANALYSIS DATA SHEET _______________TENTATIVELY IDENTIFIED COMPOUNDS !

! EDG28Lab Name: VER5AR INC._____________ Contract: __________ !______

_,b Code: VERSAR Case No. : 11724 SAS No. : 4S37E SDC No. : EAL62

Matrix: (soil/water) MATER Lab Sample ID: 69619

Sample ut/vol: 25.O (g/mL) QL__ L»b File ID: Y3253

Level: (lou/med) LOW Date Received: 04/Q4/S9

% Moisture: not dec. ___ Date Analyzed: 04/07/89

Column (pack/cap) PACK Dilution Factor: .5—&•

CONCENTRATION UNITS:Number TICs found: _C; <ug/L or ug/Kg) UC/L

11CAS NUMBER !

»i

itCOMPOUND NAME t RT

>t

iiEST. CONC. ! Q

i•


j00399

1AVOLATILE ORQANICS ANALYSIS DATA SHEET

EPA SAMPLE

I Namt: VER5AR INC Contract:EAL87

ib Codt: VERSAR Cast No.


Samp If ut/vol: 25. 0 (g/mL) ML


% Moisturt: not dac. ___


11724 SAS No. : 4337E SDC No. : EAL62

Lab Sampla ID: A962&

Lab Filt ID: Y5266

Data Racaivad Q4/Q4/B9

Data Analyitd: Q4/Q7/89

Dilution Factor: -9Q- 10

r

GAS NO. COMPOUNDCONCENTRATION UNITS:(ug/L or ug/Kg) UQ/L

74-87-3™ — - — — Ch 1 oromathana74-83-9™- —— «Br offloma t h an a73-01-4 ——————— Vinyl Chlorida75-OO-3 ———————— Chloroathana75-09-2 ——————— Mathulana Chlorida..,67-64-1 ——————— Acatona75-15-0 ——————— Carbon Di.ulfida ,..,,. ,73-33-4 ———————— 1, l-DichloroathatiaMii , , .75-33-3 ——————— 1. 1-Dichloroathana340-39-0 —————— 1. 2-Dichloroathana (total) _ 67-66-3 ———— • ——— Chloroform •107-06-2 —————— -1. 2-Dichloroathana78-93-3—- —— - — 2-Butanona71-33-6 ——————— li 1. 1-Trichloroathana36-23-3 ———————— Carbon Tfttrachlarida108-03-4 ——————— Vinul Acatata „„__73-27-4™——— -BromodichloroMathana78-87-3 ——————— 1. 2-Dichloropropana mfm_10061-01-3 ———— ci*-l> 3. -Dichloropropana ____79-0 1 -6 ———————— Tr ichloroathana124-48-1 —————— Dibromochloronathana .79-OO-5 ——————— 1* lj 2-Triehloroathana7 1 -43-2 — —— — — B a n z an a75-25-2 ——— —— - fir onto f or m108-10-1 —————— 4-Mathul-2-Pentanona ,_, .,, _ „

127-18-4 —————— Tatrachloroathana79-34-5 ——————— li 1» 2< 2-Tatrachloroathana ___1 08-88-3 • - — — To 1 u an a108-90-7 ——————— Chlorobaniana100-41-4 ——————— Ethylbanzana1 00-42- 3 —————— S t u r an a1330-20-7 —————— Total Xul.n.t107-02-8 ——————— Aero lain , _IM107-13-1 ——————— Acrylonitrila

•

42132

EraQT190267

270

1714330

13212

360222623232702

5501

2lAfl+ Q\J

6329

1IUtu1tuIt:u1tt1-Itu1:utuiutu:u!UJUttutu• IIiUitututu*tutu! %

1ttt

I111

11II1

it1!ti«I

!ii•iitt*ii!i1Ii

FORM I VOA , 1/87 Rav.

100046

IEVOLATILE ORGAN1CS ANALYSIS DATA SHEETTENTATIVELY IDENTIFIED COMPOUNDS

EPA SAMPLE NCJ

Namt: VERSAR INC.EALB7

Contract:

b Cod»: VERSAR Cast No. : 11724

Matrix: <»oil/uattr) WATER

Sampl* ut/vol: 23. 0 <g/nL) ML

Lavtl: <low/mid) LOW

X Moiftura: not d»c. _^__


iNumbtr TIC* found: 0

SA8 No. : 4537E SDC No. : EAL&2

Lab Saoiplt ID: 69626

Lab Filt ID: Y32AA

Datt Rtctivtd: Q4/O4/B9

Data Analyxvd: Q4/O7/89

Dilution Factor: -P6- ro


I I I 1CAS NUMBER COMPOUND NAME RT I EST. CONC. I

FORM I VOA-TIC 1/B7 R»v.

100047

-,- --——————--- --"r i r- Mi iirr •—• —•—•—•—~- ** "--•—•""••Mfcrrt. i i nirfT r •. if i m r • tr-ti i •• rfrf» f f rtir i ar


EPA SAMPLE NO.

! EALBSLab Name: VERSAR INC. Contract:

Code: VERSAR Case -No. : 11724 SAS No. : 4537E SDC No. : EAL62

Matrix: <soil/uater) WATER Lab Sample ID: 69627A

Sample ut/vol: 25. Q (fl/mL)

Level: (low/med) LDU

Lab File ID: Y5267

": Moisture: not dec. ____




Dilution Factor: i. Q \

c

CAS NO. COMPOUNDCONCENTRATION UNITS:<ug/L or ug/Kg) UC/L

74-87-3————————Chloromethane ________74-B3-9—————————Bromomethane ___________75-01-4———————Vinyl Chlorid*_____________75-00-3———————Ch 1 oroethane______________75-O9-2———————Methglene Chloride_________67-64-1 ———————Ac e tone__________________.75-15-0———————Carbon Di*ulfide___________75-35-4———————1» l-Dichloroethene_________75-35-3———————1, l-Dichloroeth«nt________54O-59-0———————l>2-Dichloroethene (total)__67-66-3————————Ch 1 or o form _________^107-06-2——————1, 2-Dichlorotthane________78-93-3————————2-Butanone _____.71-55-6———————1, 1, 1-Trichloroethane______56-23-5———————Carbon Tetrachloride_______103-05-4——————Vinyl Acetate^_______-75-27-4———————Bromodichloromtthane_______73-57-5———————1, 2-Dichloropropane________10O61-01-5—————cis-1/3i-Dichloropropene____79-O i -6—————*-- Tr i c h 1 or oe th ene<_________«_124-48-1——————Dibromoch loromethane_______79-00-5———————1, 1, a-Trlehltt^6^thaffe- f T'71-43-2———————Benzene__________________75-25-2————————Bromof orm _________iOS-:o-l———-———4-Methyl-2-Pentanone______591-7S-6———————2-Hexanone________________127-18-4—•————Tetrachloroethene_________79-34-5———————1, 1, 2. 2-Tetrachloroethane__108-88-3—-——-—Taluene-- ' "' ••••' -108-9O-7——————Ch 1 orobenzene ______•1OO-41-4——————Ethy Ibenzene______________10O-42-5——————Styrene__________________1330-20-7——————Total Xylenef_____________107-O2-8———————Ac r o 1 e i n__________________107-13-1———————Aery Ion itrile_____________

0.0.0.0.220.

4!U2!U3IU2!U!:u

2!U0. 08! Uo. 09: ui :O. 1 !U0. 1!Ui :u6 :0. 1 !U0.0.0.0.13 :o. z;uo. aiu0. 1 ,' U0. 2!U

UU

!U!U!U!U

0.2190,

• 1*0.0.0.0.73

3

21U

i iui ;u2!U21U!U;u


10C100



ERA SAMPLE NO.

EAL8SLab Name: VERSAR INC. Contract:

^ - Code: VERSAR Case No. : 11724

Matrix: (soil/water) MATER

Sample wt/vol: 25. 0 (g/mL> ML


% Moisture: not dec. ___„




Lab Sample ID: 69&27A

Lab File ID:- YS267


Date Analgzed: Q4/Q7/S9

Dilution Factor: 5. 0- \


11

CA5 NUMBER ! COMPOUND NAME11

RT EST. CONC.f

Q


100101

1A

Lab Name: VERSAR INC.____________

V. J Code: VERSAR Case No. : 11724


Sample ut/vol: . 25. 0 (fl/mL)


X Moisture: not dec. ____


Contract:

EPA SAMPLE NO.

EALB9

CAS NO. COMPOUND


Lab Sample ID: 6962B

Lab File ID: Y5269


Date Analyzed: O4/Q7/89

Dilution Factor: 3. 0- I


74-B7-3———————Chloromethane^____________74-83-9—i————--Bromomethane____________75-01-4———————Vinyl Chloride____________75-00-3———————Chloroethane_____________75-09-2———————Methylene Chloride________67-64-1—-—————Acetone ______75-15-0———————Carbon Disulf'ide_________75-35-4———————l, l-Dichloroethtne________75-35-3———————it l-Dichlorotth»n»________54Q--59-O——————l,2-Dichloroeth»ne (total)_67-66-3————————Chloroform _______107-06-2——————1« 2-Dichloroethane________73-93-3————————2-Butanone __________71-55-6———————1, 1, 1-Trichloroethane______56-23-5———————Carbon Tetrachloride_______IOS-05-4——————Vinyl Acetate_____________75-27-4———————Bromodichloromethane79-87-5———————1» 2-Dichloropropane________10061-01-5—————ci»-lf3*-Dichloropropene___79-Q1 -6————•———Tr i c h 1 oroethene ______124-48-1———————Dibromochloromethane^______79-00-5———————1. 1> 2-Trichloroethane______71 -43-2————————B en z en e___________________"75-25-2————————Bromof orm _________103-10-1——————4-Methyl-2-Pentanone_______591-73-6——•————2-Kexanona_________127-1S-4——————Tetrac hi oroethene_________79-34-5—-—————1, 1,2, 2-Tetraehlhrbethane "108-B8-3————•-—tpl'fretv» •''••••''•''•'••••'*•'• "":- --• •<'•-•':•• '••• '-'•:1 OS-90-7——————C h 1 or ob en z ene^___________100-41-4—-—————Ethulbenzena ___________100-42-5——————Styrene__________________1330-20-7——————Total. Xylenes_____________1Q7-02-B———————Ac r o 1 e in ________;_________107-13-1———————Aery Ionitrile_____________

0.0.0.20.

0. 4IUo. 2; u3!UU

2!UJUU

0. 08 tU0. 09 I U0. 3!Uo. i :u-o. iiui ;u0. 710. 1 ! U0.0.0.0.20.0.0.0.0.290.

31U2!U1 IU2iU

ZiU2!U1 !U

I V

:uIU

2!UO:fll

i :ui :u2;u2!U!U;u

FORM I VQA 1/87 Rev.

100124

IE ERA SAMPLE NO.VOLATILE ORGANICS ANALYSIS DATA SHEET _____________


Lab Name: VERSAR INC._____________ ContractEALS9

^ .- Code: VERSAR Case No. : 11724 SAS No. : 4337E SDC No. : EAL62

Matrix: (soil/water) WATER Lab Sample ID: 69628

Sample ut/vol: 23.0 (g/mL) QL__ Lab File ID: Y5269

Level: (low/med) LOUI Date Received: 04/04/89

7. NoiEture: not dec. ___ Date Analyzed: 04/Q7/B9

Column (pack/cap) PACK Dilution Factor: -frr-» v

CONCENTRATION UNITS:Number TICs found: _Q <ug/L or ug/Kg> UC/L

CAS NUMBER ! COMPOUND NAME ! RT E3T. CONC.

FORM I VOA-TIC 1/S7 Rev.

100125


ERA SAHPLE N

EAL90-b Name: VERSAR INC. Contract:

11724S-;ab Code: VERSAR Case No.

Matrix: (moil/water) WATER

Sample ut/vol: 25. 0 (g/mL) QU _


% Moisture: not dec. _^_




Lab File ID: Y5299



Dilution Factor:

r

GAS NO. COMPOUNDCONCENTRATION UNITS:(ug/L or ug/Kg) UO/L

74-37-3-—•————'-Chloromethana ________74-S3-9-—-——-—Bromome thane ________75-01-4———————Vingl Chloride__________75-00-3———————Ch 1 or oe thane____________75-09-2———————Methylene Chloride_______67-64-1———————Acetone________________75-15-0———————Carbon Ditulfide________75-35-4———————1, 1-Di c h 1 oroethene_______75-35-3———————l, 1-Di ch lor oethane_______540-59-0———————1,2-Dichloroethene (total),67-66-3™————C h 1 orof orm ______107-06-2——————li 2-Dich lor oethane______78-93-3———————2-Butanone_________71-55-6———————1, 1, 1-Trichlorotthane____56-23-5———————Car b on Te trac h 1 or i d e_____.108-05-4——————Vinyl Acetate___________75-27-4—-————-Bromodichloromethane78-87-5———————lf 2-Dich loropropane_____10061-01-5—————cit-li3*-Dichloropropene_79-01 -6———————Tr i c h 1 or oe.th«n*}_________124-48-1——————Dibromochloromethane____79-00-5———————1, 1, 2-Trichloroethane____71 -43-2—————-—— B en z ene _______^_75-25-2————————Bromof orm ______^__^: 09-10-1———————4-Metnyl-2-Pentanone_____591-7S-6———————2-Hexanone______________127-1S-4——————Tetrachloroethtnt._______79-34-5- ————*-r -lr 1.- 2/.2-1OB-BS-3——————To 1 u en'e108-90-7——————Chlorobenient100-41 -4——————Et h y 1 b en i ene100-42- 5———————S t y r ene1330-20-7——————Total Xylenet107-02-8———————Ac r o 1 s in107-13-1——————Aery Ion itrile

FORM I VOA

1056565062264333523039544

41046125757

310-..,'6;3403356216072

:u;utu!U:uiuIU:u:u•!U!U;u•i:u:u:u:u:uiiuIUII

!U;u!U

:u;u:uii!UIU

1/B7 Rev.

100142


EPA SAMPLE NJ

EAL90Name: VERSAR INC. Contract

b Code: VERSAR Case No. : 11724


Sample ut/vol: 23. Q <g/mL> QL.__

Level: Clou/med) LOW

;: Moisture: not dec. ___


Number TICs found: ,_0.



Lab File ID: YS299


Date Analgzed: O4/ 11/89

Dilution Factor:

CONCENTRATION UNITS:(ug/L or ug/Kg) UPXL

iCAS NUMBER ! COMPOUND NAME RT i EST. CONC. Q

FORM I VOA-TIC 1/B7 Rev.

J.U0143


EPA SAMPLE NC

Name: VERSAR INC. Contract:EAL91

Code: VERSAR Case No. : 11724 3AS No. : 4537E SDG No. : EAL62


Sample ut/vol: 25.0 (g/mL) ML

Level: <lou/m*d> LOW


Column: ( p a c k / c a p ) PACK

Lab Sample ID: 69629D

Lab File ID: Y526S



Dilution Factor: 5. Q- \

CAS NO. COMPOUNDCONCENTRATION UNITS:(ug/L or ug/Kg) US/L Q

74-B7-3—————•—-Ch1 o r o m e t h a n e _ _ _ _ _ _7 4 - B 3 - 9 — — — — — — — — B r o m o m e t h a n * _ _ _ _ _ _75-01-4———————Vingl Chloridt__________75-OO-3———————C h 1 oroethane ________75-09-2———————Methglene Chloride_______67-64-1———————Acetone________________75-15-0———————Carbon Di»ulfide________75-35-4———————1* l-Dichloro«th*n*_______75-35-3———————1. 1-Dichlorotthan*______54O-59-O——————li 2-Dichloroethen* (total)67-66-3———————C h 1 oroform ____107-06-2——————1, 2-Dichloro*than*_______78-93-3———————2-B u tan on e____,_________71-55-6———————1. 1* l-Trichloro*than«____56-23-5———————Carbon Tetrachloride_____108-05-4———————Vingl Acetate___________75-27-4—————Bromodi c h1oromethane78-87-5———————I/ 2-Dichloropropane_____10061-01-5—————ci*-l*3»-Dichloropropene_79-01 -6™—————Tr i c h 1 or oe th ana124-48-1 —————-D i b r offlo c h 1 oromethane79-OO-5———————l, 1. 2-Trichloro*thane____71 -43-2———-—---Ben zene _______75—25-2————-———Bromo-Form___________1 OS-10-1———————4-Methgl-2-Pentanone_____591-78-6——————2-Hexanon* __________127-12-4——————Tetrachloroethtne_______79-34-5—————~~*~1' 1*.2> 2-T*tr.achloij.o*.th;ana_10S-SS-3———-----T o-l liana '"' ' '"-'• "•• ' '"•••''1 OS-90-7——————C hloroben: ene ______100-41 -4——————Et h y 1 b en z en*____________100-42-5——————Stgrene_______„_________1330-20-7——————Total Xyltntft____________107-02-8———————Acrolein________________107-13-1 ———————Ac r ylonitril e ________

FORM I VOA

42722

0. 20. 080. 090. 30. 10. 111000003O. 20. 2O 10. 20. 3

15Q,0.0.0.0.0.73

!U:ui•;u:u!U!U:u:u:u!U'-!U!UII

!U;u;u!UiUiiUIU;u!U:u:u

1/B7 Rev.

1C0169

-B4ae ^



ERA SAMPLE N-r

EAL91i »b Name: VERSAR INC. Contract:

Code: VERSAR Case No.: 11724

Matrix: <*oil/uater> MATER

Sample ut/vol: 25.0 (g/mL) ML

Level: (lou/med) LOUJ

T; Moisture: not dec. ___.


Number TICs -found: _3

SAS No. : 4S37E SDC No. : EAL62

Lab Sample ID: 69629D

Lab File ID: Y526B

Datt Received: O4/O4/89


Dilution Factor: 60 \


CAS NUMBER

12. 75-43-43. 75-69-4

COMPOUND NAME

UNKNOWNMETHANE, D I CHLOROFLUORO-METHANE, TRICHLOROFLUORO-

1

RT I EST.

2. 25 !6. 65 !9. 55 !

11

CONC.

33

Q

JJJ


100170

^ *<- ..-..- . -K,~

iAVOLATILE ORGANICS ANALYSIS DATA SHEET

EPA SAMPLE NO.

EAL92Lab Name: VERSAR INC. Contract:

11724^. -b Code: VER5AR Case No


Sample wt/vol: 29. 0 <g/mL> ML

Level: ( low/med ) LOW

Moisture: not dec


r

CA5 NO. COMPOUND


Lab Sample ID: 6963QA

Lab File ID: Y5294

Date Received: Q4/04/89

Date Analyzed: 04/1 1/S9

Dilution Factor:

CONCENTRATION UNITS:<ug/L or u g / K g > UG/L

74-87-3————————Chloromethane_______74-93-9———————Bromomethane____________75-01-4———————Vinyl Chloridt__________75-00-3———————C h 1 or o e t h an e ___________75-09-2———————Methglene Chloride_______67-64-1———————Acetone________________75-15-0———————Carbon Ditulfidt________75-35-4———————1* 1-Dichloroetbene_______75-35-3———————1. 1-Dichloroethant_______540-59-0———————1. 2-Dichloroethtne (total)67-66-3————————Chloroform ________107-06-2——————1,2-Dichlorotthane______78-93-3———————2-But»none______________71-55-6———————1. 1, l-Trichloroeth»ne____56-23-5———————Carbon Tetrachloride_____108-05-4——————Vinyl Acetate___________75-27-4———————Bromodichloromethane_____78-67-5———————1. 2-Dichloropropane______10O61-01-5————— cis-1*3*-Diehloropropen*_79-01-6————————Trichloroethene__________124-48-1——————Dibromochloro*»than»____79-00-5———————i, 1, 2-Trichloro«th«ne____71-43-2———————Benzene________________75-25-2————————Bromof orm ________108-10-1———————4-Methyl-2-P»ntanone_____591 -79-6———————2-He x an one______________127-1S-4——————-Tetrachloroethene_______79-34-5—r——-.-—1* 1* 2* 2-Tetrachloroethane_108-88-3—--irr—-Tolti'»n« ' .••.'•.Jy ••.•-*•.••• '"..;• ' •-.108-90-7———-——C h 1 or o b enzene'100-41-4——————Ethyl benzene____________100-42-5———————Styrene________________1330-20-7——————Total Xylenes___________107-02-8——————Ac r o 1 e i n_____;__________107-13-1 ——————Aery 1 on i tr i 1 e___________

105656

86062253333549039544

10OO461458657

940' 6

12003475

46016072

FORM I VOA

1UiUJU:u

iUJU!U

UU

UUUUU

uU

IUI •

IU-r!Ui!Ui*:u!U

1/87 Rev.

100197'

r ^ aux& aaKittaas&SMVft&p&ttsa* ^ -c.



ERA SAMPLE NO.

EAL92' en Name: VERSAR Contract

j Code: VERSAR Cast No. : 11724


Sample uit/vol: 25. Q <g/mL) QL.__


X Moisture; not dec. ____




Lab Sample ID: 6963QA

Lab File ID: Y5294

Date Received: 04/O4/B9


Dilution Factor: -fr93 a.*


CAS NUMBER COMPOUND NAME' RT••

EST. CONC. I

f ii

Q

rFORM I VOA-TIC 1/87 Rev.

100198


EPA SAMPLE NO.

EAL93L *b Name: VERSAR INC. Contract:

,o Code: VERSAR Case No. : 11724


Sample ut/vol: 25. O (g/mL) ML,__

Level: Uou/med) LDU



r

CA5 NO. COMPOUND


Lab Sample ID: 69613C

Lab File ID: Y5298



Dilution Factor: >& A


74-87-3 ——— •

75-01-4 —— •75-OO-3 ———

75-15-0 ———75-35-4 —— -

• ———— Bromome thane

———— Ch 1 oroethane immi-— —— Methylene Chloride————— Acetone-1 ———— Carbon Disulf ide ..,• ——— — 1* 1-Dichloroethene

75-35-3 ———————— 1. 1-Dichloroe thane540-59-0 — -67-66-3 —— -

/ O . •» «9

108-05-4 — •

7E-S7-5 ——— -10O61-01-5-79-01-6 ——— -

79-00-5 —— -71-43-2 ——— -

i P*. P*t A I*. "J103— 1O— 1 ——591-7S-6 — -

108-90-7 — -100-41-4 — •100-42-5 — •£ ww\J Lw /

———— 1* 2-Dichloroethene (total ) __-- — ——Chloroform mmmm—— „ — lt 2-Dichloroethane- — i —— 2— Butanone———— 1> 1. 1-Trichloroethane———— Carbon Tetrachloride————— Vinijl Acetate .,——— •"-Bromodichloromethane• ———— 1* 2-Dich lorooropane———— ci»-l* 3> -Dichloropropene ____————— Tr ichloroethene ._..———— Dibromochloromethane— ——— 1* 1. 2-Trichloroethane————— Benzene „„—— —— Bromof orm———— 4-Methul-2-Pentanone————— 2-Hexanone ,.--- ——— Tetrachloroethene————— 1, 1* 2; 2-Tetrachloroethanemm • ii • • | . | £ U V Fl w ' ' ' '

———— Chlorobenzene M-n_ „————— Et h y 1 b en z ene _ IM— — • — — Styrene- ———— Total Xylene*————— Acrolein- ———— Acr 4 1 on i tr i 1 e

0. 8!U0. 4JU0. 5tU0. 4!U2 UB 1

4 :u0. 5!U0. 2!U0. 2!U2 i0. 2IU-0. 2!U3 iU10 :0. 2!U0. 7!U0. 4!U0. 3iU0. 3iU

53 ;0. 3!U0. 5!U0. 8!0. 4!U0 . 5 ! U5 !U

. . , ,59 :o. 4 : u0. 21U2 :0. 4!U

11 :13 tU6 ;u

*


JU0236

IEVOLATILE QRGANICS ANALYSIS DATA SHEET


EPA SAMPLE NO.

EAL93Lab Name: VERSAR INC. Contract

v ,b Code: VER5AR Case No.: 11724


Sample ut/vol: 25. Q (g/mL) QL__

Level: Uow/med) LOW

7. Moisture: not dec. _^___


Number TIC* found: _Q

SAS No. : 4537E SDG No. : EAL&2

Lab Sample ID: 69613C

Lab File ID: Y5298

Date Received: . 04/04/89

Date Analyied: 04/11/B9

Dilution Factor:

CONCENTRATIDN UNITS:(ufl/L or ug/Kg) UQ/L

ttCAS NUMBER { COMPOUND NAME

ii

RT EST. CONC.

'

Q

rFORM I VOA-TIC 1/S7 Rev.

100237

'?^ ;

C2qC2(

L Hi

^3b CtMatri)

Sampli

Lavtl:

X Moil

Columr

•

^

I 1AVOLATILE OROANICS ANALYSIS DATA SHEET

ima: VERSAR INC. Contract:

iEPA SAMPLE NC|

" - • •" "- •1 ^ i1 EAL62 ^ ! f! !

>da: VERSAR Cata No. : 11724 SAS No. : 5375 SDO No. : EAL62

t: doil/uatar) WAJgR. Lab Samola ID: 69623

» ut/vol: 29. 0 <g/«L) HL _ L*b Fi

<lou/mad) UOH , _ ' Data F

itura: not dac. Data /

i: (pack/cap) P. .QK. DilutJ

Lla ID: Y J97

lactivtd: 04/Q4/89

^nalyzad: O4/O7/B9

Lon Factor: fc-e- \ P4*-J

CONCENTRATION UNITS:CAS NO. COMPOUND (ug/L or ug/Kg> UQ/L Q

1 . -74-87-3 ———————— C h 1 or oma t h an a74-83-9 ——— - — — — Br offlona t h ana79-01-4 ——————— Vinyl Chlorida79-OO-3 ——————— Ch 1 or oathana mm ____79-09-2 ———————— Mathylana Chlorid.67-64-1 ———————— Acatona ,. _79-19-O ——————— Carbon Di»ulf Ida .,„..79-33-4 ———————— 1, 1-Dichloroathana79-39-3 ———————— 1. 1-Dichloroathaha94O-99-0 —————— 1.2-Dichlorotthana <total> __67-66-3 ——————— Chloroform107-06-2 ——————— 1, 2-Dichloroathana78-93-3 —— —— ——— 2-Butanona .71-99-6 ——————— 1;1, 1-Trichloroathana ,_',„,__,96-23-9 ——————— Carbon Tatrachlorida , ...108-09-4 ———————— Vinyl Acatat* MIMI79-27-4 ———————— BromodichloroAathana78-87-9 —— - —— — — 1, 2-Dichloropropana m1OO61— Ol— 9- —— — — ci»— 1* 3, — Diehloroprooana79-0 1 -&——-. —— -Tr i c h 1 or oa t h ana124-48-1 ———— - — Dibromoehlornaathana m m_n_i79-OO-9 ———————— 1. 1* 2-Triehloroathana71-43-2—— ——— —-Banzana ,79-29-2— — — - —— -Bromof orm108-1O-1 ——————— 4-M«thVl-2-Pantanon» . .._ .991-78-6 ———————— 2-Haxanona ,127-18-4 ——————— Tatrachloroathana79-34-9 ——————— 1, 1* 2. 2-Tatrachloroathane ___1 08-S8-3—— — — — To 1 u ana1 08-9O-7 ——————— C h 1 or ob an z an a100-41-4 ——————— Ethulbanzana _.„„„.,.,1OO-42-9 ——————— Sturana1330-20-7 —————— Total Xylanaa ,. ,,„., ,1 07-02-8 ——————— Ac r o 1 a i n1O7-13-1 ——————— Acrulonitrila

••

10. 4IU

, 0. 2IU0. 3!U0. 2!U0. 2JU2 IU0. 21 U

0. 08IU0. 09IUO. 3(U0. 1IU-0. 1!U1 IU0. 1IUo. i :u0. 3!U0. 2IU0. ItUo. 2 : u0. 1IU0. 2!U0. 2!U0,1 :u0.2IU0.3SU2 IU0. 1IU0, 2IU2 I0. 1IU0. ItU0. 2IU0. 2!U7 IU3 !U

!

"

i

FORM I VQA 1/87 Rav.

100019

C2<iC2q, IE ' EPA SAMPLE NtVOLATILE ORCANICS ANALYSIS DATA SHEET _____________ |.

TENTATIVELY IDENTIFIED COMPOUNDS i {'! EAL62

Lab Nama: VERSAR INC.____________ Contract: _________ I

Coda: VERSAR Cast No. : 11724 SAS No. : 4337E SDQ No. : EAL&2

Matrix: <*oil/wat»r> WATER . Lab Sanpla ID: A9623

Sampl* ut/vol: _23. Q (g/mL) ffli_ Lab Fila ID: YS257

Ltval: (lou/mad) LOW Datt Rtcaivad: Q4/04/89

X Moistur*: not dtc. ___ Data Analyzid: Q4/O7/B9

Column (pack/cap) PACK Dilution Factor: *r-Q- \

CONCENTRATION UNITS:Numbar TIC» found: _ft <ug/L or ug/Kg> UQ/L

i i '. i i T~• CAS NUMBER t COMPOUND NAME I RT I EST. CONC. 1

I______________(_________________________S_______I *___________l_

C


100020

&:<>rt:-?^^


EPA SAMPLE NO.

L*b Name: VER5AR INC Contract:EAL83 V

Codt: VERSAR Ca»» No.: 11724 SAS No.: 4537E SDfi No. : EAL62

Matrix: (*oil/uat«r) WATER

Sample ut/vol: 23. q (g/mL)

L»v»l: <1ow/mad) LOW

X Moiiturv: not d*c. ___


CAS NO. COMPOUND

Lab Samp la ID: 69624

Lab Fila ID: Y323S

Dattt Rtctivtd: 04/04/89

Data Analyzed: Q4/Q7/B9

Dilution Factor: '9r& \


74-87-3 ——— — —— C h 1 or oma t h ana74-83-9 ——— - ——— Bromomathana73-01-4 ——————— Vinyl Chlorida75-OO-3 ———————— C h 1 or o at h an •73-09-2 ———————— M«thYl»n» Chlorid»._67-&4-1 ———————— Ac»tona73-13-0 ———————— Carbon Di«ul*id»mii75-33-4 ———————— 1, 1-Dichloroathana73-33-3 ——————— 1, 1-Dichloroathana340-39-0 ——————— l,2-Dichlorotth«nt (total) __&7-AA-3 ————————— Chloroform107-06-2 ——————— 1,2-Dichloroathana78-93-3 ——————— 2-Su tan on a71-33-6 ———————— 1. 1, l-Trichloroathan« , ,36-23-3 ——————— Carbon Tvtrachlorida108-03-4 ———————— Vinyl Ac. tat. MMI75-27-4 ———— - ——— Br omod i c h 1 oroAathan*78-87-3 ——————— li 2-Dichloropropana , __10O61-O1-3 ———— cic-l> 3. -Oichloropropana ____79-01-6 ————————— Trichloro«th«fl»124-4B-1 —— - ——— — Dibromochlorottathani79-00-3 ———————— 1. l,2-Trichloroathan»_71-43-2 ————————— B.ni.n. ,„„,„,_73-23-2 ——— - — • — Bromoform1O8-10-1 ——————— 4-M»thMl-2-Pantanon»39 1 -78-6 ——————— 2-H» x anon.127-18-4 ——————— T.trachloroathana79-34-3 ——————— 1* l, 2. 2-Tatrachloroathana ___108-88-3 ———————— Tolu»n«108-90-7 ———— —— Chlorobanz.na1 00-4 1 -4 ——————— E thulbanzans „„, ,,.,„100-42-3 ——————— Stvr.na1330-20-7 —————— Total Xultn.m ,107-02-8 ——————— Acrolain .,107-13-1 ——————— Acrylonitril*

I0. 4!U0. 2IU0.3IU0. 2IU0. 2tU

14 t0. 21 U0. 081U0. 091U0. 3IU0. 1IU-o. i:u1 IU0. 11Uo. i:u0. 3tU0. 2LU0. 1IU0. 2IU0. 1IU0. 2JU0. 21U0. UU0. 2!U0. 3IU2 IU0. 1!U0. 2iU0. 1IU-0. 1IU0. 1IU0. 2IU0. 2!U7 !U3 iU

1

FORM I VOA 1/87 R»v.

100028

IE EPA SAMPLE NO. |VOLATILE ORGANICS ANALYSIS -DATA SHEET _____________ tTENTATIVELY IDENTIFIED COMPOUNDS 1 \'

I EAL83 fLab Name: VERSAR I N C . C o n t r a c t : t

Code: VERSAR Ca«e No. :. 11724 SAS No. : 4337E SDG No. : EAL&2

Matrix: (soil/water) MATER Lab Samplt ID:

Sample wt/vol: 25. O (g/mL) M^_ Lab File ID:

Level: <low/med> LOW Date Received: Q4/04/99

X Moisture: not dec. ___ Data Analyzed: O4/Q7/99

Column (pack/cap) PACK Dilution Factor: "9.Q- v

CONCENTRATION UNITS:Number TIC* found: _£ (ug/U or ug/Kg) UQ/L

! i - i i i :1 CAS NUMBER i COMPOUND NAME t RT I EST. CONC. 1 Q !

_ . _ . ! _ _ _ __ __ ___ __ !___ __\*__________\____1

C

FORM I VOA-TIC 1/87 Rev. [t

100029 I

g v:. >;?v••" •• ijd ^ „•*-iV*-,"* v1, Jki S -Sfcf*1r-


EPA SAMPLE NO.

EAL84Lab Namt: VERSAR Contract:

^ - Codt: VERSAR Cast No. : 11724 SA3 No. : 4537E SDO No. : EAL62

Matrix: <*oil/wat»r) WATER - Lab Samp It ID: 69625

SampIt wt/vol: 25. 0 <g/mL) OL_ Lab File ID: Y3259

Ltvtl: Mou/mtd) LDUI Datt Ractivvd: 04/04/89

.Moiftturt: not d»c.

Column: (pack /cap) PACK

Datt Analyzed: O4/Q7/B9

CAS NO. COMPOUND

Dilution Factor:


I

74-87-3 ——————— Chloromtthana74-83-9 ——————— Bromontthana.j;75-01-4 ——————— Vinyl Chlorida.__

* 75-OO-3 ———————— Chlorotthana ,_ (75-09-2 ——————— Mtthultnt Chloridt67-64-1 ———————— Acttont75-15-0 ——————— Carbon Di.ulfidt75-35-4 ——————— 1, l-Dichloroathan»75-35-3 ——————— 1, 1-Dichloroathana540-59-0 ——————— 1.2-Dichloro*th«n» ttotal) __67-66-3 —— - —— - — -C h 1 or of or m107-06-2 ——————— 1, 2-Dichloro»than»78-93-3—— — — — 2-Butanont _71-53-6 ———————— 1. 1. l-Trichloro«thant ..,., ., ......56-23-5 ———————— Carbon Tttraehloridt1O8-O5-4 ——————— Vinyl Acttatt75-27-4 —— —— - —— -BrootodichloroAathan*78-87-5 ———— : ——— 1* 2-Dichloropropana _10061-O1-3 ————— ci«-l» 3* -Dichloroproptnt ____79-O1 -6 ——— — - —— Trichloro»th»n»124-48-1 —————— Dibromochloromtthant79-00-5 ———————— 1. 1,2-Trichloroathant .,_.71-43-2 ———————— Btnz.nt ., ,„ .f mf ^«/ ^ lii 1 Qflluf^UnB

108-10-1 ——————— 4-MtthVl-2-Ptn-tanont . .,._. .391-7B-6 ———————— 2-H»xanana , „127-18-4—-: — — — Tttrtchlorotthtnt79-34-5 —————— : — 1* If 2> 2-Tttrachlorotthant ___1 08-88-3 ——————— To 1 u an t1 08-90-7 ——————— Ch 1 or ob tn i ana10O-41-4 ——————— Ethijlbtnztnt1OO— 42-5 ——— • —— — — Styrtnt1330-20-7 —————— Total Xgltna*1 07-02-8 ——————— Ac r o 1 • i n107-13-1 ——————— Acrylonitrila

.

\0. 41U0. 2JU0.3IU0. 2IU

. 0. 312 IU0. 2IUO 081 U0. 09 1 U0.3IU0. 1IU-0. 11U1 JU0. 1IU0. 1IU0. 3tU0. 21U0. 11U0. 21UO. 1 *U0. 2IU0. 2IU0. 11U0. 2IU0. 31U2 IU0. 11U0. 21U0. 11U'0.1 IU0.1 IU0. 21U0. 21U7 IU3 IU

I


100037

^ ^IE ERA SAMPLE NO.

VOLATILE ORCANICS ANALYSIS DATA SHEETTENTATIVELY IDENTIFIED COMPOUNDS 1

I EALS4 ! K'v Name: VER5AR INC.____________ Contract: _________ I

g^b Codt: VERSAR Cast No.: 11724 SAS-No. : 4337E SD« No, : EALA2

Matrix: (»oil/uiat»ri WATER Lab Sample ID:

Sampl* wt/vol: 29. 0 <fl/mL) ffl._ Lab Fil* ID: Y3259

L»v«l: <low/m»d> LOW Data Rtctivad: O4/O4/89

Z Moiiturt: not d«c. . _ Dat* Analyztd: O4/O7/B9

Column (pack/cap) PACK Dilution Factor: **"fr \

CONCENTRATION UNITS:Numb«r T1C« found: _a (ug/L or uj/Kg) UO/L

CAS NUMBER COMPOUND NAME. 1

1 RT

I

1t EST.

I

I ICONC. I Q t

1 I


100038

{•

UNITED STATES ENVIRONMENTAL PROTECTION AGENCYREGION V

PAGE 1 OF

: Review of Region V CLP DataReceived for Review onCurtis Ross, Director (5SCRL)Central Regional LaboratoryData User: ________(_

.APR, 1 4 1389—— ---a -

Ife have reviewed the data for the following case(s)SITE RAHE; \f0Jr/tfC( \jJpJjff Q^ToJOf j_ SMO Cast Ro.

EPA Data Set N(

CRL

CLP Llboritory:

Following are our findings:> P/rr#

.

Hri. Requiredfor B.vUw:

5r& Be

-r*

•-una are preliminary - pending verification by Contractor Laboratory.See Case Suonary above.

( ) Data are unacceptable.cc: Carla Deiiosey.CLP Quality Assurance Officer, .Analytical Operations Branch

James Petty. Chief Quality Assurance Research, EMSL, Las Vegas

•AGE ^ or_c_DATA QUALIFIERS

>ntr actor: . S0n>l&l4(£fn ______ •_ ' | east jf(f f % / yZ3{^ . \

Itlo* 1s a siiwfttrjr of the out-of-control audits and tht oosslblt tfftct en tht4ata for this cast:

?in LAB

ML

/A/

LIST

&L

vw<VKnhH}

by:

MBE 3 OFDATA QUALIFIERS

wtractor; Case

Be1o« 1s a sutm.irjr of tne out*of-contro1 audits and the possible effect on thetfata for this case:

fl

]#Ueffte ffffff

Ihstftt*

Gr\S

f\ 610 Unfit t

fart-fag,

hte

tfftfaus

Gen*

rttlttiat trs rtth

A- z<~re.6? I

tti ->

evlttfed by:•hone:Date: \foUfo

DATA QUALIFIERS_» OF

ontractor;

telo- U a lumwarj of tht owt-of-eontrol audit! and tht poitlblt tfftct on thttfata for thU cast:

fff Ll-

Tfr E//M/K-me

t/trr tci

Mr+r

/*/

tvlttftd by:

OUt:

BMA QUALIFIERS

>ntr»ctor: \ Cue (f--'

Brio* 1» • tuimtv of the eut»ef-contre1 audits and th» powlblt if feet en thi<«t« for this e»»»:

0? tanU&r?

/l/f? -rtfgfat

/

//

//

//

/

CA5E/SAS

FACE C OFSTATES ENVIWNHEHTAL MOTECT10N A6ENCT REGION V ——

, CAIURATJON OUTUfRSMil.* ? / VOLATILE HSi. COHPOUNPS

0 / lT7*>y tyt3t£- COMTRACTOR

Instrument 1

tioromethane

nyi Chlorideroethane

Chloridee o n e

:aropn nisuifide,l»DicMoroethane1-Dichioroethene

ChiorOTortn

; , - c o r o e t » n el.l.I-Tnchioroetnaof

•Don TetrachiorioeV»n>l Acetate

Tr*i$-I ,3-Dichloropropenein

3.1.?-inchToroethane

C-!S*3,3«D^ChToropropyne-CMoToei*yi vinyl ether

Teoroethane

o

rr-r

AFFECTED

Revie-er'sInitials/Date

init. CaJ.

r1£U

timr

11*1

Cont* Cai.• ' so

Cont. Cal

KF 10

com. caSHT7

TC

il£2

g-

**,

tont. cai

RF

t

• These flags should be applied tc the analytes on the sample data sheets

1/87

//DATAFor reporting reeulta tr *no BSDA, tho following oontraet epeeifiefualifiera aro to bo uaod. lha aerva {ualifiera dof iaad below mSAfi aubjoet to nodifiaation by tina laboratory. Up to fivefualifiora nay bo roportod am Fern Z for oach •oupniinl.* " •

lha ae-ren IPA-dofiaod fnallfiara to bo uaod aro aa follow*:- Xadieataa eoapound uaa analyst* for but not detected.

aanple foantitation Unit nuat bo oorreeted for dilution endfor percent aoiature. For aunpla, 10 V for phenol ia water ifthe aaaple final Tolune ia the protoeol-apoeified final voliaM.Xf a 1 to 10 dilution of avtraat ia neeeaaery, the reportedlinic i* 100 0. For a aoil aanple, tho vnlua Boat ilia beadjuatad for percent noiatare. For asaaple. if tho aanplo bad

liature SD& a 1 to 10 dilution factor, the aanplefoaati'tatioa Unit for fbaBol (330 V) would bo aorroatod to:

and df • dilution fMtorat 24% noiatura, 0 -

100

- 0.7«100

n 10 • 4300 0 rotated to the appropriateaipifieant figurea

vab«r of

J *

e -

For aoil aasploo at^jaetad to OK aloan-up proooduraa, tho C&Q1ia alao Bultipliad by 2. to aaeount for tho fact that only h*K•f tho ostraet ia rooovorod. - -Xadieataa an oatinatod aluo. Thia flag ia naod oithar whanoatiaating a aoneontration for tontativoly idontifiad oonpouncavh«r« a 1:1 raaponao ia aaaiaMd, or nhon tho naaa ap«etral d*t*indieata tho proaonaa of a aovpoimd that Boota th«idantifieation tritoria but tha raault £a laaa than tho^uantitatien Unit but graatar tkan saro. For oxaaela; ifaaapla ojuaatitation liadt ia 10 na/L, but a aonotacrmtion of 3ua/L ia oaloulatad, roport it aa 3J. Iho aaa^lo fuantitation-^»t. » »> I i HJ ,n, i 9mm Igft •«1»»«Mi m*A y*^M» Mf««i^1aa diaouaaod for tho V flag, ao that if a aaa^la vidi 24%•oiaturo and a 1 to 10 dilution faotor haa a aalaulatadooneontration of 300 ug/L and a aanplo foantitation liadt of430 ug/kg. roport tho aoaoontration aa 300J an Fom 1.Thia flag applioa to poatiaido rooulta i^ara tho idontifleationhaa boon eoafitnad by 6C/HS. Singla oonpenont poacieidoang/ul in tho fical oxtraat aball bo oonfixBod by CC/MS.

B*2f 2/88

1 •This flag is ased when Ac aaalyta is found la the associated•lank aa voll as la the sample. It ladicatas possible/probableblank contamination and vans tha data user to take appropriate«etloa. This flag suet bo used for a TIC as veil as for a

Idaatif lad TCL

1 - Ibis flag iden whoee •oaeeatratioas exceed th«calibration range of tao CC/MS iastzuaeat for that specif ieanalysis. This flag will ao£ «Pply *• fastteidas/?CIs analyxadby GC/IC BMtaods. If oaa or aor» suapuiindi bavo a vaspoasagraatar ttaa foil saalo, tba aaapla or oattract avst to dllutodand va-aaaljxod aaoardtas; to taa •poclfteatloaa la fthlblt D.All sueh soppoimrti vita a roapoaso graatar taaa full seal*should hew tbo •oaooatratloa flauod wlta aa *X* oa tfa* Fora Ifor tao orlflnal aaal7«ls. If taa dilutlsa of tb« oxtraet

telov the calibration raageresults of beta analyses shall be reported on separate forme *.Tha form X for tho diluted sample shall have the *&!.• suffixappended to the sample number. VOTZ: for total mylenea. vh« :rthree learners are fosntified as two peaks, the calibrationraage of «*eh B««V should be considered seperately, e.g., adiluted analysis Is ap£ required for total xylencs unless th*concentration of either peak separately exceeds 200 mg/L.

this flag Idaatif las all sflsrpminrts idoatlflod la sa aaalysls A-a soeoadary dilution faatar. If a aaapla or oxtraet laro-anAly»«d at a hlgbar dilution factor, aa la tho *I* flagabowo, tho *OL' suffix Is appondod to tho saaplo auabor on th*Tora X for tho dllutod saaplo, sad all aoaeaatratlon valu*j *xoportad oa that fora X aro flagged wlsa tna •&• flag.

This flag ladleatas that a TIC la a sua>octad«ldol*«oad«akatioa product.

Othor spoclflc flags aaj bo roojulrod to proptrly daflao th^rosults. If uaod. th«7 aust bo fully doscribod and suchdftserlpclen attaehod to tha Saaplo Data Suaaary Vaeltagt and * -.Caso lUrratlvo. Bagla by uslag *X*. Xf aoro than oao flag i.

rs sxoojtoflag might ooablao

required forrsl flags, ai

" "

a result, use the *X* flaxfor lusrsnre, the *Z*

•0" flags for some sampl

is expressly prohibited. SI.. '.detected In -r-i

tlaatloB of flags 10* er*0»ilaaats are flagged *S* nib

sample.

If analyses at two different dilution fectora ate required C*«*Exhibit 0), follow the data reportlrg instructions given In Exh9 «rd with the «D" and *f flag* above.

»-30 2/i

USER* CONTRACT LABORATORY PH(K,H*wSAMPIF MANAf.FMtNT OFf !ttP <) HO* fllH ALl XANDRtA. VA 27.1) I70 ! • ' • . 7 .'*'tO MS S'j7 2440


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Cast Narrative-SAS* 4231ESOC No. EAU40

Contract: SAS4831ECompuChem Laboritorit5, Inc.

SAHPLE: EAU40, EAU41, EAW42, EAU43, EAU44, EAW4S, EAW46, EAU47,EAU48, EAU49, EAU50, EAUS1, EAU52, EAU53, EAU54, EAU55>EAU56, EAU57, EAU58, EAUS9

Attached art pertinent Quality Assurance notices dealing with theanalysis of twenty (SO) LDL water samples associated with SASt 4231E,SDG No. EAU40. The samples were scheduled for volatile analysis.

The samples were received in good condition on March 3, 1989 withthe chain-of-custody in order. No irregularit ies were encounteredduring receipt of the sample.

Lower Detection Limit (LDL) Comment);t) Compuchem is following EPA roundiny convention for CRQL's and

result reporting. Volatiles are reported to one significantfigure below ten.

2) J values are being reported down to half of modified CRQL.3) The word 'NO' on quantitation report means compounds were not

found and also means the compounds concentration was less thanhalf CRQL.

VOLATILES:All volatile fractions were prepared and analyzed within holdingt ime requirements. The samples contained 0-10 Target Compounds.Some samples contained the Target Compound methylene chloride invarying concentrations. In some of the samples this compound waspresent in low levels in the associated blanks, all concentrat ionsw i l l be flagged with a 'B'. Zero to three Tentatively IdentifiedCompounds (TIC) were found. Some samples contained Freon, tentativelyidentified by NBS Library Search as 1,1,2-trichloro-1,2,2-trifluoro-ethane was detected. This is occasionally observed in volatile instru-ment blanks/ and is known to be a commom lab artifact. The same compoundwas detected in the associated blank, but not at a sufficient concentra-tion to require a library search. Nevertheless/ the, compound has beenflagged in the sample data with a 'B', denoting its presence in the blank.The compound should be considered a lab contaminant not native to the as-received sample. Please note the attached QA notice. In the initial in-jections, of the neat extract, of samples EAU56 and EAU44 contained highconcentrations of Target Compounds which fell outside the analytical rangeand were flagged with an '£'. An effective dilution was then performedand all concentrations affected by the dilution will be flagged with a'D'. Sample EAU53 was identified on the traffic report as being a sampl-ing blank. This sample contained £ target compounds, methylene chlorideand toluene. Since the preceding analyzed sample did not contain elevatelevels of these compounds, we do not beleive the reported values are aresult of caryover. The original, MS and USD comparisons along with

surrogate and internal standard recoveries were within the control limits

Release of the data contained in this hardcopy datacomput»r readable data submitted on floppy disketteby the laboratory manager or hi*signature.

package and in thehas b*tn authoriz*d

as verified by th* following

B«tty J. And*rshockTechnical R*vi*w*rflarch 17, 1989

Not*: This report 1* paginated for reference and accountability increasing numerical sequence.

de-


Lab Name: CQMPUCHEM LABS________ Contract: SAS4231E

Lab Code: CQMPU Case Mo.: QOQQ SAS Mo.: 4231E SDG No.EAW4Q

010203040506070809101112131415161718192021222324252627

EPASAMPLE NO.

EAW40EAW41EAW42EAW43EAW44EAW44REEAW45EAW46EAW47EAW48EAW50EAWS1EAW52EAW53EAW54EAW55EAWS6EAW56REEAW57EAW58EAWS9EAW59HSEAW59MSDVBLKSLVBLKVKVBLKBPVBLKVK

SI(TOL)f

10210710010098991021041021051051041041041031001009798110105971109810399102

52(BFB)#

9896909091979291909999100101949195929393103949198959995101

S3(DCE)#

959794969598981009710397989894959391919211296871079410192104

OTHER TOTOUT

000000000000000000000000000

QC LIMITS51 (TOL) - Toluene-d8 { 88-110)52 (BFB) * Bromofluorobenzene ( 86-115)53 (DCE) - l,2-Dichloroethane-d4 ( 76-114)

f Column to be used to flag recovery values

* Values outside of contract required QC limits

D Surrogates diluted out

page 1 of 1FORM II VOA-1 1/87 Rev,

3AWATER VOLATILE MATRIX SPIKE/MATRIX SPIKE DUPLICATE RECOVERY


Lab Code: COMPU Case No.: OQQQ SAS No.: 4231E SDG No.: EAW40

Matrix Spike - EPA Sampl« No.: BAH52______

COMPOUND

l,l-Dichloroethene_ . _TrichloroetheneBenzeneTolueneChlorobenzene

SPIKEADDED(ug/L)

12.512.512.512.512.5

SAMPLECONCENTRATION

(ug/L)00000

MSCONCENTRATION

(ug/L)17.614.314.715.013.9

MS%REC i

141114118120111

QCLIMITSREC.

61-14571-12076-12776-12575-130

COMPOUND

1, 1-Dichloroethene ____TrichloroetheneBenzeneTolueneChlorobenzene

SPIKEADDED(ug/L)

12.512.512.512.512.5

MSDCONCENTRATION

(ug/L)19.914.914.815.514.4

MSD%

REC #

159 *119118124115

%RPD #

-12-40

-3-4

QC LJRPD

1414111313

'HITSREC.

61-14571-12076-12776-12575-130

# Column to be used to flag recovery and RPD values with an asterisk

* Values outside of QC limits

RPD: _Q, out ofSpike Recovery: _

outside limitsout of 10 outside limits

COMMENTS: CLP ,4231,EEAW40,-EAW5,LOW,WATER,247678,PEST, ,TUNE: 0011 030789 0819

FORM III VOA-1 1/87 Rev,


Lab Name: coMPUCHEM LABS________ Contract: SAS4231E

Lab Code: COMPU Case Mo.: OOQQ SAS No.: 4231E SDG No.: EAW4Q

Lab File ID: CB8903Q7A11 Lab Sample ID: VBLKSL____

Date Analyzed: 03/07/89 Time Analyzed: 0930


Instrument ID: 11


0102030405

EPASAMPLE NO.

EAW40EAW41EAW53EAW59EAW59MS

LABSAMPLE 10

247654247655247672247678247657

LABFILE ID

CN047654B11CN047655B11CN047672A11CN047678B11CN047657B11

TIMEANALYZED

17071956144016261813


page 1 of 1FORM IV VOA 1/87 Rev,


Lab Name: COMPUCHEM LABS________ Contract: SAS4231E

Lab Code: COMPU Cas* Mo.: QQOQ SAS Mo.: 4231E SDG Mo.: EAW40

Lab File ID: CBB90307B11 Lab Sample. ID: VBLKVK____



Instrument ID: 11


010203040506070809

EPASAMPLE MO.

EAW42EAW43EAW44EAW44REEAW45EAW46EAW47EAW48EAW54

LABSAMPLE ID

247656247658247661247661247662247663247664247665247673

LABFILE ID

CN047656C11CN047658C11CM047661C11CR047661C11CR047662C11CN047663C11CN047664C11CH047665A11CR047673C11

TIMEANALYZED

003802120304043406100659074309020128


page 1 of 1FORM IV VOA 1/87 Rev.



Lab Code: COMPU Case No.: QOOQ SAS No.: 4231E SDG No.: EAW4Q

Lab File ID: CB89Q3Q8A11


Matrix: (soil/water) WATERInstrument ID: 11

Lab Sample ID: VBLKBP

Time Analyzed:

Level:(lov/med)

1231

LOW

THIS METHOD BLANK APPLIES TO THE FOLLOWING SAMPLES, MS AND MSD;


0102030405060708

EPASAMPLE NO.

EAW49EAW50EAW51EAW52EAW55EAW56EAW56REEAW57

LABSAMPLE ID

247667247669247670247671247674247675247675247676

LABFILE ID

CN047667A11CN047669A11CN047670A11CN047671A11CR047674B11CN047675B11CR047675B11CN047676B11

TIMEANALYZED

13251404144715241844165719252018

page 1 of 1FORM IV VGA 1/87 Rev.


Lab Name: COMPUCHEM LABS_________ Contract: SAS4231E

Lab Code: COMPU Case Mo.: QQQQ SAS No.: 4231E SDG No.: EAW40

Lab File ID: CB8903Q9B11 Lab Sample ID: VBLKVK____



Instrument ID: ll


0102

EPASAMPLE NO.

EAW58EAW59MSD

LABSAMPLE ID

247677247659

LABFILE ID

CR047677B11CR047659B11

TIMEANALYZED

21342213


page 1 of 1FORM IV VOA 1/87 Rev,


EPA SAMPLE NO.

Lab Name: COMPUCHEMVBLKSL

Lab Code: COMPU Case No.; 0000


Sample wt/vol: 20.0 (g/mL) MI.




GAS NO. COMPOUND

Contract: SAS4231E

SAS No.: 4231E SDG No.: EAW40

Lab Sample ID: VBLKSL____

Lab File ID: CB89Q307A11



Dilution Factor: 4.0 /. o


74-87-3——-——'Chloroinethane_________74-83-9-————Bromomethane__________75-01-4——————Vinyl Chloride_________75-00-3———————Chloroethane___________75-09-2———————Methylene Chloride______67-64-1———————Acetone_______________75-15-0———————Carbon Disulfide________75-35-4———————1,1-Dichloroethene______75-34-3——————1, l-Dichloroethane_____540-59-0——————1,2-Dichloro«thene (total).67-66-3-————Chloroforn___________107-06-2—————1,2-Dichloroethane_____78-93-3———--—2-Butanone____________71-55-6———————1,1,1-Trichloroe thane____56-23-5—————Carbon Tetrachloride____108-05-4——————Vinyl Acetate__________75-27-4——————Bromodichloromethane____78-87-5—-———-1,2-Dichloropropane_____10061-01-5-———cis-l,3-Dichloropropene__79-oi-s——————Trichloroethene________124-48-1——•>——— Dibromochloromethane____79-00-5———————1,1,2-Trichloroe thane____71-43-2——-——-Benzene _____________10061-02-6————Trans-1,3-Dichloropropene_75-25-2— -—-——Bromoforn____________108-10-1——————4-Methyl-2-Pentanone____591-78-6——————2-Hexanone____________127-18-4-————Tetrachloroethene_______79-34-5———————1,1,2,2-Tetrachloroethane_108-88-3—————Toluene ___________108-90-7—————Chlorobenzene_________100-41-4—————Ethylbenzene__________100-42-5——————Styrene_______________1330-20-7————Total Xylenes_________107-02-8—————Acrolein_____________107-13-1—————Acrylonitrile_________

FORM I VOA

10.80.912210.90.90.90.9141111111111121110.910.91122026

1/87 Rev,


EPA SAMPLE NO,


Lab Code: COMPU Case No.: OQOQ

Matrix: (soil/water) WATERSample wt/vol: 20.0 (g/»L) ML




Number Ties found: _a

VBLKSLContract: SAS4231E

SAS No.: 4231E SDG No.: EAW4Q

Lab Sample ID: VBLKSL____

Lab Pile ID: CB89Q3Q7A11



Dilution Factor: 4.0___





EPA SAMPLE NO.


Lab Code: COMPU case Mo.: QQOO


Sample wt/vol: 20.0 (g/mL) MLLevel: (low/med) LOW



VBLKVKContract: SAS4231E

SAS Mo.: 423IE SDG Ho.: EAW40

CAS NO. COMPOUND

Lab sample ID: VBLKVK

Lab File ID: CB8903Q7B11


Date Analyzed: 03/07/89A9*

Dilution Factor:


74-87-3-——————Chlorome thane__________74-83-9———————- Bromomethane _________75-01-4——————Vinyl Chloride________75-00-3-—————Chloroethane__________75-09-2——————Methylene Chloride_____67-64-1————————Acetone _____________75-15-0———————Carbon Diaulfide_______75-35-4——————1,1-Dichloroethene_____75-34-3——————1,1-Dichloroethane_____540-59-0——————1,2-Dichloroethene (total).67-66-3——•———Chloroform____________107-06-2——————1,2-Dichloroethane______78-93-3--————2-Butanone____________71-55-6——————1,1,1-Trichloroe thane___56-23-5——————Carbon Tetrachloride____108-05-4—————vinyl Acetate_________75-27-4——-———-Bromodichloromethane____78-87-s——————1,2-Dichloropropane_____10061-01-5————cis-l,3-Dichloropropene__79-01-6——————Trichloroethene________124-48-1-————Dibromochloromethane____79-00-5———————1,1,2-Trichloroethane____71-43 -2———-———Benzene_____________10061-02-6———Tran»-l,3-Dichloropropene_75-25-2——————Bromoforn____________108-10-1——————4-Methyl-2-Pentanone____591-78-6--————2-Hexanone____________127-18-4 ——•———Tetrachloroethene_______79-34-5——————l,l,2,2-Tetrachloroethane_108-88-3—————Toluene_____________108-90-7—————Chlorobenzene_________100-41-4—————Ethylbenzene__________100-42-5——————Styrene_______________1330-20-7————Total Xylenes_________107-02-8——————Acrolein______________107-13-1—————Acrylonitrile_________

FORM I VOA

10.80.913210.90.90.90.9141111111111121110.910.91122026

1/87 Rev,

ST


EPA SAMPLE NO

VBLKVKLab Name: CQMPUCHEM LABS________ Contract: SAS4231E

Lab Code: CQMPU Case No.: 0000 SAS No.: 4231B SDG No.: EAW4Q


Sample wt/voi: 20.0 (g/aL) ML

Leve1: (1ow/med) LOW




Lab Sample ID: VBLKVK____




Dilution Factor: 4-r»/.O *V




"50"

1AVOLATILE ORGAN ICS ANALYSIS DATA SHEET

EPA SAMPLE NO.


Lab Code: COMPU Case No.: QQQQ


Sample wt/vol: 2TQ.O (g/nL) m.




VBLKBPContract: SAS4231E

SAS NO.: 4231E SDG No.: EAW4Q

Lab Sample ID: VBLKBP____

Lab File ID: CB8903oaMi


Date Analyzed: 03/08/89A tr

Dilution Factor: <•*-»• (- ° s>


74-87-3—————Chloromethane_________74-83-9—————Bromomethane__________75-01-4———————Vinyl Chloride_________75-00-3——————chloroethane__________75-09-2——————Methylene Chloride_____67-64-1———————Acetone_______________75-15-0———————Carbon Disulfide_______75-35-4——————1,1-Dichloroethene_____75-34-3——————1,1-Dichloroethane_____540-59-0——————1,2-Dichloroethene (total)67-66-3-———-—Chloroform^,__________107-06-2—————1,2-Dichloroethane_____78-93-3——-———2-Butanone___________71-55-6——————1,1,1-Trichloroethane___56-23-5———————carbon Tetrachloride____108-05-4———-—Vinyl Acetate__________75-27-4——————Bromodichloromethane____78-87-5——————1,2-Dichloropropane_____10061-01-5————cis-l,3-Dichloropropene__79-01-6——————Trichloroethene_______124-48-1—•—-—Dibroaochloroaethane____79-00-5———————1,1,2-Trichloroethane____71-43-2——————Benzene_____________10061-02-6————Tran»-l,3-Dichloropropene__75-25-2—————-Bromoforw_____________108-10-1——————4-Methyl-2-Pentanone____591-78-6——————2-Hexanone____________127-18-4—————Tetrachloroethene______79-34-5——————1,1,2,2-Tetrachloroethane_108-88-3——————Toluene_______________108-90-7—————Chlorobenzene_________100-41-4——————Ethylbenzene___________100-42-5—————Styrene_____________1330-20-7————Total Xylenes_________107-02-8——————Acrolein______________107-13-1——————Acrylonitrile__________

FORK I VOA

10.80.912210.90.90.90.9141111111111121110.910.91122026

1/87 Rev,

^- .---*«.


EPA SAMPLE NO

Lab Name: CQMPUCHEM LABS_________

Lab Code: COMPU Case No.: OOQO


Sample vt/vol: 20.0 (g/mL) ML





VBLKBPContract: SAS4231E

SAS NO.: 4231E SDG No,: EAW4Q

Lab Sample ID: VBLKBP____

Lab File ID: CB89Q3Q8A11



Dilution Factor: a-ro /.O *\\*}





EPA SAMPLE NO.

Lab Ham*: coMPPCHEM LABS_________

Lab Code: COMPU Case Ho.: 0000


Sample wt/vol: 20.0 (g/mL) ML


% Moimture: not dec. ___

column; (pack/cap) PACK


SAS MO.: 4231E SDG Mo.: EAW4Q

Lab Sample ID: VBLKVK


Date Received:

CAS NO. COMPOUND


Dilution Factor:


74-87-3—--———Chlorome thane__________74-83-9-———«—Bromomethan*___________75-01-4——————Vinyl Chloride________75-00-3——————Chloroethan*___________75-09-2———————Methylene Chloride______67-64-1——————Acetone_______________75-15-0——————Carbon Disuifide_______75-35-4——————1, l-Dichloroethen«_____75-34-3———————1,1-Dichloroethane______540-59-0—————1,2-Dichloroethene (total).67-66-3---——-Chlorofora___________107-06-2—————1,2-Dichloroethane_____78-93-3—————2-Butanone____________71-55-6———————1,1,1-Trichloroe thane___56-23-5——————Carbon Tetrachloride____108-05-4——————Vinyl Acetate__________75-27-4-————Bromodichloromethane____78-87-5———————1,2-Dichloropropane_____10061-oi-s————ci*-i,3-Dichloropropen«__79-01-6——————Trichloroeth«ne________124-48-1--———-Dibromochloromethane____79-00-5———————1,1,2-Trichloroethane____71-43-2———-——Benzene_______________10061-02-6——™Tran«-l,3-Dichloropropene_75-25-2—————-Bromoform_____________108-10-1——————4-Methyl-2-P«ntanone____591-78-6——————2-Hexanone____________127-18-4——————Tetrachloroethene_______79-34-5——————l,l,2,2-Tetrachloroethane_108-88-3-—-——-Toluene______________108-90-7—————Chlorobenzene__________100-41-4——————Ethylbenzene___________100-42-5——————Styrene______________1330-20-7—————Total Xylenes__________107-02-8——————Acrolein______________107-13-1——————Acrylonitril*__________

2026

10.80.912510000141111111111121110.910.9112



EPA SAMPLE NO


Lab Code: COMPU Case No.: QOOQ

Matrix: (soil/water) WATERSample wt/vol: 20.0 (g/nL) ML


* Moisture: not dec. ___




SAS No,: A231E SDG No.: EAW40

Lab Sample ID: VBLKVK___Lab File ID: CB89Q3Q9B11


Date Analyzed: 03/09/89tij

Dilution Factor:




VOLATILE ORGANI' 5 ANALYSIS DATA SHEET


Lab Code: CQMPU Case No.: 0000






CAS NO. COMPOUND


SAS NO.: 4231E SDG NO.: EAW40




Date Analyzed: 03/07/89nt

Dilution Factor:


74-87-3——————chloroaethane_________74-83-9——————-Bromomethane___________75-01-4——————Vinyl Chloride_________75-00-3——————-Chloroethane___________75-09-2———————Methylene Chloride______67-64-1——————Acetone_______________75-15-0——————Carbon Di»ulfide_______75-35-4——————1,1-Dichloroethene_____75-34-3———————1,1-Dichloroethane______540-59-0——————l,2-Dichlor3ethene (total).67-66-3——————Chloroform____________107-06-2——————1,2-Dichloroethane______78-93-3——————2-Butanone____________71-55-6———————1,1,1-Trichloroe thane____56-23-5——————Carbon Tetrachloride____108-05-4—————Vinyl Acetate_________75-27-4—————-Bronodichlorome thane____78-87-5——————1,2-Dichloropropane_____10061-01-5————cis-l,3-Dichloropropene__79-01-6——————Trichloroethene________124-48-1——————Dibromochloromethane_____79-00-5———————1,1,2-Trichloroethane____71-43-2™————Benzene_______________10061-02-6————Trans-l,3-Dichloropropene__75-25-2——————- Bromofor»______________108-10-1————---4-Methyl-2-Pentanone_____591-78-6——————2-Hexanone____________127-18-4 —————Tetrachloroethene______79-34-5———————l,l,2,2-Tetrachloroethane_108-88-3——-———Toluene_______________108-90-7—————-Chlorobenzene__________100-41-4—————Ethylbenzene__________100-42-5——————Styrene_______________1330-20-7————Total Xylenea_________107-02-8—————Acrolein_____________107-13-1—————Acrylonitrile_________

o.a0.9

210.90.90.90.9141111111111121110.910.91122026

FORM I VOA 1/87 Rev


EPA SAMPLE NO


Lab Code: CQMPU Case No.! OQOQ













Dilution Factor:





EPA SAMPLE NO.


Lab Code: COMPU Case Mo.: QQQQ




t Moisture: not dec. ___



SAS NO.: 4231E SDG No.: EAW40

CAS NO. COMPOUND





Dilution Factor:

CONCENTRATION UNITS:(ug/L or ug/Kg) Ufl/L

74-87-3—————Chloromethane_________74-83-9--———--Bromomethane___________75-01-4———————Vinyl Chloride_________75-00-3—————Chloroe thane__________75-09-2——————Methylen* Chloride_____67-64-1———————Acetone_______________75-15-0———————Carbon Disulfide_______

• 75-35-4———————1,1-Dichloroethene______75-34-3——————1,1-Dichloroethane______540-59-0—————l,2-Dichloroeth*ne (total),67-66-3—————Chloroforn___________107-06-2——————1,2-Dichloroethane______78-93-3————•—- 2-Butanone,____________71-55-6——————1,1, l-Trichloroethane___56-23-5——————Carbon T«trachloride____108-05-4—————Vinyl Acetate_________75-27-4-————-Bromodichlorone thane____78-87-5—————1,2-Dichloropropane_____10061-01-5————cis-l,3-Dichloropropene__79-01-6——————Trichloro«thene_______124-48-1—————-Dibromochlorome thane____79-00-5———————1,1,2-Trichloroethane___71-43-2——-——Benzene______________10061-02-6————Trana-l,3-Dichloropropene_75-25-2-—-——-Bromofonn___________108-10-1——————4-Methyl-2-Pentanone____591-78-6—————2-Hexanon«___________127-18-4—————Tetrachloroethene_______79-34-5——————1,1,2,2-T«trachloroethane_108-88-3-———-—Toluene_______________108-90-7—————Chlorobenzene_________100-41-4—————Ethylbenzene__________100-42-5—————Styrene_____________1330-20-7—————Total Xylenee__________107-02-8—————Acrolein_____________107-13-1—————Acrylonitrile_________

FORM I VOA

10.80.912210.90.90.90.9141111111111121110.910.91122026

1/87 Rev,


EPA SAMPLE NO


Lab Code: COMPU Case Mo.: QOQQMatrix: (soil/water) WATER


Leva1: (1ow/med) LOW



Number Tics found: _Q,







Dilution Factor: 4-i-a /. Q


CAS NUMBER COMPOUND NAME RT EST. COMC. Q


-1AVOLATILE ORGANICS ANALYSIS DATA SHEET

EPA SAMPLE NO.


Lab Code: CQMPU Casa No.: QOQQ






CAS NO. COMPOUND


SAS NO.: 4231B SDG No.: EAW40





Dilution Factor:


74-87-3———-——Chlorome thane__________74-83-9—-————-Bromomethane___________75-01-4——————vinyl Chloride________75-00-3——-——Chloroethane__________75-09-2——————Methylene Chloride______67-64-1——————Acetone_______________75-15-0——————Carbon Dimulfide_______75-35-4——————1, l-Dichloroethene_____75-34-3——————l,l-Dichloro« thane_____540-59-0——————1,2-Dichloroethene (total).67-66-3——————Chloroform____________107-06-2——————1,2-Dichloroethane______78-93-3——————2-Butanon«___________71-55-6——————1,1,1-Trichloroethane___56-23-5——————Carbon Tetrachloride____108-05-4—————Vinyl Acetate_________75-27-4———«-— Bromodichlorome thane____78-87-5——————'1,2-Dichloropropane_____10061-01-5———cis-l,3-Dichloropropene__79-01-6——————Trichloroethene________124-48-1—————Dibromochlorome thane____79-00-5———————1,1,2-Trichloroethane____71-43-2---————Benzene_______________10061-02-6———Tran»-l,3-Dichloropropena_75-25-2—-——-—Bromoforn____________103-10-1——————4-Methyl-2-Pentanone____591-78-6——————2-Hexanone____________127-18-4-———-—Tetrachloroethene_______79-34-5——————l,l,2,2-Tetrachloroethane_108-88-3——————Toluene ____________108-90-7——————Chlorobenzene__________100-41-4——————Ethylbenzene___________100-42-5—————Styrene_____________1330-20-7————Total Xylenee_________107-02-8——————Acrolein______________107-13-1—————Acrylonitrile_________

FORM I VGA

10.80.912210.90.90.90.9141211111111112110.60.910.91122026

1/87 Rev,


EPA SAMPLE NO


Lab Code: CQMPO case No.: QOOQ






Number Tics found: _0.




Lab Pile ID: CN047656C11



Dilution Factor:




492~


1EPA SAMPLE NO.


Lab Code: COMPU Case Mo.: QQQQ




\ Moisture: not dec. ___



SAS No.: 4231B SDG No.: EAW40


Lab File ID: CNQ47658C11



Dilution Factor: 4-rS- /./\


74-87-3—————-chloromethane_________74-83-9————•——Bromomethane___________75-01-4——————Vinyl Chloride________75-00-3——————chloroethane__________75-09-2——————Methylena chloride_____67-64-1————•——Acetone_______________75-15-0———————Carbon Diaulfide_______75-35-4——————1,1-Dichloroethene_____75-34-3——————1,1-Dichloroe thane_____540-59-0—————1,2-Dichloroethene (total),67-66-3——-———Chlorofon^__________107-06-2—————1,2-Dichloroethane_____78-93-3————-'—-2-Butanone___________71-55-6———————1,1,1-Trichloroethane____56-23-5——————Carbon Tetrachloride____108-05-4——————Vinyl Acetate__________75-27-4——————Bromodichlorone thane____78-87-5——————1,2-Dichloropropane_____10061-01-5—-——cis-i,3-Dichloropropene__79-01-6——————Trichloroethene_______124-48-1——--—Dibromochloromethane____79-00-5——————1,1,2-Trichloroethane___71-43-2——————Benzene..______________10061-02-6———-Tran»-l,3-Dichloropropene_75-25-2—-———-Broaofor«^____________108-10-1——————4-Methyl-2-Pentanone____591-78-6——————2-Hexanone____________127-18-4—————Tetrachloroethene______79-34-5——————1,1,2,2-Tatrachloroethane_108-38-3™———-Toluene______________108-90-7—————Chlorobenzene_________100-41-4—————Ethylbenzen«_________100-42-5—————Styrene_____________1330-20-7—————Total Xylenes__________107-02-8——————Acrolein______;_______107-13-1—————Acrylonitrile_________

FORM I VOA

10.80.912

1310.90.90.90.9141111111111121110.910.91122026

1/87 Rev.


EPA SAMPLE NO


Lab Coda: CQMPU Case No.: QOQQ






Number TICs found:







Dilution Factor:





EPA SAMPLE NO


Lab Code: CQMPU Case No.: QOQO


Sample wt/voi: 20.0 (g/mL) ML




EAW44Contract: SAS4231B





Date Analyzed: 03/08/89a *>

Dilution Factor: 4-i-9 /.Q


74-87-3——————Chlorome thane__________74-83-9—————-Bromomethane___________75-01-4——————Vinyl Chloride________75-00-3——--———Chloroethane__________75-09-2——————Methylene Chloride______67-64-1———————Acetone_______________75-15-0———————Carbon Disulfide_______75-35-4———————1,1-Dichloroethene______75-34-3——————1,1-Dichloroethane_____540-59-0——————1,2-Dichloroethene (total).67-66-3——————-Chloroform____________107-06-2——————1,2-Dichloroethane______78-93-3™——— 2-Butanone __________71-55-6——————1,1,1-Trichloroethane___56-23-5—————Carbon Tetrachloride____108-05-4—————Vinyl Acetate_________75-27-4——————Bromodi chlorome thane____78-87-5——————1,2-Dichloropropane_____10061-01-5————cis-l,3-Dichloropropene__79-01-6———————Trichloroethene________124-48-1————-Dibromochloromethane____79-00-5———————1,1,2-Trichloroethane____71-43-2-—————Benzene^^.____________10061-02-6————Trans-l,3-Dichloropropene_75-25-2————•—- Bromoform_____________108-10-1——————4-Methyl-2-Pentanone____591-78-6——————2-Hexanone____________127-18-4——————Tetrachloroethene_______79-34-5——————1,1,2,2-Tetrachloroethane__108-88-3——————Toluene_______________108-90-7——————Chlorobenzene__________100-41-4——————Ethylbenzene___________100-42-5——————Styrene_______________1330-20-7————Total Xylenes_________107-02-8——————Acrolein______________107-13-1—————Acrylonitrile_________

FORM I VOA

10,20.2

11010,620.141111110,111121160,10.21182026

1/87 Rev,


EPA SAMPLE NO



Matrix: (soil/water) WATERSample vt/vol: 20.0 (g/mL) ML




Number TICs found:







Dilution Factor: +r* /• Q





EPA SAMPLE NO.

EAW44RELab Name: CQMPUCHEM LABS_________ Contract :r SAS4231E

Lab Code: COMPU Case No.: 0000 SAS No.: 4231E SDG No.: EAW4Q



Lave1: (1ow/med) LOW



CAS NO. COMPOUND


Lab File ID: CRQ47661C11



Dilution Factor:


74-87-3———————Chlorome thane__________74-83-9———-———Bromomethane___________75-01-4——————vinyl Chloride________75-00-3—————- Chloroethane___________75-09-2——————Methylene Chloride_____67-64-1———————Acetone_______________75-15-0———————Carbon Dieulfide_______75-35-4——————1,1-Dichloroethene_____75-34-3——————l,l-Dichloroethane_____540-59-0——————1,2-Dichloroethene (total).67-66-3—————chloroform___________107-06-2——————1,2-Dichloroethane______78-93-3——————2-Butanone____________71-55-6——————1,1,1-Trichloroethane___56-23-5——————Carbon Tetrachloride____108-05-4—————Vinyl Acetate_________75-27-4—————Bronodichlorome thane____78-87-5————™1,2-Dichloropropane_____10061-01-5--—--ci»-l,3-Dichloropropene__79-01-6——————Trichloroethene________124-48-1——•———— Dibromochloromethane_____79-00-5———————1,1,2-Trichloroethane____71-43-2———--—Benzene ____________10061-02-6————•Tran»-l,3-Dichloropropene_75-25-2———™—Bromofom_____________108-10-1——————4-Methyl-2-Pentanone____591-78-6——————2-Hexanone____________127-18-4—————Tetrachloroethene______79-34-5——————l,l,2,2-Tetrachloroethane_108-88-3-——---Toluene_____________108-90-7—————chlorobenzene_________100-41-4——————Ethylbenzene___________100-42-5——————Styrene_______________1330-20-7—————Total Xylenes__________107-02-8—————Acrolein_____________107-13-1——————Acrylonitrile__________

FORM I VOA

32134

1103252231133333333343433523223155066

UuDJ

DUUDDJUUUUUUUUUUUuuuuuuDUUUDJUDUU

1/87 Rev


EPA SAMPLE NO.

Lab Name: COMPUCHEM LABS________

Lab Code: COMPU _ Case No.: QQQQMatrix: (soil/water) WATER

Sample wt/vol: 8.0 (g/mL) MLLevel: (low/mad) LOW



Number TICs found: _fi



Lab Sample ID: 247661_____

Lab File ID: CR047661CH



Dilution Factor: -A fr /.•n J//I/F




436


EPA SAMPLE NO.


Lab Code: COMPU Case Mo.: QOOQ






,EAW45

Contract: SAS4231E


CAS NO. COMPOUND


Lab File ID: CR047662C11



Dilution Factor: -*re- /.o


74-87-3———————Chloromethane__________74-83-9——————Bromomethane__________75-01-4——————vinyl Chloride________75-00-3——————Chloroethane ________75-09-2——————Methylene Chloride_____67-64-1——————Acetone_______________75-15-0——————Carbon Disulfide_______75-35-4——————1,1-Dichloroethene_____75-34-3——————l, l-Dichloroethane_____540-59-0—————1,2-Dichloroethene (total)67-66-3———————Chloroform____________107-06-2—————1,2-Dichloroethane_____78-93-3——————2-Butanone___________71-55-6——————1,1,1-Trichloroethane___56-23-5——————Carbon Tetrachloride____108-05-4—————Vinyl Acetate_________75-27-4——————Bromodi Chloromethane____78-87-5——————1,2-Dichloropropane_____10061-01-5————cis-l,3-Dichloroprbpene__79-01-6——————Trichloroethene________124-48-1—•—•——Dibromochloronethane____79-00-5-—————-1,1,2-Trichloroethane___71-43-2———————• Benzene ______________10061-02-6-———Trana-l,3-Dichloropropene_75-25-2————™-Bromoform^____________108-10-1——————4-Methyl-2-Pentanone____591-78-6——————2-Hexanone____________127-18-4——————Tetrachloroethene_______79-34-5———————l,l,2,2-Tetrachloroethane_108-88-3—————Toluene...____________108-90-7™——Chlorobenz«ne________100-41-4—————Ethylbenzen*__________100-42-5——————Styrene______________1330-20-7————Total Xylenes_________107-02-8—————Acrolein_____________107-13-1—————Acrylonitrile_________

FORM I VGA

10.80.912210.920.90.9141111111111121110.910.91122026

1/87 Rev.


EPA SAMPLE NO














Date Analyzed: 03/08/89tfft

Dilution Factor: 4-rft /.o


CAS NUMBER

1.2. 75-43-4

COMPOUND NAME

UNKNOWNMETHANE , DICHLOROFLUORO-

RT

0.451.38

EST. CONC.

2.03.0

Q

JJ



EPA SAMPLE NO.\


Lab Coda: CQMPU Case Mo.: QQQQ






EAW46Contract: SA54231E

SAS HO.: 4231E SDG No.: EAW40

GAS NO. COMPOUND




Date Analyzed: 03/08/89AH

Dilution Factor:CONCENTRATION UNITS:(ug/L or ug/Kg) UG/L

74-87-3——————chloromethane__________74-83-9——————'Bromomethane___________75-01-4———————Vinyl Chloride_________75-00-3——————Chloroethane___________75-09-2——————Methylene Chloride_____67-64-1——————Acetone_______________75-15-0———————Carbon Disulfide_______75-35-4——————i,l-Dichloroethene_____75-34-3——————1,1-Dichloroethane_____540-59-0—————1,2-Dichloroethene (total),67-66-3-—————Chloroform____________107-06-2——————1,2-Dichloroethane______78-93-3—————2-Butanone___________71-55-6———————1,1,1-Trichloroethane____56-23-5——————carbon Tetrachloride____108-05-4—————Vinyl Acetate_________75-27-4——————Bromodi chloromethane____78-87-5———————1,2-Dichloropropane_____10061-01-5————cis-l,3-Dichloropropene__79-01-6——•———Trichloroethene_______124-48-1—————"-Dibromochloroaethane_____79-00-5———————1,1,2-Trichloroethane____71-43-2——« —— Benzene—____________10061-02-6——--Trans-l,3-Dichloropropene__75-25-2————*---Bromofora____________108-10-1——————4-Methyl-2-Pentanone____591-78-6—————2-Hexanone___________127-18-4—————Tetrachloroethene______79-34-5——————l,l,2,2-Tetrachloroethane_108-88-3—————Toluene—____________108-90-7————-Chlorobenzene_________100-41-4——————Ethylbenzene___________100-42-5——————Styrene______________1330-20-7—————Total Xylenea__________107-02-8——————Acrolein______________107-13-1—————Acrylonitrile_________

FORM I VOA

10.8112210.9120.9141111112111121110.910.91122026

1/87 Rev,


EPA SAMPLE NO.








Number TICs found:







Dilution Factor: -*rO /.o


CAS NUMBER

1.2. 75-43-4

COMPOUND NAME


RT

0.471.38

EST. CONC.

3.04.0

Q

JJ



EPA SAMPLE NO.


Lab Code: COMPU Case No.: OQQQ








CAS NO. COMPOUND




Date Analyzed: 03/08/89£?Dilution Factor: -t^o- /. O «'


74-87-3———————Chlorome thane__________74-83-9————-—Bromom«thane___________75-01-4——————vinyl chloride________75-00-3———-——Chloroethane^_________75-09-2——————Methylene Chloride______67-64-1-———————Acetone __________75-15-0——————Carbon Diaulfide_______75-35-4——————l,l-Dichloroethene_____75-34-3——————1,1-Dichloroethane_____540-59-0——————1,2-Dichloroethene (total).67-66-3——————-Chlorofona____________107-06-2——————1,2-Dichloroethane______78-93-3-——•——-2-Butanone____________71-55-6——————1,1,1-Trichloroethane___56-23-5——————Carbon Tetrachloride____108-05-4—————Vinyl Acetate_________75-27-4—————"Bromodichloromethane____78-87-5———-——1,2-Dichloropropane_____10061-01-5————cis-l,3-Dichloropropene__79-01-6——————Trichloroethene________124-48-1————— Dibromochloronethane____79-00-5——————1,1,2-Trichloroethane____71-43-2——-———Benzene_______________10061-02-6————Tran»-l,3-Dichloropropene_75-25-2————•-—Bronoforn ___________108-10-1—————4-Methyl-2-Pentanone____591-78-6——————2-Hexanone____________127-18-4—————Tetrachloroethene______79-34-5——————l,l,2,2-Tetrachloroethane__108-88-3——————Toluene_______________108-90-7-—————Chlorobenzene__________100-41-4——————Ethylbenzene___________100-42-5——————Styrene_______________1330-20-7————Total Xylenes_________107-02-8——————Acrolein______________107-13-1—————Acrylonitrile_________

10.8112210.9220.9141111112111121110.910.91122026



EPA SAMPLE NO.


Lab Coda: CQMPU cas* No.: QQQO

Matrix: (soil/water) WATERSample wt/vol: 20.0 (g/nL) ML




Number TICs found:







Dilution Factor: *ro- />S>


CAS NUMBER

1.2. 75-43-4

COMPOUND NAME


RT

0.471.38

EST. CONC,

3.04.0

Q

JJ


37Z


EPA SAMPLE NO.


Lab Code: COMPU Case Mo.: QQOO


Sample wt/voi: 20.Q (g/mL) ML






CAS NO. COMPOUND


Lab File ID: CN047665A11



Dilution Factor: +r* /.o


74-87-3————— -Chloromethane__________74-83-9——————Bromomethane___________75-01-4——————vinyl Chloride________75-00-3——————Chloroethane__________75-09-2——————Methylene Chloride_____67-64-1———————Acetone_______________75-15-0——————Carbon Disulfide_______75-35-4——————1,1-Dichloroethene______75-34-3———————1,1-Dichloroethane______540-59-0—————1,2-Dichloroethene (total).67-66-3---————Chloroform ____________107-06-2——————1,2-Dichloroethane______78-93-3——————2-Butanone____________71-55-6——————1,1,1-Trichloroethane___56-23-5——————Carbon Tetrachloride____loa-05-4—————Vinyl Acetate_________75-27-4———«——Bromodichloronethane____78-87-s——————1,2-Dichloropropane_____10061-01-5————ci»-l,3-Dichloropropene__79-01-6———-——Trichloroethene________124-48-1-————-Dibromochloromethane____79-00-5———————1,1,2-Trichloroethane___71-43-2———————Benzene_______________10061-02-6——--Tranm-1,3-Dichloropropene_75-25-2™———-Bromoforn_____________108-10-1——————4-Methyl-2-Pentanone____591-78-6——————2-Hexanone____________127-18-4————-Tetrachloroethene_______79-34-5———————l,l,2,2-Tetrachloroethane_108-88-3—•—————Toluene ____________los-90-7—————Chlorobenzene________100-41-4—————Ethylbenzene__________100-42-5—————styrene_____________1330-20-7————Total Xylenea_________107-02-8——————Acrolein______________107-13-1—————Acrylonitrile_________

FORM I VOA

10.80.912210.90.90.90.9141111111111121110.910.91122026

1/87 Rev,

351


EPA SAMPLE NO.


Lab Code: COMPU Case No.: QQQO


Sample wt/vol: 20.0 (g/mL) MLLevel: (1ow/med) LOW



Number TICs found: _fi

EAW43Contract: SAS423IE






Dilution Factor:


<;* _. »//v n




EPA SAMPLE NO.


Lab Code: CQMPU Case No.: QQQQ






CAS NO. COMPOUND

EAW4*Contract: SAS4231E

SAS NO.: 4231E SDG NO.: EAW4Q


Lab File ID: CNQ47667AH



Dilution Factor:


74-87-3————-—Chlorome thane__________74-83-9—————Bromomethane___________75-01-4——————Vinyl Chloride_________75-00-3—————--Chloroe thane___________75-09-2——————Methylene Chloride______67-64-1——————Acetone_______________75-15-0——————Carbon Disulfide_______75-35-4——————1,1-Dichloroethene_____75-34-3——————1,1-Dichloroethane_____540-59-0——————1,2-Dichloroethene (total).67-66-3———————Chloroform____________107-06-2——————1,2-Dichloroe thane______78-93-3———— —— 2-Butanone___________71-55-6——————1,1,1-Trichloroethane___56-23-5——————Carbon Tetrachloride____108-05-4——————Vinyl Acetate__________75-27-4——————Bromodichloromethane____78-87-5———————1,2-Dichloropropane_____10061-01-5———-cis-l,3-Dichloropropene__79-01-6——————Trichloroethene_______124-48-1————-Dibromochloromethane____79-00-5——————1,1,2-Trichloroethane____71-43-2—————-—Benzene ___________10061-02-6--———Tran»-l,3-Dichloropropene_75-25-2——------ Bromoform,_____________108-10-1—————4-Methyl-2-Pentanone____591-78-6——————2-Hexanone____________127-18-4——————Tetrachloroethene_______79-34-5——————l,l,2,2-Tetrachloroethane_108-88-3-—————Toluene_______________108-90-7—————-Chlorobenzene__________100-41-4——————Ethylbenzene___________100-42 - 5—————Sty rene_____________1330-20-7—————Total Xylenee__________107-02-8—————Acrolein_____________107-13-1—————Acrylonitrile_________

10.80.912210.90.90.90.9141111111111121120.920.9131

342026



EPA SAMPLE NO

EAW49Lab Nam«: COWPUCHEM IABS ____ Contract: SAS4231E

Lab Coda: CQWPU Case No.: QQOQ SAS No.: 4231E SDG No.: EAWBO








Lab File ID: CNQ47667AH



Dilution Factor: 4r-6- /, o


CAS NUMBER

1.

COMPOUND NAME

FREON

RT

12.99

EST. CONC.

3.0

Q

3P



EPA SAMPLE NO.


Lab Code: COMPU Cast Ho.: QQQQ






CAS NO. COMPOUND




Lab File ID: CNQ47669A11


Date Analyzed: 03/08/89.•!«

Dilution Factor:


74-87-3——————-Chloromethane._________74-83-9———————Bromomethanei___________75-01-4——————Vinyl Chloride________75-00-3———————Chl or oe thane___________75-09-2——————Methylene Chloride_____67-64-1————————Acetone _____________75-15-0——————Carbon Disulfide_______75-35-4——————1,1-Dichloroethene_____75-34-3——————1, l-Dichloroethane_____540-59-0—————1,2-Dichloroethene (total)67-66-3——————Chloroforn____________107-06-2——————1,2-Dichloroethane______78-93-3———————2-But an one __________71-55-6———————1,1,1-Trichloroethane____56-23-5——————Carbon Tetrachloride____108-05-4————-Vinyl Acetate__________75-27-4——————Bromodi chlorome thane____78-87-5————-1,2-Dichloropropane_____10061-01-5————cis-l,3-Dichloropropene__79-01-6—————Trichloroethene________124-48-1—————Dibromochloromethane____79-00-5———————1,1,2-Trichloroethane____71-43-2 ————-—Benzene ____________10061-02-6————Trane-1,3-Dichloropropene__75-25-2——————Bromofona ___________108-10-1———"——4-Methyl-2-Pentanone____591-78-6———~ -2-Hexanone_____________127-18-4————•—Tetrachloroethene_______79-34-5——————1,1,2,2-Tetrachloroethane_108-88-3——————Toluene ___________108-90-7————Chlorobenzene_________100-41-4——————Ethylbenzen*___________100-42-5——————Styrene_______________1330-20-7————Total Xylenea_________107-02-8——————Acrolein______________107-13-1—————Acrylonitrile_________

FORM I VGA

10.80.912210.90.90.90.9141111111111121110.910.0112

2026

1/87 Rev,


EPA SAMPLE NO

Lab Name: COMEUCHEM LABS__________

Lab Code: coMPU Case No.: OOOQ

Matrix: (soil/water) WATERSample wt/vol: 20.0 (g/mL) MI.





EAW50contract: SAS4231S

SAS NO.: 423IE SDG No.: EAW4Q


Lab Pile ID: CNQ47669A11



Dilution Factor:


/. o *




EPA SAMPLE NO.










CAS NO. COMPOUND


Lab File ID: CNQ47670A11



Dilution Factor: 4 • o /> o


74-87-3——-——-Chloromethane_________74-83-9-———-—Bromomethane___________75-01-4——————Vinyl Chloride_________75-00-3——————Chloroe thane__________75-09-2——————Methylene Chloride______67-64-1——————Acetone_______________75-15-0——————Carbon Disulfide_______75-35-4——————1,1-Dichloroethene______75-34-3——————1, l-Dichloroe thane______540-59-0——————1,2-Dichloroethene (total),67-66-3————•——Chloroform ___________107-06-2——————1,2-Dichloroe thane______78-93-3———--—2-Butanone____________71-55-6——————1,1,1-Trichloroethane___56-23-5™———Carbon Tetrachloride____108-05-4——————Vinyl Acetate__________75-27-4———-———Bromodi chloromethane____78-87-5——————-1,2-Dichloropropane_____10061-01-5———cis-l,3-Dichloropropene__79-01-6——————Trichloroethene________124-48-1——-———Dibromochlorome thane____79-00-5———————1,1,2-Trichloroethane____71-4 3-2-™———Benzene_______________10061-02-6-™—Tran»-l,3-Dichloropropene_75-25-2———«—Bromoform____________108-10-1—————4-Methyl-2-Pentanone____591-78-6—————2-Hexanone___________127-18-4———«-Tetrachloroethene_______79-34-5———————l,l,2,2-Tetrachloroethane_108-88-3™———-Toluene^_____________108-90-7——————Chlorobenzene__________100-41-4—————Ethylbenzen*__________100-42-5——————Styrene_______________1330-20-7————Total Xylenes_________107-02-8——————Acrolein______________107-13-1—————Acrylonitrile_________

FORM I VOA

l0.80.912210.90.90.90.9141111111111121110.910.91122026

1/87 Rev,


EPA SAMPLE NO


Lab Code: CQMPU Case NO.: QQQQMatrix: (soil/water) WATER





Number TICs found:



Lab Sample ID: 24767Q

Lab Pile ID: CN04767QA11



Dilution Factor: 4-rO f.o


(JJA.




EPAJ

SA&PLE NO.


Lab Code: COMPU Case No.: QQOQMatrix: (soil/water) WATER





CAS NO. COMPOUND







Dilution Factor:


74-87-3——*——Chlorome thane_________74-83-9——•———Bromomethane___________75-01-4——————Vinyl Chloride________75-00-3——————Chloroethane___________75-09-2———————Methylene Chloride______67-64-1———————Acetone_______________75-15-0———————Carbon Diaulfide_______75-35-4——————1,1-Dichloroethene_____75-34-3——————1,1-Dichloroe thane_____540-59-0——————1,2-Dichloroethene (total).67-66-3—————Chloroform.__________107-06-2—————1,2-Dichloroethane_____78-93-3——————2-Butanone____________71-55-6——————i, i, l-Trichloroethane___56-23-5-—————Carbon Tetrachloride____108-05-4—————vinyl Acetate_________75-27-4——————Bromodichlorone thane____78-87-5—————-1,2-Dichloropropane_____10061-01-5————cis-1,3-Dichloropropene__79-01-6——————Trichloroethene________124-48-1——•———Dibromochloroinethane____79-00-5——————1,1,2-Trichloroethane___71-43-2————-—Benzene______________10061-02-6————Tran»-l,3-Dichloropropene_75-25-2—————Bromofora*_____________108-10-1——————4-Methyl-2-Pentanone____591-78-6——————2-Hexanone____________127-18-4 ——•——Tetrachloroethene______79-34-5———————l,l,2,2-Tetrachloroethane_108-88-3—————Toluene_____________108-90-7—————Chlorobenzene_________100-41-4—————Ethylbenzene__________100-42-5—————styrene_____________1330-20-7————Total Xylenes_________107-02-8—————Acrolein_____________107-13-1—————Acrylonitrile_________

FORM I VOA

10.30.912210.90.90.90.9141111111111121110.910.91122026

1/87 Rev,


EPA SAMPLE NO


Lab Code: COMPU Case No.t QQQQ






Number TICs found:







Dilution Factor: +rtt- f.Q





EPA SAMPLE NO.


Lab Code: COMPU case Ho.: QQQO


Sample wt/voi: 20.0 (g/mL) ML






CAS NO. COMPOUND





Dilution Factor: 4~» I-O


74-87-3———-———Chl or one thane__________74-83-9———•———Bromomethane___________75-01-4——————Vinyl Chloride_________75-00-3—-———--Chloroe thane___________75-09-2——————Methylene Chloride______67-64-1———————Acetone_______________75-15-0———————Carbon Disulfide_______75-35-4———————1,1-Dichloroethene______75-34-3——————1,1-Dichloroethane_____540-59-0—————1,2-Dichloroethene (total),67-66-3-———-—Chloroform___________107-06-2——————1,2-Dichloroethane______78-93-3—----——-2-Butanone____________71-55-6———————1,1,1-Trichloroethane____56-23-5———————Carbon Tetrachloride____108-05-4—————Vinyl Acetate_________75-27-4—————— Bromodi chl orome thane____78-87-5———-——1,2-Dichloropropane_____10061-01-5————cis-l,3-Dichloropropene__79-01-6——————Trichloroethene________124-48 -1—-———Dibromochloromethane____79-00-5———————1,1,2-Trichloroethane____71-43-2—————-—Benzene_______________10061-02-6™-—Trans-l, 3-Dichloropropene_75-25-2™————Bromofona______________108-10-1——————4-Methyl-2-Pentanone____591-78-6————— 2-Hexanone____________127-18-4—————Tetrachloroethene______79-34-5———————l,l,2,2-Tetrachloroethane_108-88-3—————Toluene_______________108-90-7™——-Chlorobenzen«_________100-41-4—————Ethylbenzene__________100-42-5——————Styrene_______________1330-20-7—————Total Xylenes__________107-02-8——————Acrolein______________107-13-1—————Acrylonitrile_________

FORM I VOA

0.80.9

10.90.90.90.9141111111111121110.90.70.91122026

1/87 Rev

28y


EPA SAMPLE NO


Lab Code: COMPU Case No.: QOQO




.% Moisture: not dec, ___


Number TICs found: _0.

EAWS3Contract: SAS4231E






Dilution Factor: 4-ro /.o




IAVOLATILE ORGANICS ANALYSIS DATA SHEET

EPA SAMPLE NO.


Lab Code: COMPU Case No.: QQOQ












CAS NO. COMPOUND

Dilution Factor: 4-rO- l.O

QCONCENTRATION UNITS:(ug/L or ug/Kg) UG/L

74-87-3——————Chloromethane__________74-83-9 —•————Bromome thane___________75-01-4——————Vinyl Chloride_________75-00-3——————-Chloroethane___________75-09-2——————Methylene Chloride_____67-64-1——————Acetone_______________75-15-0———————Carbon Diaulfide_______75-35-4———————1,1-Dichloroethene______75-34-3———————1,1-Dichloroethane______540-59-0——————1,2-Dichloroethene (total).67-66-3—-————Chloroforw____________107-06-2—————1,2-Dichloroethane_____78-93-3——-———'2-Butanone___________71-55-6———————1,1,1-Trichloroe thane____56-23-5——————Carbon Tetrachloride____108-05-4—————Vinyl Acetate_________75-27-4—-———-Bromodichloromethane____78-87-5——————— 1,2-Dichloropropane_____10061-01-5--———cis-l,3-Dichloropropene___79-01-6——————Trichloroethene________124-48-1—————Dibromochloromethane____79-00-5——————1,1,2-Trichloroethane____71-43-2———-—Benzene_______________10061-02-6————Trans-1,3-Dichloropropene_75-25-2——————Bromofor«____________108-10-1——————4-Methyl-2-Pentanone____591-78-6—————2-Hexanone___________127-18-4—————Tetrachloroethene_______79-34-5—————-l,l,2,2-Tetrachloroethane_108-88-3-—————Toluene_______________108-90-7—————Chlorobenzen«__________100-41-4——————Ethylbenzene___________100-42-5——————Styrene______________1330-20-7————Total Xylene*_________107-02-8——————Acrolein______________107-13-1—————Acrylonitrile_________

FORM I VOA

2026

10.80.912210000141111111111121110.910.9112

1/87 Rev,

274


EPA SAMPLE NO








Number TICs found:




Lab File ID: CR047673C11


Date Analyzed: 03/08/89**Dilution Factor:





EPA SAMPI3: NO.


Lab Code: COMPU Case No.: OOQO



Level: (low/mod) LOW





CAS NO. COMPOUND


Lab File ID: CRQ47674B11



Dilution Factor:

CONCENTRATION UNITS:(ug/L or ug/Xg) UG/L

74-87-3—•————Chloromethane__________74-83-9—————•-Bronomethane___________75-01-4——————Vinyl Chloride________75-00-3————•——Chloroethane___________75-09-2———————Methylene Chloride______67-64-1———————Acetone______________75-15-0——————Carbon Disulfide_______75-35-4——————1,1-Dichloroethene_____75-34-3——————1,1-Dichloroe thane_____540-59-0——————1,2-Dichloroethene (total),67-66-3—————--Chloroform____________107-06-2——————1,2-Dichloroethane______78-93-3——————2-Butanone____________71-55-6——————1,1,1-Trichloroethane____56-23-5———————Carbon Tetrachloride____108-05-4———.——Vinyl Acetate__________75-27-4————-Bromodichloromethane____78-87-5——-———1,2-Dichloropropane_____10061-01-5———•-cis-l,3-Dichloropropene__79-01-6-—————-Trichloroethene________124-48-1—————Dibr omochl oromethane____79-00-5———————1,1,2-Trichloroethane____71-43-2———————Benzene_______________10061-02-6————Tran»-l,3-Dichloropropene_75-25-2—-————Bromoform,___m________108-10-1——————4-Methyl-2-Pentanone_____591-78-6——————2-Hexanone_____________127-18-4—————Tetrachloroethene______79-34-5——————l,l,2,2-Tetrachloroethane__108-88-3—————Toluene______________108-90-7-————chlorobenzene_________100-41-4—————Ethylbenzene__________100-42-5——————Styrene_______________1330-20-7————Total Xylenem_________107-02-8—————Acrolein_____________107-13-1—————Acrylonitrile_________

FORM I VOA

211233211

311275222221222222225511110.92203141

1/87 Rev,


EPA SAMPLE NO

Lab Name: coMPUCHEM LABS_______Lab Code: COMPU Case No.: OQQO


Sample wt/voi: 13.o (g/mL) ML




Number TICs found:

EAW5SContract: SAS4231E



Lab Pile ID: CRQ47674B11



Dilution Factor: 4 e ',-Q




263


EPA SAMPLE, NO.

Lab Kama: COMPUCHEM LABS_________

Lab Code: COMPU Case No.: OOOQ


Sample wt/vol: 20.o (g/mL) Ml.






CAS NO. COMPOUND

Lab Sample ID: 24767S

Lab File ID: CN047675B11


Data Analyzed: Q3/QB/89

Dilution Factor: 4rQ- /. o


3 /it It

74-87-3———-——Chlorome thane_________74-83-9——————Bromome thane___________75-01-4——————Vinyl Chloride________75-00-3—————-Chloroethane___________75-09-2———————Methylene Chloride______67-64-1——————Acetone_____________75-15-0——————Carbon Disulfide_______75-35-4——————1,1-Dichloroethene_____75-34-3——————1,1-Dichloroethane_____540-59-0——————1,2-Dichloroethene (total)67-66-3——————Chloroform____________107-06-2—————1,2-Dichloroethane_____78-93-3-——————2-Butanone_____________71-55-6———————1,1,1-Trichloroe thane___56-23-5——————carbon Tetrachloride____108-05-4—————Vinyl Acetate_________75-27-4—-————Bromodichlorome thane____78-87-5———™l,2-Dichloropropane_____10061-01-5———ci»-l,3-Dichloropropene__79-01-6——————Trichloroethene_______124-48-1—————Dibromochlorome thane____79-00-5———————1,1,2-Trichloroethane___71-43-2—™--—B«nzane______________10061-02-6————Tran*-l,3-Dichloropropene_75-25-2—-——™ Bromoform_____________108-10-1——————4-Methyl-2-Pentanone____591-78-6——————2-Hexanone____________127-18-4—————Tetrachloroethene_______79-34-5———————l,l,2,2-Tetrachloroethane_108-88-3——————Toluene______________108-90-7—————Chlorobenzene_________100-41-4—————Ethylbenzene__________100-42-5—————Styrene_____________1330-20-7—————Total Xylenea_________107-02-8——————Acrolein______________107-13-1—————Acrylonitrile_________

FORM I VOA

10.80.712210.98

1900.914411111

1201141211

2200.910.9212

2026

1/87 Rev,


EPA SAMPLE NO.

Lab Name: COMPUCHEM LABS________

Lab Code: CQMPU Case No.: QQOQ


Sample vt/vol: 20.Q (g/»L) ML








Lab File ID: CNQ47675BH



Dilution Factor:


<***

GAS NUMBER

1.2.3.

COMPOUND NAME

FREONUNKNOWN HYDROCARBONUNKNOWN

RT

12.994.055.42

EST. CONC.

3.0101.0

Q

3W-JJ

#;(



EPA SAMPLE NO.


Lab Code: COMPU Case Ho.: 0000Matrix: (soil/water) WATERSample wt/vol: 3.7 (g/mL) ML


% Moisture: not dec. ___.


CAS NO. COMPOUND

EAW56REContract: SAS4231ESAS No.: 4231E SDG No.: EAW4Q




Date Analyzed: 03/08/89^AA

Dilution Factor:


74-87-3———-——chloroaethane__________74-83-9———-——Bromomethane___________75-01-4——————vinyl Chloride________75-00-3——————Chloroe thane__________75-09-2——————Methylene Chloride______67-64-1——————Acetone______________75-15-0——————Carbon Disulflde_______75-35-4——————1,1-Dichloroethene_____75-34-3——————l, l-Dichloroe thane_____540-59-0——————1,2-Dichloroethene (total),67-66-3——•———Chloroform___________107-06-2——————1,2-Dichloroethane______78-93-3———-——2-Butanone^____________71-55-6——————1,1,1-Trichloroethane___56-23-5—————-carbon Tetraehloride____108-05-4—————Vinyl Acetate_________75-27-4--———•—Bromodichloromethane____78-87-5--——--—1,2-Dichloropropane_____10061-01-5————cis-l,3-Dichloropropene__79-01-6——-——Trichloroethene________124-48-1—•——"Dibromochloromethane____79-oo-S——•———1,1,2-Trichloroethane____71-4 3-2 ———-——Benzene_______________10061-02-6————Tran»-l,3-Dichloropropene_75-25-2—™——-Bronte fora ________108-10-1——————4-Methyl-2-Pentanone____591-78-6——————2-Hexanone____________127-18-4—————Tetrachloroethene______79-34-5——————l,l,2,2-Tetrachloroethane_108-88-3™——"Toluene______________108-90-7-—————Chlorobenzene__________100-41-4—————Ethylbenzene__________100-42-5—————styrene_____________1330-20-7————Total Xylenee_________107-02-8—————Acrolein_____________107-13-1—————Acrylonitrile_________

FORM I VOA

745589657

18056

23367676

1106647867

1905655511110140

uuuuuuuuDDUUUDJUUUUUDUUDJUUUUDUUUUuuuu

1/87 Rev,

28+


EPA SAMPLE NO,




Sample wt/vol: 3.7 (g/mL) MI.








Lab File ID: CR047675B11


Date Analyzed: Q3/Q8/89

Dilution Factor: 4.0____


CAS NUMBER

1.

COMPOUND NAME

UNKNOWN HYDROCARBON

RT

4.05

EST. CONC.

70

Q

J



EPA SAMPLE NO.

EAW57Lab Name: COMPUCHEM LABS________ Contract: SASA23IE

Lab Code: COMPU Case Mo.: OOQQ SAS No.: 4231E SDG No.: EAW40






3AS NO. COMPOUND




Date Analyzed: 03/08/89-. . A

Dilution Factor:


74-87-3————•——Chloromethane__________74-83-9 —————— Bromomethane___________75-01-4——————Vinyl Chloride________75-00-3——————Chloroethane__________75-09-2——————Methylene Chloride______67-64-1——————Acetone_______________75-15-0——————Carbon Diaulfide_______75-35-4——————1,1-Dichloroethene_____75-34-3——————1,1-Dichloroethane_____-540-59-0—————1,2-Dichloroethene (total).67-66-3——————Chloroform____________107-06-2——————1,2-Dichloroethane______78-93-3—————2-Butanon«___________71-55-6——————1,1,1-Trichloroe thane___56-23-S--————-Carbon Tetrachloride____108-05-4——————Vinyl Acetate__________75-27-4——————Bromodichloromethane____78-87-5——————1,2-Dichloropropane_____10061-01-5————ci»-l,3-Dichloropropene__79-01-6——————Trichloroethene________124-48-1—————-Dibromochloromethane____79-00-5———————1.1.2 -Tr ichloroethane71-43-2————-—Benzene_______________10061-02-6————Tran»-l,3-Dichloropropene_7 5-2 5-2———-—Bromof om____________108-10-1——————4-Methyl-2-Pentanone_____591-78-6—-————2-Hexanone____________127-18-4——————Tetrachloroethene_______79-34-5——————l,l,2,2-Tetrachloroethane_108-88-3—————Toluene_______________108-90-7-—————Ch 1 orobenz ene _________100-41-4——————Ethylbenzene___________100-42-5——————Styrene_______________1330-20-7—————Total Xylene*__________107-02-8——————Acrolein______________107-13-1—————Acrylonitrile_________

FORM I VOA

534467446

1504417345455955435655

17034444880110

1/87 Rev.


EPA SAMPLE NO

Lab Name: COHPUCHEM LABS_________

Lab Coda: COMPU Case No.: QQQO













Dilution Factor: 4.0____


CAS NUMBER

1.

COMPOUND NAME

UNKNOWN HYDROCARBON

RT

4.05

EST. CONC.

44

Q

J

FORM I VOA-TIC . 1/87 Rev,

1S&


EPA SAMPLE NO.


Lab Coda: COMPU Casa No.: 0000



% Moisture: not dac. ___


CAS NO. COMPOUND

EAWS3Contract: SAS4231E

SAS No.; 4231E SDG No.: EAW40





Dilution Factor:


74-87-3——————Chloromethane_________74-83-9—————•—Bromomethana___________75-01-4——————Vinyl Chloride________75-00-3——————Chloroe thana___________75-09-2——————Methylena Chloride_____67-64-1———————Acetone_______________75-15-0———————Carbon Diaulfida_______75-35-4——————1,1-Dichloroethene_____75-34-3——————l,i-Dichloroethane_____540-59-0—————1,2-Dichloroethene (total).67-66-3——-———Chloroform^___________107-06-2—————1,2-Dichloroethane_____78-93-3——————— 2-Butanone____________71-55-6———————1,1,1-Trichloroethane___56-2 3-5 ——————Carbon Tetrachloride____108-05-4—————Vinyl Acetate_________75-27-4——•———— Bromodi chl orome thane____78-87-5——————1,2-Dichloropropane_____',10061-01-5————ci»-l,3-Dichloropropene__79-01-6——————Trichloroathane_______124-48-1—————• Dibr omoch loromethane____79-oo-S———————1,1,2-Trichloroethane____71-43-2——-——-Benzene_______________10061-02-6--——Tran»-l,3-Dichloropropene__75-25-2™——•——Bromoform_____________108-10-1——————4-Methyl-2-Pentanone____591-78-6——————2-Haxanone____________127-18-4-—-——-Tetrachloroethane_______79-34-5——————l,l,2,2-Tetrachloroethane__108-88-3——————Toluene_______________108-90-7—————Chlorobeniene_________100-41-4——————Ethylbenzene___________100-42-5——————Styrene_______________1330-20-7————Total Xylenas_________107-02-8——————Acrolein______________107-13-1—————Acrylonitrile_________

FORM I VOA

0.80.9

210.92140.9141111111111121110.910.9112

2026

1/87 Rev


EPA SAMPLE NO

'Lab Name: COMPUCHEM LABS_________











Lab File ID: CR047677B11



Dilution Factor: +rQ '.Q *Kn-





EPA SAMPLE NO,


Lab Code: COMPTT Case No.: OOQQ




Column: (pacX/cap) PACK



CAS NO. COMPOUND


Lab File ID: CN047678BH



Dilution Factor:


74-87-3——--———Chloromethane__________74-83 -9——-———Bromomethane__________75-01-4———————Vinyl Chloride_________75-00-3——•—-—Chloroe thane___________75-09-2——————Methylene Chloride_____67-64-1———————Acetone_______________75-15-0——————carbon Disulfide_______75-35-4———————1,1-Dichloroethene______75-34-3———————1,1-Dichloroethane______540-59-0——————1,2-Dichloroethene (total).67-66-3———————Chloroform_____________107-06-2—————1,2-Dichloroethane_____78-93-3——————2-Butanone_____________71-55-6———————1,1,1-Trichloroethane____56-23-5——————Carbon Tetrachloride____108-05-4————-Vinyl Acetate_________75-27-4——————Br omod i chloromethane____78-87-5—————-1,2-Dichloropropane_____10061-01-5————cia-l,3-Dichloropropene__79-01-6——————Trichloroethene________124-48-1————— Dibromochloromethane____79-00-5——————1,1,2-Trichloroethane___71-43-2———-——Benzene __________10061-02-6-———Trans-l,3-Dichloropropene__75-25-2——————Bromoform______________108-10-1——————4-Methyl-2-Pentanone____591-78-6-————2-Hexanone___..________127-18-4-———-—Tetrachloroethene______79-34-5———————l,l,2,2-Tetrachloroethane_108-88-3-—————Toluene __________108-90-7-————Chlorobenzene_________100-41-4——————Ethylbenzene___________100-42-5——————Styrene_______________1330-20-7————Total Xylene»_________107-02-8—————Acrolein_____________107-13-1—————Acrylonitrile_________

FORM I VOA

10.80.912210.90.90.90.9141111111111121110.910.91122026

1/87 Rev,

°T—140-


EPA SAMPLE NO


Lab Code: COMPP Case No.: QOQQ






EAW59Contract: SAS4231ESAS NO.: 4231E SDG No.: EAW4Q





Dilution Factor:


'• °



UNITED STATES EHYIROKMEHTAI. PROTECTION AGENCYREC10M V

En/Central Regional LaboratoryOAT* TRACKING FORM FOR CONTRACT SAMPLES

CRL Oati Set Ho.^ P SQ M R CERCLIS Ho. M £

SMO Case No. I }<4ffi/Qfrft / £~< Site Ra«e and Location;

Name of Contractor or ERA liberator?: ( fifaM i^l/T^Data User:

No. of Samples: <O&/ P>tt Staples or Data Received:

1. Have chatn-of-custody records been rectived? TES2. Have Teattic Reports or packing lists been received"^ TE?^—*03. If no, are T r a f f i c Report or packing Ifif numbers written on the ch»in-of-custody

record? TES___ HO__4. If no. *hich T r a f f i c report or packing list numbers are missing?

Are basic data fonns in? TES *0

Number of samples cl * i we 4^ Qx>^ Humfa e r of samples received:

Checked by: ________ Q '& CD F) 0 JU^ Date:•,ejved by Contract Project /Management Section: S\j77t<//L Date; 3 -

Started: ^b^(r^\9 Reviewer Signature:"™~^^^^"

Total time spent on review: ><W4-< Date review campleted:__ --Cspted (xeroxed) by:

Mt.il td to Data User by:PATA USERS;Plei.se f i l l in the blanks below and return this fora to: Sjlvia Griffin. DataManagement Coordinator, Region I. 5SCRU

Data received b y : _ _ _ _ _ _ _ D * t t :

0-A. review received by:Inorganic Gate Complete C ]Organic Data CompleteDiexintlata Complete _ tSAS Data Complete C .\\ , Suitable for Intended Purposes C !

. Suitable for Intended Purposes C, Suitable for Intended Purposes L. Suitable for Intended Purposes [

/[ ] if acceptable.List problem^ belo*.

See Attached "Missing Data Request For«" C 3 j • „„PROBLEMS: Please indicate reasons (if »nyj «hy data are not suitable for your uses

Other problems.

Received bj Data Management Coordinate^ CRL for File: Date:,Signature:

07. DP-10J

V

TO

Cp u3-C-.\-4To

O

"*

UNITED STATES ENVIRONMENTAL PROTECTION AGENCYREGION V

PAGE 1 OF 6

/9?9of Region V CLP Data

Received for Review on

Data User: APR. 1989;

We have reviewed the data for the following case(s).SITE HAHE: ^OJiOmG UlMfr &.J &CQ S«0 C«e Ho.

EPA Dat» Set pr>Siiiip?t»; * ^Numbers ff 05

- n . . ssa-

CLP Laboratory:Mrs. Requiredfor Review;

Following are our findings:

1 *

cc:

Data are acceptable for use.Data are acceptable for use *See Data Qualifier sheets ancadditional comments*Data ire preliminary - pendirSee Case Summary above.

) Data are unacceptable*

Carla Oe-npsey.CLP Quality AssJames Petty, Chief Quality A«

DATA QUALIFIERSPAGE 2~_ OF ^

Contractor:

Below is a summary of the out-of-control audits and the possible effect on thedata for this case:

/T)

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Reviewed by:Phone:Date:

DATA QUALIFIERSPAGE 3 OF £

Contractor:

Below is a Summary of the out-of-control audits and the possible effect on thedata for this case:

^' VRL k X D

o


PAGEDATA QUALIFIERS

Contractor;I.

Below is a summary of the out-of-control audits and the possible effect on thedata for this case:

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CASE/SAS f

PAGE * OFUNITE". STATES ENVIRONMENTAL PROTECTION AGENCY REGION V ——

CALIBRATION OUTLIERSVOLATILE HSL COMPOUNDS

g" CONTRACTOR Q>M PiJt f4Ett_L

Instrument * OîDATE/TIME: 1-7- 1*1 2/:3J

CMoromethaneBromomethaneVinyl ChlorideChloroethaneMethylene ChlorideAcetoneCarbon nisulfide1,1-Olchloroethane1,1-DlchloroetheneTpans-l,?-0ichlopoetheneChloroformZ-Butanone1,2-DtcMoPoetnane1,1.1-Tri ChloroethaneCarbon TetrachlorTde

IVinyl AcetateBronDd1* chl oromethane1,2-D^chloropropaneTrans-1 ,3-OichloPOpPOpeneTricnloroetheneDi bromochl opomet hane1,1,2-TrichloPoetnaneBenzenecis-1 ,3-Dlchioropropene1 iChloôethyl v-a-nylofrhcfBromoform4-Methyi-Z-Pentanone2-Hexanone

JTetrachloroethenel,l,?,Z*TetrachloroethaneTolueneCnlorobenzeneEthylbenzeneStyrenemc^yiene (-Zpfaf)A^dfcpfc*tt» Acrvlenii-rl /£.

AFFECTEDSAMPLES:

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These flags should be applied to the analytes on the sample data sheets.

€/87

CASE /S AS «

OFUNITED STATES ENVIRONMENTAL PROTECTION AGENCY REGION V

.. CALIBRATION OUTLIERSVOLATILE HSL COMPOUNDS

CONTRACTOR/-/^ PVZfteM

Instrument i J |DATE/TIME: ^-/C-^f 231?/

ChlorometnaneBromomethaneVinyl ChlorideChloroethaneMethylene ChlorideAcetoneCarbon nisulfide1,1-Oichloroethane1,1-DicnloroetheneTrans-1 .Z-DichloroetheneChloroformZ-Butanone1,2-Dicnioroethane1,1 ,1-Tri ChloroethaneCarbon Tetrachlo rideVinyl AcetateBroT'od'ichloromethanel.Z-Dichloropropane

|Trans-l ,3-DichloropropeneTrichloroetheneDibromochloromethane1,1,2-Tri ChloroethaneBenzenecis-l,3-Dichioropropene

BronDform4-Methyl-Z-Pentanone2-Hexanone

JTetrachloroethene1,1,2,2-TetrachloroethaneTolueneCnlorobenzeneEtnyibenzeneStyreneTtKXylene ( ^t?t54o/p«Yylrnr A en

AFFECTEDSAMPLES:

Reviewer's AInit1als/Date:/T

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These flags should be applied to the analytes on the sample data sheets.

€/87

sampling data documents (part 3 of 7) · tmpls ids &9918a le ids r2587 deceived s q4/07/89...

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