sample id: dico 1 cohp date analyzed: 06/25/03 19:45 lab ... · sw305ob/601ob metals by icp client...

SU3050B/6010BHETALS BY ICP

SDMSDocID 164946

Client : ECOLOGY AND ENVIRONMENTProject : oico SIGNAL HILLSDG NO. : 03F116Sample ID: DICO 1 COHPLab Samp IDs F1U-01Lab File ID: 107F02Q013Ext Btch 10: IPF044SCallb. Raf.: I07FQ2Q008

PARAMETERS

AntimonyBariumBeryllium

Cadmium •chromiumCobaltCopperMolybdenumNickelSilverVanadiumZinc

KL: Reporting Limit

Date Collected; 06/20/03Date Racoived: 06/20/03Date Extracted: 06/24/03 15:15Date Analyzed: 06/25/03 19:45Dilution factor: 1Matrix : SOIL% Moisture ; 5.2Instrument IB : ENAXTI07

RESULTS(mg/kg)

RL(mg/lcg)

ND132.33J

-777J18.3S.06Z4.4

ND10.7

ND22.9

163

10.5,05,05,05.11.1111

5.27,11.11

2.111.05

MDL(mg/ko)

2.22.131.124.382.648.729.498.778.58

.662

.462

.304

V

20 'd 200S

SW3050B/6010BMETALS BY TRACE ICP

ClientProjectSOG MO.

: DICO SIGNAL HILL: 03F116

Sample ID: DICO 1 COWLab Samp 10: F116-01Lab File ID: I31F020013Ext Btch ID: IPF044SCalib. Ref.: I31F020008

ENVIRONMENTHtLU

Date Collected;Date Received:Date Extracted;Date Analyzed:Dilution Factor:Matrix :% MoistureInstrument ID :

06/20/0306/20/0306/24/03 15:1506/25/03 20:291SOIL5.2EHAXTI31

PARAMETERS

ArsenicLeadSeleniumThallium

RL: Reporting Limit

RESULTS

(rngAg)RL

(ma/kg)

3.6178,1

NOND

1.051.051.0S1.05

MDL(mg/leg)

.222

.164

.301,32Z

ZT'd I£:6 £002 L

SW305OB/601OBMETALS BY ICP

ClientProjectSDG NO.Sample 10Lab Samp IDLab file IDExt Btch IDCalib. Ref.

ECOLOGY AND ENVIRONMENTDtCO SIGNAL HILL03F116DtCO 2 COMPF116-02I07F02QQ14IPF044SI07F02000S

Date Collected: 06/20/03Date Received: 06/20/03Date Extracted; 06/24/03 15:15Date Analyzed: 06/25/03 19:50Dilution Factor: 1Matrix : SOIL% Moisture : n.einstrument ID : EMAXTI07

PARAMETERS

AntimonyBariimBerylliumCadmiumChromiumCobaltCopperMolybdenumNickelSIiverVanadiumZinc

BL: Reporting Limit

RESULTS(nig/kg)

RL(mg/lca)

2.36J150.308J.976J16

6.2733NO

17.8ND22163

11.3.13.13.13.27Z.Z72.275.672.272.272.271.13

WDL(ma/kg)

2.38.141.134.41,696.783.535.837.624.712.497.327

WTd £002 L

SW3050B/6010BMETALS 8V TRACE ICO

Client : ECOLOGY AND ENVIRONMENT Date Collected: 06/20/03Project ; DICO SI6HAL HILL Data Received: 06/20/03SDG NO. : 03F116 Date Extracted: 06/24/03 15:15Sample ID: 01 CO Z CQMPLab Samp 10: F 116- 02Lab File ID: I51F020014Ext Btch ID: IPF044SCelib. Ref.-. I31F020008

PARAMETERS

ArsenicL«adSeleniumThallium

Date Analysed; 06/25/03 20:35Dilution Factor: 1Matrix : SOIL% Moisture : 11.8Instrument ID : EMAXTI31

RESULTS RL KDL(ma/kg) Cmg/kg)

4.67 1.135V. 1 1.15

ND 1.13.764J 1.13

C ing/ kg)

.239

.107

.323

.346

RL: Reporting Limit

£Td 12:6 £002 L I"f

SU30508/60108METALS BY ICP

client : ECOLOGY AND ENVIRONMENTProject : oico SIGNAL HILL506 NO. ; 03F116Sample ID: DICO 6 COMPLab samp ID: F116-03Lab File ID: I07F020015Ext Btch ID: IPF044SCalib. Ref.: IQ7F020008

Date Collected: 06/20/03Date Received: 04/20/03Date Extracted: 06/24/03 15:15Date Analyzed: 06/25/03 19:54Dilution Factor; 1Matrix : SOIL% Moisture : 4.7Instrument ID : EMAXT107

PARAMETERS

AntimonyBariumBeryl Ii urnCadmiumchromiumcobaltCopperMolybdenumNickelS1iverVanadiumZinc

RL: Reporting Limit

RESULTS(ma/kg)

RL<ntg/kg)

MDL

4.25J594.269J.9J

34.864.345.711618.3ND

36.6276

10.51.051.0S1.052.1a.i2.1

5.2S2.12.12.11.05

2.21.13.124.38.644-7Z5.499-77«.577.659.46.302

SO'd £002 L

SW3050B/60108METALS BY TRACE ICP

Client : ECDLOGT AND ENVIRONMENT <>»<•, couched:Project : oico SIGNAL HILL Date Received: 06/20/03SDC NO. i 03F116 Date Extracted: 06/24/03 15:15Sample ID: DICO 6 COM? Date Analyzed: 06/25/03 20:40Lab Samp 10: F116-03 Dilution Factor: 1Lab File ID: l31fOS0015 Matrix : SOILExt Btch ID: IPF044S % Moisture : 4.rCalib. Ref.: I31F020008 instrument ID : EMAXTI31

RESULTS RL MDLPARAMETERS (rnsAg) Cmfl/kg)

Araenie 7.21 1.05 .221Lead 214 1.05 .183Sslenlum ND 1.05 .299Thallium ND 1.05 .32

RL: Reporting Limit

12:6 200S L

SW3050B/6010BMETALS BY ICP

Client : ECOLOGY AND ENVIRONMENT Date Collected: 06/20/03Project : OICO SIGNAL HILL Date Received: 06/20/03SPG NO. ; 03M16 Date Extracted: 06/24/03 15:15Sample ID: DICQ 7 COOP Date Analyzed: 06/25/03 19:59Lab sun? ID: F116-OA Dilution Factor: 1Lab File ID: I07F020016 Matrix : SOILExt Btch ID: IPF044S % Moisture : 3.5Ctlib. Ref,; I07F02000B Instrument ID : EMAXTI07

RESULTS RL MDLPARAMETERS <mg/kg> (mg/k9> (mj/kg)

Antimony 2.7U 10.4 2.18Barium 298 1.04 .128Dcr/llitm .277J 1.Q4 .122cadmium 1.93 1.04 .375Chronriun 27.5 2.07 .636Cobalt 6.13 2.07 .716Copper 43.1 2.07 .489Molybdenum NO 5.18 .765Nickel 38 2.07 .57Silver ND 2.07 .651Vanadium 41.3 2.07 .4542inc 303 1.04 .298

RL: Reporting Limit

90'd Z£:6 £002 L

SW305QB/6010BMETALS BY TRACE ICP

Client : ECOLOGY AND ENVIRONMENT Date Collected: 06/20/03Project : D1CO SIGNAL HILL Date Received: 06/20/03SDG NO. ; 03F116 Date Extracted: 06/24/03 15:15Sample ID: DICO 7 COMP Date Analyzed; 06/2S/03 20:46Lab Samp ID: F116-Q4 Dilution Factor; 1Lab File ID: 131F020016 Matrix : SOILExt Btch ID; IPFD44S 5C Moisture : 3.5Calib. Ref.: I31F020008 Instrument ID : EMAXT131

PARAMETERS


RESULTS(mg/ks)

7.11282NDND

RL MDL(mg/kg) (ma/kg)

1.041.041,0*1.04

.218.18

.2!>S

.316

RL: Report ins L i m i t

ST'd 12:6 £003 L

SU3050B/60108METALS BY ICP

client : ECOLOGY AND ENVIRONMENTProject : DICO SIGNAL HILLSPG NO. ; 03F116Sample ID; DICO 3 COMPLab Samp ID: F116-05Lab File ID: I07F020017Ext etch ID: IPFD44SCalib. Ref.: I07F02000B

Date collected; 06/20/03Date Received: 06/20/03Date Extracted; 06/24/03 15:15Date Analyzed; 06/25/03 20:04Dilution Factor: 1Matrix : SOIL% Moisture : 2.5Instrument ID : EMAXTI07

PARAMETERSRESULTSCms/tea)

RL(ma/kg)

AntimonyBariumBerylliumCadmiunChromiumCobaltCopperMolybdenumNickelSiIverVanadiumZinc

RL: Reporting Limit

ND171-257J.732J21.74.9125.8ND

13.9ND

24.2113

10.303030305

2.052.055.13Z.052.05£.051.93

MDL(ma/lea)

2.16.127.121.371.63.709.484.757,564.644.449.295

ZO'd 82:6 2002 L

5W3050E/6010B

METALS BY TRACE ICP

Client : ECOLOGY AND ENVIRONMENT Date Collected: 06/20/03Project ; DICO SIGNAL HILL Date Received: 06/20/03SOG NO. : 03F116 Date Extracted: Qe/24/03 15i1SSample ID: DICO 3 COMP Date Analyzed: 06/25/03 20:51Lab Samp ID: F116-03 Dilution Factor: 1Lab File ID: I31FOJQ017 Matrix : SOILExt Btcr, ID; IPF044S % Moisture : 2.5Calfb. Kef.; I31F02000* Instrument ID : EHAXTJ31

RESULTS RL WDLPARAMETERS (mg/kfl) (mg/ita) (mg/fcgj

Arsenic 4.98 1.03 .£16Lead 12? 1.03 .179Seleniun ND 1.03 .292Thallium ND 1.03 .313

RL: Reporting Limit

9T'd I£:6 2002 L

SW3050B/6010B

METALS BY ICF1

Client ECOLOGY AND ENVIRONMENTProject : DICO SIGNAL HILLSDG NO. :Sample ID:Lab Samp ID:Lab File ID:Ext Btch ID:callb, Ref,:

03F116DICO 4 COMPF116-06107F020018IPF044SI07F020008

Date Collected: 06/20/03Date Received: 06/20/03Date Extracted: 06/24/03 15:15Date Analyzed: 06/25/03 20:08Dilution Factor: 1Matrix : SOILX Moisture ; 2.9Instrument ID : EMAXTI07

PARAMETERS

AntimonyBariumBerylliumCadmiumChromiumcobaltCopperMolybdenumNickelSiIvcrVanadiumZinc

RL: Reportins Limit

RESULTStmg/kg)

8.45J2090.312J3.03

767.Z1

13810.4

47ND

41.5577

RL

10.31.03

030306

2.062.065.152.062.062.061.03

MDL(mg/kg)

2.17.128.122.373.632.712.486.76

.566

.647

.451.297

80'd 82:6 2002 L IT


Client : ECOLOGY MO ENVIRONMENTProject : DICO SIGNAL HILLSDG NO. ; 03F116Sample ID i DICO 4 COHPLab Samp ID: f 116-06Lab File ID: I31F020018Ext Btch ID; IPF044SCalib. Ref.: 131F02000S

Date Collected: 06/20/D3Bate Reeaivod: 06/20/03Date Extracted: 06/24/03Date Analyzed: 06/25/03Dilution Factor: 1Matrix : SOIL% Moisture : 2.9Instrument ID : EIHAXTI31

15:1520:57

RESULTS RL HDLPARAMETERS (rag/kg) (ma/kg) (mg/kg)

Arsenic 17.8 1.03 .217Load 1000 1.03 .179Selenium ND 1.03 .293Thallium ND 1.03 .314

RL; Reporting Limit

ZT'd 12:6 2002 L IT

SU3050B/6010BMETALS BY ICP

Client ; ECOLOGY AMD ENVIRONMENTProject :

SDG NO. :Sample ID;Lab Samp ID:Lab File ID;Ext Btch ID;

DICO SIGNAL HILL

03F116DICO 5 COUPF116-07107F020019IPF044S

CaUb. Ref.! 107FOZOOQ8

Data Collected: 06/20/03Date R«c«iv*d: 06/20/03

Date Extracted: 06/24/03 15:15Date Analyzed; 06/25/03 20:13Dilution Factor: 1Matrix : SOIL% Moisture : 2.4instrument ID ; EMAXTICT

PARAMETERS

AntimonyBariumBerylliumCadmiumChromiumCobaltCopperMolybdenumNickelSi LverVanadiumZinc

RL: Reporting Limit

RESULTS(mg/kg)

RLCmg/kfl)

26.61190.521J2.3154.8B.16

8911.937.5

ND43.5337

10.202020205OS

0512050505

1.02

MDL(mg/kg)

2.15.127.121.371.629.roe.484.756.564.643.449.295

60'd 82:6 2002 L IT

SU3050S/6010BMETALS BY TRACE ICP

Cltsnt ; ECOLB6T A.NP ENVIRONMENTProject : DICO SIGNAL HILLSDG NO. : 03F116Sample ID: DICO 5 COUPLab Samp ID: F116-07Lab File ID: I31FQ20019Ex* Bteh ID: 1PFO&4SCalib. Ref.: I51F02000B

Data Collected: 06/20/03Rccoiv.d:

extracted: 06/24/03 15:15Analyzed; 06/25/03 21:03

1SOIL2.4

DateDateDilution Factor:MatrixX MoistureInstrument ID : EMAXT131

RESULTS RLPARAMETERS


RL: Reporting Limit

8.6264NDND

1.021.021.021.02

MDL(mo/kg)

.216

.178

.292

.313

8I'd 12:6 2002 L IT

SWSOSQB/6010BMETALS BY ICP

Client : ECOLOGY AND ENVIRONMENT Date Collected: 06/20/03Project : DICO S16MAL MILL Date Received: 06/20/03SDC NO. : 03F116 Date Extracted: 06/24/03 15:15Sample ID; DICO #6 Date Analyzed: 06/25/03 20:27Lab Samp ID: F116-08 Dilution Factor: 1Lab File ID: IQ7FQ200Z2 Matrix : SOILExt Btch ID: IPF044S X Moiatura : 4.7Co Lib. Ref.: I07F020020 Instrument ID : EMAXT107

RESULTS RL MDLPARAMETERS (mg/kg) (mg/kg) (mg/kg)

Antimony ND 10.5 2.21Barium 39.9 1.05 .13Beryllium NO 1.05 .124Cadmium ND 1.05 .38Chromium 5.18 2.1 .644Cobalt 3.4S 2.1 .725Copper 2Q.1 2.1 .495Molybdenum ND 5.2S .774Nickel 4.82 2.1 .577Silver ND 2.1 .659Vanadium 11.7 2.1 .46Zinc 129 1.05 .302

RL: Reporting Limit

01'd 82:6 2002 L IT

SW3050B/6010SMETALS BY TRACE ICP

client ; ECOLOGY AND ENVIRONMENTProject C DICQ SIGNAL HILLSDC NO. : 03F116

S«mpl» ID: OICO #8

Lab Samp ID: F116-OBLab File ID: 131F020022Ext Btch ID: IPF044SCalib. Ref.: I31F020020

Date Collected: 06/20/03Dat* Received: 06/20/03Date Extracted; 06/24/03 15:15Date Analyzed: 06/25/03 21:19Dilution Factor: 1Matrix : SOIL% Moisture : 6.7Instrument ID

-===tt««tt;;5==mi:s==

PARAMETERS

ArsenicLa«dSeleniumThallium

RL; Reporting Limit

RESULTS(mg/kg)

RL(mg/kg)

2.5411.4NDND

1.051.051.051.05

MDL(mg/kg)

.221

.183

.zw.32

61 'd 12 = 6 £002 L IT

Clientproject :SDG NO. :Sample ID:Lab Samp ID:Lab File ID:Ext Btch ID:Calib. Ref.:

ECOLOGY ANDDICO SISNAL03F116DICO 49 COMPF116-09I07F020023IPF044SI07F020020


ENVIRONMENTHILL

Date collected:Date Received;Date Extracted:Date Analyzed:Dilution factor:Matrix :% Moisture :Instrument 10 :

06/20/0306/EO/0306/24/03 15:1506/25/03 20:311SOIL4.2EMAXTI07

PARAMETERS

AntimonyBariumBerylliumCadmiumChromiumCobaltCopperMolybdenumNickelSiIvervanadiumZinc

RESULTSting/kg)

RL(tns/ka)

ND112-25J.597J13.24.5535

-908JS.61

ND

19.6215

10.40404040909

2.095.222.092.092.091.04

MDL(mg/kg)

2.2.129.123.378.641.721.493.77.574.656.457.301

RL: Reporting Limit

ird 82:6 2002 L IT

SW305OB/601 OB

METALS BY TRACE ICP

==s ======•

Client !Project :SOG NO. :Sample ID;Lab Samp ID:Lab File ID:Ext etch ID:Calib. Ref.:

ECOLOGY AND ENVIRONMENTDICO SIGNAL HILL03F116DICO *9 COM?F116-09131F020023IPF044SI31F020020

Pate Collected:Date Received:Date Extracted:Date Analyzed:Dilution Factor!Matrix :% Moisture :Instrument 10 :

06/20/0306/20/0306/24/03 15:1506/25/03 21:251SOIL4.2EMAXTI31

PARAMETERS

ArsenicLeadSeleniumTrtallium

RL; Reporting Limit

RESULTS(mg/kg)

RL(mg/kg)

3.1449.5

NDND

1.041.041.041.04

MDL(mg/kg)

.22.182.297.318

02'd 22:6 2002 L IT

SW305OB/601 OBMETALS BY ICP

Client : ECOLOGY AND ENVIRONMENTProject : DICO SIGNAL HILLSDG NO. : 03F116Sample ID; DICO #10 COMPLab Samp ID: F116-1DLib File ID: 107F020024Ext Btch ID: IPF044SCaltb. Ref.: I07FOEOOEO

Date Collected; 06/20/03Date Received! 06/20/03Date Extracted: 06/24/03 15:15Date Analyzed: 06/25/03 20:36Dilution Factor; 1Matrix : SOILX Moisture ; 19.0Instrument ID : EMAXTI07

PARAMETERS

AntimonyBariumBerylliumCadmiumChromiumCobaltCopperMolybdenumNickelSiIverVanadiumZinc

RL: Reporting Limit

RESULTS(ing/kg)

RL(mg/kg}

NO212

.4B4J1.12J24.96.5037.4

ND14.8

ND30.5

310

12.31.231.231.232.472.472.476.172.472.472.471.23

MDL(mg/lcg)

2.6,153.146.447.758.653.583.911.679.775.541.356

20 'd 62:6 2002 L IT

SU30SOB/6010B

METALS BY TRACE ICP

Client :Project ;SOS NO. ;Sample ID;Lab Samp ID;Lab File ID:Ext Btch ID:Calib. Ref.:«==m»K=__£

ECOLOGY AND ENVIRONMENTDICO SIGNAL HILL03F116DICO #10 COMPF116-10I31F020024IPF044S131F02002D

Date Collected:Date Received:Date Extracted:Date Analyzed:Dilution Factor:Matrix :X Hoi a tare :Instrument ID :

06/20/0306/20/0306/24/0306/25/031SOIL19,0EMAXT131

15:1521:30

PARAMETERS


RL: Reporting Limit

RESULTS(mg/kg)

RL(mg/kg)

4.9184.9

NDND

1.231.231.251.23

(mg/kg)

.26.215.352.377

12'd 22:6 2002 L IT

SW3050B/6010BMETALS 8Y ICP

=3BB=========»«==========HK===~======3-==="====S===="=

Client ; ECOLOGY AND ENVIRONMENTProject : DICO SIGNAL HILL

SDG NO. : 03F116SampU ID: DICO *11Lab Samp ID: F116-12Lab File ID: I07F020030Ext Btch ID: IPF044SCalib. Ref.: I07F020020

Date Collected: 06/20/03Data Received: 06/20/03Data Extracted: 06/24/03 15:15Date Analyzed: 06/25/03 21:09Dilution Factor; 1Matrix : SOILX Moisture : 19.2Instrument ID : EMAXTI07

PARAMETERS

RESULTS(mg/kg)

RL(mg/kg)

AntimonyB«r i urnBerylliumcadmiumChromiumCobaltcopperMolybdenumNickelSilverVanadi urnZinc

RL: Reporting Limit

3.17J364.342J2.4922.49.9348.6£.53.123.4

ND23.5235

12.41.241.241.242.48Z.4B2.4B6.192.482.482.481.24

HDL(mg/kg)

2.6.153.146.448.76.653.564.913,681.777.542.356

SO'd 62:6 2002 L IT


Client ;project :SDG NO. :Sample ID:Lab Samp ID:Lab File ID:Ext Btch ID1.Colib. Ref.:

PARAMETERS

AraenieLeadSeleniumThallium

ECOLOGY AND ENVIRONMENTDICO SIGNAL HILL03F116DICO #11F116-12I31F020030IPF044SI31F020020

Date Collectad:Data Received:Date Extracted:Date Analyzed:Dilution Factor;Matrix :X Moisture :Instrument 10

06/20/0306/20/0306/24/03 15:1506/25/03 22:041SOIL19.2EMAXTI31

RESULTS(ma/kg)

8.58769

NDND

RL(mg/kg)

1.241.241.24

HDL(mg/kg)

.26.215.353.378

Reporting Limit

22'd 22:6 2002 L IT


Client ECOLOGY AND ENVIRONMENTProject DICO SIGNAL HILLSDG NO. 03F116Sample ID DICO #12lab Samp ID F116-11Lab File ID: I07F020029Ext Btch ID; IPF044S

Date Collected: 06/20/03Dote Rocctvcd: OA/BO/03

Date Extraetodi 06/24/03 15:15Date Analyzed:Dilution Factor:Matrix :% Moisture :

Calib. Ref.: I07F020020 Instrument ID

06/25/03 21:031SOIL6.6EMAXT107

PARAMETERSRESULTS(mg/kg)

RL(mg/kg)

AntimonyBariumB cry I HunCadniumChromiumCobaltCopperMolybdenumNickelSILverVanadiumZinc

RL: Reporting Limit

2.46J262.758J1.0736.514.946.8

ND27.2

ND60.9142

10.71.071.071.072.142.142.145.352.142.142.141.07

MDL

(mg/kg)

2.25.133.126.388.657.74.505.79.589.672.469.508

WTd 62:6 2002 L IT

SU3Q50B/6010BMETALS BY TKACE ICP

Client : ECOLOGY AND ENVIRONMENT Date Collected; 06/20/03Project : DICO SISNAL HILL Date Received: 06/20/03SDC NO. : 03F116 Date Extracted: 06/24/03 15:15Sample ID: DICO #12Lab Samp ID; F116-11Lab File ID: I31F020029Ext 9tch ID: IPFQ44SCalib. Ref.: I31F020020

PARAMETERS


Date Analyzed:Dilution Factor:Matrix :X Moisture :Instrument ID :

RESULTS RL(mg/kg) (mg/kg)

11 1.0729.4 1.07

ND 1.07.46J 1.07

06/25/02 21:501SOIL6.6EHAXTI31

MDL(mg/kg)

.225

.186

.305

.327

RL: Reporting Limit

22'd 22:6 2002 L \r\£


ClientProjectSDG NO.sample ID: DICO #15Lab Samp ID:Lab File ID:Ext Btch 10:Cslib. Ref,!

ECOLOGY AND ENVIRONMENTOICO SIGNAL HILL

03F116

F116-13I07F020Q31IPF044SI07FOZ0020

Date Collected: 06/20/03Date Received: 06/20/0!Date Extracted: 06/24/03 15:15Dato Analyzed: 06/25/03 21:13Dilution Factor: 1Matrix ; SOILX Moisture : 19.2Instrument ID ; EMAXTiO?

PARAMETERS

AntimonyBariumBerylliumCadmiumChromiumCobaltCopperMolybdenumNickelSilverVanadium

Zinc

RL: Reporting Limit

RESULTS

(mg/kg)RL

(ma/kg)

ND358.336J2.8923,110.144.71.3J25ND24242

12.41.241.241.242.482.*e2.486.192.482.462.481.24

MDL(mg/kg)

2.6.153.146.448.76.855.584,913.681.777.542.356

90'd 02:6 2002 L IT

SU3050B/6010BMETALS BY TRACE ICP

Client : ECOLOGY AND ENVIRONMENT Date Collected: 06/20/03Project : D1CQ SIGNAL HILL Date Received: 00/20/03SDG NO. : 03F116 Date Extracted: 06/24/03 15:15Sample ID; DICO #15 Date Analyzed: 06/25/03 22:09Lab Samp ID: F116-13 Dilution Factor: 1Lab File ID; 131*020031 Matrix : SOILExt Etch ID: IPFQ44S % Moisture : 19.2Calib. Ref.: I31F020D20 Instrument ID : EMAXTI31

RESULTS RL MDLPARAMETERS (ng/kg) (ma/kg) (mg/kg)

Arsenic 7.64 1,24 ,26Lead 701 1.24 .215Selenium ND 1,24 .353Thallium ND 1.24 .378

RL: Reporting Limit

t?2'd 22:6 2002 L IT


Client : ECOLOGY AND ENVIRONMENT Date Collected: 06/20/03Project : DICO SIGNAL HILL Date Received: 06/20/03

SDG NO. : 03F116 Date Extracted; 06/24/03 15:15sample ID: DICO #13 Date Analyzed; 06/25/03 21:27Lab Samp ID: F116-14 Dilution Factor: 1Lab File ID; 107F020034 Matrix : SOILExt Btch ID: IPF044S % Moisture ; NACalib. Ref.: 107F020032 Instrument ID ; EHAXT107

RESULTS RL MDLPARAMETERS (mg/kg) (ma/kg) (mg/kg)

Antimony ND 10 2.1Barium 2 1 .124Beryllium ND 1 .118Cadmium ND 1 .362Chromium ND 2 .614Cobalt ND £ .<A\Copper H.7 2 .472Molybdenum a.68j 5 .738Nickel MO 2 .55Silver ND 2 .628Vanadium ND 2 .438Zinc 107 1 .288

RL: Reporting Limit

02:6 2002 L IT

SW30SOB/6010BMETALS BY TRACE ICP

Client : ECOLOGY AND ENVIRONMENT Date Collected: 06/20/03Project : DICO SIGKAL HILL Date Received: 06/20/03SDG NO. : 03F116 Date Extracted: 06/24/03 15:15Sample ID: DICO #13 Date Analyzed; 06/25/03 22:26Lab Samp ID: F116-14 Dilution Factor: 1Lab File ID: I31F020034 Matrix : SOILExt Btch ID: IPF044S % Moisture : NACalib. Ref.: 131F02003E Instrument ID : EMAXTI31

PARAMETERS


RESULTS(mg/kg)

ND8.19

NDND

RL HDL(mg/kg) (mg/kg)

11l1

.21.174.285.305

RL: Reporting Limit

S2'd 22:6 2002 L IT

SW3050B/6Q108METALS BY ICP

ID:

ClfcntProjactSDG NO.SampleLab Samp ID:Lab File ID:Ext Btch ID:Calib. Ref.:

ECOLOGY AMD 6UVIftOHMENTDICO SIGNAL HILL03F116DICO #14F116-1SI07F020035IPF044SI07FOZ0032

Date Collected: 06/20/03Date Recaived: 06/20/03Date Extracted: 06/E4/03 15:15Date Analyzed; 06/25/03 21:31Dilution Factor: 1Matrix i SOIL54 Moisture : 29.1Instrument ID : EMAXTI07

PARAMETERS

AntimonyBariumBerylliumCadmiumChromiumCobaltCopperMolybdenumNickelSilverVanadiumZinc

RL-. Reporting Limit

RESULTS(mg/ks)

RL

25.68420.516J7,7348432.466870.6367ND2341530

14,11.411.411.412.822.822.827.052.62£.82Z.K1.41

MDL(mg/kg)

2.97.175.166.511.866.975.6661.04.776.886.618.406

80 "d 02:6 2002 Z IT

SU3050B/6010BMETALS BY TRACE ICP

s=s:==seE'ClientProjectSDG NO.SampleLab Samp ID: F116-15Lab File ID: I31F02003SExt Btch ID;Calib. «ef.:

ECOLOGY AND ENVIRONMENTDICO SIGNAL HILL03F116OICO m

IPF044SI31F020032

Date Collected; 06/20/03Date Received: 06/20/03Date Extracted: 06/24/03 15:15

06/25/03 22:311SOIL29.1EMAXTI31

Date Analyzed:Dilution Factor:Matrix :% Moisture :Instrument ID :

PARAMETERS

ArsenicLeadselenium

RESULTS(mg/kg)

RL(mg/kg)

30.916401.962-41

1.411.411.411.41

HDL(mg/kg>

.297

.246

.402.43

RL: Reporting Limit

92'd 22:6 2002 L IT


Client :Project :SDG NO. :sample ID:Lab Samp ID:Lab File ID:Ext Btch ID:celib. Ref.:

ECOLOGY ANDDICO SIGNAL03F116MBLK1S1PF044SBI07P020010IPF044S107F02000B

ENVIRONMENT Date collected:HILL Date Received:

Date Extracted:Date Analyzed:Dilution Factor:Matrix :% Moisture :Instrument ID :

WA06/24/0306/24/0306/25/031SOILNAEMAXTI07

15:1519:29

PARAMETERS

AntimonyBariumBerylliumcadmiumChromiumCobaltCopperMolybdenumNickelSilverVanadiumZinc

RL: Reporting Limit

RESULTSCrng/ka)

RL(mg/kg)

NDNDNDNDNDND

WNDNDNDNDND

1011122252221

MDL(mg/k9>

2.1.124.118.362.614.691.472.738.55.626.438.288

60'd 02:6 2002 L IT


Client : ECOLOGY AND ENVIRONMENTProject : Dico SIGNAL HILLsee NO. t 03M16Sample ID: MBLK1SLab Samp ID: IPF044SBLab File IDt I31F020010Ext Btch ID: IPF044SCalib. Ref.; I31F0200D8

Date collected; NADate Received: 06/24/03Date Extracted: 06/84/03 15:15Date Analyzed: 06/25/03 20:12Dilution Factor:Matrix ;% Moisture :Instrument ID

1SOILNAEMAXT131

PARAMETERS

LeadSeleniumThallium

RL: Reporting Limit

RESULTS(mg/ks)

RL(ma/kg)

ND

.203JNDNO

MDL(mg/kg)

.21.174.285.305

22:6 2002 L IT

HETHOD 747JAHERCURY BY OHO VAPOR

CMO

a!

CN

cn

to0

R^~, (i— >

Client : ECOLOGY AND EHVIROWEHrProject : DICO SISMAL HCLLBatch No. : 03F116

SAMPLE ID

teuisLCS1SLC01SDICO #10 COHPASDICO #10 COHPDICO #10 COflPDLDICO #10 COWHSDICO #10 COHPHSODICO 1 COHPDICO 2 COHPDICO € COHPDICO 7 COHPDICO 3 CO*DICO 5 CONPDICO #8DICO ft) CWPDICO #12DICO #11DICO #15DICO #13OICO 4 COHPDICO *14

EHAXSAHPLE ID

HGF030SBHGF030SLHGF030SCF116-1DAF116-10FU6-10TF116-10MF116-10SF116-01F116-OZF116-03F116-04F116-05F116-07F116-D8FU6-09F116-11F116-12Fllfi-13F116-14F116-D6F116-16

RESULTS(ng/ltg>

NO.847.848.574.173

HO1.271.21.542.314.451.836.3231.68

NO-0919J

.25.782.943

.043ZJ2.39.1

DUF

111315a1111111

5LC

noisr

NANANA

19.819.019.019.019.05.2

11.84.73-52.52.44.74.26.619.219.2

RA2.9

29.1

Rl(eg/leg)

.1

.1

.1.123.123.617.123.123.105.113.105.104.103.102.105.104.107.124.124

.1.5151.41

MDL(•gflcgl

.013

.033

.033.0407.0407.204

.0407

.0407

.0348

.0374

.0346

.0342

.0338

.0338

.0346

.0344

.0353

.owe

.040B.033.17

.465

AnalysisDATETIHE

06/26/0311:1606/26/0311:2105/26/0311:2305/26/0311:2505/26/0311:2806/26/0311:3005/26/0311:32(6/26/0311:3405/26/0311:3705/26/0311:3905/26/0311:4605/26/0311:4845/26/0311:5006/26/0311:55(6/26/8311:57(6/26/0311:5906/26/0312:0206/26/0312:05(16/26/0312:0706/26/0312:1406/26/0312:1806/26/0312:23

ExtractionDATETIHE LFJD

06/25/0316:00 H47FD2001006/25/0316:00 H47F020D1106/25/0316:00 H47F020D1205/25/0316:03 N47F02001305/25/0316:00 M7F02001406/25/0316:00 H47F02D01506/25/G316:C» H47F02001606/25/0316: CD H47F02001705/25/0316:00 H47F02001806/25/0316:00 N47F02001905/25/0316:00 H47F020022OS/25/0316: CQ H47F020D2306/25/0316:00 H47F0200E406/25/0316:00 H47F0200Z606/25/0316:00 H47F02002705/25/0316:00 HWOZOOM05/25/0316: CO N47f 02002906/25/0316:10 H47F02903005/25/0316 :KJ H47F02Q03106/25/0316:00 HtTFOZOOM06/25/0316:00 H47F020U3506/25/0316:00 H47F020D37

CAL REF

H47FDZC008N(7F02000BNW0200DBH47F020BOBH47FOZOD08N47F02BDD8N47F020003M47F0200DBm7F02000BH47F020DOSW7F029D2CN47F020020Hi7f02D020W.7F020tJ20H47F020D20N47F024D20H47FOHOOZON47f02M20H47F020920H47F020D32m7F020D32H47F020032

Matrix : SOILInstrument ID : TIM7

me BATCH

«Sf030SHGF030SHSF030SHGF0395HGFQ30SHOF030SHGf030SHCJTJ30SKGF030SMGT030SKSF030SUGF03DSHCF03DSHGF030SHGf03D5HSFC30SHSF030SUGF030S(ttF03!TSHGF030SHCF030SHGFC33S

CollectionDATITIHE

NAHAHA

06/20/0306/20/0306/20/0366/20/0306/20/0306/20/0306/20/0306/20/0306/20/0306/20/0306/20/0305/20/0306/20/0306/20/0306/20/0306/20/0305/20/0306/20/0306/20/03

ReceivedOATETIHE

06/25/8306/25/0305/25/0306/20/0306/20/0306/20/0306/20/0306/20/0305/20/0306/20/0306/20/0306/20/0306/20/0306/20/0306/20/0366/20/0306/20/03OS/20/0306/20/0305/20/0305/20/03C6/20/03

RL: Reporting Limit

*'*«* ^ '"-"''-

METHOD M8015TOTAL PETROLEUM HYDROCARBONS BT EXTRACTION

Client : ECOLOGT AND ENVIRONMENT Date Collected: 06/20/03»roject : DICO SIGNAL HILL Date Received: 06/20/03Batch No. : 03F116 Date Extracted: 06/23/03 17:50sample ID: DICO 1 COHP Date Analysed-. 06/26/03 07:32tab Samp ID: F116-01 Dilution Factor; 1Lab File 10: TF24066A Meui* -. SOILExt Btch ID: DSF020S % Moisture : 5.2Calib. ftef.: TF2406&A Instrument ID : GCT050

RESULTS RL MDL'ARAHETERS (ma/kg) (mg/lcg) (mg/xs)

)I£SEI. ND 11 2.1^lOTOR OIL 380 53 2.1

SURROGATE PARAMETERS X RECOVERY QC LIMIT

SROMOBENZENE 114 4S-165MEXACOSANE 133 27-176

RL ! Reporting LimitSUSftl : BromobenzeneSURR2 : Hexacosane

£002 8

METHOD H8015TOTAL PETROLEUM HYDROCARBONS BY EXTRACTION

=i;.~< : ECOLOGY AMD EWVlROHMgNT"reject : DICO SIGNAL HILL3atch No. : 03F116Sample ID: DICO 2 CQMP.ab Samp 10: F116-OZtab File ID: TF24067Aext Btch IDs 03F020SCBlib. Ref.; TF24064A

Bfife Collected:Date Rsceivea;Data Extracted:Date Analyzed:Dilution Factor:Matru ;% Moisture ;Instrument ID :

06/20/0306/20/0306/23/03 17:5006/26/03 06 ;H1SOIL11.8GCT050

PARAMETERS

OIESEL

RESULTS(ma/kg)

RL

OIL

SURROGATE PARAMETERS

3ROMOBENZEKEHEXACQSANE

RL : Reporting LimitSUR.R1 ; BromooenzencSURR2 ; Hexacoaenc

NO440

RECOVERY

115143

1157

QC LIMIT

45-16527-176

MDL

(mg/k9)

2.3

"d £2:8 £002 8

METHOD M8015TOTAL PETROLEUM HYDROCARBONS BY EXTRACTION

: ECOLOGY AND ENVIRONMENT: DICO SIGNAL HILL: 03F116

ID; DICO 3 COMP10: F116-OSTID: TF24089AID: DSF020S

Calib. Ref.: TF24080A

ClientProjectBatch No.S atrip Le16D SampLab FilcExt etch

Date Collected: 06/20/03Date Received: 06/20/03Date Extracted: 06/23/03 17:50Date Analyzed: 06/26/03 23:32Dilution Factor: SOMatrix ; sou% Moisture : 2.5Instrument ID : GCT050

PARAMETERS

OIESELMOTOR OIL


SROMOBENZcNEHEXACOSANE

RESULTS(mg/kg)

RLCms/kg)

ND16000

55 RE COVERT

DODO

510£600

oc LIMIT

45-16527-176

MDL(rag/kg)

100100

•aSUUR1SURR2

30

Reporting L i m i t

BromobenieneHexacosane

Diluted out

'd 172:8 200S 8

METHOD MB015TOTAL PETROLEUM HYDROCARBONS BY EXTRACTION

:l lent

aatcn No.Sample ID:Lab Samp ID;Lab F i l e ID:

ECOLOGY AND

DICO SIGNAL HILL03F116DICO t COMPF116-06TTF24090A

Date Collected: 06/20/03Date Received: 06/20/03

Ext BtCti ID: DSF020SCalib. Ref.: TF24080A

Date Extracted;Date Analyzed:Dilution Factor:Matrix !S Moisture !Instrument ID i

06/23/03 17:5006/27/03 00; 13100SOIL2.9QCT050

PARAMETERS

DIESELMOTOR OIL


3ROMOBEN2EME

HEXACOSANE

RL : Reporting LimitSURR1 s BromobenzeneSURR2 : Hexacosane

30 ; Diluted out

RESULTS(mg/kg)

RL(mg/kg)

MDL

ND28000

RECOVERY

DODO

10005100

QC LIMIT

45-16527-176

210210

0£'d £002 8

M6THOO M6015TOTAL PETROLEUM HYDROCARBONS BY EXTRACTION

ClientProjectBatch NoSampletab samp-ab File£xt Btch

:= ; : = 3 V » » ~ -: ECOLOGY AND ENVIRONMENT: Oico SIGNAL HILL: 03F116

ID: DICO 5 COHPID: F116-07TID: TP24091AID: DSF020S

:aUb. Ref,: TF24060A

PARAMETERS

DIESELMOTOR OIL


aROMOBENZENE^EKACOSANE

Rl ; Reporting LimitSURR1 : BromobenzeneSURR2 : Hexacosane

==:;Sa=»Date collected: 06/20/03Date Received: 06/20/03Date Extracted: 06/23/03 17:50Date Analyzed: 06/27/03 00:55Dilution Factor: 100Matrix ; SOIL% Moisture : 2.4Instrument ID : GCT050

RESULTS(ms/Vg)

RL(ms/k9)

MDL

ND34000

% RECOVERY

DODO

10005100

QC LIMIT

&5-16SE7-176

200200

00 : Diluted out

T£'d £002 8

(10015TOTAL PETROLEUM HYDROCARBONS BY EXTRACTION

Client :Project :

Batch No. :Sample ID:•-ab Samp ID: F116-03T-ab file 10: TF24068A:xt Btch ID: OSFOZOSCallb, Ref,: TF2«80A

ECOLOGY AND ENVIRONMENTDICO SIGNAL HILL03F116DICO 6 COMP

Date Collected: 06/20/03Date Received: 06/20/03Date Extracted; 06/Z3/W 17:50Date Analyzed; 06/26/03 22:50Dilution Factor: 3Matrix ; SOILX Moisture : 4.7Instrument ID : GCTOSO

PARAMETERS

DIESELMOTOR OIL


3ROMOBENZENEHEXACOSANE

RESULTS(ing/Kg)

NP

3100 '

% RECOVERY

126337*

RL

(ing/Kg)MDL

160

OC LIMIT

45-16527-176

6.36.3

U '. Reporting Limit3URR1 : BromobenieneSUSRZ : Hexacosana

" : out of QC limits due to matrix interference

£00^ 8

METHOD M8015TOTAL PETROLEUM HYDROCARBONS BT tMRACTiON

Client : ECOLOGY AND ENVIRONMENTProject : DICO SIGNAL HILLBatch No. i 03M14Sample ID: DICO 7 COMPLab Samp ID: F116-04 .uab Fi l e ID: TF24069ASxt Btch ID: DSF020SCalib. Ref.! TF24064A

D8te Collected; 06/20/03Date Received: 06/20/03Date Extracted: 06/23/03 17:50Date Analyzed: 06/26/03 09:37Dilution Factor: 1Matrix ; SOILX Moisture : 3.5Instrument ID : CCT050

PARAMETERS

DIESEL

MOTOR OIL


3ROMOBENZENE

-itXACOSANE

<L : Reporting LimitSURR1 : BromobenzeneSURR2 : Htxacosane

RESULTS(mg/kg)

RL(mg/kg)

ND1500

% RECOVERY

119173

1052

QC LIMIT

45-16527-176

MDLcms/kg)

2.12.1

82'd £002 8


Client : ECOLOGY AND ENVIRONMENT Date Collected: 06/20/03Project : DICO SIGNAL HILL Date Received; 06/20/03Batch No- : 03F116 Date Extracted: 06/23/03 17:50Sample ID; DICO #8 0»te Analysed: 06/27/03 01:36v.ab Samp ID: F116-08T Dilution Fsetor: 100.ab File ID: TF24092A Matrix : SOIL••xt Btch ID: OSF020S H Moisture ; 4.7:shb. Ref.s TF24080A Instrument 10 : GCT050

PARAMETERS

DIESELMOTOR OIL

RESULTS RL MCu(mg/kg) (mg/kg) (mg/l<9)

ND 1000 21031DOO S200 210


3RON08ENZENE4EXACOSAH6

^L : Reporting LimitSURR1 : Bromo&enieneSURRE ; Mexacossne

30 t Diluted out

RECOVERY

DODO

CC LIMIT

45-16527-176

£2:8 £002 8


ClientProjectBatch No.SampleLab SampLab FileExt Btch

10:ID;ID;

ECOLOGY AND ENVIRONMENTDICO SIGNAL HILL03F116DICO <P? COMPF116-09TTF2409SA

ID: DSF020SCalib. Ref.: TF24093A

Date coUectea; 06/80/osDate Received: 06/20/03Date Extracted: 06/23/03 17:50Date Analyzed: 06/27/03 03:41Dilution Factor: 5Matrix : SOILX Moisture : 4.2Instrument ID : GCTOSO

RESULTS(mg/ksl

ND7300

V, RECOVERY

PARAMETERS

31S5ELVICTOR OIL


SROMOBENZENEHEXACOSANE

3L : Reporting LimitSURR1 ; 8 rouwbenzoneSURR2 : Hexacoeane

: Out of OC limits due to matrix interference

RL(mo/kg)

52260

QC LIMIT

45-16527-176

MDL(mg/Kg)

1010

££'d 52:8 £002 8


Client : ECOLOGY AND ENVIRONMENTProject : DICO SIGNAL HILLSatcn NO. : 03F116Sample ID: 51 CO 1*10 COMPLab Samp ID: F116-10Lab File ID: TF24075AExt Btch ID: OSF020SCalib. Ref.: TF24064A

Date Collected; 06/20/03Date Received; 06/20/03Date Extracted: 06/23/03 17:50Date Analyzed: 06/26/03 13:48Dilution Factor: 1Matrix : SOILX Moisture : 1°-0Instrument ID : GCT050

'ARAHETERS

3TESELMOTOR OIL


8ROMQ6ENZENEHEXACOSANE

RESULTS(ms/kg>

RL(mg/kg)

NDZ100

RECOVERY

244*

126Z

QC LIMIT

45-16527-176

MDL(mg/ks)

2,52.S

RL : Reporting LimitSURR1 : BrotnobenieneSURR2 : Hexacosane

• : Out Ot QC limits due to matrix interference

I7£'d £002 8


Date Collected: 06/20/03Date Received: 06/20/03Date Extracted: 06/23/05 17:50Date Analyzed: 06/29/03 11:06Dilution Factor: 10Matrix ; SOILX Moisture : 19.2Instrument ID : GCT050

clientProjectBatch No.SampleLab SampLab FileExt BtchCalib. Re

; ECOLOGY AND ENVIRONMENT; DICO SIGNAL HILL: 03F116

ID: DICO *nID: F116-12TID: TFZ7062AID: DSF020Sif.: TF27060A

PARAMETERS

DIESELMOTOR OIL


BROMOBENZENE

HEXACOSANE

RL : Reporting LimitSURR1 : BromobenreneSURR2 : Hexacosane

RESULTS(mg/kg)

RL(mg/kg)

450015000

X RECOVERY

00DO

120620

QC LIMIT

45-16527-176

HDL(ng/kg)

2525

00 : Diluted out

9£'d S2:8 £002 8

METHOD H8015TOTAL PETROLEUM HYDROCARBONS BY EXTRACTION

-s===ca*===s:

Client :'roject :•Jatch No. :Sample 10:_ab Samp ID:uab File 10:Fxt BtCh 10:Calib. Ref.;

PARAMETERS

3USELMOTOR OIL

ECOLOGY ANDDICO SIGNAL03F116DICO #12H16-11TF26082AD5F020STF24080A

ENVIRONMENT Date Collected:HILL Date Received:

Date Extracted;Date Analyzed:Di lution Factor;Matrix ;X Moisture :instrument ID :


ND 112ZQ 54

06/20/0306/20/0306/23/03 17:5006/26/03 18:411SOU6.6CCTD50

MOL(mg/kg)

2,12.1


6R0140BEN&ENEHEXACQSAHE

% RECOVERY

115115

OC LIMIT

45-16527-176

RLSURR1SURR2

Reporting LimitBromobenzeneHexacosane

S2:8 £002 8


clientProjectCatch No.Simple IDLab Samp IDLab File IDEXt Btch IDCalib. Ref.

PARAMETERS

DIESELMOTOR OIL

; ECOLOGY AND: DICO SIGNAL'. 03F116: DICO #13: F116-14T: TF24096A: DSFOE1S: Tf£40«3A

ENVIRONMENT Date Collected: 06/20/03HILL Date Received: 06/20/03

Date Extracted: 06/24/03 16:30Date Analyzed: 06/27/03 04:23Dilution Factor: 1000Matrix : SOIL% Moisture : NAInstrument ID : GCT050

RESULTS RL MDL(ma/kg) (mg/kg) (mgAg)

24000 10000 20006BOOOO 50000 2000


BROM08EHZENE

UCXACOSANE

RL ; Reporting LimitSURR1 : BromobenzeneSURR2 ; Hexacosane

RECOVERY

00DO

QC LIMIT

27-176

00 ; 0i Luted out

8£'d S2:8 £002 8


clientProjectBatch No.SampleLab ScirpLftb FileExt BtchCalib. Ref.:

ECOLOGY AND ENVIRONMENTDICO SIGNAL HILL03F116DICO #14F116-15TTC0200SAOSF020STS02003A

Date collected; oo/go/03pate Received: 06/20/03Date Extracted: 06/23/03 17:30Date Analyzed: 07/02/03 17:09Dilution Factor: 1000Matrix ; SOILX Moisture : 29.1Instrument ID : GCTD50

RESULTSPARAMETERS

RL

(ma/kg)

MOTOR OIL


BROM08ENZENEHEXACOSANE

RL : Reporting LimitSURR1 : BroroobcnicneSURR2 : Hexacosane

DO : Diluted out

ND58000

RECOVERY

DODO

1400071000

OC LIMIT

4S-16527-176

HDL(ms/ks)

28002800

6£'d S2:8 £002 8

.rtaBuswda fcw_

METHOD H801STOTAL PETROLEUM HYDROCARBONS BY EXTRACTION

clUnt : ECOLOGY AMD ENVIRONMENTProject : DICO S1QNAL HILLBatch No. : 03F116Sample ID: DICO 015Lab Samp ID: F116-13Tlefa File ID: TF2706/AEXt BtCh ID: OSF020SCalib, ftef.; TF27060A

Date Collectedi 06/20/03Date Received; 06/20/03Date Extracted: 06/23/03Date Analyzed: 06/29/03Dilution Factor: 10Matrix : SOIL% Moisture : 19.2Instrument ID : GCT05Q

17:5014:35

PARAMETERS

DIESELMOTOR OIL


8ROHOBENZENEHEXACOSANE

RL • Reporting LimitSURR1 : SromobenzeneSURR2 : HORocoaane

RESULTS(mg/ks)

RL

780019000

X RECOVERY

DO00

120620

QC LIMIT

45-16527-176

MOL(me/kg)

2525

DO : Diluted out

92:8 £002 8

METHOD HS015

TOTAL PETROLEUM HYDROCARBONS BY EXTRACTION

Date Collected: NADate Received; 06/23/03»at« Extracted! 06/23/03 17:50Date Analyzed: 06/23/03 18:16Dilution Factor: 1Matrix : SOILX Moisture : NAInstrument ID : GCT050

Client :5roject :Satch No. :Sample ID;

ECOLOGY AND ENVIRONMENTDICO SIGNAL HILL03F116MBLK1S

Cab Samp ID; DSF020SBlab File ID: TF23004AExt Bteh ID: DSF020SCalib. Re* ! TF23002A

PARAMETERSRESULTS

(mg/k8)RL

(mg/kg)

1DTOR OIL


3ROMOBEN2ENEHEXACOSANE

RL : Reporting LimitSURR1 : QromobenxcneSURR2 : HexecosaneParameter H-C RangeOiesel C10-C24

Oil C16-C34

NOND

RECOVERY

10787

1050

QC LIMIT

45-16527-176

MDL(mg/kg)

22

017 'd 92:8 £002 8

EHAX QUALITY CONTROL DATALCS/LCD ANALYSIS

CLIENT: ECOLOGY AND ENVIRONMENTPROJECT: DICO SIGNAL HILL3ATCH NO.: 03F116METHOD: METHOD M8015

MATRIX:DILUTION FACTORSAMPLE ID:uAB SAMP ID;-AS fILE ID:JATE EXTRACTED:JATE ANALYZED:'SEP. BATCH;CALIB. REF:

ACCESSION:

SOIL1H8LK1SDSF020SBTF23004A

DSF020SLTF23005A

06/23/0317:50 06/23/0317:50

1

DSF020SCTFZ3006A06/23/03 \f; 50

06/23/0316:16 06/23/0318:56 06/23/0319]39DSF020STF23002A

DSF020S DSFQ20STFZ3002A

MOISTURE; NA

BATE COLLECTED: MA

DATE RECEIVED: 06/23/03

PARAMETER

Diesel

BLNK RSLT(mg/kg)

SPIKE AMT<mg/kg)

BS(itK

RSLT)Aa>

BS% REC

SPIKE AMT(mg/ks)

BSD RSLT(mg/ki>

BSDX REC

RPD QCC

LIMIT MAX RPD

ND 500 464 93 500 478 96 3 50-160 50

SURROGATE PARAMETER

Bromobenzenenexacoaane

SPIKE AMT(mg/kg j

10025

BS RSLT(mg/kgj

12023

BS% REC

12092

SPIKE AMT(mg/kg>

10025

BSD RSLT

12122.9

BSD'4 REC

12192

QC LIMI'

50-15030-160

92:8 £002 8

METHOD MB015TOTAL PETROLEUM HYDROCARBONS BY EXTRACTION

Client :Project ;Batch NO. ;Sample ID;Lab Samp ID:..ab File ID:£xt fitch ID:Calib. Ref.:

PARAMETERS

DIESELMOTOR OIL

ECOLOGY AND ENVIRONMENTDICO SIGNAL HILL

03F116

MBLK2S

DSF021SB

TF24060ADSF021STF24054A

Date Collected:Dote Rec«wod:Date Extracted:Date Analyzed:Dilution Factor;Matrix :X Moisture •Instrument ID :


ND 10ND 50

NA06/24/0306/24/0306/26/031SOILMAGCT050

(

16:3003:23

MDlms/ks )

22


JKQM08ENZENEItXACOSANE

*L : Reporting LimitSURR1 : Bromobenzenc5URR2 : Hexacosaneparameter H-C RangeOiesel C10-C24Motor Oil C18-C34

X RECOVERY

119101

8C LIMIT

45-16527-176

217'd 92:8 £002 8

EHAX QUALITY CONTROL DATALCS/LCD ANALYSIS

CLIENT: ECOLOGY AND ENVIRONMENTPROJECT: DICO SIGNAL HILLBATCH NO.: 03F116METHOD: METHOD

MATRIX:DILUTION FACTOR:SAMPLE ID:LAB SAMP ID:LAB FILE ID:DATE EXTRACTED:DATE ANALYZED:POEP. BATCH:CALIB. REF:

ACCESSION:

PARAMETER

Oicael

SOIL1HBIK2SDSF021SBTF2406QA06/E4/0316:3006/26/0303:23DSF021STF24054A

1

DSF021SLTF24061A06/24/0316:3006/26/0304:04DSF021STF24054A

1

DSF021SCTF24062A06/24/03\4:3006/26/0304:46DSF021STF24054A

BLNK RSLT SPIKE AMTCmaAg)

BS RSLT

% MOISTURE: NA

DATE COLLECTED: NADATE RECEIVED: 06/24/03

BSREC

SPIKE AMT(me/kg)

BSD RSLT(mg/kg:

BSDX REC

RPD QC LIMIT( X )

MAX RPO< X )

500 504 101 500 472 94 50-140 SO

SURROGATE PARAMETER

8romobenzeneHexacosane

SPIKE AMT BS RSLT(mg/kg) (n>s/k9>

10025

11326.8

BS SPIKE AMT BSD RSLT% REC (mg/kg) <tng/kg>

113107

10025

11225. B

BSD% REC

112103

QC LIMIT( X )

50-15030-160

£17'd 92:8 £002 8 \r\£

EMAX QUALITY CONTROL DATAHS/MSD ANALYSIS

CLIENT:PROJECT:BATCH NO.:METHOD:

MATRIX;DILUTION FACTOR;SAMPLE ID:LAB SAMP ID:LAB FILE ID!DATE EXTRACTED:DATE ANALYZED;PREP. BATCH:CALIB. REP:

ECOLOGY AND ENVIRONMENTDICO SIGNAL HILL03F116METHOD H8015

SOIL101 CO #10 COMPF116-10TF24075A06/23/0317:5006/26/0313:48DSF020STF24064A

1

F116-10MTFZ4077A06/23/0317:5006/26/0315:11DSF020STC26064A

1

F116-10STF24078A06/23/0317:5006/26/0315:53BSF020STF24064A

X MOISTURE: 19.0

DATE COLLECTED; 06/20/03BATE RECEIVED! 06/20/03

ACCESSION;

PARAMETER

Diesel

SMPL RSLT(mg/kg)

SPUE AMT(ma/kg)

MS RSLT(mg/kg) %

MSREC

SPIKE AMT(rag/kg)

MSD RSLTCms/ kg)

USDX REC

RPD( X )

QC LIMITX >

MAX RPO( X )

617 365 617 364 59 45-154 50

SURROGATE PARAMETER

BromobenseneHexacoaanc

SPIKE AMT(mg/kg)

12330.9

MS RSLT(mg/kg)

15770.7

MS SPIKE AMT MSD RSLT% REC (mg/kg) (mg/kg)

127229*

12330.9

15566.6

MSD% REC

125222*

OC LIMIT( X )

45-16527-176

Out of QC limits due to matrix interference

1717'd 92:8 £002 8

• A. . 3 -JO-*.*»*

SH3550B/S082

PCBs

ECOLOGY AND ENVIRONMENTOICO SIGNAL HILL

03F116

DICO 1 COMPF116-01WF 23071A

ClUntProjectBatch No.Sample IDLab Samp IDLab File IDExt Oteh ID: 60F019S

CaUb. Ref.: WF23QS4A

Date Collected:Date Received:Date Extracted:Date Analyzed:Dilution Factor:Matrix :X Moisture ;Instrument ID :

06/20/0306/20/0306/23/0306/24/031SOIL

5.2QCTQ16

18:3020:32

PARAMETERS

PCB-1016PCB-1221PCB-1232PCB-1242PCB-1248PCB-1254PCB-1260


TETRACHLORO-M-XYLENEDECACHLOROBIPHENYL

RESULTS(ug/kg)

ND|(ND)ND|(ND)NDJ(ND)NDJ(ND)NO|(NO)ND|(ND>

620£|(630E)

% RECOVERY

102|(82)93|(81)

RL(U9/kg)

53535353535355

MDl(U9/k

18181818181818

9)

18181818181818

QC LIMIT

54-14536-176

RL: Reporting LimitLeft of | is related to first column( > included the raported column* Out sida of QC Limit

Right of | related to second column

20'd 61:8 £002 8

SW3550B/8D82PCBs

Client ; ECOLOGY AND ENVIRONMENT

Project : DICO SIGNAL HILLBatch NO. : 03F116Sample ID; DICO 1 COHPDLLab Samp ID: H16-01TLab File IDi WF23100AEXt fitch ID: 60F019SCalfb. Rcf.i UF23099A

Date Collected: 06/20/03Date Received: 06/20/03Date Extracted: 06/23/03 18:30Date Analyzed: 06/25/03 11:01Dilution Factor; 5Matrix : SOIL% Moisture : 5.2Instrument ID : GCT016

PARAMETERS

PCB-1016

PCB-12Z1

PCS-1232PCB-1242PCB-124B

PCB-1254PCS-1260


TETRACHLORO-M-XYLENE

DECACHLOROB1PHENYL

RESULTS(ug/kg>

NDNDNDNONDND

(ND)(ND)(ND)(ND)(ND)(ND)

?20|(690)

% RECOVERY

85 | (77)

RL; Report ins LimitLeft of | is related to first column( ) included the reported colunn• Out aide of QC Limit

RL(ug/kg)

260

sw260260260260260

QC LIMIT

54-14336-176

MDL(us/kg)

686688

888888

88188881888818888188

Right of I related to second column

£0'd 61:8 £002 8

frl*4t- \v^

SU3550B/8082PCBs

Client : ECOLOGY AND ENVIRONMENT

Project : DICO SIGNAL HILLBatch No, : 03F116Sample ID: ptco 2 COUPLab Samp ID: F116-02Lab File ID: WF23072AExt Btch ID: 60F019SCalib. Ref.: UF230S4A

Date Collected; 06/20/03Date Received: 06/20/03Date Extracted: 06/23/03Date Ana Iyled: 06/24/03Dilution Factor: 5Matrix : SOILX Moisture : 11.8Instrument ID : QCT016

18:3020:57

PARAMETERS

PCS-1016PCB-1221PCB-1232PCB-1242PCB-1248PCB-1254PCB-1260


TETRACHLORO-M-XYLENEOECACHLOROBIPHENYL

RESULTS(US/kg)

NDNDNDND

(ND)(ND)(ND)(ND)

ND|(ND)ND|(ND>

1000|(7?0)

% RECOVERY

99|(84)97|(83>

RL: Reporting LimitLeft of | is related to first column( } included the reported column* out aide of QC limit

RLCug/kg)

280260280280280280280

MDL(ug/kg)

95 9595J959595

9595

95|959S|9S9SJ9S

QC LIHIT

54-14336-176

Right of 1 related to second column

170'd 02:8 £002 8

SW3550B/80S2PCBS

Date Collected: 06/20/03Date Received: 06/20/03Date Extracted: 06/23/03 18:30Date Analyzed: 06/25/03 12:16Dilution Factor: 15Matrix : SOILX Notsrure ; 2.5Instrument ID ; ecrou

(KentProI actBatch NosampleLab samp IDLab File IDExt Btch ID

ID;

ECOLOGY AND ENVIRONMENT

DICQ SIGNAL HILL03F116DICO 3 COMPF116-05WF23103A60F019S

Calib. Ref.; WF23099A

PARAMETERS

PCB-1016PCB-1221PCB-1232PCB-1242PCS•1248PC8-1Z54PCB-1260


TETRACHLORO-H-XYLENEDCCACHLOROBIPHENYL

RESULTS(us/kg)

NDNDNDNDNDND

(ND)(ND)(WO)(ND)(ND>(ND)

2500[C2200)

% RECOVERY

85|C67)711(47)

RL MOL(ug/kg) (ug/ks)

770770770770770770770

260(260260 j 260Z60|260Z6Q|260260)260260)260260)260

QC LIMIT

54-14336-176

RL: Reporting LimitLtft of | is related to first column ; Right of( ) included the reported column« Out side of QC Limit

[ related to second column

02:8 £0028

SU3S50S/S082PCBs

Client :Project :Batch No. :Sample ID:Lab Samp ID:Lsb File ID;Ext Btch 10:Calib. Ref.:

PARAMETERS

PCB-1016PCB-1221PCB-1232

PCS -1246PCB-1254PCB-1260

ECOLOGY ANDDICO SIGNAL03F116OICO 4 COUPF116-06HF23104A60F019SWFZ3099A

ENVIRONMENTHILL

RESULTS(ug/kg)

NDNDNDNDNDND

3700

(ND)<KD)(NO)(ND)(ND)(ND)(3400)

Date Collected:Date Received:Date Extracted:Date Analyzed:Oi lution Factor:Matrix :% Moisture :Instrument ID i

RL(ug/kg)

770770770770770770770

06/20/0306/20/0506/23/03 18:06/25/03 12:15SOIL2.96CT016

HDL(US/kg)

2601260260 | 260260 | 260260 | 260260 | 260Z60J260260 | 260

3042


TETRACHLORO-M-XYLENEDECACNLOROB1PHENYL

% RECOVERY

65|(53>146)(93)

RL: Reporting LimitLeft of | is related to first column ; Right of( ) included the reported column* Out side of QC Limit

QC LIMIT

S4-14S36-176

related to second column

80 'd 02:8 £002 8

CUent 5

Project

Batch No.SampleLab SartpLab FileExt 8tch

;*

ID:ID:ID:ID:

Calib. Ref.:

SW3550B/B082PCBs

ECOLOGY AND ENVIRONMENT

DICO SIGNAL HILL

03F116

OICO 5 COHP

F1 16-07UF23105A60FQ19SWF23099A

Date Collected:Date Received:Date Extracted:Date Analyzed:Dilution Factor:Matrix :% Hoisture :Instrument ID ;

06/20/0306/20/0306/ZS/0306/25/03250SOIL2.4CCT016

18:3013:07

RESULTSPARAMETERS

PCB-1016PCB-1221PCB-1232PCB-1242PCB-1248PCB-1E54PCB-1260


TETRACHLORO-M-XYLENE

OeCACHLOROBlPHENYL

ND|(NP)NDJ(ND)

ND|(ND)ND|(ND)

NDJ(ND)

75000 | (62000)

% RECOVERY

DO | DODO j DO

RL; Reporting LimitLaft of | is related to first column ; Right of( ) included the reported column* Out side of QC Limft

RL HPL(us/kg) (ug/kg)

13000 4300|430013000 &IODJ430013000 43DO|430013000 4300|430015000 43001630013000 4300|430013000 43CO|4300

QC LIMIT

54-14336-176


60'd 02:8 £002 8

SW355C9/8062PCBS

clientProjectBatch NoSampleLab samp ID;Lab Pile IDiExt Btch

: ECOLOGY AMD ENVIRONMENT; DICO SIGNAL HILL: 03F116

ID: DICO 6 COUPF11o-03UF23101A

ID; 6DF019SCalib. Ref.: UF2309QA

Date Collected: 06/20/03Date Received: 06/20/03Date Extracted: 06/23/03 18:30Date Analyzed: 06/25/03 11:26Dilution Factor: 100Matrix : SOILX Moisture : 4,7Instrument ID : GCT016

PARAMETERS

PCB-1016PCS-1221PCB-1232PCB-1242PCS-1246PCS-1254PCB-1260


TETRACHLORO-H-XYLENEDECACHLOROBIPNENYL

RESULTS(ug/kg)

NDNDND

(ND)(ND)(NO)

ND|(ND)NDND

(ND)(ND)

35000|(27000)

% RECOVERY

115|(80)B9|(92>

RL: Reporting LimitLeft of | is related to first column( ) Included the reported column* Out side of QC Limit

RL(ug/ks)

MDL(ug/kg)

5200 1800|18005200 1800j18005200 1600j18005200 1800j18005200 1800j16005200 1BOO|18005200 1800j1800

QC LIMIT

54-14336-176


SO'd 02:8 £002 8

A *. l_ „,.,

SW3550B/60B2PCBs

client : ECOLOGY AND ENVIRONMENTProject : DICO SIGNAL HILLBatch No. s Q3F116Sample ID; DICO 7 COHPLab San? ID: M16-04Lab File ID: UF23102AExt Bteh ID: 60F019SCalib. Ref.: UF23099A

PARAMETERS

Oate Collected: 06/20/03Date Received: 06/20/03Date Extracted: 06/23/03 18:30Date Analyzed: 06/25/03 11:51Dilution Factor: 100Matrix : SOIL2 Moisture : 3.5Instrument ID : CCT016

PCB-1016PCB-1221PCB-1232PCS-1242PCB-1248PCB-1254PCB-1260


TETRACHLORO-H-XYLENEDECACHLOROBIPHEKYL

RESULTS(ug/kg)

ND (ND)ND (ND)ND (ND)ND (ND?ND (ND)ND (NO)

33000 (26000)

RL(ug/Kg)

S200520052005200520052005200

MDL<U8/kg>

1700 | 17001700 17001700 17001700 17001700 17001700 17001700 1700

% RECOVERY

99|(87)100|(85)

RL: ReportfngLeft of | ia related to first column ; Right of( } included the reported colum* Out side of QC Limit

QC LIMIT

54-14336-176


90'd 02:8 £0028

SU35SOB/8082PCBS

Client : ECOLOGY ANDProject : DICO SIGNALBatch No. : 03F116Sample ID: DICO «8Lab Samp ID: F116-OSLab File ID: WFZ3083AExt Btch ID: 60F019SCalib. Ref.: WF23078A

PARAMETERS

PCB-1016PCB-1221PCB-1232PCB-1242

PCB-1248PCB-1254PCB-1260


TETRACHLORO-M-XYLENEDECACHLOROB1PHENYL

ENVIRONMENTHILL

RESULTS(us/kg)

NDl(ND)NDl(ND)NO (ND)ND (ND)ND (ND)ND (ND)

1704|(180J)

% RECOVERY

77 |(68)70|(58)

Date coUcctod;Date Received;Date Extracted:Date Analyzed:Di lution Factor:Matrix :% Moisture ;Instrument ID ;

RL(ug/kg)

260260260260260260260

ac LIMIT

54-14336-176

s»=£3Z=::=£

06/20/0306/20/0306/23/03 1806/25/03 015SOIL4.7GCT016

MDL(ug/kg)

88 1 8888 1 8888 8866 8088 88B8 &888 86

=3-

-.30:34

RL: Reporting LimitLeft of | is related to first column( ) included the reported* Out side of QC Limit


OT'd 12:8 £002 8 inr;

>*«.

SUJ550B/8082PCBe

ClientProjectBatch No,Sample ID:Lab Samp IDLib Ftle ID: UF23004AExt Btch ID: 60F019SCalib. Ref.: WF23076A

ECOLOGY AND ENVIRONMENTDICO SIGNAL HILL03F116DICO W) COWF116-09

Date Collected: 06/20/03Date Received: 06/20/03Date Extracted: 06/23/03 18:30Date Analyzed: 06/25/03 02:00Dilution Factor: 5Matrix : SOIL% Moisture : 4.2Instrument ID ; CCT016

RESULTSPARAMETERS

PCB-1016PCB-1221PCB-1232PCB-1242PCS-1248PCB-1254PCB-1260


T6TRACHLORO-M-XYIENEDECACHLOROB1PHENYL

NDNDHDNDND

(ND)(MO)(ND)(ND)(ND)

NO ItNO)1900EJO600E)

% RECOVERY

102|(80)781(64)

RL: Reporting LimitLeft of 1 1s related to first column ,- Rijht of( ) included the reported eel urn* Out side of QC Limit

RL(us/kg)

260Z60Z60260260260260

MDL(us/kg)

87er8787876787

87678747678787

OC LIMIT

54-14336-176


12:8 £002 8

SW3550B/8082PCBs

ClientProjectBatch No.Sample IDLab Samp 10Lab File 20Ext Btch IDCalib. Ref.s==3SB==:«==

: ECOLOGY AND ENVIRONMENT; DICO SIGNAL HILL: 03F116: DICO #9 COMPDL: F116-09T: UF23106A: 60F019S: WF23099A=53KC=»=artE=v=s*CC=»==tflC=w=~R

Datv C<jll«etedtDate Received:Date Extracted:Date Analyzed:Dilution Factor:Matrix :% Moisture :Instrument ID :

06/20/0306/20/0306/23/0306/25/0315SOIL4.2CCT016

18:3013:32

PARAMETERS

PCB-1016PCB-1221PCB-1232PCB-1242PCB-1248PCB-1254PCB-1260


TETRACHLORO-M-XYLENEOECACHLOR08IPHEMYL

RESULTS(ug/kg)

NDNDNDNDNDND

(ND)(ND)(ND)(NO)(ND)(ND)

2300|(1900)

X RECOVERY

1051(75)831 (71)

RL; Reporting LimitLeft of ] is related to first column ,- Right of( ) included the reported col urn* Out side of ac Limit

RL(ug/kg)

7807BO780780780780780

MDL(ug/Kg)

260(260260 260260260260260

260260260260

260 1 260

QC LIMIT

54-14336-176


'd 12:8 £002 8

SU3550B/60B2PCBs

Date Collected: 06/20/03Date Received: 06/20/03Date Extracted: 06/23/05 18:30Date Analyzed: 06/25/03 02:25Dilution Factor: 5Matrix : SOIL55 Moisture : 19.0Instrument ID : QCT016

CUentProjectBatch No.SampleLab Samp ID:Lab File ID:

: ECOLOGY AND ENVIRONMENT; DICO SIGNAL HILL: 03F116

ID: DtCO #10 COMPF116-10WFZ3085A

Ext Bteh ID: 60F019SCalib. Ref.: UF230raA

PARAMETERS

PCB-1016PC8-1221PC6-1232PCB-U42PCB-1248PCB-1254PCB-1260


TETRACHLORO-M-XYLENEDECACHLOROB1PHEHYL

RL; Reporting LimitLeft of | is related to first colum( ) included the reported column* Out side of QC Limit

RESULTS(us/kg)

ND|(ND)NDJ(ND)NDJ(ND)NDJ(ND)NDl(ND)NO UNO

9400E|(12000E)

X RECOVERY

104 |(89)81) (69)

nr ; Right of |

RL(ug/kg)

210310310310310310310

QC LIMIT

5VH336-176

MDL(ug/kg)

100)100100)100100J100100|100100)100100)100100)100

related to second colutm

21 'd 12:8 £002 8

SW3550B/8082PCB6

Client : ECOLOGY AND ENVIRONMENT Date Collected: 06/20/03Project ; DICO SIGNAL HILLBatch No. : 03F116Sanpl» 10: DICO 910 COMPDLLab Sanf ID: F116-10TLab File ID; WF2310TAExt Btch ID; 60F019SCaUb. Ref.: WF23099A

PARAMETERS

PCB-1016PCB-1221PCB-1232PCS -1242PCB-12&8PCB-1254PCB-1260


TETRACHLORO-H-XYLENEDECACHLOROBIPHENYL

RESULTS(ug/k3)

ND (ND)ND (ND)NDJ(ND)ND (ND)ND (ND)ND (ND)

25000 (20000)

X RECOVERY

103 | (84)99 (75)

Dote Received: 06/20/03Date Extracted: 06/23/03 18:30Date Analyzed: 06/25/03 13:57Dilution Factor; 100Matrix : SOILX Moisture i 19.0instrument ID : GCT016

RL MDL(ug/Xg) (ug/kg)

6200 2100(21006200 2 100 j 21 006200 2100 21006200 2100 21006200 2100 21006200 2100 21006200 2100 2100

QC LIMIT

54-14336-176

RL: Reporting LimitLeft of | is related to first column( ) included the reported column* Out side of ac Limit


12:8 £0028 jnf

SW3550B/SOB2PCBs

Client : ECOLOGY AND ENVIRONMENTProject : DICO SIGNAL HILLBatch No. : 03F116Sample ID: DICO #11Lab Samp 10: F116-12Lab File ID: UF23112AExt Btch ID: 60F019SCalib. Ref.: UF25099A

Date Collected: 06/20/03Date Received: 06/20/03Date Extracted: 06/23/03 18:30Date Analyzed: 06/25/03 16:03Dilution Factor: 500Matrix : SOILX Moisture : 19.2Instrument ID : &CT016

PARAMETERS

PCB-1016PCS-1221PCB-1232PCB-1242PCB-1248PCB-1254PCB-1260


TETRACHLORO-M-XYLENEDECACHLORQBIPHENYL

RESULTS(ug/kg)

NDNDNOND

NDND

200000

(ND)(ND)(NO)(ND)(ND)(ND)(160000)

RECOVERY

DO [00DO | DO

RL: Reporting LimitLeft of | is related to first column( ) Included the reported column* Out side of QC Limit

ftL H&L(ug/kg) <ufl/k9>

31000 10000j1000031000 10000j1000031000 10000)1000031000 1000011000031000 10000)1000031000 10000)1000031000 10000(10000

QC LIMIT

54-14336-176


9I'd 22:8 £002 8

5W53508/8082PCBS

...:*.* *• ._

CUent : ECOLOGY AND ENVIRONMENTProject : DICO SIGNAL HILLBatch No. s 03F116

ID; DICO #12Lob Samp ID: F116-11Lab File ID: UF23108AExt Btch ID; 60F019SCaUb. Ref.: WF23099A

Date Collected: 06/20/03Date Received: 06/20/03Date Extracted; 06/23/03 18:30Date Analyzed: 06/25/03 14:22Dilution Factor:Matrix% MoistureInstrument ID

20SOU6.6GCT016

PARAMETERS

PCB-1016PCB-1221PCB-1232PCB-1242PCB-1248PCB-1254PC8-1E60


TETRACHLORO-M-XYLENEOECACHLOROBIPHENYL

RESULTS(uo/kg)

NDNDNDNDNDND

(ND)(NO)(ND)(ND)(NO)(ND)(3500)

X RECOVERY

103|<85)I0a|(82)

RL: Reporting LimitLeft of | is related to first column< ) included the reported column* Out side of OD Limit

RL(ug/kg)

MDL

1100110011001100110011001100

OC LIMIT

54-145

36-176

560|360360360360360

360360360360

360 j 360360 | 360


ST'd T2:8 2002 8 \r\£

SW3550B/8082PCBs

Client :Project ;Batch No. :Sample ID:Lab Samp ID:Lab File ID: UF23113AExt Btch ID! 60F0195Calib. Ref.: WF23099A

ECOLOGY AND ENVIRONMENTPICO SIGNAL HILL03F116DICO #15F116-13

Date Collected: 06/20/03Pat* ft««eived: 06/20/03

Date Extracted: 06/23/03 18:30Date Analyzed: 06/25/03 16:29Dilution Factor: 500Matrix : SOILX Moieturc : 19.2Instrument ID : GCT016

PARAMETERS

PCB-1016PCB-1221PCS -1232

PCS -1248PCB-12S4PCB-126Q


TETRACHLORO-M-XYLENEDECACHLOROB1PHENYL

RESULTSCuo/kg)

NDNONDND

(ND)(ND)(ND)(ND)

NO|(ND)NDJ(NO)

190000|(150000)

% RECOVERY

DQ|00DO | DO

RL: Reporting limitLeft of j is related to first column( ) included the reported column* Out side of QC Limit

RL MDL(US/kg) (ug/kg)

31000 10000(1000031000 10000|1000031000 10000)1000031000 10000|1000031000 1000011000031000 1000031000 10000

QC LIMIT

1000010000

54-14336-176


22:8 £0028

SW355OB/8082PCB5

Client : ECOLOGY ANDProject ; DICO SIGNALBatch No. : 03F116Sanple ID: DICO #13Lab Samp ID: F116-14Lab File ID: WF23095AExt Btch ID: 60F019SCalib. Ref.: UF2307BA

PARAMETERS

PCB-TOlePCB-1221PCB-1232PCB-1242PCB-1248PCB-1254PCB-1260



RL: Reporting LimitLeft of ) is related to f( ) included the reported* Out side of QC Limit

ENVIRONMENTHILL

RESULTS(ug/kg)

ND|(ND)NDJ(ND)ND (ND)ND (ND)ND (HD)ND (NO)ND|(ND)

% RECOVERY

117|(104)104 j (66)

Irst column ; Right ofcolum

Date Collected: 06/20/03Date Received: 06/20/03Date Extracted: 06/23/03 18:30Plate Analyzed: 06/25/03 04:37Dilution Factor: 30Matrix : SLUDGE% Moisture : NAInstrument ID : GCT016

RL MDL(ug/kg) < us/kg)

1500 500 5001500 500 5001500 500 5001500 500 | 5001500 500)5001500 500(5001500 508 | 500

QC LIMIT

54-14336-176

| related to second column

81 'd 22:8 £002 8

PCB3

Client : ECOLOGY AND ENVIRONMENTProject : DICO SIGNAL HILL

Batch No. : 03F116Sample ID: DICO #14Lab Samp ID; F116-15Lab File ID: WF23111AExt Btch ID: 60F019SCaltb. Ref.: WF23Q99A

Date Collected: 06/20/03Date Received: 06/20/03Date Extracted: 06/23/03 18:30Date Analyzed: 06/25/03 15:38Dilution Factor: 250Matrix : SOIL% Moisture ; 29.1Instrument ID : acTOio

RESULTSPARAMETERS (us/kg)

PCB-1016 ND|(ND)PCB-1221 ND|(NP)PCB-1232 NPJ(ND)PCB-12C2 ND|(ND)PCS-1248 360001(31000)

PCB-1254 NDJ(ND)

PCB-1260 6700JJC6600J)

SURROGATE PARAMETERS % RECOVERY

TETRACHLORO-M-XYLENE 00|DODECACHLOROBIPHENYL DOJDO

RLc Reporting LimitLoft of | is related to first column( ) included the reported eolunn* out side of QC Limit

Calib. Ref. file for PCB 1248: UG03007A

RL MDL(ug/kg) (us/kg)

16000 5500|590016000 59001590018000 5900J50QO18000 5900)590018000 5000)590018000 5900|590018000 5900)5900

QC LIMIT

54-14336-176


61 'd 22:8 £002 8

(.-*.

SU355 OB/6082

cuent ECOLOGY ANDProject DICO SIGNALBatch NO. 03F116Sample ID MBLK1SLob Samp ID 60F019SBLab File ID UF23066AExt Btch ID 60F019SCalib. Ref. WF23054A

PCBS

ENVIRONMENTHILL

RESULTSPARAMETERS

PCB-1016KB-1Z21PCB-1232PCB-1242PCB-1248PCB-1254PCB-1260


TETRACHLORO-M-XYLENEDECACHLQROBIPHENYL

(ug/kg)

ND|(ND)NDJ(ND)NDNDNDNDND

?ND)(NO)(ND)(ND)(ND)

X RECOVERY

71|C60)95 | (75)

Date Collected: NADate Received: 06/23/03Date Extracted: 06/23/03 IBDate Analyzed: 06/24/03 18Dilution Factor: 1Matrix : SOILX Moisture : NAInstrument ID : CCT016

:30:26

RL MDL(U9/k9) (ug/ks)

SO 17|1750 17|1750 17 1750 17 1750 17 1750 17 1750 17 17

OC LIMIT

54-14336-176

RL: Reporting LimitLeft of [ is related to first column< ) included the reported column* Out aida of OC Limit

Right of | related to second col urn

02 'd 22:8 £002 8 \r\£

SW3550B/808ZPCBs

clientProjectBatch No.Sample IDLab Samp 10Lab File IDExt Btch IDCalib. Ref.

f-ARAnETCKS

PCB-1016PCB-1221PCB-1232PCB-1ZA2

PCB-1248PCS -1254PCB-1260

; ECOLOGY AND-. DICO SIGNAL; 03F116: MBLK2S: 60F020SB: WFZ3092A: 60F019S: MF2907SA

ENVIRONMENTHILL

RESULTS(ug/kg)

ND|(ND)ND|(ND)ND|(ND)NO (ND)ND|(ND)ND|(ND)NDJ(NO)

Date Collected:Bate Received;

Date Extracted:Date Analyzed;Dilution Factor;Matrix :% Moisture :Instrument ID :

RL(us/ks)

150015001500150015001SOD1500

NA06/23/0306/23/03 18:3006/25/03 05:2130SOILNAGCT016

MDL<uj/kB)

500|SOC500 | 500500(500500 500SOO 500500(500500 500



X RECOVERY

117|(97)721(69)

QC LIMIT

54-14336-176

Rl: Reporting LimitLeft of | is related to ftrst colum( ) included the reported column* Out side of QC Limit

Right of I related to ascend column

£2:8 £002 8 \r\£

EHOC OUAUTY CflHTKOI. DATALCS/LCD ANALYSIS

CLIENT:

PROJECT:

CM BATCH NO.:

^ METHOD:

MATRIX:

£0 DILUTION FACTOR:

" SAMPLE ID:

LAB SWP ID:

LAB FILE ID:

0 DATE EXTRACTED:CN DATE ANM.YZEO:

Oo PREP- BATCH:CALIB. REF:

3•~> ACCESSION:

PARAMETER

PCS- 1016

PCB-1260

ECOIOGY AMD

DICO SIGNAL

03F116

EWmcHHEfiT

HILL

SW3550B/B082

SOUtMBLK1S

60F019SB

WF23066AOi/23/0318:

60F019S

WFZ3054A

X N3ISTUKE: KA1 1

60F019SL 60F019SC

MF25067A WF2306BA30 06/23/0318:30 06/23/0318:30 DATE COLLECTED: NA

26 06/24/0318:51 06/24/0319:16 DATE RECEIVED: 06/Z3/0360F019S 60r019s

VF23054A WFZJ054A

BLNK NSLT SPUE AW BS RSL1 BS SPIKE ANT

<«3/kg> (u9/k9) (m/M) % R£C (ug/kg)

NDJ(ND) 167 149|<117) 89|(70) 167

«D|(NO) 167 20S((t56) 123|(94) 167

BSD RSLT BSD RPD flC LIMIT MAX «fD

<ug/kg) XREC ( X ) ( % ) ( 5 ! )

150|t12D) 90iC7Z) 1|<3) 30-150 50

206 j< 156) 124|<94) 0|(0) 40-160 50

SPIKE AMI BS RsirSURROGATE PARAMETER

BS SPIKE ANT% REC

BSD RSI! BSD OC L I M I T

% REC ( % )

Oecach (orobiphenyl

13.3 11|(9.15) S$|<69) 13.3 11.2|<9.Z9) M|(70) 60-15013.3 13.6J(10.5) 10H|(78) 13.3 13.8|(10.6> 103(<79) 40-160

EHAX QUALITY COMTJtOL DATA

LCS/LCB ANALYSIS

CLIENT: ECOLOGY AMD EHVI ROHHEW

PROJECT: DICO SIGNAL HILL

^ BATCH »0.: 03F116

^ METHOD: SVB550B/80B2

KATRIX: SOIL

£0 DILUTION FACTOR: 30

" SAMPLE 10: NBLK25

LUB SAMP ID: 60FOZOSB

LAB FILE ID: WF23092A0 DATE EXTRACTED: 06/23/0318:50R DATE ANALYZED: 06/25/0305:21

CO PREP. BATCH: 60F019SCALIB. REF: UF23078A

^ ACCESSION:

PARAMETER

PCB-1016

PCB-1H60

30 30

60FC20St 60FOZOSC

06/Z5/031B:30 0£/2J/031506/25/03C$:4& 06/25/03066QF019S 60F019SUF3307flA HFZ307BA

BLNK R5LT SPIKE AH T(us/ks) m»/k9>

ND|(HD) 167NO j (NO) 167

SPIKE ANT BS RS1T

SURROGATE PARAMETER

letrach toro-ro- xyleneDecachlorobi phenyl

(Mg/kg) <ua/kg)

13.3 15.7|(1Z.7)13.3 9.62JC9.25)

X MOISTURE: HA

:30 DATE COLLECTED: MA:11 DATE REtZIYED: 05/23/03

B5 RSLT BS SPIKE ANT BSD RSLT BSD RPD(ug/kg) X REC 0«/kg> (na/kg) X REC C X )

1W|<149) 116|C«9) 167 176|(144> 10&|C8*5 9|(3)IB3|(154) 110|(92) 167 1W((156) 113JC9O 3|(13

KS SPIKE ANT BSO SSLT BSD QC LIMIT% K.L <ua/kg) (us/kg) % REC ( X )

11B|<96> 13.3 15.1) (12.8) 113) (94) 60-130

72|<69) 13.3 10.7}<a.OZ) 80] (60) 40-160

OC LIMIT HAX RPD

( X ) < * >

30- 150 50

40-160 50

EHAX QUALITY CONTROL DATA

Ht/NSD ANALYSIS

CLIENT: ECOLOGY AND ENVIRONMENTPROJECT: HI CO SIGNAL HI LI

^ BATCH NO.: 03FI16<N NETKQO: SU3550B/80B2

MATRIX: SOILK> DILUTION FACTOR: 5^ SAMPLE ID: DICO #10 CONP00 LAB SAMP ID: F1 16-10

LAB FILE 10: UP 23085 A0 DATE EXTRACTED: 06/23/0318:30£3 DATE ANALYZED: 06/25/0302:25oo PREP- BATCH: 60F019S

CALI8. REF: UFZ3078A

>~> ACCESSION:

PARAMETER

PCB-1016

PCB-12AO

5

F116-10NW23CS6A05/23/03 1fl:3fl05/25/0502:5060F019SMF23CrfiA

SMPL RSLT<ug/ks>

8100[(12000)

% MOISTURE: 19.05

F116-10SWFZ30B7A

06/23/0318:30 DATE COtLEcrEO: 06/20/0306/ZS/OJ03:15 OAfE RECEIVED: OA/20/C360F019SWF23078A

SPIKE AMI MS RSL1 HS SPIKE AMT(U3/kg> do/kg) X REC (us/kg)

1030 1370 1 (3020) 327* (C2W) 10301030 W80JC1420D) ia3*(C214») 1030

SPIKE AMI MS RSLT MS SPIKE AMI USD RSLT

SURROGATE PARAMETER (

Tetrachloro-m-xyleneDeoachl orobi ph wiyl

;u3/ks) <iug/kg) X REC < ug/kg) (ug/kg)

82.3 80.6|(66.3) 98|(81) B2.3 83.7|<69.6)82.3 46.1 1(63.5) 80|(7/) 82.3 70.5(<65.6)

USD RSLT KSt> RPO OC LIMIT MAX RPD

(us/kg) % REC < % ) c % ) < X )

33BOl<2690) 32B*|(Z61*) OJ(12) 2T-165 509810JO3500) 16tj(146> 2|<5) 36-176 50

HSO QC LIH1TX REC ( X )

102|<85) 54-14386|(80) 36-176

* : Outside of QC limits

sample id: dico 1 cohp date analyzed: 06/25/03 19:45 lab ... · sw305ob/601ob metals by icp client...

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