s1 titan - benelux scientific€¦ · s1 titan hh xrf for various applications andré schmuck...
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BRUKER COMPANY CONFIDENTIAL 2014 1
S1 Titan
HH XRF for various applications
André SchmuckDirector Sales EMEAHandheld, Mobile Portable Products
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Contents
• Bruker Instruments
• What Is XRF?
• How Does It Work?
• XRF for Metals
• XRF for Mining
• Models & Accessories
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Bruker
• Founded 1960 in Germany
• Headquarters in Billerica, MA
• Analytical Equipment
• $1.84 Billion revenue (2013)
• Bruker Elemental
• HHXRF in Kennewick, USA
• OES & CGA in Kalkar, Germany
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Technologies
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Mass Spectrometry and Separations Remote Sensing CS/ONH-Analysis IMS
GC Systems Imaging Spectrographs Magnetic Resonance MS
GC-MS Terahertz NMR FT-IR
FTMS OPUS - Software EPR ELISA
MALDI-MS X-ray Diffraction and Elemental Analysis MRI PCR
MALDI Biotyper X-ray Diffraction Time Domain (TD)-NMR ASAS
LC-MS Single Crystal X-ray Diffraction Power Electronics NAA
ICP-MS X-ray Micro-CT Surface Analysis Preclinical Imaging
Software X-ray Spectrometry Atomic Force Microscopy MR Imaging
Molecular Vibrational Spectroscopy Handheld XRF 3D Optical Microscopy Optical imaging
FT-IR X-ray Metrology Stylus Profilometry PET/ SPECT/ CT
FT-NIR EDS, EBSD and SEM Micro-CT Tribology and Mechanical Testing micro-CT
Raman Optical Emission Spectrometry Mobile Detection X-ray
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What Is XRF?
• Analytical Method For Determining Elemental Content
• Qualitative And Quantitative
• Mg - U
• Fast – All Elements At Once
• Wide Range (PPM to 100%)
• Accurate & Precise
• Non Destructive
• Near Surface
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How Does It Work?
An X-ray of sufficient energy strikes an inner
shell electron of an atom in the sample, ejecting the electron
from its orbit.
Next-- an electron from an outer shell
moves to fill the vacancy in the inner
shell.
An X-ray photon is released and hits the analyzer’s detector.
This photon’s energy is unique to the element
it came from.
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XRF Components
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Line Energy Graphite Glass Iron Lead
Cd KA1 23.17 keV 14.46 cm 8.20 mm 0.70 mm 77.30 m
Mo KA1 17.48 6.06 3.60 0.31 36.70
Cu KA1 8.05 5.51 mm 0.38 36.40 m 20.00
Ni KA1 7.48 4.39 0.31 29.80 16.60
Fe KA1 6.40 2.72 0.20 * 164.00 11.10
Cr KA1 5.41 1.62 0.12 104.00 7.23
S KA1 2.31 116..0 m 14.80 m 10.10 4.83
Mg KA1 1.25 20.00 7.08 1.92 1.13
F KA1 0.68 3.70 1.71 0.36 0.26
N KA1 0.39 0.83 1.11 0.08 0.07
C KA1 0.28 * 13.60 0.42 0.03 0.03
B KA1 0.18 4.19 0.13 0.01 0.01
0.01 m = 10 nm = 100 Å
atom radius: 0.5 - 3 Å
What is “Near Surface”?
(C) AS
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Radiation Safety
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Backscatter Shut-off
IR Sample Sensor
Warning Lights
Multilevel User Log-in User Supervisor
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S1 TITAN for Metal Application
21.05.2014Innovation with Integrity
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• Originated in the refinery industry
• Used to Ensure plant safety
• Over 75% of refinery failures are caused by installation of incorrect alloy
• Major refineries require 100% inspection and verification
Material TestingPositive Material Identification (PMI)
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Material TestingPMI
Why is HHXRF used for PMI?
• Non-destructive testing
• Battery powered
• Speed & accuracy
• Ease of use
• Library size – over 400 alloys
• Customizeable user library
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Material TestingPMI
Why is HHXRF used for PMI?
• Avoid material mixups
• Provide alloy verification to customers
• Can be used on almost any metals
• Easy data storage & transfer to a report
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Scrap/Recycling
Why is HHXRF used forScrap/Recycling?
• Rapid, On-the-spot analysis of incoming materials
• Ease of use
• Weight/Field use
• Speed
• Faster = more $
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Scrap/Recycling
Why is HHXRF used forScrap/Recycling?
• Accuracy (esp. valuable elements)
• Customizable user library
• Sort & Grade Incoming & OutgoingScrap for higher value
• Light Elemental Analysis – Al, Si, Mg
• Analysis of Tramp Elements
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Alloy Analysis
21.05.2014Bruker Confidential
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Alloy SMARTGrade
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• Provides complete timing of the measurement
• All with Automatic Trigger
• No user judgment required
• Custom table can be created
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ALLOYS SMARTGRADE™Press button get grade!
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Pass/Fail Mode
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Pass/Fail mode allows the quick investigation of samples with little or no background in alloy composition
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S1 TITAN for Mining Application
May 21, 2014
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XRF In Mining
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Applications in Mining
Exploration
Grade Control
Mineral Processing
Plant Maintenance
Mine Closure & Reclamation
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Exploration
• Field Based Analytical Solution
• Real-Time Spatially Registered Geochemistry
• Interactive & Immediate Feedback in the Field
• Dramatically Increase Sample Density (100’s Samples per Day)
• Compared to laboratory analysis, handheld XRF provides a huge time savings.
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Exploration
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Used for:
• Soil Sampling
• Percussion Drill Chip Screening
• Core Analysis
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Grade Control
• More Samples, More Often = More Confidence!
• Significantly Reduce Decision Making Timeframes
• Blast Hole Sampling
• Open Pit - Ore Boundary Definition & Mapping
• Underground Face Sampling & Mapping
• Stockpile Checking & Monitoring
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Mineral Processing
• Investigation, Refinement & Problem Solving
• Use Real-Time Geochemistry in Your Flow-Sheet
• Simple Pre-Feasibility & Pre-Mining Data Acquisition (Met-Testing)
• Geometallurgy – Analysis of Elements not in the Standard Assay Package
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Plant Maintenance
• Preventative & Predictive Maintenance Tool
• Alloy & PMI Analysis
• Oil Analysis – Wear Metals: Ca, V, Cr, Fe, Ni, Cu, Zn, Pb & P
• Sulfur Level Determination in Diesel Fuels
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Mine Closure & Reclamation
• Real-Time In-Situ Soil & Filter Analysis
• Instant Delineation of contaminated soil boundaries
• Improved project management & cost savings
• Interactive Monitoring
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Handheld XRF ApplicationsIndustrial Minerals
• Limestone, Calcium carbonate (CaCO3) is one of the most versatile minerals found in the earth's crust. Physical properties and low processing cost makes it the most widely used filler material.
• Handheld XRF can be used to measure Calcium carbonate composition directly from rock or from quarry. This information can be used to effectively control mining and excavation process.
• Sand and Feldspar grade and Fe control
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Limits of Detection
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Different sample cups
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1530 cup with 1630 lid31mm/23mm/24mm
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Lose powder/slurry/pastes preparation
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CONFIGURATIONS
34BRUKER COMPANY CONFIDENTIAL 2014
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The UNIQUE and MOST IMPORTANTNow standard on ALL units
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TITAN Detector Shield
BRUKER COMPANY CONFIDENTIAL 2014
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Camera functionality
36BRUKER COMPANY CONFIDENTIAL 2014
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Make up to 5 pictures per object.Trigger pull makes the measurement.
37BRUKER COMPANY CONFIDENTIAL 2014
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S1 Remote
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Limits Editor
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Report Generator
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Spectrum ViewerOptions Dialog
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Spectrum ViewerAtomic Table
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Optional Accessories
• Test Stand
• Holster
• Bluetooth GPS Receiver
• Data Reporting Software
• Bluetooth Printer
• Tablet Computer
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21. Mai 2014 44© Copyright Bruker Corporation. All rights reserved