[report of findings for 2012 deep monitoring well … · 2020. 11. 29. · report of findings 20 f...
TRANSCRIPT
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FTS
~G i\IL-
p ... 3: 4~ 13 FEB 26 n
· '~~~ Field & Technical Services 200 Third Avenue • Carnegie, PA 15106 • Phone: 41 2·429·2694 • Fax: 412-279·4512
February 27. 20 13
Ms. Raji Josiam Mail Code 6SF-AP U.S. Environmental Protection Agency 1445 Ross A venue. Suite 1200 Dallas, Texas 75202-2733
RE: Report of Findings 2012 Deep Monitoring WeU Sampling and Analysis South Cavalcade Superfund Site Houston, Texas
Dear Ms. Josiam:
This report presents the results of the 20 12 deep monitoring wel l groundwater sampl ing and analysis program conducted in accordance with the Record of Decision (ROD) and United States Environmental Protection Agency approved Remedial Design Work Plan (RDWP) for the South Cavalcade Superfund Site located in Houston. Texas. The annual groundwater sampling event was conducted on May I 0. 2012 in accordance with the procedures outlined in the Remedial Design Sampling and Analysis Plan and the Remedial Design Quality Assurance Plan.
The objective of the deep well sampling program is to determine if potential.ly carcinogenic polycyc lic aromatic hydrocarbon (pcPAH) compounds are present above background concentrations in groundwater in the deep aquifers beneath the site. To meet the sampling program objective. two deep monitoring wells (well DW-02 [approximately 200 feet deep] and well LCW-01 [approximately 500 feet deep]) (Figure I) are sampled annually. However. due to an obstruction in the wel l. the operator was not able to sample or measure the tota l depth of the deeper monitoring well (LCW-01 ).
The results or the fie ld and laboratory analyses of groundwater sampled from DW-02 (Table 1 and Attachments A and B) indicate pcPAH concentrations were less than method detection limits. As shown in Table I. these data are consistent with the previous 16 years of data. Although the deeper well could not be sampled, the results of the analysis of groundwater from the shallo~ver 'vVell (DW -02) were less than the detection I irnit. Therefore. there is no indication
006984
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Report of Findings 20 f 2 Deep .\foniloring /Fell Sampling and Analysis Sowh Cavalcade 5;upe1jimd Site. Houslon. Texas Page 2 Februwr 27. 2nt 3
of potential impact to the deeper aquifers because if any migration existed. constituents would be detected fi rst in \Ve il DW-02.
If you have questions. fee l free to ca ll Angela Gate hie ofFTS at ( 4 12) 428-941 1.
Sincerely.
Field & Technical Services
~J~ Angela Gatch ie Project Scientist
Attachments
cc: Mike Bollinger- Beazer (.pdt) Jim Zubrow- Key (.pdt) Fay Duke-TCEQ (Report)
Enclosures:
Copy of Letter Report and .pdf submittal
FTS
006985
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Report Q( Findings lnJ 1 Deep .lfoniforing Well Sampling anti .-lna(l'Sis Svwh Camlcade Supe1jimd Sile. Hous/on. Texas
TABLE
Report of Findings 20 12 Deep Monitoring Well Sampling and Analysis South Cavalcade Superfund Site Houston. Texas
F"T S
006986
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Samplo Location: DW-02 LCW-01 OW-02 Sample Date: Mar-95 Mar-95 Apr-96
I METHOD I BENZO(AlPYRENE UGIL 002 u 002 u 002 u BENZO(A)ANTHRACENE UGIL 002 u 002 u 0.02 u BENZO(B)FLUORANTHENE UG/L 0 02 u 0.02 u 0.02 u BENZO(K)FLUORANTHENE UG/L 0 02 u 0.02 u 002 u CHRYSENE UG/L 0 15 u 0.15 u 015 u DIBENZOiA.H)ANTHRACENE UG/L 0 03 u 0.03 u 0.03 u INDEN0(1 ,2,3-CD)PYRENE UGIL 0.05 u 0.05 u 0.05 u
Notes: U indicates compound was analyzed lor. bul not detected In 1998, neuher well LCW-01 nor well DW-02 were sampled
Table 1 South Cavalcade
Analytical Summary 1995 -2012 Annual Deep Well Groundwater Sampling
South Cavalcade, Texas
LCW-01 OW-02 DW-02 OW-02 DW-02 DW-02 DW-02 DW-02 Apr-96 Mar-97 Sep-S9 Mar-00 Mar-01 Dec-02 Dec-03 Dec-04
0.02 u 0.054 u 0.02 UJ 0.02 u 0.22 u 020 u 0.19 u 019 u 0.02 u 0.02 u 0.02 u 0.02 u 0,22 u 0.20 u 019 u 019 u 0.02 u 0.053 u 0.02 UJ 0 02 u 0.22 u 020 u 019 u 0 19 u 0.02 u 0.046 u 0.02 u 0.02 u 0.22 u 0.20 u 0 19 u 0 19 u 0.20 u 0.150 u 0.15 u 0.15 u 2.20 u 0 20 u 019 u 0,19 u 0.03 u 0.03 u 0.03 u 0.03 u 0.22 u 0.20 u 019 u 0.19 u 0.05 u 0.05 u 0.05 u 0.05 u 0.22 u 0.20 u 0 19 u 0.19 u
FTS
DW-02 DW-02 DW-02 DW-02 DW-02 DW-02 DW-02 DW-02 Dec-05 Dec-06 Dec-07 Dec-08 Dec-09 Dec-10 Apr-11 May-12
019 u 020 u 020 u 019 u 020U 020U 019 u 019 u 019 u 020 u 020 u 019 u 020 u 0 20 u 019 u 0 19 u 019 u 0 20 u 020 u 0 19 u 0 20 u 0 20 u 0 19U 0 19 u 019 u 0 20 u 0 20 u 0 19 u 020 u 0 20 u 019 u 0 19 u 0.19 u 0.20 u 0 20 u 0 19 u 0.20 u 0.20 u 0.19 u 0 19 u 0.19 u 0.20 u 0 20 u 019 u 0.20 u 0.20 u 0.19 u 019 u 0.19 u 0.20 u 0 20 u 0 19 u 0.20 u 0 20 u 0.19 u 0 19 u
lol l
006987
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Report of Findings ?O!'J Deep .\loni10ring ll'el/ Sampling and Ana~I'Sis South ("(ll'a/cade Supet:ftmd Site. Houston. Texas
FIGURE
Site Location Map South Cavalcade Superfund Site Houston. Texas
FT S
006988
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• I
\ •·
l r r
\ I
I
DW-02
-$-
LCW-01
-$-
\ I
\ I
\ I I
I
\ I
\ I
I
\
LQCAllON Of fORMER WOOD TREAllNC AREA
N LEGEND
PROPERlY IIOIJNOAA'r
RAI.JER IIONI!llRJHG WEll. LOCATION
AREA OF LOCATION
BEAZER EAST, INC PITISBURGH, PENNSYLVANIA
SOliTH CAVALCADE HOUSTON, TEXAS
SrrE LOCATION MAP
FIELD ac TECHNICAl SERI/ICES, llC
200 THIRD AVENUE CARNEGIE, PA 15106
006989
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Report of Findings 2012 Deep .l!onitoring Well Sampling and Analysis South Cal'a!cade Superfimd Site. Houslon. Texas
ATTACHMENT A
Analytical Data Package
Report of Findings 20 12 Deep Monitoring Well Sampling and Analysis South Cavalcade Superfund Site Houston. Texas
006990
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·········· LINKS
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Test America THE LEADER IN ENVIRONMENTAL TESTING
ANALYTICAL REPORT TestAmerica Laboratones Inc TestAmerica Pittsburgh 301 Alpha Drive RIDC Park Pittsburgh, PA 15238 Tel: (412)963-7058
TestAmerica Job ID. 180-10681 -1 Client Project/Site: South Cavalcade
For Field & Technical Services LLC 200 Third Avenue Carnegie, Pennsylvania 15106
Attn: Ms. Angie Gatchie
~~ Authorized for release by: 512512012 9:07:21 AM
Veronica Bortot Project Manager II veronica [email protected]
This report has been electronically signed and authorized by the signatory. Electronic signature is intended to be the legally binding equivalent of a traditionally handwritten signature.
Results relate only to the items tested and the sample(s) as received by the laboratory.
D
006991
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Client: Field & Technical Services LLC Project/Site: South Cavalcade
Table of Contents
TestAmerica Job 10: 180-10661-1
Cover Page . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . 1 Table of Contents . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . 2 Case Narrative . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . 3 Definitions . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . 4 Certification Summary. . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . 5 Sample Summary . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . 6 Method Summary . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . 7 Client Sample Results . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . 8 QC Sample Results . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . 9 QC Association . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . 11 Chain of Custody . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . 12 Receipt Checklists. . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . 14
Page 2 of 14 TestAmenca Pittsburgh
5/25/2012
B
006992
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Client: Field & Technical Services LLC Project/Site: South Cavalcade
Job ID: 180-10681 -1
Laboratory: TestAmerica Pittsburgh
Narrative
Comments
No additional comments.
Receipt
Case Narrative
Job Nar rative 180-10681-1
TestAmerica Job 10 180-10681-1
The samples were received on 5111!2012 9:25AM; the samples arrived in good condition, properly preserved and, where required. on ice. The temperatures of the 2 coolers at receipt time were 1 .2° C and 3.8° C.
GC/MS Semi VOA
No analytical or quality issues were noted.
Organic Prep No analytical or quality issues were noted.
Page 3 of 14 TestAmerica Pittsburgh
5/25/2012
El
006993
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Defi nitions/Giossary Client: Field & Technical Services LLC Project/Site: South Cavalcade
Qualifiers
GCIMS Semi VOA
Qualifier
u
Glossary
Abbreviation
l)
%R
CNF
DL. RA. RE. IN
EDL
EPA
MDL
ML
NO
PQL
QC
RL
RPD
TEF
TEO
Qualifier Description
lndicatesihe -anaiyte -was anaiyzed fOrbut noicietected.-
These commonly used abbreviations may or may not be present in this report.
Percent Recovery
Contains no Free Liquid
Indicates a Dilution, Reana:ysis, R,e-extraction, or additional initial metals/anion analysis of the sample
Estimated Detection Limit
United States Environmental Protection Agency
Method Detection Limit
Minimum Level (Dioxin)
Not detected at the reporting limit {or MDL or EDL if shown)
Practical Quantitation Limit
Quality Control
Reporting Limit
Relative Percent Difference. a measure of the relative difference between two points
Toxicity Equivalent Factor (Dioxin)
Toxicity Equivalent Quotient (Dioxin)
Page 4 of 14
TestAmerica Job 10: 180-10681 -1
TestAmerica Pittsburgh 5/25/2012
II
006994
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Client: Field & Technical Services LLC Project/Site: South Cavalcade
Laboratory Authority
TestAmerlca Pltisburgh Arkansas CEQ
TestAmerica Pittsburgh California
TestAmer~ca Pittsburgh Connecticut
TestAmenca Pittsburgh Florida
TestAmenca Pittsburgh IllinoiS
TestAmertca Pittsburgh Kansas
TestAmenca Pittsburgh L·A·B
TestAmenca Pittsburgh Lou1siana
TestAmerica Pittsburgh New Hampshire
TestAmerlca Pitlsburgh New Jersey
TestAmerlca Pittsburgh New York
TestAmerica Pittsburgh North Carolina DENR
TestAmerica Pittsburgh Pennsylvania
TestAmerica Pittsburgh Pennsylvania
TestAmerica Pittsburgh South Carolina
TestAmerica Pittsburgh USDA
TestAmerica Pittsburgh USDA
TestAmenca Pittsburgh Utah
TestAmenca Pittsburgh Virginia
TestAmerica Pittsburgh West Virginia OEP
TestAmerica Pittsburgh 'Msconsln
Certification Summary
Program
State Program
NELAC
State Program
NELAC
NELAC
NELAC
OoOELAP
NELAC
NELAC
NELAC
NELAC
State Program
NELAC
State Program
State Program
Federal
Federal
NELAC
NELAC
State Program
State Program
EPA Region
6
5
7
6
3
3
8
3
3
5
TestAmerica Job 10: 180-10681 -1
Certification 10
88-0690
4224CA
PH-0688
E87t008
002602
E-10350
l2314
04041
203011
PAOOS
11182
434
02-00416
02-416
89014002
P330- 1 0-{)0 139
P-Soil-01
STLP
460 189
142
998027800
Accreditation may not be offered or required tor all methods and analytes reported In th1s package. Please contact your project manager for the laboratory's
current list of certdied methods and analytes.
Page 5 of 14 TestAmerica Pittsburgh
5/25/2012
006995
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Client Field & Technical Services LLC Project/Site: South Cavalcade
Lab Sam pie 10
18o:iasai-=-1
180-10681 -2
180-1068 1-3
Client Sample 10
0'1\102-051012
Dl!P-051012
DVV02-051012 FIELD BLANK
Sample Summary
Page 6 of 14
Matrix
Waler
Waler
Water
TestAmerica Job 10: 180-10681-1
Collected Received
0511011211 :10 0 511 1/1209:25
05/10/12 11 :10 0 5/11/12 09:25
05/10/1211 :10 05111/1209:25
TestAmerica Pittsburgh 5125/2012
006996
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Client: Field & Technical Services LLC Project/Site: South Cavalcade
Method Description
Method Summary
Method
8270C LL semivoialiie0;9aniC: compoundsbyGCMs - i:owlevels
Protocol References:
TestAmerica Job ID: 180-10681 -1
Protocol ·sws4s ·--
Laboratory
TAL PIT
SW846 ="Test Methods For Evaluating Solid Waste. Physical/Chemical Methods", Third Edition. November 1986 And Its Updates.
Laboratory References:
TAL PIT = TestAmerica Pittsburgh, 301 Alpha Drive. RIDC Park. Pittsburgh, PA 15238, TEL (412)963-7058
Page 7 of 14 TestAmerica Pittsburgh
5/25/2012
II
006997
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Client Sample Results Client: Field & Technical Services LLC
Project/Site: South Cavalcade
Client Sample ID: DW02-051012 Date Collected: 05/1 0/12 11 1 0
Date Received: 05/11 /12 09 25
Method: 8270C LL - Semlvolatile Organic Compounds by GCMS -Low Levels Analyte Result Qualifier RL MDL
8enzoJaJanit1racei16
Benzo[b]fluoranthene
Benzo[k]fluoranthene
Benzo[alpyrene
Chrysene
Di~enz(a. h)anthracene
lndeno[1 ,2.3-cd]pyrene
Surrogate
ra/Pile-i1;,T-ei14 Nitrobenzene-d5
2-F/uorobipheny/
Client Sample ID: DUP-051012 Date Collected 05/1 Of12 11.10
Date Received· 05/11112 09·25
0.19
0.19
0,19
0.19
0.19
0.19
0.19
%Recovery
83
78
77
u
u u u u u
u
Qualifier
0.19
0,19
0.19
0.19
0.19
0.19
0,19
Limits
10. 132
23.112
19 . 107
Method: 8270C LL- Semivolatile Organic Compounds by GCMS - Low Levels Analyte Result Qualifier RL MDL
Benzo[a]anthracene 0.21 u Benzo[b]fluoranthene 0.21 u Benzo[k]fluoranthene 0.21 u Benzo[a]pyrene 0.21 u Chrysene 0.21 u Oibenz(a.h)anthracene 0.21 u lndeno[1 .2,3-cd]pyrene 0.21 u
Surrogate %Recovery Qualifier
ieiP"henyr-d i4 99 Nilrobenzene-d5 85
2-F/uorobipheny! 81
Client Sample ID: DW02-051012 FIELD BLANK Date Collected 05/10/1211 10
Date Received: 05/11/12 09:25
0.21
0.21
0.21
0.21
0.21
0.21
0.21
Limits
10 - 132
23- 112
19 . 107
M ethod 8270C LL - Semivolatile Organic Compounds by GCMS -Low Levels Analyte Result Qual ifier RL
Benzo[a]anthracene 0.20 u o.2o Benzo[b]fluoranlhene 0.20 u 0.20 Benzo[k]fiuorant.,ene 0.20 u 0.20 Benzo[a]pyrene 0.20 u 0.20 Chrysene 0.20 u 0.20 Oibenz(a.h)anthracene 0.20 u 0.20 lndeno[1.2,3-cdjpyrene 0.20 u 0.20
Surrogate %Recovery Qualifier Limits
rerphenyl-d14 101 10 . 132
Nitrobenzene-d5 92 23 - 112
2-Fiuorobiphenyl 87 19 . 107
Page 8 of 14
MDL
Unit D
ug/L
ug/L
ug/L
ug/L
ugiL
ugll
ugll
Unit D
ugll
ug/L
ug/L
ug/L
ug/l
ug/L
ug/L
Unit D
ug/L
ug/L
ug/L
ugll
ug/L
ugiL
ug/L
TestAmerica Job ID: 180-1 0681-1
Lab Sample 10: 180-10681-1 Matrix Water
Prepared Analyzed 011 Fac
osh?i12 o8 22 05123/1217:12
05117112 08:22 05123112 17:12
05/17/12 08:22 0512311217: 12
05117/12 08; 22 05123112 17:12
05/17/12 08:22 05/23/121 7:12
05117/12 08:22 05123/12 17:12
05/17/12 08:22 05123/12 17:12
Prepared Analyzed Di/Fac
05117112 08:22 ii5123!T2 ii. i2 1 05117112 08:22 05123/12 17: 12
05117112 08.22 05123/12 17.·12
Lab Sample ID 180-10681-2 Matrix· Water
Prepared Analyzed Oil Fac
05117112" 08 22 05123112 18:26
05117112 08:22 05/23112 18:26
0511 7112 08:22 05/23,112 18:26
05117112 08:22 05/23112 18:26
05117112 08:22 05123112 18:26
05/17/12 08:22 05123112 18:26
05/17/12 08:22 05123/12 18:26
Prepared Analyzed Di/Fac ·· ··-·-·-····--··-··-··-·--·-···--
05123/12 18:26 05117112 08:22
05117/12 08:22 05/23/12 18:26
05117112 08.·22 0512311218.26
Lab Sample 10: 180-10681-3 Matrix Water
Prepared
osi1"7ii2 os22 05/17/12 08:22
05/17/12 08:22
05/17/12 08:22
05117112 08:22
05117/12 08:22
05117/12 08 22
Prepared
05117112 08:22
05117112 08.·22
05117112 08:22
Analyzed Oil Fac
osi2-:lh2·i-s:si 05/23/121851
05123/12 1 8:51
05/23112 18:51
05/23,112 1 8:51
05123112 18:51
05123/12 18;51
Analyzed DiiFac
05123/12 18:51
05123112 18:51
05123/12 18:51
TestAmerica Pittsburgh 5/25/2012
I
006998
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Client: Field & Technical Services LLC Project/Site: South Cavalcade
QC Sample Results
Method: 8270C LL - Sem•volatile Organic Compounds by GCMS - Low Levels
Lab Sample 10: MB 180-36296/1-A Matrix: Water
Analysis Batch: 36988 MB MB
Ana lyle Resull Qualifier RL MDL Unit
Benzo[ai anthracene-- ··- 0.20 u 0.20 ug/L Benzo[bjftuoranthene 020 u 0.20 ugiL Benzo[k]fluoranthene 0.20 u 0.20 ug/L Benzo[ajpyrene 0.20 u 0.20 ug/L Chrysene 0.20 u 0.20 ug/L Dibenz(a,h)anthracene 0.20 u 0.20 ugiL lndeno[1.2, 3-cd]pyrene 0.20 u 0.20 ug/L
MB MB
Surrogate %Recove1)' Qualifier Limils
rerpi>enyl-d14 ················---
83 10 . 132
Nitrobenzene-d5 84 23 . 112
2-Fiuorobiphenyl 84 19.107
Lab Sample 10: LCS 180-36296/2-A
Matrix: Water Analysis Batch: 36988
Spike LCS LCS
Analyte Added Result Qualifier Unit - - ·--·····-·-···-Benzo[ajanthracene 20.0 14.1 ugiL
Benzo[b]fluoranthene 20.0 14.2 ug/L
Benzo[k]fluoranthene 20.0 12.6 ug/L
Benzo[a]pyrene 20.0 14.1 ug/L
Chrysene 20.0 14.2 ugiL
Dibenz(a,h)anthracene 20.0 13.6 ug/L
lndeno(t ,2.3-cdjpyrene 20.0 14.3 ug/L
LCS LCS
Surrogate %Recovery Qualifier Limits ··-··- · -·-··-·-
Terphenyl-d14 82 10.132
Nitrobenzene-d5 78 23 . 112
2-Fiuorobiphenyl 78 19 .107
Lab Sample 10: 180-10681-1 MS
Matnx: Water
Analysis Batch: 36988 Sample Sample Spike MS MS
Analyte Result Qualifier Added Result Qualifier Unit
Benzo(ajanthracene 0.19 u 19 2 13.• ug/L Benzo(b]fluoranthene 0.19 u 19.2 12.3 ug/L Benzo(k]Ouoranthene 0.19 u 19.2 10.9 ug/L Benzo[a]pyrene 0.19 u 19.2 12.3 ug/L Chrysene 0.19 u 19.2 12.0 UQIL Oibenz(a,h)anthracene 0.19 u 19.2 12.3 ugil lndeno(1 ,2.3-cdjpyrene 0.19 u 19.2 12.4 ugil
MS MS
Surrogate %Recovery Qualifier Limits
Terphenyi-d1 4 76 10 . 132 Nitrobenzene-d5 70 23 - 11 2
2-Fiuorobiphenyl 60 19 . 107
Page 9 of 14
Te
c
D Pre~
05117/1
05/17/1
0511711
05117/1
05/1711
0511711
05/1711
Pre1
05117/;
05/171;
05/17/;
ClientS
D
c
D
006999
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Client: Field & Technical Services LLC Project/Site: South Cavalcade
QC Sample Results TestAmerica Job 10: 180-10681-1
Method. 8270C LL • Semivolatile Organic Compounds by GCMS • Low Levels (Continued)
Lab Sample 10: 180-10681·1 MSD Matrix: Water Analysis Batch 36988
Sample Sample
Anaiyte Result Qualifier
eienzo[aJantii-fficene - -- -· ··-·-
0.19 u Benzo[b]fluoranthene 0.19 u Benzo[k]fiuoranthene 0.19 u Benzo[a]pyrene 0.19 u Chrysene 0.19 u Dibenz(a.h)anthracene 0.19 u lndeno[1 .2.3-cd]pyrene 0.19 u
MSD MSD
Surrogate %Recovery Qualifier
T erphen yl-di.4 ·-------- -----------
81
Nitrobenzene-ciS 72
2-F/uorobiphenyl 65
Spike MSD MSD
Added Result Qualifier Unit D
20.4 14.7 ug/L
20.4 13.0 ugll
20.4 12.8 ug/L
20.4 13.5 ugll
20.4 13.5 ug/L
20.4 13.7 ug/L
20.4 13.7 ug/L
Umits ---------···--
10. 132
23. 112
19 . 107
Page 10 of 14
Client Sample ID: DW02-051012
%Rec
72
64
63
66
66
67
67
Prep Type: Totai/NA Prep Batch: 36296
%Rec. RPD
Limits RPD Limit
36: 101 ........ 9
3s 29 - 98 5 46
28 - 107 17 31
26 - 108 40
37-99 12 42
19- 118 11 44
22- 115 10 54
TestAmerica Pittsburgh 5/25/2012
D
007000
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QC Association Summary Client: Field & Technical Services LLC ProjecVSite: South Cavalcade
GC/MS Semi VOA
Prep Batch: 36296
Lab Sample 10
180-10681-1
180-10681-1 MS
18Q-10681· 1 MSD
180-10681-2
180-10681-3
LCS 180-36296/2-A
MB 180-3629611-A
Analysis Batch: 36988
Lab Sample 10
180-10681·1
180· 10681· 1 MS
180-10681-1 MSO
180-10681·2
180-10681·3
LCS 180-3629612-A
MB 180-36296/1-A
Client Sample 10
owo2:osi ii12
OW02-051012
DW02-051012
DUP-051012
DW02-051012 FIELD BLANK
Lab Control Sample
Method Blank
Client Sample 10
owo2-0S1o12-
owo2-os1o12
DW02-Q51012
DUP-051012
OW02-051012 FIELD BLANK
Lab Control Sample
Method Blank
Prep Type
Totai/NA
Totai/NA
Totai/NA
Totai!NA
Totai/NA
Totai/NA
Totai/NA
Prep Type
Totai/NA
Total iNA
Total iNA
Totai/NA
Totai/NA
Totai/NA
Totai/NA
Page 11 of 14
Matrix
Water
Water
Water
Water
Water
Water
Water
Matrix
Water
Water
Water
Water
Water
Water
Water
TestAmerica Job ID: 180-10681-1
Method
3520C
3520C
3520C
3520C
3520C
3520C
3520C
Method 8276-CLL
8270C LL
8270C LL
8270C LL
8270C LL
8270C LL
8270C LL
Prep Batch
Prep Batch
36296
36296
36296
36296
36296
36296
36296
TestAmerica Pittsburgh 5/25/2012
007001
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Chain of
-
,-
..... 1_..._...~- .• ..,..._._. - aa....• - ......... fiT~~--
C:'Jain of Custody Recof"d Te?tAmerica
TAl~18 (1008)
0 M
Q) Cl
-
Login Sample Receipt Checklist
Client Field & Technical Services LLC
Login Number: 10681
List Number: 1
Creator : Ras, Erin F
Question
Radioactivity either was not measured or, if measured. is at or below background
The cooler's custody seal. if present, is intact.
The cooler or samples do not appear to have been compromised or tampered with.
Samples were received on Ice.
Cooler Temperature Is acceptable.
Cooler Temperature Is recorded.
COC is present.
COC is filled out in ink and legible.
COC is filled out with all pertinent information.
Is the Field Sampler's name present on COC?
There are no dlscrepancles between the sample IDs on the containers and theCOC
Samples are received within Holding Time.
S ample containers have legible tabels.
Containers are not broken or leaking.
Sample collection date/times are provided.
Appropriate sample containers are used.
Sample bottles are completely filled.
Sample Preservation Verified.
There is sufficient vol. for all requested analyses. Incl. any requested MS/MSDs
VOA sample vials do not have headspace or bubble is
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Report ojFindings :!Of] Deep Jlonitoring Well Sampling and Ana~vsis South Cavalcade Supe!:fimd Site. Houston. Texas
ATTACHMENT B Groundwater Sampling Report Form
Report of Findings 2012 Deep Monitoring Well Sampling and Anal South Cavalcade Superfund Site Houston, Texas
007005
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FTS
[wELL NO.: DW-02
GROUNDWATER SAMPLE COLLECTION RECORD
Time: Start: /0 t.ro Fiolsb: 11 10
1. WATER LEVEL DATA (meas urcd from top of well casing) CoMet:\ion Fat.tors (Gf) (e xcf·· f)
a. Total Casing Length: .j?? 1110 .!.-- J'D- 1>? QCSamplcs(uaml!, timc,date): OW 0 .J. - /15/J1$.0 Q.rfot;z 1/JO .$~-JI)~t~
/)tJ(J:K - os-10 ',;z, l}I"'· .. A< !liD Analytical Parameters Polynuclear Aromatic Hydrocarbons (8310) and :viet hods:
Comments: l,ist of PAll's- Benzo(a)anthrocene, Benzo(a)pyrenc, Benzo(b)flouranthene, Benzo(k)flourantbene,
Cl1rysene, Dibenz.o(a,h)anthruc::ene,lndeno( 1 ,2,3-cd)pyrene
u:1\uscrs\a"'dy !WUies\Copy ofGW sample coUcction 1-09 fonn ill5 07116/99
007006
ATTACHMENT A - Analytical Data PackageATTACHMENT B - Groundwater Sampling Report Form
barcodetext: 684748barcode: *684748*