[redacted] letter transmitting results of residential … · project: laboratory analysis . report...

Olin 3855 NORTH OCOEE STREET SUITE 200 CLEVELAND TN 37312

OFFICE (423) 336-4000 FAX (423) 336-4166

February 182009

Wilmington MA 01887

Re Residential Well Sampling Program

Dear

Please find enclosed the laboratory analysis report from the independent laboratory that analyzed the water sample collected in October 2008 from your home Also enclosed is a review by the consultant that has been retained to review all data that is related to human health that might be associated with the Olin facilities located at 51 Eames Street

As you can see from the report the only analytical results outside of the regulatory standards or guidelines are those for dissolved sodium The guideline for sodium was established so that people on a salt restricted diet would be aware of the sodium content of their water While concentrations of other parameters including NshyNitrosodimethylamine (NDMA) were detected they were all below regulatory standards or guidelines

Should there be any questions after you review this information you can call the facility at (978)658-6121 Inform them that you would like for me to call you and I will return your call

Sincerely

Steve Morrow Principal Environmental Specialist

cc Jim DiLorenzo USEP A Greg Erickson Town of Wilmington Board of Health

OLIN CORPORATION

REDACTED

MACTEC engineering and constructing a better tomorrow

February 112009

Mr Steve Morrow Olin Corporation PO Box 248 Lower River Road Charleston TN 37310

Subject Residential Well Sampling 51 Eames Street Facility

Dear Mr Morrow

Per your request MACTEC Engineering and Consulting has evaluated the chemical data for the water sample collected in October 2008 from the residence in Wilmington under Olins residential well sampling program was performed to confirm the suitability of drinking water at the residential property Chemical concentrations in the well water were compared to Massachusetts and federal drinking water standards and guidelines

This evaluation

Attached is a table summarizing well monitoring data for the residence The table lists all detected analytes and their associated concentrations The appropriate standard andor guideline for each parameter is provided for comparison

Results for all detected parameters were below available Massachusetts and federal drinking water standards and guidelines

The water testing results shown here indicate that the overall well water quality is consistent with available Massachusetts and federal drinking water standards and guidelines

If you have any questions about the evaluation or if you require additional information please feel free to contact Michael Murphy at (781) 245-6606

MACTEC Engineering and Consulting Inc 107 Audubon Rood Bldg 2 Suite 301 bull Wakefield IvA01880middot Phone 7812456606 Fox 7812465060 wwwmacteccom

REDACTED

~MACTEC

Sincerely

MACTEC Engineering and Consulting

for Peter Thompson MlM Project Manager with permission Sr Principal Environmental Scientist

Attachment

cc Project File [P P6107090016 - Olin Wilmington CSS 200910 Project Management Administration15 CorrespondenceI52 Letters RESUL TS _09 pdf]

20f2 MACTEC Engineering amp Consulting 107 Audubon Road

Wakefield MA 01880 (781) 245-6606

(781) 246-5060 (FAX)

REDACTED

SUMMARY OF PRIVATE RESIDENCE WELL MONITORING DATA 1

AND COMPARISON TO FEDERAL AND MASSACHUSETTS DRINKING WATER STANDARDSGUIDELINES

RESIDENCE

Sample Drinking Water Type of Parameter Results Units StandardGuideline StandardGuideline Volatiles None Detected Semi-Volatiles Bis(2-Ethylhexyl)phthalate 00018 J mgL 0006 MCL N-Nitrosodimethylamine Not Detected Metals Calcium Total 62 mgL NS NS Sodium Total 15 mgL 20 ORSG Ammonia Not Detected Anions Sulfate as S04 22 mgL 250 SMCL

Chloride 65 mgL 250 SMCL

Prepared byDate SEB 013009 Seurog Notes Checked byDate BJR 020209 iStrl-- NS - No standard or guideline available MCL - Federal and Massachusetts Maximum Contaminant Level - USEPA 2006 MassDEP 2008 SMCL - Federal and Massachusetts Secondary Maximum Contaminant Level - USEPA 2006 MassDEP 2008 ORSG - Massachusetts Drinking Water Guideline - MassDEP 200B

J - Value is estimated mgL - milligrams per liter

1Data were collected in October 200B

USEPA2006 2006 Edition of the Drinking Water Standards and Health Advisories EPA B22-R-06-013

Massachusetts Department of Environmental Protection (MassDEP) 200B Spring 2008 Standards and Guidelines for Contaminants in Massachusetts Drinking Waters

PIOllNIWiiminglonlPrivalel October 20081 OCT o8-T ABxisSheetl of 1

REDACTED

- 53 Southampton Road -148 Rangeway Road Westfield MA 01085 N Billerica MA 01862TestAmerico Chain of Custody Form (P) 413-572-4000 (P) 978-667-1400

(F) 413-572-3707 (F) 978-667-7871 THE LEADER IN ENVIRONMENTAL TESTING 884

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TestAmerico

ANALYTICAL REPORT

Job Number 360-19248lt

Job Description Laboratory Analysis

For Olin Corporation

3855 North Ocoee Street Suite 200

Cleveland TN 37312--4441

lttention Mr Steven Morrow

Designee for Becky C Mason

Project tv1anager II becky masontestamericainccom

1113i2008

-h (est resuits in thiE report meet all NELlP requirements for accrediled parameters hny excepjefs ) NEL)P reqLirerrierits Gre noted in this 1epo1 Pursuant to NELAP this report rnay not b~ reprc-ckJcpd t~XC(r in fl Iif r~j gt~middotit

wriien cpprovai from the laboratory 1t5tfVTleric8 VVestfielj Certifications and Approvals MADEP MA014 RDCH57 CTDFr~ O~94 1 DECiSC NH D~ 2539 ~=Ur FL E87912 TOX rltELfp NJ MA008 TOX NEtJlP NY 10843 NY DOH 10843

Field saTpiing is perbrrned under SOPs WEmiddotFlOmiddotQOi an WE-FLD-002

--~tAT(r-ca Vest7ield V-tslfieJd EXEtJ~e Parr 53 Southarnpi-)o Road -Icstncld hiP 01C3S

~e (413) 572-4000 F2X (42) 572~37D7 tr0YJ~sectlg3ricqjOGcDm

Page 1 of 425

REDACTED

CASE NARRATIVE

Client Olin Corporation

Project Laboratory Analysis

Report Number 360-19248-1

This case narrative is in the form of an exception report where only the anomalies related to this report method specific performance andlor QAQC issues are discussed If there are no issues to report this narrative will include a statement that documents that there are no relevant data issues as stipulated in the MCP reporting requirements

In order to facilitate report review a separate MCP Analytical Method Report Certification Form is included for each method requested

It should be noted that samples with elevated Reporting Limits (RLs) as a result of a dilution may not be able to satisfy MCP program reporting limits in some cases if the adjusted RL is greater than the applicable MCP standards or criterion to which the concentration is being compared Such increases in the RLs are an unavoidable but acceptable consequence of sample dilution that enables quantification of target analytes which exceed the calibration range

Calculations are performed before rounding to avoid round-off errors in calculated results

All holding times were met and proper preservation noted for the methods performed on these samples unless otherwise detailed in the individual sections below

The samples were received on 101082008 the samples arrived in good condition properly preserved and on ice The temperatures of the coolers at receipt were 28 14 and OsoC

Note All samples which require thermal preservation are considered acceptable if the arrival temperature is within 2C of the required temperature or method specified range For samples with a specified temperature of 4C samples with a temperature ranging from just above freezing temperature of water to 6C shall be acceptable Samples that are hand delivered immediately following collection may not meet these criteria however they will be deemed acceptable according to NELAC and MADEP standards if there is evidence that the chilling process has begun such as arrival on ice etc

MCP regulatory standard criteria were not specified for this report Therefore method reporting limits (RLs) were not assessed against any MCP standards as it may pertain to Question E on the Presumptive Certainty Certification Form (MADEP reference WSC-CAM-AN-09300S - WSCshyCAM Analytical Notes)

VOLATILE ORGANIC COMPOUNDS

Samples 360-19248-1 through 360-19248-7 were analyzed for volatile organic compounds in accordance with EPA Method 5242 The samples were analyzed on 1016200S

All QAQC procedures required to meet Presumptive Certainty for the specified analytical method were performed as per section B of the MADEP MCP analytical method report Certification form

All QC performance standards and recommendations which may affect Data Usability for this specific method were achieved

Page 5 of 425

REDACTED

General method information For purposes of Presumptive Certainty status MADEP stipulates that analytical methods EPA 5242 and SW846 8260B are equivalent Additionally TestAm~rica Westfield is required under QAlOC guidelines for the acquisition and reporting of analytical data to report only those compounds for which we hold MAOEP drinking water certification This compound list typically differs from the CAMs SW846 8260B list (EPA 5242 vs WSC CAM II-A)

The following reported methods are not listed in the MADEP Massachusetts Contingency Plan (MCP) Compendium of Analytical Methods (CAM) pursuant to the provisions of 310 CMR 400017(2)

EPA 5252

Samples 360-19248-1 through 360-19248-6 were analyzed for EPA 5252 in accordance with EPA method 5252 The samples were prepared on 10142008 and analyzed on 10152008 and 10172008

This analysis was performed at TestAmerica Savannah 5102 LaRoche Avenue Savannah GA 31404

All QC performance standards and recommendations for this specific method were achieved with the exception of

Simazine failed the criteria high for the ICV Recoveries were greater than 300 and less than 450 This analyte was not detected in any associated samples

Heptachlor epoxide failed the criteria high for the CCV This analyte was not detected in any associated samples

TOTAL METALS

Samples 360-19248-1 through 360-19248-6 were analyzed for total metals in accordance with EPA 2007 Rev 44 The samples were prepared and analyzed on 101092008


Chromium was detected in method blank MB 360-372492 at a level that was above the method detection limit but below the reporting limit The value should be considered an estimate and has been flagged J If the associated sample reported a result above the MOL andlor RL the result has been 8 flagged Refer to the QC report for details

NITRATENITRITE BY LACHAT

Sample 360-19248-6 was analyzed for NitratelNitrite by Lachat in accordance with method 10shy107 -04-1 The samples were analyzed on 10162008

All QC performance standards and recommendations for this specific method were achieved

AMMONIA

Samples 360-19248-1 through 360-19248-6 were analyzed for ammonia in accordance with LACHAT 10-107-06-1 The samples were prepared and analyzed on 10152008 and 10212008


Page 6 of 425

REDACTED

ANIONS

Samples 360-19248-1 through 360-19248-6 were analyzed for anions in accordance with EPA Method 3000 The samples were analyzed on 100912008 and 101142008

All OC performance standards and recommendations for this specific method were achieved

Samples 360-19248-1 through 360-19248-3(10X) 360-19248-5 and 360-19248-6(10X) required dilution prior to analysis The reporting limits have been adjusted accordingly Dilutions were due to high Chloride concentration

NITRITE BY COLORIMETRIC

Sample 360-19248-6 was analyzed for Nitrite by Colorimetric in accordance with SM 4500B The samples were analyzed on 101102008


This analysis was performed at TestAmerica West Sacramento 880 Riverside Parkway West Sacramento CA 95605

Refer to subcontract report for case narrative

This case narrative is available in Word format upon request

Page 7 of 425

REDACTED

METHOD SUMMARY


Description

Matrix Water

Volatile Organic Compounds (GCMS)

Semivolatile Organic Compounds (GCMS) Extraction of Semivolatile Compounds

Metals (ICP) Preparation Metals

Lachat - Nitrate-Nitrite

Lachat Ammonia Distiflation Ammonia

Anions Ion Chromatography


Nitrogen Nitrite

EPA 1625 Organic Compounds by Isotope Dilution GCMS

Lab References

TAL SAY = TestAmerica Savannah

TAL WFD = TestAmerica Westfield

TAL WSC =TestAmerica West Sacramento

Method References

EPA =US Environmental Protection Agency

Lab Location

TALWFD

TAL SAV TAL SAV

TAL WFD TAL WFD

TAL WFD

TAL WFD TAL WFD

TAL WFD

TAL WFD

TALWFD

TAL WSC

Job Number 360-19248-1

Method Preparation Method

EPA-OW 5242

EPA 5252 EPA 5252

EPA 2007 Rev 44 EPA 200

QuickChem 10-1 07-04-1-C

QuickChem 10-107-06-1-K DistillAmmonia

MCAWW3000

MCAWW3000

SM SM 4500 N02 B

EPA EPA

EPA-OW = Methods For The Determination Of Organic Compounds In Drinking Water EPAl6004-88039 December 1988 And Its Supplements

MCAWW =Methods For Chemical Analysis Of Water And Wastes EPA-6004-79-020 March 1983 And Subsequent Revisions

QuickChem =Lachat Instruments

SM =Standard Methods For The Examination Of Water And Wastewater

TestAmerica Westfield

Page 8 of 425

REDACTED

~~

TestAmerica

ANALYTICAL REPORT

Job Number 360~19248-1

Jeb Description Laboratory Analysis

For Olin Corpcration


Cleveland TN 37312-4441

ttention Mr Steven Morrow

~Y~kY-eft~~I_

Jcraquot~~


Droject Manager 11 beckyrnasontestnlericainccom

12052]08 Hevisicn 1

~middotre test results in ihis -fDcrt rneei ~ j imiddotmiddotmiddotjEL~P requlreTiGnt5 f)r ccredited p8ran1eters Any exceptions to NELAP requirements are cec in this [eot Pursusnt to tlELAP tris report may not be reproduced except in fuJi and with vrHten a~proai frorn ne laLgtef2kTY TesiAmerlca Viesmeld CerJi1c2Iions 2~C ApproV2is MACEY 1gt014 RDO57 CTDPH 0494 VI DECVVSD NH DES 2539 NELAP FL E87G2 TO)lt ~~ELAp ~J M008 lOX fELPP rN 0843 rlY DOH 10843

Field s3iTpling is

~ctal nurrber of pages in this report if10 TestAmeri~L~bortorics Inc

J6st~rnerica V1festfield Ve~0e~d EX~~ut9 ltJrK 53 Soutn2npor Eoce iesfsic 4 01DC5

Tel (413) 572-4000 Fax (413) 572-3707 -middotmiddottdmiddot tssta~prcajnc fQlJJ

REDACTED

REVISION CASE NARRATIVE




This revision provides the requested additional data and also corrects the Volatile Organic Compounds and EPA 5252 portions of the narrative

This case narrative is in the form of an exception report where only the anomalies related to this report method specific performance andlor QAfQC issues are discussed If there are no issues to report this narrative will include a statement that documents that there are no relevant data issues as stipulated in the MCP reporting requirements

__----____ _____ In order to facilitate report review a separate MCP Analytical Method Report Certification Formjs___________ incluciecrtor eacn methoa requestea - -



AWholcHngtimes were meCand proper preservation noted for the methods performed on these samples unless otherwise detailed in the individual sections below

The samples were received on 10082008 the samples arrived in good condition properly preserved and on ice The temperatures of the coolers at receipt were 28 14 and 08DC


Mep regulatory standard criteria were not specified for this report Therefore method reporting limits (RLs) were not assessed against any MCP standards as it may pertain to Question F on the Presumptive Certainty Certification Form (MADEP reference WSC-CAM-AN-093008 - WSCshyCAM Analytical Notes)


Samples 360-19248-1 through 360-19248-7 were analyzed for volatile organic compounds in accordance with EPA Method 5242 The samples were analyzed on 10162008

All QAQC procedures required to meet Presumptive Certainty for the specified analytical method

REDACTED

5

-- -------------------------

were performed as per section B of the MADEP MCP analytical method report Certification form_

All OC performance standards and recommendations which may affect Data Usability for this specific method were achieved with the exception of

The internal standard 14-Dichlorobenzene-d4 failed the criteria low for sample 360-19248-3 No target compounds were detected in this sample results would be biased high

General method information For purposes of Presumptive Certainty status MADEP stipulates that analytical methods EPA 5242 and SW846 8260B are equivalent Additionally TestAmerica Westfield is required under OAJOC guidelines for the acquisition and reporting of analytical data to report only those compounds for which we hold MADEP drinking water certification This compound list typically differs from the CAMs SW846 8260B list (EPA 5242 vs_ WSC CAM II-A)


EPA 5252 -----~- ---- -----shy

--~-----~----




TOTAL METALS

Samples 360-19248-1 through 360-19248-6 were analyzed for total metals in accordance with -----------------EPA 2007 Rev 44 The samples were prepared and analyzed 00-10092008-----------------middot--------------------------shy

All OC performance standards and recommendations for this specific method were achieved with the exception of

Chromium was detected in method blank MB 360-372492 at a level that was above the method detection limit but below the reporting limit The value should be considered an estimate and has been flagged J_ If the associated sample reported a result above the MOL andor RL the result has been B flagged Refer to the OC report for details


Sample 360-19248-6 was analyzed for NitrateNitrite by Lachat in accordance with method 10shy107-04-1_ The samples were analyzed on 10162008


AMMONIA

Samples 360-19248-1 through 360-19248-6 were analyzed for ammonia in accordance with LACHAT 10-107-06-1_ The samples were prepared and analyzed on 10152008 and 10212008


REDACTED

ANIONS



Samples 360-19248-1 through 360-19248-3(1 OX) 360-19248-5 and 360-19248-6(10X) required dilution prior to analysis The reporting limits have been adjusted accordingly Dilutions were due to high Chloride concentration




NOMA ----__--------_ _----- -------~--------------------~ -------------------------~--------- ------------------~--

-- _-- __-- - - - - _- shyThis analysis was performed at TestAmerica West Sacramento 880 Riverside Parkway West Sacramento CA 95605



REDACTED

7

ANALYTICAL REPORT

Job tum~8r 360-19248-1

Fe) 0in CQmor8h~J

JR55 North OrnAA StrAR

Suite 200 Clevelend Ti 37) 12-44L 1

tUenticn tvli Steven 1010

8Acky C tvlClson Project f1anager 1

beckymason(cDtestamer C6i nccern 1212008

T- test results in this report meet 11i1 I~EL~P flIlrUWfimiddotj )i OVj lenimiddotr gt1V xpl()fIiO NFl P (equ~rernents are notedn thrs reurop8rt PUf3en to tmiddot~El)rJ hjs r(r-middot-middotmiddotY~ fr ~01 (~_middotpr-middotlt~ 1~middot~~-l Cyccpt in ull rJn~ vdr writen approval from ihe laboratory TrslflI)0rim WeHield Cerilic31iono-md PI0o10 vll)F Lmiddot1ltr1middotj f-ltIUUd___ (~ U~d (HSmiddotl j UECVvSD Wi Ul3 2529 NELAP FL EB7912 Tex NELAP NJ icACCE --0gt IltELAP ~y -13 i-jmiddot Ce--i 43

TeuroS1~nH~ric~ LnhortltorjR~1 rH~

T~stfn~erca VifesiHeld loVEStie-d Et~cL1Hv~ Par~~l )J S)u1hamp- J~~C~ -middotstpoundlj J~ ort~~

REDACTED

Mr Steven Morrow Olin Corporation 3855 North Ocoee Street Suite 200 Cleveland TN 37312-4441

Client Sample 10 OC-M24L72A Lab Sample 10 360-19248-6

Analyte

Method 5252 Prep Method 5252 Alachlor Atrazine Benzo[ a ]pyrene Bis(2-ethylhexyl) phthalate Di(2-ethylhexyl)adipate Heptachlor Heptachlor epoxide Endrin Hexachlorobenzene Hexachlorocyclopentadiene gamma-BHC (Lindane) Methoxychlor Simazine

Surrogate T riphenylphosphate 2-Nitro-m-xylene Perylene-d12

Method 2007 Rev 44 Prep Method 200 Calcium Chromium NO Sodium

ResultQualifier

ND ND ND 1S J ND ND ND Ur ND ND NO NO NO NO

104 109 95

62000 -tr-5-7 (tr

15000

Date Sampled Date Received

Client Matrix

Unit MDL

Date Analyzed Date Prepared

ugfL 0061 ugL 0044 ugL 0026 ugL 051 ugL 051 ugL 0039 ugL 0093 ugL 012 ugL 0033 ugL 0057 ugL 0070 ugL 010 ugL 007S


ugL 47 ugL 03S ugL 120


1010S200S 0905

1010S200S 1500 Potable

RL Dilution

1015200S 1S16 1014200S OS56

020 10 020 10 020 10 20 10 15 10 020 10 020 10 051 10 020 10 20 10 020 10 051 10 051 10

Acceptance Limits 70 - 130 70 - 130 70 - 130

10109200S 1S40 10092008 1150

400 10 50 10 2000 10

Page 27 of 425

REDACTED

Mr Steven Morrow Job Number 360-19248-1 Olin Corporation 3855 North Ocoee Street Suite 200 Cleveland TN 37312-4441

Date Sampled 10082008 0905 Client Sample ID OC-M24L72A Date Received 10082008 1500Lab Sample ID 360-19248-6 Client Matrix Potable

Analyte ResultQualifier Unit RL RL Dilution

Method 5242 Date Analyzed 10162008 1930

1112-Tetrachloroethane NO ugL 050 050 10

1 1 i-Trichloroethane NO ugL 050 050 10

1122-Tetrachloroethane ND ugL 050 050 10

112-Trichloroethane NO ugL 050 050 10

11-Dichloroethane NO ugL 050 050 10

11-Dichloroethene ND ugL 050 050 10

1 1-Dichloropropene NO ugL 050 050 10

123-T richlorobenzene ND ugL 050 050 10

123-T richloropropane ND ugL 050 050 10

124-Trichlorobenzene NO ugL 050 050 10

124-Trimethylbenzene ND ugL 050 050 10

12-Dibromo-3-Chloropropane NO ugL 050 050 10

12-Dichlorobenzene NO ugL 050 050 10

12-Dichloroethane ND ugL 050 050 10

12-Dichloropropane ND ugL 050 050 10

135-T rimethylbenzene ND ugL 050 050 10

13-Dichlorobenzene ND ugL 050 050 10




2-Chlorotoluene ND ugL 050 050 10

4-Chlorotoluene ND 050ugL 050 10

4-lsopropyltoluene ND ugL 050 050 10

Benzene NO ugL 050 050 10

Bromobenzene NO ugL 050 050 10 10Bromoform ND ugL 050 050

Bromomethane ND ugL 050 050 10

Carbon tetrachloride ND ugL 050 050 10

Chlorobenzene ND ugL 050 050 10

Chlorobromomethane ND ugL 050 050 10

Chlorodibromomethane ND ugL 050 050 10

Chloroethane ND ugL 050 050 10

Chloroform ND ugL 050 050 10

ugL 050Chloromethane ND 050 10

cis-12-Dichloroethene ND ugL 050 050 10

cis-13-Dichloropropene ND ugL 050 050 10

Dibromomethane ND ugfL 050 050 10

Dichlorobromomethane ND ugL 050 050 10

Dichlorodifiuoromethane NO ugfL 050 050 10

Ethylbenzene ND ugfL 050 050 10

Page 28 of 425 C (L~6~

REDACTED

Mr Steven Morrov Olin Corporation 3855 North Oooee Street Suite 200 Cleveland TN 37312-4441

Client Sample ID OC-M24L72A Lab Sample ID 360middot19248middot6

Analyte

Ethylene Dibromide Hexechlorobutadiene Isopropybenzene mmiddotXylere amp p-Xylene Methyl lert-butyl ether Methylene Chloride n-Butylbenzene Nmiddot Propylbenzere Naphthalene omiddotXylene sec-Butylbenzene Styrene tertmiddotButylbenzene Tetrachlofoethene Toluene trans-12-oichloroethene irans- 3-oichloropropene

Trichioroethene Trichorofiuoromethane Vinyl cJllorioe 244-Trimetryl-2-pentene 244-T rimetrylmiddot1-pentene

Surrogate 4-8romofluOfJbenzene Oibromoiluoramethane

Method 10middot107-04middot1-C Nitrate as N

Method 10-107-06-1-K Prep Method DistillAmrronia Ammonia

Method 3000 Sulfate

Method 3000 Chloride

Method SM 4500 NOZ B Nitrite as N

Cale Sampled Cale ReCBived Client tl1atrix

ResultiQualifier Unit RL

NO ugJL 050 NO ugL 050 NO ugL 050 NO ugL 10 NO ugL 050 NO uglL 050 NO ugfL 050 NO ugL 050 ND ugiL 050 NO uglL 050 NO ugL 050 NO ugL 050 NO ugJL 050 ND ugiL 050 NO ugL 050 NO ugfL 050 NO ugl 050 NO ugfL 050 NO ugL 050 NO ugfL 050 NO ugL 10~r ND r ~ uofL 10l

i 1)oO

middotif92 I]

103 Cl0

Dale Analyzed NO nngfL 0050

DatE Anayzed Date Prepared

ND rrgL 010

DatE- Analyzed 22 rngl 20

Oaieuro Analyzed 65 rngiL 10

Date Analyzed ND nngL 0010


10082008 0905 10082008 1500 Potbie

RL Dilution

050 l0 050 10 050 10 10 10 050 i 0 050 10 050 10 050 10 050 10 050 10 050 LO 050 10 050 10 050 10 050 10 050 10 050 10 050 10 050 10 050 iO

10 10 10 10

ACCBptance Umits

eo - 120 80 - 120

10162008 1125 0050 0

10212008 1548 10212008 1335

010 C

10142008 1809 20 0

101142008 1824 10 0

10102008 0614 oJ10 0

REDACTED

DATA REPORTING QUALIFIERS


Lab Section Qualifier

GCMS VOA

GCMS Semi VOA

J

Metals

B

J


Description

LCS or LCSO exceeds the control limits

Result is less than the RL but greater than or equal to the MOL and the concentration is an approximate value

Compound was found in the blank and sample



REDACTED

~

~~

~stAmerica THl LEADER IN ENVIRONMENTAL TESTING

November 12 2008

TGstAmerica Project Number G8J100200 POContract 360-19248

Becky Mason T eSJmerica Westfield 53 Southampton Road Westfied MA 01085

Dear Ms Mason

This report contains the analytical results for the samples received under chain of custody by TestAmerica on October 10 2008 These samples are associated with your 360-19248 project

The test results in this report meet all NELAC requirements for parameters that accreditation is required or available Any exceptions to NELAC requirements are noted in the case narrative The case narrative is an integral part of this report

If you have any questions please feel free to call me at (916) 374-4384

Sincerely

Karen Dahl Project Manager

880 Riverside Parkway West Sacramento CA 95605 teI9163735600 fax 9163721059 wwwtestamericainccom GO 4 G3J100200 TestAmerica west Sacramento (916) 373 - 5600 1of367

REDACTED

Case Narrative

TestAmerica West Sacramento Project Number G8J100200

WATER 1625M NOMA Sample(s) 1 2 34 56 As discussed the associated laboratory control sample had a low recovery (70) The samples were re-extracted outside recommended holding times for confirmation Both sets of results for these samples have been reported

Sample(s) 1 2 34 5 6 The laboratory control samples (associated with the re-extraction) had low internal standard recoveries (23 amp20) Generally data quality is not considered affected if the internal standard signal-to-noise ratio is greater than 10 1 which is achieved for all internal standards in the laboratory control samples There should be no impact on the data

There were no other anomalies associated with this project

Gamp]100200 TestAmerica West Sacramento (916) 373 -SSOO 30t367

REDACTED

606

__

Lot-Sample bullbullbull Date sampled Prep Date Prep Batch Dilution Factor

PARAMETER

TestAmerica Westf~eld

Client Sample In OC-M24L72A (360-19248-6)

Trace Level Organic Compounds

G8JI00200-006 100808 101408 8289284 1

N-Nitrosodimethylamine

INTERNAL STANDARD~~S____________ N-Nitrosodimethylamine-d6

Work Order If bullbullbull KOK3JIAA Matrix WATER Date Received 101008 Analysis Date 103008

DETECTION RESULT LIMIT UNITS METHOD ND 20 ngL CFR136A 1625 Modi

PERCENT RECOVERY RECOVERY LIMITS 70 (25 - 150)

Page 75 of 425

8J100200 T~tAmerfca West Sactamento (916) 373 - 56DO 20 of 3S7

REDACTED

barcodetext SDMS DocID 485041

barcode 485041

MACTEC engineering and constructing a better tomorrow

February 112009

Mr Steve Morrow Olin Corporation PO Box 248 Lower River Road Charleston TN 37310

Subject Residential Well Sampling 51 Eames Street Facility

Dear Mr Morrow

Per your request MACTEC Engineering and Consulting has evaluated the chemical data for the water sample collected in October 2008 from the residence in Wilmington under Olins residential well sampling program was performed to confirm the suitability of drinking water at the residential property Chemical concentrations in the well water were compared to Massachusetts and federal drinking water standards and guidelines

This evaluation

Attached is a table summarizing well monitoring data for the residence The table lists all detected analytes and their associated concentrations The appropriate standard andor guideline for each parameter is provided for comparison

Results for all detected parameters were below available Massachusetts and federal drinking water standards and guidelines

The water testing results shown here indicate that the overall well water quality is consistent with available Massachusetts and federal drinking water standards and guidelines

If you have any questions about the evaluation or if you require additional information please feel free to contact Michael Murphy at (781) 245-6606

MACTEC Engineering and Consulting Inc 107 Audubon Rood Bldg 2 Suite 301 bull Wakefield IvA01880middot Phone 7812456606 Fox 7812465060 wwwmacteccom

REDACTED

~MACTEC

Sincerely



Attachment



Wakefield MA 01880 (781) 245-6606

(781) 246-5060 (FAX)

REDACTED



RESIDENCE








PIOllNIWiiminglonlPrivalel October 20081 OCT o8-T ABxisSheetl Page 1 of 1

REDACTED





Site 10 amp State












-

RED





RED

ACTED






545 Wlllr X

10f708 1725 Water X

x

-r




IDalaTimo

TestAmerico

ANALYTICAL REPORT









1113i2008






Page 1 of 425

REDACTED

CASE NARRATIVE
















Page 5 of 425

REDACTED



EPA 5252






TOTAL METALS







AMMONIA



Page 6 of 425

REDACTED

ANIONS










Page 7 of 425

REDACTED

METHOD SUMMARY


Description

Matrix Water








Nitrogen Nitrite


Lab References




Method References


Lab Location

TALWFD

TAL SAV TAL SAV

TAL WFD TAL WFD

TAL WFD

TAL WFD TAL WFD

TAL WFD

TAL WFD

TALWFD

TAL WSC



EPA-OW 5242

EPA 5252 EPA 5252

EPA 2007 Rev 44 EPA 200



MCAWW3000

MCAWW3000

SM SM 4500 N02 B

EPA EPA






Page 8 of 425

REDACTED

~~

TestAmerica

ANALYTICAL REPORT







~Y~kY-eft~~I_

Jcraquot~~



12052]08 Hevisicn 1


Field s3iTpling is




REDACTED

















REDACTED

5

-- -------------------------






EPA 5252 -----~- ---- -----shy

--~-----~----




TOTAL METALS







AMMONIA



REDACTED

ANIONS







NOMA ----__--------_ _----- -------~--------------------~ -------------------------~--------- ------------------~--




REDACTED

7

ANALYTICAL REPORT

Job tum~8r 360-19248-1

Fe) 0in CQmor8h~J









REDACTED



Analyte




ResultQualifier


104 109 95

62000 -tr-5-7 (tr

15000


Client Matrix

Unit MDL






1010S200S 0905


RL Dilution

1015200S 1S16 1014200S OS56

020 10 020 10 020 10 20 10 15 10 020 10 020 10 051 10 020 10 20 10 020 10 051 10 051 10


10109200S 1S40 10092008 1150

400 10 50 10 2000 10

7 of 425

REDACTED












































Page 28 of 425 C (L~6~

REDACTED



Analyte






Method 3000 Sulfate






i 1)oO

middotif92 I]

103 Cl0



ND rrgL 010





10082008 0905 10082008 1500 Potbie

RL Dilution

050 l0 050 10 050 10 10 10 050 i 0 050 10 050 10 050 10 050 10 050 10 050 LO 050 10 050 10 050 10 050 10 050 10 050 10 050 10 050 10 050 iO

10 10 10 10

ACCBptance Umits

eo - 120 80 - 120

10162008 1125 0050 0

10212008 1548 10212008 1335

010 C

10142008 1809 20 0

101142008 1824 10 0

10102008 0614 oJ10 0

REDACTED




GCMS VOA

GCMS Semi VOA

J

Metals

B

J


Description






REDACTED

~

~~


November 12 2008



Dear Ms Mason




Sincerely



REDACTED

Case Narrative






REDACTED

606

__


PARAMETER




G8JI00200-006 100808 101408 8289284 1






Page 75 of 425


REDACTED


barcode 485041

~MACTEC

Sincerely



Attachment



Wakefield MA 01880 (781) 245-6606

(781) 246-5060 (FAX)

REDACTED



RESIDENCE









REDACTED





Site 10 amp State












-

RED





RED

ACTED






545 Wlllr X

10f708 1725 Water X

x

-r




IDalaTimo

TestAmerico

ANALYTICAL REPORT









1113i2008






Page 1 of 425

REDACTED

CASE NARRATIVE
















Page 5 of 425

REDACTED



EPA 5252






TOTAL METALS







AMMONIA



Page 6 of 425

REDACTED

ANIONS










Page 7 of 425

REDACTED

METHOD SUMMARY


Description

Matrix Water








Nitrogen Nitrite


Lab References




Method References


Lab Location

TALWFD

TAL SAV TAL SAV

TAL WFD TAL WFD

TAL WFD

TAL WFD TAL WFD

TAL WFD

TAL WFD

TALWFD

TAL WSC



EPA-OW 5242

EPA 5252 EPA 5252

EPA 2007 Rev 44 EPA 200



MCAWW3000

MCAWW3000

SM SM 4500 N02 B

EPA EPA






Page 8 of 425

REDACTED

~~

TestAmerica

ANALYTICAL REPORT







~Y~kY-eft~~I_

Jcraquot~~



12052]08 Hevisicn 1


Field s3iTpling is




REDACTED

















REDACTED

5

-- -------------------------






EPA 5252 -----~- ---- -----shy

--~-----~----




TOTAL METALS







AMMONIA



REDACTED

ANIONS







NOMA ----__--------_ _----- -------~--------------------~ -------------------------~--------- ------------------~--




REDACTED

7

ANALYTICAL REPORT

Job tum~8r 360-19248-1

Fe) 0in CQmor8h~J









REDACTED



Analyte




ResultQualifier


104 109 95

62000 -tr-5-7 (tr

15000


Client Matrix

Unit MDL






1010S200S 0905


RL Dilution

1015200S 1S16 1014200S OS56

020 10 020 10 020 10 20 10 15 10 020 10 020 10 051 10 020 10 20 10 020 10 051 10 051 10


10109200S 1S40 10092008 1150

400 10 50 10 2000 10

Page 27 of 425

REDACTED












































Page 28 of 425 C (L~6~

REDACTED



Analyte






Method 3000 Sulfate






i 1)oO

middotif92 I]

103 Cl0



ND rrgL 010





10082008 0905 10082008 1500 Potbie

RL Dilution

050 l0 050 10 050 10 10 10 050 i 0 050 10 050 10 050 10 050 10 050 10 050 LO 050 10 050 10 050 10 050 10 050 10 050 10 050 10 050 10 050 iO

10 10 10 10

ACCBptance Umits

eo - 120 80 - 120

10162008 1125 0050 0

10212008 1548 10212008 1335

010 C

10142008 1809 20 0

101142008 1824 10 0

10102008 0614 oJ10 0

REDACTED




GCMS VOA

GCMS Semi VOA

J

Metals

B

J


Description






REDACTED

~

~~


November 12 2008



Dear Ms Mason




Sincerely



REDACTED

Case Narrative






REDACTED

606

__


PARAMETER




G8JI00200-006 100808 101408 8289284 1






Page 75 of 425


REDACTED


barcode 485041



RESIDENCE









REDACTED





Site 10 amp State












-

RED





RED

ACTED






545 Wlllr X

10f708 1725 Water X

x

-r




IDalaTimo

TestAmerico

ANALYTICAL REPORT









1113i2008






Page 1 of 425

REDACTED

CASE NARRATIVE
















Page 5 of 425

REDACTED



EPA 5252






TOTAL METALS







AMMONIA



Page 6 of 425

REDACTED

ANIONS










Page 7 of 425

REDACTED

METHOD SUMMARY


Description

Matrix Water








Nitrogen Nitrite


Lab References




Method References


Lab Location

TALWFD

TAL SAV TAL SAV

TAL WFD TAL WFD

TAL WFD

TAL WFD TAL WFD

TAL WFD

TAL WFD

TALWFD

TAL WSC



EPA-OW 5242

EPA 5252 EPA 5252

EPA 2007 Rev 44 EPA 200



MCAWW3000

MCAWW3000

SM SM 4500 N02 B

EPA EPA






Page 8 of 425

REDACTED

~~

TestAmerica

ANALYTICAL REPORT







~Y~kY-eft~~I_

Jcraquot~~



12052]08 Hevisicn 1


Field s3iTpling is




REDACTED

















REDACTED

5

-- -------------------------






EPA 5252 -----~- ---- -----shy

--~-----~----




TOTAL METALS







AMMONIA



REDACTED

ANIONS







NOMA ----__--------_ _----- -------~--------------------~ -------------------------~--------- ------------------~--




REDACTED

7

ANALYTICAL REPORT

Job tum~8r 360-19248-1

Fe) 0in CQmor8h~J









REDACTED



Analyte




ResultQualifier


104 109 95

62000 -tr-5-7 (tr

15000


Client Matrix

Unit MDL






1010S200S 0905


RL Dilution

1015200S 1S16 1014200S OS56

020 10 020 10 020 10 20 10 15 10 020 10 020 10 051 10 020 10 20 10 020 10 051 10 051 10


10109200S 1S40 10092008 1150

400 10 50 10 2000 10

Page 27 of 425

REDACTED












































Page 28 of 425 C (L~6~

REDACTED



Analyte






Method 3000 Sulfate






i 1)oO

middotif92 I]

103 Cl0



ND rrgL 010





10082008 0905 10082008 1500 Potbie

RL Dilution

050 l0 050 10 050 10 10 10 050 i 0 050 10 050 10 050 10 050 10 050 10 050 LO 050 10 050 10 050 10 050 10 050 10 050 10 050 10 050 10 050 iO

10 10 10 10

ACCBptance Umits

eo - 120 80 - 120

10162008 1125 0050 0

10212008 1548 10212008 1335

010 C

10142008 1809 20 0

101142008 1824 10 0

10102008 0614 oJ10 0

REDACTED




GCMS VOA

GCMS Semi VOA

J

Metals

B

J


Description






REDACTED

~

~~


November 12 2008



Dear Ms Mason




Sincerely



REDACTED

Case Narrative






REDACTED

606

__


PARAMETER




G8JI00200-006 100808 101408 8289284 1






Page 75 of 425


REDACTED


barcode 485041





Site 10 amp State












-

RED





RED

ACTED






545 Wlllr X

10f708 1725 Water X

x

-r




IDalaTimo

TestAmerico

ANALYTICAL REPORT









1113i2008






Page 1 of 425

REDACTED

CASE NARRATIVE
















of 425

REDACTED



EPA 5252






TOTAL METALS







AMMONIA



Page 6 of 425

REDACTED

ANIONS










Page 7 of 425

REDACTED

METHOD SUMMARY


Description

Matrix Water








Nitrogen Nitrite


Lab References




Method References


Lab Location

TALWFD

TAL SAV TAL SAV

TAL WFD TAL WFD

TAL WFD

TAL WFD TAL WFD

TAL WFD

TAL WFD

TALWFD

TAL WSC



EPA-OW 5242

EPA 5252 EPA 5252

EPA 2007 Rev 44 EPA 200



MCAWW3000

MCAWW3000

SM SM 4500 N02 B

EPA EPA






Page 8 of 425

REDACTED

~~

TestAmerica

ANALYTICAL REPORT







~Y~kY-eft~~I_

Jcraquot~~



12052]08 Hevisicn 1


Field s3iTpling is




REDACTED

















REDACTED

5

-- -------------------------






EPA 5252 -----~- ---- -----shy

--~-----~----




TOTAL METALS







AMMONIA



REDACTED

ANIONS







NOMA ----__--------_ _----- -------~--------------------~ -------------------------~--------- ------------------~--




REDACTED

7

ANALYTICAL REPORT

Job tum~8r 360-19248-1

Fe) 0in CQmor8h~J









REDACTED



Analyte




ResultQualifier


104 109 95

62000 -tr-5-7 (tr

15000


Client Matrix

Unit MDL






1010S200S 0905


RL Dilution

1015200S 1S16 1014200S OS56

020 10 020 10 020 10 20 10 15 10 020 10 020 10 051 10 020 10 20 10 020 10 051 10 051 10


10109200S 1S40 10092008 1150

400 10 50 10 2000 10

Page 27 of 425

REDACTED












































Page 28 of 425 C (L~6~

REDACTED



Analyte






Method 3000 Sulfate






i 1)oO

middotif92 I]

103 Cl0



ND rrgL 010





10082008 0905 10082008 1500 Potbie

RL Dilution

050 l0 050 10 050 10 10 10 050 i 0 050 10 050 10 050 10 050 10 050 10 050 LO 050 10 050 10 050 10 050 10 050 10 050 10 050 10 050 10 050 iO

10 10 10 10

ACCBptance Umits

eo - 120 80 - 120

10162008 1125 0050 0

10212008 1548 10212008 1335

010 C

10142008 1809 20 0

101142008 1824 10 0

10102008 0614 oJ10 0

REDACTED




GCMS VOA

GCMS Semi VOA

J

Metals

B

J


Description






REDACTED

~

~~


November 12 2008



Dear Ms Mason




Sincerely



REDACTED

Case Narrative






REDACTED

606

__


PARAMETER




G8JI00200-006 100808 101408 8289284 1






Page 75 of 425


REDACTED


barcode 485041



RED

ACTED






545 Wlllr X

10f708 1725 Water X

x

-r




IDalaTimo

TestAmerico

ANALYTICAL REPORT









1113i2008






Page 1 of 425

REDACTED

CASE NARRATIVE
















Page 5 of 425

REDACTED



EPA 5252






TOTAL METALS







AMMONIA



of 425

REDACTED

ANIONS










Page 7 of 425

REDACTED

METHOD SUMMARY


Description

Matrix Water








Nitrogen Nitrite


Lab References




Method References


Lab Location

TALWFD

TAL SAV TAL SAV

TAL WFD TAL WFD

TAL WFD

TAL WFD TAL WFD

TAL WFD

TAL WFD

TALWFD

TAL WSC



EPA-OW 5242

EPA 5252 EPA 5252

EPA 2007 Rev 44 EPA 200



MCAWW3000

MCAWW3000

SM SM 4500 N02 B

EPA EPA






Page 8 of 425

REDACTED

~~

TestAmerica

ANALYTICAL REPORT







~Y~kY-eft~~I_

Jcraquot~~



12052]08 Hevisicn 1


Field s3iTpling is




REDACTED

















REDACTED

5

-- -------------------------






EPA 5252 -----~- ---- -----shy

--~-----~----




TOTAL METALS







AMMONIA



REDACTED

ANIONS







NOMA ----__--------_ _----- -------~--------------------~ -------------------------~--------- ------------------~--




REDACTED

7

ANALYTICAL REPORT

Job tum~8r 360-19248-1

Fe) 0in CQmor8h~J









REDACTED



Analyte




ResultQualifier


104 109 95

62000 -tr-5-7 (tr

15000


Client Matrix

Unit MDL






1010S200S 0905


RL Dilution

1015200S 1S16 1014200S OS56

020 10 020 10 020 10 20 10 15 10 020 10 020 10 051 10 020 10 20 10 020 10 051 10 051 10


10109200S 1S40 10092008 1150

400 10 50 10 2000 10

Page 27 of 425

REDACTED












































Page 28 of 425 C (L~6~

REDACTED



Analyte






Method 3000 Sulfate






i 1)oO

middotif92 I]

103 Cl0



ND rrgL 010





10082008 0905 10082008 1500 Potbie

RL Dilution

050 l0 050 10 050 10 10 10 050 i 0 050 10 050 10 050 10 050 10 050 10 050 LO 050 10 050 10 050 10 050 10 050 10 050 10 050 10 050 10 050 iO

10 10 10 10

ACCBptance Umits

eo - 120 80 - 120

10162008 1125 0050 0

10212008 1548 10212008 1335

010 C

10142008 1809 20 0

101142008 1824 10 0

10102008 0614 oJ10 0

REDACTED




GCMS VOA

GCMS Semi VOA

J

Metals

B

J


Description






REDACTED

~

~~


November 12 2008



Dear Ms Mason




Sincerely



REDACTED

Case Narrative






REDACTED

606

__


PARAMETER




G8JI00200-006 100808 101408 8289284 1






Page 75 of 425


REDACTED


barcode 485041

TestAmerico

ANALYTICAL REPORT









1113i2008






Page 1 of 425

REDACTED

CASE NARRATIVE
















Page 5 of 425

REDACTED



EPA 5252






TOTAL METALS







AMMONIA



Page 6 of 425

REDACTED

ANIONS










of 425

REDACTED

METHOD SUMMARY


Description

Matrix Water








Nitrogen Nitrite


Lab References




Method References


Lab Location

TALWFD

TAL SAV TAL SAV

TAL WFD TAL WFD

TAL WFD

TAL WFD TAL WFD

TAL WFD

TAL WFD

TALWFD

TAL WSC



EPA-OW 5242

EPA 5252 EPA 5252

EPA 2007 Rev 44 EPA 200



MCAWW3000

MCAWW3000

SM SM 4500 N02 B

EPA EPA






Page 8 of 425

REDACTED

~~

TestAmerica

ANALYTICAL REPORT







~Y~kY-eft~~I_

Jcraquot~~



12052]08 Hevisicn 1


Field s3iTpling is




REDACTED

















REDACTED

5

-- -------------------------






EPA 5252 -----~- ---- -----shy

--~-----~----




TOTAL METALS







AMMONIA



REDACTED

ANIONS







NOMA ----__--------_ _----- -------~--------------------~ -------------------------~--------- ------------------~--




REDACTED

7

ANALYTICAL REPORT

Job tum~8r 360-19248-1

Fe) 0in CQmor8h~J









REDACTED



Analyte




ResultQualifier


104 109 95

62000 -tr-5-7 (tr

15000


Client Matrix

Unit MDL






1010S200S 0905


RL Dilution

1015200S 1S16 1014200S OS56

020 10 020 10 020 10 20 10 15 10 020 10 020 10 051 10 020 10 20 10 020 10 051 10 051 10


10109200S 1S40 10092008 1150

400 10 50 10 2000 10

Page 27 of 425

REDACTED












































Page 28 of 425 C (L~6~

REDACTED



Analyte






Method 3000 Sulfate






i 1)oO

middotif92 I]

103 Cl0



ND rrgL 010





10082008 0905 10082008 1500 Potbie

RL Dilution

050 l0 050 10 050 10 10 10 050 i 0 050 10 050 10 050 10 050 10 050 10 050 LO 050 10 050 10 050 10 050 10 050 10 050 10 050 10 050 10 050 iO

10 10 10 10

ACCBptance Umits

eo - 120 80 - 120

10162008 1125 0050 0

10212008 1548 10212008 1335

010 C

10142008 1809 20 0

101142008 1824 10 0

10102008 0614 oJ10 0

REDACTED




GCMS VOA

GCMS Semi VOA

J

Metals

B

J


Description






REDACTED

~

~~


November 12 2008



Dear Ms Mason




Sincerely



REDACTED

Case Narrative






REDACTED

606

__


PARAMETER




G8JI00200-006 100808 101408 8289284 1






Page 75 of 425


REDACTED


barcode 485041

CASE NARRATIVE
















Page 5 of 425

REDACTED



EPA 5252






TOTAL METALS







AMMONIA



Page 6 of 425

REDACTED

ANIONS










Page 7 of 425

REDACTED

METHOD SUMMARY


Description

Matrix Water








Nitrogen Nitrite


Lab References




Method References


Lab Location

TALWFD

TAL SAV TAL SAV

TAL WFD TAL WFD

TAL WFD

TAL WFD TAL WFD

TAL WFD

TAL WFD

TALWFD

TAL WSC



EPA-OW 5242

EPA 5252 EPA 5252

EPA 2007 Rev 44 EPA 200



MCAWW3000

MCAWW3000

SM SM 4500 N02 B

EPA EPA






of 425

REDACTED

~~

TestAmerica

ANALYTICAL REPORT







~Y~kY-eft~~I_

Jcraquot~~



12052]08 Hevisicn 1


Field s3iTpling is




REDACTED

















REDACTED

5

-- -------------------------






EPA 5252 -----~- ---- -----shy

--~-----~----




TOTAL METALS







AMMONIA



REDACTED

ANIONS







NOMA ----__--------_ _----- -------~--------------------~ -------------------------~--------- ------------------~--




REDACTED

7

ANALYTICAL REPORT

Job tum~8r 360-19248-1

Fe) 0in CQmor8h~J









REDACTED



Analyte




ResultQualifier


104 109 95

62000 -tr-5-7 (tr

15000


Client Matrix

Unit MDL






1010S200S 0905


RL Dilution

1015200S 1S16 1014200S OS56

020 10 020 10 020 10 20 10 15 10 020 10 020 10 051 10 020 10 20 10 020 10 051 10 051 10


10109200S 1S40 10092008 1150

400 10 50 10 2000 10

Page 27 of 425

REDACTED












































Page 28 of 425 C (L~6~

REDACTED



Analyte






Method 3000 Sulfate






i 1)oO

middotif92 I]

103 Cl0



ND rrgL 010





10082008 0905 10082008 1500 Potbie

RL Dilution

050 l0 050 10 050 10 10 10 050 i 0 050 10 050 10 050 10 050 10 050 10 050 LO 050 10 050 10 050 10 050 10 050 10 050 10 050 10 050 10 050 iO

10 10 10 10

ACCBptance Umits

eo - 120 80 - 120

10162008 1125 0050 0

10212008 1548 10212008 1335

010 C

10142008 1809 20 0

101142008 1824 10 0

10102008 0614 oJ10 0

REDACTED




GCMS VOA

GCMS Semi VOA

J

Metals

B

J


Description






REDACTED

~

~~


November 12 2008



Dear Ms Mason




Sincerely



REDACTED

Case Narrative






REDACTED

606

__


PARAMETER




G8JI00200-006 100808 101408 8289284 1






Page 75 of 425


REDACTED


barcode 485041



EPA 5252






TOTAL METALS







AMMONIA



Page 6 of 425

REDACTED

ANIONS










Page 7 of 425

REDACTED

METHOD SUMMARY


Description

Matrix Water








Nitrogen Nitrite


Lab References




Method References


Lab Location

TALWFD

TAL SAV TAL SAV

TAL WFD TAL WFD

TAL WFD

TAL WFD TAL WFD

TAL WFD

TAL WFD

TALWFD

TAL WSC



EPA-OW 5242

EPA 5252 EPA 5252

EPA 2007 Rev 44 EPA 200



MCAWW3000

MCAWW3000

SM SM 4500 N02 B

EPA EPA






Page 8 of 425

REDACTED

~~

TestAmerica

ANALYTICAL REPORT







~Y~kY-eft~~I_

Jcraquot~~



12052]08 Hevisicn 1


Field s3iTpling is




REDACTED

















REDACTED

5

-- -------------------------






EPA 5252 -----~- ---- -----shy

--~-----~----




TOTAL METALS







AMMONIA



REDACTED

ANIONS







NOMA ----__--------_ _----- -------~--------------------~ -------------------------~--------- ------------------~--




REDACTED

7

ANALYTICAL REPORT

Job tum~8r 360-19248-1

Fe) 0in CQmor8h~J









REDACTED



Analyte




ResultQualifier


104 109 95

62000 -tr-5-7 (tr

15000


Client Matrix

Unit MDL






1010S200S 0905


RL Dilution

1015200S 1S16 1014200S OS56

020 10 020 10 020 10 20 10 15 10 020 10 020 10 051 10 020 10 20 10 020 10 051 10 051 10


10109200S 1S40 10092008 1150

400 10 50 10 2000 10

Page 27 of 425

REDACTED












































Page 28 of 425 C (L~6~

REDACTED



Analyte






Method 3000 Sulfate






i 1)oO

middotif92 I]

103 Cl0



ND rrgL 010





10082008 0905 10082008 1500 Potbie

RL Dilution

050 l0 050 10 050 10 10 10 050 i 0 050 10 050 10 050 10 050 10 050 10 050 LO 050 10 050 10 050 10 050 10 050 10 050 10 050 10 050 10 050 iO

10 10 10 10

ACCBptance Umits

eo - 120 80 - 120

10162008 1125 0050 0

10212008 1548 10212008 1335

010 C

10142008 1809 20 0

101142008 1824 10 0

10102008 0614 oJ10 0

REDACTED




GCMS VOA

GCMS Semi VOA

J

Metals

B

J


Description






REDACTED

~

~~


November 12 2008



Dear Ms Mason




Sincerely



REDACTED

Case Narrative






REDACTED

606

__


PARAMETER




G8JI00200-006 100808 101408 8289284 1






Page 75 of 425


REDACTED


barcode 485041

ANIONS










Page 7 of 425

REDACTED

METHOD SUMMARY


Description

Matrix Water








Nitrogen Nitrite


Lab References




Method References


Lab Location

TALWFD

TAL SAV TAL SAV

TAL WFD TAL WFD

TAL WFD

TAL WFD TAL WFD

TAL WFD

TAL WFD

TALWFD

TAL WSC



EPA-OW 5242

EPA 5252 EPA 5252

EPA 2007 Rev 44 EPA 200



MCAWW3000

MCAWW3000

SM SM 4500 N02 B

EPA EPA






Page 8 of 425

REDACTED

~~

TestAmerica

ANALYTICAL REPORT







~Y~kY-eft~~I_

Jcraquot~~



12052]08 Hevisicn 1


Field s3iTpling is




REDACTED

















REDACTED

5

-- -------------------------






EPA 5252 -----~- ---- -----shy

--~-----~----




TOTAL METALS







AMMONIA



REDACTED

ANIONS







NOMA ----__--------_ _----- -------~--------------------~ -------------------------~--------- ------------------~--




REDACTED

7

ANALYTICAL REPORT

Job tum~8r 360-19248-1

Fe) 0in CQmor8h~J









REDACTED



Analyte




ResultQualifier


104 109 95

62000 -tr-5-7 (tr

15000


Client Matrix

Unit MDL






1010S200S 0905


RL Dilution

1015200S 1S16 1014200S OS56

020 10 020 10 020 10 20 10 15 10 020 10 020 10 051 10 020 10 20 10 020 10 051 10 051 10


10109200S 1S40 10092008 1150

400 10 50 10 2000 10

Page 27 of 425

REDACTED












































Page 28 of 425 C (L~6~

REDACTED



Analyte






Method 3000 Sulfate






i 1)oO

middotif92 I]

103 Cl0



ND rrgL 010





10082008 0905 10082008 1500 Potbie

RL Dilution

050 l0 050 10 050 10 10 10 050 i 0 050 10 050 10 050 10 050 10 050 10 050 LO 050 10 050 10 050 10 050 10 050 10 050 10 050 10 050 10 050 iO

10 10 10 10

ACCBptance Umits

eo - 120 80 - 120

10162008 1125 0050 0

10212008 1548 10212008 1335

010 C

10142008 1809 20 0

101142008 1824 10 0

10102008 0614 oJ10 0

REDACTED




GCMS VOA

GCMS Semi VOA

J

Metals

B

J


Description






REDACTED

~

~~


November 12 2008



Dear Ms Mason




Sincerely



REDACTED

Case Narrative






REDACTED

606

__


PARAMETER




G8JI00200-006 100808 101408 8289284 1






Page 75 of 425


REDACTED


barcode 485041

METHOD SUMMARY


Description

Matrix Water








Nitrogen Nitrite


Lab References




Method References


Lab Location

TALWFD

TAL SAV TAL SAV

TAL WFD TAL WFD

TAL WFD

TAL WFD TAL WFD

TAL WFD

TAL WFD

TALWFD

TAL WSC



EPA-OW 5242

EPA 5252 EPA 5252

EPA 2007 Rev 44 EPA 200



MCAWW3000

MCAWW3000

SM SM 4500 N02 B

EPA EPA






Page 8 of 425

REDACTED

~~

TestAmerica

ANALYTICAL REPORT







~Y~kY-eft~~I_

Jcraquot~~



12052]08 Hevisicn 1


Field s3iTpling is




REDACTED

















REDACTED

5

-- -------------------------






EPA 5252 -----~- ---- -----shy

--~-----~----




TOTAL METALS







AMMONIA



REDACTED

ANIONS







NOMA ----__--------_ _----- -------~--------------------~ -------------------------~--------- ------------------~--




REDACTED

7

ANALYTICAL REPORT

Job tum~8r 360-19248-1

Fe) 0in CQmor8h~J









REDACTED



Analyte




ResultQualifier


104 109 95

62000 -tr-5-7 (tr

15000


Client Matrix

Unit MDL






1010S200S 0905


RL Dilution

1015200S 1S16 1014200S OS56

020 10 020 10 020 10 20 10 15 10 020 10 020 10 051 10 020 10 20 10 020 10 051 10 051 10


10109200S 1S40 10092008 1150

400 10 50 10 2000 10

Page 27 of 425

REDACTED












































Page 28 of 425 C (L~6~

REDACTED



Analyte






Method 3000 Sulfate






i 1)oO

middotif92 I]

103 Cl0



ND rrgL 010





10082008 0905 10082008 1500 Potbie

RL Dilution

050 l0 050 10 050 10 10 10 050 i 0 050 10 050 10 050 10 050 10 050 10 050 LO 050 10 050 10 050 10 050 10 050 10 050 10 050 10 050 10 050 iO

10 10 10 10

ACCBptance Umits

eo - 120 80 - 120

10162008 1125 0050 0

10212008 1548 10212008 1335

010 C

10142008 1809 20 0

101142008 1824 10 0

10102008 0614 oJ10 0

REDACTED




GCMS VOA

GCMS Semi VOA

J

Metals

B

J


Description






REDACTED

~

~~


November 12 2008



Dear Ms Mason




Sincerely



REDACTED

Case Narrative






REDACTED

606

__


PARAMETER




G8JI00200-006 100808 101408 8289284 1






Page 75 of 425


REDACTED


barcode 485041

~~

TestAmerica

ANALYTICAL REPORT







~Y~kY-eft~~I_

Jcraquot~~



12052]08 Hevisicn 1


Field s3iTpling is




REDACTED

















REDACTED

5

-- -------------------------






EPA 5252 -----~- ---- -----shy

--~-----~----




TOTAL METALS







AMMONIA



REDACTED

ANIONS







NOMA ----__--------_ _----- -------~--------------------~ -------------------------~--------- ------------------~--




REDACTED

7

ANALYTICAL REPORT

Job tum~8r 360-19248-1

Fe) 0in CQmor8h~J









REDACTED



Analyte




ResultQualifier


104 109 95

62000 -tr-5-7 (tr

15000


Client Matrix

Unit MDL






1010S200S 0905


RL Dilution

1015200S 1S16 1014200S OS56

020 10 020 10 020 10 20 10 15 10 020 10 020 10 051 10 020 10 20 10 020 10 051 10 051 10


10109200S 1S40 10092008 1150

400 10 50 10 2000 10

Page 27 of 425

REDACTED












































Page 28 of 425 C (L~6~

REDACTED



Analyte






Method 3000 Sulfate






i 1)oO

middotif92 I]

103 Cl0



ND rrgL 010





10082008 0905 10082008 1500 Potbie

RL Dilution

050 l0 050 10 050 10 10 10 050 i 0 050 10 050 10 050 10 050 10 050 10 050 LO 050 10 050 10 050 10 050 10 050 10 050 10 050 10 050 10 050 iO

10 10 10 10

ACCBptance Umits

eo - 120 80 - 120

10162008 1125 0050 0

10212008 1548 10212008 1335

010 C

10142008 1809 20 0

101142008 1824 10 0

10102008 0614 oJ10 0

REDACTED




GCMS VOA

GCMS Semi VOA

J

Metals

B

J


Description






REDACTED

~

~~


November 12 2008



Dear Ms Mason




Sincerely



REDACTED

Case Narrative






REDACTED

606

__


PARAMETER




G8JI00200-006 100808 101408 8289284 1






Page 75 of 425


REDACTED


barcode 485041

















REDACTED

5

-- -------------------------






EPA 5252 -----~- ---- -----shy

--~-----~----




TOTAL METALS







AMMONIA



REDACTED

ANIONS







NOMA ----__--------_ _----- -------~--------------------~ -------------------------~--------- ------------------~--




REDACTED

7

ANALYTICAL REPORT

Job tum~8r 360-19248-1

Fe) 0in CQmor8h~J









REDACTED



Analyte




ResultQualifier


104 109 95

62000 -tr-5-7 (tr

15000


Client Matrix

Unit MDL






1010S200S 0905


RL Dilution

1015200S 1S16 1014200S OS56

020 10 020 10 020 10 20 10 15 10 020 10 020 10 051 10 020 10 20 10 020 10 051 10 051 10


10109200S 1S40 10092008 1150

400 10 50 10 2000 10

Page 27 of 425

REDACTED












































Page 28 of 425 C (L~6~

REDACTED



Analyte






Method 3000 Sulfate






i 1)oO

middotif92 I]

103 Cl0



ND rrgL 010





10082008 0905 10082008 1500 Potbie

RL Dilution

050 l0 050 10 050 10 10 10 050 i 0 050 10 050 10 050 10 050 10 050 10 050 LO 050 10 050 10 050 10 050 10 050 10 050 10 050 10 050 10 050 iO

10 10 10 10

ACCBptance Umits

eo - 120 80 - 120

10162008 1125 0050 0

10212008 1548 10212008 1335

010 C

10142008 1809 20 0

101142008 1824 10 0

10102008 0614 oJ10 0

REDACTED




GCMS VOA

GCMS Semi VOA

J

Metals

B

J


Description






REDACTED

~

~~


November 12 2008



Dear Ms Mason




Sincerely



REDACTED

Case Narrative






REDACTED

606

__


PARAMETER




G8JI00200-006 100808 101408 8289284 1






Page 75 of 425


REDACTED


barcode 485041

-- -------------------------






EPA 5252 -----~- ---- -----shy

--~-----~----




TOTAL METALS







AMMONIA



REDACTED

ANIONS







NOMA ----__--------_ _----- -------~--------------------~ -------------------------~--------- ------------------~--




REDACTED

7

ANALYTICAL REPORT

Job tum~8r 360-19248-1

Fe) 0in CQmor8h~J









REDACTED



Analyte




ResultQualifier


104 109 95

62000 -tr-5-7 (tr

15000


Client Matrix

Unit MDL






1010S200S 0905


RL Dilution

1015200S 1S16 1014200S OS56

020 10 020 10 020 10 20 10 15 10 020 10 020 10 051 10 020 10 20 10 020 10 051 10 051 10


10109200S 1S40 10092008 1150

400 10 50 10 2000 10

Page 27 of 425

REDACTED












































Page 28 of 425 C (L~6~

REDACTED



Analyte






Method 3000 Sulfate






i 1)oO

middotif92 I]

103 Cl0



ND rrgL 010





10082008 0905 10082008 1500 Potbie

RL Dilution

050 l0 050 10 050 10 10 10 050 i 0 050 10 050 10 050 10 050 10 050 10 050 LO 050 10 050 10 050 10 050 10 050 10 050 10 050 10 050 10 050 iO

10 10 10 10

ACCBptance Umits

eo - 120 80 - 120

10162008 1125 0050 0

10212008 1548 10212008 1335

010 C

10142008 1809 20 0

101142008 1824 10 0

10102008 0614 oJ10 0

REDACTED




GCMS VOA

GCMS Semi VOA

J

Metals

B

J


Description






REDACTED

~

~~


November 12 2008



Dear Ms Mason




Sincerely



REDACTED

Case Narrative






REDACTED

606

__


PARAMETER




G8JI00200-006 100808 101408 8289284 1






Page 75 of 425


REDACTED


barcode 485041

ANIONS







NOMA ----__--------_ _----- -------~--------------------~ -------------------------~--------- ------------------~--




REDACTED

7

ANALYTICAL REPORT

Job tum~8r 360-19248-1

Fe) 0in CQmor8h~J









REDACTED



Analyte




ResultQualifier


104 109 95

62000 -tr-5-7 (tr

15000


Client Matrix

Unit MDL






1010S200S 0905


RL Dilution

1015200S 1S16 1014200S OS56

020 10 020 10 020 10 20 10 15 10 020 10 020 10 051 10 020 10 20 10 020 10 051 10 051 10


10109200S 1S40 10092008 1150

400 10 50 10 2000 10

Page 27 of 425

REDACTED












































Page 28 of 425 C (L~6~

REDACTED



Analyte






Method 3000 Sulfate






i 1)oO

middotif92 I]

103 Cl0



ND rrgL 010





10082008 0905 10082008 1500 Potbie

RL Dilution

050 l0 050 10 050 10 10 10 050 i 0 050 10 050 10 050 10 050 10 050 10 050 LO 050 10 050 10 050 10 050 10 050 10 050 10 050 10 050 10 050 iO

10 10 10 10

ACCBptance Umits

eo - 120 80 - 120

10162008 1125 0050 0

10212008 1548 10212008 1335

010 C

10142008 1809 20 0

101142008 1824 10 0

10102008 0614 oJ10 0

REDACTED




GCMS VOA

GCMS Semi VOA

J

Metals

B

J


Description






REDACTED

~

~~


November 12 2008



Dear Ms Mason




Sincerely



REDACTED

Case Narrative






REDACTED

606

__


PARAMETER




G8JI00200-006 100808 101408 8289284 1






Page 75 of 425


REDACTED


barcode 485041

ANALYTICAL REPORT

Job tum~8r 360-19248-1

Fe) 0in CQmor8h~J









REDACTED



Analyte




ResultQualifier


104 109 95

62000 -tr-5-7 (tr

15000


Client Matrix

Unit MDL






1010S200S 0905


RL Dilution

1015200S 1S16 1014200S OS56

020 10 020 10 020 10 20 10 15 10 020 10 020 10 051 10 020 10 20 10 020 10 051 10 051 10


10109200S 1S40 10092008 1150

400 10 50 10 2000 10

Page 27 of 425

REDACTED












































Page 28 of 425 C (L~6~

REDACTED



Analyte






Method 3000 Sulfate






i 1)oO

middotif92 I]

103 Cl0



ND rrgL 010





10082008 0905 10082008 1500 Potbie

RL Dilution

050 l0 050 10 050 10 10 10 050 i 0 050 10 050 10 050 10 050 10 050 10 050 LO 050 10 050 10 050 10 050 10 050 10 050 10 050 10 050 10 050 iO

10 10 10 10

ACCBptance Umits

eo - 120 80 - 120

10162008 1125 0050 0

10212008 1548 10212008 1335

010 C

10142008 1809 20 0

101142008 1824 10 0

10102008 0614 oJ10 0

REDACTED




GCMS VOA

GCMS Semi VOA

J

Metals

B

J


Description






REDACTED

~

~~


November 12 2008



Dear Ms Mason




Sincerely



REDACTED

Case Narrative






REDACTED

606

__


PARAMETER




G8JI00200-006 100808 101408 8289284 1






Page 75 of 425


REDACTED


barcode 485041



Analyte




ResultQualifier


104 109 95

62000 -tr-5-7 (tr

15000


Client Matrix

Unit MDL






1010S200S 0905


RL Dilution

1015200S 1S16 1014200S OS56

020 10 020 10 020 10 20 10 15 10 020 10 020 10 051 10 020 10 20 10 020 10 051 10 051 10


10109200S 1S40 10092008 1150

400 10 50 10 2000 10

Page 27 of 425

REDACTED












































Page 28 of 425 C (L~6~

REDACTED



Analyte






Method 3000 Sulfate






i 1)oO

middotif92 I]

103 Cl0



ND rrgL 010





10082008 0905 10082008 1500 Potbie

RL Dilution

050 l0 050 10 050 10 10 10 050 i 0 050 10 050 10 050 10 050 10 050 10 050 LO 050 10 050 10 050 10 050 10 050 10 050 10 050 10 050 10 050 iO

10 10 10 10

ACCBptance Umits

eo - 120 80 - 120

10162008 1125 0050 0

10212008 1548 10212008 1335

010 C

10142008 1809 20 0

101142008 1824 10 0

10102008 0614 oJ10 0

REDACTED




GCMS VOA

GCMS Semi VOA

J

Metals

B

J


Description






REDACTED

~

~~


November 12 2008



Dear Ms Mason




Sincerely



REDACTED

Case Narrative






REDACTED

606

__


PARAMETER




G8JI00200-006 100808 101408 8289284 1






Page 75 of 425


REDACTED


barcode 485041












































Page 28 of 425 C (L~6~

REDACTED



Analyte






Method 3000 Sulfate






i 1)oO

middotif92 I]

103 Cl0



ND rrgL 010





10082008 0905 10082008 1500 Potbie

RL Dilution

050 l0 050 10 050 10 10 10 050 i 0 050 10 050 10 050 10 050 10 050 10 050 LO 050 10 050 10 050 10 050 10 050 10 050 10 050 10 050 10 050 iO

10 10 10 10

ACCBptance Umits

eo - 120 80 - 120

10162008 1125 0050 0

10212008 1548 10212008 1335

010 C

10142008 1809 20 0

101142008 1824 10 0

10102008 0614 oJ10 0

REDACTED




GCMS VOA

GCMS Semi VOA

J

Metals

B

J


Description






REDACTED

~

~~


November 12 2008



Dear Ms Mason




Sincerely



REDACTED

Case Narrative






REDACTED

606

__


PARAMETER




G8JI00200-006 100808 101408 8289284 1






Page 75 of 425


REDACTED


barcode 485041



Analyte






Method 3000 Sulfate






i 1)oO

middotif92 I]

103 Cl0



ND rrgL 010





10082008 0905 10082008 1500 Potbie

RL Dilution

050 l0 050 10 050 10 10 10 050 i 0 050 10 050 10 050 10 050 10 050 10 050 LO 050 10 050 10 050 10 050 10 050 10 050 10 050 10 050 10 050 iO

10 10 10 10

ACCBptance Umits

eo - 120 80 - 120

10162008 1125 0050 0

10212008 1548 10212008 1335

010 C

10142008 1809 20 0

101142008 1824 10 0

10102008 0614 oJ10 0

REDACTED




GCMS VOA

GCMS Semi VOA

J

Metals

B

J


Description






REDACTED

~

~~


November 12 2008



Dear Ms Mason




Sincerely



REDACTED

Case Narrative






REDACTED

606

__


PARAMETER




G8JI00200-006 100808 101408 8289284 1






Page 75 of 425


REDACTED


barcode 485041




GCMS VOA

GCMS Semi VOA

J

Metals

B

J


Description






REDACTED

~

~~


November 12 2008



Dear Ms Mason




Sincerely



REDACTED

Case Narrative






REDACTED

606

__


PARAMETER




G8JI00200-006 100808 101408 8289284 1






Page 75 of 425


REDACTED


barcode 485041

~

~~


November 12 2008



Dear Ms Mason




Sincerely



REDACTED

Case Narrative






REDACTED

606

__


PARAMETER




G8JI00200-006 100808 101408 8289284 1






Page 75 of 425


REDACTED


barcode 485041

Case Narrative






REDACTED

606

__


PARAMETER




G8JI00200-006 100808 101408 8289284 1






Page 75 of 425


REDACTED


barcode 485041

__


PARAMETER




G8JI00200-006 100808 101408 8289284 1






Page 75 of 425


REDACTED


barcode 485041

[redacted] letter transmitting results of residential … · project: laboratory analysis . report...

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