r-cd o · log# i.-,:-', divisio n hal la dept of env quality/i&a inactive & abandoned...

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144195 i : ^iW!<t> ' B S T - P A I N J B f l * " " ' I 1 ' ! ' " ' l ^ 7878 QSftl AVE. • BATON ROUGE, LA 70820 r- CD ^* o o Combustion SAMPLE ANALYSES for L.A. DEPT. OF ENVIRONMENTAL QUALITY i.-,:-', DIVISION LOG# hal LA DEPT OF ENV QUALITY/I&A INACTIVE & ABANDONED SITES DIV PO BOX 82282 BATON ROUGE, LA 708842282 ATTENTION: MR HAROLD ETHRIDGE March 30, 1993 301567

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Page 1: r-CD o · log# i.-,:-', divisio n hal la dept of env quality/i&a inactive & abandoned sites div ... 12 n/a 5.0/5.0 93/03/25 13:21 dlg hal 301567 •p est-paine 7978 gsbi ave. •

144195i : ^ i W ! < t >' B S T - P A I N J B f l * " " ' I 1 ' ! ' " ' l ^

7878 QSftl AVE. • BATON ROUGE, LA 70820

r-CD̂*oo

Combus t ion

S A M P L E A N A L Y S E S

f o r

L.A. DEPT. OFE N V I R O N M E N T A L Q U A L I T Yi . - , : - ' , D I V I S I O NL O G #hal

LA DEPT OF ENV QUALITY/I&AI N A C T I V E & A B A N D O N E D S I T E S D I VPO BOX 82282BATON ROUGE, LA 708842282

A T T E N T I O N : M R H A R O L D E T H R I D G E

March 30, 1993

301567

Page 2: r-CD o · log# i.-,:-', divisio n hal la dept of env quality/i&a inactive & abandoned sites div ... 12 n/a 5.0/5.0 93/03/25 13:21 dlg hal 301567 •p est-paine 7978 gsbi ave. •

E S T - P A I N Ey*j~~~_. •—

7879 GSR1 AVE. • BATON ROUGE, LA 70620

LA DEPT OF ENV QUALITY/I&ABATON ROUGE, LA 708842282March 30, 1993

S a m p l e receipt a t WEST-PAINE LABORATORIES INC i s documented f or yourdes ignated s a m p l e ( s ) . Cha in-o f - cu s t ody documentation, i f p rov id ed , i s includedin this report. S a m p l e analys i s was in accordance with Environmental Protect ionAgency pro t o co l .A . T e s t Methods f o r Evaluat ing S o l i d W a s t e . S W - 8 4 6 , J u l y 1982

ParameterLead Method7420B . T e s t M e t h o d s f o r Evalua t ing S o l i d W a s t e , S W - 8 4 6 , J u l y 1982

ParameterBase-Neutral Frac t i onV o l a t i l e Organic CompoundsP C B ' S

Method8270 ( G C / M S )8240 ( H S L )8080

Documented re sul t s are shown on the f o l l o w i n g p a g e ( s ) .

W. R. PalmerC h i e f Operat ing O f f i c e r

hal 301567

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•pE S T - P A I N E7879 QSW AVE. • BATON ROUGE, LA 70620

LA DEPT OF ENV QUALITY/I&ABATON R O U G E , LA 708842282March 30, 1993

S a m p l e Source:Date C o l l e c t e d :Date Received:Parameter( U n i t )

A18031793-B9 3 / 0 3 / 1 79 3 / 0 3 / 1 7

T i m e C o l l e c t e d : 15:00Time Received: 20:00PercentResult Recovery Quality AssuranceActual / F o u n d Date/ TimeA n a l y s t

Lead( r a g / k g P b ) 12 N / A 5 . 0 / 5 . 0 9 3 / 0 3 / 2 5 13:21 D L G

hal 301567

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•pE S T - P A I N E7978 GSBI AVE. • BATON ROUGE, LA 70820

LA DEPT OF ENV QUALITY/I&ABATON ROUGE, LA 708842282March 30, 1993

S a m p l e Source: A18031793-ADate C o l l e c t e d : 9 3 / 0 3 / 1 7 T i m e C o l l e c t e d : 15:30Date Received: 9 3 / 0 3 / 1 7 T i m e Received: 20:00Parameter( U n i t ) Result PercentRecovery Quali ty AssuranceA c t u a l / F o u n d D a t e / T i m eAnalys tLead( m g / k g P b ) 8.9 N / A 5 . 0 / 5 . 0 9 3 / 0 3 / 2 5 13:21 DLG

hal 301567

Page 5: r-CD o · log# i.-,:-', divisio n hal la dept of env quality/i&a inactive & abandoned sites div ... 12 n/a 5.0/5.0 93/03/25 13:21 dlg hal 301567 •p est-paine 7978 gsbi ave. •

pE S T - P A I N E; . _ _ _ _ _ — —,— — _ _ lnv>*' * * * — 1 - ~

7079 GSR1 AVE. * BATON ROUGE. LA 70620

LA DEJPT OF ENV Q U A L I T Y / 1 &ABATON! R O U G E , LA 708842282SAMPLJ3 #: 9303180074

P R I O R I T Y P O L L U T A N T SBase-Neutral Frac t i on All re sul t s in mi l l igrams per kilogramS A M P L E S O U R C E : A 1 8 0 3 1 7 9 3 - BS a m p l e Date: 9 3 / 0 3 / 1 7 S a m p l e T i m e : 15:00

ParameterAcenaph th eneA c e n a p h t h v l e n eAnthraceneBenzidineBenzo ( a ) anthraceneBenzo (a.) pvreneBenzo (b) f luorantheneBenzo (crhi ) p eryl eneBenzo (k) f luoranthenebis ( 2 - C h l o r o e t h o x y ) methanebis ( 2 - C h l o r o e t h y l ) etherbis ( 2 - C h l o r o i s o p r o p y l ) etherb i s ( 2 - E t h v l h e x y l ) p h t h a l a t e4-Bromophenyl phenyl ether :Butvl benzvl p h t h a l a t e2 - C h l o r o n a p h t h a l e n e4-Chlorophenyl phenyl etherChryseneDibenzo ( a f h ) anthracenel f 2-Dichlorobenzene1 , 3-Dichlorobenzene1 , 4— Dichlorobenzene3 , 3 ' -Dichlorobenz idineDiethyl p h t h a l a t eDimethyl p h t h a l a t eDi-n-butyl p h t h a l a t e ;2 , 4-Dini tro to luene2 , 6-DinitrotolueneDi-n-octyl p h t h a l a t eH e x a c h l o r o b u t a d i e n eF l u o r a n t h e n eFluoreneHexach l orob enz eneH e x a c h l o r o c y c l o p e n t a d i e n eH e x a c h l o r o e t h a n e

Result001

< 2< 0< 0< 0< 0< 0< 0< 0< 0< 0< 0< 0< 0< 0< 0< 0< 0< 0< 0< 1< 0< 0

0< 0< 0< 0< 011< 0< 0< 0

.72

.68

.26

.68

.67

.67

.67

.67

.67

.67

.67

.67

.67

.67

.67

.67

.67

.67

.67

.67

.67

.67

.34

.67

.67

.80

.67

.67

.67

.67

.12

.82

.67

.67

.67

DetectionLimit0.670.670.672.680.670.670.670.670.670.670.670.670.670.670.670.670.670.670.670.670.670.671.340.670.670.670.670.670.670.670.670.670.670.670.67

hal 301567

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pE S T - P A I N Eat&tiebim.7879 GSRI AVE. • BATON ROUGE, LA 70820

P R I O R I T Y P O L L U T A N T SBase-Neutral Frac t i on

LA DEPT OF ENV QUALITY/I&ABATON R O U G E , LA 708842282S A M P l i E #: 9303180074

All results in mi l l i grams per kilogramS A M P L E S O U R C E : A18031793-BS a m p l e Date: 9 3 / 0 3 / 1 7 S a m p l e Time: 15:00

Parameter ( C o n t i n u e d )I n d e n o ( 1 . 2 , 3 -c , d ) pyr eneI s o p h o r o n eN a p h t h a l e n eN i t r o b e n z e n eN - N i t r o s o d i m e t h v l a m i n eN - N i t r o s o d i - n - p r o p y l a m i n eN - N i t r o s o d i p h e n y l a m i n ePhenanthrenePyrene1 , 2 , 4-Tri ch l orob enz ene1 . 2 - D i p h e n v l h y d r a z i n e

Result< 0.67< 0.67

3.34< 0.67< 0.67< 0.67< 0.67

5.291.38

< 0.67< 0.67

Detect ionLimit0.670.670.670.670.670.670.670.670.670.670.67

Date o f A n a l y s i s : 9 3 / 0 3 / 2 6 A n a l y s t : J M K

hal 301567

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E S T - P A I N E7879 GSRIAVE. • BATON ROUGE, LA 70820

LA DE^T OF ENV QUALITY/I&ABATON! ROUGE, LA 708842282S A M P L E #: 9303180074

Q U A L I T Y A S S U R A N C E / Q U A L I T Y C O N T R O LP E R C E N T RECOVERY

Base-Neutral F r a c t i o n

Parameter A18031793-BN i t r o b e n z e n e - d S2 - F l u o r o b i p h e n y 1T e r p h e n y l - d l 4

919597

hal 301567

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E S T - P A I N E7 8 7 9 Q S R I A V E . • BATON ROUGE, LA 70620

H A Z A R D O U S S U B S T A N C E L I S TV o l a t i l e Organic Compounds

LA DEPT OF ENV QUALITY/I&AB A T O l f R O U G E , LA 708842282S A M P L E #: 9303180074

All re su l t s in m i l l i g r a m s per k i logramS A M P L E SOURCE: A18031793-BS a m p l e Date: 9 3 / 0 3 / 1 7 S a m p l e T i m e : 15:00

ParameterMethyl chlorideMethyl bromideV i n y l ch l or id eChloroe thaneM e t h y l e n e c h l o r id eAcetoneCarbon d i s u l f i d e1 , 1-Dichloroethene1 . 1-Dichloroethanetrans-1 , 2 -Dichloroethene iC h l o r o f o r m1 , 2-DichloroethaneMethyl ethyl ketone1.1. 1-Trich loroe thaneCarbon t e t r a c h l o r i d eVinyl A c e t a t eD i ch 1 or obromome thane1 t 2-Dich loropropanecis-1. 3 -DichloropropeneTr i ch 1 or oetheneChlorodibromomethane1,1. 2-Tri ch l oro e thaneBenzenetrans-1 , 3 -Dich loropropeneBromoform4-Methyl-2-pentanone2-HexanoneT e t r a c h lor oethene1 , 1 , 2 , 2-Tetra ch l oro e thaneT o l u e n eCh 1 or oben z eneEthylbenzeneStyreneT o t a l X v l e n e

Result< 0.625< 0.625< 0.625< 0.625< 0.625

9.12< 0.625< 0.625< 0.625< 0.625< 0.625< 0.625< 3.13< 0.625< 0.625< 0.625< 0.625< 0.625< 0.625< 0.625< 0.625< 0.625< 0.625< 0.625< 0.625< 0.625< 0.625< 0.625< 0.625< 0.625< 0.625< 0.625< 0.625

1.09

Detect ionLimit0.6250.6250.6250.6250.6250.6250.6250.6250.6250.6250.6250.6253.130.6250.6250.6250.6250.6250.6250.6250.6250.6250.6250.6250.6250.6250.6250.6250.6250.6250.6250.6250.6250.625

Date o f A n a l y s i s : 9 3 / 0 3 / 2 5 A n a l y s t : H J P

hal 301567

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pE S T - P A I N E7979 QSm AVE. • BATON ROUGE, LA 70820

LA D$PT OF ENV QUALITY/ISABATOIf R O U G E , LA 708842282S A M P L E #: 9303180074

Q U A L I T Y A S S U R A N C E / Q U A L I T Y C O N T R O LP E R ' C E N T R E C O V E R YV o l a t i l e Organic Compounds

Parameter A 1 8 0 3 1 7 9 3 - B1,2-Dichloroe thane-d4T o l u e n e - d 84-Bromof luorobenzene

838383

hal 301567

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E S T - P A I N E7878 Q S R 1 A V E . • BATON ROUGE, LA 70820

P R I O R I T Y P O L L U T A N T SP C B ' S

LA DEPT OF ENV QUALITY/I&ABATON R O U G E , LA 708842282S A M P L E #: 9303180074

All re sul t s in m i l l i g r a m s per ki logramS A M P L E S O U R C E : A18031793-BS a m p l e Date: 9 3 / 0 3 / 1 7 S a m p l e T i m e : 15:00

ParameterAroclor-1242Aroc lor-1254Aroclor-1221Aroclor-1232Aroclor-1248Aroclor-1260Aroclor-1016Aroclor-1262Aroc lor-1268

Result< 10.0< 10.0< 10.0< 10.0< 10.0< 10.0< 10.0< 10.0< 10.0

Detec t ionLimit10.010.010.010.010.010.010.010.010.0

Date o f A n a l y s i s : 9 3 / 0 3 / 2 3 A n a l y s t : T S B

hal 301567

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pE S T - P A I N E7879 OSBt AVE. • BATON ROUGE, LA 70620

LA DEPT OF ENV QUALITY/I&AB A T O N ROUGE, LA 708842282S A M P L E #: 9303180076

P R I O R I T Y P O L L U T A N T SBase-Neutral F r a c t i o n All r e su l t s in m i l l i g r a m s per k i logramS A M P L E SOURCE: A18031793-AS a m p l e Date: 9 3 / 0 3 / 1 7 S a m p l e T i m e : 15:30

ParameterAcenaphtheneAcenaohthvleneAnthraceneBenzidineBenzo (a) anthraceneBenzo (a) pyreneBenz o ( b ) f luor antheneBenzo ( c r h i ) p e r v l e n eBenzo ( J c ) f luoranthenebis ( 2 -Chloro e thoxv) methanebis f 2 -Chlor oethvl ) etherbis ( 2 - C h l o r o i s o p r o p y l ) etherbis ( 2 -Ethylhexy l ) ph tha la t e4-Bromophenyl phenyl etherButyl benzyl p h t h a l a t e2 - C h l o r o n a p h t h a l e n e4— Chlorophenyl phenyl ether :Chrvsene iD ibenz o ( a , h ) anthracene1 f 2-Dichlorobenzene1, 3-Dichlorobenzene1 , 4-Dichlorobenzene3 f 3 ' -Dichlorobenz idineDiethvl D h t h a l a t eDimethyl p h t h a l a t eDi-n-butyl p h t h a l a t e2 , 4-Dini tro to luene '2 . 6-Dini tro to lueneDi-n-octyl p h t h a l a t eH e x a c h l o r o b u t a d i e n eF l u o r a n t h e n eFluoreneH e x a c h lor oben z eneH e x a c h l o r o c y c l o o e n t a d i e n eHexachloroe thane

Result1.731.883.23

< 2.680.90

< 0.67< 0.67< 0.67< 0.67< 0.67< 0.67< 0.67< 0.67< 0.67< 0.67< 0.67< 0.67

0.71< 0.67< 0.67< 0.67< 0.67< 1.34< 0.67< 0.67

0.94< 0.67< 0.67< 0.67< 0.67

3.094.54

< 0.67< 0.67< 0.67

Detect ionLimit0.670.670.672.680.670.670.670.670.670.670.670.670.670.670.670.670.670.670.670.670.670.671.340.670.670.670.670.670.670.670.670.670.670.670.67

hal 301567

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pE S T - P A I N E7879 GSfll AVE. • BATON ROUGE, LA 70620

P R I O R I T Y P O L L U T A N T SBase-Neutral Frac t i on

LA DEjPT OF ENV Q U A L I T Y / 1 & ABATON ROUGE, LA 708842282S A M P L E #: 9303180076

All result s in mi l l igrams per kilogramS A M P L E S O U R C E : A 1 8 0 3 1 7 9 3 - AS a m p l e Date: 9 3 / 0 3 / 1 7 S a m p l e Time: 15:30

Parameter ( C o n t i n u e d )I n d e n o ( 1 , 2 , 3 -c , d ) pyr eneI s o p h o r o n eN a p h t h a l e n eN i t r o b e n z e n eN - N i t r o s o d i m e t h y l a m i n eN - N i t r o s o d i - n - p r o p y l a m i n eN— N i t r o s o d i p h e n y l a m i n e :PhenanthrenePyrene ;1 , 2 , 4-Trich l orob enzene1, 2 - D i p h e n y l h v d r a z i n e

Result< 0.67< 0.676.97< 0.67< 0.67< 0.67< 0.67

11.44.02

< 0.67< 0.67

DetectionLimit0.670.670.670.670.670.670.670.670.670.670.67

Date o f A n a l y s i s : 9 3 / 0 3 / 2 6 A n a l y s t : J M K

hal 301567

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pE S T - P A I N Eme.7879 GSffl A V £ . • BATON HOUQE, LA 70620

LA DEPT OF ENV QUALITY/I&ABATON ROUGE, LA 708842282S A M P L E #: 9303180076

Q U A L I T Y A S S U R A N C E / Q U A L I T Y C O N T R O LP E R C E N T RECOVERY

Base-Neutral F r a c t i o n

Parameter A 1 8 0 3 1 7 9 3 - AN i t r o b e n z e n e - d 52-Fluorob ipheny1T e r p h e n y l - d l 4

106112115

hal 301567

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E S T - P A I N EI INC.

7879 QSRI AVE. • BATON ROUOE, LA 70820

H A Z A R D O U S S U B S T A N C E L I S TV o l a t i l e Organic Compounds

LA DEPT OF ENV QUALITY/I&ABATO4 R O U G E , LA 708842282S A M P L E #: 9303180076

(All re su l t s in m i l l i g r a m s per ki logramS A M P L E S O U R C E : A 1 8 0 3 1 7 9 3 - AS a m p l e Date: 9 3 / 0 3 / 1 7 S a m p l e T i m e : 15:30

ParameterMethyl ch l or id eMethyl bromideVinyl ch l or id eChloroe thaneMethvl ene ch l or id eAcetoneCarbon d i s u l f ide1 , 1-Dichloroethene1 . 1-Dichloroethanetrans-1 , 2-DichloroetheneC h l o r o f o r m1 , 2-DichloroethaneMethvl ethvl ketone1,1. 1-Trich loroe thaneCarbon t e t r a c h l o r i d eV i n y l A c e t a t e ;D i ch lor obromome thane1 f 2-Dich loropropanecis-1, 3-Dich loropropeneTrich loroe theneChlorodibromomethane1,1. 2 - T r i c h l o r o e t h a n eBenzenetrans— 1 , 3 -Dich loropropeneBromoform4-Methvl-2-oentanone2-Hexanone 'T e t r a c h l o r o e t h e n e1 , 1 , 2 , 2 - T e t r a chloroethaneT o l u e n eChlorobenzeneEthylbenzeneStyreneT o t a l X y l e n e

Result< 0< 0< 0< 0< 0

3< 0< 0< 0< 0< 0< 0< 3< 0< 0< 0< 0< 0< 0< 0< 0< 0< 0< 0< 0< 0< 0< 0< 0

2< 0

4< 0

32

.625

.625

.625

.625

.625

.12

.625

.625

.625

.625

.625

.625

.13

.625

.625

.625

.625

.625

.625

.625

.625

.625

.625

.625

.625

.625

.625

.625

.625

.25

.625

.30

.625

.5

DetectionLimit0.0.0.0.0.0.0.0.0.0.0.0.3.0.0.0.0.0.0.0.0.0.0.0.0.0.0.0.0.0.0.0.0.0.

62562562562562562562562562562562562513625625625625625625625625625625625625625625625625625625625625625

Date o f A n a l y s i s : 9 3 / 0 3 / 2 5 A n a l y s t : H J P

hal 301567

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E S T - P A I N Eme.7878 GSRI AVE. • BATON ROUGE. LA 70620

LA DEPT OF ENV QUALITY/I&ABATON] R O U G E , LA 708842282S A M P L E #: 9303180076

Q U A L I T Y A S S U R A N C E / Q U A L I T Y C O N T R O LP E R C E N T RECOVERY

V o l a t i l e Organic Compounds

Parameter A 1 8 0 3 1 7 9 3 - A1,2-Dichloroe thane-d4Toluene-d84-Bromofluorobenzene

99102

97

hal 301567

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pE S T - P A I N E7879 GSRIAVE. • BATON ROUGE, LA 70820

P R I O R I T Y P O L L U T A N T SP C B ' S

LA DEPT OF ENV QUALITY/ISAB A T O l f ROUGE, LA 708842282S A M P L E #: 9303180076

re su l t s in m i l l i g r a m s per ki logramS A M P L E S O U R C E : A 1 8 0 3 1 7 9 3 - AS a m p l e Date: 9 3 / 0 3 / 1 7 S a m p l e T i m e : 15:30

ParameterAroclor-1242Aroclor-1254Aroclor-1221Aroclor-1232A r o c l o r — 1248Aroclor-1260Aroclor-1016Aroc l or-1262A r o c l o r - 1 2 6 8

Result< 10.0< 10.0< 20.0< 10.0< 10.0< 10.0< 10.0< 10.0< 10.0

Detect ionLimit10.010.020.010.010.010.010.010.010.0

Date o f A n a l y s i s : 9 3 / 0 3 / 2 3 A n a l y s t : T S B

hal 301567

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E S T - P A I N E7 9 7 9 G S R I A V E . • BATON ROUGE, LA 70820

S O I L V O L A T I L E M A T R I X S P I K E / M A T R I X S P I K E D U P L I C A T E RECOVERY

S a m p l e No: 9303220041 L e v e l : ( l o w / m e d ) : Med

COMPOUND1, 1-DichloroethaneT r i c h l o r e t h e n eBenzeneT o l u e n eChlorobenzene

S P I K E S A M P L EADDED C O N C E N T R A T I O N( m g / K a ) f m a / K a )0.0500.0500.0500.0500.050

< 0.005< 0.005< 0.005< 0.005< 0.005

MSC O N C E N T R A T I O Nf m a / K a )

0.0540.0550.0550.0590.054

MSREC#108110110118108

QCT 3 M T T R

REC.59-17262-33760-33359-33966-142

C O M P O U N D1 , 1-DichloroetheneTrichloroe theneBenzeneT o l u e n eCh lor obenz ene

S P I K EADDED( m c r / K c n0.0500.0500.0500.0500.050

M S DC O N C E N T R A T I O Nf m a / K a )

0.0610.0580.0550.0600.057

M S D%REC#

122116110120114

%RPD#12

5025

QC LIMITSRPD 1812224212121

59-33282-13780-3333>33965-142

# Column to be used to f l a g recovery and RPD values with an asterisk* Value s outside of QC l imi t sRPD: 0 out of 5 outside l imit sS p i k e Recovery: 0 out of 10 outside l imi t sC O M M E N T S : VOSME-022

A Member of the Inchcape Environmental Group

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•pE S T - P A I N EI N C .7979 GSRI AVE. • BATON ROUGE, LA 70820

S O I L S E M I V O L A T I L E M A T R I X S P I K E / M A T R I X S P I K E D U P L I C A T E RECOVERY

S a m p l e No: 9303180076 L e v e l : ( l o w / m e d ) : Low

COMPOUNDPhenol ( A / E )2-chlorophenol ( A / E )1 . 4-DichlorobenzeneN - N i t r o s o d i - n - p r o p . ( 1 )1,2 , 4-Trichlorobenzene4 -Ch lor o- 3 -me thy I p h e n o 1Acenaphthene4-Nitrophenol ( A / E )2 , 4-DinitrotoluenePentachlorophenol ( A / E )Pyrene

C O M P O U N DPhenol ( A / E )2-Chlorophenol ( A / E )1 f 4— DichlorobenzeneN - N i t r o s o - d i - n - p r o p . ( 1 )1.2, 4-Trichlorobenzene4 , Chloro-3 -methy Ipheno 1Acenaphthene4-Nitropheno l ( A / E )2 , 4-DinitrotoluenePentachlorophenol ( A / E )Pyrene

S P I K E S A M P L E M S M SADDED C O N C E N T R A T I O N C O N C E N T R A T I O N %( m c r X K c r ) (mcr\Kcn ( m c r X K c r t REC#

6.6.3.3.3.6.3.6.3.6.3.

7070303030703070307030

S P I K EADDED(mcr \Kcrt6.6.3.3.3.6.3.6.3.6.3.

7070303030703070307030

00000010004

.00

.00

.00

.00

.00

.00

.70

.00

.30

.00

.00

M S DC O N C E N T R A T I O N

( m c r X K c f )66334643227

.50

.10

.40

.80

.00

.30

.40

.50

.90

.10

.70

66344643307

.70

.00

.30

.00

.00

.50

.30

.30

.10

.80

.10

M S DREC#

98*92

100110120*

9480527931

110

100*91

100120120*

9877508312*

RPD#210804334

88*16

93

QCL I M I T S

REC.26- 9025-10228-10441-12638-10726-10331-13711-11428- 8917-10935-142

QC LIMITSRPD REC.3550273823331950474736

26- 9025-10228-10441-12638-10726-10331-13711-11428- 8917-10935-142

( 1 ) N - N i t r o s o - d i - n - p r o p y l a m i n e# Column to be used to f l a g recovery and RPD values with an asterisk* Value s outs ide of QC l imi t sRPD; 1 out of 11 outside l i m i t sS p i k e Recovery: 5 out of 22 outside l imi t sC O M M E N T S : SVSLO-145__________________________________________________

A Member of the I n c h c a p e Environmental Group

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E S T - P A I N Ek l N C .

7979 GSRI AVE. « BATON R O U G E , LA 70820

N A R R A T I V E(( A N A L Y S I S )

S p i k e A l l o c a t i o n : S V S L O - 1 4 5Date: 0 3 / 3 1 / 9 3

____The M a t r i x S p i k e , Matr i x S p i k e D u p l i c a t e showed s l i g h t l y|

higher recoveries than the QC l i m i t s , but, they are not out ofa n a l y t i c a l bounds. The M a t r i x S p i k e had low recoveries oni

P e n t a c h l o r o p h e n o l which re sul t ed in a high Relat ive Percenti;D i f f e r e n c e due to the s a m p l e matrix.________________________

A Member of the Inchfape Environmental Group

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S t a t e of Louis iana /£ 7 5793Department of Environmenta l Q u a l i t yI n a c t i v e a n d A b a n d o n e d S i t e s D i v i s i o nP.O. Box 44066, Baton Rouge, LA 70804(504) 342-8925

S T A : N O ,

P R O J . N O . P R O J E C T N A M E

S A M P L E R S : (Signature)

D A T E T I M E S T A T I O N L O C A T I O N

N O .OF •

C O N -T A I N E R S

O R I G I N A LR E M A R K SL A R

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