properties of materials - module a lab report
DESCRIPTION
Civil engineeringTRANSCRIPT
DETERMINATION OF
NORMAL CONSISTENCY OF HYDRAULIC CEMENT
I. OBJECTIVES
This experimental work is intended to determine normal consistency of
hydraulic cement in order to know the initial setting time (determining
volume of water needed to prepare hydraulic cement past).
II. TOOLS AND EQUIPMENT
1. Mixer, with some leaves mixers that are made out of stainless steel
and removable bowl
2. Vicat cement (using the end of C as shown in the picture A.2
3. Scale with 1.0 gram of sensitivity
4. Scraper that is made out of stiff rubber
5. Measuring cup (capacity 150 or 200 mL)
6. Trowel
7. Rubber gloves
III. MATERIAL
1. Portland cement ± 3.5 kg (for approximately six experiments)
2. Clean water (room temperature)
IV. PROCEDURE
Hydraulic cement past
1. Set the leave, mixer, and its bowl.
2. Fill all the materials into the bowl and mix as follows:
a. Pour water (±155-125 cc for Cement Type I and ±130 – 140 cc
for Cement Type II).
b. Pour 500 grams of cement into the water; let the absorption
occur for approximately 30 seconds.
3. Turn the mixer on, use the 140±5 rpm and mix the paste around for
around 30 seconds.
4. Turn the mixer off during 15 seconds and sweep the paste on the
inner part of bowl
5. Turn the mixer on with normal speed rotation (285±10 rpm) and
mix the paste for 1 minute.
Testing with vicat tool
1. take the paste from the bowl and form a ball. Throw the cement
paste ball from one hand to another at around 15 cm of distance
several times. Place it into a vicat tool (see Figure A.2). Push it into
the conic ring (G) therefore it fills properly into the ring.
2. Place the ring to a plate of glass (H) and pour the rest of the cement
paste into the ring from two directions. Equalize the cement paste
using spatula but do not push the cement paste.
3. Place the ring containing cement paste under the shaft (B) so that
the needle of the vicat tool can contact/touch the surface of the
cement paste. Lock the shaft by turning the key (K).
4. Place the indicator (F) precisely to zero point (upper layer). By
turning the key (K) open, we release the shaft (B), and at the same
time needle (C) will penetrate into the cement pate.
5. If in thirty seconds the depth of needle © is around 10±1 mm from
the surface, the consistency of cement paste is normal.
6. If the normal consistency is unreached, repeat step 1 until 1 so that
the condition is reached.
7. Record the volume of water that was used to reach normal
consistency.
8. Plot the (graph) relationship of the depth of needle penetration and
water content (in percentage) in cement paste
VI. CALCULATIONS
Constant: 500 grams of cement
Depth of Needle
Penetration (mm)
Water Content (%)
24 23.07
9 20.00
24 918
19
20
21
22
23
24
Depth of Needle Penetration with Different Water Content
Water Content
Depth of Needle Penetration (mm)
Wat
er C
onte
nt (%
)
VII. EXPERIMENTAL ANALYSIS
1. Analysis of the Experiment:
In order to start testing with the vicat tool, we first needed to make
several samples of cement paste. We gathered the leave, mixer,
and a bowl. We then poured water and 500 grams of cement into
the water, leaving 30 seconds for water absorption, before mixing
using a speed of 140 ± 5 rpm for 30 seconds. We the turn off the
mixer, sweep the paste off the inner part of the bowl to ensure an
even mixture, and then turned the mixer on with a rotational speed
of 285 ± 10 rpm for one minute.
After the sample of cement paste was ready, we took the entire
sample and made it into a ball. We then threw the cement paste
ball back and forth between each hand, with a distance of 15 cm,
for several times, before placing inside the conic ring of the vicat
tool. Afterwards, we placed the ring onto a plate a glass and poured
the remaining amount of cement paste into the ring from two
directions. We also made sure that the surface of the conic ring is
smooth, without compressing the cement paste. After these
preparations were completed, we placed the needle of the vicat tool
just so it barely contacts the surface of the cement paste and then
locked the shaft. Afterwards, we placed the indicator to the zero
point and released the shaft, causing the needle to penetrate the
cement. After thirty seconds, we measure the depth of the needle. If
the depth is not around 10 ± 1 mm from the surface, we repeat the
experiment using different water contents.
2. Analysis of the Results:
It was necessary to repeat this experiment once. In the first text, we
used 500 grams of cement and 150 grams of water. This means
that the resultant cement paste had a weight of 650 grams and a
water content of 23.07%. However, the consistency of this cement
paste was not considered normal. With this cement paste, the
needle penetrated, within 30 seconds, to the depth of 24 mm, which
is greater than the normal consistency by 240%.
With the first result having a very high depth of needle penetration,
we reduced the water content of the cement paste in the second
test. The result cement paste had 500 grams of cement and 125
grams of water. This means that the cement paste now possessed a
weight of 625 grams and a water content of 20%. After testing with
the vicat tool, we gained a depth of needle penetration of 9 mm,
after thirty seconds. As this depth of needle penetration is within
the acceptable limits of 10 ± 1 mm, it was determined that this
mixture of cement and water possesses the normal consistency of
hydraulic cement paste.
3. Error Analysis:
During the multiple weightings to obtain the constant weight of
cement and the needed weight of water for each cement paste
sample, an offset error may occur due to improper reading of the
scale. Additionally, as the scale has a random error of .1%, the
weight of each sample of aggregates may not be completely
accurate. An error may also occur during the uniform distribution of
the top of each cement paste sample in the conic ring. Finally, an
error may also occur from reading the indicator of the vicat tool.
However, all these errors are extremely minor, and do not have a
significant effect on the results of this experiment.
VIII. CONCLUSIONS
Overall, the purpose of this experiment is to determine the normal
consistency of hydraulic dement in order to know its initial setting
time. This is done by determining the volume of water needed to
prepare hydraulic cement paste. In the end, the result is that in order
to obtain the normal consistency of hydraulic cement paste, a water
content of 20% is required.
IX. REFERENCES
American Society for Testing and materials. “Standards Test method
for Normal Consistency of Hydraulic Cement”, No. ASTM C 187 – 98
(Reapproved 2003). Annual Book of ASTM Standards, Vol. 04. 01.
X. APPENDIX
PROPERTIES OF MATERIALS EXPERIMENTAL REPORT
DETERMINATION OF NORMAL CONSISTENCY OF HYDRAULIC CEMENT
MODULE A.2
GROUP 29
Fajar Surya Muhammad 1306437170
Muhammad Alif Maggalatta 1306388906
Raihan Alisha Nabila 1306437126
R.A Tamara R F Iskandar 1306388894
Zain Zahran Azzaino 1306437044
Date of Experimental : October 30th 2013
Experimental Assistant : Putri Marastuti
Date of Approval :
Score :
Assistant’s Signature :
LABORATORY OF STRUCTURE AND MATERIAL
CIVIL ENGINEERING DEPARTEMENT
ENGINEERING FACULTY
UNIVERSITY OF INDONESIA