physical synthesis and jetting behaviour of metal oxide ... · sonia sharma, sumukh s pande, and p....
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Physical synthesis and jetting behaviour of metal oxide based inks
for printed electronics
Introduction Results and Discussion
Methods
References
Mn doped ZnO
ZnO
Zn1-xMnxO; (0 ≤ x ≤ 0.25)
Solid state rxn @ 1100 °C_6 h
Single phase: Mn-ZnO
MnO
Zn1-xAlxO; (0 ≤ x ≤ 0.05)
ZnO Al2O3 Toluene
Spark plasma sintering
• 1100 °C _4 min
• 100 °C/min, 40 MPa
[A] [B]
1. Sonia Sharma, Raghavendar Bayikadi, and P. Swaminathan, RSC Adv., 6, 86586 (2016).
2. Sonia Sharma, Pranith Ramesh, and P. Swaminathan, J. Elec. Matls, 44, 4710 (2015).
3. Sonia Sharma, Sumukh S Pande, and P. Swaminathan, Appl. Mater. & Interfaces
submitted.
• Stable metal oxide particle inks of pure and doped ZnO are synthesized
by top-down wet milling approach.
• Ethylene glycol based inks are found to be suitable for inkjet printing.
• Synthesis can be extended to other metal oxide systems.
Single phase: Al-ZnO
Sonia Sharma1, Sumukh Shankar Pande2, and P. Swaminathan1
1Dept. of Metallurgical and Materials Engineering, IIT– Madras, India2Dept. of Metallurgical and Materials Engineering, NIT– Tiruchirappalli, India
E-mail: [email protected], [email protected]
Conclusions
Acknowledgements
Top-down approach for synthesizing nanoparticles
Metal oxide ink preparation
Wet milling with
Toluene for 12 h
Pure & doped
Zinc oxideNanoparticles +
solvent +surfactant
Stable
ink
[C]
Al doped ZnO
Custom developed direct writer and printed patterns[D]
Research supported by New Faculty Seed Grant, IIT Madras. Travel supported by Institute Graduate Student Assistantship, IIT Madras.
Size reduction by milling
Unfiltered & filtered ZnO ink
Ink formulation
Ink stability, fluid property & jettability study
Particle size distribution and TEM image of filtered ink
Ink extrusion printing: Custom built printer Inkjet printing: Commercial printer
3D optical images and thickness profile % Transmittance
Drop patterns Printed line patterns