photo-thermal deflection spectroscopy

14
Photo-thermal Photo-thermal Deflection Deflection Spectroscopy Spectroscopy George Noid LIGO SURF Student

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Photo-thermal Deflection Spectroscopy. George Noid LIGO SURF Student. Summary. Introduction Theory Experiment Results. Fused Silica Currently uses Thermal Conductivity is 1.38 W/mK. Synthetic Sapphire Proposed for LIGO II Crystal Systems - PowerPoint PPT Presentation

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Page 1: Photo-thermal Deflection Spectroscopy

Photo-thermal DeflectionPhoto-thermal DeflectionSpectroscopySpectroscopy

George Noid

LIGO SURF Student

Page 2: Photo-thermal Deflection Spectroscopy

SummarySummary

Introduction Theory Experiment Results

Page 3: Photo-thermal Deflection Spectroscopy

LIGOLIGO TESTTEST MASSESMASSES

Fused Silica– Currently uses– Thermal Conductivity

is 1.38 W/mK

Synthetic Sapphire– Proposed for LIGO II– Crystal Systems– Thermal Conductivity

is 23.1 parallel to optical axis

Page 4: Photo-thermal Deflection Spectroscopy

Photothermal Deflection Spectroscopy (PDS)Photothermal Deflection Spectroscopy (PDS)

PDS First used: 1979 Two Lasers:

– Pump– Probe

Temperature Gradient => Gradient in the index of refraction

Useful as a non-destructive spectroscopic method– Can observe microscopic impurities in a crystal– Ex: trace metals in a sapphire crystal

Page 5: Photo-thermal Deflection Spectroscopy

PDSPDS

Probe– Does not disturb sample– Detected

Pump- More powerful- Modulated- Not detected

Page 6: Photo-thermal Deflection Spectroscopy

DeflectionDeflection

Page 7: Photo-thermal Deflection Spectroscopy

Deflection (cont.)Deflection (cont.)

Snells law: a sin A = b sin B (..) = arcsin { (n0)/(n(..)) * sin (pi/2 - )}

= laser angles = angle of deflection

– n0 = index of refraction of sapphire (1.862)

– n = index of refraction function caused by PDS

Page 8: Photo-thermal Deflection Spectroscopy

The Experiment: two laser The Experiment: two laser tablestables

Pump table– 700 mW Nd YAG laser– Chopper– Fiber coupler – Fiber

Probe table– 5 mW He Ne– Fiber – Telescope– 1064 mirror– Biconvex lens– Sapphire crystal – Quad cell Detetector

Page 9: Photo-thermal Deflection Spectroscopy

Pump TablePump Table

Nd YAG

chopper

5- axis fiberaligner

PolarizationSelecting filter

Page 10: Photo-thermal Deflection Spectroscopy

Injecting and MaximizingInjecting and Maximizing

Page 11: Photo-thermal Deflection Spectroscopy

Probe tableProbe table

Photo detector

sample

He Ne laser

Fiber conduit

telescope

Fiber chuck

Aspheric lensholder

1064 mirror

beam tube

XY stage

XYZstage

Page 12: Photo-thermal Deflection Spectroscopy

Probe Table: laser alignmentProbe Table: laser alignment

Small angle theta in the y direction– Increases interaction length

Beam waists: 80 microns Nd Yag

– Magnified, collimated in telescope– Reflected off mirror – Focused in biconvex lens into sapphire

He - ne– Passes through 1064 mirror– Focused in biconvex lens into sapphire

Page 13: Photo-thermal Deflection Spectroscopy

DataData

• Initial results were inconclusive with lock- in amplification.

• Observed PDS with signal analyzer • Pump power incident: 300 mw • Chopping frequency: 500 Hz • Maximum signal to noise ratio: 27 to 3

• Crystal mapping ongoing

Page 14: Photo-thermal Deflection Spectroscopy

Representative PeakRepresentative Peakfourier transform of photothermal deflection

0.00E+005.00E-061.00E-051.50E-052.00E-052.50E-053.00E-053.50E-054.

50E+

02

4.58

E+02

4.67

E+02

4.75

E+02

4.83

E+02

4.91

E+02

5.00

E+02

5.08

E+02

5.16

E+02

5.24

E+02

5.33

E+02

5.41

E+02

5.49

E+02

frequency(Hz)

sign

al(m

Vrm

s)

Series2