pesticide control laboratory - inab control laboratory department of agriculture, food and the...

Edition 29, 13/04/2018 121T of 35

Pesticide Control Laboratory Department of Agriculture, Food and The Marine

Backweston Laboratory Campus, Young's Cross, Backweston, Celbridge,

Co Kildare

Testing Laboratory

Registration number: 121T

is accredited by the Irish National Accreditation Board (INAB) to undertake testing as detailed in

the Schedule bearing the Registration Number detailed above, in compliance with the

International Standard ISO/IEC 17025:2005 2nd Edition

“General Requirements for the Competence of Testing and Calibration Laboratories”

(This Certificate must be read in conjunction with the Annexed Schedule of Accreditation)

Date of award of accreditation: 11:12:2000

Date of last renewal of accreditation: 18:05:2015

Expiry date of this certificate of accreditation: 18:05:2020

This Accreditation shall remain in force until further notice subject to continuing compliance

with INAB accreditation criteria, ISO/IEC 17025 and any further requirements specified by the

Irish National Accreditation Board.

Manager: ____________________ Chairperson: ____________________

Dr Adrienne Duff Mr Tom O’Neill

Issued on 18 May 2015

Organisations are subject to annual surveillance and are re-assessed every five years. The renewal date on this

Certificate confirms the latest date of renewal of accreditation. To confirm the validity of this Certificate, please

contact the Irish National Accreditation Board.

The INAB is a signatory of the European co-operation for Accreditation (EA) Testing Multilateral Agreement (MLA) and the

International Laboratory Accreditation Cooperation (ILAC) Mutual Recognition Arrangement.

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Schedule of Accreditation

(Annex to Accreditation Certificate) Permanent Laboratory:

Category A

PESTICIDE CONTROL LABORATORY

Chemical Testing Laboratory

Initial Registration Date : 11-December-2000

Postal Address:

(Address of other locations

as they apply)

Backweston Laboratory Campus

Young's Cross

Backweston

Celbridge

Co Kildare

Telephone: +353 (1) 6157552

Fax: +353 (1) 6157574

E-mail: [email protected]

Contact Name: Sean Hyland

Facilities: Normally not available for Public testing

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Schedule of Accreditation

Permanent Laboratory: Category A

THE IRISH NATIONAL ACCREDITATION BOARD (INAB) is the Irish body for the accreditation of

organisations including laboratories.

Laboratory accreditation is available to testing and calibration facilities operated by manufacturing

organisations, government departments, educational institutions and commercial testing/calibration

services. Indeed, any organisation involved in testing, measurement or calibration in any area of

technology can seek accreditation for the work it is undertaking.

Each accredited laboratory has been assessed by skilled specialist assessors and found to meet criteria

which are in compliance with ISO/IEC 17025 or ISO/IEC 15189 (medical laboratories). Frequent audits,

together with periodic inter-laboratory test programmes, ensure that these standards of operation are

maintained.

Testing and Calibration Categories:

Category A:

Permanent laboratory calibration and testing where the laboratory is erected on a fixed

location for a period expected to be greater than three years.

Category B: Site calibration and testing that is performed by staff sent out on site by a permanent

laboratory that is accredited by the Irish National Accreditation Board.

Category C: Site calibration and testing that is performed in a site/mobile laboratory or by staff sent

out by such a laboratory, the operation of which is the responsibility of a permanent

laboratory accredited by the Irish National Accreditation Board.

Category D: Site calibration and testing that is performed on site by individuals and organisations that

do not have a permanent calibration/testing laboratory. Testing may be performed using

(a) portable test equipment

(b) a site laboratory

(c) a mobile laboratory or

(d) equipment from a mobile or site laboratory

Standard Specification or Test Procedure Used:

The standard specification or test procedure that is accredited is the issue that is current on the date of the most

recent visit, unless otherwise stated.

Glossary of Terms

Facilities:

Public calibration/testing service: Commercial operations which actively seek work from others.

Conditionally available for public

calibration/testing:

Established for another primary purpose but, more commonly than not,

is available for outside work.

Normally not available for public

calibration/testing:

Unavailable for public calibration/testing more often than not.

Laboratory users wishing to obtain assurance that calibration or test results are reliable and carried out to the Irish

National Accreditation Board criteria should insist on receiving an accredited calibration certificate or test report.

Users should contact the laboratory directly to ensure that this scope of accreditation is current. INAB will, on

request, verify the status and scope.

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Scope of Accreditation

Pesticide Control Laboratory Permanent Laboratory:

Category A


INAB Classification number (P9)

Materials/products tested

Type of test/properties

measured

Range of measurement

Standard specifications

Equipment/techniques used

752

.02

Residues in Foods and

Agricultural Materials

Pesticides

Pesticide residues in

food of plant origin

- Fruit + Vegetables +

Honey

- Cereals

Screening, confirmation and

quantification of pesticide

residues in food of plant origin

A list of pesticides as defined in

Annex 1.

Documented in house methods

Extractions (SOP 101) based

on: Standard multi-residue

method used based on

“Analytical methods for

pesticide residues in

foodstuffs” 6th Ed – Ministry of

Health, Welfare and Sport, The

Netherlands

Analysis using GC-MS/MS

(SOP227) and LC-MS/MS

(SOP228)

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Category A





measured




752

.02



Pesticides


food of animal origin

(fat)



residues in food of animal

origin (i.e. animal fats)


Annex 1.

Documented in house method

(SOP 106) based on: Standard

multi-residue Method based on

“Manual of Pesticide Residue

Analysis Vol 1”.

DFG Deutsche

Forschungs Gemeinshaft



(SOP228)

752

.02



Pesticides

Pesticide residues in Milk



residues in Milk

A list of pesticides as defined

in Annex 1.

Documented in-house method

(SOP 111) based on standard

multi-residue method -

Lehotay et al JAOAC Vol 88

No.2 (2005) 615


(SOP227)

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Category A





measured




752

.02


agricultural materials

Pesticides



Fruit vegetables and

honey


quantification of Amitraz and

its metabolites, DMPF and DMF

as defined in Annex 6



multi-residue method

published as J. AOAC Int. 88

615-629 - Steven J. Lehotay,

Katerina Mastrovska & Alam R.

Lightfield Analysis by LC-

MS/MS

761

.11

.12

.13

.99

Agricultural Products

and materials

Insecticides and

acaricide formulations

Herbicide formulations

Fungicide formulations

Other Agricultural

products

- Pesticides

- Biocides

Quantitation of active

substance in plant protection

products as defined in Annex 2.

Range

0 - 100%



CIPAC/AOAC/EU1107/2009

methods

Analysis using GC-FID (SOP224)

or HPLC DAD/CoronaCAD (SOP

207)

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Category A





measured




752

.02



Pesticides

Pesticides and PCB

residues in infant

formula, follow on

formula and milk

powder


quantification of pesticide residues

in infant formula, follow on

formula and milk powder.


Annex 1

Documented in-house method


multi-residue method -

Lehotay et al JAOAC Vol 88

No.2 2005 615



(SOP228)

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Category A





measured




752

.02



Pesticides



Fruit vegetables and

cereals


quantitation of a range of

quaternary ammonium salts and

other pesticides in fruit,

vegetables and cereals

See Annex 3 for list of salts

SOP 113 based on the

http://www.crl-

pesticides.eu/library/docs/srm

/meth_QuPPe.pdf

Quick Method for the Analysis

of Residues of numerous Highly

Polar Pesticides in Foods of

Plant Origin involving

Simultaneous Extraction with

Methanol and LC-MS/MS

Determination (QuPPe-

Method), Version 7.1 Nov 2013.

752

.02



Pesticides


cereals


quantitation of Glyphosate,

Glufosinate, Ethephon and

some of their metabolites in

cereals

See Annex 4 for list of

compounds

SOP 116 based on N. Yoshioka,

M. Asano, A. Kuse, T.

Mitsuhashi, Y. Nagasaki, Y.

Ueno and J of Chromatography

A 1218 (2011) 2675 - 3680

752

.02



Pesticides


Fruit and vegetables

and infant

formula/follow on

formula


quantitation of a range of

dithiocarbamates in fruit,

vegetables and infant

formula/follow on formula

See Annex 5 for list of

compounds

SOP 110 based on FERA method

FD 98 – 46

http://www.crl-

pesticides.eu/library/docs/srm

/meth_DithiocarbamatesCs2_E

urlSrm.PDF

http://www.crl-pesticides.eu/library/docs/srm/meth_QuPPe.pdf



http://www.crl-pesticides.eu/library/docs/srm/meth_DithiocarbamatesCs2_EurlSrm.PDF




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Category A


ANNEX 1

Pesticide

Instrument

Matrix

Food of

plant origin

Range mg/kg

Cereals

Range mg/kg

Milk

Range mg/kg

Food of Animal

Origin

Range mg/kg

Infant

Formula/Follow

on Formula

Range mg/kg

1-Naphthylacetamide LC 0.01 – 0.2 0.01 – 0.05 - - 0.01 - 0.05

4,4-Dichlorobenzophenone

GC 0.01 – 0.2 0.01 – 0.1 - 0.005 – 0.025 0.01 - 0.1

Abamectin LC - 0.1 - 0.5 - - 0.1 -0.5

Acephate LC - 0.01 – 0.05 - - 0.01 - 0.05

Acephate GC 0.01 - 0.2 0.01 – 0.1 - 0.005 – 0.025 -

Acetamiprid LC 0.01 - 2.0 0.01 – 0.05 - - 0.01 - 0.05

Acetochlor LC 0.02 - 0.2 0.02 – 0.1 - - 0.02 - 0.1

Aclonifen GC 0.01 - 0.2 - - 0.005 – 0.025 0.01 - 0.1

Acrinathrin GC 0.01 – 0.2 0.01 – 0.1 - 0.005 – 0.025 0.01 - 0.1

Alachlor GC 0.01 – 0.2 0.01 – 0.1 - 0.005 - 0.025 0.01 - 0.1

Aldicarb LC 0.02 – 0.2 0.02 – 0.1 - - 0.02 - 0.1

Aldicarb-sulfone LC 0.01 – 0.2 0.01 – 0.05 - - 0.01 - 0.05

Aldicarb-sulfoxide LC 0.02 – 0.2 0.02 – 0.1 - - 0.02 - 0.1

Aldrin GC 0.01 – 0.2 0.01 – 0.1 - 0.005 – 0.025 0.003 – 0.1

Ametryn LC 0.01 – 0.2 0.01 – 0.05 - 0.01 - 0.05 0.01 - 0.05

Amidosulfuron LC - 0.01 – 0.05 - - 0.01 - 0.05

Aminocarb LC 0.01 -0.2 0.01 – 0.05 - 0.01 -0.05 0.01 – 0.05

Atrazine LC 0.01 - 0.2 0.01 – 0.05 - - 0.01 - 0.05

Flexible Scope: Additional substances and new matrices may be added and ranges extended in accordance with the laboratory’s approved

and documented procedures. For details refer to the laboratory’s master list of flexible scope changes, available from the laboratory.

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Category A


ANNEX 1

Pesticide

Instrument

Matrix

Food of

plant origin

Range mg/kg

Cereals

Range mg/kg

Milk

Range mg/kg

Food of

Animal Origin

Range mg/kg

Infant

Formula/Follow

on Formula

Range mg/kg

Atrazine-desethyl LC 0.01 – 0.2 0.01 – 0.05 - - 0.01 – 0.05

Atrazine-desisopropyl LC 0.01 – 0.2 0.01 – 0.05 - - 0.01 – 0.05

Azaconazole GC 0.01 – 0.2 0.01 – 0.1 - 0.005 - 0.025 0.01 – 0.5

Azamethiophos GC 0.01 – 0.2 0.01 – 0.1 - 0.005 - 0.025 0.01 – 0.1

Azinphos-ethyl GC 0.01 – 0.2 0.01 – 0.1 0.005 - 0.025 0.005 - 0.025 0.01 – 0.1

Azinphos-methyl GC 0.01 – 0.2 0.01 – 0.1 0.005 - 0.025 0.01 – 0.025 -

Azoxystrobin LC 0.01 – 2 0.01 – 0.05 - - 0.01 – 0.05

Azoxystrobin GC 0.01 – 0.2 0.01 – 0.1 - 0.01 – 0.025 0.01 – 0.1

BAC 10 LC - 0.01 – 0.05 - - -

BAC 12 LC - 0.01 – 0.05 - - -

BAC 14 LC - 0.01 – 0.05 - - -

BAC 16 LC - 0.01 – 0.05 - - -

Benalaxyl LC 0.01 – 0.2 0.01 – 0.05 - 0.01 – 0.05 0.01 – 0.05

Bendiocarb LC 0.01 – 0.2 0.01 – 0.05 - 0.01 - 0.05 0.01 – 0.05

Bentazone LC 0.01 – 0.2 0.01 – 0.05 - - 0.01 – 0.05

Benthiavalicarb-isopropyl

LC 0.01 – 0.2

0.01 – 0.05 - - 0.01 – 0.05

Benzoximate LC 0.01 – 0.2 0.01 – 0.05 - - 0.01 – 0.05

Bifenthrin GC 0.01 – 0.2 0.01 – 0.1 - 0.005 - 0.025 0.01 – 0.1

Binapacryl GC 0.01 – 0.2 0.01 – 0.1 - - -

Bioresmethrin LC - 0.01 – 0.05 - - 0.01 – 0.05



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Category A


ANNEX 1

Pesticide

Instrument

Matrix

Food of

plant origin

Range mg/kg

Cereals

Range mg/kg

Milk

Range mg/kg

Food of Animal

Origin

Range mg/kg

Infant

Formula/Follow

on Formula

Range mg/kg

Biphenyl GC 0.05 – 0.5 0.05 – 1 - 0.025 – 0.25 0.01 -0.1

Bitertanol GC 0.01 – 0.2 0.01 – 0.1 - 0.005 - 0.025 0.01 – 0.1

Bixafen LC - 0.01 – 0.05 - - 0.01 – 0.05

Boscalid LC 0.01 - 2 0.01 – 0.05 - 0.005 - 0.025 0.01 – 0.05

Boscalid GC 0.01 -2 0.01 – 0.1 - 0.005 - 0.025 0.01 - 0.05

Bromacil LC 0.01 – 0.2 0.01 – 0.05 - 0.01 - 0.05 0.01 - 0.05

Bromophos-ethyl GC 0.01 – 0.2 0.01 – 0.1 0.005 – 0.025

0.005 – 0.025 -

Bromophos-methyl GC 0.01 – 0.2 0.01 – 0.1 0.005 – 0.025

0.005 – 0.025 0.01 – 0.1

Bromopropylate GC 0.01 – 0.2 0.01 – 0.1 - 0.005 – 0.025 0.01 - 0.1

Bromoxynil LC 0.01 – 0.2 0.01 – 0.05 - - -

Bromuconazole LC 0.01 – 0.2 0.01 – 0.05 - 0.01 – 0.05 0.01 - 0.05

Bupirimate LC 0.01 – 0.2 0.01 – 0.05 - 0.01 – 0.05 0.01 - 0.05

Buprofezin LC 0.01 – 0.2 0.01 – 0.05 - 0.01 – 0.05 0.01 - 0.05

Butocarboxim Sulfoxide

LC 0.01 – 0.2

0.01 – 0.05 - 0.01 – 0.05 0.01 - 0.05

Butoxycarboxim LC 0.02 – 0.4 0.02 – 0.4 - - 0.02 -0.1

Cadusafos LC 0.01 – 0.2 0.01 – 0.05 - 0.01 – 0.05 0.003 - 0.05

Carbaryl LC 0.01 – 0.2 0.01 – 0.05 - 0.01 – 0.05 0.01 - 0.05

Carbendazim LC 0.01 – 1.0 0.02 -0.1 - - 0.02 - 0.1

Carbofuran LC 0.01 – 0.2 0.01 – 0.05 - - 0.01 - 0.05

Carbofuran 3 Hydroxy LC - 0.01 – 0.05 - - 0.01 - 0.05



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Category A


ANNEX 1

Pesticide

Instrument

Matrix

Food of

plant origin

Range mg/kg

Cereals

Range mg/kg

Milk

Range mg/kg

Food of Animal

Origin

Range mg/kg

Infant

Formula/Follow

on Formula

Range mg/kg

Carbosulfan LC - 0.01 – 0.05 - - 0.01 - 0.05

Carboxin LC - - - 0.01 – 0.05 0.01 - 0.05

Carfentrazone-ethyl LC 0.01 - 0.2 0.01 – 0.05 - - 0.01 - 0.05

Chlorantraniliprole LC - 0.01 – 0.05 - - 0.01 - 0.05

Chlorbromuron LC 0.01 - 0.2 0.01 – 0.05 - 0.01 - 0.05 0.01 - 0.05

Chlorbufam GC 0.01 - 0.2 0.01 – 0.1 - - 0.01 - 0.1

Chlordane-cis GC 0.01 - 0.2 0.01 – 0.1 0.005 – 0.025 0.005 – 0.025 0.05 – 0.1

Chlordane-trans GC 0.01 - 0.2 0.01 – 0.1 0.005 – 0.025 0.005 – 0.025 0.05 - 0.1

Chlorfenapyr GC 0.01 - 0.2 0.01 – 0.1 - 0.005 – 0.025 -

Chlorfenvinphos LC 0.01 - 0.2 0.01 – 0.05 - 0.01 – 0.05 0.01 - 0.05

Chlorfluazuron LC 0.01 - 0.2 0.01 – 0.05 - - 0.01 - 0.05

Chloridazon LC 0.01 - 0.2 0.01 – 0.05 - - 0.01 - 0.1

Chlorobenzilate GC 0.01 - 0.2 0.01 – 0.1 0.005 – 0.025 0.005 –0.025 0.01 - 0.1

Chlorothalonil GC 0.01 – 5.0 0.01 – 0.1 - 0.005 – 0.025 0.01 - 0.1

Chlorotoluron LC 0.01 - 0.2 0.01 – 0.05 - - 0.01 - 0.1

Chloroxuron LC 0.01 - 0.2 0.01 – 0.05 - - 0.01 - 0.1

Chlorpropham GC 0.01 – 2.0 0.01 – 0.1 - 0.005 – 0.025 0.01 - 0.1

Chlorpyrifos LC 0.01 – 1.0 0.01 – 0.05 - 0.01 – 0.05 0.01 - 0.1

Chlorpyrifos Methyl GC 0.01 - 0.2 0.01 – 0.1 0.005 – 0.025 0.005 – 0.025 0.01 - 0.1

Chlorsulfuron LC 0.01 - 0.2 0.01 – 0.05 - - 0.05 - 0.1

Flexible Scope: Additional substances and new matrices may be added and ranges extended in accordance with the laboratory’s approved and

documented procedures. For details refer to the laboratory’s master list of flexible scope changes, available from the laboratory.

Edition 29, 13/04/2018 121T of 35



Category A


ANNEX 1

Pesticide

Instrument

Matrix

Food of

plant origin

Range mg/kg

Cereals

Range mg/kg

Milk

Range mg/kg

Food of Animal

Origin

Range mg/kg

Infant

Formula/Follow

on Formula

Range mg/kg

Chlorthal-dimethyl GC 0.01 – 0.2 0.01 – 0.1 - 0.005 – 0.025 0.01 - 0.1

Chlozolinate GC 0.01 – 0.2 0.01 – 0.1 - 0.005 - 0.025 0.05 - 0.1

Clethodim LC - - - - 0.01 - 0.05

Clodinafop-propargyl LC 0.01 – 0.2 - - - -

Clofentezine LC 0.01 – 1.0 0.01 – 0.05 - 0.01 – 0.05 0.01 - 0.05

Clomazone LC 0.01 – 0.2 0.01 – 0.05 - - 0.01 - 0.05

Clothianidin LC - 0.01 – 0.05 - - 0.01 - 0.05

Coumaphos GC 0.01 – 0.2 0.01 – 0.1 0.005 – 0.025

0.005 – 0.025 0.01 - 0.1

Cyanazine LC 0.01 – 0.2 0.01 – 0.05 - 0.01 – 0.05 0.01 - 0.05

Cyanofenphos GC 0.01 – 0.2 0.01 – 0.1 - 0.005 – 0.025 0.01 - 0.1

Cyanophos GC 0.01 – 0.2 0.01 – 0.1 - 0.005 – 0.025 0.01 - 0.1

Cyazofamid LC 0.01 – 0.2 - - - -

Cyclanilide LC 0.1 – 0.2 - - - -

Cycloate LC 0.01 – 0.2 0.01 – 0.05 - - 0.01 - 0.05

Cycloxydim LC 0.05 - 2 0.05 - 0.1 - - 0.05 - 0.5

Cyfluthrin GC 0.01 – 0.2 0.01 - 0.1 0.02 – 0.1 0.02 – 0.1 0.05 – 0.1

Cyhalothrin-lambda GC 0.01 – 0.2 0.02 -0.1 0.005 – 0.1 0.005 – 0.025 0.01 - 0.1

Cymiazol LC 0.01 – 0.2 0.01 - 0.05 - - 0.01 - 0.05

Cymoxanil LC 0.01 – 0.2 0.01 - 0.05 - - -

Cypermethrin GC 0.02 - 1 0.02 - 0.1 - 0.01 – 0.54 0.1 – 0.2



Edition 29, 13/04/2018 121T of 35



Category A


ANNEX 1

Pesticide

Instrument

Matrix

Food of

plant origin

Range mg/kg

Cereals

Range mg/kg

Milk

Range mg/kg

Food of Animal

Origin

Range mg/kg

Infant

Formula/Follow

on Formula

Range mg/kg

Cyproconazole GC 0.01 - 0.2 0.01 - 0.1 - 0.005 – 0.025 0.01 - 0.1

Cyprodinil LC 0.01 – 2.0 0.01 - 0.05 - 0.01 – 0.05 0.01 - 0.05

DDD-op GC 0.01 - 0.2 0.01 - 0.1 0.005 0.025 0.005 - 0.025 0.01 - 0.1

DDAC LC - 0.01 - 0.05 - - -

DDD-pp GC 0.01 - 0.2 0.01 - 0.1 0.005 0.025 0.005 – 0.025 0.01 - 0.1

DDE-op GC 0.01 - 0.2 0.01 - 0.1 0.005 0.025 0.005 – 0.025 0.01 - 0.1

DDE-pp GC 0.01 - 0.2 0.01 - 0.1 0.005 0.025 0.005 – 0.025 0.01 - 0.1

DDT-op GC 0.01 - 0.2 0.01 - 0.1 0.005 0.025 0.005 – 0.025 0.01 - 0.1

DDT-pp GC 0.01 - 0.2 0.01 - 0.1 0.005 0.025 0.005 – 0.025 -

DEET LC 0.05 – 1.0 0.05 – 1.0 - - 0.05 – 0.25

Deltamethrin GC 0.01 – 0.5 0.01 - 0.5 - 0.02 – 0.05 0.05 – 0.1

Demeton-S-mesulfone GC 0.01 - 0.2 0.01 - 0.1 - 0.005 - 0.025 0.003 – 0.1

Demeton-S-methyl-sulfoxide

LC 0.01 - 0.2

0.01 - 0.05 - - 0.01 – 0.05

Desmedipham LC 0.01 - 0.2 0.01 - 0.05 - - 0.01 – 0.05

Diazinon GC 0.01 - 0.2 0.01 - 0.1 0.01 – 0.1 0.005 – 0.54 0.01 – 0.1

Dichlobenil GC 0.01 - 0.2 0.01 - 0.1 - 0.005 – 0.025 0.01 – 0.1

Dichlofenthion LC - 0.05 - 0.25 - - 0.05 - 0.25

Dichlofluanid GC 0.01 - 0.2 - - 0.005 - 0.025 0.01 - 0.1

Dichlorvos GC 0.01 - 0.2 0.01 - 0.1 0.005 0.025 0.005 – 0.025 0.01 - 0.1

Diclobutrazol LC 0.01 - 0.2 0.01 - 0.05 - - 0.01 - 0.05



Edition 29, 13/04/2018 121T of 35



Category A


ANNEX 1

Pesticide

Instrument

Matrix

Food of

plant origin

Range mg/kg

Cereals

Range mg/kg

Milk

Range mg/kg

Food of

Animal Origin

Range mg/kg

Infant

Formula/Follow

on Formula

Range mg/kg

Dicloran GC 0.01 - 0.2 0.01 - 0.1 - 0.005 - 0.025 0.01 - 0.1

Dicrotophos LC - 0.01 - 0.05 - - 0.01 - 0.05

Dieldrin GC 0.01 - 0.2 0.01 - 0.1 - 0.005 - 0.025 0.003 – 0.1

Diethofencarb LC 0.01 - 0.2 0.01 - 0.05 - 0.01 - 0.05 0.01 - 0.05

Difenoconazole LC 0.01 - 0.2 0.01 - 0.05 - 0.01 – 0.05 0.01 - 0.05

Diflubenzuron LC 0.01 - 0.2 0.01 - 0.05 - - 0.01 - 0.05

Diflufenican LC - 0.01 - 0.05 - - 0.01 - 0.05

Dimethenamid LC 0.01 - 0.2 0.01 - 0.05 - 0.01 – 0.05 0.01 - 0.05

Dimethoate GC 0.01 - 0.2 0.01 - 0.1 0.005 - 0.025 0.005 - 0.025 0.01 - 0.1

Dimethomorph LC 0.01 - 0.5 0.01 - 0.05 - 0.01 - 0.05 0.01 - 0.05

Dimoxystrobin GC - 0.01 - 0.1 - 0.005 - 0.025 -

Diniconazole LC 0.01 - 0.2 0.01 - 0.05 - 0.01 - 0.05 0.01 - 0.05

Dinoseb LC 0.02 - 0.2 0.02 - 0.1 - - 0.02 - 0.1

Dinoterb LC 0.02 - 0.2 0.02 - 0.1 - - 0.02 - 0.1

Dioxacarb LC 0.01 - 0.2 0.02 - 0.1 - - 0.02 - 0.1

Diphenamid LC 0.01 - 0.2 0.02 - 0.1 - - 0.02 - 0.1

Diphenylamine GC 0.05 – 10 - - 0.025 - 0.25 0.01 - 0.05

Ditalimfos LC - 0.01 - 0.05 - - 0.01 - 0.05

Diuron LC 0.01 – 0.2 0.01 - 0.05 - 0.01 - 0.05 0.01 - 0.05

DMSA LC 0.02 – 0.2 0.02 - 0.1 - - 0.02 - 0.1



Edition 29, 13/04/2018 121T of 35



Category A


ANNEX 1

Pesticide

Instrument

Matrix

Food of

plant origin

Range mg/kg

Cereals

Range mg/kg

Milk

Range mg/kg

Food of

Animal Origin

Range mg/kg

Infant

Formula/Follow

on Formula

Range mg/kg

DMST LC 0.02 - 0.2 - - - 0.02 - 1

DNOC LC 0.01- 0.2 - - - 0.02 - 1

Dodine LC - - - - 0.01 – 0.05

Emamectin B1a LC 0.01- 0.2 - - - 0.01 -0.05

Endosulfan sulfate LC 0.02 - 0.2 - - 0.01 – 0.05

Endosulfan-alpha GC - - - 0.005 - 0.025 0.01 – 0.1

Endosulfan-beta GC 0.01- 0.2 - - 0.005 - 0.025 0.01 – 0.1

Endosulfan-ether GC 0.01- 0.2 - - 0.005 - 0.025 0.01 – 0.1

Endosulfan-lacton GC 0.01- 0.2 - - 0.005 - 0.025 0.01 – 0.1

Endosulfan-sulfate GC 0.02 - 0.2 - - 0.02 – 0.1 -

Endrin GC 0.01- 0.2 - - 0.005 - 0.025 0.003 – 0.1

EPN GC 0.01- 0.2 - - 0.005 - 0.025 0.01 – 0.1

Epoxyconazole LC 0.01- 0.2 - - 0.01- 0.05 0.01- 0.05

Esfenvalerate LC 0.01- 0.2 - - 0.05 – 0.5 0.01- 1

Ethiofencarb LC 0.05-1 - - 0.05 – 0.25 0.05 – 0.25

Ethiofencarb-sulfone LC 0.05-1 - - - 0.05 – 0.25

Ethiofencarb-sulfoxide LC 0.05-1 - - 0.05 – 0.25 0.05 – 0.25

Ethion LC 0.2 - - 0.01 – 0.05 0.01- 0.05

Ethirimol LC - - - - 0.01- 0.05

Ethofumesate LC 0.01- 0.2 - - 0.01 – 0.05 0.01- 0.05

Ethoprophos GC 0.01 -0.2 - - 0.005 - 0.025 0.003 – 0.1

Flexible Scope: Additional substances and new matrices may be added and ranges extended in accordance with the laboratory’s approved and

documented procedures. For details refer to the laboratory’s master list of flexible scope changes, available from the laboratory.

Edition 29, 13/04/2018 121T of 35



Category A


ANNEX 1

Pesticide

Instrument

Matrix

Food of

plant origin

Range mg/kg

Cereals

Range mg/kg

Milk

Range mg/kg

Food of Animal

Origin

Range mg/kg

Infant

Formula/Follow

on Formula

Range mg/kg

Etofenprox LC 0.01 - 0.2 - - 0.01 – 0.05 0.01 - 0.05

Etoxazole GC 0.01 - 0.2 0.01 - 0.1 - - 0.05 - 0.1

Etridazole GC 0.01 - 0.2 0.01 - 0.1 - 0.005 - 0.025 0.01 - 0.1

Etrimfos LC 0.01 - 0.2 0.01 - 0.05 - 0.01 -0.05 0.01 -0.05

Famoxadone LC 0.01 - 0.2 0.01 - 0.05 - 0.01 – 0.05 0.01 -0.05

Fenamidone GC 0.01 - 0.2 0.02 - 0.1 - 0.005 – 0.025 0.01 -0.1

Fenamiphos LC 0.01 - 0.2 0.01 - 0.05 - 0.01 -0.05 0.01 -0.05

Fenamiphos-sulfone LC 0.01 - 0.2 0.01 - 0.05 - - 0.01 -0.05

Fenamiphos-sulfoxide LC 0.01 - 0.2 0.01 - 0.05 - - 0.01 -0.05

Fenarimol GC 0.01 - 0.2 0.01 - 0.1 - 0.005 – 0.025 0.01 -0.1

Fenazaquin GC 0.01 - 0.2 0.01 - 0.1 - 0.005 – 0.025 0.01 -0.1

Fenbuconazole GC 0.01 - 0.2 0.01 - 0.1 - 0.005 – 0.025 0.01 -0.1

Fenchlorphos GC 0.01 - 0.2 0.01 - 0.1 0.005 0.025 0.005 – 0.025 0.01 -0.1

Fenhexamid LC 0.01 - 10 0.01 - 0.05 - 0.01 -0.05 0.01 -0.05

Fenitrothion GC 0.01 - 0.2 0.01 - 0.1 - 0.005 – 0.025 0.01 -0.1

Fenothiocarb LC 0.01 - 0.2 0.01 - 0.05 - - 0.01 -0.05

Fenoxaprop-P LC - 0.05 - 0.25 - - 0.05 - 0.25

Fenoxycarb LC 0.01 - 0.2 0.01 - 0.05 - 0.01 -0.05 0.01 -0.05

Fenpiclonil LC 0.01 - 0.2 0.01 - 0.05 - - 0.01 -0.05

Fenpropathrin GC 0.01 - 0.2 0.01 - 0.1 - 0.005 – 0.025 0.01 -0.1



Edition 29, 13/04/2018 121T of 35



Category A


ANNEX 1

Pesticide

Instrument

Matrix

Food of

plant origin

Range mg/kg

Cereals

Range mg/kg

Milk

Range mg/kg

Food of Animal

Origin

Range mg/kg

Infant

Formula/Follow

on Formula

Range mg/kg

Fenpropidin LC 0.01 -0.2 0.01 - 0.05 - 0.01 – 0.05 0.01 -0.05

Fenpropimorph LC 0.01 -0.2 0.01 - 0.05 - 0.01 – 0.05 0.01 -0.05

Fenpyroximate LC 0.01 -0.2 0.01 - 0.05 - 0.01 – 0.05 -

Fenthion LC 0.01 -0.2 - - 0.01 – 0.05 0.01 - 0.05

Fenthion Sulfone LC 0.01 -0.2 - - 0.01 – 0.05 0.01 - 0.05

Fenthion Sulfoxide LC - - - 0.01 – 0.05 0.01 - 0.05

Fenuron LC - 0.05 - 0.25 - - 0.05 - 0.25

Fenvalerate GC 0.01 -0.2 0.01 - 0.1 - 0.01 - 0.025 0.01 - 0.1

Fipronil LC 0.01 -0.2 0.01 - 0.05 - - 0.003 - 0.05

Fipronil desulfynil LC 0.01 -0.2 0.01 - 0.05 - - 0.003 - 0.05

Fipronil sulfide LC 0.01 -0.2 0.01 - 0.05 - - 0.003 - 0.05

Fipronil sulfone LC 0.01 -0.2 0.01 - 0.05 - - 0.003 - 0.05

Flamprop-isopropyl LC 0.01 -0.2 0.01 - 0.05 - 0.01 - 0.05 0.01 - 0.05

Flazasulfuron LC 0.01 -0.2 0.01 - 0.05 - - 0.01 - 0.05

Flonicamid LC - 0.01 - 0.05 - - 0.01 - 0.05

Florasulam LC 0.01 -0.2 0.01 - 0.05 - - 0.01 - 0.05

Fluazifop LC 0.02 -0.2 0.02 - 0.1 - - -

Fluazifop-P-butyl LC 0.01 -0.2 0.02 - 0.1 - - 0.02 - 0.1

Fluazinam LC 0.01 -0.2 0.02 - 0.1 - - 0.02 - 0.1

Flubendiamide LC - 0.01 - 0.05 - - 0.01 - 0.05



Edition 29, 13/04/2018 121T of 35



Category A


ANNEX 1

Pesticide

Instrument

Matrix

Food of

plant origin

Range mg/kg

Cereals

Range mg/kg

Milk

Range mg/kg

Food of Animal

Origin

Range mg/kg

Infant

Formula/Follow

on Formula

Range mg/kg

Flucycloxuron LC 0.01 - 0.2 - - - 0.01 - 0.05

Flucythrinate GC 0.01 - 0.2 0.01 - 0.1 - 0.005 – 0.025 0.01 - 0.1

Fludioxonil LC 0.01 – 5.0 0.01 - 0.05 - - 0.01 - 0.05

Fludioxonil GC 0.01 – 5.0 0.01 - 0.1 - 0.005 - 0.025 0.01 - 0.1

Flufenacet LC 0.01 - 0.2 0.01 - 0.05 - 0.01 - 0.05 0.01 - 0.05

Flufenoxuron LC 0.01 - 0.2 0.01 - 0.05 - 0.01 - 0.05 0.01 - 0.05

Fluopicolide LC 0.01 - 0.2 0.01 - 0.05 - - 0.01 - 0.05

Fluopyram LC - 0.02 - 0.1 - - 0.02 – 0.1

Fluquinconazole LC 0.01 - 0.2 0.01 - 0.05 - - -

Flurochloridone LC 0.01 - 0.2 0.01 - 0.05 - - 0.01 – 0.05

Flurtamone GC 0.01 - 0.2 0.01 - 0.1 - 0.005 – 0.025 0.01 – 0.1

Flusilazole GC 0.01 - 0.2 0.01 - 0.1 - 0.005 – 0.025 0.01 – 0.1

Flutolanil LC 0.01 - 0.2 0.01 - 0.05 - 0.01 – 0.05 0.01 – 0.05

Flutriafol LC 0.01 - 0.5 0.01 - 0.05 - 0.01 – 0.05 0.01 – 0.05

Fluvalinate-tau GC 0.01 - 0.2 0.01 - 0.1 - 0.005 – 0.025 0.01 – 0.1

Fluxapyroxad LC 0.01 - 0.2 0.01 - 0.05 - - 0.01 – 0.05

Fonofos GC 0.01 - 0.2 - 0.005 0.025 0.005 – 0.025 0.01 – 0.1

Forchlorfenuron LC 0.01 - 0.2 - - - 0.01 – 0.05

Formothion GC - - - 0.005 – 0.025 -

Fosthiazate LC - 0.01 - 0.05 - 0.01 – 0.05 0.01 – 0.05



Edition 29, 13/04/2018 121T of 35



Category A


ANNEX 1

Pesticide

Instrument

Matrix

Food of

plant origin

Range mg/kg

Cereals

Range mg/kg

Milk

Range mg/kg

Food of

Animal Origin

Range mg/kg

Infant

Formula/Follow

on Formula

Range mg/kg

Fuberidazole LC 0.01 - 0.2 0.01 - 0.05 - 0.01 – 0.05 0.01 – 0.05

Furalaxyl GC 0.01 - 0.2 0.01 - 0.1 - 0.005 - 0.025 0.01 – 0.1

Furathiocarb LC 0.01 - 0.2 0.01 - 0.05 - 0.01 – 0.05 0.01 – 0.05

Furmecyclox LC - - - - 0.01 – 0.05

Haloxyfop LC 0.02 – 0.2 0.02 - 0.1 - - -

Haloxyfop-methyl LC 0.01 - 0.2 0.02 - 0.1 - - 0.02 – 0.1

HCH-alpha GC 0.01 - 0.2 0.02 - 0.1 0.005 -0.025 0.005 -0.025

HCH-beta GC 0.01 - 0.2 0.02 - 0.1 0.005 -0.025 0.005 -0.025 0.01 – 0.1

HCH-delta GC 0.01 - 0.2 0.02 - 0.1 0.005 -0.025 0.005 -0.025 0.01 – 0.1

Heptachlor GC 0.01 - 0.2 0.02 - 0.1 0.005 -0.025 0.005 -0.025 0.003 – 0.1

Heptachlor endo-epoxide,trans

GC - - - 0.005 -0.025 0.003 – 0.1

Heptachlor exo-epoxide,cis

GC 0.01 – 0.2 0.01 - 0.1 0.005 -0.025 0.005 -0.025 -

Heptenophos LC 0.01 - 0.2 0.01 - 0.05 - 0.01 – 0.05 0.01 – 0.05

Hexachlorobenzene GC 0.01 - 0.2 0.01 - 0.1 0.005 -0.025 0.005 -0.025 0.003 – 0.1

Hexaconazole GC 0.01 - 0.2 0.01 - 0.1 - 0.005 -0.025 0.01 – 0.1

Hexaflumuron LC 0.01 - 0.2 0.01 - 0.05 - - 0.01 – 0.05

Hexythiazox LC 0.01 - 0.2 0.01 - 0.05 - 0.01 – 0.05 0.01 – 0.05

Imazalil LC 0.01 - 10 0.01 - 0.05 - - 0.01 – 0.05

Imazamox LC 0.01 – 0.2 0.01 - 0.05 - - -

Imidacloprid LC 0.01 – 0.5 0.01 - 0.05 - - 0.01 – 0.05



Edition 29, 13/04/2018 121T of 35



Category A


ANNEX 1

Pesticide

Instrument

Matrix

Food of

plant origin

Range mg/kg

Cereals

Range mg/kg

Milk

Range mg/kg

Food of Animal

Origin

Range mg/kg

Infant

Formula/Follow

on Formula

Range mg/kg

Indoxacarb LC 0.01 – 0.2 0.01 - 0.05 - 0.01 – 0.05 0.01 – 0.05

Iodofenphos GC 0.01 – 0.2 0.01 - 0.1 0.005 0.025 0.005 -0.025 -

Iodosulfuron-methyl LC 0.01 – 0.2 0.01 - 0.05 - - 0.01 - 0.05

Ioxynil LC 0.01 – 0.2 0.01 - 0.05 - - -

Iprodione GC 0.01 – 2.0 - - - 0.01 - 0.1

Iprovalicarb GC 0.01 – 0.2 0.01 - 0.1 - 0.005 – 0.025 0.05 - 0.1

Isazophos GC 0.01 – 0.2 0.01 - 0.1 - 0.005 – 0.025 0.01 - 0.1

Isocarbofos GC 0.01 – 0.2 0.01 - 0.1 - - -

Isodrin GC 0.01 – 0.2 0.01 - 0.1 - 0.005 – 0.025 0.01 - 0.1

Isofenphos LC 0.01 – 0.2 0.02 - 0.1 - 0.01 – 0.05 0.01 - 0.05

Isofenphos GC 0.01 – 0.2 0.01 - 0.1 - 0.005 – 0.025 0.01 - 0.1

Isofenphos-methyl GC 0.01 – 0.2 - - 0.005 – 0.025 0.01 - 0.1

Isofenphos-oxon GC - - - 0.005 - 0.025 -

Isoprocarb LC - 0.01 - 0.05 - 0.01 - 0.05 0.01 - 0.05

Isoprothiolane LC - 0.01 - 0.5 - - 0.01 - 0.05

Isoproturon LC 0.01 – 0.2 0.01 - 0.05 - 0.01 - 0.05 0.01 - 0.05

Kresoxim-methyl LC 0.01 – 2.0 0.01 - 0.05 - 0.01 - 0.05 0.01 - 0.05

Lenacil GC 0.01 – 0.2 0.01 - 0.1 - 0.005 - 0.025 0.01 - 0.1

Lindane GC 0.01 – 0.2 0.01 - 0.1 0.005 0.025 0.005 - 0.025 0.01 - 0.1

Linuron LC 0.01 – 0.2 0.01 - 0.05 - 0.01 - 0.05 0.01 - 0.05



Edition 29, 13/04/2018 121T of 35



Category A


ANNEX 1

Pesticide

Instrument

Matrix

Food of

plant origin

Range mg/kg

Cereals

Range mg/kg

Milk

Range

mg/kg

Food of Animal

Origin

Range mg/kg

Infant

Formula/Follow

on Formula

Range mg/kg

Lufenuron LC 0.01 - 0.2 0.01 - 0.05 - 0.01 - 0.05 0.01 - 0.05

Malaoxon LC 0.01 - 0.2 0.01 - 0.05 - 0.01 - 0.05 0.01 - 0.05

Malathion LC 0.01 - 0.2 0.01 - 0.05 - 0.01 - 0.05 0.01 - 0.05

Mandipropamid LC - 0.01 - 0.05 - - 0.01 - 0.05

MCPA LC 0.02 - 0.2 - - - -

MCPA methyl ester GC 0.01 - 0.2 - - 0.005 – 0.025 0.01 - 0.1

MCPB LC 0.01 - 0.2 0.01 - 0.05 - - -

Mecarbam GC 0.01 - 0.2 0.01 - 0.1 - 0.005 - 0.025 0.01 - 0.1

Mecoprop LC 0.01 - 0.2 0.01 - 0.05 - - -

Mefenpyr-Diethyl LC 0.01 - 0.2 0.01 - 0.05 - - 0.01 - 0.05

Mepanipyrim LC 0.01 - 1 0.01 - 0.05 - 0.01 - 0.05 0.01 - 0.05

Mephosfolan LC 0.01 - 0.2 0.01 - 0.05 - - 0.01 - 0.05

Mepronil LC 0.01 - 0.2 0.01 - 0.05 - 0.01 - 0.05 0.01 - 0.05

Mesosulfuron methyl LC 0.01 - 0.2 0.01 - 0.05 - - 0.01 - 0.05

Metalaxyl LC 0.01 - 0.5 0.01 - 0.05 - 0.01 - 0.05 0.01 - 0.05

Metamitron LC 0.01 - 0.2 0.01 - 0.05 - - 0.01 - 0.05

Metazachlor LC 0.01 - 0.2 0.01 - 0.05 - 0.01 - 0.05 0.01 - 0.05

Metconazole LC 0.01 - 0.2 0.01 - 0.05 - 0.01 – 0.05 0.01 - 0.05

Methacrifos GC 0.01 - 0.2 0.01 - 0.1 - 0.005 – 0.025 0.01 - 0.1

Methamidophos LC - 0.01 - 0.05 - - 0.01 – 0.05

Methamidophos GC - 0.01 - 0.1 - - 0.01 – 0.1



Edition 29, 13/04/2018 121T of 35



Category A


ANNEX 1

Pesticide

Instrument

Matrix

Food of

plant origin

Range mg/kg

Cereals

Range mg/kg

Milk

Range mg/kg

Food of Animal

Origin

Range mg/kg

Infant

Formula/Follo

w on Formula

Range mg/kg

Methidathion LC 0.01 - 0.2 0.01 - 0.05 - 0.01 - 0.05 0.01 - 0.05

Methiocarb LC 0.01 - 0.2 - - 0.01 - 0.05 0.01 - 0.05

Methomyl LC - 0.01 - 0.05 - - 0.01 - 0.05

Methoprene LC 0.01 - 0.2 - - - 0.01 - 0.05

Methoxychlor GC 0.01 - 0.2 0.01 - 0.1 0.005 - 0.025 0.005 – 0.025 -

Methoxyfenozide LC 0.01 - 0.2 0.01 - 0.05 - 0.01 - 0.05 0.01 - 0.05

Metobromuron LC 0.01 - 0.2 0.01 - 0.05 - 0.01 - 0.05 0.01 - 0.05

Metolachlor LC 0.01 - 0.2 0.01 - 0.05 - 0.01 - 0.05 0.01 - 0.05

Metosulam LC 0.01 - 0.2 0.01 - 0.05 - - 0.01 - 0.05

Metoxuron LC 0.01 - 0.2 0.01 - 0.05 - - 0.01 - 0.05

Metrafenone LC 0.01 - 0.2 0.01 - 0.05 - - 0.01 - 0.05

Metribuzin GC 0.01 - 0.2 0.01 - 0.1 - 0.005 – 0.025 0.01 - 0.1

Metsulfuron-methyl LC 0.01 - 0.2 0.01 - 0.05 - - 0.01 - 0.05

Mevinphos GC 0.01 - 0.2 0.01 - 0.1 0.02 - 0.1 0.005 – 0.025 0.01 - 0.1

Mirex GC 0.01 - 0.2 0.01 - 0.1 - 0.005 - 0.025 0.01 - 0.1

Molinate GC 0.01 - 0.2 - - 0.005 – 0.025 0.01 - 0.1

Molinate LC - 0.01 - 0.05 - - -

Monocrotophos LC 0.01 - 0.2 0.01 - 0.05 - - 0.02 - 0.1

Monolinuron LC 0.01 - 0.2 0.02 - 0.1 - - 0.02 - 0.1

Myclobutanil LC 0.01 - 0.5 0.02 - 0.1 - - 0.02 - 0.1



Edition 29, 13/04/2018 121T of 35



Category A


ANNEX 1

Pesticide

Instrument

Matrix

Food of

plant origin

Range mg/kg

Cereals

Range mg/kg

Milk

Range mg/kg

Food of Animal

Origin

Range mg/kg

Infant

Formula/Follow

on Formula

Range mg/kg

Napropamide LC 0.01 - 0.2 0.01 - 0.05 - 0.01 - 0.05 0.01 - 0.05

Naptalam LC 0.01 - 0.2 - - - -

Neburon LC 0.01 - 0.2 0.02 - 0.1 - - 0.02 - 0.05

Nicosulfuron LC 0.01 - 0.2 0.02 - 0.1 - - -

Nitenpyram LC - 0.01 - 0.05 - - 0.01 - 0.05

Nitrofen GC - 0.01 - 0.1 - 0.005 - 0.025 -

Nonachlor-trans GC 0.01 - 0.2 0.01 - 0.1 - 0.005 - 0.025 0.01 - 0.1

Nuarimol GC 0.01 - 0.2 0.01 - 0.1 - 0.005 - 0.025 0.01 - 0.1

Omethoate GC 0.01 - 0.2 0.01 - 0.1 - 0.005 - 0.025 -

o-Phenylphenol GC 0.01 - 10 - - 0.005 - 0.025 0.01 - 0.1

Oxadiazon LC 0.01 - 0.05 0.01 - 0.1 - - -

Oxadixyl GC - 0.01 - 0.05 - - 0.01 - 0.1

Oxamyl LC 0.01 - 0.2 0.01 - 0.05 - - 0.01 - 0.05

Oxamyl Oxime LC 0.01 - 0.2 0.01 - 0.1 - - 0.01 - 0.05

Oxychlordane GC 0.01 - 0.2 0.01 - 0.5 - 0.005 - 0.025 -

Oxyfluorfen LC - 0.01 - 0.5 - - 0.01 - 0.05

Paclobutrazol LC 0.01 - 0.2 0.01 - 0.05 - 0.01 - 0.05 0.01 - 0.05

Paraoxon methyl GC - 0.01 - 0.1 - 0.005 - 0.025 0.01 - 0.1

Paraoxon-ethyl LC 0.01 - 0.2 0.01 - 0.05 - 0.01 - 0.05 0.01 - 0.05

Parathion-ethyl GC 0.01 - 0.2 0.01 - 0.1 0.01 - 0.1 0.01 - 0.05 0.01 - 0.05



Edition 29, 13/04/2018 121T of 35



Category A


ANNEX 1

Pesticide

Instrument

Matrix

Food of

plant origin

Range mg/kg

Cereals

Range mg/kg

Milk

Range mg/kg

Food of

Animal Origin

Range mg/kg

Infant

Formula/Follow

on Formula

Range mg/kg

Parathion-methyl GC 0.01 - 0.2 0.01 - 0.1 0.01 - 0.05 0.01 - 0.025 0.01 - 0.05

PCB 101 GC 0.005 - 0.05 0.01 - 0.05 0.005 - 0.025 0.01 - 0.05

PCB 118 GC 0.005 - 0.05 0.01 - 0.05 0.005 - 0.025 0.01 - 0.05

PCB 138 GC - 0.005 - 0.05 0.01 - 0.05 0.005 - 0.025 0.01 - 0.05

PCB 153 GC - 0.005 - 0.05 0.01 - 0.05 0.005 - 0.025 0.01 - 0.05

PCB 180 GC - 0.005 - 0.05 0.01 - 0.05 0.005 - 0.025 0.01 - 0.05

PCB 28 GC - 0.005 - 0.05 0.01 - 0.05 0.005 - 0.025 0.01 - 0.05

PCB 52 GC - 0.005 - 0.05 0.01 - 0.05 0.005 - 0.025 0.01 - 0.05

Penconazole LC 0.01 - 0.2 0.01 - 0.05 - 0.01 - 0.05 0.01 - 0.05

Pencycuron LC 0.01 - 0.2 0.01 - 0.05 - 0.01 - 0.05 0.01 - 0.05

Pendimethalin GC 0.01 - 0.2 0.01 - 0.1 - 0.01 - 0.05 0.01 - 0.1

Pentachloroaniline GC - 0.01 - 0.1 - 0.01 - 0.05 -

Permethrin GC 0.01 - 0.5 0.01 - 0.1 0.01 - 0.05 0.01 - 0.44 0.01 - 0.1

Pethoxamid LC 0.01 - 0.2 0.01 - 0.05 - 0.01 - 0.1

Phenmedipham LC - 0.01 - 0.05 - 0.01 - 0.05 0.01 - 0.05

Phenthoate GC 0.01 - 0.2 0.01 - 0.1 - 0.005 - 0.025 0.01 - 0.1

Phorate Sulfoxide LC 0.01 - 0.2 - - 0.01 - 0.05 0.01 - 0.05

Phosalone GC 0.01 - 0.2 0.01 - 0.1 0.005 - 0.025 0.005 - 0.025 0.01 - 0.1

Phosmet GC 0.01 - 0.2 0.01 - 0.1 - 0.005 - 0.025 -

Phosphamidon GC 0.01 - 0.2 0.01 - 0.1 - 0.005 - 0.025 0.01 - 0.1



Edition 29, 13/04/2018 121T of 35



Category A


ANNEX 1

Pesticide

Instrument

Matrix

Food of

plant origin

Range mg/kg

Cereals

Range mg/kg

Milk

Range mg/kg

Food of

Animal Origin

Range mg/kg

Infant

Formula/Follow

on Formula

Range mg/kg

Phoxim LC - - - 0.01 - 0.05 0.01 - 0.05

Picoxystrobin LC 0.01 - 0.2 0.01 - 0.05 - 0.01 - 0.05 0.01 - 0.05

Piperonyl butoxide LC 0.01 - 0.2 0.01 – 5.0 - 0.01 - 0.05 0.01 - 0.05

Pirimicarb GC 0.01 - 2 - - 0.005 - 0.025 0.01 - 0.1

Pirimicarb desmethyl GC - 0.01 - 0.1 - 0.005 - 0.025

Pirimiphos-ethyl LC 0.01 - 0.2 0.01 - 0.05 - 0.01 – 0.05 0.01 – 0.05

Pirimiphos-methyl LC 0.01 - 0.5 0.01 - 0.5 - 0.01 - 0.05 0.01 - 0.05

Prochloraz GC 0.01 - 2 0.01 - 0.1 - 0.005 - 0.025 0.01 - 0.1

Procymidone GC 0.01 - 0.2 0.01 - 0.1 - 0.005 - 0.025 0.01 - 0.1

Profenofos GC 0.01 - 0.2 0.01 - 0.1 - 0.005 - 0.025 0.01 - 0.1

Promecarb LC 0.01 - 0.2 0.01 - 0.05 - - 0.01 - 0.05

Promethryn LC 0.01 - 0.2 0.01 - 0.05 - 0.01 - 0.05 0.01 - 0.05

Prometon LC 0.01 - 0.2 0.01 - 0.05 - - 0.01 - 0.05

Propachlor GC 0.01 - 0.2 0.01 - 0.1 - 0.005 - 0.025 0.01 - 0.1

Propamocarb LC - - - - 0.01 - 0.05

Propanil GC 0.01 - 0.2 0.01 - 0.1 - 0.005 - 0.025 0.01 - 0.1

Propaquizafop LC 0.01 - 0.2 0.01 - 0.05 - - 0.01 - 0.05

Propargite GC 0.01 - 0.2 0.01 - 0.1 - 0.005 - 0.025 0.01 - 0.1

Propazine LC 0.01 - 0.2 0.01 - 0.05 - - 0.01 - 0.05

Propetamphos GC 0.01 - 0.2 0.01 - 0.1 0.005 - 0.025 0.005 - 0.025 0.01 - 0.1



Edition 29, 13/04/2018 121T of 35



Category A


ANNEX 1

Pesticide

Instrument

Matrix

Food of

plant origin

Range mg/kg

Cereals

Range mg/kg

Milk

Range mg/kg

Food of Animal

Origin

Range mg/kg

Infant

Formula/Follow

on Formula

Range mg/kg

Propham GC 0.01 - 0.2 0.01 - 0.1 - 0.005 - 0.025 0.01 - 0.1

Propiconazole GC 0.01 – 5.0 0.01 - 0.1 - 0.005 - 0.025 -

Propoxur LC 0.01 - 0.2 0.01 - 0.05 - 0.01 - 0.05 0.01 - 0.05

Propoxycarbazone LC - 0.01 - 0.05 - - 0.01 - 0.05

Propyzamide LC 0.01 - 0.2 0.01 - 0.05 - 0.01 - 0.05 0.01 - 0.05

Proquinazid LC 0.01 – 0.2 0.01 - 0.05 - - 0.01 - 0.05

Prosulfocarb LC 0.05 - 1 0.05 – 1 - - 0.01 - 0.05

Prosulfuron LC 0.01 - 0.2 0.01 - 0.05 - - 0.01 - 0.05

Prothioconazole desthio

LC - 0.01 - 0.05 - - 0.01 - 0.05

Prothiofos GC 0.01 - 0.2 0.01 - 0.1 - 0.005 - 0.025 0.01 - 0.1

Pymetrozine LC 0.02 - 0.2 0.02 - 0.1 - - 0.02 - 0.1

Pyraclostrobin LC 0.01 - 0.5 0.01 - 0.05 - - 0.01 - 0.05

Pyrazophos LC 0.01 - 0.2 0.01 - 0.05 - 0.01 - 0.05 0.01 - 0.05

Pyrethrins LC - 0.01 - 0.25 - 0.01 - 0.05 0.01 - 0.05

Pyridaben LC 0.01 - 0.2 0.01 - 0.05 - 0.01 - 0.05 0.01 - 0.05

Pyridaben GC 0.01 - 0.2 0.01 - 0.1 - 0.01 – 0.1 0.01 - 0.1

Pyridaphenthion LC 0.01 - 0.2 0.01 - 0.05 - 0.01 - 0.05 0.01 - 0.05

Pyrifenox GC 0.02 - 0.1 0.02 - 0.2 - 0.02 – 0.1 -

Pyrimethanil LC 0.01 – 10 0.01 - 0.05 - 0.01 - 0.05 0.01 - 0.05

Pyriproxifen LC 0.01 – 0.2 0.01 - 0.05 - 0.01 - 0.05 0.01 - 0.05



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Category A


ANNEX 1

Pesticide

Instrument

Matrix

Food of

plant origin

Range mg/kg

Cereals

Range mg/kg

Milk

Range mg/kg

Food of

Animal Origin

Range mg/kg

Infant

Formula/Follow

on Formula

Range mg/kg

Quinalphos LC 0.01 - 0.2 0.01 - 0.05 - 0.01 - 0.05 0.01 - 0.05

Quinoxyfen LC 0.01 - 0.2 0.01 - 0.05 - 0.01 - 0.05 0.01 - 0.05

Quintozene GC 0.01 - 0.2 0.01 - 0.1 0.005 - 0.025 0.005 - 0.025 0.01 - 0.05

Quizalofop LC 0.02 - 0.2 0.02 - 0.1 - - -

Quizalofop-ethyl LC 0.01 - 0.2 0.02 - 0.1 - - 0.02 - 0.1

Resmethrin GC - 0.1 - 1 - 0.1 - 1 -

Rimsulfuron LC 0.01 - 0.2 - - - 0.02 - 0.1

Rotenone LC 0.01 - 0.2 0.01 - 0.05 - 0.01 - 0.05 0.01 - 0.05

Silthiofam GC - 0.01 - 0.1 - 0.005 - 0.025 -

Simazine LC 0.01 - 0.2 0.01 - 0.05 - - 0.01 - 0.05

Simetryn LC 0.01 - 0.2 0.01 - 0.05 - - 0.01 - 0.05

Spinosyn A LC 0.01 - 10 0.01 - 0.05 - - 0.01 - 0.05

Spinosyn D LC 0.01 - 10 0.01 - 0.05 - - 0.01 - 0.05

Spirodiclofen LC 0.01 - 0.2 - - - -

Spirodiclofen GC 0.01 – 0.2 - - 0.005 - 0.025 0.01 - 0.1

Spiromesifen LC - 0.01 - 0.05 - - 0.01 - 0.05

Spirotetramat LC 0.01 - 0.5 0.01 - 0.05 - - 0.01 - 0.05

Spiroxamine LC 0.01 - 0.2 - - 0.01 - 0.05 0.01 - 0.05

Sulfentrazone LC 0.01 - 0.2 0.01 - 0.05 - - 0.02 - 0.1

Sulfotep LC 0.01 - 0.2 0.01 - 0.05 - - 0.01 - 0.05



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Category A


ANNEX 1

Pesticide

Instrument

Matrix

Food of

plant origin

Range mg/kg

Cereals

Range mg/kg

Milk

Range mg/kg

Food of Animal

Origin

Range mg/kg

Infant

Formula/Follow

on Formula

Range mg/kg

Sulprofos LC - - - - 0.01 - 0.05

Tebuconazole LC 0.01 - 1 0.01 - 0.05 - 0.01 - 0.05 0.01 - 0.05

Tebufenozide LC 0.01 - 0.2 0.01 - 0.05 - 0.01 - 0.05 0.01 - 0.05

Tebufenpyrad LC 0.01 - 0.2 0.01 - 0.05 - 0.01 – 0.05 0.01 - 0.05

Tecnazene GC 0.01 - 0.2 0.01 - 0.1 0.005 0.025 0.005 – 0.025 0.01 - 0.1

Teflubenzuron LC 0.01 - 0.2 0.01 - 0.05 - - 0.01 - 0.05

Tefluthrin GC - 0.02 - 0.2 - 0.005 – 0.025 -

Terbumeton LC 0.01 - 0.2 0.01 - 0.05 - - 0.01 - 0.05

Terbuthylazine LC 0.01 - 0.2 0.01 - 0.05 - 0.01 - 0.05 0.01 - 0.05

Terbuthylazine-2-hydroxy

LC - - - - 0.01 - 0.05

Terbuthylazine-desethyl

LC 0.01 - 0.2 0.01 - 0.05 - - 0.01 - 0.05

Terbutryn LC 0.01 - 0.2 0.01 - 0.05 - - 0.01 - 0.05

Tetraconazole GC 0.01 - 0.2 0.01 - 0.1 - 0.005 – 0.025 0.01 - 0.1

Tetradifon GC 0.01 - 0.2 0.01 - 0.1 - 0.005 – 0.025 0.01 - 0.1

Tetramethrin GC 0.02 - 0.4 0.02 -0.4 - 0.005 – 0.025 -

Thiabendazole LC 0.01 - 5 0.01 - 0.05 - 0.01 - 0.05 0.01 - 0.05

Thiacloprid LC 0.02 - 0.2 0.02 - 0.1 - - 0.02 - 0.1

Thiamethoxam LC 0.01 - 0.2 0.01 - 0.05 - - 0.01 - 0.05

Thifensulfuron-methyl LC 0.05 - 0.2 0.01 - 0.05 - - 0.01 - 0.05

Thiobencarb LC 0.01 - 0.2 0.01 - 0.05 - - 0.01 - 0.05



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Category A


ANNEX 1

Pesticide

Instrument

Matrix

Food of

plant origin

Range mg/kg

Cereals

Range mg/kg

Milk

Range mg/kg

Food of Animal

Origin

Range mg/kg

Infant

Formula/Follow

on Formula

Range mg/kg

Thiodicarb LC - 0.01 - 0.05 - - 0.01 - 0.05

Thionazin LC 0.02 - 0.2 0.01 - 0.05 - - 0.01 - 0.05

Tolclofos-methyl GC 0.01 - 0.2 0.01 - 0.1 - 0.005 – 0.025 0.01 - 0.1

Tolyfluanid GC 0.01 - 0.2 - - 0.005 – 0.025 0.01 - 0.1

Triadimefon GC 0.01 - 0.5 0.01 - 0.1 - 0.005 – 0.025 0.01 - 0.1

Triadimenol GC 0.01 - 0.5 0.01 - 0.1 - 0.005 – 0.025 0.01 - 0.1

Tri-Allat LC 0.01 - 0.2 0.01 - 0.05 - - 0.01 - 0.05

Triasulfuron LC 0.01 - 0.2 0.01 - 0.05 - - 0.01 - 0.05

Triazophos LC 0.01 - 0.2 0.01 - 0.05 - 0.005 – 0.025 0.01 - 0.05

Triclopyr LC - 0.01 – 0.05 - - -

Tricyclazole LC - 0.01 - 0.05 - - 0.01 - 0.05

Trifloxystrobin LC 0.01 - 0.5 0.01 - 0.05 - 0.01 - 0.05 0.01 - 0.05

Triflumizole LC 0.02 – 0.2 0.02 – 0.1 - 0.02 - 0.1 0.01 - 0.05

Triflumizole GC 0.02 - 0.2 0.02 – 0.1 - 0.02 - 0.1 0.01 - 0.05

Triflumuron LC 0.01 - 0.49 0.01 - 0.05 - - 0.01 - 0.05

Trifluralin GC 0.01 - 0.2 0.01 - 0.1 - 0.005 - 0.025 0.01 - 0.1

Triflusulfuron-methyl LC 0.01 - 0.2 0.01 - 0.05 - - -

Triticonazole LC 0.01 - 0.2 0.01 - 0.05 - 0.01 - 0.05 0.01 - 0.05

Vamidothion LC 0.01 - 0.2 0.01 - 0.05 - 0.01 - 0.05 0.01 - 0.05

Vinclozolin GC 0.01 - 0.2 0.01 - 0.1 - 0.005 - 0.025 0.01 - 0.05

Zoxamide LC 0.01 - 0.2 0.01 - 0.05 - 0.01 - 0.05 0.01 - 0.05



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Category A


ANNEX 2

Quantitation of active substance in plant protection products.

GC-FID & LC-DAD

Pesticide Range % Pesticide Range % Pesticide Range %

Abamectin 0.1-100 Chlorpropham 0.1-100 Difenoconazole 0.1-100

Acetamiprid 0.1-100 Chlorpyrifos 0.1-100 Diflufenican 0.1-100

alpha-Cypermethrin 0.1-100 Chlorpyrifos-methyl 0.1-100 Dimethenamid-P 0.1-100

Amidosulfuron 0.1-100 Clodinafop 0.1-100 Dimethoate 0.1-100

Aminopyralid 0.1-100 Chlomazone 0.1-100 Dimethomorph 0.1-100

Amisulbrom 0.1-100 Clopyralid 0.1-100 Dimoxystrobin 0.1-100

Asulam 0.1-100 Cloquintocet-mexyl 0.1-100 Diquat (dibromide) 0.1-100

Azoxystrobin 0.1-100 Clothianidin 0.1-100 Diuron 0.1-100

Bentazone 0.1-100 Cyazofamid 0.1-100 Dodine 0.1-100

Bendiovalicarb-isopropyl 0.1-100 Cycloxydim 0.1-100 Epoxiconazole 0.1-100

Bifenthrin 0.1-100 Cymoxanil 0.1-100 Esfenvalerate 0.1-100

Bixafen 0.1-100 Cypermethrin 0.1-100 Ethamesulfuron-me 0.1-100

Boscalid 0.1-100 Chloralose 0.1-100 Ethofumesate 0.1-100

Bromadiolone 0.1-100 Cyproconazole 0.1-100 Fenpropidin 0.1-100

Bromoxynil 0.1-100 Cyprodinil 0.1-100 Fenpropimorph 0.1-100

Bupirimate 0.1-100 d-Phenotrin 0.1-100 Fenamidone 0.1-100

Carbendazim 0.1-100 Daminozide 0.1-100 Fenhexamid 0.1-100

Carfentrazone-ethyl 0.1-100 Deltamethrin 0.1-100 Fenoxaprop-P (ethyl) 0.1-100

Chloridazon 0.1-100 Desmedipham 0.1-100 Flazasulfuron 0.1-100

Chlorfenapyr 0.1-100 Dicamba 0.1-100 Flonicamid 0.1-100

Chlormequat 0.1-100 Dichlobenil 0.1-100 Florasulam 0.1-100

Chlorothalonil 0.1-100 Difenacoum 0.1-100 Fluazinam 0.1-100

Flexible Scope: Additional substances and may be added an extended in accordance with the laboratory’s approved and documented

procedures. For details refer to the laboratory’s master list of flexible scope changes, available from the laboratory.

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Category A


ANNEX 2


GC-FID & LC-DAD


Fluazifop-P-butyl 0.1-100 Ioxynil 0.1-100 Metconazole 0.1-100

Fludioxonil 0.1-100 Iprodione 0.1-100 Methiocarb 0.1-100

Flufenacet 0.1-100 Isoproturon 0.1-100 Metrafenone 0.1-100

Flumioxazin 0.1-100 Isopyrazam 0.1-100 Metribuzin 0.1-100

Fluopicolide 0.1-100 Isoxaben 0.1-100 Metsulfuron (-methyl) 0.1-100

Fluoxastrobin 0.1-100 Isoxaflutole 0.1-100 Myclobutanil 0.1-100

Flupyrsulfuron Methyl 0.1-100 Kresoxim Methyl 0.1-100 Nicosulfuron 0.1-100

Fluroxypyr 0.1-100 lambda-Cyhalothrin 0.1-100 Octanoate 0.1-100

Flusilazole 0.1-100 Lenacil 0.1-100 Oxadiazon 0.1-100

Flutolonil 0.1-100 Linuron 0.1-100 Oxyfluorfen 0.1-100

Fluxapyroxad 0.1-100 Malathion 0.1-100 Paclobutrazol 0.1-100

Folpet 0.1-100 MCPA 0.1-100 Pencycuron 0.1-100

Fosetyl (-aluminium) 0.1-100 Mecoprop 0.1-100 Pendimethalin 0.1-100

Fosthiazate 0.1-100 Mecoprop-P 0.1-100 Penthiopyrad 0.1-100

Glufosinate (- ammonium)

0.1-100 Mefenpyr Diethyl 0.1-100 Permethrin 0.1-100

Glyphosate 0.1-100 Mepiquat Chloride 0.1-100 Phenmedipham 0.1-100

Imazalil 0.1 -100 Mesosulfuron - Methyl 0.1-100 Picolinafen 0.1-100

Imidacloprid 0.1-100 Mesotrione 0.1-100 Picoxystrobin 0.1-100

Imazamox 0.1-100 Metalaxyl M 0.1-100 Pinoxaden 0.1-100

Imazaquin 0.1-100 Metaldehyde 0.1-100 Piperonyl butoxide 0.1-100

Indoxacarb 0.1-100 Metamitron 0.1-100 Pirimicarb 0.1-100

Iodosulfuron-methyl-sodium

0.1-100 Metazachlor 0.1-100 Pirimiphos-me 0.1-100

Flexible Scope: Additional substances may be added and ranges extended in accordance with the laboratory’s approved

and documented procedures. For details refer to the laboratory’s master list of flexible scope changes, available from the

laboratory.

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Category A


ANNEX 2


GC-FID & LC-DAD


Prochloraz 0.1-100 Spiroxamine 0.1-100 Fluroxypyr-1-methyl

heptyl ester 0.1-100

Prodiamine 0.1-100 Spirotetramat 0.1-100 MCPB 0.1-100

Prohexadione Calcium 0.1-100 Sulfentrazone 0.1-100 Trisulfuron-methyl 0.1-100

Propamocarb 0.1-100 Sulfosulfuron 0.1-100 Picloram 0.1-100

Propaquizafop 0.1-100 Tebuconazole 0.1-100 Fluopyram 0.1-100

Propiconazole 0.1-100 Tepraloxydim 0.1-100 Halauxifen Methyl 0.1-100

Propyzamide 0.1-100 Terbutylazine 0.1-100 Maleic Hydrazide 0.1-100

Proquinazid 0.1-100 Thiabendazole 0.1-100 Triclopyr 0.1-100

Prosulfocarb 0.1-100 Thiacloprid 0.1-100 Triclopyr butoxyethyl

ester (BEE)

0.1-100

Prothioconazole 0.1-100 Thiamethoxan 0.1-100

Pymetrozine 0.1-100 Thifensulfuron (-

methyl) 0.1-100

Pyraclostrobin 0.1-100 Thiophanate-methyl 0.1-100

Pyrethrins 0.1-100 Tralkoxydim 0.1-100

Pyridate 0.1-100 Tribenuron (-methyl) 0.1-100

Pyrimethanil 0.1-100 Trifloxystrobin 0.1-100

Pyraflufen-Ethyl 0.1-100 Trifluralin 0.1-100

Pyroxsulam 0.1-100 Trinexapac ethyl 0.1-100

Quinmerac 0.1-100 Triticonazole 0.1-100

Quizalofop-P-ethyl 0.1-100 2,4-DB 0.1-100

Rimsulfuron 0.1-100 2,4 D 0.1-100

Silthiofam 0.1-100 2,4-D-ethyl hexyl ester 0.1-100

Spinosad 0.1-100

Flexible Scope: Additional substances may be added and ranges extended in accordance with the laboratory’s approved

and documented procedures. For details refer to the laboratory’s master list of flexible scope changes, available from the

laboratory.

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Category A


ANNEX 3

List of Quaternary ammonium salts and other pesticides SOP 113

Pesticide Instrument

Fruit and

Vegetables Range mg/kg

Cereals Range mg/kg

Chlormequat LC 0.01 – 0.1 0.02 – 10

Cyromazine LC 0.02 – 0.1 0.02 – 0.2

Daminozide LC 0.01 – 0.1 0.02 – 0.2

Mepiquat LC 0.01 – 0.1 0.02 – 0.5

Paraquat LC 0.10 – 1.0 0.05 – 0.2

Flexible Scope: Additional substances may be added and ranges extended in accordance with the laboratory’s approved and documented procedures. For details refer to the laboratory’s master list of flexible scope changes, available from the laboratory.

ANNEX 4

List of Glyphosate and Co Compounds SOP 116


Cereals

Range mg/kg

AMPA (metabolite of Glyphosate) LC

0.08 – 0.3

Ethephon LC 0.04 – 0.3

Glufosinate LC 0.08 – 0.3

N-acetyl Glufosinate (metabolite of Glufosinate) LC

0.08 – 0.3

Glyphosate LC 0.08 - 0.8

Flexible Scope: Additional substances may be added and ranges extended in accordance with the laboratory’s approved and documented procedures. For details refer to the laboratory’s master list of flexible scope changes, available from the laboratory.

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Category A


ANNEX 5

Dithiocarbamates SOP 110


Fruit and Vegetables

Range mg/kg

Cereals

Range mg/kg

Infant

Formula/Follow On Formula

Range mg/kg

Dithiocarbamates (as CS2) LC

0.05 - 2 0.05 – 2 0.05 – 2

Flexible Scope: Additional matrices may be added and ranges extended in accordance with the laboratory’s approved and documented procedures. For details refer to the laboratory’s master list of flexible scope changes, available from the laboratory.

ANNEX 6

Amitraz and its Metabolites SOP 114

Amitraz and Metabolites Instrument

Fruit, Vegetables and Honey Range mg/kg

Amitraz LC 0.01 – 0.1

DMF LC 0.01 – 0.1

DMPF LC 0.01 – 0.1

Flexible Scope: Additional matrices may be added and ranges extended in accordance with the laboratory’s approved and documented procedures. For details refer to the laboratory’s master list of flexible scope changes, available from the laboratory.

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