performance and appearance of packaging grades of paper study on quality measurement methods author...
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Performance and Appearance of packaging grades of paper Study on quality measurement methods
Author and Presenter:
Manoj SukumaranManager – Lorentzen and Wettre ProductsABB India Limited
Presented at IPPTA Workshop on 10th December 2015
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World packaging material consumption
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World paper and board packaging consumption by region
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Performance of a Corrugated board BoxPractical considerations…• A corrugated-board box is intended to be filled with contents
which will to a greater or lesser extent exert forces on the insides of the box so that these tend to bend outwards.
• The load will act for a long period of time.
• During transport the box will be exposed to vibrations and shock loads.
• The corrugated-board box will in all probability be exposed to different atmospheric conditions.
• The load in a stack in a storeroom is probably not as uniform as in a compression tester.
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Notations used in Corrugated board
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Flute types and dimensions
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Structure of Corrugated Board Box
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Liner and Fluting Medium in use worldwide
* Natural kraft linerboard – Mainly unbleached kraft fibre, some recycled content allowed* White top linerboard – Bleached top layer on an unbleached base layer* Testliner – Top layer and base layer made from 100 % recycled fibres* Other recycled liner– Mainly kraft top layer, which is a natural kraft layer on a recycled base layer* Recycled medium – 100 % recycled fluting * Semi-chemical medium – Contains mostly NSSC hardwood and/or softwood (NSSC= Neutral Sulphite Semi-Chemical pulp. Produced by defibration in a disc refiner.)
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Testing of components
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McKee Formula for Box Compression strength (BCT)
BCT = k1 × (ECT b)0.75 × (SbB )0.25×Z0.5.
•ECT is the edgewise crush resistance of the corrugated board, the value in kN/m
•SbB is the geometric mean given by
SbB = √Sb
B MD x SbB CD
where SB,MD and SB,CD are the bending stiffness in the machine and cross-machine directions of the corrugated board, in Nm•The periphery of the box, Z in m.
McKee found the formula useful if the relationship of
depth/periphery is > 1/7 (0.143)
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Simplified McKee formula
BCT = k2 × ECTb × T0.5 × Z0.5
•In the simplified equation, the bending stiffness is replaced by the thickness of the corrugated board T.
The theoretical background is that the bending stiffness of corrugated board to a very great extent is influenced by the distance from the neutral bending center line of the sheet to the centers of the surface liners, i.e. roughly the thickness of the board
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Stress distribution along the edges of a corrugated board box
The corners take higher load than the sides. Failure of the vertical edge at corners lead to breakdown of the Box
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Edgewise Compression Test (ECT)according to FPL method
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The relationship between the ECT- value and the compression strengths of liner and fluting medium can in general be written as:
ECTb = k (σbC,L1 + σb
C, L2 + α σbC,F)
Where σbC is the compression strength, L1= liner1, L2= Liner 2…F= fluting
medium, α = flute take up factor and k is a constant
The value of k was determined by SCA depending on the method used for measuring compression strength of the liner and medium and published as:
•RCT 1.28 ± 0.08
•CCT 0.97 ± 0.04
•SCT 0.71± 0.03
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Short-span Compression Test (SCT)
In the measurement of the compression strength of liner and fluting medium according to the “short (span) compression test” method (SCT), the paper sample is placed between two clamps with a 0.7 mm free clamping length. When the clamps are moved towards each other, the length is reduced and the stresses in the strip increase. Since the sample is short in relation to its thickness, the slenderness ratio is low and buckling is prevented. Consequently failure occurs due to compression
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Ring Crush Test (RCT)
In the Ring Crush Test (RCT) method, the test strip is formed into a ring when it is inserted into an annular gap in a special holder. The width of the gap is adapted to the thickness of the test sample by using discs of different diameters. The great disadvantage of the RCT test is the buckling which occurs especially at the ends of the ring-formed test piece
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Concora Crush Test (CCT) and Concora Linear Test (CLT)
In the Corrugated Crush Test (CCT), or Concora Corrugated Test method, the test strip is first corrugated in a laboratory corrugator, after which it is clamped vertically into a jig having the same profile as the rollers of the corrugatorIn the Crush Linear Test (CLT) or Concora Liner Test method, a straight test strip is held in a vertical position in a special holder.
CCT CLT
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Comparison of different Compression methods
The relative ranking of the methods is clearly evident. The CLT- and RCT-methods in particular show strongly increasing values with increasing grammage, which must indicate that at low grammages failure has arisen through buckling and not through compression failure as was intended
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Summary
• In Ring Crush Tests on lightweight materials failure occurs by buckling. On heavy weight materials failure occurs at the loaded edges, which are weakened by cutting as the specimens are prepared.
(Note: The Tappi methods T818 and T822 for RCT are intended for paperboard between 0.28 mm (0.011 in.) and 0.51 mm (0.020 in.) thick. )
• The SCT-method measures the pure compressive strength i.e. what it is intended to measure. The SCT-method is quick, and easy to use. The SCT results are more indicative of the fluting medium contribution to ECT than the RCT results
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• To predict the print results on unprinted paper/board, for different printing techniques.
• It is important for the print results when using Flexo Gravure Offset
Why characterize the surface?
By characterizing unprinted substrates it is possible to predict print quality in order to reach the specifications.
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• Air-leak – PPS, Bendtsen, Sheffield– Small surface measured– ”wrong” resolution to be relevant for printing
• Stylus roughness– Reference head, laser triangulation,
chromatic aberration etc.– Small surface measured– ”wrong” resolution to be relevant for printing
• Optical topography– Photometric stereo technique– Large area measured– ”right” resolution to be relevant for printing
Height mapGradient
Methods to characterize the paper surface
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Phenomenon: topography and low angle light = shadows
Measurements: shadows and known light angle = topography
Optical image analysis measurements
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Picture from rightPicture from left
Gradient map
Height map
Stereographic picture
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Gradient map
Height map
Stereographic picture
CRATERSOSD
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OptiTopo Surface DeviationO S D
Small scale surface variations
– relevant for printing
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It is very important to divide the surface variation in fine, mid,and large scale variation because some intervals are important for the print results and some are not.
This is not possible to do with air-leak instruments (e.g. PPS, Bendtsen).
Paper and board surface characterization
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Printability according to OSD vs. PPS
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Band passing into different wavelength ranges creates a spectrum from original profile
These ranges may play different roles for the printability
Paper surface
Different wavelength ranges of the original profile are sometimes given specific names:
Form
Waviness
Roughness
Sta
ndar
d de
viat
ion
Wavelength
Mathematical characterization of surface
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LARGE scaleFINE scale MID scale
L&W OptiTopo extracts information from stereoscopic picture
Total image– a combination of all surface variations
Roughness variations
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Surface roughness
Sm
oo
thR
oug
h
Standard Deviation is calculated for each wavelength band
LARGE scaleFINE scale MID scale
Roughness variations
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Surface roughness
Sm
oo
thR
oug
hOSD
Important for printing
BendtsenSheffieldEmveco
PPS
LARGE scaleFINE scale MID scale
Roughness variations
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LARGE scaleroughness variations
FINE scaleroughness variations
MID scaleroughness variations
L&W OptiTopo extracts information from stereoscopic picture
Total image– a combination of all surface variations
OptiTopo measures the surface variation in a large number of wave-lengths and group these into 10 different bands
These ranges may play different roles for the printability
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Large scale roughness variations,Bendtsen, Sheffield, Emveco(wavelength band 5-6)
Mid scale roughness variations,PPS (wavelength band 4-5)
Small scale roughness variations,OSD (wavelength band 1-4)
Paper surface total variation = small scale + mid scale + large scale roughness variations,+ very large scale variations (waviness, cockling etc.)
Very large scale variations, form, waviness, cockling(wavelength band 7-10)
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Bendtsen: ”land”, D= 150µm, circumference 104 mm
Measured area of paper = 15,5 mm2
D
Actual paper surface (wavelength band 1-10)
D
Paper surface ”seen” by Bendtsen = large scale roughness variations (wavelength band 5-6)
A closer look at Bendtsen
Fine scale, mid scale roughness and craters are invisible to Bendtsen
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PPS: ”land”, D=51µm, circumference 100 mm
Measured area = 5,1mm2
D
D
Paper surface ”seen” by PPS = mid scale roughness variations (wavelength band 4-5)
Fine scale scale roughness and craters are invisible to PPS
A closer look at PPS
Actual paper surface (wavelength band 1-10)
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OptiTopo resolution: 15,6 µm
Measured area = 1000 mm2
Variations that OptiTopo actually ”see”= all variations from small scale roughness variations to large scale roughness variations, all the way up to 32 mm wide variations, divided into 10 wavelength bands.
++
+
Band 1-4
Band 4-5
Band 5-6
Band 7-10
Actual paper surface (wavelength band 1-10 which is 0.0315 – 32 mm variations)
OptiTopo use band 1-4 to calculate OSD value
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L&W OptiTopo Crater Value
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0 µm
-3 µm(in this example)
Identify craters of different depths…
InkPaper surface
Shallow craters are not “dangerous” Deep craters cause
missing dot or un-covered area (UCA)
Flexo printed board
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According to PPS these surfaces have the same roughness value. The PPS value will not say anything about the craters, which may cause print defects in flexo and gravure.
PPS 1.5 µm
PPS 1.5 µm
Craters deeper than 1.5 µm
Crater depth in µm
The crater value– a value of the surface deviation as regards to surface pores
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Crater 1.5 – smooth Crater 3 – medium Crater 5 – rough
Double/triple coated surfaces, hard calendared qualities like SC, MG
Liner, liquid board, newsprint, copy paper, fine paper
Sack paper, uncoated board, uncoated paper, tissue
Double coated board Liquid board Sack
Craters deeper than -1.5 µm = 3.14%
Craters deeper than -3 µm = 1.78%
Craters deeper than -5 µm = 3.48%
The crater value– depths and paper grades
• The amount of craters with a specified depth• Different crater depths are relevant for different paper grades
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To give a relevant value for printing the amount of craters in measured area should be in the range of 0.2–10%
Craters below 1.5 µm
11.4%
Craters below 5 µm
0.04%Amountof craters (%)
Craters below 3 µm
2.27%
Best choice for this paper grade
The crater value– a value of the surface deviation as regards to surface pores
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Mottle
Uncovered area (UCA)
Missing dots
Case studies - Typical print defects
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Case study 1 – rotogravure on double coated board
Missing dots
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Case study – rotogravure on double coated board
Cyan 25% Full-scale gravure print Source: Innventia
Missing dots
19 samples with different print result
Missing dots were counted manually with microscope
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Amount of missing dots [%]
Case study – rotogravure on double coated board
Source: Innventia
Missing dots
PPSvs
missing dots
Low correlation
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Case study – rotogravure on double coated board
Source: Innventia
Missing dots
L&W OptiTopo
vsmissing dots
Amount of missing dots [%]
High correlation
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Conclusion Case Study 1
OptiTopo gave a better ranking of missing dots compared to PPS
Correlation to the print results:
L&W OptiTopo R² = 0.94
PPS R² = 0.57
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Case study 2 – Improved top ply printability after rebuilding of white-top liner machine
Uncovered area (UCA)
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Importance of relevant topographical properties for print result
Before After
Rebuilt white-top liner PM ”reversed forming concept”
Source: Innventia
• Print mottle reduced• UCA reduced• Wet-in-wet printing
improved
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Rebuilt white-top liner PM– improved flexo printability
Ste
reos
copi
cgr
adie
nt im
age
Before After
Fle
xo p
rint
res
ult
Source: Innventia
Before After
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Conclusion Case Study 2
OptiTopo gave a better ranking of print prediction compared to PPS
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Case study 3 – Liquid board, flexo printed
Predict mottling
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Source: Innventia
Liquid board– flexo printed
• A set of 6 different samples gave different amount of mottle in a full scale test print.
• The mottle in the cyan 100% areas were measured using the Mottling-Expert software from Innventia
• The same 6 samples were measured using the L&W OptiTopo in the unprinted parts of the printed sheets and the amount of craters were measured
• Also PPS and Bendtsen was tested as reference
Cyan 100%Full-scale flexo print
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Source: Innventia
Mottle value
OptiTopo– print prediction correlation
High correlation
![Page 56: Performance and Appearance of packaging grades of paper Study on quality measurement methods Author and Presenter: Manoj Sukumaran Manager – Lorentzen](https://reader030.vdocuments.us/reader030/viewer/2022020920/5697c02a1a28abf838cd7fc0/html5/thumbnails/56.jpg)
Source: Innventia
Mottle value
Bendtsen– print prediction correlation
Medium correlation
![Page 57: Performance and Appearance of packaging grades of paper Study on quality measurement methods Author and Presenter: Manoj Sukumaran Manager – Lorentzen](https://reader030.vdocuments.us/reader030/viewer/2022020920/5697c02a1a28abf838cd7fc0/html5/thumbnails/57.jpg)
Source: Innventia
Mottle value
Quite low correlation
PPS– print prediction correlation
![Page 58: Performance and Appearance of packaging grades of paper Study on quality measurement methods Author and Presenter: Manoj Sukumaran Manager – Lorentzen](https://reader030.vdocuments.us/reader030/viewer/2022020920/5697c02a1a28abf838cd7fc0/html5/thumbnails/58.jpg)
Conclusion Case Study 3
OptiTopo gave a better ranking of mottling compared to PPS and Bendtsen
Correlation to the print results:
L&W OptiTopo R² = 0.91
Bendtsen R² = 0.54
PPS R² = 0.36
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• What? A proven technique to predict printability, faster and more accurate compared to air-leak instruments, stylus instruments and visual assessments.
• Why? To minimize waste, reduce customer complaints and improve quality.
• For whom? Useful for producers of paper, board and sack products that will be printed on.
Summary
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Surface topography– a key factor for print quality
Source: Innventia
(OSD)
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Benefits
•Saves resources in terms of materials, energy and time
•Reduces costly customer complaints
•Reduces waste and environmental impact
Measure printability withL&W OptiTopo
Unprinted paper / board
Benefits with early print prediction
![Page 62: Performance and Appearance of packaging grades of paper Study on quality measurement methods Author and Presenter: Manoj Sukumaran Manager – Lorentzen](https://reader030.vdocuments.us/reader030/viewer/2022020920/5697c02a1a28abf838cd7fc0/html5/thumbnails/62.jpg)
Questions?
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The Measure of Quality