our reference: units your reference ------- evl-dup …...client reference: pcbs in soil our...

Client Reference:

sTPH in Soil (ClO-C36)

Our Reference: UNITS

Your Reference -------------

Date Sampled ------------

Type of sample

Date extracted -Date analysed -TPH ClO - C14 mg/kg

TPH C15 - C28 mg/kg

TPH C29 - C36 mg/kg

Surrogate o-Terphenyl %

J

Envirolab Reference: 45067 Revision No: R 00

406484, Hunters Hill

45067-1

EVL-DUP-ool

24/08/2010

Soil

26/8/2010

26/8/2010

<50

<100

<100

85

A. NATA V' ACCREDITED FOR

TECHNICAL COMPETENCE

45067-2

EVL-DUP-002

24/08/2010

Soil

26/8/2010

26/8/2010

<50

<100

<1 00

86

Page 3 of 14

Client Reference:

PAHs in Soil



Date Sampled -- ----------

Type of sample

Date extracted -Date analysed -Naphthalene mg/kg

Acenaphthylene mg/kg

Acenaphthene mg/kg

Fluorene mg/kg

Phenanthrene mg/kg

Anthracene mg/kg

Fluoranthene mg/kg

Pyrene mg/kg

8enzo(a)anthracene mg/kg

Chrysene mg/kg

8enzo(b+k)fJuoranthene mg/kg

8enzo(a)pyrene mg/kg

Indeno(1 ,2,3-c,d)pyrene mg/kg

Dibenzo(a,h)anthracene mg/kg

8enzo(g,h,i)perylene mg/kg

Surrogate p-Terphenyl-d14 %



45067-1

EVL-DUP-001

24/08/2010

Soil

26/8/2010

27/8/2010

<0.1

<0.1

<0.1

<0.1

0.3

<0.1

0.6

0.5

0.2

0.3

0.4

0.3

0.2

<0.1

0.2

87

NATA V" ACCREDITED FOR


45067-2

EVL-DUP-002

24/08/2010

Soil

26/8/2010

27/8/2010

<0.1

<0.1

<0.1

<0.1

<0.1

<0.1

<0.1

<0.1

<0.1

<0 .1

<0.2

<0.05

<0.1

<0.1

<0.1

95

Page 4 of 14

Client Reference:

Organochlorine Pesticides in soil




Type of sample

Date extracted -Date analysed -

HCB mg/kg

alpha-BHe mg/kg

gamma-BHC mg/kg

beta-BHe mg/kg

Heptachlor mg/kg

delta-BHe mg/kg

Aldrin mg/kg

Heptachlor Epoxide mg/kg

gamma-Chlordane mg/kg

alpha-chlordane mg/kg

Endosulfan I mg/kg

pp-DDE mg/kg

Dieldrin mg/kg

Endrin mg/kg

pp-DDD mg/kg

Endosulfan II mg/kg

pp-DDT mg/kg

Endrin Aldehyde mg/kg

Endosulfan Sulphate mg/kg

Methoxychlor mg/kg

Surrogate TCLMX %



45067-1

EVL-DUP-001

24/08/2010

Soil

26/8/2010

27/8/2010

<0.1

<0.1

<0.1

<0.1

<0.1

<0.1

<0.1

<0.1

<0.1

<0.1

<0.1

<0.1

<0.1

<0.1

<0.1

<0.1

<0.1

<0.1

<0.1

<0.1

107

.A NATA V" ACCREDITED FOR


45067-2

EVL-DUP-002

24/08/2010

Soil

26/8/2010

27/8/2010

<0.1

<0.1

<0.1

<0.1

<0.1

<0.1

<0.1

<0.1

<0.1

<0.1

<0.1

<0.1

<0.1

<0.1

<0.1

<0.1

<0.1

<0.1

<0.1

<0.1

100

Page 5 of 14

Client Reference:

PCBs in Soil


Your Reference -- - ----------


Type of sample

Date extracted -Date analysed -Arochlor 1016 mg/kg

Arochlor 1221 * mg/kg

Arochlor 1232 mg/kg

Arochlor 1242 mg/kg

Arochlor 1248 mg/kg

Arochlor 1254 mg/kg

Arochlor 1260 mg/kg

Surrogate TCLMX %



45067-1

EVL-DUP-001

24/08/2010

Soil

26/8/2010

27/8/2010

<0.1

<0.1

<0.1

<0.1

<0.1

<0.1

<0.1

107

NATA V' ACCREDITED FOR


45067-2

EVL-DUP-002

24/08/2010

Soil

26/8/2010

27/8/2010

<0.1

<0.1

<0.1

<0.1

<0.1

<0.1

<0.1

100

Page 6 of 14

Client Reference:

Acid Extractable metals in soil


Your Reference -------------Date Sampled ------------

Type of sample

Date digested -Date analysed -

Arsenic mg/kg

Cadmium mg/kg

Chromium mg/kg

Copper mg/kg

Lead mg/kg

Mercury mg/kg

Nickel mg/kg

Zinc mg/kg



45067-1

EVL-DUP-001

24/08/2010

Soil

26/08/2010

26/08/2010

40

<0.5

24

19

56

<0.1

3

46

.A NATA V' ACCREDITED FOR


45067-2

EVL-DUP-002

24/08/2010

Soil

26/08/2010

26/08/2010

11

<0.5

10

8

21

<0.1

2

23

Page 7 of 14

Client Reference:

Moisture



Date Sampled ------------Type of sample

Date prepared -

Date analysed -

Moisture %



45067-1

EVL-DUP-001

24/08/2010

Soil

26/8/2010

26/8/2010

13

.A NATA V" ACCREDITED FDA


45067-2

EVL-DUP-002

24/08/2010

Soil

26/8/2010

26/8/2010

13

Page 8 of 14

Client Reference: 406484, Hunters Hill

Method ID Methodology Summary

GC.16 Soil samples are extracted with methanol and spiked into water prior to analysing by purge and trap GC-MS. Water samples are analysed directly by purge and trap GC-MS.

GC.3 Soil samples are extracted with Dichloromethane/Acetone and waters with Dichloromethane and analysed byGC-FID.

GC.12 subset Soil samples are extracted with Dichloromethane/Acetone and waters with Dichloromethane and analysed by GC-MS.

GC-5 Soil samples are extracted with dichloromethane/acetone and waters with dichloromethane and analysed by GC with dual ECD's.

GC-6 Soil samples are extracted with dichloromethane/acetone and waters with dichloromethane and analysed by GC-ECD.

Metals.20 ICP- Determination of various metals by ICP-AES. AES

Metals.21 CV- Determination of Mercury by Cold Vapour MS. AAS

LAB.S Moisture content determined by heating at 105 deg C for a minimum of 4 hours.

Envirolab Reference: 45067 .A Page 9 of 14 Revision No: R 00 NATA

V" ACCREDITED FOR



QUALITY CONTROL UNITS PQL

vTPH & BTEX in Soil

Date extracted -

Date analysed -

vTPH C6 - C9 mg/kg 25

Benzene mg/kg 0.5

Toluene mg/kg 0.5

Ethylbenzene mg/kg 1

m+p-xylene mg/kg 2

o-Xylene mg/kg 1

Surrogate aaa- % Trifluorotoluene


sTPH in Soil (C10-C36)

Date extracted -

Date analysed -

TPHC10 - C14 mg/kg 50

TPH C15 - C28 mg/kg 100

TPH C29 - C36 mg/kg 100



PAHs in Soil

Date extracted -

Date analysed -

Naphthalene mg/kg 0.1

Acenaphthylene mg/kg 0.1

Acenaphthene mg/kg 0.1

Fluorene mg/kg 0.1

Phenanthrene mg/kg 0.1

Anthracene mg/kg 0.1

Fluoranthene mg/kg 0.1

Pyrene mg/kg 0.1


METHOD

GC.16

GC.16

GC.16

GC.16

GC.16

GC.16

GC.16

METHOD

GC.3

GC.3

GC.3

GC.3

METHOD

GC.12 subset

GC.12 subset

GC.12 subset

GC.12 subset

GC.12 subset

GC.12 subset

GC.12 subset

GC.12 subset

Blank Duplicate Sm#

27/08/2 [NT] 5010

28/08/2 [NT] 5010

<25 [NT]

<0.5 [NT]

<0.5 [NT]

<1.0 [NT]

<2.0 [NT]

<1.0 [NT]

108 [NT]

Blank Duplicate Sm#

26/8/20 [NT] 10

26/8/20 [NT] 10

<50 [NT]

<100 [NT]

<100 [NT]

86 [NT]

Blank Duplicate sm#

26/8/20 [NT] 10

27/8/20 [NT] 10

<0.1 [NT]

<0.1 [NT]

<0.1 [NT]

<0.1 [NT]

<0.1 [NT]

<0.1 [NT]

<0.1 [NT]

<0.1 [NT]

NATA ~ ACCREDITED FOA


Duplicate results

Base II Duplicate II %RPD

[NT]

[NT]

[NT]

[NT]

[NT]

[NT]

[NT]

[NT]

[NT]

Duplicate results


[NT]

[NT]

[NT]

[NT]

[NT]

[NT]

Duplicate results


[NT]

[NT]

[NT]

[NT]

[NT]

[NT]

[NT]

[NT]

[NT]

[NT]

Spike Sm# Spike % Recovery

LCS-3 27/08/25010

LCS-3 28/08/25010

LCS-3 98%

LCS-3 103%

LCS-3 91%

LCS-3 98%

LCS-3 100%

LCS-3 100%

LCS-3 100%

SpikeSm# Spike % Recovery

LCS-2 26/8/2010

LCS-2 26/8/2010

LCS-2 83%

LCS-2 85%

LCS-2 83%

LCS-2 77%


LCS-3 26/8/2010

LCS-3 27/8/2010

LCS-3 97%

[NR] [NR]

[NR] [NR]

LCS-3 91%

LCS-3 100%

[NR] [NR]

LCS-3 93%

LCS-3 96%

Page100f 14

Client Reference: 406484, Hunters Hill QUALITY CONTROL UNITS PQL

PAHs in Soil

Benzo(a)anthracene mg/kg 0.1

Chrysene mg/kg 0.1

Benzo(b+k)fluoranthene mg/kg 0.2

Benzo(a)pyrene mg/kg 0.05

Indeno(1 ,2,3-c,d)pyrene mg/kg 0.1

Dibenzo(a,h)anthracene mg/kg 0.1

Benzo(g,h,i)perylene mg/kg 0.1

Surrogate p-Terphenyl- % d14



Date extracted -

Date analysed -

HCB mg/kg 0.1

alpha-BHC mg/kg 0.1

gamma-BHC mg/kg 0.1

beta-BHC mg/kg 0.1

Heptachlor mg/kg 0.1

delta-BHC mg/kg 0.1

Aldrin mg/kg 0.1

Heptachlor Epoxide mg/kg 0.1

gamma-Chlordane mg/kg 0.1

alpha-chlordane mg/kg 0.1

Endosulfan I mg/kg 0.1

pp-DDE mg/kg 0.1

Dieldrin mg/kg 0.1

Endrin mg/kg 0.1

pp-DDD mg/kg 0.1

Endosulfan II mg/kg 0.1

pp-DDT mg/kg 0.1

Endrin Aldehyde mg/kg 0.1

Endosulfan Sulphate mg/kg 0.1

Methoxychlor mg/kg 0.1

Surrogate TCLMX %


METHOD

GC.12 subset

GC.1 2 subset

GC.12 subset

GC.12 subset

GC.12 subset

GC.12 subset

GC.12 subset

GC.12 subset

METHOD

GC-5

GC-5

GC-5

GC-5

GC-5

GC-5

GC-5

GC-5

GC-5

GC-5

GC-5

GC-5

GC-5

GC-5

GC-5

GC-5

GC-5

GC-5

GC-5

GC-5

GC-5

Blank Duplicate Sm#

<0 .1 [NT]

<0 .1 [NT]

<0.2 [NT]

<0.05 [NT]

<0.1 [NT]

<0.1 [NT]

<0.1 [NT]

101 [NT]

Blank Duplicate Sm#

26/8/20 [NT] 10

27/8/20 [NT] 10

<0.1 [NT]

<0.1 [NT]

<0.1 [NT]

<0.1 [NT]

<0.1 [NT]

<0.1 [NT]

<0.1 [NT]

<0.1 [NT]

<0.1 [NT]

<0.1 [NT]

<0.1 [NT]

<0.1 [NT]

<0.1 [NT]

<0.1 [NT]

<0.1 [NT]

<0.1 [NT]

<0.1 [NT]

<0.1 [NT]

<0.1 [NT]

<0.1 [NT]

93 [NT]

A-NATA V" ACCREDI TED FOA


Duplicate results


[NT]

[NT]

[NT]

[NT]

[NT]

[NT]

[NT]

[NT]

Duplicate results


[NT]

[NT]

[NT]

[NT]

[NT]

[NT]

[NT]

[NT]

[NT]

[NT]

[NT]

[NT]

[NT]

[NT]

[NT]

[NT]

[NT]

[NT]

[NT]

[NT]

[NT]

[NT]

[NT]


[NR] [NR]

LCS-3 98%

[NR] [NR]

LCS-3 111%

[NR] [NR]

[NR] [NR]

[NR] [NR]

LCS-3 82%


LCS-2 26/8/2010

LCS-2 27/8/2010

[NR] [NR]

LCS-2 116%

[NR] [NR]

LCS-2 122%

LCS-2 104%

[NR] [NR]

LCS-2 105%

LCS-2 115%

[NR] [NR]

[NR] [NR]

[NR] [NR]

LCS-2 130%

LCS-2 121%

LCS-2 116%

LCS-2 128%

[NR] [NR]

[NR] [NR]

[NR] [NR]

LCS-2 92%

[NR] [NR]

LCS-2 105%

Page 11 of 14



PCBs in Soil

Date extracted -

Date analysed -

Aroch lor 1016 mg/kg 0.1

Arochlor 1221' mg/kg 0.1

Arochlor 1232 mg/kg 0.1





Surrogate TCLMX %



Date digested -

Date analysed -

Arsenic mg/kg 4

Cadmium mg/kg 0.5

Chromium mg/kg 1

Copper mg/kg 1

Lead mg/kg 1

Mercury mg/kg 0.1

Nickel mg/kg 1

Zinc mg/kg 1


METHOD

GC-6

GC-6

GC-6

GC-6

GC-6

GC-6

GC-6

GC-6

METHOD

Metals.20 ICP-AES

Metals.20 ICP-AES

Metals.20 ICP-AES

Metals.20 ICP-AES

Metals.20 ICP-AES

Metals.21 CV-AAS

Metals.20 ICP-AES

Metals.20 ICP-AES

Blank Duplicate Sm#

"'1"\'''''''',.. r~ I .... ~ LUlU/LV l'. 'J

10

27/8/20 [NT] 10

<0.1 [NT]

<0.1 [NT]

<0.1 [NT]

<0.1 [NT]

<0.1 [NT]

<0.1 [NT]

<0.1 [NT]

93 [NT]

Blank Duplicate Sm#

26/08/2 [NT] 010

26/08/2 [NT] 010

<4 [NT]

<0.5 [NT]

<1 [NT]

<1 [NT]

<1 [NT]

<0.1 [NT]

<1 [NT]

<1 [NT]

NATA

ACCREDITED FOR


Duplicate results


L~~7J

[NT]

[NT]

[NT]

[NT]

[NT]

[NT]

[NT]

[NT]

[NT]

Duplicate results


[NT]

[NT]

[NT]

[NT]

[NT]

[NT]

[NT]

[NT]

[NT]

[NT]


I ............. ... ,../1'\, .... ,.. ... ,.. l.VV-L L\,JfV/L.V tV

LCS-2 27/8/2010

[NR] [NR]

[NR] [NR]

[NR] [NR]

[NR] [NR]

[NR] [NR]

LCS-2 125%

[NR] [NR]

LCS-2 110%


LCS-5 26/08/2010

LCS-5 26/08/2010

LCS-5 98%

LCS-5 102%

LCS-5 106%

LCS-5 107%

LCS-5 100%

LCS-5 114%

LCS-5 105%

LCS-5 101 %

Page 12 of 14


QUALITY CONTROL UNITS PQl

Moisture

Date prepared -

Date analysed -

Moisture % 0.1


METHOD

lAB.8

Blank

26/8/20 10

26/8/20 10

<0 .10

.A NATA ~ ACCREDITED FOR


Page 13 of 14

Client Reference:

Report Comments:

Asbestos 10 was analysed by Approved Identifier:

Asbestos 10 was authorised by Approved Signatory: Asbestos counting was analysed by Approved Counter: Asbestos counting was authorised by Approved Signatory:


Not applicable for this job Not applicable for this job

@ERROR @ERROR

NT: Not tested INS: Insufficient sample for this test NA: Test not required

PQL: Practical Quantitation Limit RPD: Relative Percent Difference >: Greater than

NA: Test not required <: Less than LCS: Laboratory Control Sample

Quality Control Definitions Blank: This is the component of the analytical signal which is not derived from the sample but from reagents,

glassware etc, can be determined by processing solvents and reagents in exactly the same manner as for samples. Duplicate: This is the complete duplicate analysis of a sample from the process batch. If possible, the sample selected should be one where the analyte concentration is easily measurable. Matrix Spike: A portion of the sample is spiked with a known concentration of target analyte. The purpose of the matrix

spike is to monitor the performance of the analytical method used and to determine whether matrix interferences exist. LCS (Laboratory Control Sample): This comprises either a standard reference material or a control matrix (such as a blank

sand or water) fortified with analytes representative of the analyte class. It is simply a check sample. Surrogate Spike: Surrogates are known additions to each sample, blank, matrix spike and LCS in a batch, of compounds which are similar to the analyte of interest, however are not expected to be found in real samples.

Laboratory Acceptance Criteria Duplicate sample and matrix spike recoveries may not be reported on smaller jobs, however, were analysed at a frequency to meet or exceed NEPM requirements. All samples are tested in batched of 20. The duplicate sample RPD and matrix

spike recoveries for the batch were within the laboratory acceptance criteria.

Duplicates: <5xPQL - any RPD is acceptable; >5xPQL - 0-50% RPD is acceptable. Matrix Spikes and LCS: Generally 70-130% for inorganics/metals; 60-140% for organics and 10-140% for SVOC and

speciated phenols is acceptable.

Envirolab Reference: 45067 Revision No: R 00 NATA

ACCREDITED FOR


Page 14 of 14

I

Envirolab Services Pty Ltd ABN 37112535645

12 Ashley 8t Ghatswood NSW 2067 ph 0299106200 fax 02 9910 6201

[email protected] www.envirolabservices.com.au

CERTIFICATE OF ANALYSIS 45124 Client:

CH2MHILL

PO Box 5392 Ghatswood N8W 1515

Attention: Ben Farmer

Sample log in details: Your Reference: No. of samples: Date samples received:

Date completed instructions received :

Analysis Details:


2 Soils 26/08/2010 26/08/2010

Please refer to the following pages for results, methodology summary and quality control data. Samples were analysed as received from the client. Results relate specifically to the samples as received.

Results are reported on a dry weight basis for solids and on an as received basis for other matrices. Please refer to the last page of this report for any comments relating to the results.

Report Details: Date results requested by: Date of Preliminary Report:

Issue Date:

2/09/10 Not issued 1/09/10

NATA accreditation number 2901. This document shall not be reproduced except in full. This document is issued in accordance with NATA's accreditation requirements. Accredited for compliance with ISO/IEG 17025.

Tests not covered by NATA are denoted with *.

Results Approved By:

Envirolab Reference: 45124

Revision No: R 00

Nancy Zhang Chemist



sa~! Senior Organic Chemist

!2i4L-0 /v(C~P. Rhian Morgan Metals Supef\"isor

Page 1 of 14

vTPH & BTEX in Soil

Our Reference:

Your Reference

Date Sampled

Type of sample

Date extracted

Date analysed

vTPH Cs - C9

Benzene

Toluene

Ethylbenzene

m+p-xylene

o-Xylene

Surrogate aaa-Trifluorotoluene


Client Reference:

UNITS

----------- --

------------

--

mg/kg

mg/kg

mg/kg

mg/kg

mg/kg

mg/kg

%


45124-2

EVL-DUP-006

25/08/2010

Soil

27/08/2010

28/08/2010

<25

<0.5

<0.5

<1.0

<2.0

<1 .0

96

NATA

ACCREDITED FOR


Page 2 of 14

Client Reference:





Date extracted -Date analysed -TPHC10 - C14 mg/kg

TPH C15 - C28 mg/kg

TPH C29 - C36 mg/kg




45124-2

EVL-DUP-006

25/08/2010

Soil

27/08/2010

27/08/2010

<50

<100

<100

96

.A-NATA V' ACCREDITED FOR


Page 3 of 14

Client Reference:

PAHs in Soil


Your Reference ~------------


Type of sample

Date extracted -Date analysed -Naphthalene mg/kg


Acenaphthene mg/kg

Fluorene mg/kg

Phenanthrene mg/kg

Anthracene mg/kg

Fluoranthene mg/kg

Pyrene mg/kg

8enzo(a)anthracene mg/kg

Chrysene mg/kg

8enzo(b+k)fluoranthene mg/kg

8enzo(a)pyrene mg/kg



8enzo(g,h,i)perylene mg/kg

Surrogate p-Terphenyl-d14 %



45124-2

EVL-DUP-006

25/08/2010

Soil

27/08/2010

29/08/2010

<0.1

<0.1

<0.1

<0.1

1.2

0.2

2.2

2.1

0.9

1.0

1.5

1.2

0.7

<0.1

0.6

78

NATA

ACCREDITED FOR


I )

Page 4 of 14

Client Reference:





Type of sample

Date extracted -

Date analysed -

HCS mg/kg

alpha-SHC mg/kg

gamma-SHC mg/kg

beta-SHC mg/kg

Heptachlor mg/kg

delta-SHe mg/kg

Aldrin mg/kg




Endosulfan I mg/kg

pp-DDE mg/kg

Dieldrin mg/kg

Endrin mg/kg

pp-DDD mg/kg

Endosulfan II mg/kg

pp-DDT mg/kg



Methoxychlor mg/kg

Surrogate TCLMX %



45124-2

EVl-DUP-006

25/08/2010

Soil

27/08/2010

28/08/2010

<0.1

<0.1

<0.1

<0.1

<0.1

<0.1

<0.1

<0.1

<0.1

<0.1

<0.1

<0.1

0.5

<0.1

<0.1

<0.1

<0.1

<0.1

<0.1

<0.1

115



Page 5 of 14

Client Reference:

PCBs in Soil




Type of sample

Date extracted -

Date analysed -Arochlor 1016 mg/kg

Arochlor 1221 * mg/kg

Arochlor 1232 mg/kg

Arochlor 1242 mg/kg

Arochlor 1248 mg/kg

Arochlor 1254 mg/kg

Aroch lor 1260 mg/kg

Surrogate TCLMX %



45124-2

EVL-DUP-006

25/08/2010

Soil

27/08/2010

28/08/2010

<0,1

<0,1

<0,1

<0,1

<0,1

<0 ,1

<0,1

115

.A NATA

ACCREDITED FOR TECHNICAL COMPETENCE

Page 6 of 14

Client Reference:





Type of sample

Date digested -

Date analysed -

Arsenic mg/kg

Cadmium mg/kg

Chromium mg/kg

Copper mg/kg

Lead mg/kg

Mercury mg/kg

Nickel mg/kg

Zinc mg/kg

1



45124-2

EVL-DUP-006

25/08/2010

Soil

30/08/2010

30/08/2010

16

<0.5

14

25

120

0.8

4

290



Page 7 of 14

Client Reference:

Moisture


Your Reference -------------Date Sampled -- - --- - ---- -

Type of sample

Date prepared -

Date analysed -Moisture %



45124-2

EVL-DUP-006

25/08/2010

Soil

27/08/25010

27/08/25010

10



I )

Page 8 of 14


Method 10 Methodology Summary


GC.3 Soil samples are extracted with Dichloromethane/Acetone and waters with Dichloromethane and analysed byGC-FID.




Metals.20 Determination of various metals by ICP-AES. ICP-AES

Metals.21 Determination of Mercury by Cold Vapour MS. CV-AAS

LAB.8 Moisture content determined by heating at 105 deg C for a minimum of 4 hours.

Envirolab Reference: 45124 .A Page 9 of 14 Revision No: R 00 NATA

V" ACCREDITED FOR



QUALITY CONTROL UNITS PQL METHOD

vTPH & BTEX in Soil

Date extracted -

Date analysed -

vTPH C6 - C9 mg/kg 25 GC.16

Benzene mg/kg 0.5 GC.16

Toluene mg/kg 0.5 GC.16

Ethylbenzene mg/kg 1 GC.16

m+p-xylene mg/kg 2 GC.16

o-Xylene mg/kg 1 GC.16

Surrogate % GC.16 aaa-Trifluorotoluene



Date extracted -

Date analysed -

TPHC10 - C14 mg/kg 50 GC.3

TPH C15 - C28 mg/kg 100 GC.3

TPH C29 - C36 mg/kg 100 GC.3

Surrogate % GC.3 o-Terphenyl


PAHsin Soil

Date extracted -

Date analysed -

Naphthalene mg/kg 0.1 GC.12 subset

Acenaphthylene mg/kg 0.1 GC.12 subset

Acenaphthene mg/kg 0.1 GC.12 subset

Fluorene mg/kg 0.1 GC.12 subset

Phenanthrene mg/kg 0.1 GC.12 subset

Anthracene mg/kg 0.1 GC.12 subset

Fluoranthene mg/kg 0.1 GC.12 subset

Pyrene mg/kg 0.1 GC.12 subset


Blank Duplicate Sm#

27/08/2 [NT] 01 0

28/08/2 [NT] 010

<25 [NT]

<0.5 [NT]

<0.5 [NT]

<1.0 [NT]

<2.0 [NT]

<1.0 [NT]

100 [NT]

Blank Duplicate Sm#

27/08/2 [NT] 010

27/08/2 [NT] 01 0

<50 [NT]

<100 [NT]

<100 [NT]

74 [NT]

Blank Duplicate Sm#

27/8/20 [NT] 10

29/8/20 [NT] 10

<0.1 [NT]

<0.1 [NT]

<0.1 [NT]

<0.1 [NT]

<0.1 [NT]

<0.1 [NT]

<0.1 [NT]

<0.1 [NT]



Duplicate results


[NT]

[NT]

[NT]

[NT]

[NT]

[NT]

[NT]

[NT]

[NT]

Duplicate results


[NT]

[NT]

[NT]

[NT]

[NT]

[NT]

Duplicate results


[NT]

[NT]

[NT]

[NT]

[NT]

[NT]

[NT]

[NT]

[NT]

[NT]


LCS-5 27/08/2010

LCS-5 28/08/2010

LCS-5 81%

LCS-5 74%

LCS-5 79%

LCS-5 84%

LCS-5 85%

LCS-5 86%

LCS-5 100%


LCS-4 27/08/2010

LCS-4 27/08/2010

LCS-4 89%

LCS-4 94%

LCS-4 92%

LCS-4 93%


LCS-4 27/8/2010

LCS-4 29/8/2010

LCS-4 102%

[NR] [NR]

[NR] [NR]

LCS-4 114%

LCS-4 100%

[NR] [NR]

LCS-4 95%

LCS-4 107%

Page 10 of 14

)



PAHs in Soil


Chrysene mg/kg 0.1



Indeno(1,2,3-c,d)pyrene mg/kg 0.1


Benzo(g,h, i)perylene mg/kg 0.1

Surrogate % p-Terphenyl-d14

QUALITY CONTROL UNITS POL


Date extracted -

Date analysed -

HCB mg/kg 0.1

alpha-BHC mg/kg 0.1

gamma-SHC mg/kg 0.1

beta-SHC mg/kg 0.1


delta-SHC mg/kg 0.1

Aldrin mg/kg 0.1





pp-DDE mg/kg 0.1

Dieldrin mg/kg 0.1

Endrin mg/kg 0.1

pp-DDD mg/kg 0.1


pp-DDT mg/kg 0.1




Surrogate TClMX %


METHOD

GC.12 subset

GC.12 subset

GC.12 subset

GC.1 2 subset

GC.12 subset

GC.12 subset

GC.12 subset

GC.12 subset

METHOD

GC-5

GC-5

GC-5

GC-5

GC-5

GC-5

GC-5

GC-5

GC-5

GC-5

GC-5

GC-5

GC-5

GC-5

GC-5

GC-5

GC-5

GC-5

GC-5

GC-5

GC-5

Blank Duplicate Sm#

<0.1 [NT]

<0.1 [NT]

<0.2 [NT]

<0.05 [NT]

<0.1 [NT]

<0.1 [NT]

<0.1 [NT]

84 [NT]

Blank Duplicate Sm#

27/08/2 [NT] 010

28/08/2 [NT] 010

<0.1 [NT]

120 [NT]

<0.1 [NT]

120 [NT]

110 [NT]

<0.1 [NT]

110 [NT]

120 [NT]

<0.1 [NT]

<0.1 [NT]

<0.1 [NT]

120 [NT]

120 [NT]

120 [NT]

130 [NT]

<0.1 [NT]

<0.1 [NT]

<0.1 [NT]

110 [NT]

<0.1 [NT]

127 [NT]

A-NATA V" ACCREDITED FOR


Duplicate resu lts


[NT]

[NT]

[NT]

[NT]

[NT]

[NT]

[NT]

[NT]

Duplicate results


[NT]

[NT]

[NT]

[NT]

[NT]

[NT]

[NT]

[NT]

[NT]

[NT]

[NT]

[NT]

[NT]

[NT]

[NT]

[NT]

[NT]

[NT]

[NT]

[NT]

[NT]

[NT]

[NT]


[NR] [NR]

lCS-4 114%

[NR] [NR]

lCS-4 96%

[NR] [NR]

[NR] [NR]

[NR] [NR]

LCS-4 72%


LCS-4 27/08/2010

LCS-4 28/08/2010

[NR] [NR]

lCS-4 120%

[NR] [NR]

LCS-4 119%

LCS-4 114%

[NR] [NR]

LCS-4 107%

LCS-4 116%

[NR] [NR]

[NR] [NR]

[NR] [NR]

LCS-4 120%

LCS-4 119%

lCS-4 117%

LCS-4 126%

[NR] [NR]

[NR] [NR]

[NR] [NR]

LCS-4 110%

[NR] [NR]

lCS-4 127%

Page 11 of 14



PCBs in Soil

Date extracted -

Date analysed -

Arochlor 1016 mg/kg 0.1 GC-6

Arochlor 1221 * mg/kg 0.1 GC-6




Aroch lor 1254 mg/kg 0.1 GC-6

Aroch lor 1260 mg/kg 0.1 GC-6

Surrogate TCLMX % GC-6



Date digested -

Date analysed -

Arsenic mg/kg 4 Metals.20 ICP-AES

Cadmium mg/kg 0.5 Metals.20 ICP-AES

Chromium mg/kg 1 Metals.20 ICP-AES

Copper mg/kg 1 Metals.20 ICP-AES

Lead mg/kg 1 Metals.20 ICP-AES

Mercury mg/kg 0.1 Metals.21 CV-AAS

Nickel mg/kg 1 Metals.20 ICP-AES

Zinc mg/kg 1 Metals.20 ICP-AES


Blank Duplicate Sm#

27/08/2 [NT] 010

28/08/2 [NT] 010

<0.1 [NT]

<0.1 [NT]

<0.1 [NT]

<0.1 [NT]

<0.1 [NT]

110 [NT]

<0.1 [NT]

105 [NT]

Blank Duplicate Sm#

30/08/2 [NT] 010

30/08/2 [NT] 010

<4 [NT]

<0.5 [NT]

<1 [NT]

<1 [NT]

<1 [NT]

<0.1 [NT]

<1 [NT]

<1 [NT]

NATA

ACCREDITED FOR


Duplicate results


[NT]

[NT]

[NT]

[NT]

[NT]

[NT]

[NT]

[NT]

[NT]

[NT]

Duplicate results


[NT]

[NT]

[NT]

[NT]

[NT]

[NT]

[NT]

[NT]

[NT]

[NT]


LCS-4 27/08/2010

LCS-4 28/08/2010

[NR] [NR]

[NR] [NR]

[NR] [NR]

[NR] [NR]

[NR] [NR]

LCS-4 106%

[NR] [NR]

LCS-4 105%


LCS-1 30/08/2010

LCS-1 30/08/2010

LCS-1 101%

LCS-1 101%

LCS-1 101%

LCS-1 105%

LCS-1 101%

LCS-1 108%

LCS-1 103%

LCS-1 102%

Page 12 of 14

)



Moisture

Date prepared -

Date analysed -

Moisture % 0.1


METHOD

lAB.8

Blank

27108/2 5010

27108/2 5010

<0 .10

.A NATA V' ACCREDI TED FOR


Page 13 of 14

Client Reference:

Report Comments:

Asbestos 10 was analysed by Approved Identifier:

Asbestos 10 was authorised by Approved Signatory:

Asbestos counting was analysed by Approved Counter:

Asbestos counting was authorised by Approved Signatory:


Not applicable for this job


@ERROR

@ERROR

NT: Not tested INS: Insufficient sample for this test

NA: Test not required

PQL: Practical Quantitation Limit

RPD: Relative Percent Difference

>: Greater than

NA: Test not required

<: Less than LCS: Laboratory Control Sample

Quality Control Definitions Blank: This is the component of the analytical signal which is not derived from the sample but from reagents,

glassware etc, can be determined by processing solvents and reagents in exactly the same manner as for samples.

Duplicate: This is the complete duplicate analysis of a sample from the process batch. If possible, the sample

selected should be one where the analyte concentration is easily measurable.

Matrix Spike: A portion of the sample is spiked with a known concentration of target analyte. The purpose of the matrix

spike is to monitor the performance of the analytical method used and to determine whether matrix interferences exist.

LCS (Laboratory Control Sample): This comprises either a standard reference material or a control matrix (such as a blank

sand or water) fortified with analytes representative of the analyte class. It is simply a check sample. Surrogate Spike: Surrogates are known additions to each sample, blank, matrix spike and LCS in a batch, of compounds

which are similar to the analyte of interest, however are not expected to be found in real samples.





Envirolab Reference: 45124

Revision No: R 00 NATA

ACCREDITED FOR


Page 14 of 14

}

]

}

fnmola~ Envirolab Services Pty Ltd

ABN 37 112535645 12 Ashley St Chatswood NSW 2067 ph 02 9910 6200 fax 02 9910 6201


CERTIFICATE OF ANALYSIS 45124-A Client: CH2MHILL PO Box 5392 Chatswood NSW 1515


Sample log in details: Your Reference:

No. of samples:

Date samples received:

Date completed instructions received:

Analysis Details:


Additional Testing on 1 Soil 26/08/2010

30/08/10

Please refer to the following pages for results, methodology summary and quality control data.

Samples were analysed as received from the client. Results relate specifically to the samples as received. Results are reported on a dry weight basis for solids and on an as received basis for other matrices.

Please refer to the last page of this report for any comments relating to the results.

Report Details: Date results requested by: Date of Preliminary Report:

Issue Date:

6/09/10 Not issued 3/09/10

NATA accreditation number 2901 . This document shall not be reproduced except in full. This document is issued in accordance with NATA's accreditation requirements. Accredited for compliance with ISOIIEC 17025. Tests not covered by NATA are denoted with *.


Envirolab Reference: 45124-A Revision No: R 00

Nancy Zhang Chemist

..A NATA V" ACCREDITED FOR


sa~! Senior Organic Chemist

e"4£'-0 /-tc"tjC0 Rhian Morgan Metals Super\"isor

Page 1 of 14

Client Reference:

vTPH & BTEX in Soil




Type of sample

Date extracted -Date analysed -vTPH Cs - C9 mg/kg

Benzene mg/kg

Toluene mg/kg

Ethylbenzene mg/kg

m+p-xylene mg/kg

o-Xylene mg/kg

Surrogate aaa-Trifluorotoluene %



45124-A-1

EVL-DUP-004

25/08/2010

Soil

31/08/2010

01/09/2010

<25

<0.5

<0.5

<1.0

<2.0

<1.0

85



Page 2 of 14

Client Reference:

sTPH in Soil (Cl0-C36)




Type of sample

Date extracted -Date analysed -TPH ClO - C14 mg/kg

TPH C15 - C26 mg/kg

TPH C29 - C36 mg/kg


1



45124-A-l

EVL-DUP-004

25/08/2010

Soil

01/09/2010

01/09/2010

<50

<100

<100

94

.A NATA V' ACCREDITED FDA


Page 3 of 14

Client Reference:

PAHs in Soil


Your Reference - ---~--------


Type of sample


Naphthalene mg/kg


Acenaphthene mg/kg

Fluorene mg/kg

Phenanthrene mg/kg

Anthracene mg/kg

Fluoranthene mg/kg

Pyrene mg/kg

Benzo(a)anthracene mg/kg

Chrysene mg/kg

Benzo(b+k)fluoranthene mg/kg

Benzo(a)pyrene mg/kg



Benzo(g, h ,i)pe rylene mg/kg

Surrogate p-Terphenyl-d 14 %



45124-A-l

EVL-DUP-004

25/08/2010

Soil

31/08/2010

01/09/2010

<0.1

<0.1

<0.1

<0.1

<0.1

<0.1

<0.1

<0.1

<0.1

<0.1

<0.2

<0.05

<0.1

<0.1

<0.1

94

NATA

ACCREDITED FOR


Page 4 of 14

Client Reference:





Type of sample


HCS mg/kg

alpha-SHC mg/kg

gamma-SHC mg/kg

beta-SHC mg/kg

Heptachlor mg/kg

delta-SHC mg/kg

Aldrin mg/kg




Endosulfan I mg/kg

pp-DDE mg/kg

Dieldrin mg/kg

Endrin mg/kg

pp-DDD mg/kg

Endosulfan " mg/kg

pp-DDT mg/kg



Methoxychlor mg/kg

Surrogate TCLMX %



45124-A-1

EVL-DUP-004

25/08/2010

Soil

31/08/2010

01/09/2010

<0.1

<0.1

<0.1

<0.1

<0.1

<0.1

<0.1

<0.1

<0.1

<0.1

<0.1

<0.1

<0.1

<0.1

<0.1

<0.1

<0.1

<0.1

<0.1

<0.1

117

.A-NATA V" ACCREDITED FOR


Page 5 of 14

Client Reference:

PCBs in Soil


Your Reference • _______ M ____


Type of sample


Arochlor 1221* mg/kg

Arochlor 1232 mg/kg

Arochlor 1242 mg/kg

Arochlor 1248 mg/kg

Arochlor 1254 mg/kg

Arochlor 1260 mg/kg

Surrogate TCLMX %



45124-A-1

EVL-DUP-004

25/08/2010

Soil

31/08/2010

01/09/2010

<0.1

<0.1

<0.1

<0.1

<0.1

<0.1

<0.1

117

NATA

ACCRED1TED FOR


Page 6 of 14

Client Reference:




Type of sample

Date digested -Date analysed -

Arsenic mg/kg

Cadmium mg/kg

Chromium mg/kg

Copper mg/kg

Lead mg/kg

Mercury mg/kg

Nickel mg/kg

Zinc mg/kg

J

. f'



45124-A-1

EVL-DUP-004

25/08/2010

Soil

31/08/2010

31/08/2010

4

<0.5

9

18

3

<0.1

1

7

.A NATA V" ACCREDITED FOA


Page 7 of 14

Client Reference:

Moisture




Date prepared -Date analysed -

Moisture %



45124-A-1

EVL-DUP-004

25/08/2010

Soil

31/08/2010

31/08/2010

9.4



Page 8 of 14

I

I


Method 10 Methodology Summary


GC.3 Soil samples are extracted with Dichloromethane/Acetone and waters with Dichloromethane and analysed by GC-FID.




Metals.20 Determination of various metals by ICP-AES. ICP-AES

Metals.21 Determination of Mercury by Cold Vapour AAS. CV-AAS

LAB.S Moisture content determined by heating at 105 deg C for a minimum of 4 hours.

Envirolab Reference: 45124-A .A Page 9 of 14 Revision No: R 00 NATA

V" ACCREDITED FDA




vTPH & BTEX in Soil

Date extracted -

Date analysed -

vTPH C6 - C9 mg/kg 25

Benzene mg/kg 0.5

Toluene mg/kg 0.5

Ethylbenzene mg/kg 1

m+p-xylene mg/kg 2

o-Xylene mg/kg 1

Surrogate % aaa-Trifluorotoluene



Date extracted -

Date analysed -

TPHClO - C14 mg/kg 50

TPH C15 - C28 mg/kg 100

TPH C29 - C36 mg/kg 100

Surrogate % o-Terphenyl


PAHs in Soil

Date extracted -

Date analysed -

Naphthalene mg/kg 0.1

Acenaphthylene mg/kg 0.1

Acenaphthene mg/kg 0.1

Fluorene mg/kg 0.1

Phenanthrene mg/kg 0.1

Anthracene mg/kg 0.1

Fluoranthene mg/kg 0.1

Pyrene mg/kg 0.1


METHOD

GC.16

GC.16

GC.16

GC.16

GC.16

GC.16

GC.16

METHOD

GC.3

GC.3

GC.3

GC.3

METHOD

GC.12 subset

GC.12 subset

GC.12 subset

GC.12 subset

GC.12 subset

GC.12 subset

GC.12 subset

GC.12 subset

Blank Duplicate Sm#

31/08/2 [NT] 010

01/09/2 [NT] 010

<25 [NT]

<0.5 [NT]

<0.5 [NT]

<1.0 [NT]

<2.0 [NT]

<1.0 [NT]

88 [NT]

Blank Duplicate Sm#

31/08/2 [NT] 010

01/09/2 [NT] 010

<50 [NT]

<100 [NT]

<100 [NT]

94 [NT]

Blank Duplicate Sm#

31/08/2 [NT] 010

01/09/2 [NT] 010

<0.1 [NT]

<0.1 [NT]

<0.1 [NT]

<0.1 [NT]

<0.1 [NT]

<0.1 [NT]

<0.1 [NT]

<0.1 [NT]

NATA

'" ACCREDITED FOR


Duplicate results


[NT]

[NT]

[NT]

[NT]

[NT]

[NT]

[NT]

[NT]

[NT]

Duplicate results


[NT]

[NT]

[NT]

[NT]

[NT]

[NT]

Duplicate results


[NT]

[NT]

[NT]

[NT]

[NT]

[NT]

[NT]

[NT]

[NT]

[NT]


lCS-6 31/08/2010

lCS-6 01/09/2010

lCS-6 99%

lCS-6 74%

lCS-6 140%

lCS-6 90%

lCS-6 96%

lCS-6 110%

lCS-6 125%

Spike sm# Spike % Recovery

lCS-6 31/08/2010

lCS-6 01/09/2010

lCS-6 72%

lCS-6 84%

lCS-6 83%

lCS-6 83%


lCS-6 31/08/2010

lCS-6 01/09/2010

lCS-6 98%

[NR] [NR]

[NR] [NR]

lCS-6 93%

lCS-6 103%

[NR] [NR]

lCS-6 93%

lCS-6 95%

Page 10 of 14

I ,

Client Reference: 406484, Hunters Hill QUALITY CONTROL UNITS PQL

PAHs in Soil


Chrysene mg/kg 0.1



Indeno(1,2,3-c,d)pyrene mg/kg 0.1


Benzo(g,h,i)perylene mg/kg 0.1

Surrogate % p-Terphenyl-d 14



Date extracted -

Date analysed -

HCB mg/kg 0.1

alpha-BHC mg/kg 0.1

gamma-BHC mg/kg 0.1

beta-BHC mg/kg 0.1


delta-BHC mg/kg 0.1

Aldrin mg/kg 0.1





pp-DDE mg/kg 0.1

Dieldrin mg/kg 0.1

Endrin mg/kg 0.1

pp-DDD mg/kg 0.1


pp-DDT mg/kg 0.1




Surrogate TCLMX %


METHOD

GC.12 subset

GC.12 subset

GC.12 subset

GC.1 2 subset

GC.12 subset

GC.12 subset

GC.12 subset

GC.12 subset

METHOD

GC-5

GC-5

GC-5

GC-5

GC-5

GC-5

GC-5

GC-5

GC-5

GC-5

GC-5

GC-5

GC-5

GC-5

GC-5

GC-5

GC-5

GC-5

GC-5

GC-5

GC-5

Blank Duplicate Sm#

<0.1 [NT]

<0.1 [NT]

<0.2 [NT]

<0.05 [NT]

<0.1 [NT]

<0.1 [NT]

<0 .1 [NT]

94 [NT]

Blank Duplicate Sm#

31/08/2 [NT] 010

01/09/2 [NT] 010

<0.1 [NT]

<0.1 [NT]

<0.1 [NT]

<0.1 [NT]

<0.1 [NT]

<0.1 [NT]

<0.1 [NT]

<0.1 [NT]

<0.1 [NT]

<0.1 [NT]

<0.1 [NT]

<0.1 [NT]

<0.1 [NT]

<0.1 [NT]

<0.1 [NT]

<0.1 [NT]

<0.1 [NT]

<0.1 [NT]

<0.1 [NT]

<0.1 [NT]

118 [NT]



Duplicate results


[NT]

[NT]

[NT]

[NT]

[NT]

[NT]

[NT]

[NT]

Duplicate results


[NT]

[NT]

[NT]

[NT]

[NT]

[NT]

[NT]

[NT]

[NT]

[NT]

[NT]

[NT]

[NT]

[NT]

[NT]

[NT]

[NT]

[NT]

[NT]

[NT]

[NT]

[NT]

[NT]


[NR] [NR]

LCS-6 102%

[NR] [NR]

LCS-6 99%

[NR] [NR]

[NR] [NR]

[NR] [NR]

LCS-6 97%


-LCS-6 31/08/2010

LCS-6 01/09/2010

[NR] [NR]

LCS-6 104%

[NR] [NR]

LCS-6 100%

LCS-6 92%

[NR] [NR)

LCS-6 90%

LCS-6 99%

[NR] [NR]

[NR] [NR]

[NR) [NR]

LCS-6 100%

LCS-6 100%

LCS-6 94%

LCS-6 102%

[NR] [NR]

[NR] [NR]

[NR] [NR]

LCS-6 96%

[NR] [NR]

LCS-6 107%

Page 11 of 14



PCBs in Soil

Date extracted -

Date analysed -


Arochlor 1221 ' mg/kg 0.1






Surrogate TCLMX %



Date digested -

Date analysed -

Arsenic mg/kg 4

Cadmium mg/kg 0.5

Chromium mg/kg 1

Copper mg/kg 1

Lead mg/kg 1

Mercury mg/kg 0.1

Nickel mg/kg 1

Zinc mg/kg 1


METHOD

GC-6

GC-6

GC-6

GC-6

GC-6

GC-6

GC-6

GC-6

METHOD

Metals.20 ICP-AES

Metals.20 ICP-AES

Metals.20 ICP-AES

Metals.20 ICP-AES

Metals.20 ICP-AES

Metals.21 CV-AAS

Metals.20 ICP-AES

Metals.20 ICP-AES

Blank Duplicate Sm#

31/08/2 [NT] 010

01/09/2 [NT] 010

<0.1 [NT]

<0.1 [NT]

<0.1 [NT]

<0. 1 [NT]

<0.1 [NT]

<0.1 [NT]

<0.1 [NT]

118 [NT]

Blank Duplicate Sm#

31/08/2 [NT] 010

31/08/2 [NT] 010

<4 [NT]

<0.5 [NT]

<1 [NT]

<1 [NT]

<1 [NT]

<0.1 [NT]

<1 [NT]

<1 [NT]

NATA

ACCREDITED FOR


Duplicate results


[NT]

[NT]

[NT]

[NT]

[NT]

[NT]

[NT]

[NT]

[NT]

[NT]

Duplicate results


[NT]

[NT]

[NT]

[NT]

[NT]

[NT]

[NT]

[NT]

[NT]

[NT]


LCS-6 31/08/2010

[NR] [NR]

[NR] [NR]

[NR] [NR]

[NR] [NR]

[NR] [NR]

[NR] [NR]

LCS-6 125%

[NR] [NR]

LCS-6 116%


LCS-4 31/08/2010

LCS-4 31/08/2010

LCS-4 102%

LCS-4 101%

LCS-4 105%

LCS-4 106%

LCS-4 102%

LCS-4 110%

LCS-4 105%

LCS-4 104%

Page 12 of 14

}



Moisture

Date prepared -

Date analysed -

Moisture % 0.1


METHOD

lAB.B

Blank

31/0B/2 010

31/0B/2 010

<0.10



Page 13 of 14

Client Reference:

Report Comments:

Asbestos ID was analysed by Approved Identifier: Asbestos ID was authorised by Approved Signatory: Asbestos counting was analysed by Approved Counter:

Asbestos counting was authorised by Approved Signatory:



Not applicable for this job @ERROR @ERROR

NT: Not tested INS: Insufficient sample for this test NA: Test not required

PQL: Practical Quantitation Limit

RPD: Relative Percent Difference >: Greater than

NA: Test not required <: Less than LCS: Laboratory Control Sample

Quality Control Definitions

Blank: This is the component of the analytical signal which is not derived from the sample but from reagents, glassware etc, can be determined by processing solvents and reagents in exactly the same manner as for samples. Duplicate: This is the complete duplicate analysis of a sample from the process batch . If possible, the sample selected should be one where the analyte concentration is easily measurable. Matrix Spike: A portion of the sample is spiked with a known concentration of target analyte. The purpose of the matrix spike is to monitor the performance of the analytical method used and to determine whether matrix interferences exist. LCS (Laboratory Control Sample): This comprises either a standard reference material or a control matrix (such as a blank

sand or water) fortified with analytes representative of the analyte class. It is simply a check sample. Surrogate Spike: Surrogates are known additions to each sample, blank, matrix spike and LCS in a batch, of compounds

which are similar to the analyte of interest, however are not expected to be found in real samples.





Envirolab Reference: 45124-A Revision No: R 00 NATA

ACCREDITED FOR


Page 14 of 14

{

Envirolab Services Pty Ltd ABN 37 112535645

12 Ashley St Chatswood NSW 2067 ph 02 9910 6200 fax 02 9910 6201


CERTIFICATE OF ANALYSIS 45231 Client:

CH2MHILL PO Box 5392

Chatswood NSW 1515


Sample log in details: Your Reference:

No. of samples: Date samples received: Date completed instructions received:

Analysis Details:

406484, Hunters Hill 1 Soil 26/08/2010 26/08/2010

Please refer to the following pages for results, methodology summary and quality control data.

Samples were analysed as received from the client. Results relate specifically to the samples as received. Results are reported on a dry weight basis for solids and on an as received basis for other matrices. Please refer to the last page of this report for any comments relating to the results.

Report Details: Date results requested by:

Date of Preliminary Report:

Issue Date:

6109110 Not issued

3/09/10 NATA accreditation number 2901 . This document shall not be reproduced except in full. This document is issued in accordance with NATA's accreditation requirements. Accredited for compliance with ISOIIEe 17025. Tests not covered by NATA are denoted with *.



Nancy Zhang Chemist



e'{4£-0 ~(C'r~ Rhian Morgan Metals Supervisor

Page 1 of 14

vTPH & BTEX in Soil

Our Reference:

Your Reference

Date Sampled

Type of sample

Date extracted

Date analysed

vTPH Cs - Cg

Benzene

Toluene

Ethylbenzene

m+p-xylene

a-Xylene

Surrogate aaa-Trifluorotoluene


Client Reference:

UNITS -------------

------------

--

mg/kg

mg/kg

mg/kg

mg/kg

mg/kg

mg/kg

%


45231-1

EVL-DUP-007

27/08/2010

Soil

31/08/2010

01/09/2010

<25

<0.5

<0.5

<1.0

<2.0

<1.0

83



Page 2 of 14

Client Reference:




Type of sample

Date extracted -Date analysed -TPH C10 - C14 mg/kg

TPH CIS - C28 mg/kg

TPH C29 - C36 mg/kg


1



45231-1

EVL-DUP-007

27/08/2010

Soil

01/09/2010

01/09/2010

<50

200

170

104



Page 3 of 14

PAHs in Soil

Our Reference :

Your Reference

Date Sampled

Type of sample

Date extracted

Date analysed

Naphthalene

Acenaphthylene

Acenaphthene

Fluorene

Phenanthrene

Anthracene

Fluoranthene

Pyrene

Benzo(a)anthracene

Chrysene

Benzo(b+k)fluoranthene

Benzo(a)pyrene

Indeno(1 ,2,3-c,d)pyrene

Dibenzo(a,h)anthracene

Benzo(g ,h,i)perylene

Surrogate p-Terphenyl-d14


Client Reference:

UNITS

-------------

------------

-

-mg/kg

mg/kg

mg/kg

mg/kg

mg/kg

mg/kg

mg/kg

mg/kg

mg/kg

mg/kg

mg/kg

mg/kg

mg/kg

mg/kg

mg/kg

%


45231-1

EVL-DUP-007

27/08/2010

Soil

31/08/2010

01/09/2010

0.4

0.4

0.4

0.3

5.0

1.5

8.9

8.9

4.2

4.4

6.6

4.6

2.2

0.5

2.2

93

NATA

ACCREDITED FOR


Page 4 of 14

Client Reference:





Type of sample


HCS mg/kg

alpha-SHC mg/kg

gamma-SHC mg/kg

beta-SHC mg/kg

Heptachlor mg/kg

delta-SHC mg/kg

Aldrin mg/kg




Endosulfan I mg/kg

pp-DDE mg/kg

Dieldrin mg/kg

Endrin mg/kg

pp-DDD mg/kg

Endosulfan " mg/kg

pp-DDT mg/kg



Methoxychlor mg/kg

Surrogate TCLMX %



45231-1

EVL-DUP-007

27/08/2010

Soil

31/08/2010

01/09/2010

<0.1

<0.1

<0.1

<0.1

<0.1

<0.1

<0.1

<0.1

<0.1

<0.1

<0.1

<0.1

<0.1

<0.1

<0.1

<0.1

<0.1

<0.1

<0.1

<0.1

113

.A NATA V' ACCREDITED FOR


Page 5 of 14

Client Reference:

PCBs in Soil


Your Reference ----- --------



Arochlor 1221* mg/kg

Arochlor 1232 mg/kg

Arochlor 1242 mg/kg


Arochlor 1254 mg/kg


Surrogate TCLMX %



45231-1

EVL-DUP-007

27/08/2010

Soil

31/08/2010

01/09/2010

<0.1

<0.1

<0.1

<0.1

<0.1

<0.1

<0.1

113



Page 6 of 14

--------------------------------------------------------------------------------~----.

• Qnsto Field Chain of Custody Record Document Number : S-ROH-F-019 ---- Safety ;and Roldiation Services

- - - - # . 'Sample Area collected GPS Location GPS Location Collected Date

ID UTM UTM by Collected WGS84E WGS84N (initials)

Al..! ~ 'l\.~-:) " ~ '4/% f f

Explanation of sampling regimes:

Code Sample analysis type

Low energy 13 Liquid scintillation counting

ySpec Qualitative only gamma spectroscopy to identify the radionuclide

I I

(Bulk) ySpec Quantitative gamma spectroscopy analysis to determine total activity Activity content in terms of Bq/g

Gross al13 Gross alpha I beta analysis to determine activity content

Comments:

Custodian: Health Physics Surveyor(s), OHP Approved by : Leader, Operational Health Physics - RPS

. , ..... --- _ .. __ . 11\~M;r~ C-U<S~ . f\l!2l<ilk! ~f)f . lhN{f(!.~ M, LL Time Analysis Rec'd into Analysis Rec'd into Analysis Rec'd into Analysis Rec'd into

Collected requir:ed lab by required lab by required lab by required lab by -

v Spec Initials Date , Y Spec Initials Date ,Gross Initials Date Low Initials Date (Bulk) , (activity) aI~ energy ~

emitters .,/ ..p

"-,",,, ftrtl/l>7

Purpose To detect the presence of low energy beta emitters such as 3H and 14C

Used for bulk screening purposes to detect the presence of non-natural radionuclides

To record identity and quantity (Bq/g) of radionuclides in samples to enable classification of materials

To record presence and quantity of alpha I beta emitting radionuclides in soils that may not be detectable by above means. Results compared with background samples

Uncontrolled in bard copy unless otherwise stated. Date Printed: 20-Aug-lO

Approved Date: 21 March 2007 Page 1 of!

• Qnsto Field Chain of Custody Record Document Number : S-ROH-F-019 -"--

SQ~~[Y and Radiation Services

Field chain of custody record for sample collection Project title: WAbrj/1~'; . NaSoN Pnf , lJ.v~rf~-s 4 111.. ANSTO reference:

ISample 10

Area collected GPS Location UTM

WGS84 E

GPS Location \Collected Date Time Analysis Analysis Analysis UTM by Collected Collected re uired required required

WGS84 N (initials) V Spec y Spec Initials Gross (Bulk) (activity) aJ~

IR hI! @i I~' 1)4/?' _ I I 0/ l.t,;, to/ ill!?!

Ii ~ Ie ¥4¥~( I ~ I jI-1!L mL J __ L 1;/ 1,£.'" 1''t-/1/f<i 1.4-Ix ./ oi~:-"\ l'rIV/;;

7-4-/ R /' jr." l'r/i/IQ

.~,-4-/9. ;/ cI joI\ l~/'ill<> ~4 /P i/ i N\ ilrff/I,;

:II- / X ,/ /.'''\ tt,-/W!>J

lSl<_Ui ' ! ~ r :A '/X' I I ' I v 1.11/\ I;vvrv .R3- ~ I ",' -. .'! I~ 1jA-IR I v li rA I,vw/Q IB3-~ I \ G .; I #7 1 14/~ I -1- 1./ lit\!\ li~/Vl~ I'';J -1 1\ " ;\ I~: 1)4/f 1_.. I I ,/ 1/(1\ Il'r/Y/IQ il;L - l 1\:,. !! I" ~ 1)..4!6 I v li,/, i'V7//Q

Uf- I I \l v i I 1$ - I lt(bY. I TU--I- V It,." liV''1/fa /

Explanation of sampling regimes: ,

Code Sample analysis type Purpose

Low energy 13 Liquid scintillation counting To detect the presence of low energy beta emitters such as 3H and 14C

ySpec Qualitative only gamma spectroscopy to identify the radionuclide Used for bulk screening purposes to detect the presence of non-natural radionuclides

(Bulk)

ySpec Quantitative gamma spectroscopy analysis to determine total activity Activity content in terms of Bq/g

Gross al(3 Gross alpha I beta analysis to determine activity content

Comments:

Custodian: Health Physics Surveyor(s), OHP Approved by: Leader, Operational Health Physics - RPS


To record presence and quantity of alpha I beta emitting radionuclides in soils that may not be detectable by above means, Results compared with background samples

Uncontrolled in hard copy unless otherwise stated. Date Printed : 20-Aug-IO

Approved Date: 21 March 2007 Page 1 oft

-.~

......,,,....c...~ . Qnsto Field Chain of Custody Record Docu",,,nl Num"", S-ROH-F-019

'. ' I ~I " .11,(1 Itnl'.:\ .... ,I: " .. l\ l l ~· :

r DCIU "Ilal. B VI ,""U.:tIoVU.J • ...,""'1 'tIooIi • "'. "' ...... 1...,1"'" __ I ._-_._-. 1 . . -J--- _._. " - q ,. •• .... .. ...,- ; ' . :.. ~ --'- , - , -. # •• . _ . _ ,~._ " I_L ....... _- .. . _ .. - ..

Sample Area collected GPS Location GPS Location Collected Date 10 UTM UTM by Collected

WGS84 E WGS84N (initials)

tV · r'l ¢ J.5/i!:f) t" .

" ,\ ~-

""'",,\ ') 1. 1 // # ~Ylz//(J , f', ~-_ . \1 "

-

Explanation of sampling regimes: Code Sample analysis type

Low energy p Liquid scintillation counting

ySpec Qualitative only gamma spectroscopy to identify the radionudide

(Bulk) ySpec Quantitative gamma spectroscopy analysiS to determine total activity

Activity content in terms of Bq/g

Gross aI~ Gross alpha I beta analysiS to determine activity content

Comments:

Custodian: Health Physics Surveyor(s), OHP Annroved bv: Leader. ODerational Health Physics - RPS

Time Analysis Rec'd into Analysis Rec'd into Analysis Rec'd into Analysis Rec'd into Collected required lab by required lab by required lab by reauired lab by

ySpec Initials Date ySpec Initials Date Gross Initials Date Low Initials Date

(Bulk) (activity) alP energy p emitters

, 'I 1/ ,- .tl'-\. i'i'l9//0

. : V /.~ ilifrl-o



To record identity and quantity (8q/g) of radionuclides in samples to enable classification of materials

To record presence and quantity of alpha I beta emitting radionuclides in soils that may not be detectable by above means, Results compared with background samples

Uocootrolled io bard copy unless otherwise Slated. Date Printed: 18-Mar-IO

Approved Date: 21 March 2007 Page 1 ofl

,ll' ~. ~ :.\;.\~:':' -""""'- \,lnstc Field Chain of Custody Record OOCU'"" ''' N",no".. S-ROH-F-019 ' . "·1 . 111.1 IC j. I .. 111 • • 1 ... ~,\, ' \

IrU~IU \oIDCII .. VI "U~lVUy I~"VIU IVI ~ClllIpl~ "VII~"l.VIB r I UJe:\.il 1I11e:. 1.lOl.P.-Jl .y iAJJ>,c.. /'IK'ij {1,/ nk,/1'fINI~) -ft1~~ AI\!" I U rererence: Sample Area collected GPS Location GPS Location Collected Date

10 UTM UTM by Collected WGS84 E WGS84 N (initials)

At.i~ "-,:P. • .1- L,.. ..... 0") 4? f 7~')/;Q ' --:,1 / ; I - (y(lf"~~ N" S 4t '7!~!'" f. , .. U

1< -! ;; - , .- },is n;.~\.:k.riF - ~ nlr/lo ';4 ( I - , "lill n- ~ -:U Ec.;H'.;J t:.t I ! 'J. ') 6

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~ ~ '?It )..lIR IC) , ~, 7-7/7/10 .

1/

Explanation of sampling regimes: Code Sample analysis type

Low energy /3 Liquid SCintillation counting

ySpec Qualitative only gamma spectroscopy to identify the radionuclide (Bulk) ySpec Quantitative gamma spectroscopy analysis to detennine total activity Activity content in tenns of 8q/g

Gross aI/3 Gross alpha / beta analysis to determine activity content

Comments:

CustOdian: Health Physics Surveyor(s), OHP Annroved bv: Leader. Ooerational Health Physics - RPS

Time Analysis Rec'd into Analysis Rec'd into Analysis Rec'd into Analysis Rec'd into Collected required lab by required labbv reauired lab by required lab by

ySpec Initials Date ySpec Initials Date Gross Initials Date Low Initials Date (Bulk) (activity) aI/3 energy /3

emitters ,/' j!.VI. It,fI//a ~ .. ,/ j!,f>I\ 1c.,./7jJ.(J ,

/ ;lI'i\' i~J'I/IrJ ,/ I~ ILr/<t/I<i ;/ ,1r11 I4-J1/I~

/' t./l I/~/r;/,; ,/ " .... , Jl;/'I!!rJ



To record identity and quantity (8q/g) of radionuclides in samples to enable classification of materials

To record presence and quantity of alpha / beta emitting radionuclides in soils that may not be detectable by above means. Results compared with background samples

UncontroUed in hard collY unless otherwise stated. Date Printed: 18-Mar-IO


~~ AIr\oIt1IIIII"c..n-_ Qlnsto Field Chain of Custody Record Document Number : S-ROH-F-019

~;IICI\' ~lIlct Kad j"Hlll1 ' :.:r\' IC,'\!"

Field chain of custody record for sample collection Area collected GPS Location I GPS Location Ir .... II",,.+,,,AI

UTM UTM WGS84 E WGS84N

Explanation of sampling regimes: - -

Code Sample analysis type

Low energy ~ Liquid scintillation counting

ySpec Qualitative only gamma spectroscopy to identify the radionuclide. (Bulk) ySpec Quantitative gamma spectroscopy analysis to determine total activity Activity content in terms of Bq/g

Gross a./l3 Gross alpha I beta analysis to determine activity content

Comments:

Custodian: Health Physics Surveyor(s), OHP Approved by: Leader, Operational Health Physics - RPS

v IN\ ./'

;/

;/ IJtv\

v lirv\

Purpose To detect the presence of low energy beta emitters such as ~H and 14C



To record presence and quantity of alpha I beta emitting radionuclides in soils that may not be detectable by above means. Results compared with background samples

Uncontrolled in hard copy unless othenvise stated. Date Printed: 18-Mar-l0


I t

CH2MHILL Project Name

location Hunters Hill Wast'~ Classificati

Project Number 406484

Project Manager Ben Fanner

Sample Manager Ben Farmer

0420810697

T3skOrder

Project ANSTO HUNTERS HILL

Turnaround Time 5 Days

Shipping Date: 24/08/2010

coe Number: HTH-EVL·002

OATE

EVL·DUp·OO1 24/0812010

EVL·DUP·OO2 24/08/2010

Signatures Approved by

Sampled by

Relinquished by

Received by

Relinquished by

Received by

A-f1J 7 :2

CHAIN OF CUSTODY RECORD

ConlaiM. orange OIanoe 25Om1 15Om1

4'C 4'C PrHervalives:

F1lerecl NA NA HoldIng TInw. 21 14

~ ~ 3: .:, s: =il go :l:

~ !!I 8 ~

TIME Matrix

Soli X X

Soli X X

...

DatelTime Shipping Details

Mett\od of Shipment: Courier

. On lee: yes I no

=-e318 Alrblll No:

.Lab Namo: Envirolab

·Lab.Phone: (029) 910-6200 -----

ATTN:

24108/2010 4:S3;4~ PM

TOTAL NUMBER OF CONTAINERS

; 12 Ashley SI • . ~. EnllifUlau ..,,,TV.;''';·

~~'llifG' Chats\Nood HSW 2()61 ' _ .' Plt,1I910620

0

.~~ 4CSlX>7 •• ,,~e rocelvad: ~ '5 f> ~. :1' 1\" raco.\.,cd: ~"'''-

';" :""v~a' ,.";";lU: ;00: .... " i'r.9: III ek .. . .• ,.,. \ lac rokenlltOllR

Specl"llnstructions:

Quote # SY-517·10

Sample Custody

and Report Copy to Jacinta Hurst Ben Farmer

99600200

Page OF

Z

~ CT ~ 2-g

~ .. til

COMMENl$

2

2

4

CH2MHIU. ,-----.

<Xerge Project Name COntainer 250m!

Location Hunters Hill Waste Classific:ati 4'C

Proj..,ct Number 406484 Presarvativ_

Project Manager Ben Farmer Filtered: NA

Sample Manas..,r Ben Farmer Holding Time, 21

0420870697

Task Order

Project ANSTO HUNTERS HILL C/) a>

Turnaround Time 5 Days . :x:

Shipping Date: 23/0812010 ;s: Qo

COCNumber: HTH·EVL'()01 ~ 8

DATE TIME Matrix

EVL·DUp·OO3 I 23/Q812010 I I Soil X

- --

! Signatures DatelTime I Approved by Sampled by

Relinqui!,hed by

Received by -~ 1:~ /8" 7 10 Relinquished by

Received by

CHAIN OF CUSTODY RECORD Orange 150ml

4'C

NA

14

en a>

~ ~ m ... ~

X

- ---- ---- ----

Shipping Details

M.thod of Shipment: Courier

On Ice: yes I no

AirbillNo:

lab Name: Envirolab

Lab Phone: (025) 910~200

23108120106:50:59 PM Page OF 1

,

Z c 3 ~

~ ~

b> a .. 5' m Ci1

COMMENTS

2

TOTAL NUMBER OF CONTAINERS 2 ----- ----- --- - ---

SpclCiallnstructlons: ATTN: Quote #SY·517·10

Sample Custody

and Report Copy to

Jacinta Hun:1 Ben Farmer 9950 0200

~~ Einvlrolab Sorvlce",

12 Ashiev $! :Y\tola Chatgwood NSW 201),

..-- Ph,' 9910 62[1r:

~ '-Iro ~<f-Dat.,ocelve<l, 'lJf( a- (. Q

TI .... ,...-Ivcd: k ~o.I~~tI by; S > :a .... ;~""'b·lenl

;(;,",,'PIIIIIIIIIII~ . ;> ,~lUitYi InIlGIII''III~'''NC:>

CH2MHULL CHAIN OF CUSTODY RECORD 27108120102:19:24 PM Page 1 OF 1

, Project Name Container Orange Orange 250m! 150m!

l.ocation Hunters Hill Waste Classiflcati 4'C 4'C

Project Number 406484 Preservatives:

Project Manager Ben Farmer Filtered: NA NA

Sample Manager Ben Fanner Holding Time: 21 14

0420870697

I Task Order

Project ANSTO HUNTERS HIl.L CJl CJl Z OD OD c:

Turnaround Time 5 Days . 3 r ~ <T

Shipping Date: 2710812010 s: ~ II<> ~ Q. coe Number: HTH-EVL-005 ~ (II () 0 ~ 0

::s C") 0;-s-(1)

OJ DATE nME Matrix COMMENTS

EVL-DUP-007 127/0812010 I I Soli X X 2

TOTAL NUMBER OF CONTAINERS 2 ---------- ---- -- -- ----- -- -- - --- - ---- -

Signatures -DatefTime Shipping Details Special Instructions: Approved by AnN: Quote # SY-S17-10 Sampled by Method of Shipment: Courier

Relinquished by On Ice: yes J no Sample Custody

Received by AlrbillNo: and Report Copy to Relinquished by Lab,Name: EnviroJab

JacInta Hurst Ben Farmer Received by Lab Phone: (029) 910-6200 99500200

I

CH2MHIlL CHAIN OF CUSTODY RECORD

Project Name Containe~ 0,,"," . ""'"" j 250m! 150ml Location Hunters Hili Waste Classificatl 4'C 4'C

Preservatives: Project Number 406484

Project Manager Ben Farmer Fittered: NA NA , Sample Manager Ben Farmer Holding Time: 21 14

0420870697

Task Order

Project ANSTO HUNTERS HILL I , I 0 0 r r

Turnaround Time 5 Days 0 0 , Shipping Date: 26/08/2010 I ~ :;:: "0

'cae Number: HTH-EVL.o04 l/O .I (I)

~ < ' 0 0

~I DATE liME Matrix

EVL-DUP.oOS 26/0812010 Soil X X 1

EVL·DUP.o08 26/08/201 0 Soil X I X

--_.-

I Signatures DatelTlme Shipping Details

Method of Shipment: Courier

On Ice: yes 1 no

Airbill No:

11 Approved by

Sampled by

RelinqUished by

Received by

Relinquished by

~ Received by ! I

Lab Name: Envirolab

____ _ _ _ _ __ _ _ ____ , Lab Phone: (029) 910~200

ATTN:

Sample Custody

and

Jacinta Hurst

26108120105:51 :15 PM Page 1 OF

TOTAL NUMBER OF CONTAINERS ------- -

i Special Instructions:

Quote # SY-S17-10

Report Copy to Ben Farmer 9950 0200

.. _ - ---

Z c 3 C"

~ S. () 0 ::> or S' (1)

Cil COMMENTS

2

2

4 ------

I !

C112MHILL Prolect Name Container Orange

250ml Location Hunters Hill Waste Classlfieati 4'C

Preservatives: Project Number 406484 Project Manager Ben Farmer Filtered: NA

Sample Manager Ben Farmer Holding Time: 21

0420870697 Task Order

Project ANSTO HUNTERS HILL :x 0

Turnaround Time 5 Days r-a

Shipping Date: 25/0812010 :x: :;::

coe Number: HTH-EVL-003 00 <n g

DATE TIME Matrix

EVL-DUP-004 25/08/2010 Soil X

EVL-DUP-OOG 25108/2010 Soil

Signatures DatelTirne Approved by ---Sampled by ... -Relinquished by

Received by -,-

Relinquished by

Received by

CHAIN OF CUSTODY RECORD Orange Orange Oran9" 150ml 250ml 150ml

4'C 4'C 4'C

NA NA NA

14 21 14

5 U> en r '" '" 0 , , :x ~ ~ :;::

"0 "0 Il" I _I

~ ~ ~ ~ ~

X

X X

Shipping Details

Method of Shipment: Couriel

Onlee: yes 1 no

Airbill No:

Lab Name: Envirolab

Lab P.hone: (1)29) 910~200

ATTN:

Sample Custody

and

Jacinta Hurst

25108120107:52:02 PM


Special Instructions:

Quote # SY-517-10

I Report Copy to

Ben Farmer i 99500200

Page 1 OF 1

z c: 3 C"

~ ~ (') 0 :::> ;;;-5-(1)

<il COMMENTS

2

2

4

CH2MH8lL CHAIN OF CUSTODY RECORD

Project Name Container Orange ~-j 250ml 150m!

Location Hunters Hili Waste ClaslllficliI.ti 4'C 4'C Preservatives:

Project Number 406484. I

Project Manager Sen Farme·!· Filtered: NA I ~ Sample Manager Ben Farmer Holding Time: r-21~ r-- -.~

0420870697

I I Task Order

Project ANSTO HUN.TERS HilL (Il l (Il ! Turnaround Time S Days ~I ~1 I ~ . Shipping Dllte: 2410Ilt2.0.1O. ~l ~ I cae Number: HTH·!!!VL>U(}'2: (§ J ;;j i

() i >< I I

DATE TIME Matrix 1 EVL·OIJP.oOt, 2410.3120.1.0. $o,it X I I

i X f j

INl·DUP-OOZ 24108i2n~O. SaU X X I ------

Signatures DatelTime Shipping Details Approved by

Sampled by

j Relinquished by

I Received by

'\ Rellnquished by

Received by

Method of Shipment: Courier

On Ice: yes I no

Alrbill No:

Lab Name: l;1v.vlrolab.

----- -" .,.. .- - - -. - \ Lab Phone: (02,9·) 9'\Q~~QO

L-

._.

ATTN:

·Sa.mple Cust.oc:ly

and

Jacinta Hu:~1;

24108120104:53:42 PM

i


! Special Instructions:

O.IJQt~#SY-S17AO

: Report Copy to . Ben Farmel'

29.50. 020.0.

Page OF -

z c

, 3 C"

~ ~ () 0 :::J or :5" {l) .

iii I COMMENTS

2

2

~- ~----

CH2MHILL CHAIN OF CUSTODY RECORD 23108120106:46:55 PM Page 2 OF 2

ProJett Name Container ZiJHock lab Orange Orange Orange Orange Red 100mL Maroon Plastic Supplied 250ml 150ml 250ml 150ml SOmi Amber 40ml

Location Hunters Hili Waste Classifieati 4'C Nona 4'C 4'C . 'C 4'C NitricAeid 4'C He! Acid Preservatives:


Project Manager Ben Farmer Filtered: NA NA NA NA NA NA NA NA NA

Sample Manager Ben Farmer Holding Time: 180 14 21 14 21 14 180 21 14

04211870697

Task Order

Project ANSTO HUNTERS HILL I I ~ ~ ~ z

~ 0 0 tJ) (Jl '" c: m ,... r '" '" . . 3 Turnaround Time 5 Days "tI 0 0 0 0

'" ~ 0 0 0 I ~ ~ 0' 0 '" I .I CD Shipping Date: 23/0812010 0 0 I ~ ;: "tI " "tI ~

> 0 ;: "tI flo I '" 0 I 0 .. OJ 2" _I (Jl ..:! 0 -COCNumbef: HTH-AlS-001 0'

~ m

"tI !.'.l 0 CD (Jl < -I ;: .. g OJ 0 ~ ~ 0 (; -I "tI m S .. m 0 0 x x In til 5' CD ii!

DATE llME Matrix COMMENTS

eM 23/0812010 Soil X X x 3 C8-1 23/0812010 Soil x x 2 C9-1 2310S12010 Soil X x 2 RIN·230810 23108/2010 Water X X X 4 TB-230S10 2310812010 Soli X 1

1S·230810 23108/2010 Soil x 1

TOTAL NUMBER OF CONTAINERS 45 -------------------- ---- ----- -- ---- -- --- -- ---- - ---

Signatures DatelTime Shipping Details I I Special Instructions:

Approved by ATTN: , Quote # SY-517·10 Sampled by Method of Shipment: Courier --

Onlee: yes I no I Relinquished by Sample Custody

Received by Airbill No: and I Report Copy to ----Relinquished by Lab Name; ALS Laboratory Group

Brenda Hong Ben Farmer - ----Received by ·lab Phone: (028) 784-8555 I I 99500200

CH2MHILL Project Name

Location Hunt.er.;. HII.I Waste Classificali

Project Number 401>484.

Project Manager Ben Farmllr


04208:70697

Task Order

Project ANSTO, HUNTERS 1~ILt.

Turnaround lime S Days

Shipping Date: 2310812010

cac Number: HTH.ALS..{JOf.

CHAIN OF CUSTODY RECORD Container:lZiP.lock Lab I Orange I Orange l orange Orange I Red 100mL Maroon

Plastic Supplied I 250mi 150ml 250m! 150m! , 60m! Amber 40mi

, 4'C NOn,'," I. 4'C 4'CJ 4'C 4'C j Nitric At:id 4'C ,- HCIAcid I PreservativeS! ~ ,

Filtered: NA NA .. NA ' NA r"-NA NA 1 NA ' '' -NA NA

HOldingTime:~ ~, 14 I 21 P-l. 21 I 14\. 180 • 21 I 14 'I

~ m N "0 '0 0 0 00

0 :l> II> CD g ~ . -< m XI

I ' 0 r 0 , :c :;:: jlO (j)

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! I ,

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"0 .

il 0 .I !

"0 CD -<

"'0 m 0 X CD ~I

" DATE TIME Matrix J i

j ALS-OUP..oO!\

B2A

62.-~

C1.0·1

C1'-1

C1~2:

C;1-'1:

C'2,~1

C:1.1

C3·2,

~,..<!'

C4·,1

C$·:t

CG- l

G~~rovedbY , Sampled by

Rlllinquished by

Received by

R¢linquished by

\ Rel:eived by i

Z3/GS(2Q10

2311l8/2.QtQ

23108f20'lG

23101112.010

2.310812.0 70

2310Sf2!}.1,0

23'1'08:(2;0·10

23lOIIn010

23108'12010

2l10812;O10,

2.3(08120,10

23108f20to.

2;3lUaIZO ~O,

23IQ812010,

Signatures

--, X X 1

N X ) 1

J

x: I -, X

/

lC ,

1

X i

-, -X -

!7l X I (

, lC

!--l...!. L:

) J I

i )

I L-~ ! 1 1

SoU

SoU

SQil

son x I Soil X

Sol!

SoU I So!! I , Soil x: Soil

J SoU ! Soil I Soil ,

j

! X I' -' I ,

r--r I ~

~'

L I

1

t- I X

H

~ ~

I ~,

X

~ -. :x:

X

-;\ j

~ X

X \ - , X

Soil 1 \ , .X X

----DatelTime Shipping Details

'" .,,-- . Method of Shipmenl: Courier ATTN:

, On Ice: yes I no Sample Custody,

. ____ ~_-'~ = 1 Airbill No: oII.mi:

Lab Name: AlSo labQrat:ory GroUI! Brenctiili Hong

Lab Phone: (Q28:l 11l4-8'SSS

~

23108120106:46:54 PM

Special Instructions:

QUQte#. SY-S,u .. 1Q

Report Copy to B'EmFarmer 9,950 020.0

Page 1 OF 2

z c: 3 0'

~ 8. () 0 :::>

iil' s· (I)

Cil 'j COMMENTS -'

3 -2

2

3

3 -2

2,

2 -3

2 -2,

2

2 -2

CH2MHILL Project Name Container, Lab

Supplied Location Hunters Hili Waste Classlficati None

Project Number 406484 Preservatives:

PrOject Manager Ben Farmer Filtered: NA

Sample Manager Ben Farmer Holding Tima: 14

0420870697

Task Order

Project ANSTO HUNTERS HILL m

Turnaround Time 5 Days "0 0

'" Shipping Date: 24/08/2010 0

!.l:l COC Number: HTH·ALS-002 ~

DAlE TIME Matrix

1B·240810 24/08/2010 Soil X

15·240810 24/0812010 Soil X

Signatures DatelTlme !d by

. -tfby

ished by

ApproYI

Sample

Rellnqu

Receiv,

Relinq

ReceiY'

-------.------ --,d by

Ished by

!d by

L-

CHAIN OF CUSTODY RECORD 24108120104:52:25 PM Page 2 OF 2

Zip-lock Orange Orange Orange Orange Plastic 250m! 150m! 250m! 150m!

None 4'C 4'C 4'C 4'C

NA NA NA NA NA

30 21 14 21 14

:J: :J: :z :J: 6 a (/I (/I c 0 r- '" '" 3 r- 0 , 0

0 0 0 :r ~ r::1' ro 0 :r ~

;;:: "0 ~ > ;;:: flO :J: ~ ~

CD flO .J: ~ III 0 .. rJl

~ ....

0 a <5 a ~ ::l .. ~ (')

~ (') :::) CD C;;

COMMENTS

1

1 TOTAL NUMBER OF CONTAINERS 34

---- -- ._-- _ .. " - -- --. _ _ . . _ - - -- --- .-

Shipping Details Special Instruct ions:

Method of Shipment: Courier ATTN: Quote # SY·517·10

On Ice: yes 1 no Sample CUGtody

AirblllNo: and Report Copy to

Lab Name: ALS Laboratory Group

I Brenda Hong Ben Farmer

Lab Phone: (028) 784-8555 I 99500200

ofI:H~MHHLL

Project N3me Locati()n "'IU I,t.~r.;. Hilt. Wils.te C:lassUicalJ

Project Number ",064Jl4

Project Manager B(fn, ParrnQ/'

Sample Manager a.p,", farmE',r

042() 810 <>91

Task Order

Project .,.NS,,-O HUNtERS HI.l"L. Turnaround Time S Days

Shipping Date: 24J08!2011}

COC Number: H.1"f.~ .ALS"() OL.

1-

~ M ··1

A$-1

.t\L$.OU? OOl

AJ,s.OUp·OO2;

fl q

B:).-1

fl:) ,'l.

DATE

24fQ812D'tC -

2.4l(j8f~Q1 \!

:l:41[)81:2.010

:.J:4i(}!fI~01t}

;!4tt!81;Z.D1 It

24f08f2010

I ;t4!0812010

8M 1 24/0812010

BS.l

B8 .. 1

I i Apllrovcd by

I Sarnpled by

Relinquished by

'\ Received by Relinquished by

, Received by

IZ4/0312Q1Q

2410812.010

.... ~ Signatures

CHAIN OF CUSTODY RECORD Container Lab I Zip-lock Orange I Orange ~O. range Orange

Sup lied Plastic 250m! 150ml 250m! 150m! Non;;- "'"Non. 4'C ', 4'(; ' "i-c 4'C

PrcservaUvcs! =H Filtered: -NA NA NlC~ '-NA~A-'\ NA' _ .... _ .• _._ Ioo .. ___ ~ _ _ _ . ___ --...J __ _

Holding Time! 14 -'r"- " , -"~r--'2- I "

TIME

. . -

Matrix

!i~1I

SQi!

Soil

51(>[1

Soli

So!!

SQiI

S,)il

Sell

So,n

Soli

$011

Soli

SoU

DatefTime

:t :x: '. , :x: 0 0\ C/) C/) m l 0 r- r- Q) 0)

~ ' , 0 0 I

o C I X < g , :r ~ s: =rl ~ i: !: "tI ( RO I ~ g- ~ Qo ;t l ' ~I CD

m . lei ~ lIIi 01 ril Xi g 0 rill C1 x

I n x

t=I J U,

! j j

L..--.J I X , ~

. I X I

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x: x \ x x x

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Shipping Details

x: 1

::.J K I ;-r _~i X '

X -~,

X I I

----l X I

;-i ;-T

I "T

---l X

X ---i xl

- . , Method of Shipment: Courlel'

On Ice: yes I no I ' Airbill No:

Lab Name: A1.S LabQratolY Groull

Lab Phone: (02S) 784-8555 I ---". _ - --,-" .. --- ~.,,-.-----

AnN:

24108120104:52:24 PM

! Speciili instructions:

: Quote # 5"1·511· '10 J

Sample Custody I

and I , Report Copy to Brenda Hong Ben Farmer

99500200

Page OF Z

Z to 3 0'

~ a (') 0 ;a

'" :;-ro Cil -II COMMENTS

3

2

2

2. -2

tl 2 .+-= ;1

3

~' l-------2 -2

2

2 -2

. t I .

1

J

L-

CH2MHILL CHAIN .OF CUSTODY RECORD

Project Name ContalMf Orange orange Olllllge orang .. 250ml 15Om1 25Om1 15Om1

Location Hunters Hill Waste Classifi~ 4'C 4'C 4'C 4'C

Ptojecl Number 408484 P,..~eNatlves

Project Manager Ben Farmer FIltered NA NA NA NA

Sample Manager Boen Farmer Holding TIme" 21 14 21 14

0420870697

Tali" Ordcar

Pro~t ANSTO HUNTERS HILI.. ~ is Sl ~ .-Turnaround nme 5 Cays 0 o :,T" , .

I n::=- .... :t. < ShlPfllIl9 Date: ~510812010 x ~ t~ 3:

... 3: "tI

"0 ~ go X COO Number: HnI·ltvL~03

go .r." ~ ~

~ III a gJ ~ 0

DATE TIME MatriIC

EVL·OUP·004 25108/2010 Soil X X

2- eVl·IlUP-006 25JD812010 Soil X x

"--- --- - - --- - - -_____ 0 ____

Signatures Oateffima Shipping Details ApprOVed by

Sampled by Method of Shfpment Courier

Relinquished by On lee: yes I no

Received by .~~\..;. -z,.\..... U;l~ho~ ~blIINo: , Relinquished by Lab NIIfI1II: envirolab

Received by -- Lab Phone: (029),910-6200

ATTN:

2Sf08l2010 7:52:02 PM

TOT At NUMBER OF CONl'AINERS

~-~ En\llrO~b SOIVlces

12AsltleyS. iYir~~ ChafSwoodNSW2DlI1 ..-- . Ph: 991" f2GO

Job No; t\-~\ l. 't 00>10 t8calv.d: "')J; 18 lim. t"".lv,d: "f{~ a.c8I"~"'Z...~ . TQll1p:~lent

I~~~:~!~~

Speciallnatructions:

Quote # SY-611-1 0

Sampl" Custody

and Report Copy to Jacinta Hurst Ben Fanner

9950 0200

Page OF --

% c 3 <T

!!l a .~

::J Ii" or .. iil

COMMENlS

2

2

4 -.I

from: [email protected] [mailto:Ben [email protected]} Sent: Wednesday, 25 August 20107:58 PM To: Brenda Hong Cc: [email protected] Stabject: 406484 ~ CoC for Samples Collected on 25.8.10

Hi Brenda,

Please :find attached CoCs for samples collected from the Hunters Hill site at 4:00m on Wednesday 25 Aug 2010. Please schedule the specified analysis on 5-day TAT in accordance with ALS quotation SY -517-10. I note that numerous samples are currently on HOLD, however I will schedule analysis later pending request from our client.

Also, please forward samples associated with CoC# HTH-EVL-OOI to Envirolab and direct them to conduct analysis for Heavy metals, TPH, BTEX, PAR, OCP, PCB. There was some confusion from Envirolab regarding the analysis, so please ask the sample receipt crew to specify the analytes on the Envirolab CoC (HTH~EVL-003)

Let me know if you have any questions. 1 may not answer my phone immediately as our work is being completed wearing Tyvek suits, but please leave a message and I will return your call.

Also, once all analysis for this project has been completed, I will request that all samples are returned to site for disposal. I'll let you know when this can occur and will help arrange logistics.

Regards, Ben

Ben Farmer Environmental Engineer

CH2MHILL ~.

Level 7, 9 Help Street Chatswood NSW 2067 Direct: +61 2 9950 0263 Phone: +61 2 9950 0200 Fax: +61 2 9950 0600

26/08/2010

CH2MHBlL Project Name locm'lion Hunters Hill Waste Classificati


Prolect Mlllnager Ben Farmer

Sample Manager Ben Farmer 0420870697

TasllOrder

Project ANST.O HUNTERS HilL.

Turni1lround Time 5 Days

Shipping Date: 25/0812010

cae Number: HTH-Al$..,f)03

H4-l!

!:M t;;::

~.

~

I~ Ie ~ I~

R~'"

HI-250810

DATE

25/08/21)10

25/0812010

r iiiQUW'

25/08/2010

Signatures Approved by

Sampled by

Relinquished by

Received by

Relinquished by

Recoived by

I L--


c ...... omj c., .- 0"",,, 0,,",,"0_"1"'_ =-T'-1-" ,.- P •• " "0'" "OJ"'" '''''' eo"" "".. "'" Non. , None 4'C 4'C 4'C~ 4C Nitr1cAQd 4'C HCIAcld Pn!servative:s: '

_ __ ~____ __ l __ Filtered: NA NA NA NA NA NA NA NA NA

TIME M~trlx

Soil

Soli

~

~ .... .. ~

.set!'

~ .... a.tIo

\llliMl!r

Soil

I :r::r: :i: S

:r: ° .0 , ~ ~ w ~ S ·m 0 I r ~ ~ I ~ " rOO 1 1 I CD . V I

x

~o : ~ !.- ~ ~ : :; * ~ s: ~ , , ~ -l ""' 'l •• - 'l '

iDl l;> I 5: ! 'l R<> I !l! ° :r: -l g R<> ~ ~ m ~ 0 m m ~I ~ 'I m; § ~ ~ ·'l

1 -l

X g ' ° rrii 0 x iii , ~ ~ \ , 0 XI ., OJ

Ii : ! ,I [

~ i _v ·v _

x " :::I " ~ I ~ M It

.,

~'" iii I iii

""""--r A

x

x, x

x

i

I ~ J

1 j

-

I 1

DatelTime I Shipping Details

-- -----. Method of Shipment: Courier ATTN:

On Ice: yes 1 no ..... , I

Airbill No:

Lab Name: ALS laboratory Group

. ____ ___ l.lab'Phone: (028) 784-8555

Sample Custody

and

Brenda Hong

25108120107:51:10 PM

I Speci~llnstructions: Quote # SY-517-1U

I

I Report Copy to I

Ben Farmer 99500200

Page 2 OF 3

z c 3 0-

~ 8-o o :> iii oj'

'" U;

2

2

2

2

2

2

2

2

2

2

2

2

4

1

CO!VIMENTS

CH2MHIl L Project Name

Location Hunters liill Waste Classificatl

project Number 406484·

project Manager Ben Farmer


0420870697

" ask Order

Pl'Oject ANS,TO HUNTERS HILL

Turnaround Time 5 Days

Shipping Date: 25/08/2010

COC Number: HTH·ALS·003,

DATE

ALS.OUP..o04 \ 25/08[2(110

1. liiil1ii*O ~

F1"1 2510812010

F1-:l 25/0812010

Ft..s 25/0812010

G't·1 2:510812010

G2.-1 25108[2010

G2:-2: 2.510812010

G!H . 25(0612:0tO

G3·2 251081201C

H'l-'t 25/Q8120 10·

2510812010


Supplied Plaslic 250ml 150ml 250ml 150ml 60ml , Amber 40ml Contained Lab Zip-lock orange ! Orange Orange frange Red- raomL j-MaroOrlJ

None None ··.joC _~~'G 4 ;(:- 40C Nllnc ACId i 4'C " HCIACid-

Filtered: NA - '---NI>. . NA- - NA- -NA NA - NA --I--NA-.L~ pre$ervatives:~

""';" "",, -;·9 " I ,,"r ,. ,, - "-"-r'" I ~

TIME Matrix

Soil ,. Soil

Soil

Soil

Soli

SoU

Soil

SQH

Soil

SoU

- -,-- -- .. 1....3~-~·~-· i :t 6 6 00 1 00 ~ ~ ~

m 0 r r 0) 00 I CD ""0 rOO I co 1] o 0 ~ < > < ~ I I ~ ~ ~ ~ : ~ ~ 1 ~ ~ "'0 Qo I ~ ~ 0 I

~ g flo ;r:l til 00 ~1 Cl in ~ S ~ ~ ~ ~ ~ ~ ~

I ",Om 01

:x ~ ~ ~

x \

~ ..l

I X I

x

x

o Xl"' 00

x

Y' ".

x x

x x x x :x.

x x I x x I x x

! x I X I X . X 1

I Soil I I x X I Soil

2510812010 7:51:09 PM :Page OF 3

z c: 3 0'

~ !a. () 0 ~

0; or '" Cil

~ COMMENTS

2

2.

3

2

2

2 -2,

2

2

2 -.3 -2

2.5(01)'12.010 3;

I x \ X

X I \ : I : I Sotl I x I x X I \I--;\r-----I

,.--'\ \ Approved by

I Sampled by

RelinqUished by

! Received by

'\ Relinquished by Received by

2510812010 I Sou I \ x I X I SoU

-.--.- "------------.-~ .. -Signatures DatefTime r- ·--- ·----S-h-iP-pi~~-D-et.;;ls

·1 Method of Shipment: Cl}Urle-r I

On Ice: yes I no

Airbill No:

Lab Name: Al.S l,.a.bOl atol.Y GirQup _____ " .. _''' ____ " .. .. --= \ Lab Phone: (0·2.8) 784..-85.55:

''''1

ATTN:

Sample· Custae:!\'

and

Brenda Hon.g

2 -_ ..... _-- -----

; Special Instructions :

QUQt(~ #; S ,(·517·1 0

'I: Report Copy to Elen Farmel' 9950 O~OO

CH2MHULL Project NIIIIYle

Location Hunters Htil Waste. Classlflcatl

Project Number 4Q6484.

Project Manager Ben Fanner

S2ml,le Manager Ben Fa,rm.e,,· 04208706097

Tasl< Order

Project ANsrO HUNTERS HU •. l Turnllround Time 5 Days

Shipping Date: 2m0812.01.0

coe Number: HTH·Al.S:.l)(fS

ALS-D.UP·007

11 .:1

1:}-1

1.4-1

15-"

~ RIN.2.70610

TB·270810

TS-270S10

OAtE

2.7fOB/2!l10

:t71C)812.010

2.7/08/201.0

2710812010

27106/2010

27108/2010

27/08/2010

2.710812010

r·--· .. -----·--··---· .. ·--··-·--.. --.. ·-.. ·

Signatures Approved by _. __ . ___ ._. ___ _

Sampled by

i RelillqYished by

Received by

Relinquished by


Filtered:\ .!l~ ~~~~~ ~. __ NA I NA

Holding Timor ~30 ~.-~-t 21 14

i

I tB i 0\

~ l wi

~ I !

! tlME Matrix

:I: a r , O f , I

~ j <> ~ a C/I

:I: a 5 .:I: :;: II> en C§ (')

:I: a r o ,

~ i _:I:

~ m x

en l 00 1

i i :;: S10

~ (')

U> 00 . ~ "U :I:

~ m X

Red I 100mL I' Maroon ) SOml ! Amber , 40ml 1

NiUicAcid \~ HCIAcid i

NA

180

~ Q)

:I:

" ~ s:: !l .. iii

1 !

! NA \ NA

--~~ 1~-=-

~ , '-0 » ;I a o ."0

" I 0 , Wl

! i

~

~ " .:I:

~ m X

Soli .x l( I Soil

Soli

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Sol!

'IIIIIftI ... Water

Soli

Soil

x:

.. , "'" ... -1 S .

x I x

x )(

x X

x j X

X x

I X x I X -- I

27108120102:18:47 PM Page

z c: 3 C1'

~ 8. (') o ::J iii 5 ' CD Cil

2.

3

2.

2.

2.

2.

2

4

1

1

TOTAL NUMBER OF CONTAINERS U 21

. ~.-------

Date/Time Shipping Details I SpeciallnstrYctions:

Method of Shipment:

On' Ice: yes I no

, Airbill No:

CourIer

'--.- '-'-. -_~ .. =- -~ " Lab Name: ALS Laboratory Group

ATTN: . Qyote # SY-511.10

Sample Custody

and

Brenda Hong

Report Copy to

Received by • ____ _ ._ .... _ .. _._ .. __ Lab Phone: (028) 784-8555 Ben Farmer 9950 0200

OF

CO~~MEtnS

CH2MHU_L i Project Name

Location Hunters HlII Was.te Classificatl

Project Number 1\06484

Project Manager Ben Farmer

Sample Manager Bcn Farmer

0420870691

Task Order

Project ANSTO HUNTERS HILI..

Turnaround Time S Days

Shipping Date: 23/08120 '10

coe Number: l-m~·I,;Vl_·OO1

OATE

EVL.O\JP..QQl \2.3IQ81201Q \

Signatures

CHAIN OF CUSTODY RECORD 23108120106:50:59 PM

Container Orange Orange 250m! 150m!

- -- 4'C I ~'C I Preservatives:

I-c--.l-.-Filtered: NA NA

~ ---'--

Holding Time: 14

(f) ~ , '" ,

I < f ;:: ~ l jlo , I (n ' 0) < --< 0 ~ ()

TIME Matrix

\ SoU x. ! x:

.. -- -

---' ' ~~~'. -- -.. ·.-r--- -----. Date/Time Shipping Details

-. -- - ----.. -.. - - Method of Shipment: CQI.!!'i~~-

-- On Ice: yes I no

- - -.... . Airbill No:

Lab Name: i;:Oyfr-ofab

Lab Phone: (Ol9} '!HQ~QQ


------r---·--------S;~~i;l·i;;t;~~tion;_--

ATTN: Ql1.l?t~#- $Y.S17-1Q

s .. _ttlP~~ CustQ.dy

al'.1i

""t;;i.nla. HUlst

Report Copy to Be-II FII.rmm· 99500200

Approved by

Sampled by

Relinquished by

Reteived by

Relinquished by

Received by _____ _ _ ·oo~_-...., .......... _ __ _ _ __ ,.-._ .. ,

Page OF

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u: 2. (') 0 :::> , or s· Cl)

ijl '

COMMENTS

2

2

·ift

Page 1 0{2

Aileen Hie

From: Richard. [email protected]

Sent: Monday, 30 August 2010 12:57 PM

To: Aileen Hie

Cc: [email protected]:n.au

Subject: RE: 406484 Hunters Hill, CH2MHILL, Samples on Hold

Hi Aileen,

Three of the samples submitted for analysis last week from our site in Hunters Hill were provisionally scheduled as 'On Hold' until we received client approval . The client has given the go ahead to analyse these samples in accordance with the schedule outlined in the associated COCs provided to you. The samples that were on hold and the associated coe number are summarised

below:

Sall!PlelD Date COC Reference ALS-OUP-OO4 25/08/2010 HTH-EVL-003 ALS-OUP-005 26/08/2010 HTH-EVL-004 ALS-OUP-008 26108/2010 HTH-EVL-004

Please go ahead and conduct the required analyses. Feel free to call me at (02) 99504221 should you have any questions.

Kind regards,

Richard Hayes ~:H2M HILL Australia Ply LId f . • 61 299500221 , "6 t 299500600 I >Jvel 7. 9 Help Streel '.~hatswoo[j 2067 www.ch2m.com

Ji Think before ycu print.

From: Farmer, Ben/SYD

Z> e;VI"i~leib P-ef:. 4S'"I2-'t A OJe! 'I q-{lO

stet T f ~ .

Sent: Monday, August 30,201011:52 AM To: Hayes, Richard/SYO Subject: FW: Sample Receipt for '45124 - 406484, Hunters Hill'

From: Aileen Hie [mailto:[email protected]] Sent: Thursday, 26 August 2010 5:21 PM To: Farmer, Ben/SYD Subject: Sample Receipt for '45124 - 406484, Hunters Hill'

Please refer to attached for a copy of your coe and our Sample Receipt Advice (SRA).

Results will be available by 6.30pm on the date indicated.

Enquiries should be made directly to: Aileen Hie on [email protected]

30/08/2010

or Jacinta Hurst on [email protected]

Regards

Envirolab Services 12 Ashley StChatswood NSW2067 ph 0299106200 fax 0299106201 www.envirolabservices.com.au

..... _ ...... _-------_._--<:ONFIDENTIALITY NOTICE

'he informalion contained in these documents Illay be privileged and confidential ,,'\0 is intended for the exclusive use of the addressee designated abol/e. If you :H e not the addressee. you are herelly notified thai any disclosure. reproduction. disiribution. or other dissemination or use of this communicalion is strictly ufoh,bited . If you have received Ihis transmission in error. please infDrm us "'Hi cJeslroy Ihe original message. The opinions expressed in this correspondence .~re not necessarily tllOse of Envirolab Services Ply. Ltd. Thank you. Th.s e·mail message has been scanned for Viruses.

30/08/20 10

Page 2 of2

I )

Australian Government

Certificate Number: 10MR0062#9 201010239-9

Client:

Company I Org~nisation:

Sample Identification:

Analysis required:

Analyst:

Sample measurement started at:

Radionuclide

234Th

234mpa

2~h

214Pb

214Si

210Pb

228Ac 228Th 224Ra 212Pb

2128i

208TI

"nsto Nuclear-based science benefiting all Australians

Institutefor Environmental Research

Ph: (02)97173419

CERTIFICATE OF ANALYSIS

Robert Blackley

ANSTO-Safety for commercial

B1-1

Gamma-ray Spectrometry

Lida Mokhber-Shahin

14/10/2010 11 :52am

Fax: (02) 9717 3212

Activity (Bq.kg-1) % Uncertainty (10-)

650 10

610 10

580 10

300 10

280 10

207 10

50 10 < 210

47 21

49 10 58 10

17 10

30 17

34 10

87 10

Note: The reported activities are in the dried sample. The sample moisture content is 11.9 %.

/ /)

Results Calculated By : ~

Lida MOkhber-Shahin~ Date: i g !) Illv

f 'esult5 Checked G:/; Pate : (8 It t / 10 A LI :: T I, A I I.t.. N N U " L E IJ, R ~ e l F. Ne b A f'J 0 ; :: C H N C ~ 0 C Y Co [< G A N I SAT IO N

~-------

Ne\ fl1a~': m a l ad, Luc as Hdl~ hl : :Lockeu Ba g 2001 Kir rh de e D'.' NSW 2232) 1 +E, 29. ,7311 1 F +61 : :,5~? 3097


Certificate Number: 10MR0062#17 2010/0239-17

"nsto Nuclear-based science benefit ing all Australians


Ph: (02) 97173419 Fax: (02) 9717 3212


Client: Robert Blackley

Company I Organisation: ANSTO-Safety for commercial

Sample Identification: ANS-Dup-002

Analysis required: Gamma-ray Spectrometry

Analyst: Lida Mokhber-Shahin

Sample measurement started at: 20/10/2010 16:47pm

Radionuclide Activity (Bq.kg-1) % Uncertainty (10')

234Th 740 10 234mpa 880 14 23~h 650 10 214Pb 310 10 214Bi 300 10 210Pb 230 10

228Ac 58 10 228Th < 270 224Ra 46 22 212Pb 52 10 212Bi 66 10 208TI 17 10

235U 34 16 227Th 39 10 4°K 72 19


4 Results Calculated By: Uda MOkhber-Shah~ Date:

Results Checked By: Julia Martin iello . >P:i""",,~L· D,te: 1'6' /1, /1 D A U S T R A L I / , f\: N LJ C L .: r\ f1 S C I ENe E r N D T E: ( J rl NO L. 0 G Y 0 Fi ' ] A N I S A'- iON .--- - - . -New I!'; WBI ' 8 Re ar:, Lu cas Hei ghts ILoGkeo Sag 2001, KW3wec 9C t~~W 2232) r G1 2 B717 ~\ \ 1 F +612 95". J 50~']

www ar. -I v.gr,".au

I j

j

I I




Institute for Environmental Research

Ph: (02) 9717 3419 Fax: (02) 9717 3212


Client:

Company I Organisation:


Analysis required:

Analyst:


Radionuclide

234Th 234mpa

230Th 214Pb

214Bi

210Pb

228Ac 228Th 224Ra 212Pb

212Bi

208TI

Robert Blackley


B2-1


Lida Mokhber-Shahin

15/10/2010 14:36pm

Activity (Bq.kg-' )

2100 2200

3800

2600

2600

2600

101 < 490

< 91

98 110 31

130

310 170

% Uncertainty (10')

10

10 10

10

10 10

10

10

10 10

10

10

10


Results Calculated By: A-r

Lida MOkhber-Shahi~ Date: 16/11/10

R It r' h 0 d B I ,- '" rt ' . " / /<'/ ' D t I / o (, S u, S 'oJ (. ,1 ,(, 'j: v J 10 ",a Inle l O ,, 'l ( -" x :;:.: ? e' ,? /II r' o -:.

A I J S ! R I I L I A I\J ~{ LJ e L L 1:\ R S C I [ Ne E i-. I': D r f.: C , ~ N 0 L e G y 0 R G f', hJ I ':) A -: : \.) N - - - - --- - - - - -Nc"v 11I {lI'.a rr <1 Roa d,: ' I Ci), Heigh's ILocked Sa,; 7001, Kirrn>N8 e DC NSW 22 32 ) T '0 1297' 7311 ' f +0, 2 95t.3 5097



Qnsto Nuclear·based science benefiting all Australians

Instilutefor Environmental Research

Ph: (02) 9717 3419 Fax: (02) 97173212


Client:



Analysis required:

Analyst:

Robert Blackley


B2-2



Lida Mokhber-Shahin

18/10/2010 12:27pm

Radionuclide

234Th 234mpa

230Th 214Pb

214Bi

210Pb

228Ac 228Th 224Ra 212Pb

2128i

20sTI

Activity (8q.kg'l)

1400

1300

1200

1400

1400

1100

70

< 320

100

65

83

19

72 42

79

% Uncertainty (10-)

10

10

10

10

10

10

10

19

10

14

10

12

10

17

Note: The reported activities are in the dried sample. The sample moisture content is 20.5%.

Results Calcu lated By:

~/

Lid. Mokhber-Sh.hin ft Date:

Results Chec ~'erl By: julia rll1artiniello ..-: ~._ -o:.~ " . ./ - -~

Date: f? Ii I / " ,

: . U S T R '.\, L I A 1\1 N U C! E / , >i SCI E N ~ E A f\ D T Ee H r i o L ;J G y 0 R G A I, I S/I T I (j N --- - - - - ---

:~ew :Iaw, [( a Ro nd , LUCiJ ' HI-. ;J ilts (Locked Bag 2W)1 , K;I raw ee DC NSW 2"32) .,. t61 ~ ~' 7 1 7 ~ 111 F; G 1 2 ~543 5G97 1,..,r'/W.?r-; 5tO. 1., 1\' ,au

1

)





Ph: (02) 97173419 Fax: (02) 9717 3212


Client:



Analysis required:

Analyst:


Radionuclide

234Th 234mpa

230Th 214Pb

214Si 210Pb

228Ac 228Th 224Ra 212Pb

212Si

208T1

Robert Blackley


83-1


Lida Mokhber-Shahin

15/10/2010 13:29pm

Activity (Bq_kg-1)

73 < 83

200

290

290

140

49

< 140

40

44

53

15

< 7.5

7.2

74

% Uncertainty (10-)

10

14

10

10 10

10

14

10

10 10

15

10


" ,-

Results Calculated By: Uda Mokhb.,-Sha hin ~- Date: (/]/ 1 (/ / I)

Re!Jul ts C;r,~cked By:

:. US T R A LIt... ~ 1 N LJ C ~ E /\ R S C' E N ~ F. AN l) :- c C H N () LOG Y ) R G A N I:; AT iON --- -----~:~w ll l awarrc ~ oa(j . ~uc? Heigh ls (Lo r '8 d r) ' g2%1, Ki r(3we el ' C N~1I/ 211?: r ·612 9"'i3iI 1 F+512 95 43 5097



Nuclear-based science benefiting all Australians


Ph: (02) 97173419 Fax: (02) 9717 3212


Client:

Company / Organisation:


Analysis required:

Analyst:

Robert Blackley


B3-2



Uda Mokhber-Shahin

18/10/2010 14:1 5pm

Radionuclide

234Th 234mpa

230Th 21 4Pb

2148i

210Pb

228Ac 228Th 224Ra 212Pb

21 28i

208TI

Activity (Bq.kg01

)

< 14

< 160

< 110

44 41

44

86

< 210

83 82 95

28

< 14

< 5.6

400

% Uncertainty (10')

10

10

11

10

10

10

11

10

10


Results Calculated By:

~/

Uda MOkhber-Shahi~> \ g / 1: /1". Date : I

f:csul ts f: r: ec!~ ed ry: Julia 'Vl arti nici!o .:.-' ::f:'- :--....._2~. Date: is' / ./ /1 <:>

A U :; T rl At.: ," N N U ' LEA R SCI E\J C F AND T l C ~ , N Ul 0 G YO;' oJ h .~ I ~ A T ION - - - .- - - . - - - -- - --

N £ . J 'Ilawa rr il [hId, ll,,; as f: ~ :g h ts (lo cker' Sa .. 2001, ,,:rrawee DC 'vSW 2232' r 161 2 971~ ~111 r +6 : 'L %43 5097 ';,[Wyo ilnS:3.]Dv.a L



Qnsto Nuclear·based science benefiting all Australians

Institute/or Environmental Research

Ph: (02) 9717 3419 Fax: (02) 9717 3212


Client:



Analysis required:

Analyst:


Radionuclide

234Th

234mp a

230Th 214Pb

2148i

21°Pb

228Ac 228Th 224Ra

212Pb

212Bi

208TI

Robert Blackley


84-1


Lida Mokhber-Shahin

20/10/2010 16:59pm

Activity (Bq.kg-1)

19

< 100

< 87

25 25 25

42

< 129

35 38

51

12

< 8.9

< 4.3

270

% Uncertainty (10-)

23

10

10

16

10

15

10

11

10

10

Not e: The reported activi ties are in the dried sample. The sample moisture content is 10.3 %.

#'"

Results Calculated By: Lido MOkhbe' .Shahl$ Date: I hi II! /'

Date : i~ It· / , (j

.£\ U S f :{ A LI c- f'd f\! U l c :: II. '1 S . lEN C E .' .~ 0 T L l . H r'J 0 L C>: Y 0 F< G A N I S /I I I () N

WNW 0 ... ,10.£' v.au



Qnsto Nuclear-based science benefiting all Australians


Ph: (02) 9717 3419 Fax: (02) 9717 3212


Client:



Analysis required:

Analyst:


Radionuclide

23~h

234mpa

23~h

214Pb

2148i

210Pb

22BAc 228Th 224Ra 212Pb

2128i

206TI

Robert Blackley


86-1


Lida Mokhber-Shahin

20/10/2010 15:49pm

Activity (Bq.kg-1) % Uncertainty (10')

3900 10

3900 10

7900 10

9700 10

9600 10

7900 10

170 10

< 1000

220 24 160 10

190 10

54 10

230 10

790 10

200 10


ff

Results Calculated By: Lid, MOkhber.Shah i~ Date: 1 £, ) n J Iv

R (,~"ts Cherkec' By ' Julia Mar inie"o :-?,~'t ._.~ Date: W/" /1 0 I' U S ~ c: A t. 1 A ·\ N l) e L L ,:" R SC I ENe E ! .. 1\1 [) TE (. II NO LO r: Y I) R ef... i\j I SAT: 0 N

Now 1 1!~''V[lr ra :.oa (;. I uras Heigh ; (L ucked r;i' ~ 2001, Kirro ve e DC NSW 223?) T + ~ 1 2 9i~ 7 311 1 f +G l 29541 J097 www.an. · . go \,.ou

)

1

1

)

J

I

1

1



Qnsto Nuclear-based science benefiring all Australians


Ph: (02) 9717 3419 Fax: (02) 9717 3212




Sample Identification: 88-1




Radionuclide Activity (8q.kg'l) % Uncertainty (10')

234Th 590 10 234mpa < 31 0 2~h 1700 10 214Pb 2100 10 2148i 2100 10 210Pb 1700 10

228Ac 67 10 228Th < 520 224Ra < 83 212Pb 65 10 2128i < 34 2°BrI 21 10

235U < 22 227Th 140 10 4°K 120 17


Results Calculated By : ~

Lida MOkhber.Sh ah in.~ Date: 18/1 )/1 0 /

l~ e SIJ ts Chec: t'd fly: ' i lia Mart 'niel! o ._ :·:;:~C . . ,/<~ [late: If I I/ ;' Q

6, l' S 1 " 1'. L I A I\J I\J lJ c: L E \ R S CI E :\.) C [ A ;· : :) T ee i I~ 0 L. 0 ; Y 0 R C; 1\ I,'! ~~ A T '.' I~

~/ '.'V\/ ansI J, ( \'.211

1

. 1





Ph: (02) 9717 3419 Fax: (02) 9717 3212


Client:

Company J Organisation:


Analysis required:

Analyst:

Robert Blackley

ANSTO-Safely for commercial

F1-1



Uda Mokhber-Shahin

22/10/2010 11:33am

Radionuclide

234Th 234mpa

230Th 214Pb

214Bi

210Pb

2211Ac

228Th 224Ra 212Pb

21 2Bi

2°STI

Activity (Bq . k~fl)

3000 2900

6200

5700 5600

5600

150 <830 270 150 < 35

48

180

540 220

% Uncertainty (1 cr)

10

10

10

10

10 10

10

16 10

10

11

10 11


//

Results Calculated By: Lido Mokhber-Shohin ~ - Date, 16//1 //0

R.:s Jlts ('necked '3y : ,luli? Martinial !) i)ate: 24 / ' 1 / ( '::?

p, 'J ) T R A L ! ;', r ~ N \.) C LEA R ~'~ I .: N C F. /", N D 1 r :: .., N L' lOG Y ( h G A N I S ,"'-. T ION

WV:· J. ililS! Q. gO·:.G"



Nuclear·based science benefiting all Australians


Ph: (02) 97173419 Fax: (02) 9717 3212


Client:



Analysis required:

Analyst:


Radionuclide

234Th 234mpa

230rh 214Pb

214Bi 210Pb

22aAc 228Th 224Ra 212Pb

212Bi

208T1

Robert Blackley

ANSTO"Safety for commercial

( F1 ~2-;,,-( . -.----~ ........


Lida Mokhber-Shahin

25/10/2010' 11 :49am

Activity (Bq.kg,1) % Uncertainty (10')

12500 10

11500 10

26700 10

33100 10

33700 10

28400 10

270 10

< 1200

1100 10

460 10

540 10

150 10

710 10

2400 10

< 80


-?

Results Calculated By: L ida MOkhber-Shah;~ Date: 16/ ( 1//-0

F'esul ts Cj , ~cked Bv '

A I I S T n fl., L I ; 1 ~ N U c. : EAR S ',' l EN C E f~ hJ D T' C H i'~ 0 ~ G G YU h G A N I S' 1 leN

,'\lw ' :lI nw<i ora R0 j, ~u r ~ s fi e JlllS ".ocke , Poor' 7101. I(irrawce DC : SW "232) T +61 0 9717 ~ ll1 F +61 L :;543 5n97 .'WW.rlO rto .g.Jv.au

}

)

1

I

Australian Government Nuclear·based science benefiting all Australians


Ph: (02) 9717 3419 Fax: (02) 9717 3212





Sample Identification: c:E4I:-3,~




Radionuclide Activity (Bq.kg-1) % Uncertainty (1 cr)

234Th 9600 10 n~mPa 9500 10 230Th 22700 10 214Pb 21900 10 2148i 22100 10 210Pb 18900 10

228Ac 330 10 228Th < 1200 224Ra 490 15 212Pb 340 10 212Bi 390 10 208TI 110 10

235U 520 10 227Th 1800 10 4°K 180 18

Note: The reported activities are in the dried sample. The sample moisture content is 14.6 % .

Resu lts Calculated By'

Re- ·, ;ts Che" kec 3y .

.-A/

~~--

yr~ Lida Mok!lber-Shahin __ .' ~

...'lj f i~ M :i in iel lo _~::: - ~~-? ,!/ -- .... . -'

WW'N an~ ·~ .g o . ~ lJ

Date: It/ II/lo

Oat : :


Certificate Number: 10MROO62#35 201010239-35

Nuclear-based science beriefiting all Australians


Ph: (02) 9717 3419 Fax: (02) 9717 3212


Client:



Analysis required:

Analyst:

Robert Blackley


G1-1



Lida Mokhber-Shahin

2/11/2010 14:43pm

Radionuclide

234Th 234mpa

23'Th

214Pb

214Si

210Pb

228Ac 228Th

224Ra

21 2Pb

212Si

208TI

Activity (Bq.kg-1)

28 < 97

< 66

27 29

48

41

< 160 35

34

43

11

< 7. 3

< 4. 5

170

% Uncertainty (1cr)

14

10 10 10

10

14

10 15

10

10


Results Calculated By: Lido Mokhber-Shahin ~ 4'?

Date: )<6 )11 /10

r,,' '+ / 1/ / I e'

AL3'T Ri' IA : ' N l ',-- '-:': A r, S C:EN C[ ,'< N [ , T E r HN~ :" C G\ · ; R C,AN,":.,3, ·: IO : --- ------------- - - - -- --- - ------ - - - ---- - -----

r,~ \·: III ' Nar'ooJo a d LlIc<.oH ei; 'ts(Lt' ke dB ag2(,OI 1; lf:W8r ' JCNSW22:LI T 612'" 731 : 1 F "[ :25. 3 5Gu V.,fV ·..,.3n \ to.gO l ~ u



Nuclear-based science benefiting al/ Australians

Institllte/or Environmental Research

Ph: (02) 9717 3419 Fax: (02) 9717 3212


Client:



Analysis required:

Analyst:


Radionuclide

234Th 234mpa

230Th

214Pb

214Bi 210Pb

228Ac 228Th 224Ra 212Pb

212Bi 208TI

Robert Blackley


G2-1


Lida Mokhber-Shahin

2/11/2010 15:21 pm


15400 10

12800 10

23200 10

20600 10 20000 10 17100 10

400 10

< 1300 780 10

400 10

450 10 130 10

750 10 1800 10 < 88



£ Lida Mokhber-Shahin ~ Date ' 18/11110

Ref l lts -:;h ('(, ke d :1y : 'Z '+ I ( 11 0

~! ,' \II' iii 'wa rr? ~, :ad, luca s ' 1I"'J" ,.; {Lo ~k9 d Bag ZOO:. Kirr ewee ,,( NSW 27' ': -;- " 1 2 971', 311 ' F +~ 2 9~t. v 5091 wv·; -.r I. n c;. ~ .:'. go v. "





Ph: (02) 9717 3419 Fax: (02) 9717 3212


Client:



Analysis required:

Analyst:


Radionuclide

2~h 2341TlPa 23<Th

214Pb

214Si 210Pb

228Ac 228Th 224Ra 212Pb

212Bi 208TI

Robert Blackley


G2-2


Lida Mokhber-Shahin

3/11/2010 16:23pm

Activity (Bq.kg-1) % Uncertainty (10)

2600 10

2500 10

4600 10

4200 10

4100 10

4300 10

100 10

< 560

180 21

110 10

100 13

36 10

120 12

31J 10

24 0 12

Note: The reported activities are in the dried sample. The sample moisture content is 17%.

Results Ca '::: u la ~ed By:

1/

~-~?/

Lida Mokhber-Shah in " -, ,8 / 11 /1-0

Date:

l~bS ,; i ~s c r- ..; ked 8 y .

r, U"'JR / . L IA:v N U C EA'-i Sl, l:f" C E 'r~n TE-r: I~ OL .} G Y OR ' -.':"I~ I S .! IO N

, . ·NW.h ' ,D.ge '. 3U



" sto Nuclear·basedscience benefiting all Australians


Ph: (02) 9717 3419 Fax: (02) 9717 3212


Client:



Analysis required:

Analyst:


Radionuclide

234Th 234mpa 230Th 214Pb

214Bi 21Dpb

228Ac 228Th 224Ra 212Pb

212Bi 2D8TI

Robert Blackley


G3-1


Lida Mokhber-Shahin

2/11/2010 15:44pm


5900 10

6300 10

7700 10

3700 10

3500 10

3000 10

170 10 < 540 220 13 160 10 150 10 52 10

300 10 630 10 130 17


,,<J

Results Calc ul ated By: ~/

U da MOkhber-S h ahi n~/ Date: 19/11/( (}

A U .' -;- R ;, L I .L. . J N LJ C , :: A R SCI [ ~i C E ,'\ Ne T E L r' :~ 0 L r : G y (I R ' />. r'~ I S / . ' 'ON - - - - - - -- - - - --- - - --- - - ------ - - - --- --- -- - -

J ew ·.: iwar r ~ R oa \ LI" ' s H ei fd " s (L. c k e~: a ~ "JOl, Ki ' "wee DC I'\ <: W 121 ,6 1 2 97 1 7 :~" 1 f 51 2 .'8' 350'1 7 v, .'W.ar' ·O.gD·:.8U

I

II I j I ( I •

I I J

I I I





Ph: (02) 97173419 Fax: (02) 9717 3212




Sample Identification: G3-2




Radionuclide Activity (Bq.kg"1) % Uncertainty (10)

2~4Th 8000 10 234mpa 7600 10 23DTh 11300 10 214Pb 8200 10 214Si 8100 10 21Dpb 6800 10

228Ac 230 10 228Th < 820 2;'4Ra 460 10 21?o b 220 10 212Si 270 11 208TI 71 10

23~U 390 10 L~ Th iDOO 10

40K 110 14


~

Reft' ts Calcu lated By: Lida MOk" ber-Shah~ Date: 11 /11/10

- ,--~,t~

,)at.- '2 ' ;- / I ' / I CJ

f\ l) S T 11 " l I A ~ . N IJ ,= :.. E ; , 1\ S C I [ :'J c: E A I J ,) -:- E e l f\j C L U C \ ~. R ( NIS/" T ICN

MJl'l. a nst() v.~ u

) r

/

I

I

I I


Certificate Number: 10MR0062#40 201 010239-40

Nuclear·based sciencebenef1tingall Australians

Instill/tefor Environmental Research

Ph: (02) 97173419 Fax: (02) 9717 3212



Company I Organi~ation: ANSTO-Safety for commercial

Sample Identification: H1 -1




Rad ionuclide Activity (Bq.kg"l) % Uncertainty (1a)

234Th 280 10 234mpa < 370 230Th 990 16 214Pb 5300 10 214Bi 5400 10 210Pb 4000 10

228Ac 45 14 228Th < 620 224Ra < 130 212Pb 48 10 21 2Bi 91 22 20sTI 14 10

<35U < 36 2?7Th 32 10

4°K 230 10


Re~ults Calcu latei By: I)ate: \b / II / 1o

~ eSJ l1s t:f;' vke r' "y; Ju .;" fv'lf.-t ii"d?l!:> & '-,' -,~ - 'late : '{LJ. / 1' /, .",-(/ // - ..... z'-J~ -

(l U S i RA I AN (\1 U ; ~ F. A f 5 C ; t: N C ~ ;' 1\1 [J 1 ;: C H N ( . LlJ G Y (; R G A. I\) I :.: ~ 1 i 0 :





Ph: (02) 97173419 Fax: (02) 9717 3212


Client:



Analysis required :

Analyst:


Radionuclide

234Th

234mpa

23D-rh 214Pb

214Si

210Pb

228Ac 228Th

224Ra

212Pb

21 2Si

l 08TI

Robert Blackley


ANS-DUP-004


Lida Mokhber-Shahin

4/11/2010 16:42pm

Activity (Bq.kg-1)

300

< 42

1100

4700

4800

3600

54

< 640

180

51

< 42

16

< 29

31

230

% Uncertainty (1 a)

10

17

10 10 10

13

21

10

10

1"1

12

Note: The reported activities are in the dried sample. The sample moisture content is 9%.

F~ es li its Calculated By :

~~

~'~

~?-: Lida Mokhber-Shahin ~ ~

'/' f1a te :

~'e :::l its Checked S; : D<" te :

hi : ,~ ~ ~ A L \ N N lJ ( . E ,A R ::: ! E 1-.: C L ;, ~ , [) I r C H N ch t \ G '( l" G f N i S i\ :- I () N .. - --- ----

N6'" :" av ';> r ra . I "d, Ll cas " ' I ~~" ! LOC I ' r Ba 9 200 ~ . '<i i, ? " " e 0 ' JSW 223: , t r ' 2 97!; ; 11 1 ,; +61 0 J' 4J ~ 197





Ph: (02) 97173419 Fax: (02) 9717 3212


Client:



Analysis required:

Analyst:

Sample measurement started at :

Radionuclide

234Th 234mpa

230Th

214Pb

214Bi

210Pb

228Ac 228Th 224Ra 21 2P b

21 28 ;

208TI

Robert Blackley


H2-1


Lida Mokhber-Shahin

3/11/2010 15:59pm

Activity (Bq.kg-1)

27

< 130

< 76

20

20

25

23 < 140

25 22

< 13 7.4

< 3.6

< 4.3

170

% Uncertainty (10')

14

10

10

12

10

19

10

10

10

Note: The reported activities are in the dried sample. Tne sample moisture content is 9.7%.

""/

Results Ca l('u lc:ted By: ~

Li cl a M okhber-Shah i i'~~ 6//

Date: l1/" // /0

A U ' ~ R f\ L i A 1\1 N l) C - --- - - - - -- - - - - - - - -. - - -- - - - - - --- - -- - - - - --- -

v' t/'lW.tJn .J .J.g 'l v.au



Qn to Nuclear-based science benefiting all Australians


Ph: (02) 9717 3419 Fax: (02) 9717 3212


Client:



Analysis required:

Analyst:


Radionuclide

234Th 234mpa

23'Th 214Pb

214Si

210Pb

228Ac 228Th 224Ra 212Pb

212Bi

208TI

Robert Blackley


H3-1


Lida Mokhber-Shahin

4/11/2010 16:00pm

Activity (Bq.kg-1)

1600

1600

2400 3900 3900 2700

82 < 430

< 110

76 99 25

88 100

200

% Uncertainty (10')

10

10 10

10 10

10

10

10

14

10

17 ~o

10


/ , /

Results Calculated By : Lida Mokhber-Shal i~~ ;:"/

Date: 16//1/ / 0

!\,~j S -;-I,,\L;A,\! [\l'e Lf , R :..r:El\;l' [ /J ,LJ -:-E,~ I " , CL O .JY GF1GJ ~IIS A T ,r N ---- - -- - - --- -- --- -- - .. - - -----

1,1', 1 111 2' ,~ra:'ooci ,1 ,vc c "'tl igl.:,(Locked8a , /III' , Kirr~.,oeO('NSv'/ ,:,~\ TLI29717311 , Cie , 95, ' )097 W'-" ,on" nO V.all

j j

Australian Government Nuclear·based science benefiting all Australians


Ph: (02) 97173419 Fax: (02) 9717 3212

Certificate Number: 10MRQ062#43 201010239-43

Client:



Analysis required:

Analyst:


Robert Blackley


H4-1



Lida Mokhber-Shahin

4/11/2010 16:22pm

Radionuclide

234Th 234"Pa

230Th

21 4Pb

214Si

210Pb

228Ac 228Th 224 Ra 212P b

212S i

208TI

Activity (Bq.kg·1)

1100 11 00 1400 1900 1900 1400

61 < 480 < 76

52 35

17

47

78 210

% Uncertainty (10')

10 10

10 10

10 10

10

10 2'1

10

16 10 10

Note: The reported activities me in the dried sample. The sample moisture content is 18.6%.

Res LJ l t~ C2lcul :tted By:

,0 ,

Lida Mokhber· ';hahin ~" 4~

Date:

[ .es l'; _ Cl t'cl,~r:! lj : JI ·lia ~ a r -;';ell , ;'?~- ' k O::te' L l; /:1/ G / /. /' ~ ~",'~,

I IUS'fP" IA N ;; ',IC LEt ~ S': l f .: ~!= /-\i"~) ; c C Ii ,O,-OG" 'J r\ G /·; ;IS ~T IC .

'l/\'o,/\V 'l O.:tO. (·L.· 2"

I

I

I

I )

j Australian Government


Nuclear:based scien~e be~efiting all Australians


Ph: (02) 9717 3419 Fax: (02) 9717 3212


Client: Roqert Blackley


Sample Identification: 11-1




Radionuclide A\;tivity (Bq.kg"1) % Uncertainty (1a)

234Th 990 10 234mpa < 330 230Th 1200 111 214Pb 2800 10 21 48i 2900 10 210Pb 2100 10

228Ac 70 10 228Th < 390 224Ra < 110 212Pb 63 10 21 2Bi 94 16 206TI 18 10

235 LJ 53 11 22!Th 57 10

4UK 200 13

Note: The reported activities are in the dried sample. The sample moisture content is 15.7% .

.. '

~<iSl! ' ts Ca lcu!atec! By : ~~

Lida ,lJiokhber-Shahin /,..~ .- Date: 16/ /1/ 10

~,U C, i I{ 1\ L , A '\j r):J r I, ~ 1\ R (':: I ~ '" ': E "I\J f) " .-:, ~ i f\: () L r. G'r C) :' J.f.., i'! IS ' , ' I U N



Qn Nuclear-based scienc~ benefiting all 'Australians


Ph: (02) 9717 3419 Fax: (02) 9717 3212


Client:



Analysis required:

Analyst:


Radionuclide

234Th 234mp a

230Th

214Pb

214B i

210Pb

228Ac 228Th 224Ra 21 2Pb

212Bi 208T1

235U

2271 h

40"

Robert Blackley


ANS-DUP-007


Lida Mokhber-Shahin

24/11/2010 15:10pm

Activity (Bq.kg-1) % Uncertainty (1 a)

1000 10

1400 1:'1

1500 12

3900 10

4100 10

2900 10

60 10 < 530

180 19

60 10 95 18

19 10

59 23 60 1(j

200 12

Note: rhe reported activi ties are in the dried sample. The sample moisture cor.tent is 16%.

Pesul·s Calculated By:

:fJ/ :b::

Lida MCkh l"er-Shahi~~ Date: 2 (j il/I-o

J

J

, J



Nuclear -based sciencll benefiting all Australians


Ph: (02) 97173419 Fax: (02) 9717 3212


Client:


Sample Identification :

Analysis required:

Analyst:


Radionuclide

234Th 234mpa

230Th

214Pb

214Si

210Pb

228Ac 228Th 224Ra 212Pb

212B i

208TI

Robert BI~ckley

ANSTO-Safely for commercial

12-1


Lida Mokhber-Shahin

8/11/2010 12:1 7pm

Activity (Sq.kg-1)

220 < 230

< 190

310 310

270

91

< 380

77

86

89 30

< 19

<8

160

% Uncertainty (10)

10

10

10

10

10

18

10

10

10

10


.J

ReE ults Ca lcd?t<;ci Bv: Lida Mokhbor-Sh, hin ~ Dflte: 2 6/11/ 10

I :J S R CI. L it ~ I, 1 c: L ,~R SCI ~ .,j l' E . , ! Cl - Ee L ,'~ () L C ') v Q k ( .,~; 1 .~ AI' ,: j'd

j j I I i !





Ph : (02) 9717 3419 Fax: (02) 9717 3212


Client:



Analysis required:

Analyst:


Radionuclide

2:'4Th 234mpa

230Th 214Pb

214Bi

21°Pb

228Ac 228Th 224Ra

212Pb

212Bi

208TI

Robert Blackley


13-1


Lida Mokhber-Shahin

8/11/2010 13:31pm

Activi ty (Bq.kg·1)

30

<150

< 110

71

80 61

30

< 100

32 40

< 25

16

< 14

<6.5

110

% Uncertainty (10)

11

10

10

10

11

25

10

10

16

Note: The reported activities are in the dried sample. The sample moisture CC'ltent is 25. 8%.

r<esults Ca lcul?te(: By : Date : 2.6/! (If \,

I 1(.., I -" j '-- ,' '--

! l, ,31 ' /1, 1 :/\1" I : '. CLE, ' . ?CIF;"'-c A; ,I,' T~C H ".' LOC " or:G/~:·. , ~,:· T i ".J - -- - --- - -- - - - - -- - - - - -- - - - - - --- - -~- ---

"", 'V': ,.ds t 1Jv.al'

j

j

I



Nuclear-based science bene,fiting all Australians


Ph: (02) 97173419 Fax: (02) 97173212


Client:



Analysis required:

Analyst:


Radionuclide

2341 h

2>4rr'?a

230rh

21 4Pb

214B '

210P b

228Ac 228Th 224Rc' 212p Q

/ 1231 ?08 r:

235U 72 7., h

40K

Robert Blackley


14-1


Lida Mokhber-Shahin

8/11/2010 14:00pm

Activity (8q,kg-1)

190

< 260

< 140

230

240

170

40

< 320

< 34

41

49 13

< ~4

<7. 5

~ 30

% Uncertair ty (1a)

10

10

10

10

10

10

25 10

13

Note: The reported activi ties are in the dried sample. The sample moisture content is 17.3%.

Results Calcu l<.ted By: Date: 26/ II/Iv

1, ~: ::; T f-~ ~ I I i. i-J 'U C L ~ b.. ;., '::: C 1 E : ' ,- E : . I\' r , t. ''": 1-, () i (1:::; 'r ' ,G A , I S ,A, ~ ! 0 ",





Ph: (02) 9717 3419 Fax: (02) 9717 3212


Client:



Analysis required:

Analyst:


Radionuclide

234Th 234n' P a

230Th 214 P b

214Bi

210Pb

228Ac 228Th 224 Ra 212P b

21 Bi 2l 8TI

Robert Blackley


15-1


Lida Mokhber-Shahin

9/11/2010 15:08pm

Activity (Bq.kg·l)

11 0

< 190

<120

120

120

92

34 <220

<26

28

54 7.7

<11

<G.G

1A()

% Uncertainty (1 0')

10

10

10

10

10

10

21

10

11

Note: The reported activities are in the dried sampl,::. The sample moisture content is 16.5%.

Resu lts r. al:;:ufated By: ~

Lida MOkhber-Sh <) hin~'::::? Date: 2 t/ 11/ J~

; / I ?_ ! , ( ;

, L' <;1 R ,r", ~ I '\ r· N . (: ~ [~\ n :> " , : E N ' t £..;...; [) : ~ ( rl N : I CJ·':; ~· L r (' I'", N IS ', T . (l N


Certificate Number: 2011/0067-1

Client:



Analysis required :

Analyst:

Sample measurement started at :

Radionuclide

---- ----Nuclear·based science benefiting all Ali stralia~:~

Institute for environmental Research

Ph: (02) 9717 3419


Robert Blackley


K113 Fore


Lida Mokhber-Shahin

27/4 /11 13:41

Fax: (02) 9717 3212

Activity (Bq.kg-1) % Uncertainty (1CJ) - - ------ ---- - - - - --- --- - -

23/Th

23401Pa

23wTh

214Pb

21 48i

2H!Pb

228Ac 228Th 224Ra 212P b

21281

2°~TI

250 C!

280li 8300

23000 23000 20000

190

< 1500

600 180

21 0 53

< 80

590

290

', 0

16

10 10

10

is

1J

H: 1<;

<'0

14

Note: The reporteri activities are in the dried sample. The sample moisture content is 16.7%.

~ ~

.~eE . !Its C2!cu la t~(.i By:

/~ . , / ,

Lido ~.1o l .1bcr -S hehin..-~:.:-

J H (~ A :" , .:; . 'I 0 '

'oW I .. ",ar ro Ruc 'J ~ Ul , 11e, l:.- wr "0 1, I. Jr, , NS\II' _ 3~i 1 .G, 2 ;; , 3:1, • ;5i 2 r ,4.' '.c'!' ww . ..... a:1s; l).gr· .. ( ~ I



Client:



Analysis required:

Analyst:


Radionuclide

Qn to Nuclear-based science benefitJng all Australians

Institute for environmental Research

Ph: (02) 9717 3419


Robert Blackley


K2 13 Fore


Lica Mokhber-Shahin

27/4/11 15:42

Fax: (02) 9717 3212

Activity (Bq_kg-1) % Uncertainty (10")

-------------------------------------------234T:

1

234mOa

23~h

214Pb

214Bi 210Pb

228Ac 228Th 224Ra 212Pb

212S i 208TI

2~SlJ

227Th

401<.

1200 1100

1900 1300 1200

1100

81

< 570

< 71

80 81

23

78

150 230

10

10

10 10

10

10

17

10

12


~cs u!ts Calcula ted By: , -) / / ( (

Date: 2- 0 '-t./



Client:



Analysis required:

Analyst:


Radionuclide

23~h

234m r a

2301-h

214 Pb

214Bi 210Pb

228Ac 228Th 224Ra 21<Pb

2126 i

208 T j

23511 221;'h

4°K

Qnsto Institute fOf fnvifonmental Research

Ph: (02) 9717 3419


Robert Blackley


K3 13 Fore


Lida Mokhber-Shahin

27/4/11 15: 54

Fax: (02) 9717 3212

Activity (Bq.kg-1) % Uncertainty (10") -.--

8600 10

[j600 10 .OOO C' 10 3600 10 5400 10 .1000 10

210 10 < 990

:140 13

210 10 200 12 G8 10

·130 10

, 10 10

.8e 19

Note: Th9 ,eported activi ties ar~ .in the dried sample. The sample moisture conten t is 62%.

Results ,'il ln"ated Bv: Date: 2. ,x ) it / J/

;~rp t ' ;c, "ng

f\'e,.'v h C)V, Q, r'! P )8 ', !t.JS ·,C!jg~ .l ~ \[',v' F 1, . ~ da; ~~0\1\ 1 '.i~~.1~ 1 i 6i '7 17 ,,1 11 ww an sto go .... <, ..

Certificate Number: 09MR0002#5

Client:

Company J Organisation:


Analysis required:

Analyst:


Radionuclide

234Th

234mpa

230Th

214Pb

214Si

210Pb

228Ac

228Th

224Ra

212Pb

212Si

208TI


Results Checked By:

· ,} i !'

Institllte/or Environmental Research

Ph : (02) 9717 3419 Fax: (02) 9717 321 2

CERTIFICATE. OF ANALYSIS

Karl Mayman

ANSTO-S&RS

8G-6 (2009/0007-5)


Uda Mokhber-Shahin

12/2/09 16:00

Activity (8q/g) % Uncertainty (10)

0.03 10 < 0.07 < 0.07 0.02 10 0.02 10 0.02 10

0.04 10 < 0.1 0.03 10 0.04 10 0.03 10 0.01 10

< 0.01 < 0.003

0.2 10

Date:

Date:

/, ,,: S I !i .~i L 1 t\ f\J i\j U c: L L f\ f, SCI L N C LAN D I [" C ! 1 ~J 0 LO G Y () f{ G II fo,J 1 S ". 1 1 n I ·)

N!)w IIlmN~rr" Road. Lucu s Heights lPMB 1, Manni NSW 22341 T .61297173111 F +612 95'135097 www.anSlo.gov.au

Allstralian GO\'Cl'Illllcnt

Certificate Number: 09iV1R0002#4

Client:



Analysis required:

Analyst:


Radionuclide

Institute for Environmental ReSe(lfc/t

Ph: (02) 9717 3419


Karl Mayman

ANSTO-S&RS

8G-5 (2009f0007-4)


Uda Mokhber-Shahin

12f2/09 16:00

Fax: (02} 97173212

Activity (8q/g) % Uncertainty (1cr) ------------ ------ - ----- -- - -- -------------- - ---- --- ------ --------------- ---. - ----

234Th

234mpa

230Th

214Pb

214Si

210Pb

228Ac

228Th

224Ra

212Pb

212Si

208TI

235U

227Th

40K

Results Ca!culated By:

Results Checked By:

< 0.01 < 0.10 < 0.09 0.01 0.01 0.05

0.03 < 0.3 0.03 0.02 0.03 0.01

< 0.01 < 0.01

0.05

10 11 10

12

23 10 19 10

14

Date:

Date:

it-Ii / c: 'i

I q /-2-/01

,\ U S r " ~ L I A i'J t'-J U C LEA H S C ! L Nee i\ r'i D r L C II i~ 0 LOG Y ()" G /\ r'j I S !\ Ti C) [',j

Nuw III~warru Road. Lucas Heights (PMB 1. Men[1i NSVV 223·1) T 161 297173111 F ,61295435097 www.~nsto.gov. all


Ph: (02) 971 7 3419 Fax: (02) 9717 321 2



Client:



Analysis required:

Analyst:


Karl Mayman

ANSTO-S&RS

BG-4 (2009/0007-3)


Uda Mokhber-Shahin

11/2/09 16:28

Radionuclide Activity (Bq/g) % Uncertainty (1 a)

234Th

234mpa

230Th

214Pb

214Si

210Pb

228Ac

228Th

224Ra

212Pb

2128i

208TI

235U

227Th

4°K

...... .;:;~

/~::;i&:. -Results Calculated By: / .::\;;,,:::.::._~. -/'

Results Checked By: ~~.

0.03 < 0.1 < 0.1 0.01 0,01 0.04

0.03 < 0.2

< 0.02 0.03

< 0.02 0.01

< 0.01 < 0.01

0.2

21

10 12 11

12

10

10

10

Date: /6/ L/ (} "'(

Date: (q /2./09.

.1'1 U Sf j1~ l I .>4 I'd N U C L [ .1-\ P, SC: I l 1'-.1 C l AND r [: C I I [\) 0 L. 0 (i Y 0 H (i J\ N .! S "'\ i l () )-"1

New ·llIawurrCl Road. lu cilS Hei()hts lPMfl 1. Menal NSW 2234) T ·;1)1 2 97n 311 I F ~6 1 295435097 w,,,'w.a II stO. gov.ml


Ph: (02) 9717 3419 Fax: (02) 9717 3212



Client:



Analysis required:

Analyst:


Karl Mayman

ANSTO-S&RS

BG-3 (2009/0007 -2)


Lida Mokhber-Shahin

10/2/0916:13

Radionuclide Activity (8q/g) % Uncertainty (1(J)

234Th

234mpa

230Th

214Pb

214Bi

210Pb

228Ac

228Th

224Ra

212Pb

212Bi

208TI

235U

227Th

40K

L .7', ,1

/~> Results Calculated BE.-· - ,.:;'c.::::-y .. - . ..,..... ,

Results Checked By : ~~

< 0.02 < 0.2 <0.2 0.02 0.02 0.04

0.03 < 0.3

< 0.03 0.02

< 0.02 0.01

< 0.02 < 0.01

0.1

12 10 11

15

10

12

12

Date:

Date:

/tILlc)!

fqj2-lo~

i\ U S T ! i . .:\ L i AN i\j U eLL A H SCI [ NeE A N DI Lei if·1 () L. 0 (, y 0 I~ G !If\j ! S /\ : I C ~J

New Illawarra Road, Lucas Heights (PMB 1. Menai NSW 2234) T ;·61297173111 F +61295435097 www.ansto.gov.ou

)

}


Im;titlite/iJI' Environmental Research

Ph: (02) 9717 3419 Fax: (02) 9717 3212

Certificate Number: 09MR0002#1 .


Client:



Analysis required :

Analyst:


Karl Mayman

ANSTO-S&RS

8G-2 (2009/0007-1 )


Lida Mokhber-Shahin

9/2/09 15:41

Radionuclide Activity (Bq/g) % Uncertainty (1cr)

234Th

234mpa

230Th

214Pb

214Si

210Pb

228Ac

228Th

224Ra

212Pb .

212Si

208T.1

235U

227Th

40K

0.03 < 0.1 < 0.1 0.02 0.02 0.05

0.04 < 0.3 0.03 0.03 0.03 0.01

< 0.01 < 0.01

0.1

22

10 10 10

10

24 10 22 10

11

Date: i 6 / 1. I {' 1 Date: 1'1/2/09.

i\ U ::;: i L\ L 1 /\ f-J J\j U eLL A H S C ; L r\1 C l. A I'j D TEe I ! N 0 L. 0 (J y 0 H G f.\ I·) i S !\ T l Ot·] . -. . -. -... - _ . .•.. _._----_ ... .. . -... _.. ' " . ... .

Nc:w IIlawum Roa d, Luca s Heights (PMB 1. Menni NSW 2234) T ,6) 297) 731)) F +61295435097 www.al1slo.gov.au

Page

Work Order

Client

Project

: 2 efg ES1016932

: CH2M HILL PTY LTD

: 406484 ANSTO HUNTERS HILL

Analysis Holding Time Compliance The following report summarises extraction / preparation and analysis times and compares with recommended hold ing times. Dates reported represent first date of extraction or analysis and precludes subsequent dilutions and reruns. Information is also provided re the sample container (preservative) from which the analysis aliquot was taken. Elapsed period to analysis represents number of days from sampling where no extraction / digestion is involved or period from extraction / digestion where this is present. For composite samples, sampling date is assumed to be that of the oldest sample contributing to the composite. Sample date for laboratory produced leachates is assumed as the completion date of the leaching process. Outliers for holding time are based on USEPA SW 846, APHA, AS and NEPM (1999). A listing of breaches is provided in the Summary of Outliers.

Holding times for leachate methods (excluding elutriates) vary according to the analytes being determined on the resulting solution. For non -volatile analytes, the holding time compliance assessment compares the leach date with the shortest analyte holding time for the equivalent soil method. These soil holding times are: Organics (14 days) ; Mercury (28 days) & other metals (180 days). A recorded breach therefore does not guarantee a breach for all non-volatile parameters.

Matrix: SOIL

Soil Glass Jar - Unpreserved I ALS-DUP-003,

C10-1, C1-3, C3-1, C4-1, C6-1, C8-1,

Soil Glass Jar - Unpreserved ALS-DUP-003, C10-1, C1-3, C3-1, C4-1, C6-1, C8-1,

Soil GlasJ; Jar - Unpreserved ALS-DUP-003, C10-1, C1-3, C3-1, C4-1, C6-1, C8-1,

B2-1, C1-1, C2-1, C3-3, C5-1 , C7-1, C9-1

23-AUG-2010 26-AUG-2010

23-AUG-2010 I 26-AUG-2010

19-FEB-2011

20-SEP-2010

Evaluation: " = Holding time breach ; ./ = Within holding time.

- ---1

,/

,/

f \

24-AUG-2010

27 -AUG-201 0

27-AUG-2010

30-AUG-2010 ,/

- --of

19-FEB-2011 ,/

20-SEP-2010 ,/

A Campbell Brothers Limited Company

Page

Work Order

Client

Project

Matrix: SOIL

: 30f9 ES1016932

: CH2M HILL PTY LTD

. 406484 ANSTO HUNTERS HILL

Soil Glass Jar - Unpreserved ALS-DUP-003, C10-1, C1-3, C3-1 , C4-1 , C6-1, C8-1

Soil Glass Jar - Unpreserved ALS-DUP-003, C10-1, C1-3, C3-1, C4-1, C6-1, C8-1,

Soil Glass Jar - Unpreserved ALS-DUP-003, C10-1 , C1-3, C3-1, C4-1, C6-1, C8-1

Soil Glass Jar - Unpreserved ALS-DUP-003, C10-1, C1-3, C3-1, C4-1, C6-1,

B2-1, C1-1, C2-1, C3-3, C5-1 , C7-1,

C8-1, . ____ C9-1 Soil Glass Jar - Unpreserved ALS-DUP-003, C10-1, C1-3, C3-1, C4-1, C6-1,

_ C8-1, .

B2-1, C1-1, C2-1, C3-3, C5-1, C7-1 , C9-1

Sample Date Extraction / Preparation

23-AUG-2010 24-AUG-2010 06-SEP-2010

--- -

23-AUG-2010 24-AUG-2010 06-SEP-2010

T~

I 23-AUG-2010 I 25-AUG-2010 I 06-SEP-20 1 0 I

T 24-AUG-2010 06-SEP-2010

23-AUG-2010 25-AUG-2010 06-SEP-2010 ,

.~

A Evaluation: x = Holding time breach; ,/ = With in holding time.

Analysis

analysed I Due for analysis Evaluation

./ 25-AUG-2010

___ .l

./ 25-AUG-2010

./ ! 26-AUG-2010 I

./ • 26-AUG-2010

./ I 26-AUG-2010

I

03-0CT-2010

03-0CT-2010

04-0CT-2010

06-SEP-2010

04-0CT-2010

./

./ i I

I I I

.1 ./

./

-' ./ I

_L ___ . _' -----1


Page

Work Order

Client

Project

Matrix: SOIL

: 4of9 : ES1016932

: CH2M HILL PTY LTD : 406484 ANSTO HUNTERS HILL

Soil Glass Jar· Unpreserved ALS·DUP·003, Cl0·l, Cl·3,

I C3. 1, C4·1 , C6·1, C8·1 , TB·230810, TSC

Amber VOC Vial· HCI RIN-230810

B2·1, C1·1, C2·1 , C3·3, C5·1, C7·1, C9·1 , TS·230810,

Evaluation:

23·AUG·2010 24·AUG·2010 06·SEP·2010 ~ 26·AUG·2010 06·SEp·2010 ~

19·FEB·2011

30·AUG·2010

25·AUG·2010 30·AUG·2010

23·AUG·2010 25·AUG·2010 30·AUG·2010

23·AUG·2010 25·AUG·2010 30-AUG-2010

I 23.AUG.2010 06-SEP-2010

---r-- - -- 1- --- ---- --23·AUG·2010 ________ ~ 06·SEP-2010 27·AUG·2010 ' 06-SEP-2010 ' ~ --------.J


Page

Work Order

Client

Project

50f9 ES1016932

CH2M HILL PTY LTD

406484 ANSTO HUNTERS HILL A Quality Control Parameter Frequency Compliance The following report summarises the frequency of laboratory QC samples analysed within the analyticallot(s) in which the submitted sample(s) was(where) processed. Actual rate should be greater than or equal to the expected rate. A listing of breaches is provided in the Summary of Outliers.

Matrix: SOIL

'=.A.!:!'!,h2:nols (SIM)

!,estici~s bL~~~ f>.ol¥chlorinated Bie~enyls _(PCB) Total Mercury by FIMS

']:otal Metals bylCP-AES

-r

2 2 2

38

14 i -.- ~20

~r 20

Evaluation: " = Quality Control frequency not within specification ; "' = Quality Control frequency within specification .

Rate (%J ; Quality Control Specification ~ ------

.. NE~M ~9~ Schedule B(~nd ALS QCS3 ~uirement

I NEPM 1999 Schedule B(3) and ALS QCS3 requirement /---------- - --- --- -I NEPM 1999 Schedule B(3) and ALS o..C~_ requiremen! __ _

NEPM 1999 Schedule B(3) and ALS QCS3 requirement

_ jEJEPM 1999 Schedule B(3) -and AL S QCS~reme;.it-~~uu~. " NEPM 1999 Schedule B(3) and ALS QCS3 requirement

EP071 ! 2 14 14.3 10.0 ./ I NEPM 1999 Schedule B(3) and ALS QC·S3-;:equ;re;.;;e;.;t

5.0

5.0

5.0 5.0 ·-T -

~ - ~

./ _./ -./ -L

QCS3

I NEPM 1999 Schedule B(3) and ALS QCS3 requiremen,-_ NEPM 1999 Schedule B(3) and ALS QCS3 requirement

- --1 . -- -- -----NEPM 1999 Schedule B(3) and ALS QCS3 requirement

( NEPM 1999 · Sche dule 8(3) andAI S QCS3 requir"e;i,-;;;:rt -

, NEPM 1999 Schedule B(3) and ALS QCS3 requirement NEPM 1 999 Schedule B(3)i md- ALS -QCS3 requirem~ -~ NEPM 1999SChedule B(3) and ALS- QCS3" ·;;;nllirF!mF!n'- -

PAH'.f'. heno~s (SIM) EP07~(Sn~~ I.. 14 _ .1__ 7.! _ _ 5.0 ~~ ~ ALS ~S3 requ.jrement 1 Pesticides by GCMS EP068 20 t 5.0 ' 5.0 . ./ ALS QCS3 requirement i ~<l!Ychlorinated~B i phe-,",~s (PCB) ____ ~ ___ E P066 - _ ~_ 20 -~ 5.0 :~ - S:O--I--7 ---+;t;:Lsocs3 requirement

ITotal Mercury by FIMS : EGD35T != 2 22 : 9.1 ! 5.0 I ./ ! ALS QCS3 requirement ,Total Metals by ICP-AES -- - ----- ·--1 ~ EG005T 2 30 I 6.7 ! 5.0 I ~ ALS QCS3 requiremeni

TPH - Semivolatile Fraction _______ . _ ~P07~ __ 2-._ 14 _I. ~ __ 2:.1~ __ 1. _ 5~ ..J _____ ._ L AL~ QCS3 requir: ment . TPH Volatiles/BTEX EP080 · 1 17 5.9 ! 5.0 ! ./ ~S QCS3 requirement

Matrix: WATER Evaluation: " = Quality Control frequency not within specification ; "' = Quality Control frequency within specifica tion.


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Evaluation: " = Quality Control frequency not within specification ; .' = Quality Control frequency with in specification_

Quality Control Specification

____ _ _ .:_~~~o ~ I LU o.u o.u ,/ I ~::~ ~::: ~cneaUie t:l\~} an~ ':~~ ~~~: reqUirement _,

____ . ____ ----, t:t"~~~ I lUU.U ~.U ", I ~~ ~J""~~ 1~~tI "cneaule 0t"'} ana f\L" ~\,...\:)." requirement

__ .___ ___ _ ::: _ ~:~ I L::...~~ ~~~~ __ m._ - , -, - ~ .• :-::: :::::::::

' !otill. Met~I~.!J.y. IC£ -MS - Suite A TPH Volatiles/BTEX


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Brief Method Summaries The analytical procedures used by the Environmental Division have been developed from established internationally recognized procedures such as those published by the US EPA, APHA, AS and NEPM. In house developed procedures are employed in the absence of documented standards or by client request. The following report provides brief descriptions of the ana lytical procedures employed for results reported in the Certificate of Analysis. Sources from which ALS methods have been developed are provided with in the Method Descriptions.

Total Metals by ICP-AES EG005T SOIL

Total Mercury by FIMS EG035T SOIL

, A gravimetric procedure based on weight loss over a 12 hour drying period at 103-105 degrees C. This method is compliant with NEPM (1999) Schedule B(3) (Method 102) (APHA 21st ed-::-3120; USEPA SW 846- 6010)(ICPAES)Metals are d~termined following an appropriate acid digestion of the soil. The ICPAES technique ionises samples in a plasma, emitting a characteristic spectrum based on metals present. Intensities at selected wavelengths are compared against those of matrix matched standards. This method is compliant with NEPM (1999) Schedule B(3)

. AS 3550: APHA 21 5t ed ., 3112 Hg - B (Flo;:Tnj;;cti;;;-(SnCI2) (COld Vapour generatlon)-AAS) FIM-AAS is an automated flameless atomic absorption technique. Mercury in solids are determined following an appropriate acid

: digestion. Ionic mercury is reduced online to atomic mercury vapour by SnCI2 which is then purged into a heated ~ quartz cell. Quantification is by comparing absorbance against a calibration curve. This method is compliant with : NEPM (1999) Schedule B(3)

! Polychlorinated Biphenyls (PCB) EP066 -; - SOIL'- ; (USEPA SW 846 - 8270B) Extracts are analysed by Capillary GC/MS and quantificationis by comparison against I i an established 5 point calibration curve. This method is compliant with NEPM (1999) Schedule B(3) (Method 504) L-- -

I Pesticides by GCMS ---~,---

EP068

! TPH - Semivolatile Fraction EP071

f-- -f PAH/Phenois (SIM) EP075(SIM)

i 1--' -TPH Volatiles/BTEX

i I _' - ---1-- EP080

I Total Metals by ICP-MS - Suite A EG020A-T

! I , I Total Mercury by FIMS

I

I SOIL I (USEPA SW 846 - 8270B) Extracts are analysed by Capillary GC/MS and quantification is by comparison against I an established 5 point calibration curve. This technique is compliant with NEPM (1999) Schedule B(3) (Method 1504,505)

SOIL

SOIL

SOIL

n USEPA'SW 846 - 8015A) Sample extracts are analysed by Capillary GC/FID and quantified against alkane standards over the range C1 0 - C36. This method is compliant with NEPM (1999) Schedule B(3) (Method 506.1)

, (USEPA SW 846 - 8270B) Extracts are analysed by Capillary GC/MS in Selective Ion Mode (SIM) and quantification is by comparison against an established 5 point calibration curve. This method is compliant with NEPM (1999) Schedule B(3) (Method 502 and 507)

A

-.~

---I

I

I I::P066 WATER ! USEPA-SW846~8276D Sample extracts are analysed by Capillary GC/MS and quantification is by- comparison -

~ against an established 5 point calibration curve. This method is compliant with NEPM (1999) Schedule B(3) I ! (Appdx. 2)

~--. -----I Polychlorinated Biphenyls (PCB)

I

'PestiCides by-GeMS t - EP068 T- WATER • USEPA SW-846 - 8270D SamPle extracts are analysed-by Capillary GC/MS and quantification isby-comparison : , against an established 5 point calibration curve. This method is compliant with NEPM (1999) Schedule B(3)

! 0pp.dx. ~~


our reference: units your reference ------- evl-dup …...client reference: pcbs in soil our...

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