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Significant Achievements egRoiw.kZ miyfC/;ka

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Page 1: egRoiw.kZ miyfC/;ka - National Physical Laboratory of IndiaCSIR-National Physical Laboratory Annual Report 2012-13 xxxvii New Standards Established Continued ... temperature time and

Significant Achievements

egRoiw.kZ miyfC/;ka

Page 2: egRoiw.kZ miyfC/;ka - National Physical Laboratory of IndiaCSIR-National Physical Laboratory Annual Report 2012-13 xxxvii New Standards Established Continued ... temperature time and

xxxvi okf"kZd izfrosnu 2012-13 lh,lvkbZvkj&jk"Vªh; HkkSfrd iz;ksx'kkyk

New Standards Established

Quantum Metrology & Measurements

dimension

Fluid Flow

High Precision Roundness Measuring Machine: nominal Range : 0-4000 mm Working Range : 0-3700 mm Resolution : 0.01 µm Maximum error : 1.5 µm Repeatability : 0.1 µm

Newly Developed DN 100 Flow System

Programmable josephson voltage standard

(operating at minus 269 degree Celsius)

New DN100 Rig along with DN50 and DN200 Weighing Tanks, Fishtail, Nozzle and Diverter (designed and developed in NPL)

Page 3: egRoiw.kZ miyfC/;ka - National Physical Laboratory of IndiaCSIR-National Physical Laboratory Annual Report 2012-13 xxxvii New Standards Established Continued ... temperature time and

xxxviiAnnual Report 2012-13CSIR-National Physical Laboratory

New Standards Established Continued ...

temperature

time and Frequency

establishment of High temperature Blackbody source

(for the calibration of infrared total radiation pyrometers in the range 600 to 3000ºC.)

1. Generation of a stable UTC time scale linked to BIPM with a jitter of 0.3ns. The variation in the time scale UTC (NPLI) is within 10 ns over the last one year. Its frequency is stable to better than 1 x 10-14.

2. A new Time Service has been started over the Internet using the NTP protocol. This would enable time synchronization of Personal Computers connected to the Internet. The domain name is : time.nplindia.org

Fixed point realization facility for the new Co-C and Fe-C metal carbon eutectics using three zone heating furnace have been developed.

schematic of time scale utC(nPlI)

Establishment of High Temperature Blackbody Source for the

Temperature

calibration of infrared total radiation pyrometers in the range from 600 ºC to 3000 ºC.

d l f d l f l f h d We are developing fixed point realization facility for the new Co-C and Fe-C metal carbon eutectics using three zone heating furnace.

Time and Frequency1. Generation of a stable UTC time scale linked to BIPM with a jitter of 0.3ns.

The variation in the time scale UTC (NPLI) is within 10 ns over the last one year.The variation in the time scale UTC (NPLI) is within 10 ns over the last one year.Its frequency is stable to better than 1 x 10-14.

2. We have started a new Time Service over the Internet using the NTP protocol . This would enable time synchronization of Personal Computers connected to the Internet. The domain name is :

time.nplindia.org

Micro Phase Stepper

5 MHz

1PPS

5 MHz

IN

out

5 M

Hz

out

FREQUENCY DOUBLER

5 MHz

1PPS

To fountain lab

5 MHz

Distribution

To Calibration lab

Hydrogen Hydrogen

Schematic of Time Scale UTC(NPLI)

---

Cs Clock 25071A-C001

Cs Clock 25071A-C001

Cs Clock 35071A-C001

Cs Clock 35071A-C001

Cs Clock 65071A-C001

Cs Clock 65071A-C001

resolution= 2 (2-32)rad.Freq. Resolution = 5E-19

Automatic Switching Unit

Time interval counter 1

(25psec resolution)

START

STOP

1

2

3

4

7

6

1 PPS

1PPS

1PPS

1PPS

1PPS

IN

ou t

10 M

Hz

1PPS

Amplifier-1

1PPS

outMaser - HM1

MHM2010

Maser - HM1MHM2010

1PPS

@

Cs Clock 75071A5071A--C001C001

Cs Clock 75071A5071A--C001C001

Cs Clock 85071A5071A--C001C001

Cs Clock 85071A5071A--C001C001

5

7

Controller Workstation To To Satellite link lab.

1PPS

1PPS

Page 4: egRoiw.kZ miyfC/;ka - National Physical Laboratory of IndiaCSIR-National Physical Laboratory Annual Report 2012-13 xxxvii New Standards Established Continued ... temperature time and

xxxviii okf"kZd izfrosnu 2012-13 lh,lvkbZvkj&jk"Vªh; HkkSfrd iz;ksx'kkyk

Materials & Products

Free standing carbon based anode -for li – ion battery

csir – new Millennium indian technology leadership initiative

InnOvatIve sOlutIOn FOR sOlaR eneRgy stORage

carbon nanotube based anode carbon Fiber based anode

for clean energy generation -To be used for mobile communication towers (Reliance Industries)

nPl cecri ncl

reliance industries (industrial partner)

CSIR – TAPSUN Project

nPl – CeCRI Partnership

Discharge Capacity– 206 mAh/gDischarge capacity- 196 mAh/g

High Performing carbon Materials

development of Fuel cell

cnt incorporated carbon foam

• Porous conducting carbon paper of much better than International quality Developed by NPL Scientists

• Carbon composite bipolar plate of superb quality developed by NPL Scientists

• Fuel Cell Assembled by CECRI

• DuPont USA Polymer applied by NCL

applications EMI SHIELDING

Material for Aerospace Applications

ANODE MATERIAL for Lithium ion Batteries

Light weight Electrode for Lead Acid Batteries

advantagesSignificant weight

reductionSize reduction of batteryBetter current collection

efficiencyEasy recycling Higher energy & power

densities

Carbon foam : sponge-like rigid engineering materials low density, large surface area with open cell wall structure

Patent Applied : Light weight carbon foam as electromagnetic interference (EMI)shielding and thermal interface material for aerospace applications

Page 5: egRoiw.kZ miyfC/;ka - National Physical Laboratory of IndiaCSIR-National Physical Laboratory Annual Report 2012-13 xxxvii New Standards Established Continued ... temperature time and

xxxixAnnual Report 2012-13CSIR-National Physical Laboratory

Source materials: HVPE grown poly-crystalline GaN target & RF Nitrogen plasmaSubstrate : Sapphire (0001)Growth Temp : 720°C

laser Molecular beam epitaxy of gan based Materials

nano Fabrication

• High crystalline quality GaN epitaxial layers grown on sapphire (0001) - X-ray rocking curve FWHM of (0002) plane : 102 arcsec (Reported: ~200 arcsec)

• Low background impurity level, especially oxygen that alters the electrical property (below detection limit of sIMs : <ppm) (Reported: High Oxygen impurity level)

• Ferromagnetic (NiFe) nanorings by E-beam lithography

• Gold Break junctions < 5nm on Si/SiO2

Materials & Products Continued ...

Page 6: egRoiw.kZ miyfC/;ka - National Physical Laboratory of IndiaCSIR-National Physical Laboratory Annual Report 2012-13 xxxvii New Standards Established Continued ... temperature time and

xl okf"kZd izfrosnu 2012-13 lh,lvkbZvkj&jk"Vªh; HkkSfrd iz;ksx'kkyk

Maitri Station Since1981Ionospheric parametersRadio & microwave communicationStudies of Polar Environment

New Indian Research station ‘Bharati’ (69° 24’S, 76° 11’ E) at Larsemann Hills, Antarctica. The new station is 3000 kilometre away from the present Maitri station (70° 45’ S, 11° 44’ E) set up under the leadership of CsIR – nPl scientist set up for space physics Research

Estimated emission factor of ammonia from rice-wheat cropping system at IARI research farm, New Delhi. The average emission factor of ammonia was 96.7 gnH3-n/kg-n/ha for wheat and 82.9 g nH3-n/kg-n/ha for rice.

Estimation of Ammonia Emission from Agriculture field

radio & atmospheric sciences

Materials & Products Continued ...

Scientific facilities at Antarctica developed by CSIR-NPL