miller geotechnical consultants, inc. 3801 automation way

76
Miller Geotechnical Consultants, Inc. 3801 Automation Way, Suite 100 Fort Collins, Colorado 80525 (970) 412-1256 August 17, 2009 Attn: Document Control Desk Deputy Director Decommission and Uranium Recovery Licensing Directorate Division of Waste Management and Environmental Protection Office of Federal and State Materials and Environmental Management Programs US Nuclear Regulatory Commission Washington DC 20555 Mail Stop T8F5 Deputy Director Decommission and Uranium Recovery Licensing Directorate Division of Waste Management and Environmental Protection Office of Federal and State Materials and Environmental Management Programs US Nuclear Regulatory Commission 11545 Rockville Pike Mail Stop T8F5 Rockville, Maryland 20852-2738 RE: Source Material License SUA-56; Western Nuclear, Inc., Split Rock Uranium Mill Tailings Facility; Surface Water and Groundwater Monitoring Report Dear Deputy Director: Please find enclosed for Nuclear Regulatory Commission review, the surface water and groundwater sampling results for the second half of 2008 for the Split Rock Uranium mill tailings facility. This monitoring was performed as required by license conditions 24 and 74. Figure 1 shows the location of the monitor wells and the surface water sample locations. The table presents the analytical results. Figures are also included in the enclosure, which show the temporal changes in water quality for key constituents. Some of the wells have more historic data as they were part of the previous monitoring network. The remaining wells have limited historic data since they were only sampled as part of the characterization study. As previously coordinated with NRC staff, monitor well maintenance has been recently performed due to sanding up of two existing monitor wells such that they drew insufficient water to provide a valid sample volume. Monitor wells SWAB-1 and SWAB-1 2 were replaced by monitor wells SWAB-1 R and SWAB-1 2R, respectively. Water quality in SWAB-12R shows similar water quality to the previous values and has concentrations that are indicative of background water quality. Water quality data from the replacement well SWAB-1 R shows higher concentrations for some constituents, notably uranium and sulfate, than previous data measured from well SWAB-1. SWAB-1 has shown elevated levels of constituents indicative of tailings seepage and is in the groundwater plume. Itis thought that the higher values in SWAB-1 R are a result of higher concentrations of tailings derived constituents at a slightly deeper depth in SWAB-1 R than were encountered in well SWAB-1 which was completed at a more shallow depth. The characterization data previously submitted indicates that there are variations in concentrations within the contaminate plume at different depths. While the data from SWAB-1 R has higher concentrations for uranium and sulfate, these values are consistent with SWAB-2 which is nearby and up-gradient. Water quality data from SWAB-2 has remained constant. The next down-gradient well, SWAB-29 shows no change in concentrations and has values that are indicative of

Upload: others

Post on 19-Jan-2022

2 views

Category:

Documents


0 download

TRANSCRIPT

Page 1: Miller Geotechnical Consultants, Inc. 3801 Automation Way

Miller Geotechnical Consultants, Inc. 3801 Automation Way, Suite 100Fort Collins, Colorado 80525

(970) 412-1256

August 17, 2009

Attn: Document Control DeskDeputy DirectorDecommission and Uranium Recovery Licensing DirectorateDivision of Waste Management and Environmental ProtectionOffice of Federal and State Materials and Environmental Management ProgramsUS Nuclear Regulatory CommissionWashington DC 20555Mail Stop T8F5

Deputy DirectorDecommission and Uranium Recovery Licensing DirectorateDivision of Waste Management and Environmental ProtectionOffice of Federal and State Materials and Environmental Management ProgramsUS Nuclear Regulatory Commission11545 Rockville PikeMail Stop T8F5Rockville, Maryland 20852-2738

RE: Source Material License SUA-56; Western Nuclear, Inc., Split Rock Uranium Mill Tailings Facility;Surface Water and Groundwater Monitoring Report

Dear Deputy Director:

Please find enclosed for Nuclear Regulatory Commission review, the surface water and groundwater samplingresults for the second half of 2008 for the Split Rock Uranium mill tailings facility. This monitoring was performed asrequired by license conditions 24 and 74.

Figure 1 shows the location of the monitor wells and the surface water sample locations. The table presents theanalytical results. Figures are also included in the enclosure, which show the temporal changes in water quality forkey constituents. Some of the wells have more historic data as they were part of the previous monitoring network.The remaining wells have limited historic data since they were only sampled as part of the characterization study.

As previously coordinated with NRC staff, monitor well maintenance has been recently performed due to sanding upof two existing monitor wells such that they drew insufficient water to provide a valid sample volume. Monitor wellsSWAB-1 and SWAB-1 2 were replaced by monitor wells SWAB-1 R and SWAB-1 2R, respectively. Water quality inSWAB-12R shows similar water quality to the previous values and has concentrations that are indicative ofbackground water quality.

Water quality data from the replacement well SWAB-1 R shows higher concentrations for some constituents, notablyuranium and sulfate, than previous data measured from well SWAB-1. SWAB-1 has shown elevated levels ofconstituents indicative of tailings seepage and is in the groundwater plume. It is thought that the higher values inSWAB-1 R are a result of higher concentrations of tailings derived constituents at a slightly deeper depth in SWAB-1 Rthan were encountered in well SWAB-1 which was completed at a more shallow depth. The characterization datapreviously submitted indicates that there are variations in concentrations within the contaminate plume at differentdepths. While the data from SWAB-1 R has higher concentrations for uranium and sulfate, these values areconsistent with SWAB-2 which is nearby and up-gradient. Water quality data from SWAB-2 has remained constant.The next down-gradient well, SWAB-29 shows no change in concentrations and has values that are indicative of

Page 2: Miller Geotechnical Consultants, Inc. 3801 Automation Way

Deputy Director, NRCPage 2 of 2August 17, 2009

background water quality. Therefore, while some of the water quality values from SWAB-1 R are greater than valuesfrom SWAB-i, it is believed they are reflective of expected variations in water quality with depth and not indicative ofchanging site conditions.

In all cases, including the new data from the replacement wells, the data indicate that surface water and groundwaterquality are within expected ranges and that the system is behaving as predicted.

If you have any questions, please contact me at your convenience.

Sin ly,

Louis MillerConsulting Engineer

Enclosure

cc. Steve Hall, StollerScott Surovchak, DOEMark Thiesse, WDEQAnne Thomas, WNI

Miller Geotechnical Consultants, Inc.

Page 3: Miller Geotechnical Consultants, Inc. 3801 Automation Way

m m m m m m m m m m m m m m m m m m m

LEGEND

* MONITORING WELL LOCATIONS

PROPOSED LONG-TERM CARE BOUNDARY

A SURFACE WATER SAMPLE LOCATIONSSCALE IN FEET

0 3000 N

Page 4: Miller Geotechnical Consultants, Inc. 3801 Automation Way

Semi-Annual Groundwater and SurfaceWater Compliance Monitoring Results

First Half of Year 2009

Page 5: Miller Geotechnical Consultants, Inc. 3801 Automation Way

= M = = M = = = M = = = = = = = = M =

WNI Split Rock Mill Groundwater and1st Half 2009 (Sampled: 5/12/09 to 5/13/2009)

Surface Water Quality Semi-Annual Report

Parameter(1 ) JJ-IR SWAB-1R(3 ) SWAB-2 SWAB-12R(4 ) SWAB-4 SWAB-22 SWAB-29 SWAB-31 SWAB-32 WELL-1Aluminum (mg/L) <0.1 <0. 1 <0. 1Free Ammonia as N(2) (mg/L) <0.00017 <0.00029 0.068Antimony (mg/L) <0.003 <0.003 <0.003Arsenic (mg/L) <0.01 <0.01 <0.01Berylilum (mg/L) <0.004 <0.004 <0.004Cadmium (mg/L) <0.001 <0.001 <0.001Chloride (mg/L) 26 18 124Conductivity Field (pS/cm) 558 2630 4420 561 1608 429 416 378 459 4380Fluoride (mg/L) 0.2 0.2 0.3Lead (mg/L) <0.005 <0.005 <0.005Manganese (mg/L) 0.18 <0.05 13.3Molybdenum (mg/L) <0.1 <0.1 <0.1Nickel (mg/L) <0.05 <0.05 <0.05Nitrate + Nitrite as N (mg/L) 85.4 0.4 12.2pH Field (std units) 6.87 6.84 6.43 7.06 7.07 7.03 6.70 7.08 7.18 6.51pH Lab (std units) 7.35 7.89 6.65Radium-226 (pCi/L) 0.14 <-0.2 0.92Radium-228 (pCi/L) 1.6 1.3 <0.5Selenium (mg/L) <0.005 <0.005 0.007Sulfate (mg/L) 58 1000 1750 100 555 47 46 33 52 2060TDS (mg/L) 2240 358 3770Tempurature Field (C) 10.2 10.9 10.2 11.2 17.7 18.0 10.8 11.8 13.9 11.3Thallium (mg/L) <0.001 <0.001 0.003Thorium-230 (pCi/L) <0.02 <0.2 <0.002Uranium (mg/L) 0.011 1.91 1.38 0.037 1.11 0.027 0.041 0.031 0.121 4.87Water Elevation (ft) NA 6291.86 6291.40 6295.04 6292.15 6287.74 6276.60 6264.40 6271.30 6295.15

Notes:

(1) All metals are dissolved analyte concentrations

(2) Free.ammonia concentration calculated from the laboratory reported total ammonia concentration and field measured pH, consistent

with the method used to determine the ACL for ammonia

(3) Well SWAB-1 R installed as replacement for SWAB-I. Water Elevation taken at SWAB-1

(4) Well SWAB-12R installed as replacement for SWAB-12. Water Elevation taken at SWAB-12

< indicates analyte result less than Laboratory Reporting Limit

Page 6: Miller Geotechnical Consultants, Inc. 3801 Automation Way

= M = = M = = M M = = = = = = = = M =

WNI Split Rock Mill Groundwater and1st Half 2009 (Sampled: 5/12/09 to 5/13/2009)

Surface Water Quality Semi-Annual Report

Parameter(1 ) WELL-4R WELL-5 WN-21 WN-39B WN-41B WN-42A SW-1 SW-2 SW-3 SW-4 SW-5Aluminum (mg/L) 1.6 <0.1 <0.1

Free Ammonia as N (2) (mg/L) 0.17 <0.00018 0.014Antimony (mg/L) 0.003 <0.003 <0.003Arsenic (mg/L) <0.01 <0.01 <0.01Berylilum (mg/L) <0.004 <0.004 <0.004Cadmium (mg/L) 0.022 <0.001 <0.001Chloride (mg/L) 117 102 8Conductivity Field (hiS/cm) 6600 3910 572 1062 2420 4120 208 229 208 208 209Fluoride (mg/L) 7.2 <0.1 0.2Lead (mg/L) <0.005 <0.005 <0.005Manganese (mg/L) 93.7 0.42 0.32Molybdenum (mg/L) <0.1 <0.1 <0.1Nickel (mg/L) 0.51 <0.05 <0.05Nitrate + Nitrite as N (mg/L) 154 58.5 3.2pH Field (std units) 6.09 6.85 7.14 7.29 7.63 6.94 6.88 6.96 7.02 7.39 6.96pH Lab (std units) 6.31 6.91 7.78Radium-226 (pCi/L) 0.22 <0.01 <-0.2Radium-228 (pCi/L) <0.7 1.2 <0.6Selenium (mg/L) 0.034 0.017 <0.005 0.03Sulfate (mg/L) 3140 1730 87 268 367 2220 19 20 20 20 21TDS (mg/L) 4890 3660 354Tempurature Field (C) 11.8 11.2 11.8 10.4 10.1 10.8 12.8 12.7 12.8 12.8 12.7Thallium (mg/L) <0.001 <0.001 <0.001Thorium-230 (pCi/L) <-0.06 <0.005 <0.01Uranium (mg/L) 0.321 1.94 0.071 0.498 0.009 1.05 <0.001 <0.001 0.002 0.002 0.002Water Elevation (ft) 6286.32 6282.40 6295.91 6275.02 6272.92 6277.84 -:::1

Notes:

(1) All metals are dissolved analyte concentrations

(2) Free ammonia concentration calculated from the laboratory reported total ammonia concentration and field measured pH, consistent

with the method used to determine the ACL for ammonia

(3) Well SWAB-1 R installed as replacement for SWAB-1. Water Elevation taken at SWAB-1

(4) Well SWAB-12R installed as replacement for SWAB-12. Water Elevation taken at SWAB-12

< indicates analyte result less than Laboratory Reporting Limit

Page 7: Miller Geotechnical Consultants, Inc. 3801 Automation Way

GROUNDWATER

Page 8: Miller Geotechnical Consultants, Inc. 3801 Automation Way

Jeffrey City JJ-1 R

pH (Field) (std. Units)

10

9

8

7

6

5

4

3

2

1

0

TDS (mg/L)

500

450

400 -

350 "

300

250

200

150

100

50

0 •

Open symbols indicate value below detection limit

Page 9: Miller Geotechnical Consultants, Inc. 3801 Automation Way

Jeffrey City JJ-1 R

Sulfate (mg/L)80 -

70 -

60 -

50 -

40 -

30 -

20 -

10 -

0 I.

Open symbols indicate value below detection limit

Page 10: Miller Geotechnical Consultants, Inc. 3801 Automation Way

Jeffrey City SWAB-1

pH (Field) (std. Units)

10

9

8

6

5

4

S•SWAB-2 j WAB-11

0'

TDS (mg/L)2500

2000

1500

1000

500 - SWAB-1

SWAB-1 R

0'n80 §

Open symbols indicate value below detection limit

Page 11: Miller Geotechnical Consultants, Inc. 3801 Automation Way

Jeffrey City SWAB-1

Sulfate (mg/L)1200

1000

800

600

400 -

200 - "0"-SWAB-1

0 SWAB-1R

Uranium (mg/L)2.5

2

1.5

1

0.5 9 WAB-1

A SWAB-1R

0n

n n n

Open symbols indicate value below detection limit

Page 12: Miller Geotechnical Consultants, Inc. 3801 Automation Way

Jeffrey City SWAB-12

pH (Field) (std. Units)

10

9

8

7

6

5

4

3

2 -q-SWAB-i 2

1 [, SWAB-12R

0

n n

TDS (mg/L)1600

1400 - S1WAB-12R]

1200

1000

800

600

400 -

200

0,

Open symbols indicate value below detection limit

Page 13: Miller Geotechnical Consultants, Inc. 3801 Automation Way

Jeffrey City SWAB-12

Sulfate (mg/L)

106

105 - 9ISWAB-12

14-SWAB-12R104

103

102

101

100

99

6

Uranium (mg/L)0.07 -

0.06

0.05

0.04

0.03

0.02--- SWAB-1 2

0.01 SWAB-12R

0

Open symbols indicate value below detection limit

Page 14: Miller Geotechnical Consultants, Inc. 3801 Automation Way

Jeffrey City SWAB-2

pH (Field) (std. Units)10

9

8

7

6

5

4

3

2

1

0

TDS (mg/L)5000

4500

4000

3500

3000

2500

2000

1500

1000

500

0*

Open symbols indicate value below detection limit

Page 15: Miller Geotechnical Consultants, Inc. 3801 Automation Way

Jeffrey City SWAB-2

Sulfate (mg/L)2000

1800

1600

1400 -

1200

1000

800

600

400

200

0

Uranium (mg/L)2

1.8

1.6

1.4

1.2

1

0.8

0.6

0.4

0.2

0.

Open symbols indicate value below detection limit

Page 16: Miller Geotechnical Consultants, Inc. 3801 Automation Way

Jeffrey City SWAB-22

pH (Field) (std. Units)

10

9

8

7

6

5

4

3

2

1

0

Open symbols indicate value below detection limit

Page 17: Miller Geotechnical Consultants, Inc. 3801 Automation Way

Jeffrey City SWAB-22

Sulfate (mg/L)80

70

60

50

40

30

20

10

0.

n

Uranium (mg/L)0.04

0.035

0.03

0.025

0.02 ,

0.015

0.01

0.005

0

n n

Open symbols indicate value below detection limit

Page 18: Miller Geotechnical Consultants, Inc. 3801 Automation Way

Jeffrey City SWAB-29

Open symbols indicate value below detection limit

Page 19: Miller Geotechnical Consultants, Inc. 3801 Automation Way

Jeffrey City SWAB-29

Sulfate (mg/L)80

70

60 -

50 v

40

30

20

10

0

Uranium (mgIL)0.08

0.07

0.06

0.05 ,

0.04

0.03

0.02

0.01

0

nn n n

Open symbols indicate value below detection limit

Page 20: Miller Geotechnical Consultants, Inc. 3801 Automation Way

Jeffrey City SWAB-31

pH (Field) (std. Units)

10

9

8

7

6

5

4

3

2

1

0

TDS (mg/L)

400

350

300

250

200

150

100

50

0

Open symbols indicate value below detection limit

Page 21: Miller Geotechnical Consultants, Inc. 3801 Automation Way

Jeffrey City SWAB-31

Sulfate (mg/L)

50

45

40

35

30

25

20

15

10

5

0

Uranium (mg/L)0.05

0.045

0.04

0.035 -

0.03 ,

0.025

0.02

0.015

0.01

0.005

0

n n n n

Open symbols indicate value below detection limit

Page 22: Miller Geotechnical Consultants, Inc. 3801 Automation Way

Jeffrey City SWAB-32

pH (Field) (std. Units)

10

9

8

7

6

5

4

3

2

1

0'

n

TDS (mg/L)

400

350

300 "

250

200

150

100

50

0 u i

Open symbols indicate value below detection limit

Page 23: Miller Geotechnical Consultants, Inc. 3801 Automation Way

Jeffrey City SWAB-32

Sulfate (mg/L)80

70

60 -

50 -

40

30

20

10

0

n n

Uranium (mg/L)0.2

0.18

0.16

0.14 -

0.12 ,

0.1

0.08

0.06

0.04

0.020

Open symbols indicate value below detection limit

Page 24: Miller Geotechnical Consultants, Inc. 3801 Automation Way

Jeffrey City SWAB-4

pH (Field) (std. Units)

10

9

8

7

6

5

4

3

2

1

0

TDS (mg/L)

2000

1600

1200

800

400

0

Open symbols indicate value below detection limit

Page 25: Miller Geotechnical Consultants, Inc. 3801 Automation Way

Jeffrey City SWAB-4

Sulfate (mg/L)

800

700

600

500

400

300

200

100

0~

Uranium (mg/L)

1.6

1.4

1.2 -

1

0.8

0.6

0.4

0.2

0"

Open symbols indicate value below detection limit

Page 26: Miller Geotechnical Consultants, Inc. 3801 Automation Way

Jeffrey City WELL-1

pH (Field) (std. Units)

10

9

8

7

6

5

4

3

2

1

0

TDS (mg/L)

5000

4500

4000

3500 -

3000

2500

2000

1500

1000

500

0

Open symbols indicate value below detection limit

Page 27: Miller Geotechnical Consultants, Inc. 3801 Automation Way

Jeffrey City WELL-1

Sulfate (mg/L)3000

2500

2000 -

1500

1000

500

0

n n nn

Uranium (mg/L)8

7

6

5

4

3

2

1

0.

nn

Open symbols indicate value below detection limit

Page 28: Miller Geotechnical Consultants, Inc. 3801 Automation Way

Jeffrey City WELL-4R

pH (Field) (std. Units)

10

9

8

7

6

5

4

3

2

1

0

nI ~§§§

TDS (mg/L)

6000

5000 -

4000

3000

2000

1000

0

Open symbols indicate value below detection limit

Page 29: Miller Geotechnical Consultants, Inc. 3801 Automation Way

Jeffrey City WELL-4R

Sulfate (mg/L)

4000

3500

3000 ...... .

2500

2000

1500

1000

500

0

Open symbols indicate value below detection limit

Page 30: Miller Geotechnical Consultants, Inc. 3801 Automation Way

Jeffrey City WELL-5

pH (Field) (std. Units)

10

9

8

7

6

5

4

3

2

1

0

TDS (mg/L)

5000

4500

4000

3500

3000

2500

2000

1500

1000

500

0 "

n n n6

Open symbols indicate value below detection limit

Page 31: Miller Geotechnical Consultants, Inc. 3801 Automation Way

Jeffrey City WELL-5

Uranium (mg/L)3

2.5

2

1.5

1

0.5

0.-

8 6 8n

Open symbols indicate value below detection limit

Page 32: Miller Geotechnical Consultants, Inc. 3801 Automation Way

Jeffrey City WN-21

pH (Field) (std. Units)

10

9

8

7

6

5

4

3

2

1

0

Open symbols indicate value below detection limit

Page 33: Miller Geotechnical Consultants, Inc. 3801 Automation Way

Jeffrey City WN-21

Uranium (mg/L)0.2

0.18

0.16

0.14

0.12

0.1

0.08

0.06

0.04

0.02

0

Open symbols indicate value below detection limit

Page 34: Miller Geotechnical Consultants, Inc. 3801 Automation Way

Jeffrey City WN-39B

pH (Field) (std. Units)

10

9

8

7

6

5

4

3

2

1

0

Open symbols indicate value below detection limit

Page 35: Miller Geotechnical Consultants, Inc. 3801 Automation Way

Jeffrey City WN-39B

Uranium (mg/L)

0.6

0.5 -

0.4 -

0.3 -

0.2 -

0.1 -

0. &

Open symbols indicate value below detection limit

Page 36: Miller Geotechnical Consultants, Inc. 3801 Automation Way

Jeffrey City WN-41 B

TDS (mg/L)

1600 -

1400 -

1200

1000

800

600

400

200

0 _8 • _ !

Open symbols indicate value below detection limit

Page 37: Miller Geotechnical Consultants, Inc. 3801 Automation Way

Jeffrey City WN-41 B

Sulfate (mg/L)500

450

400 -

350

300

250

200

150

100

500

n n n n

Uranium (mg/L)0.03

0.025

0.02

0.015

0.01

0.005

0.

6n

Open symbols indicate value below detection limit

Page 38: Miller Geotechnical Consultants, Inc. 3801 Automation Way

Jeffrey City WN-42A

pH (Field) (std. Units)

10

9

897 R •=•

6

5

4

3

2

1

0•

TDS (mg/L)

6000

5000

4000

3000

2000

1000

0

Open symbols indicate value below detection limit

Page 39: Miller Geotechnical Consultants, Inc. 3801 Automation Way

Jeffrey City WN-42A

Sulfate (mg/L)3000

2500

2000 -

1500

1000

500

01

n n n

Uranium (mg/L)1.5

1.25

1

0.75

0.5

0.25

0.

n n n

Open symbols indicate value below detection limit

Page 40: Miller Geotechnical Consultants, Inc. 3801 Automation Way

I -,.•T I-• Ln • 1C,,, ,,v; . *d,.O- du LfreeI( I-lignway(fZoui1 -U. uoxJZo' - (,aspe;, Wrb'Ž'bŽU'Toll Free 888.235.0515 , 307235.0515 - Fax 307234.1639 - casper~energylab.com - www.energylab.com

FrABRAOR9 S

LABORATORY ANALYTICAL REPORT

O Client: Western NuclearProject: Split Rock Mill Site GWPPLab ID: C09050425-010Client Sample ID: JJ-1 R

Report Date: 07/13/09

Collection Date: 05/12/09 08:40DateReceived: .05/13109

Matrix: Aqueous

MCL/Analyses Result Units Qualifier RL QCL Method Analysis Date / By

MAJOR IONSSulfate

METALS - DISSOLVEDUranium

FIELD PARAMETERSpH

... Performed by Sampler

58 mg/L

0.011 mg/L

6.87 s.u.

1

0.001

A4500-S04 E 05/19/09 12:41 /jal

E200.8

FIELD

05/26/09 00:57 / ts

05/12/09 08:40 /

0

Report RL - Analyte reporting limit.Definitions: QCL - Quality control limit.

MCL - Maximum contaminant level.ND - Not detected at the reporting limit.

COPc

Page 41: Miller Geotechnical Consultants, Inc. 3801 Automation Way

AIV•flLn I L/-D'I M vrzr7,/4 , /IV(, * Z a1 La/t &ee( tK MlgaWay (brZdUV) - 1-U. LtA'7 J2b - Uasper, WY •'b'2To//Free 888 235. 0515 - 307235. 0515 - Fax 307234.1639 • [email protected] , www energy/ab.com

F:LAOP-4 #

LABORATORY ANALYTICAL REPORT

O Client:Project:Lab ID:Client Sample ID:

Western Nuclear

Split Rock Mill Site GWPPC09050425-005SWAB-1 R

Report Date: 07/13/09Collection Date: 05/13/09 08:38

DateReceived: 05/13/09Matrix: Aqueous

MCL/Qualifier RL QCLAnalyses Result Units Method Analysis Date / By

MAJOR IONSChloride

FluorideNitrogen, Ammonia as N

Nitrogen, Nitrate+Nitrite as N

Sulfate

260.2ND

85.4

1000

mg/Lmg/Lmg/L

mg/L

mg/LD

D

10.10.05

0.310

0.0110

A4500-Cl B

A4500-F CE350.1E353.2

A4500-SO4

05/26/09 12:53 / jal

05/18/09 15:52 / IjI05/15/09 14:07 / eli-b

05/15/09 15:24 / eli-bE 05/19/09 12:06/jal

PHYSICAL PROPERTIESpHSolids, Total Dissolved TDS @ 180 C

METALS - DISSOLVEDAluminumAntimonyArsenicBerylliumCadmiumLeadManganeseMolybdenumNickelSeleniumThalliumUranium

RADIONUCLIDES - DISSOLVEDRadium 226Radium 226 precision (+)Radium 226 MDCRadium 228Radium 228 precision (+)Radium 228 MDCThorium 230Thorium 230 precision (+)Thorium 230 MDC

7.35 s.u.2240 mg/L

A4500-H B 05/15/09 10:55 / ddA2540 C 05/18/09 13:17 / rp

NDND

ND

ND

NDND

0.18ND

NDND

ND1.91

0.14

0.140.22

1.6

0.71.1

0.020.10.3

mg/Lmg/L

mg/L

mg/Lmg/Lmg/Lmg/Lmg/L

mg/Lmg/L

mg/Lmg/L

pCi/LpCi/L

pCi/LpCi/LpCi/LpCi/LpCi/LpCi/LpCi/L

0.10.003

0.01

0.004

0.0010.005

0.050.1

0.050.005

0.0010.001

E200.8

E200.8

E200.8

E200.8E200.8

E200.8E200.8

E200.8E200.8E200.8E200.8

E200.8

E903.0E903.0

E903.0RA-05RA-05

RA-05

E907.0E907.0E907.0

FIELD

05/15/09 23:02 / ts05/15/09 23:02 / ts

05/15/09 23:02 / ts

05/15/09 23:02 / ts

05/15/09 23:02 / ts05/15/09 23:02 / ts05/15/09 23:02 / ts

05/15/09 23:02 / ts

05115109 23:02 /ts05/15/09 23:02 / ts05/15/09 23:02 / ts

05/15/09 23:02 / ts

06/01/09 14:08 / jah

06/01109 14:08 / jah

06/01/09 14:08 /jah

05/27/09 10:00 / plj05/27/09 10:00 / plj

05/27/09 10:00 / plj05/27/09 07:37 / dmf

05/27/09 07:37 / dmf

05t27109 07:37 1 dmf

05/13/09 08:38 /

U

U

FIELD PARAMETERSpH

_ Performed by Sampler6.84 s.u.

* Report RL - Analyte reporting limit.Definitions: QCL - Quality control limit.

MDC - Minimum detectable concentrationU - Not detected at minimum detectable concentration

cPoy

MCL - Maximum contaminant level.ND - Not detected at the reporting limit.D - RL increased due to sample matrix interference.

Page 42: Miller Geotechnical Consultants, Inc. 3801 Automation Way

IfoVr. 88,2 '5.01, LIuA 0.5,flwd1 (0Fa0(/ I0. ,OX /-L/bom, ww, Udner, ylb VomzToll Free08882350515'- 3072350515 - Fax 3072341639 - caspenffenergylab~com, wwwoenergy/ab~com

LABORATORY ANALYTICAL REPORT

O Client:Project:Lab ID:Client Sample ID:

Western Nuclear

Split Rock Mill Site GWPP

C09050425-006

SWAB-12R

Report Date: 07/13/09Collection Date: 05/12/09 13:40

DateReceived: 05/13/09

Matrix: Aqueous

MCL/Analyses Result Units Qualifier RL QCL Method Analysis Date / By

MAJOR IONSChloride

Fluoride

Nitrogen, Ammonia as N

Nitrogen, Nitrate+Nitrite as NSulfate

18

0.2

ND

0.4100

mg/L

mg/Lmg/Lmg/Lmg/L

PHYSICAL PROPERTIESpHSolids, Total Dissolved TDS @ 180 C

METALS - DISSOLVED

AluminumAntimonyArsenicBerylliumCadmiumLeadManganeseMolybdenumNickelSeleniumThalliumUranium

RADIONUCLIDES - DISSOLVEDRadium 226Radium 226 precision (+)Radium 226 MDCRadium 228Radium 228 precision (+)Radium 228 MDCThorium 230Thorium 230 precision (+)Thorium 230 MDC

FIELD PARAMETERSpH

*** Performed by Sampler

7.89 s.u.

358 mg/L

NDNDND

NDND

ND

ND

NDNDND

ND

0,037

-0.2

0.090.21

1.30.7

1.0

0.2

0.20.3

mg/L

mg/Lmg/L

mg/Lmg/Lmg/L

mg/L

mg/Lmg/Lmg/L

mg/L

mg/L

10.1

0.05

0.2

1

0.01

10

0.10.0030.01

0.0040.0010.005

0.05

0.10.05

0.005

0.001

0.001

A4500-H B 05/15/09 10:57 /ddA2540 C 05/18/09 13:17 / rp

A4500-CI B

A4500-F C

E350.1

E353.2

A4500-SO4

05/26/09 12:57 / jal

05/18/09 15:58 / IjI05/15/09 14:08 / eli-b

05/15/09 15:25 / eli-b

E 05/19/09 12:10/jal

E200.8

E200.8E200.8

E200.8E200.8

E200.8

E200.8

E200.8E200.8

E200.8

E200.8

E200.8

E903.0E903.0

E903.0

RA-05

RA-05RA-05E907.0

E907.0

E907.0

FIELD

05/15/09 23:09 /ts05/15/09 23:09 /ts05/15/09 23:09 /ts

05/15/09 23:09 / ts05/15/09 23:09 /ts

05/15/09 23:09 / ts

05/15/09 23:09 / ts

05/15/09 23:09 /ts05/15/09 23:09 /ts

05/15/09 23:09 / ts

05/15/09 23:09 / ts

05/15/09 23:09 /ts

06/01/09 14:08 / jah06/01/09 14:08 /jah

06/01/09 14:08 /jah

05/27/09 10:00 / plj

05/27/09 10:00 / plj05/27/09 10:00 / plj05/27/09 07:37 / dmf

05/27/09 07:37 / dmf

05/27/09 07:37 / dmf

05/12/09 13:40 /

pCi/LpCi/LpCi/LpCi/LpCi/LpCi/LpCi/LpCi/LpCi/L

U

U

7.06 s.u.

' O Report RL - Analyte reporting limit.Definitions: QCL - Quality control limit.

MDC - Minimum detectable concentration

I

MCL - Maximum contaminant level.

ND - Not detected at the reporting limit.U - Not detected at minimum detectable concentration

Page 43: Miller Geotechnical Consultants, Inc. 3801 Automation Way

• •*VFr1L=;nI LJWL'lm I Ln i, Oj, I/IVL,. • -oWZo Odlf L,[•b•( Fnig[Wdy (O-OUIJ - -.L/. LIOX ;izo , ,aspel VvY rzbuzToll Free 888.235 0515 - 307235 0515 • Fax 307234.1639 - [email protected] - www energylab.com

LABORATORY ANALYTICAL REPORT

O Client:Project:Lab ID:Client Sample ID:

Western NuclearSplit Rock Mill Site GWPP

C09050425-016SWAB-2

Report Date: 07/13/09Collection Date: 05/13/09 09:05

DateReceived: 05/13/09

Matrix: Aqueous

MCL/Analyses Result Units Qualifier RL QCL Method Analysis Date / By

MAJOR IONSSulfate

METALS - DISSOLVEDUranium

FIELD PARAMETERSpH

**Performed by Sampler

1750 mg/L

1.38 mg/L

6.43 s.u.

D 30 A4500-S04 E 05/19/09 12:59/jal

0.001 E200.8

FIELD

05/26/09 01:22 / ts

05/13/09 09:05 / *

ReportDefinitions:

RL - Analyte reporting limit.

QCL - Quality control limit.

D - RL increased due to sample matrix interference.

MCL - Maximum contaminant level.ND - Not detected at the reporting limit.

AVINI Tý%vfto"% EL--B

Uum- J6

Page 44: Miller Geotechnical Consultants, Inc. 3801 Automation Way

ACIVCHvL F L140UIA I UNII.b, INI. - ZdLsy alt (,reek/-l.gnway (tzbul) -1-.U. ox. ,YOX •Uasper, v ydzbUzToll Free 888235.0515 - 307235.0515 - Fax 3072341639 - casperaenergylabcom www energylab.com

48OR4 Tý

LABORATORY ANALYTICAL REPORT

O Client:Project:Lab ID:Client Sample ID:

Western Nuclear

Split Rock Mill Site GWPP

C09050425-018SWAB-22

Report Date: 07/13/09Collection Date: 05/12/09 13:33

DateReceived: 05/13/09

Matrix: Aqueous

MCLIAnalyses Result Units Qualifier RL QCL Method Analysis Date I By

MAJOR IONSSulfate

METALS - DISSOLVEDUranium

FIELD PARAMETERSpH

... Performed by Sampler

47 mg/L

0.027 mg/L

7.03 s.u.

1 A4500-SO4 E 05/19/09 13:05 /jal

0.001 E200.8

FIELD

05/26/09 02:53 / ts

05/12/09 13:33 / I

0

Report0. Definitions:

RL - Analyte reporting limit.QCL - Quality control limit.

MCL - Maximum contaminant level.ND - Not detected at the reporting limit.

COPy

Page 45: Miller Geotechnical Consultants, Inc. 3801 Automation Way

I . .l , vt,,. " Oal L.I,/A/ ni•giiwdyoC(OOUI, -I/-L/.A UXJeO0X - ubp&e, VVT •dUd

Toll Free 888.235,0515, 307235.0515 -Fax 307234,1639 - casper@energy/abcom .www.energy/ab. comrLIOATRE

LABORATORY ANALYTICAL REPORT

O Client: Western NuclearProject: Split Rock Mill Site GWPP

Lab ID: C09050425-019Client Sample ID: SWAB-29

Report Date: 07/13/09Collection Date: 05/13/09 09:35

DateReceived: 05/13/09

Matrix: Aqueous

MCL/Analyses Result Units Qualifier RL QCL Method Analysis Date I By

MAJOR IONSSulfate 46 mg/L 1 A4500-SO4 E 05/19/09 13:07 /jal

METALS - DISSOLVEDUranium

FIELD PARAMETERSpH

... Performed by Sampler

0.041 mg/L 0.001 E200.8

FIELD

05/26/09 02:58 / ts

05/13/09 09:35 / *6.70 s.u.

0

0Report RL - Analyte reporting limit.Definitions: QCL - Quality control limit.

MCL - Maximum contaminant level.ND - Not detected at the reporting limit.

COPY

Page 46: Miller Geotechnical Consultants, Inc. 3801 Automation Way

_,,"w•.I., ,c, n n,, "v-. • zJYl Oadl ,r8eek Ignway (b'2bV7J - -U. b'ox 3258 - Casper, WY82502Toll Free 888.235 0515 - 307235.0515 - Fax 307.234.1639 - casper@energy/ab.com . www energylab.com

LABORATORY ANALYTICAL REPORT

Client:

Project:Lab ID:Client Sample ID:

Western Nuclear

Split Rock Mill Site GWPP

C09050425-020

SWAB-31

Report Date: 07113109Collection Date: 05/13/09 10:01

DateReceived: 05/13/09

Matrix: Aqueous

MCL/Analyses Result Units Qualifier RL QCL Method Analysis Date / By

MAJOR IONSSulfate

METALS - DISSOLVEDUranium

FIELD PARAMETERSpH

_ Performed by Sampler

33 mg/L

0.031 mg/L

7.08 s.u.

1

0.001

A4500-SO4 E 05/19/09 13:09/jal

E200.8

FIELD

05126/09 03:02 / ts

05/13/09 10:01 / ***

0

ReportDefinitions:

RL - Analyte reporting limit.QCL - Quality control limit.

MCL - Maximum contaminant level.ND - Not detected at the reporting limit.

COPY

Page 47: Miller Geotechnical Consultants, Inc. 3801 Automation Way

--. -, -- .. ".I yllfvay (Q,ýVVI -/ FL/. OPUA 0,2ýUO -Llda',Ul4 VV f OdOUVTo/Free 888235.0515- 307.235-0515 Fax 307234.1639 - casper~energy/ab com - www energy/ab com

LABORATORY ANALYTICAL REPORT

( DClient:Project:Lab ID:Client Sample ID:

Western Nuclear

Split Rock Mill Site GWPP

C09050425-021SWAB-32

Report Date: 07/13/09

Collection Date: 05/13/09 10:30

DateReceived: 05/13/09

Matrix: Aqueous

MCL/Analyses Result Units Qualifier RL QCL Method Analysis Date / By

MAJOR IONSSulfate 52 mg/L A4500-SO4 E 05/19/09 13:10/jal

METALS - DISSOLVEDUranium

FIELD PARAMETERSpH

_ Performed by Sampler

0.121 mg/L

7.18 s.u.

0.001 E200.8

FIELD

05/26/09 03:06 / ts

05/13/09 10:30 / 1

0

ReportDefinitions:

RL - Analyte reporting limit.

QCL - Quality control limit.MCL - Maximum contaminant level.ND - Not detected at the reporting limit.

copy

Page 48: Miller Geotechnical Consultants, Inc. 3801 Automation Way

L&Aq - Toll Free 888.235.0515 3072350515 - Fax 307234. 1639 • [email protected] . www.energylab. com

LABORATORY ANALYTICAL REPORT

O Client:Project:Lab ID:Client Sample ID:

Western NuclearSplit Rock Mill Site GWPP

C09050425-017SWAB-4

Report Date: 07/13/09

Collection Date: 05/12/09 14:06

DateReceived: 05/13/09

Matrix: Aqueous

MCLIAnalyses Result Units Qualifier RL QCL Method Analysis Date / By

MAJOR IONSSulfate

METALS - DISSOLVEDUranium

FIELD PARAMETERSpH

.* Performed by Sampler

555 mg/L

1.11 mg/L

7.07 s.u.

D 6 A4500-SO4 E 05/19/09 13:03 / jal

0.001 E200.8

FIELD

05/26/09 02:49 / ts

05/12/09 14:06 /***

0

ReportDefinitions:

RL - Analyte reporting limit.

QCL - Quality control limit.

D - RL increased due to sample matrix interference.

MCL - Maximum contaminant level.ND - Not detected at the reporting limit.

copy

Page 49: Miller Geotechnical Consultants, Inc. 3801 Automation Way

. .,,v ,,4'. - 4 JO., a .C7 I-U/JylWdy (o0, ..:UI/ I/-.LA VOX '1zov - asper, vvr dz !uzV Toll Free 888,235 0515 • 307,235 0515 - Fax 307,234. 1639 o [email protected] -n.www energy/abcoam

F:9 9

LABORATORY ANALYTICAL REPORT

O Client: Western NuclearProject: Split Rock Mill Site GWPPLab ID: C09050425-001Client Sample ID: WNI-1

Report Date: 07/13/09Collection Date: 05/12/09 13:34

DateReceived: 05/13/09

Matrix: Aqueous

MCL/Analyses Result Units Qualifier RL QCL Method Analysis Date/ By

MAJOR IONSChloride

FluorideNitrogen, Ammonia as NNitrogen, Nitrate+Nitrite as N

Sulfate

124

0.3

41.9

12.22060

mg/Lmg/L

mg/L

mg/Lmg/L

10.1

D 0.2

0.2

D 30

A4500-Cl B

A4500-F C

E350.1

E353.2

A4500-SO4

05/26/09 12:46 /jal05/18/09 15:29 / Ij!05/15/09 15:48 / eli-b

05/15/09 14:56 / eli-bE 05/19/09 12:01 /jal

PHYSICAL PROPERTIESpHSolids, Total Dissolved TDS @ 180 C

METALS - DISSOLVEDAluminumAntimonyArsenicBerylliumCadmiumLeadManganeseMolybdenumNickelSeleniumThalliumUranium

RADIONUCLIDES - DISSOLVEDRadium 226Radium 226 precision (+)Radium 226 MDCRadium 228Radium 228 precision (+)Radium 228 MDCThorium 230Thorium 230 precision (+)Thorium 230 MDC ,

FIELD PARAMETERSpH

_ Performed by Sampler

6.65 s.u.3770 mg/L

.0.0110

A4500-H B 05/15/09 10:46 / ddA2540 C 05/18/09 13:15 / rp

ND

ND

ND

NDNDND13.3

ND

ND0.007

0.003

4.87

0.920.22

0.210.50.6

1.0

0.0020.2

0.5

mg/Lmg/Lmg/Lmg/Lmg/Lmg/L

mg/L

mg/Lmg/Lmg/Lmg/L

mg/L

pCi/LpCi/LpCi/LpCi/LpCi/LpCi/LpCi/LpCi/L

pCi/L

0.10.003

0.01

0.004

0.0010.005

0.05

0.10.05

0.005

0.001

0.001

E200.8E200.8

E200.8

E200.8E200.8E200.8

E200.7

E200.8E200.8E200.8

E200.8

E200.8

E903.0

E903.0E903.0RA-05

RA-05

RA-05E907.0

E907.0

E907.0

FIELD

05/15/09 21:54 / ts05/15/09 21:54 / ts05/15/09 21:54 / ts05/15/09 21:54/ts05/15/09 21:54 / ts05/15/09 21:54 / ts06/01/09 15:33 / cp

05/15/09 21:54 / ts05/15/09 21:54 / ts05/15/09 21:54 / ts05/15/09 21:54 / ts

05/15/09 21:54 / is

06/01/09 12:17/jah

06/01/09 12:17 / jah

06/01/09 12:17/jah05/27/09 10:00 / plj05/27/09 10:00 / plj

05/27/09 10:00 / plj05/27/09 07:37 / dmf05/27/09 07:37 / dmf

05/27/09 07:37 / dmf

05/12/09 13:34 /**

U

U

6.51 s.u.

Report RL - Analyte reporting limit.I Definitions: QCL - Quality control limit.MDC - Minimum detectable concentrationSU - Not detected at minimum detectable concentration

copyý%MCL - Maximum contaminant level.ND - Not detected at the reporting limit.D - RL increased due to sample matrix interference.

Page 50: Miller Geotechnical Consultants, Inc. 3801 Automation Way

........ - 1 'an LICVl fnfy//wIdy (OCOUII 'r . DUXJZ06 I L, dSPe, VVr 6OUZTo//Free 888,235.0515, 307235,0515 Fax 307234 1639 casper@energy/abcom , wwwenergy/ab com

LABORATORY ANALYTICAL REPORT

D Client:Project:

Lab ID:Client Sample ID:

Western Nuclear

Split Rock Mill Site GWPP

C09050425-023WNI-1R

Report Date: 07/13/09Collection Date: 05/12/09 13:34

DateReceived: 05/13/09

Matrix: Aqueous

MCL/Analyses Result Units Qualifier RL QCL Method Analysis Date / By

MAJOR IONSChlorideFluorideNitrogen, Ammonia as N

Nitrogen, Nitrate+Nitrite as N

Sulfate

117

0.342.2

12.0

2200

PHYSICAL PROPERTIESpHSolids, Total Dissolved TDS @ 180 C

METALS - DISSOLVEDAluminumAntimonyArsenicBerylliumCadmiumLead

' ManganeseMolybdenumNickelSeleniumThalliumUranium

RADIONUCLIDES - DISSOLVEDRadium 226Radium 226 precision (+)Radium 226 MDCRadium 228Radium 228 precision (+)Radium 228 MDCThorium 230Thorium 230 precision (+)Thorium 230 MDC

FIELD PARAMETERSpH

_ Performed by Sampler

6.633770

NDNDND

ND

ND

ND

12.5ND

NDND

0.003

4.63

1.10.23

0.18

-0.003

0.71.1

0.010.1

0.3

mg/L

mg/Lmg/Lmg/L

mg/L

S.U.mg/L

mg/Lmg/Lmg/L

mg/Lmg/Lmg/L

mg/Lmg/L

mg/Lmg/L

mg/Lmg/L

pCi/LpCi/L

pCi/L

pCi/L

pCi/L

pCi/LpCi/LpCi/L

pCi/L

1

0.1D 0.2

0.2

D 30

A4500-CI BA4500-F CE350.1

E353.2

A4500-SO4 E

05/26/09 13:07 /jal05/18/09 16:08 / IjI05/15/09 15:54 / eli-b

05/15/09 15:28 / eli-b

05/19/09 13:15 /jal

0.01

10A4500-H B 05/15/09 13:30 / ddA2540 C 05/18/09 13:17 / rp

0.1

0.0030.01

0.004

0.0010.0050.050.1

0.05

0.005

0.001

0.001

E200.8

E200.8E200.8

E200.8

E200.8E200.8E200.8E200.8

E200.8E200.8

E200.8E200.8

E903.0

E903.0

E903.0

RA-05

RA-05RA-05

E907.0E907.0

E907.0

FIELD

05/18/09 15:14 / ts05/18/09 15:14 / ts05/18/09 15:14 I ts05/18/09 15:14 / ts

05/18/09 15:14 / ts05/18/09 15:14 / ts05/18/09 15:14 / ts05/18/09 15:14 / ts05/18/09 15:14 / ts

05/18/09 15:14 / ts

05/18/09 15:14 / ts

05/18/09 15:14 / ts

05/27/09 15:48 / jah05/27/09 15:48 / jah

05/27/09 15:48 / jah

05/22/09 14:07 / plj

05/22/09 14:07 / plj

05/22/09 14:07 / plj05/27/09 07:38 / dmf05/27/09 07:38 / dmf

05/27/09 07:38 / dmf

05/12/09 13:34 /

U

U

6.51 s.u.

* Report RL - Analyte reporting limit.Definitions: QCL - Quality control limit.

MDC - Minimum detectable concentrationU - Not detected at minimum detectable concentration

COPY

MCL - Maximum contaminant level.ND - Not detected at the reporting limit.D - RL increased due to sample matrix interference.

Page 51: Miller Geotechnical Consultants, Inc. 3801 Automation Way

T e , • 30.2350- - - Fa- -- 307..3 • -, • -.. om - IVIr U/'UVc,XffCJToll Free 888 2350515'- 3072350515 , Fax 307234.1639 cansper~energy~ab com -www energy/ab. corgg~r;wir~rgerj,~w

LABORATORY ANALYTICAL REPORT

(D Client:Project:Lab ID:

Western NuclearSplit Rock Mill Site GWPP

C09050425-002

Report Date: 07/13/09Collection Date: 05/12/09 11:55

DateReceived: 05/13/09Matrix: AqueousClient Sample ID: WNI-4R

MCLIAnalyses Result Units Qualifier RL QCL Method Analysis Date / By

MAJOR IONSChloride

Fluoride

Nitrogen, Ammonia as NNitrogen, Nitrate+Nitrite as N

Sulfate

1177.2271154

3140

mg/Lmg/Lmg/Lmg/L

mg/L

DD

D

PHYSICAL PROPERTIESpHSolids, Total Dissolved TDS @ 180 C

METALS - DISSOLVEDAluminumAntimonyArsenicBerylliumCadmiumLeadManganeseMolybdenumNickelSeleniumThalliumUranium

RADIONUCLIDES - DISSOLVEDRadium 226Radium 226 precision (+)Radium 226 MDCRadium 228Radium 228 precision (+)Radium 228 MDCThorium 230Thorium 230 precision (+)Thorium 230 MDC

6.31 s.u.4890 mg/L

1.6ND

ND

ND

0.022ND

93.7ND

0.510.034

0.001

0.321

0.220.14

0.19

0.7

0.6

0.9

-0.06

0.2

0.5

mg/Lmg/Lmg/L

mg/Lmg/Lmg/L

mg/Lmg/L

mg/Lmg/L

mg/L

mg/L

pCi/LpCi/LpCi/LpCi/LpCi/LpCi/LpCi/LpCi/LpCi/L

10.12

0.3

30

0.0110

0.10.0030.01

0.004

0.0010.005

0.05

0.10.050.005

0.001

0.001

A4500-F CE350.1E353.2

A4500-SO4

A4500-H B 05/15/09 10:49 / ddA2540 C 05/18/09 13:16 / rp

A4500-Ci B 05/26/09 12:47 / jal05/18/09 15:36 / IjI05/19/09 10:47 / eli-b05/15/09 14:57 / eli-b

E 05/19/09 12:02/jal

E200.8E200.8E200.8

E200.8

E200.8

E200.8E200.7

E200.8E200.8

E200.8

E200.8

E200.8

E903.0E903.0

E903.0

RA-05

RA-05RA-05

E907.0E907.0

E907.0

FIELD

05/15/09 22:42 /ts05/15/09 22:42 / ts05/15/09 22:42 / ts05/15/09 22:42 / ts

05/15/09 22:42 / ts05/15/09 22:42 / ts06/01/09 15:37 / cp05/15/09 22:42 / ts05/15/09 22:42 / ts05/15/09 22:42 / ts05/15/09 22:42 / ts05/15/09 22:42 / ts

06/01/09 12:17 / jah06/01/09 12:17 / jah06/01/09 12:17 / jah05/27/09 10:00 / plj05/27/09 10:00 / plj05/27/09 10:00 /plj05/27/09 07:37 / dmf05/27/09 07:37 / dmf05/27/09 07:37 / dmf

05/12/09 11:55 / *

Ul

U

FIELD PARAMETERSpH

_ Performed by Sampler6.09 s.u.

ReportDefinitions:?i

RL - Analyte reporting limit.

QCL - Quality control limit.

MDC - Minimum detectable concentration

U - Not detected at minimum detectable concentration

MCL - Maximum contaminant level.ND - Not detected at the reporting limit.D - RL increased due to sample matrix interference.

I COPNA

Page 52: Miller Geotechnical Consultants, Inc. 3801 Automation Way

-- ~. -. - -- , -- ~ L -~fIIIyI/Vy (Ok--uUIJ- 1-u. ouAx a.iof L- aspe/, vr trzuuzTo//Free 888235.05/5. 307235.0515 - Fax 307234.1639 - casper@energylab comrn wwwoenergylab.com

LABORATORY ANALYTICAL REPORT

Client:Project:Lab ID:Client Sample ID:

Western Nuclear

Split Rock Mill Site GWPP

C09050425-003WNI-5

Report Date: 07/13/09Collection Date: 05/12/09 11:30

DateReceived: 05/13/09

Matrix: Aqueous

MCL/Analyses Result Units Qualifier RL QCL Method Analysis Date / By

MAJOR IONSChloride

FluorideNitrogen, Ammonia as NNitrogen, Nitrate+Nitrite as N

Sulfate

102

NDND

58.5

1730

mg/L

mg/Lmg/Lmg/L

mg/L D

1

0.10.050.2

60

0.0110

A4500-Cl B

A4500-F C

E350.1

E353.2

A4500-SO4

05/26/09 12:49 /jal

05/18/09 15:42 / Ijl05/15109 14:05 / eli-b

05/15/09 16:01 / eli-b

E 05/19/09 12:03 /jal

PHYSICAL PROPERTIESpHSolids, Total Dissolved TDS @ 180 C

METALS - DISSOLVEDAluminumAntimonyArsenicBerylliumCadmiumLeadManganeseMolybdenumNickelSeleniumThalliumUranium

RADIONUCLIDES - DISSOLVEDRadium 226Radium 226 precision (+)Radium 226 MDCRadium 228Radium 228 precision (+)Radium 228 MDCThorium 230Thorium 230 precision (+)Thorium 230 MDC

FIELD PARAMETERSpH

**Performed by Sampler

6.91 s.u.

3660 mg/LA4500-H B 05115/09 10:51 / ddA2540 C 05/18/09 13:16 / rp

NDNDND

NDND

ND

0.42ND

ND

0.017ND

1.94

0.010.12

0.211.2

0.7

1.0

0.0050.20.4

mg/Lmg/Lmg/Lmg/Lmg/Lmg/L

mg/Lmg/Lmg/L

mg/Lmg/L

mg/L

pCi/L

pCi/LpCi/L

pCi/LpCi/L

pCi/LpCi/L

pCi/LpCi/L

0.10.0030.010.004

0.0010.005

0.050.1

0.050.0050.001

0.001

E200.8E200.8E200.8

E200.8E200.8

E200.8E200.8

E200.8

E200.8E200.8E200.8

E200.8

E903.0

E903.0

E903.0RA-05RA-05

RA-05

E907.0

E907.0E907.0

FIELD

05/15/09 22:48 / ts05115/09 22:48 / ts05/15/09 22:48 / ts05/15/09 22:48 / ts

05/15/09 22:48 / ts05/15/09 22:48 / ts

05/15/09 22:48 / ts

05/15/09 22:48 / ts

05/15/09 22:48 / ts05/15/09 22:48 /ts05/15/09 22:48 / ts

05/15/09 22:48 / ts

06/01/09 12:17 /jah

06/01/09 12:17 /jah

06101109 12:17 / jah05/27/09 10:00 / plj05/27/09 10:00 / p1j05/27/09 10:00 / plj

05/27/09 07:37 / dmf

05/27/09 07:37 / dmf05/27/09 07:37 / dmf

05/12/09 11:30/ **

U

U

6.85 s.u.

Report RL - Analyte reporting limit.

7-.Report RL - Analyte reporting limit.I Definitions: QCL - Quality control limit.

MDC - Minimum detectable concentrationU - Not detected at minimum detectable concentration

Copy

MCL - Maximum contaminant level.ND - Not detected at the reporting limit.D - RL increased due to sample matrix interference.

Page 53: Miller Geotechnical Consultants, Inc. 3801 Automation Way

-To//,r11- .5 . • afl I07 . lyllay (0ZVUI/ '/";L/. DUA...,Vo - dw.e/J b.j oVrVT U&A O Toll 1F-ree-8"88.2-3-50515 -307235.0515 ' Fax 307234 1639 -caspergenergylab com -www energylab con7,frf.7AYOM.q

LABORATORY ANALYTICAL REPORT

O Client: Western NuclearProject: Split Rock Mill Site GWPPLab ID: C09050425-024

Client Sample ID: WNI-5R

Report Date: 07/13/09Collection Date: 05/12/09 11:30

DateReceived: 05/13/09

Matrix: Aqueous

Analyses Result UnitsMCL/

Qualifier RL QCL Method Analysis Date / By

MAJOR IONSChlorideFluoride

Nitrogen, Ammonia as N

Nitrogen, Nitrate+Nitrite as N

Sulfate

102NDND

58.5

1870

mg/L

mg/Lmg/L

mg/Lmg/L D

PHYSICAL PROPERTIESpHSolids, Total Dissolved TDS @ 180 C

METALS - DISSOLVEDAluminumAntimonyArsenicBerylliumCadmiumLeadManganese

() MolybdenumNickelSeleniumThalliumUranium

RADIONUCLIDES - DISSOLVEDRadium 226Radium 226 precision (+)Radium 226 MDC

Radium 228Radium 228 precision (+)Radium 228 MDCThorium 230Thorium 230 precision (+)Thorium 230 MDC

FIELD PARAMETERSpH

.* Performed by Sampler

6.92 s.u.

3690 mg/L

NDND

ND

NDNDND

0.43

NDND

0.015ND

1.79

0.07

0.12

0.200.9

"0.7

1.2

-0.050.1

0.3

mg/L

mg/L

mg/L

mg/Lmg/L

mg/L

mg/L

mg/Lmg/L

mg/Lmg/Lmg/L

pCi/L

pCi/L

pCi/LpCi/LpCi/L

pCi/L

pCi/L

pCi/LpCi/L

1

0.10.050.2

30

0.01

10

0.1

0.0030.01

0.004

0.001

'0.0050.05

0.1

0.050.005

0.001

0.001

A4500-H B 05/15/09 13:32 1 ddA2540 C 05/18/09 13:18 / rp

A4500-CI B

A4500-F C

E350.1

E353.2

A4500-S04

05/26/09 13:08 / jal

05/18/09 16:12 / Ijl05/15/09 14:17 / eli-b

05/15/09 15:29 / eli-bE 05/19/09 13:17/jal

E200.8E200.8E200.8

E200,8

E200.8E200.8

E200.8E200.8

E200.8E200.8

E200.8

E200.8

E903.0

E903.0

E903.0

RA-05

RA-05

RA-05

E907.0E907.0

E907.0

FIELD

05/18109 15:21 /ts05/18/09 15:21 / ts05/18/09 15:21 / ts

05/18/09 15:21 / ts

05/18/09 15:21 / ts

05/18/09 15:21 / ts

05/18/09 15:21 /ts05/18/09 15:21 / ts05/18/09 15:21 / ts05/18/09 15:21 / ts05/18/09 15:21 / ts

05/18/09 15:21 / ts

05/27/09 15:48 /jah

05/27/09 15:48 / jah

05/27/09 15:48 / jah05/22/09 14:07 / plj

05/22/09 14:07 / plj

05/22/09 14:07 / plj

05/27/09 07:37 / dmf05/27/09 07:37 / dmf

05/27/09 07:37 / dmf

05/12/09 11:30 /

U

U

U

6.85 s.u.

* Report RL - Analyte reporting limit.Definitions: QCL - Quality control limit.

MDC - Minimum detectable concentration

SU - Not detected at minimum detectable concentration

colu

MCL - Maximum contaminant level.

ND - Not detected at the reporting limit.

D - RL increased due to sample matrix interference.

Page 54: Miller Geotechnical Consultants, Inc. 3801 Automation Way

ga Toll Free 888.235.0515. 307235.0515 -Fax 307234.16i9 •casper@energy/ab.com-- www.enlergylab.comr

LABORATORY ANALYTICAL REPORT

Client:Project:Lab ID:Client Sample ID:

Western NuclearSplit Rock Mill Site GWPP

C09050425-025WNI-5S

Report Date: 07/13/09

Collection Date: 05/12/09 11:30DateReceived: 05/13/09

Matrix: Aqueous

MCLIQualifier RL QCLAnalyses Result Units Method Analysis Date I By

MAJOR IONSChloride

FluorideNitrogen, Ammonia as N

Nitrogen, Nitrate+Nitrite as N

Sulfate

88

NDND

58.2

1920

mg/Lmg/Lmg/L

mg/Lmg/L D

PHYSICAL PROPERTIESpHSolids, Total Dissolved TDS @ 180 C

METALS - DISSOLVEDAluminumAntimonyArsenicBerylliumCadmiumLeadManganeseMolybdenumNickelSeleniumThalliumUranium

RADIONUCLIDES - DISSOLVEDRadium 226Radium 226 precision (+)Radium 226 MDCRadium 228Radium 228 precision (+)Radium 228 MDC ...Thorium 230 /Thorium 230 precision (+)Thorium 230 MDC

FIELD PARAMETERS-...pH

*** Performed by Sampler

6.97 s.u.

3690 mg/L

NDND

ND

ND

ND

ND0.43ND

ND0.016

ND

1.81

-0.20.09

0.210.7

0.8

1.30.04

0.3

0.6

mg/Lmg/L

mg/L

mg/L

mg/Lmg/L

mg/L

mg/Lmg/Lmg/L

mg/L

mg/L

pCi/LpCi/LpCi/LpCi/LpCi/LpCi/LpCi/LpCi/LpCi/L

10.1

0.05

0.2

30

0.0110

0.10.003

0.01

0.0040.001

0.005

0.05

0.1

0.050.005

0.0010.001

A4500-H B 05/15/09 13:33 /ddA2540 C 05/18/09 13:18 / rp

A4500-Cl B

A4500-F CE350.1

E353.2

A4500-SO4 E

05/26/09 13:09 / jal05/18/09 16:30 / IjI05/15/09 14:18 / eli-b

05/15/09 16:02 / eli-b

05/19/09 13:30 /jal

E200.8E200.8

E200.8

E200.8E200.8E200.8

E200.8

E200.8E200.8

E200.8E200.8

E200.8

E903.0

E903.0

E903.0RA-05RA-05

RA-05

E907.0E907.0

E907.0I

FIELD

05/18/09 15:27 / ts05/18/09 15:27 / ts

05/18/09 15:27 / ts

05/18109 15:27 /ts

05/18/09 15:27 / ts05/18/09 15:27 /ts05/18/09 15:27 / ts

05/18/09 15:27 / ts

05/18/09 15:27 / ts05/18/09 15:27 / ts

05/18/09 15:27 / ts05/18/09 15:27 / ts

05/27/09 15:48 / jah

05/27/09 15:48 /jah

05/27/09 15:48 /jah05/22/09 14:07 / plj05/22/09 14:07 I plj

05/22/09 14:07 / plj

05/27/09 07:37 / dmf

05/27/09 07:37,/ dmf

05/27/09 07:37 / dmf

05/12/09 11:30 /***

u

U

U

6.85 s.u.

Report RL - Analyte reporting limit.SO Definitions: QCL - Quality control limit.MDC - Minimum detectable concentration

SU- Not detected at minimum detectable concentration

cOpY

MCL - Maximum contaminant level.ND - Not detected at the reporting limit.D - RL increased due to sample matrix interference.

Page 55: Miller Geotechnical Consultants, Inc. 3801 Automation Way

To// Free 888.235 0515 •307235.,515 •Fax 307234, 1639 - [email protected] . www energylab.comVL4B-ORA MO-RIES

LABORATORY ANALYTICAL REPORT

Q Client: Western NuclearProject: Split Rock Mill Site GWPP

Lab ID: C09050425-004Client Sample ID: WNI-21

Report Date: 07/13/09Collection Date: 05/12/09 15:03

DateReceived: 05/13/09

Matrix: Aqueous

MCL/Analyses Result Units Qualifier RL QCL Method Analysis Date! By

MAJOR IONSChloride

FluorideNitrogen, Ammonia as NNitrogen, Nitrate+Nitrite as N

Sulfate

8

0.21.973.2

87

mg/L

mg/L

mg/Lmg/Lmg/L D

PHYSICAL PROPERTIESpHSolids, Total Dissolved TDS @ 180 C

METALS - DISSOLVEDAluminumAntimonyArsenicBerylliumCadmiumLeadManganese

0 MolybdenumNickelSeleniumThalliumUranium

RADIONUCLIDES - DISSOLVEDRadium 226Radium 226 precision (t)Radium 226 MDCRadium 228Radium 228 precision (+)Radium 228 MDCThorium 230Thorium 230 precision (+)Thorium 230 MDC

FIELD PARAMETERSpH

... Performed by Sampler

7.78 s.u.354 mg/L

NDNDND

ND

NDND

0.32ND

ND

NDND

0.071

-0.20.090.210.6

0.6

1.0

0.010.2

0.4

mg/Lmg/Lmg/L

mg/Lmg/Lmg/L

mg/Lmg/L

mg/L

mg/Lmg/Lmg/L

pCi/LpCi/LpCi/LpCi/LpCi/LpCi/LpCi/Lp Ci/LpCi/L

1

0.10.05

0.2

2

0.0110

0.10.003

0.01

0.004

0.0010.005

0.05

0.1

0.050.005

0.0010.001

A4500-H B 05/15/09 10:53 / ddA2540 C 05/18/09 13:16 / rp

A4500-Cl BA4500-F CE350.1

E353.2

A4500-SO4 E

05/26/09 12:51 /jal05/18/09 15:45 / IjI05/15/09 14:06 / eli-b

05/15109 15:23 / eli-b

05/19/09 12:05 1 jal

E200.8E200.8

E200.8

E200.8E200.8E200.8

E200:8

E200.8

E200.8

E200.8E200.8E200.8

E903.0

E903.0

E903.0RA-05

RA-05RA-05

E907.0E907.0

E907.0

FIELD

05/15/09 22:55 / ts05/15/09 22:55 / ts

05/15/09 22:55 / ts

05/15/09 22:55 / ts

05/15/09 22:55 /ts05/15/09 22:55 / ts

05/15/09 22:55 / ts

05/15/09 22:55 / ts

05/15/09 22:55 / ts05/15/09 22:55 / ts

05/15/09 22:55 / ts05/15/09 22:55 / ts

06/01/09 14:08 /jah

06/01/09 14:08 /jah

06/01/09 14:08 / jah05/27109 10:00 / plj

05/27/09 10:00 / plj05/27/09 10:00 / plj05/27/09 07:37 / dmf

05/27/09 07:37 / dmf

05/27/09 07:37 / dmf

05/12/09 15:03 /

U

U

U

7.14 s.u.

Report RL - Analyte reporting limit.Definitions: QCL - Quality control limit.

MDC - Minimum detectable concentration

U - Not detected at minimum detectable concentrationCOPY

MCL - Maximum contaminant level.ND - Not detected at the reporting limit.D - RL increased due to sample matrix interference.

Page 56: Miller Geotechnical Consultants, Inc. 3801 Automation Way

V -- -. y l " [-- . L ',WIrl' I 11ylYVay (U-.U(IIJ - FýL/. OUA 7-UCJO - Lda)U-tV, VV f O.-UU

Le = To//Free 8882350515- 3072350515 AFax 307234A1639 -casperTenergylab com wwwenergyab com

LABORATORY ANALYTICAL REPORT

Q Client:Project:Lab ID:Client Sample ID:

Western Nuclear

Split Rock Mill Site GWPP

C09050425-007WN I-39B

Report Date: 07/13/09

Collection Date: 05/12/09 10:20DateReceived: 05/13/09

Matrix: Aqueous

MCL/Analyses Result Units Qualifier RL QCL Method Analysis Date / By

MAJOR IONSSulfate 268 mg/L D 3 A4500-SO4 E 05/19/09 12:13 /jal

METALS - DISSOLVEDUranium

FIELD PARAMETERSpH

**Performed by Sampler

0.498 mg/L

7.29 s.u.

0.001 E200.8

FIELD

05/26/09 00:28 / Its

05/12/09 10:20 /

* Report RL - Analyte reporting limit.Definitions: QCL - Quality control limit.

D - RL increased due to sample matrix interference.

C

MCL - Maximum contaminant level.ND - Not detected at the reporting limit.

Page 57: Miller Geotechnical Consultants, Inc. 3801 Automation Way

Toll Free 888.2350515 - 3072350515 Fax 307,2341639 - casper~energylab.com - www energy/ab.comELABORA

LABORATORY ANALYTICAL REPORT

10Client: Western Nuclear

Project: Split Rock Mill Site GWPP

Lab ID: C09050425-008Client Sample ID: WNI-41 B

Report Date: 07/13/09Collection Date: 05/12/09 09:40

DateReceived: 05/13/09.Matrix: Aqueous

MCL/QCLAnalyses Result Units Qualifier RL Method Analysis Date I By

MAJOR IONSSulfate

METALS - DISSOLVEDUranium

FIELD PARAMETERSpH

_ Performed by Sampler

367 mg/L

0.009 mg/L

7.63 s.u.

D 3 A4500-SO4 E 05/19/09 12:18 /jal

0.001 E200.8

FIELD

05/26/09 00:32 / ts

05/12/09 09:40 / *

0

ReportDefinitions:

RL - Analyte 'reporting limit.

QCL - Quality control limit.

D - RL increased due to sample matrix interference.

MCL - Maximum contaminant level.ND - Not detected at the reporting limit.

I COY

Page 58: Miller Geotechnical Consultants, Inc. 3801 Automation Way

LABORA TORIES.

To//Free 888.235.0515 - 307235.0515 -Fax 307234.1639 - caspergenergylab.com - www.energylab.com

LABORATORY ANALYTICAL REPORT

O Client:Project:Lab ID:Client Sample ID:

Western Nuclear

Split Rock Mill Site GWPP

C09050425-009WN I-42A

Report Date: 07/13/09

Collection Date: 05/12/09 10:51

DateReceived: 05/13/09

Matrix: Aqueous

MCL/Analyses Result Units Qualifier RL QCL Method Analysis Date I By

MAJOR IONSSulfate

METALS - DISSOLVEDUranium

FIELD PARAMETERSpH

_ Performed by Sampler

2220 mg/L

1.05 mg/L

6.94 s.u.

D 60

0.001

A4500-S04 E 05/19/09 12:39 /jal

E200.8

FIELD

05/26/09 00:53 / ts

05/12/09 10:51 /***

0

_ Report RL - Analyte reporting limit.Definitions: QCL - Quality control limit.

D - RL increased due to sample matrix interference.

Icp CY

MCL - Maximum contaminant level.ND - Not detected at the reporting limit.

Page 59: Miller Geotechnical Consultants, Inc. 3801 Automation Way

AL ENERG YLABORA TORIES, INC. • 2393 Salt Creek Highway (82601) P.RC Box 3258 - Casper WY82602Toll Free 888.235. 0515 - 307235. 0515 • Fax 3072341 639 . casper'energylab, corn • www energylab.corn

FLABORATORIES.

LABORATORY ANALYTICAL REPORT

Client:Project:Lab ID:Client Sample ID:

Western Nuclear

Split Rock Mill Site GWPP

C09050425-009WN 1-42A

Revised Date:

Report Date:

Collection Date:

DateReceived:Matrix:

07/21/09

07/14/0905/12/09 10:51

05/13/09

Aqueous

MCL/Analyses Result Units Qualifiers RL QCL Method Analysis Date / By

MAJOR IONSSulfate 2220 mg/L D 60 A4500-SO4 E 05119109 12:39 fial

METALS - DISSOLVEDSeleniumUranium

FIELD PARAMETERSpH

_ Performed by Sampler

0.030 mg/L1.05 mg/L

6.94 s.u.

0.0050.001

E200.8E200.8

FIELD

07/17/09 15:58 / sml05/26/09 00:53 / ts

05/12/09,10:51 /**

0

ReportDefinitions:

RL - Analyte reporting limit.

QCL - Quality control limit.

D - RL increased due to sample matrix interference.

MCL - Maximum contaminant level.

ND - Not detected at the reporting limit.

Page 60: Miller Geotechnical Consultants, Inc. 3801 Automation Way

LToll Free 88&8235.0515 0 30723505.1Fx0234 1639 asperenergy/ab.om wwwenergy/ab.omIFýLABORA

LABORATORY ANALYTICAL REPORT

I (-) Client:Project:Lab ID:

Western Nuclear

Split Rock Mill Site GWPP

C09050425-022

Report Date: 07/13/09Collection Date: 05/12/09 09:00

DateReceived: 05/13/09Matrix: AqueousClient Sample ID: Field Blank

MCLIAnalyses Result Units Qualifier RL QCL Method Analysis Date / By

MAJOR IONSChlorideFluorideNitrogen, Ammonia as NNitrogen, Nitrate+Nitrite as NSulfate

ND

NDND

ND

2

mg/Lmg/Lmg/L

mg/L

mg/L

1

0.10.050.2

1

0.0110

A4500-CI B 05/26/09 13:05 / jal

A4500-F C

E350.1E353.2

A4500-SO4 E

05/18/09 16:05 / Ijl05/15/09 14:09 / eli-b

05/15/09 15:26 / eli-b05/19/09 13:14/jal

PHYSICAL PROPERTIESpHSolids, Total Dissolved TDS @ 180 C

METALS - DISSOLVEDAluminumAntimonyArsenicBerylliumCadmiumLeadO ManganeseMolybdenumNickelSeleniumThalliumUranium

RADIONUCLIDES - DISSOLVEDRadium 226Radium 226 precision (+)Radium 226 MDCRadium 228Radium 228 precision (+)Radium 228 MDCThorium 230Thorium 230 precision (+)Thorium 230 MDC

5.41 s.u.ND mg/L

A4500-H B 05/15/09 13:28 / ddA2540 C 05/18/09 13:17 / rp

NDND

ND

ND

ND

NDND

ND

NDND

ND

ND

0.006

0.12

0.22-0.3

0.8

1.3

-0.040.1

0.3

mg/Lmg/Lmg/L

mg/Lmg/L

mg/Lmg/L

mg/L

mg/Lmg/Lmg/Lmg/L

pCi/LpCi/LpCi/LpCi/LpCi/L

pCi/LpCi/LpCi/LpCi/L

0.10.0030.01

0.004

0.001

0.0050.05

0.1

0.050.005

0.001

0.001

E200.8

E200.8E200.8E200.8

E200.8E200.8

E200.8

E200.8E200.8E200.8

E200.8

E200.8

E903.0E903.0

E903.0RA-05

RA-05

RA-05

E907.0E907.0E907.0

FIELD

05/18/09 15:07 / ts05/18/09 15:07 / ts05/18/09 15:07 / ts

05/18/09 15:07 / ts

05/18/09 15:07 / ts05/18/09 15:07 / ts05/18/09 15:07 / ts

05/18/09 15:07/ts05/18/09 15:07 / ts05/18/09 15:07 / ts05/18/09 15:07 / ts05/18/09 15:07 / ts

05/27/09 14:10 / jah05/27/09 14:10 / jah

05/27/09 14:10 /jah05/22/09 14:07 / plj

05/22/09 14:07 / plj

05/22/09 14:07 / plj05/27/09 07:38 / dmf

05/27/09 07:38 / dmf05/27/09 07:38 / dmf

05/12/09 09:00 / *

U

U

U

FIELD PARAMETERSpH

_ Performed by Sampler6.39 s.u.

Report RL - Analyte reporting limit.Definitions: QCL - Quality control limit.

MDC - Minimum detectable concentration

COPY

MCL - Maximum contaminant level.ND - Not detected at the reporting limit.U - Not detected at minimum detectable concentration

Page 61: Miller Geotechnical Consultants, Inc. 3801 Automation Way

SURFACE WATER

Page 62: Miller Geotechnical Consultants, Inc. 3801 Automation Way

Jeffrey City SW-1

pH (Field) (std. Units)

10

9

8

7

6

5

4

3

2

1

0~

nB

TDS (mg/L)

400

350

300

250

200

150 -

100

50

0'

Open symbols indicate value below detection limit

Page 63: Miller Geotechnical Consultants, Inc. 3801 Automation Way

Jeffrey City SW-I

Sulfate (mg/L)

80

70

60

50

40

30

20

10

0

Uranium (mg/L)

0.01

0.008 -Detects

*Non-detects

0.006

0.004

0.002

0

n 8n

Open symbols indicate value below detection limit

Page 64: Miller Geotechnical Consultants, Inc. 3801 Automation Way

Jeffrey City SW-2

pH (Field) (std. Units)

10

9

8

7

6

5

4

3

2

1

0•

Open symbols indicate value below detection limit

Page 65: Miller Geotechnical Consultants, Inc. 3801 Automation Way

Jeffrey City SW-2

Uranium (mg/L)0.008

0.007 '0 Detects

0.006 - Non-detects

0.005

0.004.

0.003

0.002

0.001

0

n n nnI 1 56

Open symbols indicate value below detection limit

Page 66: Miller Geotechnical Consultants, Inc. 3801 Automation Way

Jeffrey City SW-3

pH (Field) (std. Units)

10

9

8

7

6

5

4

3

2

1

0'o 6 8'8i i in

Open symbols indicate value below detection limit

Page 67: Miller Geotechnical Consultants, Inc. 3801 Automation Way

Jeffrey City SW-3

Sulfate (mg/L)60 -

50 -

40 -

30 -

20 -

10 -

0

Uranium (mg/L)0.01

0.008

0.006

0.004

0.002

0

n8I 1§

Open symbols indicate value below detection limit

Page 68: Miller Geotechnical Consultants, Inc. 3801 Automation Way

Jeffrey City SW-4

pH (Field) (std. Units)

10

9

8

7

6

5

4

3

2

1

0

6 B

Open symbols indicate value below detection limit

Page 69: Miller Geotechnical Consultants, Inc. 3801 Automation Way

Jeffrey City SW-4

Sulfate (mg/L)60

50

40

30 -

20

10

0

nB

Uranium (mg/L)0.01

0.008

0.006

0.004

0.002

0

n n nI I I

Open symbols indicate value below detection limit

Page 70: Miller Geotechnical Consultants, Inc. 3801 Automation Way

Jeffrey City SW-5

pH (Field) (std. Units)

10

98

7

6

5

4

3

2

1

0~

TDS (mg/L)

300

250

200

150

100

50

0

Open symbols indicate value below detection limit

Page 71: Miller Geotechnical Consultants, Inc. 3801 Automation Way

Jeffrey City SW-5

Sulfate (mg/L)60

50

40

30 -

20

10

0

n n n

Uranium (mg/L)0.008

0.007

0.006

0.005

0.004

0.003 -

0.002

0.001

0

Open symbols indicate value below detection limit

Page 72: Miller Geotechnical Consultants, Inc. 3801 Automation Way

rIllczv T r L/4lUIA I UIf::, ING." 2y3y6,"it Creek Highway (82601) • PO. Box 3258 - Casper, WY82602Toll Free 888 235.0515 ' 307235.0515 - Fax 307234. 1639 - [email protected] . www energylab. corn

F-LAB-ORA

LABORATORY ANALYTICAL REPORT

Client:Project:Lab ID:Client Sample ID:

Western Nuclear

Split Rock Mill Site GWPPC09050425-011SWR-Up-Gradient

Report Date: 07/13/09

Collection Date: 05/12/09 10:23

DateReceived: 05/13/09

Matrix: Aqueous

MCL/Analyses Result Units Qualifier RL QCL Method Analysis Date / By

MAJOR IONSSulfate 19 mg/L A4500-SO4 E 05/19/09 12:43 /jal

METALS - DISSOLVEDUranium

FIELD PARAMETERSpH

... Performed by Sampler

0.001 mg/L

6.88 s.u.

0.001 E200.8

FIELD

05/26/09 01:01 / ts

05/12/09 10:23 / **

Report RL - Analyte reporting limit.Definitions: QCL - Quality control limit.

MCL - Maximum contaminant level.ND - Not detected at the reporting limit.

I CL VP

Page 73: Miller Geotechnical Consultants, Inc. 3801 Automation Way

"BORA 1E.S_

&Iv~tfciYLAU~HLA AOUHITR5, INC. A L2393SalACreekH REwPyR(82601) -PO. Box 3258 Casper, WY82602Toll Froee888.2350515 , 307,235.0515 -Fax 307234.1639 - casper@~energy/ab~com. wwwerergylab.corn

LABORATORY ANALYTICAL REPORT

Client:Project:Lab ID:Client Sample ID:

Western NuclearSplit Rock Mill Site GWPP

C09050425-012

SWR-A

Report Date: 07/13/09

Collection Date: 05/12/09 09:11

DateReceived: 05/13/09Matrix: Aqueous

MCL/

Analyses Result Units Qualifier RL QCL Method Analysis Date / By

MAJOR IONSSulfate

METALS - DISSOLVEDUranium

FIELD PARAMETERSpH

_ Performed by Sampler

20 mg/L

0.001 mg/L

6.96 s.u.

1

0.001

A4500-SO4 E 05/19/09 12:45/jal

E200.8

FIELD

05/26/09 01:05 Its

05/12/09 09:11 /***

Report RL - Analyte reporting limit.Definitions: QCL - Quality control limit.

MCL - Maximum contaminant level.ND - Not detected at the reporting limit.

I CO0P Y.

Page 74: Miller Geotechnical Consultants, Inc. 3801 Automation Way

N•EHrGYLABORA TORIES, INC. 2393 Salt Creek Highway (82601) RO. Box 3258 • Casper, WY82602Toll Free 888.235.0515 - 307235.0515 - Fax 307234.1639 • caspergenergvlab.com . www energylab.com

F-LAB

LABORATORY ANALYTICAL REPORT

O Client:Project:Lab ID:Client Sample ID:

Western Nuclear

Split Rock Mill Site GWPP

C09050425-013

SWR-B

Report Date: 07/13/09

Collection Date: 05/12/09 09:28DateReceived: 05/13/09

Matrix: Aqueous

MCL/Analyses Result Units Qualifier RL QCL Method Analysis Date / By

MAJOR IONSSulfate

METALS - DISSOLVEDUranium

FIELD PARAMETERSpH

_ Performed by Sampler

20 mg/L

0.002 mg/L

7.02 s.u.

1 A4500-SO4 E 05/19/09 12:47 /jal

0.001 E200.8

FIELD

05/26/09 01:10 / ts

05/12/09 09:28 / *

0

ReportDefinitions:RL - Analyte reporting limit.

QCL - Quality control limit.

MCL - Maximum contaminant level.ND - Not detected at the reporting limit.

I COPY

Page 75: Miller Geotechnical Consultants, Inc. 3801 Automation Way

A-- V;r7r LAD L'yCIAI / INyU -. YJ 6bit (UreeK Hig/iway (82601) . P0. Box 3258 - Caspe, WY 82602Toll Free 888.235. 0515 307235. 0515 • Fax 307234 1639 • [email protected] - www energylab.com

"BoRAToRIE-s

LABORATORY ANALYTICAL REPORT

O Client:Project:Lab ID:Client Sample ID:

Western Nuclear

Split Rock Mill Site GWPP

C09050425-014SWR-C

Report Date: 07/13/09

Collection Date: 05/12/09 10:09

DateReceived: 05/13/09

Matrix: Aqueous

MCL/Analyses Result Units Qualifier RL QCL Method Analysis Date / By

MAJOR IONSSulfate

METALS - DISSOLVEDUranium

FIELD PARAMETERSpH

_ Performed by Sampler

20 mg/L

0.002 mg/L

7.39 s.u.

I A4500-SO4 E 05/19/09 12:49 / jal

0.001 E200.8

FIELD

05/26/09 01:14 / ts

05/12/09 10:09 / *

0

Report RL - Analyte reporting, limit.Definitions: QCL - Quality control limit.0

MCL - Maximum contaminant level.ND - Not detected at the reporting limit.

I

Page 76: Miller Geotechnical Consultants, Inc. 3801 Automation Way

ýIVAýryur L.4AI.IA-1 I .Lil-ap, IIVN G Z'j !alr (,TBeeK i-I/g/way (•1• -)-. P. OX 3258 aGasper, WY 82602TollFree 888.235.0515 • 307235.0515 • Fax 307234.1639 • casper@energylab. corn wwwenergylab.com

LABORATORY ANALYTICAL REPORT

O Client:Project:Lab ID:Client Sample ID:

Western NuclearSplit Rock Mill Site GWPP

C09050425-015

SWR-Down-Gradient

Report Date: 07/13/09Collection Date: 05/12/09 11:10

DateReceived: 05/13/09

Matrix: Aqueous

MCL/Analyses Result Units Qualifier RL QCL Method Analysis Date I By

MAJOR IONSSulfate

METALS - DISSOLVEDUranium

FIELD PARAMETERSpH

_ Performed by Sampler

21 mg/L

0.002 mg/L

6.96 s.u.

1 A4500-SO4 E 05/19/09 12:51 /jal

0.001 E200.8

FIELD

05/26/09 01:18 / ts

05/12/09 11:10 / **

Report RL - Analyte reporting limit.Definitions: QCL - Quality control limit.

MCL - Maximum contaminant level.ND - Not detected at the reporting limit.

copy