microbac laboratories, inc.date timtech accrede . all samples received in proper condition and...

$: Microbac Laboratories, Inc.DATE TIMTECH ACCREDE . All samples received in proper condition and results conform to ISO 17025 standards unless olhen\'i-,e noted Accred. 3£ This symbol$
EPA Region 5 Records Ctr.

Microbac Laboratories, Inc.ERIE DIVISION

1962 WAGER ROADERIE, PA 16509

(814)825-8533 FAX (814)825-9254

MARK MATROZZA , MANAGING DIRECTOR

http://www.microbac.com E-Mail: [email protected]

276921

STATE CERT ID.25-067. 10I21

C-PA-05

CHEMISTRY • MICROBIOLOGY • FOOD SAFETY CONSUMER PRODUCTSWATER AIR • WASTES FOOD • PHARMACEUTICALS NUTRACEUTICALS

PRELIMINARY CERTIFICATE OF ANALYSIS

D E M A X I M I S , INC.MS. VALERIA A. RULE, P.E.450 MONTBROOK LANE

KNOXVILLE,TN 37919

Date ReportedDale ReceivedOrder NumberInvoice No.Custtf

9/5/20070709-01502

004229

Permit No.Cust P.O. PROJECT 3075F

SUBJECT: SOLID SAMPLES FOR ANALYSIS

TEST METHOD RESULT

001 FBEXB14

Date Sampled: 9/4/2007PCBs ON SOLID

AROCHLOR-1016, DRY WT.






AROCHLOR-1260, DRYWT.

DECACHLOROBIPHENYL

TETRACHLORO-M-XYLENE

SOLIDS, TOTAL

E8082

E8082

E8082

E8082

E8082

E8082

E8082

E8082

E8082

EB082

A2540G

<57.2

<57.2

<57.2

<57.2

150

<57.2

<57.2

57.4

UNITS

ANALYSIS

DATE TIME

Time Sampled:

MG/KG DRYWT

MG/KG DRYWT

MG/KG DRY WT

MG/KG DRYWT

MG/KG DRYWT

MG/KG DRYWT

MG/KG DRYWT

%

%

%

9/11/2007

9/11/2007

9/11/2007

9/11/2007

9/11/2007

9/11/2007

9/11/2007

9/5/2007

TECH ACCRED.

12:57 pm

11:12

11:12

11:12

11:12

11:12

11:12

11:12

11:12

OST

OST

OST

OST

OST

OST

OST

OST

FBEXB15

PCBs ON SOLID








DECACHLOROBIPHENYL


SOLIDS, TOTAL

Date Sampled:E80B2

E8082

E8082

E8082

E8082

E8082

E8082

E8082

E8082

E8082

A2540G

9/4/2007 Time Sampled: 1:01 pm

<5.73 MG/KG

<5.73 MG/KG

<5.73 MG/KG

<5.73 MG/KG

9.39 MG/KG

<5.73 MG/KG

<5.73 MG/KG

87.2 %

DRYWT

DRYWT

DRYWT

DRY WT

DRYWT

DRYWT

DRYWT

9/11/2007

9/11/20079/11/2007

9/11/2007

9/11/2007

9/11/2007

9/11/2007

9/5/2007

11:12

11:14

11:14

11:14

11:14

11:14

11:14

11:14

OST

OST

OST

OST

OST

OST

OST

OST

003 FBEXB16

PCBs ON SOLID


Date Sampled:EB082

E8082


<563 MG/KG DRYWT 9/10/2007 11:14 OST

The data and information on This, and other accompanying documents, represent only the sample(s) analyzed and is rendered upon condition

that it is not to be reproduced wholly or in part for advertising or other purposes without approval from the laboratory.

USDA-EPA-NIOSH Testing Food Sanitation Consulting Chemical and Microbiological Analyses and Research

NELAP accredited by PA, NY. Visit our website to view our current NELAC accreditations for

vanous drinking water, wastewater and solid & chemical materials,air & emissions anatytesAC11



(814)X25-X533 KAX (814)825-9254

MARK MATROZZA . M A N A G I N G DIRECTOR

http://\v\v\v.microbac.com K-Mail : cric(fl'microbac.ci)m

Pai>e 7 of 7

STATE CERT ID.25-067. 10121

C-PA-U5

CHEMISTRY • MICROBIOLOGY • FOOD SAFETY • CONSUMER PRODUCTSWATER AIR • WASTES FOOD PHARMACEUTICALS NUTRACEUTICALS


DE MAXIMIS , INC.MS. VALERIA A. RULE. P.E.450 MONTBROOK LANE

KNOXVILLE.TN 37919

Date ReportedDate ReceivedOrder NumberInvoice No.Cust #

8/31/20070709-01402

004229

Permit NoCust P.O. PROJECT 3075F

SUBJECT: SOLID SAMPLES RECEIVED 8/31/07

TEST METHOD RESULT UNITSANALYSIS

DATE TIME TECH ACCRED.

All samples received in proper condition and results conform to ISO 17025 standards unless olhen\'i-,e noted

Accred.

3£ This symbol at the end of the lest line means the lesl analysis met the requirements o t 'NHLAC (PA ID 25-00067)

*J» This symbol at the end of ' the test line means the test analysis met the requirements of A1HA (ID 100386)

^ This symbol at the end of the test l ine means the lesl analysis met the requi rements of" NY EiLAP (NY ID 1 0 1 2 1 )

ABBREVIATIONS:

TMTC = Too Numerous To CountUG/L = Micrograms per Liter (PPB)UG/KG = Micrograms per Kilogram (PPB)MG/L = Milligrams per Liter (PPM)1000 UG = 1 MGPostive = Bactena or target analyte detected

MG/KG = Milligram per Kilogram (PPM)CPU = Colony Forming UnitND = Not delected at or below the reporting limitTIC = Tentatively Identified Compound"<" = less than (also see "ND")Negative = Bactena or target analyte not detected

For any feedback concerning our services, please contact Mark Matrozza. Managing Director at mmatrozza(«'microbac.com or Trevor Boycc.President at prcsident'r; microbac.com

The data and information on this, and other accompanying documents, represent on v the sample(s) analyzed and is rendered upon condition

that it is not to be reproduced wholly or in part for advertising or other purposes without approval from the labo'ato'v

USDA EPA-NIOSH Testing Food Sanitation Consulting Chemical a-<] Microbiological Analyses and Research

NELAP accredited by PA, NV Visit our website to view our .un-ent NELAC accreditations forvarious drinking water, wastewater and wl'd & chemical rr j:enals,air & emissions analytes

MEMBER

Acr



(814)825-8533 FAX (814)825-9254



P;igc 6 of?

STATE CERT ID.25-067, 10121C-PA-05

CHEMISTRY • MICROBIOLOGY • FOOD SAFETY CONSUMER PRODUCTSWATER AIR • WASTES FOOD • PHARMACEUTICALS NUTRACEUTICALS


DEMAX1MIS, INC.MS. VALERIA A. RULE, P.E.450 MONTBROOK LANE

KNOXVILLE.TN 37919

Date ReportedDate ReceivedOrder NumberInvoice No.Cusl#

8/31/20070709-01402

004229





on FBEX7402

continuedSOUDS, TOTAL

Date Sampled: 8/30/2007

A2540G 81.8 %

Time Sampled: 11:15 am

9/7/2007 10:56 OST

012 FBEX7501


AROCHLOR-1016,

AROCHLOR-1221,

AROCHLOR-1232,

AROCHLOR-1242,

"ROCHLOR-1248,

JCHLOR-1254,

AROCHLOR-1260,

DRYWT.

DRY WT.

DRYWT.

DRY WT.

DRYWT.

DRYWT.

DRYWT.

DECACHLOROBIPHENYL

TETRACHLORO-M

SOLIDS, TOTAL

-XYLENE

E8082

E8082

E8082

E8082

E8082

E80B2

E8082

E8082

E8082

E8082

A2540G

<0.060

<0.060

<0.060

<0.060

0.050

<0.060

<0.060

84.0

MG/KG

MG/KG

MG/KG

MG/KG

MG/KG

MG/KG

MG/KG

%

%

%

Time Sampled:

DRYWT

DRYWT

DRYWT

DRYWT

DRYWT

DRYWT

DRYWT

9/7/2007

9/7/2007

9/7/2007

9/7/2007

9/7/2007

9/7/2007

9/7/2007

9/7/2007

1:45 pm

10:56

10:56

10:56

10:56

10:56

10:56

10:56

10:56

OST

OST

OST

OST

OST

OST

OST

OST

The data and information on this, and other accompanying documents, represent only the samples) analyzed and is rendered upon condition

that It is not to be reproduced whotty or In part for advertising or other purposes without approval from the laboratory.



various drinking water, wastewater and solid & chemical materiats,air & emissions anatytes Acr

Microbac Laboratories, Inc.ERIE DIVISION1962 WAGER ROADERIE, PA 165(19

(814)825-8533 FAX (814)825-9254

MARK MATROZZA . MANAGING DIRECTOR

http://\vw\v.microhac.com E-Mail: [email protected]

Page 5 of 7


CHEMISTRY • MICROBIOLOGY • FOOD SAFETY CONSUMER PRODUCTSWATER AIR • WASTES • FOOD • PHARMACEUTICALS • NUTRACEUTICALS


DEMAXIMIS, INC.MS. VALERIA A. RULE, P.E.450 MONTBROOK LANEK.NOXVILLE.TN 37919

Date ReportedDate ReceivedOrder NumberInvoice No.Cust#

8/31/20070709-01402

004229





009 FBEX74SWNcontinued


DECACHLOROBIPHENYL

TETRACHLOROM-XYLENE

SOUDS, TOTAL

E8082

E8062

E8082

A2540G

<0.060 MG/KG DRYWT 9/7/2007 10:56 OST

%

83.2 % 9/7/2007 10:56 OST

010 FBEX7401

PCBs ON SOLID



AROCHLOR 1232, DRY WT.





DECACHLOROBIPHENYL

TETRACHLOROM-XYLENE

SOUDS, TOTAL

Date Sampled:E8082

E8082

E8082

E8082

E8082

E8082

E8082

E8082

E8082

E8082

A2540G

8/30/2007 Time Sampled: 11:12 am

<33.7 MG/KG

<33.7 MG/KG

<33.7 MG/KG

<33.7 MG/KG

56.1 MG/KG

<33.7 MG/KG

<33.7 MG/KG

74.2

DRYWT

DRYWT

DRYWT

DRYWT

DRYWT

DRYWT

DRYWT

9/7/2007

9/7/2007

9/7/2007

9/7/2007

9/7/2007

9/7/2007

9/7/2007

9/7/2007

10:56

10:56

10:56

10:56

10:56

10:56

10:56

10:56

OST

OST

OST

OST

OST

OST

OST

OST

on FBEX7402

PCBs ON SOUD








DECACHLOROBIPHENYL


Date Sampled:E8082

E8082

E8082

E8082

E8082

E8082

E8082

E8082

E8082

E8082


<O.CC1 MG/KG DRYWT 9/7/2007 10:56 OST

<0.;C1 MG/KG DRYWT 9/7/2007 10:56 OST

<0.061 MG/KG DRYWT 9/7/2007 10:56 OST

<0.061 MG/KG DRYWT 9/7/2007 10:56 OST

0.044 MG/KG DRYWT 9/7/2007 10:56 OST

<0.061 MG/KG DRYWT 9/7/2007 10:56 OST

<0.061 MG/KG DRYWT 9/7/2007 10:56 OST

The daw and informaton on this, and other accompanying documents, represent only the sample(s) analyzed and is rendered upon condition

that it is not to be reproduced wholly or in part for advertising or other purposes without approval from the laboratory.

USDA EPA NIOSH Testjrtg Food Sanitation Consulting Chernirdl and Micrrjtuotogical Analyses and Research

NELAP accredited by PA, NY Visit our website to view ou< current NELAC accreditations for

vanous drinking water, wastewater and solid a chemical Tiatenals.air a emissions analytes Acr

Microbac Laboratories, Inc.ERIE DIVISION1962 WAOF.R ROAD STATE CERT ID.

ERIE, PA 16509 25-067, 10121

(814)825-8533 FAX (814)825-9254 C-PA-05



CHEMISTRY • MICROBIOLOGY • FOOD SAFETY CONSUMER PRODUCTSWATER • AIR • WASTES FOOD PHARMACEUTICALS NUTRACEUTICALS


DEMAXIMIS, INC.MS. VALERIA A. RULE, P.E.450 MONTBROOK. LANE

KNOXV1LLE.TN 37919


SUBJECT: SOLID SAMPLES RECEIVED 8/31/07-

TEST METHOD

07 FBEX7302

Date Sampled: 8/30/2007continued

AROCHLOR-1242, DRY WT. E8082



AROCHLOR- 1260, DRYWT. E8082

DECACHLOROBIPHENYL E8082

TETRACHLORO-M-XYLENE E8082

SOUDS, TOTAL A2540G

38 FBEX7303

Date Sampled: 8/30/2007-SON SOLID E8082

AROCHLOR-1016, DRYWT. E8082





AROCHLOR- 1 254, DRY WT. E8082


DECACHLOROBIPHENYL E8082

TETRACHLORO-M-XYLENE E8082

SOLIDS, TOTAL A2540G

19 FBEX74SWN

PCBs ON SOLID E8082




o.ROCHLOR-1242, DRY WT. E8082

".ROCHLOR- 1248, DRYWT. E8082

Date ReportedDate Received 8/31/2007Order Number 0709-01402Invoice No.Cust # 004229

ANALYSISRESULT UNITS DATE TIME TECH ACCRED.


<0.056 MG/KG DRYWT 9/7/2007 10:56 OST

0.043 MG/KG DRYWT 9/7/2007 10:56 OST

<0.056 MG/KG DRYWT 9/7/2007 10:56 OST

<0.056 MG/KG DRYWT 9/7/2007 10:56 OST

%

%

89.2 % 9/7/2007 10:56 OST

Time Sampled: 1 1 :00 am

<0.057 MG/KG DRYWT 9/7/2007 10:56 OST

< 0.057 MG/KG DRYWT 9/7/2007 10:56 OST

<0.057 MG/KG DRYWT 9/7/2007 10:56 OST

<0.057 MG/KG DRYWT 9/7/2007 10:56 OST

0.023 MG/KG DRYWT 9/7/2007 10:56 OST

<0.057 MG/KG DRYWT 9/7/2007 10:56 OST

<0.057 MG/KG DRYWT 9/7/2007 10:56 OST

%

%

88.3 % 9/7/2007 10:56 OST

<0.060 MG/KG DRYWT 9/7/2007 10:56 OST

<0.060 MG/KG DRYWT 9/7/2007 10:56 OST

<0.060 MG/KG DRYWT 9/7/2007 10:56 OST

<0.060 MG/KG DRYWT 9/7/2007 10:56 OST

0.112 MG/KG DRYWT 9/7/2007 10:56 OST

AROCHLOR-1254, DRYWT. E8082 <0.060 MG/KG DRY WT 9/7/2007 10:56 OST

'' ffiS^kfek?-' thal 'r 'S "** to "* rePnx*Jced whoNV or In part for advertising or other purposes without approval from the laboratory."t/y -BjE^ r- USDA-EPA-NIOSH Testing Food Sanita km Consulting Chemical and Microbiotogol Analyse and Research • • •• ^ ^ H

• •• IV deH = NELAP accredited by PA, NY. Visit our website to view our current NELAC accreditauons for Pi L H I Bvarious drinking water, wastcwater and solid & chemical materials.air & emission analytes


1962 WAGER ROAD

ERIE. PA 16509

(814)825-8533 FAX (814)825-9254


http://\v\v\v.microbac.com E-Mail: [email protected]

Page 3 of?

STATE CERT ID.

25-067. 10121

C-PA-05

CHEMISTRY • MICROBIOLOGY • FOOD SAFETY CONSUMER PRODUCTSWATER • AIR • WASTES • FOOD PHARMACEUTICALS • NUTRACEUTICALS


D E M A X I M I S , INC.

MS. VALERIA A. RULE, P.E.

450 MONTBROOK LANE

KNOXVILLE.TN 37919

Date Reported

Date Received

Order NumberInvoice No.Custtf

8/31/2007

0709-01402

004229

Permit No.

Cust P.O. PROJECT 3075F




005 FBEX73SWW

continuedAROCHLOR-1232, DRY WT.





DECACHLOROBIPHENYL


SOLIDS, TOTAL

Date Sampled:

ES082E8082E8082E8082E8082

E8082E8082

A2510G


<0.560 MG/KG DRY WT 9/7/2007 10:56 OST

<0.560 MG/KG DRYWT 9/7/2007 10:56 OST

1.18 MG/KG DRYWT 9/7/2007 10:56 OST

<0.560 MG/KG DRYWT 9/7/2007 10:56 OST

<0.560 MG/KG DRYWT 9/7/2007 10:56 OST

89.1 % 9/7/2007 10:56 OST

006 FBEX7301

PCBs ON SOLID








DECACHLOROBIPHENYL


SOLIDS, TOTAL

Date Sampled:

E8062E8082E8082E8082

E8082E8082

E8082E8082

E8082E8082A2540G


<234 MG/KG

<234 MG/KG

<234 MG/KG

<234 MG/KG

-599 MG/KG

<234 MG/KG

<234 MG/KG

DRYWT

DRYWT

DRYWT

DRYWT

DRYWT

DRYWT

DRYWT

9/7/2007

9/7/2007

9/7/2007

9/7/2007

9/7/2007

9/7/2007

9/7/2007

85.6 % 9/7/2007

10:56

10:56

10:56

10:56

10:56

10:56

10:56

10:56

OST

OST

OST

OST

OST

OST

OST

OST

007 FBEX7302

PCBs ON SOLID




Date Sampled:E8082

E8082

E8082E8082


<O.O56 MG/KG DRYWT 9/7/2007 10:56 OST

<0.056 MG/KG DRYWT 9/7/2007 10:56 OST-

<0.056 MG/KG DRYWT 9/7/2007 10:56 OST

TTie data and information on this, and other accompanying documents, represent oniy the sample(s) analyzed and is rendered upon condition

that rt is not to be reproduced wholly or >n part lor advertising or other :njrposes without approval from Che ^boralory

USDA-EPA-NIOSH Testing Food Sanitation Consulting Chemical d'id Microbiological Analyses and Research

-NtLAP accredited by PA, NY. Visit our website to view ou- runent NELAC accreditations forvarious drinking water, wastewater and solid ft chemical ^atenals.air a emissions anatytes

MEMBER

ACI


1962 WAGER ROADERIE. PA 16509

(814)825-8533 FAX (814)825-9254



Pace 2 ol"

STATE CERT ID.25-067. 10121C-PA-05

CHEMISTRY • MICROBIOLOGY • FOOD SAFETY CONSUMER PRODUCTSWATER • AIR • WASTES • FOOD PHARMACEUTICALS • NUTRACEUT1CALS


DEMAXIMIS, INC.MS. VALERIA A. RULE, P.E.450 MONTBROOK LANEKNOXVILLE,TN 37919


8/31/20070709-01402

004229





003 FBEX7701







DECACHLOROBIPHENYL


SOLIDS, TOTAL


E8082

E8082

E8082

E8082

E8082

E8082

E8082

E8082

A2540G


<0.661 MG/KG DRYWT 9/7/2007 10:56 OST

<0.661 MG/KG DRYWT 9/7/2007 10:56 OST

<0.661 MG/KG DRYWT 9/7/2007 10:56 OST

0.510 MG/KG DRYWT 9/7/2007 10:56 OST

<0.661 MG/KG DRYWT 9/7/2007 10:56 OST

<0.661 MG/KG DRYWT 9/7/2007 10:56 OST

75.7 % 8/31/2007 10:56 OST

004 FBEX7702

PCBs ON SOUD








DECACHLOROBIPHENYL


SOUDS, TOTAL

Date Sampled:E8082

E8082

E8082

E8082

E8082

E8082

E8082

E8082

E8082

E8082

A2540G


<6,680 MG/KG

<6,680 MG/KG

< 6,680 MG/KG

< 6,680 MG/KG

26,300 MG/KG

< 6,680 MG/KG

< 6,680 MG/KG

DRYWT

DRYWT

DRYWT

DRYWT

DRYWT

DRYWT

DRYWT

9/7/2007

9/7/2007

9/7/2007

9/7/2007

9/7/2007

9/7/2007

9/7/2007

74.9 % 9/7/2007

10:56

10:56

10:56

10:56

10:56

10:56

10:56

10:56

OST

OST

OST

OST

OST

OST

OST

OST

005 FBEX73SWW

PCBs ON SOUD



Date Sampled:E8082

E8082

E8082


<0.560 MG/KG DRYWT 9/7/2007 10:56 OST

<0.560 MG/KG DRYWT 9/7/2007 10:56 OST

The data and information on this, and other accompanying documents, represent only the sample(s) analyzed and is rendered upon condition

that >t is not to be reproduced wholly or in part for advertising or other purposes without approval from the laboratory.

USOA-EPA-NIOSH Testing Food Sanitation Consulting Chemcal and Microbiological Analyses and Research

NELAP accredited by PA, NY. Visit our website to view our current NELAC accreditations forvarious drinking water, wastewater and solid & chemical rnalerials.air & emissions analytes AC!

Microbac Laboratories, Inc.LRIL DIVISION1962 WAGER ROADLRIL. PA 16504

( X 1 4 1 K 2 5 - 8 5 3 3 FAX (814)X25-9254


http://\v\v\v. microbac.com F.-Mail: [email protected]

Page I of 7

STATL CHRT ID.25-067. lOlIC-PA-05

CHEMISTRY • MICROBIOLOGY • KOOD SAFETY CONSUMtR PRODUCTSWATER • AIR WASTES FOOD PHARMACEUTICALS NUTRACEUT1CALS


DE MAXIMIS. INC.MS. VALERIA A. RULE. P.E.450 MONTBROOK LANEKNOXVILLE.TN 37919

Date ReportedDate ReceivedOrder NumberInvoice No.Cust tf

8/31/20070709-01402

004229

Permit No.



TEST METHOD RESULT UNITS

ANALYSIS


001 FBEXB13

PCBs ON SOLID

AROCHLOR-1016,

AROCHLOR 1221,

AROCHLOR-1232,

AROCHLOR-1242,

AROCHLOR- 1248,

AROCHLOR-1254,

AROCHLOR- 1260,

DRY WT.

DRY WT.

DRY WT.

DRY WT.

DRY WT.

DRY WT.

DRY WT.

DECACHLOROBIPHENYL

TETRACHLORO-M

SOLIDS, TOTAL

•XYLENE

Date Sampled: 8/29/2007E8082

E8082

E8082

E8082

E8082

E8082

E8082

E8082

E8082

E8082

A2540G

<2.27

<2.27

<2.27

<2.27

3.31

<2.27

<2.27

88.3

MG/KG

MG/KG

MG/KG

MG/KG

MG/KG

MG/KG

MG/KG

%

%

%

Time

DRY WT

DRY WT

DRYWT

DRY WT

DRYWT

DRYWT

DRYWT

Sampled:

9/7/2007

9/7/2007

9/7/2007

9/7/2007

9/7/2007

9/7/2007

9/7/2007

8/31/2007

2:25 pm

10:56

10:56

10:56

10:56

10:56

10:56

10:56

10:56

OST

OST

OST

OST

OST

OST

OST

OST

002 FBEX77SWS

PCBs ON SOLID








DECACHLOROBIPHENYL


SOUDS, TOTAL

Date Sampled:E8082

E8082

E8082

E8082

E8082

E8082

E8082

E8082

E8082

E8082

A2540G


<0.289 MG/KG

<0.289 MG/KG

<0.289 MG/KG

<0.289 MG/KG

0.002 MG/KG

<0.289 MG/KG

<0.289 MG/KG

DRY WT

DRYWT

DRY WT

DRY WT

DRYWT

DRY WT

DRY WT

9/7/2007

9/7/2007

9/7/2007

9/7/2007

9/7/2007

9/7/2007

9/7/2007

86.5 % 8/31/2007

10:56

10:56

10:56

10:56

10:56

10:56

10:56

10:56

OST

OST

OST

OST

OST

OST

OST

OST

00.1 FBEX7701

PCBs ON SOLID


Date Sampled:E8082

E80B2


<0.661 MG/KG DRYWT 9/7/2007 10:56 OST

The data and information on tnis, and other accornpany.ng documents, represent om* the sample(s) analyzed and is rendered uoon condition

that it is not to oe reproduced wholly or in part for advertising or other ixrposes without approval from me laboratory

USDA-EPA WOSH Testing Food Sanitation Consulting Chemical . -xl Mioobiologtal Analyses and Research

NELAP accredited by PA. NY Vsit our weDsite to view our ojrrent NELAC accreditations lor

various drinking water, wastewate' and solid a chemical rr.aterials,air 6> emissions analytes AC]'

Microbac Laboratories, Inc.ERIE DIVISION1962 WAGER ROAD

ERIE, PA 16509

(814)825-8533 FAX (814)825-9254



Page 8 of 8


CHEMISTRY • MICROBIOLOGY • FOOD SAFETY CONSUMER PRODUCTSWATER • AIR • WASTES FOOD • PHARMACEUTICALS NUTRACEUTICALS


DEMAXIM1S. INC.MS. VALERIA A. RULE, P.E.450 MONTBROOK. LANEK.NOXV1LLE.TN 37919

Dale ReportedDate ReceivedOrder NumberInvoice No.Cust#

9/5/20070709-01502

004229





All samples received in proper condition and results conform to ISO 17025 standards unless otherwise noted

Accred.

§g This symbol at the end of the test line means the test analysis met the requirements of NELAC (PA ID 25-00067)

*J» This symbol at the end of the lest line means the test analysis met the requirements of AIHA (ID 100386)

^ This symbol at the end of the test line means the test analysis met the requirements of NY ELAP (NY ID 10121)

ABBREVIATIONS

TNTC = Too Numerous To CountUG/L = Micrograms per Liter (PPB)UG/KG = Micrograms per Kilogram (PPB)MG/L = Milligrams per Liter (PPM)1000 UG =1MGPostive = Bacteria or target analyte detected

MG/KG = Milligram per Kilogram (PPM)CPU = Colony Forming UnitNO = Not detected at or below the reporting limitTIC = Tentatively Identified Compound"<" = less than (also see "ND")Negative = Bacteria or target analyte not detected

For any feedback concerning our services, please contact Mark Matrozza, Managing Director at [email protected] or Trevor Boyce.President at presidenUwmicrobac.com

The data and information on this, and other accompanying documents, represent only the sample(s) analyzed and Is rendered upon condition

that it is not to be reproduced wholly or In part for advertising or other purposes without approval from the laboratory

USDA-EPA N10SH Testing Food Sanitation Consulting Chemical and Microbiological Analyses and Research

NEIAP accredited by PA, NY. Visit our website to view our current NELAC accreditations forvarious drinking, water, wastewater and solid ft chemical materials,air & ernlssnns analytes

Acr

Microbac Laboratories, Inc.H R I E DIVISION

1962 WAGER ROADLRIL. PA 165(19

(814)825-8533 FAX (814)825-9254

M A R K MATROZZA , MANAGING DIRECTOR

http://\v\v\v.microbac.com E-Mail: eriefa.'microbnc.com

Pace 7 of 8


CHEMISTRY • MICROBIOLOGY • FOOD SAFETY CONSUMER PRODUCTSWATER • AIR • WASTES FOOD • PHARMACEUTICALS • NUTRACEUTICALS


DEMAXIMIS , INC.MS. VALERIA A. RULE, P.E.450 MONTBROOK LANE

KNOXVILLE.TN 37919

Date ReportedDate ReceivedOrder NumberInvoice No.Custtf

9/5/20070709-01502

004229





013 FBEXMSD2


DECACHLOROBIPHENYL

TETRACHLOROM-XYLENE

SOUDS, TOTAL


E8082

E8082

E8082

A2540G

Time Sam pled: 1:55 pm

UG/KG DRYWT

OI4 FBEXB23







AROCHLOR-12S4, DRY WT.


DECACHLOROBIPHENYL


SOLIDS, TOTAL

E8082

E8082

E8082

E8082

E8082

E8082

E8082

E8082

E8082

E8082

A2540G

Time Sampled: 2:30 pm

UG/KG DRYWT

UG/KG DRYWT

UG/KG DRYWT

UG/KG DRYWT

UG/KG DRYWT

UG/KG DRYWT

UG/KG DRYWT

%

%

%

THE TECH INITIALS "OST" (OUTSIDE TESTING) INDICATE THAT THE PCBANALYSES WERE SUB-CONTRACTED TO MICROBAC, PITTSBURGH DIVISION.

The data and information on this, and other accompanying documents, represent o^v the sampJef s) anaryzed and is rendered upon condition

that It is not to be reproduced wholly or m part for advertising or other purposes without approval from the laboratory

U5DA-EPA NIOSH Tesong Food Sanitation Consulting Chemical and Microbiological Analyses and Research

NELAP accredited by PA, NY. Visit our website to view out current NELAC eccredrtations for

vark)us drinkmg water, wastewater and solid & chemical materials.air & emissions anarytes ACIi



(814)825-8533 FAX (814)825-9254



Page 6 of 8


CHEMISTRY • MICROBIOLOGY • FOOD SAFETY • CONSUMER PRODUCTSWATER • AIR WASTES FOOD • PHARMACEUTICALS • NUTRACEUTICALS


DEMAXIM1S, INC.MS. VALERIA A. RULE, P.E.450 MONTBROOK LANEKNOXVILLE,TN 37919

Date ReportedDale ReceivedOrder NumberInvoice No.Cus t f l

9/5/20070709-01502

004229



TESTANALYSIS

METHOD RESULT UNITS DATE TIME TECH ACCRED.

11 FBEXB22



DECACHLOROBIPHENYL


SOLIDS, TOTAL

Date Sampled: 91412007

E8082E8082E8082E8082A2540G


UG/KG DRYWT

UG/KG DRYWT

012 FBEXEMS2

PCBs ON SOLID

•''OCHLOR-lOie, DRYWT.

CHLOR-1221, DRYWT.






DECACHLOROBIPH EN YL


SOUDS, TOTAL

Date Sampled:E8062E8082E8082E8082E8082E8082E8082E8082E8082E8082A2540G

9/4/2007 Time Sampled: 1:55pm

UG/KG

UG/KG

UG/KG

UG/KG

UG/KG

UG/KG

UG/KG

DRYWT

DRYWT

DRYWT

DRYWT

DRYWT

DRYWT

DRYWT

013 FBEXMSD2

PCBs ON SOLID







Date Sampled:E8082E8082EB082E8082E8082E8082E8082


UG/KG DRYWT

UG/KG DRYWT

UG/KG DRYWT

UG/KG DRYWT

UG/KG DRYWT

UG/KG DRYWT

The data and information on this, and other accompanying documents, represent only the sampled) analyzed and is rendered upon condition

that rt is not to be reproduced wholty or In part tor advertising or other purposes wrthout approval from the Moratory.



various drinking water, wastewater and solid ft chemical rnateriars,air & emissions analytesAC11

Microbac Laboratories, Inc.E R I E DIVISION1962 WAGliR ROADERIE, PA 16509

(814)825-8533 FAX (814)825-9254



Page 5 of 8

STATE CERT ID,25-067. 1 0 1 2 )C-PA-05

CHEMISTRY • MICROBIOLOGY • FOOD SAFETY CONSUMER PRODUCTSWATER • AIR WASTES • FOOD PHARMACEUTICALS • NUTRACEUTICALS


D E M A X I M I S . INC.MS. VALERIA A. RULE, P.E.450 MONTBROOK LANE

K.NOXV1LLE.TN 37919


9/5/20070709-01502

004229



TESTANALYSIS —


9 FBEXDUP2




DECACHLOROBIPHENYL

TETRACHLOROM-XYLENE

SOLIDS, TOTAL


E8082

E8082

E8082

E8082

E8082

A2540G

Time Sampled:

384 MG/KG DRYWT 9/11/2007

<551 MG/KG DRYWT 9/11/2007

<551 MG/KG DRYWT 9/11/2007

90.8 9/5/2007

11:14

11:14

11:14

11:14

OST

OST

OST

OST

010 FBEXB21

PCBs ON SOLID








DECACHLOROBIPHENYL


SOLIDS, TOTAL

Date Sampled:E8082

E8082

E8082

E80B2

E8082

E8082

E8082

E8082

E8082

E8082

A2540G


UG/KG

UG/KG

UG/KG

UG/KG

UG/KG

UG/KG

UG/KG

DRYWT

DRYWT

DRYWT

DRYWT

DRYWT

DRYWT

DRYWT

Oil FBEXB22

PCBs ON SOLID






Date Sampled:E8082

E8082

E8082

E8082

E8082

E8082


UG/KG DRY WT

UG/KG DRY WT

UG/KG DRY WT

UG/KG DRYWT

UG/KG DRYWT

The data and information on this, and other accompanying documents, represent oni, the sample(s) analyzed and is rendered upon condition

tnat it is not to be reproduced wholly or in part for advertising or other purposes without approval from the Moratory

USDA-EPA NIOSH Testing Food Sanitation Consulting Chemical a-x! Microbiological Analyses and Research

NELAP accredited by PA, NY visit our website to view our oj-rent NFLAC accreditations for

vanous dnnkirwj water, wastewater and solid ft chemical materials.a'r & emissions anatytes ACl'


1962 WAGER ROAD

ERIE, PA 16509

(814)825-8533 FAX (814)825-9254



Pagc4ol',S

STATE CERT ID.

25-067. 10121

C-PA-05

CHEMISTRY • MICROBIOLOGY • FOOD SAFETY • CONSUMER PRODUCTSWATER AIR • WASTES FOOD • PHARMACEUTICALS NUTRACEUTICALS


DEMAXIMIS, INC.

MS. VALERIA A. RULE, P.E.

450 MONTBROOK LANE

KNOXV1LLE,TN 37919

Date Reported

Date Received

Order Number

Invoice No.

Custtf

9/5/2007

0709-01502

004229

Permit No.



TEST METHOD RESULT UNITS

ANALYSIS


007 FBEXB20

continued





DECACHLOROBIPHENYL


SOLIDS, TOTAL


E8082

E8082

E8082

E8082

E8082

E8082

A2540G

Time Sampled: 1:39pm

<111 MG/KG DRYWT 9/10/2007

283 MG/KG DRYWT 9/10/2007

<111 MG/KG DRYWT 9/10/2007

<111 MG/KG DRYWT 9/10/2007

89.7 % 9/5/2007

11:14

11:14

11:14

11:14

11:14

OST

OST

OST

OST

OST

008 FBEXB20SN

, s ON SOLID








DECACHLOROBIPHENYL


SOLIDS, TOTAL

Date Sampled:

E8082

E8082

E8082

E8082

E8082

EB082

EB082

E8082

E8082

E8082

A2540G


<578 MG/KG

<578 MG/KG

<578 MG/KG

<578 MG/KG

851 MG/KG

<578 MG/KG

<S78 MG/KG

DRYWT

DRYWT

DRYWT

DRYWT

DRYWT

DRYWT

DRYWT

9/11/2007

9/11/2007

9/11/2007

9/11/2007

9/11/2007

9/11/2007

9/11/2007

11:14

11:14

11:14

11:14

11:14

11:14

11:14

OST

OST

OST

OST

OST

OST

OST

86.5 % 9/5/2007 11:14 OST

009 FBEXDUP2

PCBs ON SOLID





Date Sampled:

E8082

E8082

E8082

E8082

E8082

9/4/2007 Time Sampled:

<551 MG/KG DRYWT 9/11/2007 11:14 OST

<551 MG/KG DRYWT 9/11/2007 11:14 OST

<551 MG/KG DRYWT 9/11/2007 11:14 OST

<551 MG/KG DRYWT 9/11/2007 11:14 OST

The data and information on this, and other accompanying documents, represent only the sampte(s) analyred and is rendered upon condition

that t is not to be reproduced wholly or in part for advertising or other purposes without approval from the laboratory.

USDA-EPA-NIOSH Testing Food Sanitation Consulting Chemical art Moobological Analyses and Research

NELAP accredited by PA, NY Visit our website to view our current NELAC accreditations forvarious drinking water, wastewater and solid & chemical materials.air & emissions artalytes

Acr

Microbac Laboratories, Inc.HRIE DIVISION

1962 WAGER ROADERIC. PA 16509

(814)825-8533 FAX (814)825-9254

MARK MATRO2ZA , MANAGING DIRECTOR


Paee 3 of 8


CHEMISTRY • MICROBIOLOGY • FOOD SAFETY CONSUMER PRODUCTSWATER • AIR • WASTES • FOOD PHARMACEUTICALS • NUTRACEUTICALS


DEMAXIM1S, INC.MS. VALERIA A. RULE, P.E.450 MONTBROOK LANE

KNOXV1LLE.TN 37919


9/5/20070709-01502

004229





005 FBEXB18






DECACHLOROBIPHENYL


SOLIDS, TOTAL


E8082

E8082

E8082

E8082

E8082

E8082

E8082

A2540G


UG/KG DRYWT

UG/KG DRYWT

UG/KG DRY WT

UG/KG DRYWT

UG/KG DRY WT

006 FBEXB19

PCBs ON SOLID








DECACHLOROBIPHENYL


SOLIDS, TOTAL

Date Sampled:E8082

E8082

E8082

E8082

E8082

E8082

E8082

E8082

E8082

E8082

A2540G


<58i MG/KG

<581 MG/KG

<58i MG/KG

<581 MG/KG

1,430 MG/KG<58i MG/KG<581 MG/KG

86.1

DRYWT

DRYWT

DRYWT

DRYWT

DRYWT

DRYWT

DRYWT

9/10/2007

9/10/2007

9/10/2007

9/10/2007

9/10/2007

9/10/2007

9/10/2007

9/5/2007

11:14

11:14

11:14

11:14

11:14

11:14

11:14

11:14

OST

OST

OST

OST

OST

OST

OST

OST

007 FBEXB20

PCBs ON SOLID




Date Sampled:E8082

E8082

E8082

E8082


<111 MG/KG DRYWT 9/10/2007 11:14 OST

<ni MG/KG DRYWT 9/10/2007 11:14 OST<111 MG/KG DRYWT 9/10/2007 11:14 OST

The data and information on this, and other accompanying documents, represent cmly the sample(s) analyzed and is rendered upon condition

that it is not to be reproduced wholly or m part lor advertising or other purposes witnout approval from the laboratory


NELAP accredited by PA, NY. visit our website to view our current NELAC accreditations for

various drinking water, wastewater and solid & chem.ca rnatenals.air & emissions analvtes AO



(814)825-8513 FAX (814)825-9254



Page 2 ol'8


CHEMISTRY • MICROBIOLOGY • FOOD SAFETY CONSUMER PRODUCTSWATER AIR WASTES FOOD • PHARMACEUTICALS • NUTRACEUTICALS


DEMAX1MIS, INC.MS. VALERIA A. RULE, P.h.450 MONTBROOK LANE

KNOXVILLE.TN 37919

Date ReportedDate ReceivedOrder NumberInvoice No.Cust#

9/5/20070709-01502

004229



TESTANALYSIS


3 FBEXB16







DECACHLOROBIPHENYL


SOLIDS, TOTAL


E8082

E8082

E8082

E8082

E8082

E8082

E8082

E8082

A2540G


<563 MG/KG DRYWT 9/10/2007 11:14 OST

<563 MG/KG DRYWT 9/10/2007 11:14 OST

<563 MG/KG DRYWT 9/10/2007 11:14 OST

675 MG/KG DRYWT 9/10/2007 11:14 OST

<563 MG/KG DRYWT 9/10/2007 11:14 OST

<563 MG/KG DRYWT 9/10/2007 11:14 OST

88.8 % 9/5/2007 11:14 OST

004 FBEXB17

PCBs ON SOLID



AROCHLOR-1232, DRf WT.





DECACHLOROBIPHENYL


SOLIDS, TOTAL

Date Sampled:E8082

E8082

E8082

E8082

E8082

E8082

E8082

E8082

E8082

E8082

A2540G


UG/KG DRYWT

UG/KG DRYWT

UG/KG ORYWT

UG/KG DRYWT

UG/KG DRYWT

UG/KG DRYWT

UG/KG DRYWT

005 FBEXB18

PCBs ON SOLID


AROCHLOR-1221, DRY WT

Date Sampled:E8082

E8082

E8082


UG/KG DRYWT

UG/KG DRYWT

The data ana information on this, and other accompanying documents, represent only the sample{s) analyzed and is rendered upon cond'tion

thai it is not to be reproduced wholly c* m part (or advertising or other purposes without aporwsl from the laboratory.USDA-EPA-NIOSH Testing Food Sanitation Consulting Chemical and Microbiological Analyses and Research

NELAP accredited by PA, NY Visit our website to view our current NELAC accreditations for

various drinking water, wastewater and solid & chemical materials.alr & emissions analytes Acr

Microbac Laboratories, Inc.100 MARSHALL DRIVEWARRENDALE, PA 15086

(724)772-0610 FAX (724) 772-1686MARK A. MATROZZA, MANAGING DIRECTOR

http://w-wu-.mJcrobac.com

Page 1 of 1

State Laboratory Certification Numbers:PADEP: 02-257, NC: 42703, WVDEP: 215, 9951 CM KY: 90136

CHEMISTRY • MICROBIOLOGY • FOOD SAFETY - CONSUMER PRODUCTSWATER • AIR • WASTES • FOOD PHARMACEUTICALS • NUTRACEUTICALS

CERTIFICATE OF ANALYSIS

MICROBAC ERIE DIVISION

CHERI BROLASKI


Permit No.:Cust P.O.:

SUBJECT: 0708-2872/DeMaximis - Oil Sample for Analysis

Date Reported:Date Received:Order Number:Invoice No.:

Cust #:Sample Date:Sample Time:

Sampler/Temp:

8/31/2007

0708-02667

M296

8/29/20070:00

TEST METHOD RESULT UNITS DATE 1 >I

001 0708-2872

Collected 8/29/07

PCBs (Oil)

PCB-1016

PCB-1221

PCB-1232

PCB-1242

PCB-1248

PCB-1254

PCB-1260

SW-846 8082

< 20,000

< 20,000

<20,000

< 20,000

1,140,000

< 20,000

< 20,000

mg/Kg

mg/Kg

mg/Kg

mg/Kg

mg/Kg

mg/Kg

mg/Kg

09/07/07

09/07/07

09/07/07

09/07/07

09/07/07

09/07/07

09/07/07

TWCTWCTWCTWCTWCTWCTWC

Submitted By:

Mark A. Matrozza, Managing Director

Trie data and information on this, and other accompanying documents, represent only the samplers) analyzed and is rendered upon condition

that ft is not to be reproduced wholly or m part for advertising or other purposes without approval from the laboratory.

USDA-EPA-NIOSH Testing Food Sanitation Consulting Chemical and Microbdogical Analyses and Research

MEMBER

microbac laboratories, inc.date timtech accrede . all samples received in proper condition and...

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