resource… · 1 icp test report certification packet company name : littelfuse, inc. product...

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1 ICP Test Report Certification Packet Company name: Littelfuse, Inc. Product Series: FUSE - BF1 58V Product #: 142.5631.xxx Series Issue Date: August 22, 2012 It is hereby certified by Littelfuse, Inc. that there is neither RoHS (EU Directive 2002/95/EC, 2011/65/EU)-restricted substance nor such use, for materials to be used for unit parts, for packing/packaging materials, and for additives and the like in the manufacturing processes. In addition, it is hereby reported to you that the parts and sub-materials, the materials to be used for unit parts, the packing/packaging materials, and the additives and the like in the manufacturing processes, are all composed of the following components. Issued by: <Global EHS Engineer> (1) Parts, sub-materials and unit parts This document covers the FUSE - BF1 58V RoHS-Compliant series products manufactured by Littelfuse, Inc. Raw Materials Used Please see Table 1 (2) The ICP data on all measurable substances Please see appropriate pages as identifed in Table 1 Remarks.

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Page 1: resource… · 1 ICP Test Report Certification Packet Company name : Littelfuse, Inc. Product Series: FUSE - BF1 58V Product #: 142.5631.xxx Series Issue Date: August 22, 2012 It

1

ICP Test Report Certification Packet

Company name : Littelfuse, Inc.

Product Series: FUSE - BF1 58V

Product #: 142.5631.xxx Series

Issue Date: August 22, 2012

It is hereby certified by Littelfuse, Inc. that there is neither RoHS (EU Directive 2002/95/EC,

2011/65/EU)-restricted substance nor such use, for materials to be used for unit parts, for

packing/packaging materials, and for additives and the like in the manufacturing processes.

In addition, it is hereby reported to you that the parts and sub-materials, the materials to be used

for unit parts, the packing/packaging materials, and the additives and the like in the manufacturing

processes, are all composed of the following components.

Issued by:

<Global EHS Engineer>

(1) Parts, sub-materials and unit parts

This document covers the FUSE - BF1 58V RoHS-Compliant series products

manufactured by Littelfuse, Inc.

< Raw Materials Used

Please see Table 1

(2) The ICP data on all measurable substances

Please see appropriate pages as identifed in Table 1

Remarks:.

Page 2: resource… · 1 ICP Test Report Certification Packet Company name : Littelfuse, Inc. Product Series: FUSE - BF1 58V Product #: 142.5631.xxx Series Issue Date: August 22, 2012 It

2

Table 1: List of Raw Materials covered by this report

Total Parts Raw Material Part Number Raw Material Description Page(s)

1 353.2131.4300 Housing - orange 3-11

2 353.2131.4400 Housing – Light green 12-20

3 353.2131.4500 Housing - red 21-29

4 353.2131.4600 Housing - yellow 30-38

5 353.2130.4700 Housing - brown 39-47

6 353.2131.4800 Housing – white 48-56

7 353.2131.5100 Housing – blue 57-65

8 353.2131.5125 Housing – pink 66-74

9 353.2131.5150 Housing – gray 75-83

10 353.1119.4043 Band CuZn (base) 84-86

11 353.1119.4043 Band CuZn (plating) 84-86

12 353.1126.4043 Band Cu Fe2P (base) 87-89

13 353.1126.4043 Band Cu Fe2P (plating) 87-89

14 355.1115.2053 Band Cu-ETP 90-94

15 355.1115.3053 Band Cu-ETP 95-99

16 325.2131.0001 Housing – natural 100-108

17 353.2131.5200/ 325.7692.0810 Housing – violet 109-117

18 353.2140.1000 BF1 Clear Cover 118-126

19 353.1590.0001 Solder 127-131

Form 585-047 Rev. A 2/21/06

Page 3: resource… · 1 ICP Test Report Certification Packet Company name : Littelfuse, Inc. Product Series: FUSE - BF1 58V Product #: 142.5631.xxx Series Issue Date: August 22, 2012 It

Test Report Number : TWNC00241666

Authorized By: On Behalf Of Intertek Testing Services Taiwan Limited

K. Y. Liang Director

This report shall not be reproduced except in full, without the written approval of the laboratory.

Page 1 of 9 Intertek Testing Services Taiwan Ltd.

8F., No. 423, Ruiguang Rd., Neihu District, Taipei 114, Taiwan, R.O.C. 全國公證檢驗股份有限公司 114台北市內湖區瑞光路 423號 8樓

Tel: (+886-2) 6602-2888.2797-8885 Fax: (+886-2) 6602-2400.6602-2401

Applicant: Littelfuse, S.A. de C.V. Date : Feb 01, 2012 Blvd. Fausto Z. Martinez #1800

Col. Magisterio Seccion 38 C.P. 26070 Piedra Negras, Coahuila, Mexico

Sample Description:

One (1) group of submitted samples said to be : Part Description : HOUSING ORANGE Part Number : 353.2131.4300 Date Sample Received : Jan 20, 2012 Date Test Started : Jan 30, 2012

Test Conducted :

As requested by the applicant, for details please refer to attached pages.

Page 4: resource… · 1 ICP Test Report Certification Packet Company name : Littelfuse, Inc. Product Series: FUSE - BF1 58V Product #: 142.5631.xxx Series Issue Date: August 22, 2012 It

Number : TWNC00241666

Test Conducted

Page 2 of 9 Intertek Testing Services Taiwan Ltd.

8F., No. 423, Ruiguang Rd., Neihu District, Taipei 114, Taiwan, R.O.C. 全國公證檢驗股份有限公司 114台北市內湖區瑞光路 423號 8樓

Tel: (+886-2) 6602-2888.2797-8885 Fax: (+886-2) 6602-2400.6602-2401

(Ⅰ) Test Result Summary : Result (ppm)

Test Item Orange Plastic

Heavy Metal

Cadmium (Cd) content ND Lead (Pb) content 17 Mercury (Hg) content ND Chromium VI (Cr6+) content ND

Polybrominated Biphenyls (PBBs) Monobrominated Biphenyls (MonoBB) ND Dibrominated Biphenyls (DiBB) ND Tribrominated Biphenyls (TriBB) ND Tetrabrominated Biphenyls (TetraBB) ND Pentabrominated Biphenyls (PentaBB) ND Hexabrominated Biphenyls (HexaBB) ND Heptabrominated Biphenyls (HeptaBB) ND Octabrominated Biphenyls (OctaBB) ND Nonabrominated Biphenyls (NonaBB) ND Decabrominated Biphenyl (DecaBB) ND

Polybrominated Diphenyl Ethers (PBDEs) Monobrominated Diphenyl Ethers (MonoBDE) ND Dibrominated Diphenyl Ethers (DiBDE) ND Tribrominated Diphenyl Ethers (TriBDE) ND Tetrabrominated Diphenyl Ethers (TetraBDE) ND Pentabrominated Diphenyl Ethers (PentaBDE) ND Hexabrominated Diphenyl Ethers (HexaBDE) ND Heptabrominated Diphenyl Ethers (HeptaBDE) ND Octabrominated Diphenyl Ethers (OctaBDE) ND Nonabrominated Diphenyl Ethers (NonaBDE) ND Decabrominated Diphenyl Ether (DecaBDE) ND

Halogen Content Fluorine (F) ND Chlorine (Cl) ND Bromine (Br) 59154 Iodine (I) ND

Page 5: resource… · 1 ICP Test Report Certification Packet Company name : Littelfuse, Inc. Product Series: FUSE - BF1 58V Product #: 142.5631.xxx Series Issue Date: August 22, 2012 It

Number : TWNC00241666

Test Conducted

Page 3 of 9 Intertek Testing Services Taiwan Ltd.

8F., No. 423, Ruiguang Rd., Neihu District, Taipei 114, Taiwan, R.O.C. 全國公證檢驗股份有限公司 114台北市內湖區瑞光路 423號 8樓

Tel: (+886-2) 6602-2888.2797-8885 Fax: (+886-2) 6602-2400.6602-2401

(Ⅰ) Test Result Summary : Result (ppm)

Test Item Orange Plastic

Phthalates Di(2-ethylhexyl) Phthalate (DEHP) ND Dibutyl Phthalate (DBP) ND Benzyl Butyl Phthalate (BBP) ND

Others Hexabromocyclododecane (HBCDD) ND

Remarks: ppm = Parts per million based on weight of tested sample = mg/kg ND = Not detected

Responsibility of Chemist :Irene Chiou / Kevin Liu / Cathy Chen

Date Sample Received : Jan 20, 2012 Test Period : Jan 30, 2012 To Feb 01, 2012

(Ⅱ) RoHS Requirement:

Restricted Substances Limits

Cadmium (Cd) Content 0.01% (100ppm) Lead (Pb) Content 0.1% (1000ppm) Mercury (Hg) Content 0.1% (1000ppm) Chromium VI (Cr6+) Content 0.1% (1000ppm) Polybrominated Biphenyls (PBBs) 0.1% (1000ppm) Polybrominated Diphenyl Ehters (PBDEs) 0.1% (1000ppm)

The above limits were quoted from 2002/95/EC and amendment 2005/618/EC for homogeneous material.

Page 6: resource… · 1 ICP Test Report Certification Packet Company name : Littelfuse, Inc. Product Series: FUSE - BF1 58V Product #: 142.5631.xxx Series Issue Date: August 22, 2012 It

Number : TWNC00241666

Test Conducted

Page 4 of 9 Intertek Testing Services Taiwan Ltd.

8F., No. 423, Ruiguang Rd., Neihu District, Taipei 114, Taiwan, R.O.C. 全國公證檢驗股份有限公司 114台北市內湖區瑞光路 423號 8樓

Tel: (+886-2) 6602-2888.2797-8885 Fax: (+886-2) 6602-2400.6602-2401

(Ⅲ) Test Method: Test Item Test Method Reporting Limit

Cadmium (Cd) content

With reference to IEC 62321 edition 1.0:2008 in clause 8/9/10, by microwave digestion until the tested samples are totally dissolved and determined by ICP-OES.

2 ppm

Lead (Pb) content

With reference to IEC 62321 edition 1.0:2008 in clause 8/9/10, by microwave digestion until the tested samples are totally dissolved and determined by ICP-OES.

2 ppm

Mercury (Hg) content

With reference to IEC 62321 edition 1.0:2008 in clause 7, by microwave digestion until the tested samples are totally dissolved and determined by ICP-OES.

2 ppm

Chromium VI (Cr6+) content

With reference to IEC 62321 edition 1.0:2008 in annex C, by alkaline digestion and determined by UV-Vis spectrophotometer.

1 ppm

Polybrominated Biphenyls (PBBs)

With reference to IEC 62321 edition 1.0:2008 in annex A, by solvent extraction and determined by GC-MS and further HPLC-DAD confirmation when necessary.

5 ppm

Polybrominated Diphenyl Ethers (PBDEs)

With reference to IEC 62321 edition 1.0:2008 in annex A, by solvent extraction and determined by GC-MS and further HPLC-DAD confirmation when necessary.

5 ppm

Halogen Content With reference to EN 14582:2007 by calorimetric bomb with oxygen and determined by Ion Chromatograph.

50 ppm

Phthalates With reference to ASTM D3421-75, by solvent extraction and determined byGC-MSD or GC-FID

10 ppm

Hexabromocyclododecane(HBCDD)

With reference to USEPA 3540C, by solvent extraction and determined byGC-MSD

10 ppm

Remark: Reporting limit = Quantitation limit of analyte in sample

Page 7: resource… · 1 ICP Test Report Certification Packet Company name : Littelfuse, Inc. Product Series: FUSE - BF1 58V Product #: 142.5631.xxx Series Issue Date: August 22, 2012 It

Number : TWNC00241666

Test Conducted

Page 5 of 9 Intertek Testing Services Taiwan Ltd.

8F., No. 423, Ruiguang Rd., Neihu District, Taipei 114, Taiwan, R.O.C. 全國公證檢驗股份有限公司 114台北市內湖區瑞光路 423號 8樓

Tel: (+886-2) 6602-2888.2797-8885 Fax: (+886-2) 6602-2400.6602-2401

(Ⅳ) Measurement Flowchart: Test for Cd/Pb/Hg/Chromium (VI)/PBBS/PBDES Contents Reference Standard: IEC 62321 edition 1.0:2008

Remarks: *1: List of Appropriate Acid:

Material Acid Added for Digestion Polymers HNO3,HCl,HF,H2O2,H3BO3 Metals HNO3,HCl,HF Electronics HNO3,HCl,H2O2,HBF4

*2: If the result of spot test is positive, Chromium VI would be determined as detected.

Sample preparation

For different material, digest the sample with appropriate acid*1

Make up with deionized water

Cd/Pb/Hg

Analyzed by ICP-OES

Weigh sample and add alkaline solution

Definite temp. extraction

Make up with deionized water and add diphenyl-carbazide solution

Cool and filter the extract

Cr6+

Weigh sample and add organic solvent

By Soxhlet extraction or Solvent extraction

Concentrate the extract and make upwith organic solvent

PBBs/PBDEs

Analyzed by UV-VIS

Analyzed by GC-MSD

By spot test

Get 50cm2 sample

By boiling water extraction

Metal Polymers / electronics

Negative *2

Confirm the tested samples are totally dissolved

Take sample and immerse into Aqua Regia, start to strip plating layer

Stop the stripping procedure upon color change completely

Take the Aqua solution as plating component and stripped body as substrate component

For non-metal part For metal part

Page 8: resource… · 1 ICP Test Report Certification Packet Company name : Littelfuse, Inc. Product Series: FUSE - BF1 58V Product #: 142.5631.xxx Series Issue Date: August 22, 2012 It

Number : TWNC00241666

Test Conducted

Page 6 of 9 Intertek Testing Services Taiwan Ltd.

8F., No. 423, Ruiguang Rd., Neihu District, Taipei 114, Taiwan, R.O.C. 全國公證檢驗股份有限公司 114台北市內湖區瑞光路 423號 8樓

Tel: (+886-2) 6602-2888.2797-8885 Fax: (+886-2) 6602-2400.6602-2401

(Ⅳ) Measurement Flowchart:

Test for Halogen Content Reference Standard:EN 14582

Add absorbent in a combustion flask & place weighed sample in equipment

Fill oxygen into calorimetric bomb

Ignite then leave the bomb at room temperature

Transfer the absorbent into a volumetric flask

Make up with deionized water

Sampling/grinding or cutting

Analyzed by ion chromatography

Page 9: resource… · 1 ICP Test Report Certification Packet Company name : Littelfuse, Inc. Product Series: FUSE - BF1 58V Product #: 142.5631.xxx Series Issue Date: August 22, 2012 It

Number : TWNC00241666

Test Conducted

Page 7 of 9 Intertek Testing Services Taiwan Ltd.

8F., No. 423, Ruiguang Rd., Neihu District, Taipei 114, Taiwan, R.O.C. 全國公證檢驗股份有限公司 114台北市內湖區瑞光路 423號 8樓

Tel: (+886-2) 6602-2888.2797-8885 Fax: (+886-2) 6602-2400.6602-2401

(Ⅳ) Measurement Flowchart: Test For Phthalates Contents Reference Method: EN 14372: 2004

Sampling/grinding or cutting

Weigh sample and add organic solvent

By solvent extraction

Concentrate the extract and make up with organic solvent

Analyzed by GC-MSD

Page 10: resource… · 1 ICP Test Report Certification Packet Company name : Littelfuse, Inc. Product Series: FUSE - BF1 58V Product #: 142.5631.xxx Series Issue Date: August 22, 2012 It

Number : TWNC00241666

Test Conducted

Page 8 of 9 Intertek Testing Services Taiwan Ltd.

8F., No. 423, Ruiguang Rd., Neihu District, Taipei 114, Taiwan, R.O.C. 全國公證檢驗股份有限公司 114台北市內湖區瑞光路 423號 8樓

Tel: (+886-2) 6602-2888.2797-8885 Fax: (+886-2) 6602-2400.6602-2401

(Ⅳ) Measurement Flowchart:

Test For Hexabromocyclododecane (HBCDD) Reference Standard:USEPA 3540C

End of Report

Sampling/grinding or cutting

Weigh sample and add organic solvent

By soxhlet extraction

Concentrate the extract and make up with organic solvent

Analyzed by GC-MSD

Page 11: resource… · 1 ICP Test Report Certification Packet Company name : Littelfuse, Inc. Product Series: FUSE - BF1 58V Product #: 142.5631.xxx Series Issue Date: August 22, 2012 It

Number : TWNC00241666

Test Conducted

Page 9 of 9 Intertek Testing Services Taiwan Ltd.

8F., No. 423, Ruiguang Rd., Neihu District, Taipei 114, Taiwan, R.O.C. 全國公證檢驗股份有限公司 114台北市內湖區瑞光路 423號 8樓

Tel: (+886-2) 6602-2888.2797-8885 Fax: (+886-2) 6602-2400.6602-2401

Photo

Page 12: resource… · 1 ICP Test Report Certification Packet Company name : Littelfuse, Inc. Product Series: FUSE - BF1 58V Product #: 142.5631.xxx Series Issue Date: August 22, 2012 It

Test Report Number : TWNC00241667

Authorized By: On Behalf Of Intertek Testing Services Taiwan Limited

K. Y. Liang Director

This report shall not be reproduced except in full, without the written approval of the laboratory.

Page 1 of 9 Intertek Testing Services Taiwan Ltd.

8F., No. 423, Ruiguang Rd., Neihu District, Taipei 114, Taiwan, R.O.C. 全國公證檢驗股份有限公司 114 台北市內湖區瑞光路 423 號 8 樓

Tel: (+886-2) 6602-2888.2797-8885 Fax: (+886-2) 6602-2400.6602-2401

Applicant: Littelfuse, S.A. de C.V. Date : Feb 01, 2012 Blvd. Fausto Z. Martinez #1800

Col. Magisterio Seccion 38 C.P. 26070 Piedra Negras, Coahuila, Mexico

Sample Description:

One (1) group of submitted samples said to be : Part Description : HOUSING LIGHT GREEN Part Number : 353.2131.4400 Date Sample Received : Jan 20, 2012 Date Test Started : Jan 30, 2012

Test Conducted :

As requested by the applicant, for details please refer to attached pages.

Page 13: resource… · 1 ICP Test Report Certification Packet Company name : Littelfuse, Inc. Product Series: FUSE - BF1 58V Product #: 142.5631.xxx Series Issue Date: August 22, 2012 It

Number : TWNC00241667

Test Conducted

Page 2 of 9 Intertek Testing Services Taiwan Ltd.

8F., No. 423, Ruiguang Rd., Neihu District, Taipei 114, Taiwan, R.O.C. 全國公證檢驗股份有限公司 114 台北市內湖區瑞光路 423 號 8 樓

Tel: (+886-2) 6602-2888.2797-8885 Fax: (+886-2) 6602-2400.6602-2401

(Ⅰ) Test Result Summary : Result (ppm)

Test Item Green Plastic

Heavy Metal

Cadmium (Cd) content ND Lead (Pb) content 12 Mercury (Hg) content ND Chromium VI (Cr6+) content ND

Polybrominated Biphenyls (PBBs) Monobrominated Biphenyls (MonoBB) ND Dibrominated Biphenyls (DiBB) ND Tribrominated Biphenyls (TriBB) ND Tetrabrominated Biphenyls (TetraBB) ND Pentabrominated Biphenyls (PentaBB) ND Hexabrominated Biphenyls (HexaBB) ND Heptabrominated Biphenyls (HeptaBB) ND Octabrominated Biphenyls (OctaBB) ND Nonabrominated Biphenyls (NonaBB) ND Decabrominated Biphenyl (DecaBB) ND

Polybrominated Diphenyl Ethers (PBDEs) Monobrominated Diphenyl Ethers (MonoBDE) ND Dibrominated Diphenyl Ethers (DiBDE) ND Tribrominated Diphenyl Ethers (TriBDE) ND Tetrabrominated Diphenyl Ethers (TetraBDE) ND Pentabrominated Diphenyl Ethers (PentaBDE) ND Hexabrominated Diphenyl Ethers (HexaBDE) ND Heptabrominated Diphenyl Ethers (HeptaBDE) ND Octabrominated Diphenyl Ethers (OctaBDE) ND Nonabrominated Diphenyl Ethers (NonaBDE) ND Decabrominated Diphenyl Ether (DecaBDE) ND

Halogen Content Fluorine (F) ND Chlorine (Cl) ND Bromine (Br) 55286 Iodine (I) ND

Page 14: resource… · 1 ICP Test Report Certification Packet Company name : Littelfuse, Inc. Product Series: FUSE - BF1 58V Product #: 142.5631.xxx Series Issue Date: August 22, 2012 It

Number : TWNC00241667

Test Conducted

Page 3 of 9 Intertek Testing Services Taiwan Ltd.

8F., No. 423, Ruiguang Rd., Neihu District, Taipei 114, Taiwan, R.O.C. 全國公證檢驗股份有限公司 114 台北市內湖區瑞光路 423 號 8 樓

Tel: (+886-2) 6602-2888.2797-8885 Fax: (+886-2) 6602-2400.6602-2401

(Ⅰ) Test Result Summary : Result (ppm)

Test Item Green Plastic

Phthalates Di(2-ethylhexyl) Phthalate (DEHP) ND Dibutyl Phthalate (DBP) ND Benzyl Butyl Phthalate (BBP) ND

Others Hexabromocyclododecane (HBCDD) ND

Remarks: ppm = Parts per million based on weight of tested sample = mg/kg ND = Not detected

Responsibility of Chemist :Irene Chiou / Kevin Liu / Cathy Chen

Date Sample Received : Jan 20, 2012 Test Period : Jan 30, 2012 To Feb 01, 2012

(Ⅱ) RoHS Requirement:

Restricted Substances Limits

Cadmium (Cd) Content 0.01% (100ppm) Lead (Pb) Content 0.1% (1000ppm) Mercury (Hg) Content 0.1% (1000ppm) Chromium VI (Cr6+) Content 0.1% (1000ppm) Polybrominated Biphenyls (PBBs) 0.1% (1000ppm) Polybrominated Diphenyl Ehters (PBDEs) 0.1% (1000ppm)

The above limits were quoted from 2002/95/EC and amendment 2005/618/EC for homogeneous material.

Page 15: resource… · 1 ICP Test Report Certification Packet Company name : Littelfuse, Inc. Product Series: FUSE - BF1 58V Product #: 142.5631.xxx Series Issue Date: August 22, 2012 It

Number : TWNC00241667

Test Conducted

Page 4 of 9 Intertek Testing Services Taiwan Ltd.

8F., No. 423, Ruiguang Rd., Neihu District, Taipei 114, Taiwan, R.O.C. 全國公證檢驗股份有限公司 114 台北市內湖區瑞光路 423 號 8 樓

Tel: (+886-2) 6602-2888.2797-8885 Fax: (+886-2) 6602-2400.6602-2401

(Ⅲ) Test Method: Test Item Test Method Reporting Limit

Cadmium (Cd) content

With reference to IEC 62321 edition 1.0:2008 in clause 8/9/10, by microwave digestion until the tested samples are totally dissolved and determined by ICP-OES.

2 ppm

Lead (Pb) content

With reference to IEC 62321 edition 1.0:2008 in clause 8/9/10, by microwave digestion until the tested samples are totally dissolved and determined by ICP-OES.

2 ppm

Mercury (Hg) content

With reference to IEC 62321 edition 1.0:2008 in clause 7, by microwave digestion until the tested samples are totally dissolved and determined by ICP-OES.

2 ppm

Chromium VI (Cr6+) content

With reference to IEC 62321 edition 1.0:2008 in annex C, by alkaline digestion and determined by UV-Vis spectrophotometer.

1 ppm

Polybrominated Biphenyls (PBBs)

With reference to IEC 62321 edition 1.0:2008 in annex A, by solvent extraction and determined by GC-MS and further HPLC-DAD confirmation when necessary.

5 ppm

Polybrominated Diphenyl Ethers (PBDEs)

With reference to IEC 62321 edition 1.0:2008 in annex A, by solvent extraction and determined by GC-MS and further HPLC-DAD confirmation when necessary.

5 ppm

Halogen Content With reference to EN 14582:2007 by calorimetric bomb with oxygen and determined by Ion Chromatograph.

50 ppm

Phthalates With reference to ASTM D3421-75, by solvent extraction and determined byGC-MSD or GC-FID

10 ppm

Hexabromocyclododecane(HBCDD)

With reference to USEPA 3540C, by solvent extraction and determined byGC-MSD

10 ppm

Remark: Reporting limit = Quantitation limit of analyte in sample

Page 16: resource… · 1 ICP Test Report Certification Packet Company name : Littelfuse, Inc. Product Series: FUSE - BF1 58V Product #: 142.5631.xxx Series Issue Date: August 22, 2012 It

Number : TWNC00241667

Test Conducted

Page 5 of 9 Intertek Testing Services Taiwan Ltd.

8F., No. 423, Ruiguang Rd., Neihu District, Taipei 114, Taiwan, R.O.C. 全國公證檢驗股份有限公司 114 台北市內湖區瑞光路 423 號 8 樓

Tel: (+886-2) 6602-2888.2797-8885 Fax: (+886-2) 6602-2400.6602-2401

(Ⅳ) Measurement Flowchart: Test for Cd/Pb/Hg/Chromium (VI)/PBBS/PBDES Contents Reference Standard: IEC 62321 edition 1.0:2008

Remarks: *1: List of Appropriate Acid:

Material Acid Added for Digestion Polymers HNO3,HCl,HF,H2O2,H3BO3 Metals HNO3,HCl,HF Electronics HNO3,HCl,H2O2,HBF4

*2: If the result of spot test is positive, Chromium VI would be determined as detected.

Sample preparation

For different material, digest the sample with appropriate acid*1

Make up with deionized water

Cd/Pb/Hg

Analyzed by ICP-OES

Weigh sample and add alkaline solution

Definite temp. extraction

Make up with deionized water and add diphenyl-carbazide solution

Cool and filter the extract

Cr6+

Weigh sample and add organic solvent

By Soxhlet extraction or Solvent extraction

Concentrate the extract and make upwith organic solvent

PBBs/PBDEs

Analyzed by UV-VIS

Analyzed by GC-MSD

By spot test

Get 50cm2 sample

By boiling water extraction

Metal Polymers / electronics

Negative *2

Confirm the tested samples are totally dissolved

Take sample and immerse into Aqua Regia, start to strip plating layer

Stop the stripping procedure upon color change completely

Take the Aqua solution as plating component and stripped body as substrate component

For non-metal part For metal part

Page 17: resource… · 1 ICP Test Report Certification Packet Company name : Littelfuse, Inc. Product Series: FUSE - BF1 58V Product #: 142.5631.xxx Series Issue Date: August 22, 2012 It

Number : TWNC00241667

Test Conducted

Page 6 of 9 Intertek Testing Services Taiwan Ltd.

8F., No. 423, Ruiguang Rd., Neihu District, Taipei 114, Taiwan, R.O.C. 全國公證檢驗股份有限公司 114 台北市內湖區瑞光路 423 號 8 樓

Tel: (+886-2) 6602-2888.2797-8885 Fax: (+886-2) 6602-2400.6602-2401

(Ⅳ) Measurement Flowchart:

Test for Halogen Content Reference Standard:EN 14582

Add absorbent in a combustion flask & place weighed sample in equipment

Fill oxygen into calorimetric bomb

Ignite then leave the bomb at room temperature

Transfer the absorbent into a volumetric flask

Make up with deionized water

Sampling/grinding or cutting

Analyzed by ion chromatography

Page 18: resource… · 1 ICP Test Report Certification Packet Company name : Littelfuse, Inc. Product Series: FUSE - BF1 58V Product #: 142.5631.xxx Series Issue Date: August 22, 2012 It

Number : TWNC00241667

Test Conducted

Page 7 of 9 Intertek Testing Services Taiwan Ltd.

8F., No. 423, Ruiguang Rd., Neihu District, Taipei 114, Taiwan, R.O.C. 全國公證檢驗股份有限公司 114 台北市內湖區瑞光路 423 號 8 樓

Tel: (+886-2) 6602-2888.2797-8885 Fax: (+886-2) 6602-2400.6602-2401

(Ⅳ) Measurement Flowchart: Test For Phthalates Contents Reference Method: EN 14372: 2004

Sampling/grinding or cutting

Weigh sample and add organic solvent

By solvent extraction

Concentrate the extract and make up with organic solvent

Analyzed by GC-MSD

Page 19: resource… · 1 ICP Test Report Certification Packet Company name : Littelfuse, Inc. Product Series: FUSE - BF1 58V Product #: 142.5631.xxx Series Issue Date: August 22, 2012 It

Number : TWNC00241667

Test Conducted

Page 8 of 9 Intertek Testing Services Taiwan Ltd.

8F., No. 423, Ruiguang Rd., Neihu District, Taipei 114, Taiwan, R.O.C. 全國公證檢驗股份有限公司 114 台北市內湖區瑞光路 423 號 8 樓

Tel: (+886-2) 6602-2888.2797-8885 Fax: (+886-2) 6602-2400.6602-2401

(Ⅳ) Measurement Flowchart:

Test For Hexabromocyclododecane (HBCDD) Reference Standard:USEPA 3540C

End of Report

Sampling/grinding or cutting

Weigh sample and add organic solvent

By soxhlet extraction

Concentrate the extract and make up with organic solvent

Analyzed by GC-MSD

Page 20: resource… · 1 ICP Test Report Certification Packet Company name : Littelfuse, Inc. Product Series: FUSE - BF1 58V Product #: 142.5631.xxx Series Issue Date: August 22, 2012 It

Number : TWNC00241667

Test Conducted

Page 9 of 9 Intertek Testing Services Taiwan Ltd.

8F., No. 423, Ruiguang Rd., Neihu District, Taipei 114, Taiwan, R.O.C. 全國公證檢驗股份有限公司 114 台北市內湖區瑞光路 423 號 8 樓

Tel: (+886-2) 6602-2888.2797-8885 Fax: (+886-2) 6602-2400.6602-2401

Photo

Page 21: resource… · 1 ICP Test Report Certification Packet Company name : Littelfuse, Inc. Product Series: FUSE - BF1 58V Product #: 142.5631.xxx Series Issue Date: August 22, 2012 It

Test Report Number : TWNC00241664

Authorized By: On Behalf Of Intertek Testing Services Taiwan Limited

K. Y. Liang Director

This report shall not be reproduced except in full, without the written approval of the laboratory.

Page 1 of 9 Intertek Testing Services Taiwan Ltd.

8F., No. 423, Ruiguang Rd., Neihu District, Taipei 114, Taiwan, R.O.C. 全國公證檢驗股份有限公司 114台北市內湖區瑞光路 423號 8樓

Tel: (+886-2) 6602-2888.2797-8885 Fax: (+886-2) 6602-2400.6602-2401

Applicant: Littelfuse, S.A. de C.V. Date : Feb 01, 2012 Blvd. Fausto Z. Martinez #1800

Col. Magisterio Seccion 38 C.P. 26070 Piedra Negras, Coahuila, Mexico

Sample Description:

One (1) group of submitted samples said to be : Part Description : HOUSING RED Part Number : 353.2131.4500 Date Sample Received : Jan 20, 2012 Date Test Started : Jan 30, 2012

Test Conducted :

As requested by the applicant, for details please refer to attached pages.

Page 22: resource… · 1 ICP Test Report Certification Packet Company name : Littelfuse, Inc. Product Series: FUSE - BF1 58V Product #: 142.5631.xxx Series Issue Date: August 22, 2012 It

Number : TWNC00241664

Test Conducted

Page 2 of 9 Intertek Testing Services Taiwan Ltd.

8F., No. 423, Ruiguang Rd., Neihu District, Taipei 114, Taiwan, R.O.C. 全國公證檢驗股份有限公司 114台北市內湖區瑞光路 423號 8樓

Tel: (+886-2) 6602-2888.2797-8885 Fax: (+886-2) 6602-2400.6602-2401

(Ⅰ) Test Result Summary : Result (ppm)

Test Item Red Plastic

Heavy Metal

Cadmium (Cd) content ND Lead (Pb) content 7 Mercury (Hg) content ND Chromium VI (Cr6+) content ND

Polybrominated Biphenyls (PBBs) Monobrominated Biphenyls (MonoBB) ND Dibrominated Biphenyls (DiBB) ND Tribrominated Biphenyls (TriBB) ND Tetrabrominated Biphenyls (TetraBB) ND Pentabrominated Biphenyls (PentaBB) ND Hexabrominated Biphenyls (HexaBB) ND Heptabrominated Biphenyls (HeptaBB) ND Octabrominated Biphenyls (OctaBB) ND Nonabrominated Biphenyls (NonaBB) ND Decabrominated Biphenyl (DecaBB) ND

Polybrominated Diphenyl Ethers (PBDEs) Monobrominated Diphenyl Ethers (MonoBDE) ND Dibrominated Diphenyl Ethers (DiBDE) ND Tribrominated Diphenyl Ethers (TriBDE) ND Tetrabrominated Diphenyl Ethers (TetraBDE) ND Pentabrominated Diphenyl Ethers (PentaBDE) ND Hexabrominated Diphenyl Ethers (HexaBDE) ND Heptabrominated Diphenyl Ethers (HeptaBDE) ND Octabrominated Diphenyl Ethers (OctaBDE) ND Nonabrominated Diphenyl Ethers (NonaBDE) ND Decabrominated Diphenyl Ether (DecaBDE) ND

Halogen Content Fluorine (F) ND Chlorine (Cl) ND Bromine (Br) 55745 Iodine (I) ND

Page 23: resource… · 1 ICP Test Report Certification Packet Company name : Littelfuse, Inc. Product Series: FUSE - BF1 58V Product #: 142.5631.xxx Series Issue Date: August 22, 2012 It

Number : TWNC00241664

Test Conducted

Page 3 of 9 Intertek Testing Services Taiwan Ltd.

8F., No. 423, Ruiguang Rd., Neihu District, Taipei 114, Taiwan, R.O.C. 全國公證檢驗股份有限公司 114台北市內湖區瑞光路 423號 8樓

Tel: (+886-2) 6602-2888.2797-8885 Fax: (+886-2) 6602-2400.6602-2401

(Ⅰ) Test Result Summary : Result (ppm)

Test Item Red Plastic

Phthalates Di(2-ethylhexyl) Phthalate (DEHP) ND Dibutyl Phthalate (DBP) ND Benzyl Butyl Phthalate (BBP) ND

Others Hexabromocyclododecane (HBCDD) ND

Remarks: ppm = Parts per million based on weight of tested sample = mg/kg ND = Not detected

Responsibility of Chemist :Irene Chiou / Kevin Liu / Cathy Chen

Date Sample Received : Jan 20, 2012 Test Period : Jan 30, 2012 To Feb 01, 2012

(Ⅱ) RoHS Requirement:

Restricted Substances Limits

Cadmium (Cd) Content 0.01% (100ppm) Lead (Pb) Content 0.1% (1000ppm) Mercury (Hg) Content 0.1% (1000ppm) Chromium VI (Cr6+) Content 0.1% (1000ppm) Polybrominated Biphenyls (PBBs) 0.1% (1000ppm) Polybrominated Diphenyl Ehters (PBDEs) 0.1% (1000ppm)

The above limits were quoted from 2002/95/EC and amendment 2005/618/EC for homogeneous material.

Page 24: resource… · 1 ICP Test Report Certification Packet Company name : Littelfuse, Inc. Product Series: FUSE - BF1 58V Product #: 142.5631.xxx Series Issue Date: August 22, 2012 It

Number : TWNC00241664

Test Conducted

Page 4 of 9 Intertek Testing Services Taiwan Ltd.

8F., No. 423, Ruiguang Rd., Neihu District, Taipei 114, Taiwan, R.O.C. 全國公證檢驗股份有限公司 114台北市內湖區瑞光路 423號 8樓

Tel: (+886-2) 6602-2888.2797-8885 Fax: (+886-2) 6602-2400.6602-2401

(Ⅲ) Test Method: Test Item Test Method Reporting Limit

Cadmium (Cd) content

With reference to IEC 62321 edition 1.0:2008 in clause 8/9/10, by microwave digestion until the tested samples are totally dissolved and determined by ICP-OES.

2 ppm

Lead (Pb) content

With reference to IEC 62321 edition 1.0:2008 in clause 8/9/10, by microwave digestion until the tested samples are totally dissolved and determined by ICP-OES.

2 ppm

Mercury (Hg) content

With reference to IEC 62321 edition 1.0:2008 in clause 7, by microwave digestion until the tested samples are totally dissolved and determined by ICP-OES.

2 ppm

Chromium VI (Cr6+) content

With reference to IEC 62321 edition 1.0:2008 in annex C, by alkaline digestion and determined by UV-Vis spectrophotometer.

1 ppm

Polybrominated Biphenyls (PBBs)

With reference to IEC 62321 edition 1.0:2008 in annex A, by solvent extraction and determined by GC-MS and further HPLC-DAD confirmation when necessary.

5 ppm

Polybrominated Diphenyl Ethers (PBDEs)

With reference to IEC 62321 edition 1.0:2008 in annex A, by solvent extraction and determined by GC-MS and further HPLC-DAD confirmation when necessary.

5 ppm

Halogen Content With reference to EN 14582:2007 by calorimetric bomb with oxygen and determined by Ion Chromatograph.

50 ppm

Phthalates With reference to ASTM D3421-75, by solvent extraction and determined byGC-MSD or GC-FID

10 ppm

Hexabromocyclododecane(HBCDD)

With reference to USEPA 3540C, by solvent extraction and determined byGC-MSD

10 ppm

Remark: Reporting limit = Quantitation limit of analyte in sample

Page 25: resource… · 1 ICP Test Report Certification Packet Company name : Littelfuse, Inc. Product Series: FUSE - BF1 58V Product #: 142.5631.xxx Series Issue Date: August 22, 2012 It

Number : TWNC00241664

Test Conducted

Page 5 of 9 Intertek Testing Services Taiwan Ltd.

8F., No. 423, Ruiguang Rd., Neihu District, Taipei 114, Taiwan, R.O.C. 全國公證檢驗股份有限公司 114台北市內湖區瑞光路 423號 8樓

Tel: (+886-2) 6602-2888.2797-8885 Fax: (+886-2) 6602-2400.6602-2401

(Ⅳ) Measurement Flowchart: Test for Cd/Pb/Hg/Chromium (VI)/PBBS/PBDES Contents Reference Standard: IEC 62321 edition 1.0:2008

Remarks: *1: List of Appropriate Acid:

Material Acid Added for Digestion Polymers HNO3,HCl,HF,H2O2,H3BO3 Metals HNO3,HCl,HF Electronics HNO3,HCl,H2O2,HBF4

*2: If the result of spot test is positive, Chromium VI would be determined as detected.

Sample preparation

For different material, digest the sample with appropriate acid*1

Make up with deionized water

Cd/Pb/Hg

Analyzed by ICP-OES

Weigh sample and add alkaline solution

Definite temp. extraction

Make up with deionized water and add diphenyl-carbazide solution

Cool and filter the extract

Cr6+

Weigh sample and add organic solvent

By Soxhlet extraction or Solvent extraction

Concentrate the extract and make upwith organic solvent

PBBs/PBDEs

Analyzed by UV-VIS

Analyzed by GC-MSD

By spot test

Get 50cm2 sample

By boiling water extraction

Metal Polymers / electronics

Negative *2

Confirm the tested samples are totally dissolved

Take sample and immerse into Aqua Regia, start to strip plating layer

Stop the stripping procedure upon color change completely

Take the Aqua solution as plating component and stripped body as substrate component

For non-metal part For metal part

Page 26: resource… · 1 ICP Test Report Certification Packet Company name : Littelfuse, Inc. Product Series: FUSE - BF1 58V Product #: 142.5631.xxx Series Issue Date: August 22, 2012 It

Number : TWNC00241664

Test Conducted

Page 6 of 9 Intertek Testing Services Taiwan Ltd.

8F., No. 423, Ruiguang Rd., Neihu District, Taipei 114, Taiwan, R.O.C. 全國公證檢驗股份有限公司 114台北市內湖區瑞光路 423號 8樓

Tel: (+886-2) 6602-2888.2797-8885 Fax: (+886-2) 6602-2400.6602-2401

(Ⅳ) Measurement Flowchart:

Test for Halogen Content Reference Standard:EN 14582

Add absorbent in a combustion flask & place weighed sample in equipment

Fill oxygen into calorimetric bomb

Ignite then leave the bomb at room temperature

Transfer the absorbent into a volumetric flask

Make up with deionized water

Sampling/grinding or cutting

Analyzed by ion chromatography

Page 27: resource… · 1 ICP Test Report Certification Packet Company name : Littelfuse, Inc. Product Series: FUSE - BF1 58V Product #: 142.5631.xxx Series Issue Date: August 22, 2012 It

Number : TWNC00241664

Test Conducted

Page 7 of 9 Intertek Testing Services Taiwan Ltd.

8F., No. 423, Ruiguang Rd., Neihu District, Taipei 114, Taiwan, R.O.C. 全國公證檢驗股份有限公司 114台北市內湖區瑞光路 423號 8樓

Tel: (+886-2) 6602-2888.2797-8885 Fax: (+886-2) 6602-2400.6602-2401

(Ⅳ) Measurement Flowchart: Test For Phthalates Contents Reference Method: EN 14372: 2004

Sampling/grinding or cutting

Weigh sample and add organic solvent

By solvent extraction

Concentrate the extract and make up with organic solvent

Analyzed by GC-MSD

Page 28: resource… · 1 ICP Test Report Certification Packet Company name : Littelfuse, Inc. Product Series: FUSE - BF1 58V Product #: 142.5631.xxx Series Issue Date: August 22, 2012 It

Number : TWNC00241664

Test Conducted

Page 8 of 9 Intertek Testing Services Taiwan Ltd.

8F., No. 423, Ruiguang Rd., Neihu District, Taipei 114, Taiwan, R.O.C. 全國公證檢驗股份有限公司 114台北市內湖區瑞光路 423號 8樓

Tel: (+886-2) 6602-2888.2797-8885 Fax: (+886-2) 6602-2400.6602-2401

(Ⅳ) Measurement Flowchart:

Test For Hexabromocyclododecane (HBCDD) Reference Standard:USEPA 3540C

End of Report

Sampling/grinding or cutting

Weigh sample and add organic solvent

By soxhlet extraction

Concentrate the extract and make up with organic solvent

Analyzed by GC-MSD

Page 29: resource… · 1 ICP Test Report Certification Packet Company name : Littelfuse, Inc. Product Series: FUSE - BF1 58V Product #: 142.5631.xxx Series Issue Date: August 22, 2012 It

Number : TWNC00241664

Test Conducted

Page 9 of 9 Intertek Testing Services Taiwan Ltd.

8F., No. 423, Ruiguang Rd., Neihu District, Taipei 114, Taiwan, R.O.C. 全國公證檢驗股份有限公司 114台北市內湖區瑞光路 423號 8樓

Tel: (+886-2) 6602-2888.2797-8885 Fax: (+886-2) 6602-2400.6602-2401

Photo

Page 30: resource… · 1 ICP Test Report Certification Packet Company name : Littelfuse, Inc. Product Series: FUSE - BF1 58V Product #: 142.5631.xxx Series Issue Date: August 22, 2012 It

Test Report Number : TWNC00258321

Authorized By: On Behalf Of Intertek Testing Services Taiwan Limited

K. Y. Liang Director

This report shall not be reproduced except in full, without the written approval of the laboratory.

Page 1 of 9 Intertek Testing Services Taiwan Ltd.

8F., No. 423, Ruiguang Rd., Neihu District, Taipei 114, Taiwan, R.O.C.

全國公證檢驗股份有限公司 114 台北市內湖區瑞光路 423 號 8 樓

Tel: (+886-2) 6602-2888.2797-8885 Fax: (+886-2) 6602-2400.6602-2401

Applicant: Littelfuse, S.A. de C.V. Date : May 29, 2012 Blvd. Fausto Z. Martinez #1800

Col. Magisterio Seccion 38 C.P. 26070 Piedra Negras, Coahuila, Mexico

Sample Description:

One (1) group of submitted samples said to be : Part Description : YELLOW BOTTOM HOUSING Part Number : 353.2131.4600 Date Sample Received : May 17, 2012 Date Test Started : May 19, 2012

Test Conducted :

As requested by the applicant, for details please refer to attached pages.

Page 31: resource… · 1 ICP Test Report Certification Packet Company name : Littelfuse, Inc. Product Series: FUSE - BF1 58V Product #: 142.5631.xxx Series Issue Date: August 22, 2012 It

Number : TWNC00258321

Test Conducted

Page 2 of 9 Intertek Testing Services Taiwan Ltd.

8F., No. 423, Ruiguang Rd., Neihu District, Taipei 114, Taiwan, R.O.C.

全國公證檢驗股份有限公司 114 台北市內湖區瑞光路 423 號 8 樓

Tel: (+886-2) 6602-2888.2797-8885 Fax: (+886-2) 6602-2400.6602-2401

(Ⅰ) Test Result Summary : Result (ppm)

Test Item Yellow Plastic

Heavy Metal

Cadmium (Cd) content ND Lead (Pb) content 15 Mercury (Hg) content ND Chromium VI (Cr6+) content ND

Polybrominated Biphenyls (PBBs) Monobrominated Biphenyls (MonoBB) ND Dibrominated Biphenyls (DiBB) ND Tribrominated Biphenyls (TriBB) ND Tetrabrominated Biphenyls (TetraBB) ND Pentabrominated Biphenyls (PentaBB) ND Hexabrominated Biphenyls (HexaBB) ND Heptabrominated Biphenyls (HeptaBB) ND Octabrominated Biphenyls (OctaBB) ND Nonabrominated Biphenyls (NonaBB) ND Decabrominated Biphenyl (DecaBB) ND

Polybrominated Diphenyl Ethers (PBDEs) Monobrominated Diphenyl Ethers (MonoBDE) ND Dibrominated Diphenyl Ethers (DiBDE) ND Tribrominated Diphenyl Ethers (TriBDE) ND Tetrabrominated Diphenyl Ethers (TetraBDE) ND Pentabrominated Diphenyl Ethers (PentaBDE) ND Hexabrominated Diphenyl Ethers (HexaBDE) ND Heptabrominated Diphenyl Ethers (HeptaBDE) ND Octabrominated Diphenyl Ethers (OctaBDE) ND Nonabrominated Diphenyl Ethers (NonaBDE) ND Decabrominated Diphenyl Ether (DecaBDE) ND

Halogen Content Fluorine (F) 403 Chlorine (Cl) 139 Bromine (Br) 22339 Iodine (I) ND

Z

Page 32: resource… · 1 ICP Test Report Certification Packet Company name : Littelfuse, Inc. Product Series: FUSE - BF1 58V Product #: 142.5631.xxx Series Issue Date: August 22, 2012 It

Number : TWNC00258321

Test Conducted

Page 3 of 9 Intertek Testing Services Taiwan Ltd.

8F., No. 423, Ruiguang Rd., Neihu District, Taipei 114, Taiwan, R.O.C.

全國公證檢驗股份有限公司 114 台北市內湖區瑞光路 423 號 8 樓

Tel: (+886-2) 6602-2888.2797-8885 Fax: (+886-2) 6602-2400.6602-2401

(Ⅰ) Test Result Summary : Result (ppm)

Test Item Yellow Plastic

Phthalates Di(2-ethylhexyl) Phthalate (DEHP) ND Dibutyl Phthalate (DBP) ND Benzyl Butyl Phthalate (BBP) ND

Others Hexabromocyclododecane (HBCDD) ND

Remarks: ppm = Parts per million based on weight of tested sample = mg/kg ND = Not detected

Responsibility of Chemist :Irene Chiou / Kevin Liu / Cathy Chen

Date Sample Received : May 17, 2012 Test Period : May 19, 2012 To May 28, 2012

(Ⅱ) RoHS Requirement:

Restricted Substances Limits

Cadmium (Cd) Content 0.01% (100ppm) Lead (Pb) Content 0.1% (1000ppm) Mercury (Hg) Content 0.1% (1000ppm) Chromium VI (Cr6+) Content 0.1% (1000ppm) Polybrominated Biphenyls (PBBs) 0.1% (1000ppm) Polybrominated Diphenyl Ehters (PBDEs) 0.1% (1000ppm)

The above limits were quoted from 2002/95/EC and amendment 2005/618/EC for homogeneous material.

Z

Page 33: resource… · 1 ICP Test Report Certification Packet Company name : Littelfuse, Inc. Product Series: FUSE - BF1 58V Product #: 142.5631.xxx Series Issue Date: August 22, 2012 It

Number : TWNC00258321

Test Conducted

Page 4 of 9 Intertek Testing Services Taiwan Ltd.

8F., No. 423, Ruiguang Rd., Neihu District, Taipei 114, Taiwan, R.O.C.

全國公證檢驗股份有限公司 114 台北市內湖區瑞光路 423 號 8 樓

Tel: (+886-2) 6602-2888.2797-8885 Fax: (+886-2) 6602-2400.6602-2401

(Ⅲ) Test Method: Test Item Test Method Reporting Limit

Cadmium (Cd) content

With reference to IEC 62321 edition 1.0:2008 in clause 8/9/10, by microwave digestion until the tested samples are totally dissolved and determined by ICP-OES.

2 ppm

Lead (Pb) content

With reference to IEC 62321 edition 1.0:2008 in clause 8/9/10, by microwave digestion until the tested samples are totally dissolved and determined by ICP-OES.

2 ppm

Mercury (Hg) content

With reference to IEC 62321 edition 1.0:2008 in clause 7, by microwave digestion until the tested samples are totally dissolved and determined by ICP-OES.

2 ppm

Chromium VI (Cr6+) content

With reference to IEC 62321 edition 1.0:2008 in annex C, by alkaline digestion and determined by UV-Vis spectrophotometer.

1 ppm

Polybrominated Biphenyls (PBBs)

With reference to IEC 62321 edition 1.0:2008 in annex A, by solvent extraction and determined by GC-MS and further HPLC-DAD confirmation when necessary.

5 ppm

Polybrominated Diphenyl Ethers (PBDEs)

With reference to IEC 62321 edition 1.0:2008 in annex A, by solvent extraction and determined by GC-MS and further HPLC-DAD confirmation when necessary.

5 ppm

Halogen Content With reference to EN 14582:2007 by calorimetric bomb with oxygen and determined by Ion Chromatograph.

50 ppm

Phthalates With reference to EN 14372: 2004, bysolvent extraction and determined byGC-MS.

50 ppm

Hexabromocyclododecane(HBCDD)

With reference to USEPA 3540C, by solvent extraction and determined byGC-MSD.

10 ppm

Remark: Reporting limit = Quantitation limit of analyte in sample

Page 34: resource… · 1 ICP Test Report Certification Packet Company name : Littelfuse, Inc. Product Series: FUSE - BF1 58V Product #: 142.5631.xxx Series Issue Date: August 22, 2012 It

Number : TWNC00258321

Test Conducted

Page 5 of 9 Intertek Testing Services Taiwan Ltd.

8F., No. 423, Ruiguang Rd., Neihu District, Taipei 114, Taiwan, R.O.C.

全國公證檢驗股份有限公司 114 台北市內湖區瑞光路 423 號 8 樓

Tel: (+886-2) 6602-2888.2797-8885 Fax: (+886-2) 6602-2400.6602-2401

(Ⅳ) Measurement Flowchart: Test for Cd/Pb/Hg/Chromium (VI)/PBBS/PBDES Contents Reference Standard: IEC 62321 edition 1.0:2008

Remarks: *1: List of Appropriate Acid:

Material Acid Added for Digestion Polymers HNO3,HCl,HF,H2O2,H3BO3 Metals HNO3,HCl,HF Electronics HNO3,HCl,H2O2,HBF4

*2: If the result of spot test is positive, Chromium VI would be determined as detected.

Sample preparation

For different material, digest the sample with appropriate acid*1

Make up with deionized water

Cd/Pb/Hg

Analyzed by ICP-OES

Weigh sample and add alkaline solution

Definite temp. extraction

Make up with deionized water and add diphenyl-carbazide solution

Cool and filter the extract

Cr6+

Weigh sample and add organic solvent

By Soxhlet extraction or Solvent extraction

Concentrate the extract and make upwith organic solvent

PBBs/PBDEs

Analyzed by UV-VIS

Analyzed by GC-MSD

By spot test

Get 50cm2 sample

By boiling water extraction

Metal Polymers / electronics

Negative *2

Confirm the tested samples are totally dissolved

Take sample and immerse into Aqua Regia, start to strip plating layer

Stop the stripping procedure upon color change completely

Take the Aqua solution as plating component and stripped body as substrate component

For non-metal part For metal part

Page 35: resource… · 1 ICP Test Report Certification Packet Company name : Littelfuse, Inc. Product Series: FUSE - BF1 58V Product #: 142.5631.xxx Series Issue Date: August 22, 2012 It

Number : TWNC00258321

Test Conducted

Page 6 of 9 Intertek Testing Services Taiwan Ltd.

8F., No. 423, Ruiguang Rd., Neihu District, Taipei 114, Taiwan, R.O.C.

全國公證檢驗股份有限公司 114 台北市內湖區瑞光路 423 號 8 樓

Tel: (+886-2) 6602-2888.2797-8885 Fax: (+886-2) 6602-2400.6602-2401

(Ⅳ) Measurement Flowchart:

Test for Halogen Content Reference Standard:EN 14582

Add absorbent in a combustion flask & place weighed sample in equipment

Fill oxygen into calorimetric bomb

Ignite then leave the bomb at room temperature

Transfer the absorbent into a volumetric flask

Make up with deionized water

Sampling/grinding or cutting

Analyzed by ion chromatography

Page 36: resource… · 1 ICP Test Report Certification Packet Company name : Littelfuse, Inc. Product Series: FUSE - BF1 58V Product #: 142.5631.xxx Series Issue Date: August 22, 2012 It

Number : TWNC00258321

Test Conducted

Page 7 of 9 Intertek Testing Services Taiwan Ltd.

8F., No. 423, Ruiguang Rd., Neihu District, Taipei 114, Taiwan, R.O.C.

全國公證檢驗股份有限公司 114 台北市內湖區瑞光路 423 號 8 樓

Tel: (+886-2) 6602-2888.2797-8885 Fax: (+886-2) 6602-2400.6602-2401

(Ⅳ) Measurement Flowchart: Test For Phthalates Contents Reference Method: EN 14372: 2004

Sampling/grinding or cutting

Weigh sample and add organic solvent

By solvent extraction

Concentrate the extract and make up with organic solvent

Analyzed by GC-MSD

Page 37: resource… · 1 ICP Test Report Certification Packet Company name : Littelfuse, Inc. Product Series: FUSE - BF1 58V Product #: 142.5631.xxx Series Issue Date: August 22, 2012 It

Number : TWNC00258321

Test Conducted

Page 8 of 9 Intertek Testing Services Taiwan Ltd.

8F., No. 423, Ruiguang Rd., Neihu District, Taipei 114, Taiwan, R.O.C.

全國公證檢驗股份有限公司 114 台北市內湖區瑞光路 423 號 8 樓

Tel: (+886-2) 6602-2888.2797-8885 Fax: (+886-2) 6602-2400.6602-2401

(Ⅳ) Measurement Flowchart: Test For Hexabromocyclododecane (HBCDD) Reference Standard:USEPA 3540C

End of Report

Sampling/grinding or cutting

Weigh sample and add organic solvent

By soxhlet extraction

Concentrate the extract and make up with organic solvent

Analyzed by GC-MSD

Page 38: resource… · 1 ICP Test Report Certification Packet Company name : Littelfuse, Inc. Product Series: FUSE - BF1 58V Product #: 142.5631.xxx Series Issue Date: August 22, 2012 It

Number : TWNC00258321

Test Conducted

Page 9 of 9 Intertek Testing Services Taiwan Ltd.

8F., No. 423, Ruiguang Rd., Neihu District, Taipei 114, Taiwan, R.O.C.

全國公證檢驗股份有限公司 114 台北市內湖區瑞光路 423 號 8 樓

Tel: (+886-2) 6602-2888.2797-8885 Fax: (+886-2) 6602-2400.6602-2401

Photo

Page 39: resource… · 1 ICP Test Report Certification Packet Company name : Littelfuse, Inc. Product Series: FUSE - BF1 58V Product #: 142.5631.xxx Series Issue Date: August 22, 2012 It

Test Report Number : TWNC00241665

Authorized By: On Behalf Of Intertek Testing Services Taiwan Limited

K. Y. Liang Director

This report shall not be reproduced except in full, without the written approval of the laboratory.

Page 1 of 9 Intertek Testing Services Taiwan Ltd.

8F., No. 423, Ruiguang Rd., Neihu District, Taipei 114, Taiwan, R.O.C. 全國公證檢驗股份有限公司 114台北市內湖區瑞光路 423號 8樓

Tel: (+886-2) 6602-2888.2797-8885 Fax: (+886-2) 6602-2400.6602-2401

Applicant: Littelfuse, S.A. de C.V. Date : Feb 01, 2012 Blvd. Fausto Z. Martinez #1800

Col. Magisterio Seccion 38 C.P. 26070 Piedra Negras, Coahuila, Mexico

Sample Description:

One (1) group of submitted samples said to be : Part Description : HOUSING BROWN Part Number : 353.2131.4700 Date Sample Received : Jan 20, 2012 Date Test Started : Jan 30, 2012

Test Conducted :

As requested by the applicant, for details please refer to attached pages.

Page 40: resource… · 1 ICP Test Report Certification Packet Company name : Littelfuse, Inc. Product Series: FUSE - BF1 58V Product #: 142.5631.xxx Series Issue Date: August 22, 2012 It

Number : TWNC00241665

Test Conducted

Page 2 of 9 Intertek Testing Services Taiwan Ltd.

8F., No. 423, Ruiguang Rd., Neihu District, Taipei 114, Taiwan, R.O.C. 全國公證檢驗股份有限公司 114台北市內湖區瑞光路 423號 8樓

Tel: (+886-2) 6602-2888.2797-8885 Fax: (+886-2) 6602-2400.6602-2401

(Ⅰ) Test Result Summary : Result (ppm)

Test Item Brown Plastic

Heavy Metal

Cadmium (Cd) content ND Lead (Pb) content 17 Mercury (Hg) content ND Chromium VI (Cr6+) content ND

Polybrominated Biphenyls (PBBs) Monobrominated Biphenyls (MonoBB) ND Dibrominated Biphenyls (DiBB) ND Tribrominated Biphenyls (TriBB) ND Tetrabrominated Biphenyls (TetraBB) ND Pentabrominated Biphenyls (PentaBB) ND Hexabrominated Biphenyls (HexaBB) ND Heptabrominated Biphenyls (HeptaBB) ND Octabrominated Biphenyls (OctaBB) ND Nonabrominated Biphenyls (NonaBB) ND Decabrominated Biphenyl (DecaBB) ND

Polybrominated Diphenyl Ethers (PBDEs) Monobrominated Diphenyl Ethers (MonoBDE) ND Dibrominated Diphenyl Ethers (DiBDE) ND Tribrominated Diphenyl Ethers (TriBDE) ND Tetrabrominated Diphenyl Ethers (TetraBDE) ND Pentabrominated Diphenyl Ethers (PentaBDE) ND Hexabrominated Diphenyl Ethers (HexaBDE) ND Heptabrominated Diphenyl Ethers (HeptaBDE) ND Octabrominated Diphenyl Ethers (OctaBDE) ND Nonabrominated Diphenyl Ethers (NonaBDE) ND Decabrominated Diphenyl Ether (DecaBDE) ND

Halogen Content Fluorine (F) ND Chlorine (Cl) ND Bromine (Br) 54767 Iodine (I) ND

Page 41: resource… · 1 ICP Test Report Certification Packet Company name : Littelfuse, Inc. Product Series: FUSE - BF1 58V Product #: 142.5631.xxx Series Issue Date: August 22, 2012 It

Number : TWNC00241665

Test Conducted

Page 3 of 9 Intertek Testing Services Taiwan Ltd.

8F., No. 423, Ruiguang Rd., Neihu District, Taipei 114, Taiwan, R.O.C. 全國公證檢驗股份有限公司 114台北市內湖區瑞光路 423號 8樓

Tel: (+886-2) 6602-2888.2797-8885 Fax: (+886-2) 6602-2400.6602-2401

(Ⅰ) Test Result Summary : Result (ppm)

Test Item Brown Plastic

Phthalates Di(2-ethylhexyl) Phthalate (DEHP) ND Dibutyl Phthalate (DBP) ND Benzyl Butyl Phthalate (BBP) ND

Others Hexabromocyclododecane (HBCDD) ND

Remarks: ppm = Parts per million based on weight of tested sample = mg/kg ND = Not detected

Responsibility of Chemist :Irene Chiou / Kevin Liu / Cathy Chen

Date Sample Received : Jan 20, 2012 Test Period : Jan 30, 2012 To Feb 01, 2012

(Ⅱ) RoHS Requirement:

Restricted Substances Limits

Cadmium (Cd) Content 0.01% (100ppm) Lead (Pb) Content 0.1% (1000ppm) Mercury (Hg) Content 0.1% (1000ppm) Chromium VI (Cr6+) Content 0.1% (1000ppm) Polybrominated Biphenyls (PBBs) 0.1% (1000ppm) Polybrominated Diphenyl Ehters (PBDEs) 0.1% (1000ppm)

The above limits were quoted from 2002/95/EC and amendment 2005/618/EC for homogeneous material.

Page 42: resource… · 1 ICP Test Report Certification Packet Company name : Littelfuse, Inc. Product Series: FUSE - BF1 58V Product #: 142.5631.xxx Series Issue Date: August 22, 2012 It

Number : TWNC00241665

Test Conducted

Page 4 of 9 Intertek Testing Services Taiwan Ltd.

8F., No. 423, Ruiguang Rd., Neihu District, Taipei 114, Taiwan, R.O.C. 全國公證檢驗股份有限公司 114台北市內湖區瑞光路 423號 8樓

Tel: (+886-2) 6602-2888.2797-8885 Fax: (+886-2) 6602-2400.6602-2401

(Ⅲ) Test Method: Test Item Test Method Reporting Limit

Cadmium (Cd) content

With reference to IEC 62321 edition 1.0:2008 in clause 8/9/10, by microwave digestion until the tested samples are totally dissolved and determined by ICP-OES.

2 ppm

Lead (Pb) content

With reference to IEC 62321 edition 1.0:2008 in clause 8/9/10, by microwave digestion until the tested samples are totally dissolved and determined by ICP-OES.

2 ppm

Mercury (Hg) content

With reference to IEC 62321 edition 1.0:2008 in clause 7, by microwave digestion until the tested samples are totally dissolved and determined by ICP-OES.

2 ppm

Chromium VI (Cr6+) content

With reference to IEC 62321 edition 1.0:2008 in annex C, by alkaline digestion and determined by UV-Vis spectrophotometer.

1 ppm

Polybrominated Biphenyls (PBBs)

With reference to IEC 62321 edition 1.0:2008 in annex A, by solvent extraction and determined by GC-MS and further HPLC-DAD confirmation when necessary.

5 ppm

Polybrominated Diphenyl Ethers (PBDEs)

With reference to IEC 62321 edition 1.0:2008 in annex A, by solvent extraction and determined by GC-MS and further HPLC-DAD confirmation when necessary.

5 ppm

Halogen Content With reference to EN 14582:2007 by calorimetric bomb with oxygen and determined by Ion Chromatograph.

50 ppm

Phthalates With reference to ASTM D3421-75, by solvent extraction and determined byGC-MSD or GC-FID

10 ppm

Hexabromocyclododecane(HBCDD)

With reference to USEPA 3540C, by solvent extraction and determined byGC-MSD

10 ppm

Remark: Reporting limit = Quantitation limit of analyte in sample

Page 43: resource… · 1 ICP Test Report Certification Packet Company name : Littelfuse, Inc. Product Series: FUSE - BF1 58V Product #: 142.5631.xxx Series Issue Date: August 22, 2012 It

Number : TWNC00241665

Test Conducted

Page 5 of 9 Intertek Testing Services Taiwan Ltd.

8F., No. 423, Ruiguang Rd., Neihu District, Taipei 114, Taiwan, R.O.C. 全國公證檢驗股份有限公司 114台北市內湖區瑞光路 423號 8樓

Tel: (+886-2) 6602-2888.2797-8885 Fax: (+886-2) 6602-2400.6602-2401

(Ⅳ) Measurement Flowchart: Test for Cd/Pb/Hg/Chromium (VI)/PBBS/PBDES Contents Reference Standard: IEC 62321 edition 1.0:2008

Remarks: *1: List of Appropriate Acid:

Material Acid Added for Digestion Polymers HNO3,HCl,HF,H2O2,H3BO3 Metals HNO3,HCl,HF Electronics HNO3,HCl,H2O2,HBF4

*2: If the result of spot test is positive, Chromium VI would be determined as detected.

Sample preparation

For different material, digest the sample with appropriate acid*1

Make up with deionized water

Cd/Pb/Hg

Analyzed by ICP-OES

Weigh sample and add alkaline solution

Definite temp. extraction

Make up with deionized water and add diphenyl-carbazide solution

Cool and filter the extract

Cr6+

Weigh sample and add organic solvent

By Soxhlet extraction or Solvent extraction

Concentrate the extract and make upwith organic solvent

PBBs/PBDEs

Analyzed by UV-VIS

Analyzed by GC-MSD

By spot test

Get 50cm2 sample

By boiling water extraction

Metal Polymers / electronics

Negative *2

Confirm the tested samples are totally dissolved

Take sample and immerse into Aqua Regia, start to strip plating layer

Stop the stripping procedure upon color change completely

Take the Aqua solution as plating component and stripped body as substrate component

For non-metal part For metal part

Page 44: resource… · 1 ICP Test Report Certification Packet Company name : Littelfuse, Inc. Product Series: FUSE - BF1 58V Product #: 142.5631.xxx Series Issue Date: August 22, 2012 It

Number : TWNC00241665

Test Conducted

Page 6 of 9 Intertek Testing Services Taiwan Ltd.

8F., No. 423, Ruiguang Rd., Neihu District, Taipei 114, Taiwan, R.O.C. 全國公證檢驗股份有限公司 114台北市內湖區瑞光路 423號 8樓

Tel: (+886-2) 6602-2888.2797-8885 Fax: (+886-2) 6602-2400.6602-2401

(Ⅳ) Measurement Flowchart:

Test for Halogen Content Reference Standard:EN 14582

Add absorbent in a combustion flask & place weighed sample in equipment

Fill oxygen into calorimetric bomb

Ignite then leave the bomb at room temperature

Transfer the absorbent into a volumetric flask

Make up with deionized water

Sampling/grinding or cutting

Analyzed by ion chromatography

Page 45: resource… · 1 ICP Test Report Certification Packet Company name : Littelfuse, Inc. Product Series: FUSE - BF1 58V Product #: 142.5631.xxx Series Issue Date: August 22, 2012 It

Number : TWNC00241665

Test Conducted

Page 7 of 9 Intertek Testing Services Taiwan Ltd.

8F., No. 423, Ruiguang Rd., Neihu District, Taipei 114, Taiwan, R.O.C. 全國公證檢驗股份有限公司 114台北市內湖區瑞光路 423號 8樓

Tel: (+886-2) 6602-2888.2797-8885 Fax: (+886-2) 6602-2400.6602-2401

(Ⅳ) Measurement Flowchart: Test For Phthalates Contents Reference Method: EN 14372: 2004

Sampling/grinding or cutting

Weigh sample and add organic solvent

By solvent extraction

Concentrate the extract and make up with organic solvent

Analyzed by GC-MSD

Page 46: resource… · 1 ICP Test Report Certification Packet Company name : Littelfuse, Inc. Product Series: FUSE - BF1 58V Product #: 142.5631.xxx Series Issue Date: August 22, 2012 It

Number : TWNC00241665

Test Conducted

Page 8 of 9 Intertek Testing Services Taiwan Ltd.

8F., No. 423, Ruiguang Rd., Neihu District, Taipei 114, Taiwan, R.O.C. 全國公證檢驗股份有限公司 114台北市內湖區瑞光路 423號 8樓

Tel: (+886-2) 6602-2888.2797-8885 Fax: (+886-2) 6602-2400.6602-2401

(Ⅳ) Measurement Flowchart:

Test For Hexabromocyclododecane (HBCDD) Reference Standard:USEPA 3540C

End of Report

Sampling/grinding or cutting

Weigh sample and add organic solvent

By soxhlet extraction

Concentrate the extract and make up with organic solvent

Analyzed by GC-MSD

Page 47: resource… · 1 ICP Test Report Certification Packet Company name : Littelfuse, Inc. Product Series: FUSE - BF1 58V Product #: 142.5631.xxx Series Issue Date: August 22, 2012 It

Number : TWNC00241665

Test Conducted

Page 9 of 9 Intertek Testing Services Taiwan Ltd.

8F., No. 423, Ruiguang Rd., Neihu District, Taipei 114, Taiwan, R.O.C. 全國公證檢驗股份有限公司 114台北市內湖區瑞光路 423號 8樓

Tel: (+886-2) 6602-2888.2797-8885 Fax: (+886-2) 6602-2400.6602-2401

Photo

Page 48: resource… · 1 ICP Test Report Certification Packet Company name : Littelfuse, Inc. Product Series: FUSE - BF1 58V Product #: 142.5631.xxx Series Issue Date: August 22, 2012 It

Test Report Number : TWNC00258324

Authorized By: On Behalf Of Intertek Testing Services Taiwan Limited

K. Y. Liang Director

This report shall not be reproduced except in full, without the written approval of the laboratory.

Page 1 of 9 Intertek Testing Services Taiwan Ltd.

8F., No. 423, Ruiguang Rd., Neihu District, Taipei 114, Taiwan, R.O.C.

全國公證檢驗股份有限公司 114 台北市內湖區瑞光路 423 號 8 樓

Tel: (+886-2) 6602-2888.2797-8885 Fax: (+886-2) 6602-2400.6602-2401

Applicant: Littelfuse, S.A. de C.V. Date : May 29, 2012 Blvd. Fausto Z. Martinez #1800

Col. Magisterio Seccion 38 C.P. 26070 Piedra Negras, Coahuila, Mexico

Sample Description:

One (1) group of submitted samples said to be : Part Description : WHITE BOTTOM HOUSING Part Number : 353.2131.4800 Date Sample Received : May 17, 2012 Date Test Started : May 19, 2012

Test Conducted :

As requested by the applicant, for details please refer to attached pages.

Page 49: resource… · 1 ICP Test Report Certification Packet Company name : Littelfuse, Inc. Product Series: FUSE - BF1 58V Product #: 142.5631.xxx Series Issue Date: August 22, 2012 It

Number : TWNC00258324

Test Conducted

Page 2 of 9 Intertek Testing Services Taiwan Ltd.

8F., No. 423, Ruiguang Rd., Neihu District, Taipei 114, Taiwan, R.O.C.

全國公證檢驗股份有限公司 114 台北市內湖區瑞光路 423 號 8 樓

Tel: (+886-2) 6602-2888.2797-8885 Fax: (+886-2) 6602-2400.6602-2401

(Ⅰ) Test Result Summary : Result (ppm)

Test Item White Plastic

Heavy Metal

Cadmium (Cd) content ND Lead (Pb) content 15 Mercury (Hg) content ND Chromium VI (Cr6+) content ND

Polybrominated Biphenyls (PBBs) Monobrominated Biphenyls (MonoBB) ND Dibrominated Biphenyls (DiBB) ND Tribrominated Biphenyls (TriBB) ND Tetrabrominated Biphenyls (TetraBB) ND Pentabrominated Biphenyls (PentaBB) ND Hexabrominated Biphenyls (HexaBB) ND Heptabrominated Biphenyls (HeptaBB) ND Octabrominated Biphenyls (OctaBB) ND Nonabrominated Biphenyls (NonaBB) ND Decabrominated Biphenyl (DecaBB) ND

Polybrominated Diphenyl Ethers (PBDEs) Monobrominated Diphenyl Ethers (MonoBDE) ND Dibrominated Diphenyl Ethers (DiBDE) ND Tribrominated Diphenyl Ethers (TriBDE) ND Tetrabrominated Diphenyl Ethers (TetraBDE) ND Pentabrominated Diphenyl Ethers (PentaBDE) ND Hexabrominated Diphenyl Ethers (HexaBDE) ND Heptabrominated Diphenyl Ethers (HeptaBDE) ND Octabrominated Diphenyl Ethers (OctaBDE) ND Nonabrominated Diphenyl Ethers (NonaBDE) ND Decabrominated Diphenyl Ether (DecaBDE) ND

Halogen Content Fluorine (F) 248 Chlorine (Cl) 149 Bromine (Br) 25496 Iodine (I) ND

Z

Page 50: resource… · 1 ICP Test Report Certification Packet Company name : Littelfuse, Inc. Product Series: FUSE - BF1 58V Product #: 142.5631.xxx Series Issue Date: August 22, 2012 It

Number : TWNC00258324

Test Conducted

Page 3 of 9 Intertek Testing Services Taiwan Ltd.

8F., No. 423, Ruiguang Rd., Neihu District, Taipei 114, Taiwan, R.O.C.

全國公證檢驗股份有限公司 114 台北市內湖區瑞光路 423 號 8 樓

Tel: (+886-2) 6602-2888.2797-8885 Fax: (+886-2) 6602-2400.6602-2401

(Ⅰ) Test Result Summary : Result (ppm)

Test Item White Plastic

Phthalates Di(2-ethylhexyl) Phthalate (DEHP) ND Dibutyl Phthalate (DBP) ND Benzyl Butyl Phthalate (BBP) ND

Others Hexabromocyclododecane (HBCDD) ND

Remarks: ppm = Parts per million based on weight of tested sample = mg/kg ND = Not detected

Responsibility of Chemist :Irene Chiou / Kevin Liu / Cathy Chen

Date Sample Received : May 17, 2012 Test Period : May 19, 2012 To May 28, 2012

(Ⅱ) RoHS Requirement:

Restricted Substances Limits

Cadmium (Cd) Content 0.01% (100ppm) Lead (Pb) Content 0.1% (1000ppm) Mercury (Hg) Content 0.1% (1000ppm) Chromium VI (Cr6+) Content 0.1% (1000ppm) Polybrominated Biphenyls (PBBs) 0.1% (1000ppm) Polybrominated Diphenyl Ehters (PBDEs) 0.1% (1000ppm)

The above limits were quoted from 2002/95/EC and amendment 2005/618/EC for homogeneous material.

Z

Page 51: resource… · 1 ICP Test Report Certification Packet Company name : Littelfuse, Inc. Product Series: FUSE - BF1 58V Product #: 142.5631.xxx Series Issue Date: August 22, 2012 It

Number : TWNC00258324

Test Conducted

Page 4 of 9 Intertek Testing Services Taiwan Ltd.

8F., No. 423, Ruiguang Rd., Neihu District, Taipei 114, Taiwan, R.O.C.

全國公證檢驗股份有限公司 114 台北市內湖區瑞光路 423 號 8 樓

Tel: (+886-2) 6602-2888.2797-8885 Fax: (+886-2) 6602-2400.6602-2401

(Ⅲ) Test Method: Test Item Test Method Reporting Limit

Cadmium (Cd) content

With reference to IEC 62321 edition 1.0:2008 in clause 8/9/10, by microwave digestion until the tested samples are totally dissolved and determined by ICP-OES.

2 ppm

Lead (Pb) content

With reference to IEC 62321 edition 1.0:2008 in clause 8/9/10, by microwave digestion until the tested samples are totally dissolved and determined by ICP-OES.

2 ppm

Mercury (Hg) content

With reference to IEC 62321 edition 1.0:2008 in clause 7, by microwave digestion until the tested samples are totally dissolved and determined by ICP-OES.

2 ppm

Chromium VI (Cr6+) content

With reference to IEC 62321 edition 1.0:2008 in annex C, by alkaline digestion and determined by UV-Vis spectrophotometer.

1 ppm

Polybrominated Biphenyls (PBBs)

With reference to IEC 62321 edition 1.0:2008 in annex A, by solvent extraction and determined by GC-MS and further HPLC-DAD confirmation when necessary.

5 ppm

Polybrominated Diphenyl Ethers (PBDEs)

With reference to IEC 62321 edition 1.0:2008 in annex A, by solvent extraction and determined by GC-MS and further HPLC-DAD confirmation when necessary.

5 ppm

Halogen Content With reference to EN 14582:2007 by calorimetric bomb with oxygen and determined by Ion Chromatograph.

50 ppm

Phthalates With reference to EN 14372: 2004, bysolvent extraction and determined byGC-MS.

50 ppm

Hexabromocyclododecane(HBCDD)

With reference to USEPA 3540C, by solvent extraction and determined byGC-MSD.

10 ppm

Remark: Reporting limit = Quantitation limit of analyte in sample

Page 52: resource… · 1 ICP Test Report Certification Packet Company name : Littelfuse, Inc. Product Series: FUSE - BF1 58V Product #: 142.5631.xxx Series Issue Date: August 22, 2012 It

Number : TWNC00258324

Test Conducted

Page 5 of 9 Intertek Testing Services Taiwan Ltd.

8F., No. 423, Ruiguang Rd., Neihu District, Taipei 114, Taiwan, R.O.C.

全國公證檢驗股份有限公司 114 台北市內湖區瑞光路 423 號 8 樓

Tel: (+886-2) 6602-2888.2797-8885 Fax: (+886-2) 6602-2400.6602-2401

(Ⅳ) Measurement Flowchart: Test for Cd/Pb/Hg/Chromium (VI)/PBBS/PBDES Contents Reference Standard: IEC 62321 edition 1.0:2008

Remarks: *1: List of Appropriate Acid:

Material Acid Added for Digestion Polymers HNO3,HCl,HF,H2O2,H3BO3 Metals HNO3,HCl,HF Electronics HNO3,HCl,H2O2,HBF4

*2: If the result of spot test is positive, Chromium VI would be determined as detected.

Sample preparation

For different material, digest the sample with appropriate acid*1

Make up with deionized water

Cd/Pb/Hg

Analyzed by ICP-OES

Weigh sample and add alkaline solution

Definite temp. extraction

Make up with deionized water and add diphenyl-carbazide solution

Cool and filter the extract

Cr6+

Weigh sample and add organic solvent

By Soxhlet extraction or Solvent extraction

Concentrate the extract and make upwith organic solvent

PBBs/PBDEs

Analyzed by UV-VIS

Analyzed by GC-MSD

By spot test

Get 50cm2 sample

By boiling water extraction

Metal Polymers / electronics

Negative *2

Confirm the tested samples are totally dissolved

Take sample and immerse into Aqua Regia, start to strip plating layer

Stop the stripping procedure upon color change completely

Take the Aqua solution as plating component and stripped body as substrate component

For non-metal part For metal part

Page 53: resource… · 1 ICP Test Report Certification Packet Company name : Littelfuse, Inc. Product Series: FUSE - BF1 58V Product #: 142.5631.xxx Series Issue Date: August 22, 2012 It

Number : TWNC00258324

Test Conducted

Page 6 of 9 Intertek Testing Services Taiwan Ltd.

8F., No. 423, Ruiguang Rd., Neihu District, Taipei 114, Taiwan, R.O.C.

全國公證檢驗股份有限公司 114 台北市內湖區瑞光路 423 號 8 樓

Tel: (+886-2) 6602-2888.2797-8885 Fax: (+886-2) 6602-2400.6602-2401

(Ⅳ) Measurement Flowchart:

Test for Halogen Content Reference Standard:EN 14582

Add absorbent in a combustion flask & place weighed sample in equipment

Fill oxygen into calorimetric bomb

Ignite then leave the bomb at room temperature

Transfer the absorbent into a volumetric flask

Make up with deionized water

Sampling/grinding or cutting

Analyzed by ion chromatography

Page 54: resource… · 1 ICP Test Report Certification Packet Company name : Littelfuse, Inc. Product Series: FUSE - BF1 58V Product #: 142.5631.xxx Series Issue Date: August 22, 2012 It

Number : TWNC00258324

Test Conducted

Page 7 of 9 Intertek Testing Services Taiwan Ltd.

8F., No. 423, Ruiguang Rd., Neihu District, Taipei 114, Taiwan, R.O.C.

全國公證檢驗股份有限公司 114 台北市內湖區瑞光路 423 號 8 樓

Tel: (+886-2) 6602-2888.2797-8885 Fax: (+886-2) 6602-2400.6602-2401

(Ⅳ) Measurement Flowchart: Test For Phthalates Contents Reference Method: EN 14372: 2004

Sampling/grinding or cutting

Weigh sample and add organic solvent

By solvent extraction

Concentrate the extract and make up with organic solvent

Analyzed by GC-MSD

Page 55: resource… · 1 ICP Test Report Certification Packet Company name : Littelfuse, Inc. Product Series: FUSE - BF1 58V Product #: 142.5631.xxx Series Issue Date: August 22, 2012 It

Number : TWNC00258324

Test Conducted

Page 8 of 9 Intertek Testing Services Taiwan Ltd.

8F., No. 423, Ruiguang Rd., Neihu District, Taipei 114, Taiwan, R.O.C.

全國公證檢驗股份有限公司 114 台北市內湖區瑞光路 423 號 8 樓

Tel: (+886-2) 6602-2888.2797-8885 Fax: (+886-2) 6602-2400.6602-2401

(Ⅳ) Measurement Flowchart: Test For Hexabromocyclododecane (HBCDD) Reference Standard:USEPA 3540C

End of Report

Sampling/grinding or cutting

Weigh sample and add organic solvent

By soxhlet extraction

Concentrate the extract and make up with organic solvent

Analyzed by GC-MSD

Page 56: resource… · 1 ICP Test Report Certification Packet Company name : Littelfuse, Inc. Product Series: FUSE - BF1 58V Product #: 142.5631.xxx Series Issue Date: August 22, 2012 It

Number : TWNC00258324

Test Conducted

Page 9 of 9 Intertek Testing Services Taiwan Ltd.

8F., No. 423, Ruiguang Rd., Neihu District, Taipei 114, Taiwan, R.O.C.

全國公證檢驗股份有限公司 114 台北市內湖區瑞光路 423 號 8 樓

Tel: (+886-2) 6602-2888.2797-8885 Fax: (+886-2) 6602-2400.6602-2401

Photo

Page 57: resource… · 1 ICP Test Report Certification Packet Company name : Littelfuse, Inc. Product Series: FUSE - BF1 58V Product #: 142.5631.xxx Series Issue Date: August 22, 2012 It

Test Report Number : TWNC00234713S1

Authorized By: On Behalf Of Intertek Testing Services Taiwan Limited

K. Y. Liang Director

This report shall not be reproduced except in full, without the written approval of the laboratory.

Page 1 of 9 Intertek Testing Services Taiwan Ltd.

8F., No. 423, Ruiguang Rd., Neihu District, Taipei 114, Taiwan, R.O.C. 全國公證檢驗股份有限公司 114台北市內湖區瑞光路 423號 8樓

Tel: (+886-2) 6602-2888.2797-8885 Fax: (+886-2) 6602-2400.6602-2401

Applicant: Littelfuse, S.A. de C.V. Date : Dec 15, 2011 Blvd. Fausto Z. Martinez #1800

Col. Magisterio Seccion 38 C.P. 26070 Piedra Negras, Coahuila, Mexico

This is to supersede report NO. TWNC00234713 dated Dec 02, 2011

Sample Description:

One (1) group of submitted samples said to be : Part Description : BOTTOM HOUSING BLUE Part Number : 353.2131.5100 Date Sample Received : Nov 28, 2011 Date Test Started : Nov 29, 2011

Test Conducted :

As requested by the applicant, for details please refer to attached pages.

Page 58: resource… · 1 ICP Test Report Certification Packet Company name : Littelfuse, Inc. Product Series: FUSE - BF1 58V Product #: 142.5631.xxx Series Issue Date: August 22, 2012 It

Number : TWNC00234713S1

Test Conducted

Page 2 of 9 Intertek Testing Services Taiwan Ltd.

8F., No. 423, Ruiguang Rd., Neihu District, Taipei 114, Taiwan, R.O.C. 全國公證檢驗股份有限公司 114台北市內湖區瑞光路 423號 8樓

Tel: (+886-2) 6602-2888.2797-8885 Fax: (+886-2) 6602-2400.6602-2401

(Ⅰ) Test Result Summary : Result (ppm)

Test Item Blue Plastic

Heavy Metal

Cadmium (Cd) content ND Lead (Pb) content 22 Mercury (Hg) content ND Chromium VI (Cr6+) content ND

Polybrominated Biphenyls (PBBs) Monobrominated Biphenyls (MonoBB) ND Dibrominated Biphenyls (DiBB) ND Tribrominated Biphenyls (TriBB) ND Tetrabrominated Biphenyls (TetraBB) ND Pentabrominated Biphenyls (PentaBB) ND Hexabrominated Biphenyls (HexaBB) ND Heptabrominated Biphenyls (HeptaBB) ND Octabrominated Biphenyls (OctaBB) ND Nonabrominated Biphenyls (NonaBB) ND Decabrominated Biphenyl (DecaBB) ND

Polybrominated Diphenyl Ethers (PBDEs) Monobrominated Diphenyl Ethers (MonoBDE) ND Dibrominated Diphenyl Ethers (DiBDE) ND Tribrominated Diphenyl Ethers (TriBDE) ND Tetrabrominated Diphenyl Ethers (TetraBDE) ND Pentabrominated Diphenyl Ethers (PentaBDE) ND Hexabrominated Diphenyl Ethers (HexaBDE) ND Heptabrominated Diphenyl Ethers (HeptaBDE) ND Octabrominated Diphenyl Ethers (OctaBDE) ND Nonabrominated Diphenyl Ethers (NonaBDE) ND Decabrominated Diphenyl Ether (DecaBDE) ND

Page 59: resource… · 1 ICP Test Report Certification Packet Company name : Littelfuse, Inc. Product Series: FUSE - BF1 58V Product #: 142.5631.xxx Series Issue Date: August 22, 2012 It

Number : TWNC00234713S1

Test Conducted

Page 3 of 9 Intertek Testing Services Taiwan Ltd.

8F., No. 423, Ruiguang Rd., Neihu District, Taipei 114, Taiwan, R.O.C. 全國公證檢驗股份有限公司 114台北市內湖區瑞光路 423號 8樓

Tel: (+886-2) 6602-2888.2797-8885 Fax: (+886-2) 6602-2400.6602-2401

(Ⅰ) Test Result Summary : Result (ppm)

Test Item Blue Plastic

Halogen Content Fluorine (F) ND Chlorine (Cl) ND Bromine (Br) 50000 Iodine (I) ND

Phthalates Di(2-ethylhexyl) Phthalate (DEHP) ND Dibutyl Phthalate (DBP) ND Benzyl Butyl Phthalate (BBP) ND

Others Hexabromocyclododecane (HBCDD) ND

Remarks: ppm = Parts per million based on weight of tested sample = mg/kg ND = Not detected

Responsibility of Chemist :Irene Chiou / Kevin Liu / Cathy Chen

Date Sample Received : Nov 28, 2011 Test Period : Nov 29, 2011 To Dec 02, 2011

(Ⅱ) RoHS Requirement:

Restricted Substances Limits

Cadmium (Cd) Content 0.01% (100ppm) Lead (Pb) Content 0.1% (1000ppm) Mercury (Hg) Content 0.1% (1000ppm) Chromium VI (Cr6+) Content 0.1% (1000ppm) Polybrominated Biphenyls (PBBs) 0.1% (1000ppm) Polybrominated Diphenyl Ehters (PBDEs) 0.1% (1000ppm)

The above limits were quoted from 2002/95/EC and amendment 2005/618/EC for homogeneous material.

Page 60: resource… · 1 ICP Test Report Certification Packet Company name : Littelfuse, Inc. Product Series: FUSE - BF1 58V Product #: 142.5631.xxx Series Issue Date: August 22, 2012 It

Number : TWNC00234713S1

Test Conducted

Page 4 of 9 Intertek Testing Services Taiwan Ltd.

8F., No. 423, Ruiguang Rd., Neihu District, Taipei 114, Taiwan, R.O.C. 全國公證檢驗股份有限公司 114台北市內湖區瑞光路 423號 8樓

Tel: (+886-2) 6602-2888.2797-8885 Fax: (+886-2) 6602-2400.6602-2401

(Ⅲ) Test Method: Test Item Test Method Reporting Limit

Cadmium (Cd) content

With reference to IEC 62321 edition 1.0:2008 in clause 8/9/10, by microwave digestion until the tested samples are totally dissolved and determined by ICP-OES.

2 ppm

Lead (Pb) content

With reference to IEC 62321 edition 1.0:2008 in clause 8/9/10, by microwave digestion until the tested samples are totally dissolved and determined by ICP-OES.

2 ppm

Mercury (Hg) content

With reference to IEC 62321 edition 1.0:2008 in clause 7, by microwave digestion until the tested samples are totally dissolved and determined by ICP-OES.

2 ppm

Chromium VI (Cr6+) content

With reference to IEC 62321 edition 1.0:2008 in annex C, by alkaline digestion and determined by UV-Vis spectrophotometer.

1 ppm

Polybrominated Biphenyls (PBBs)

With reference to IEC 62321 edition 1.0:2008 in annex A, by solvent extraction and determined by GC-MSD and further HPLC confirmation when necessary.

5 ppm

Polybrominated Diphenyl Ethers (PBDEs)

With reference to IEC 62321 edition 1.0:2008 in annex A, by solvent extraction and determined by GC-MSD and further HPLC confirmation when necessary.

5 ppm

Halogen Content With reference to EN 14582:2007 by calorimetric bomb with oxygen and determined by ion chromatography

50 ppm

Phthalates

With reference to EN14372:2004, by solvent extraction and determined by GC-MSD

10 ppm

Hexabromocyclododecane(HBCDD)

With reference to USEPA 3540C, by solvent extraction and determined by GC-MSD

10 ppm

Remark: Reporting limit = Quantitation limit of analyte in sample

Page 61: resource… · 1 ICP Test Report Certification Packet Company name : Littelfuse, Inc. Product Series: FUSE - BF1 58V Product #: 142.5631.xxx Series Issue Date: August 22, 2012 It

Number : TWNC00234713S1

Test Conducted

Page 5 of 9 Intertek Testing Services Taiwan Ltd.

8F., No. 423, Ruiguang Rd., Neihu District, Taipei 114, Taiwan, R.O.C. 全國公證檢驗股份有限公司 114台北市內湖區瑞光路 423號 8樓

Tel: (+886-2) 6602-2888.2797-8885 Fax: (+886-2) 6602-2400.6602-2401

(Ⅳ) Measurement Flowchart: Test for Cd/Pb/Hg/Chromium (VI)/PBBS/PBDES Contents Reference Standard: IEC 62321 edition 1.0:2008

Remarks: *1: List of Appropriate Acid:

Material Acid Added for Digestion Polymers HNO3,HCl,HF,H2O2,H3BO3 Metals HNO3,HCl,HF Electronics HNO3,HCl,H2O2,HBF4

*2: If the result of spot test is positive, Chromium VI would be determined as detected.

Sample preparation

For different material, digest the sample with appropriate acid*1

Make up with deionized water

Cd/Pb/Hg

Analyzed by ICP-OES

Weigh sample and add alkaline solution

Definite temp. extraction

Make up with deionized water and add diphenyl-carbazide solution

Cool and filter the extract

Cr6+

Weigh sample and add organic solvent

By Soxhlet extraction or Solvent extraction

Concentrate the extract and make upwith organic solvent

PBBs/PBDEs

Analyzed by UV-VIS

Analyzed by GC-MSD

By spot test

Get 50cm2 sample

By boiling water extraction

Metal Polymers / electronics

Negative *2

Confirm the tested samples are totally dissolved

Take sample and immerse into Aqua Regia, start to strip plating layer

Stop the stripping procedure upon color change completely

Take the Aqua solution as plating component and stripped body as substrate component

For non-metal part For metal part

Page 62: resource… · 1 ICP Test Report Certification Packet Company name : Littelfuse, Inc. Product Series: FUSE - BF1 58V Product #: 142.5631.xxx Series Issue Date: August 22, 2012 It

Number : TWNC00234713S1

Test Conducted

Page 6 of 9 Intertek Testing Services Taiwan Ltd.

8F., No. 423, Ruiguang Rd., Neihu District, Taipei 114, Taiwan, R.O.C. 全國公證檢驗股份有限公司 114台北市內湖區瑞光路 423號 8樓

Tel: (+886-2) 6602-2888.2797-8885 Fax: (+886-2) 6602-2400.6602-2401

(Ⅳ) Measurement Flowchart:

Test for Halogen Content Reference Standard:EN 14582

Add absorbent in a combustion flask & place weighed sample in equipment

Fill oxygen into calorimetric bomb

Ignite then leave the flask at room temperature

Transfer the absorbent into a volumetric flask

Make up with deionized water

Sampling/grinding or cutting

Analyzed by ion chromatography

Page 63: resource… · 1 ICP Test Report Certification Packet Company name : Littelfuse, Inc. Product Series: FUSE - BF1 58V Product #: 142.5631.xxx Series Issue Date: August 22, 2012 It

Number : TWNC00234713S1

Test Conducted

Page 7 of 9 Intertek Testing Services Taiwan Ltd.

8F., No. 423, Ruiguang Rd., Neihu District, Taipei 114, Taiwan, R.O.C. 全國公證檢驗股份有限公司 114台北市內湖區瑞光路 423號 8樓

Tel: (+886-2) 6602-2888.2797-8885 Fax: (+886-2) 6602-2400.6602-2401

(Ⅳ) Measurement Flowchart:

Test For Phthalates Contents Reference Method: EN 14372: 2004

Sampling/grinding or cutting

Weigh sample and add organic solvent

By solvent extraction

Concentrate the extract and make up with organic solvent

Analyzed by GC-MSD

Page 64: resource… · 1 ICP Test Report Certification Packet Company name : Littelfuse, Inc. Product Series: FUSE - BF1 58V Product #: 142.5631.xxx Series Issue Date: August 22, 2012 It

Number : TWNC00234713S1

Test Conducted

Page 8 of 9 Intertek Testing Services Taiwan Ltd.

8F., No. 423, Ruiguang Rd., Neihu District, Taipei 114, Taiwan, R.O.C. 全國公證檢驗股份有限公司 114台北市內湖區瑞光路 423號 8樓

Tel: (+886-2) 6602-2888.2797-8885 Fax: (+886-2) 6602-2400.6602-2401

(Ⅳ) Measurement Flowchart:

Test For Hexabromocyclododecane (HBCDD) Reference Standard:USEPA 3540C

End of Report

Sampling/grinding or cutting

Weigh sample and add organic solvent

By soxhlet extraction

Concentrate the extract and make up with organic solvent

Analyzed by GC-MSD

Page 65: resource… · 1 ICP Test Report Certification Packet Company name : Littelfuse, Inc. Product Series: FUSE - BF1 58V Product #: 142.5631.xxx Series Issue Date: August 22, 2012 It

Number : TWNC00234713S1

Test Conducted

Page 9 of 9 Intertek Testing Services Taiwan Ltd.

8F., No. 423, Ruiguang Rd., Neihu District, Taipei 114, Taiwan, R.O.C. 全國公證檢驗股份有限公司 114台北市內湖區瑞光路 423號 8樓

Tel: (+886-2) 6602-2888.2797-8885 Fax: (+886-2) 6602-2400.6602-2401

Photo

Page 66: resource… · 1 ICP Test Report Certification Packet Company name : Littelfuse, Inc. Product Series: FUSE - BF1 58V Product #: 142.5631.xxx Series Issue Date: August 22, 2012 It

Test Report Number : TWNC00241669

Authorized By: On Behalf Of Intertek Testing Services Taiwan Limited

K. Y. Liang Director

This report shall not be reproduced except in full, without the written approval of the laboratory.

Page 1 of 9 Intertek Testing Services Taiwan Ltd.

8F., No. 423, Ruiguang Rd., Neihu District, Taipei 114, Taiwan, R.O.C. 全國公證檢驗股份有限公司 114台北市內湖區瑞光路 423號 8樓

Tel: (+886-2) 6602-2888.2797-8885 Fax: (+886-2) 6602-2400.6602-2401

Applicant: Littelfuse, S.A. de C.V. Date : Feb 01, 2012 Blvd. Fausto Z. Martinez #1800

Col. Magisterio Seccion 38 C.P. 26070 Piedra Negras, Coahuila, Mexico

Sample Description:

One (1) group of submitted samples said to be : Part Description : HOUSING PINK Part Number : 353.2131.5125 Date Sample Received : Jan 20, 2012 Date Test Started : Jan 30, 2012

Test Conducted :

As requested by the applicant, for details please refer to attached pages.

Page 67: resource… · 1 ICP Test Report Certification Packet Company name : Littelfuse, Inc. Product Series: FUSE - BF1 58V Product #: 142.5631.xxx Series Issue Date: August 22, 2012 It

Number : TWNC00241669

Test Conducted

Page 2 of 9 Intertek Testing Services Taiwan Ltd.

8F., No. 423, Ruiguang Rd., Neihu District, Taipei 114, Taiwan, R.O.C. 全國公證檢驗股份有限公司 114台北市內湖區瑞光路 423號 8樓

Tel: (+886-2) 6602-2888.2797-8885 Fax: (+886-2) 6602-2400.6602-2401

(Ⅰ) Test Result Summary : Result (ppm)

Test Item Pink Plastic

Heavy Metal

Cadmium (Cd) content ND Lead (Pb) content 16 Mercury (Hg) content ND Chromium VI (Cr6+) content ND

Polybrominated Biphenyls (PBBs) Monobrominated Biphenyls (MonoBB) ND Dibrominated Biphenyls (DiBB) ND Tribrominated Biphenyls (TriBB) ND Tetrabrominated Biphenyls (TetraBB) ND Pentabrominated Biphenyls (PentaBB) ND Hexabrominated Biphenyls (HexaBB) ND Heptabrominated Biphenyls (HeptaBB) ND Octabrominated Biphenyls (OctaBB) ND Nonabrominated Biphenyls (NonaBB) ND Decabrominated Biphenyl (DecaBB) ND

Polybrominated Diphenyl Ethers (PBDEs) Monobrominated Diphenyl Ethers (MonoBDE) ND Dibrominated Diphenyl Ethers (DiBDE) ND Tribrominated Diphenyl Ethers (TriBDE) ND Tetrabrominated Diphenyl Ethers (TetraBDE) ND Pentabrominated Diphenyl Ethers (PentaBDE) ND Hexabrominated Diphenyl Ethers (HexaBDE) ND Heptabrominated Diphenyl Ethers (HeptaBDE) ND Octabrominated Diphenyl Ethers (OctaBDE) ND Nonabrominated Diphenyl Ethers (NonaBDE) ND Decabrominated Diphenyl Ether (DecaBDE) ND

Halogen Content Fluorine (F) ND Chlorine (Cl) ND Bromine (Br) 54183 Iodine (I) ND

Page 68: resource… · 1 ICP Test Report Certification Packet Company name : Littelfuse, Inc. Product Series: FUSE - BF1 58V Product #: 142.5631.xxx Series Issue Date: August 22, 2012 It

Number : TWNC00241669

Test Conducted

Page 3 of 9 Intertek Testing Services Taiwan Ltd.

8F., No. 423, Ruiguang Rd., Neihu District, Taipei 114, Taiwan, R.O.C. 全國公證檢驗股份有限公司 114台北市內湖區瑞光路 423號 8樓

Tel: (+886-2) 6602-2888.2797-8885 Fax: (+886-2) 6602-2400.6602-2401

(Ⅰ) Test Result Summary : Result (ppm)

Test Item Pink Plastic

Phthalates Di(2-ethylhexyl) Phthalate (DEHP) ND Dibutyl Phthalate (DBP) ND Benzyl Butyl Phthalate (BBP) ND

Others Hexabromocyclododecane (HBCDD) ND

Remarks: ppm = Parts per million based on weight of tested sample = mg/kg ND = Not detected

Responsibility of Chemist :Irene Chiou / Kevin Liu / Cathy Chen

Date Sample Received : Jan 20, 2012 Test Period : Jan 30, 2012 To Feb 01, 2012

(Ⅱ) RoHS Requirement:

Restricted Substances Limits

Cadmium (Cd) Content 0.01% (100ppm) Lead (Pb) Content 0.1% (1000ppm) Mercury (Hg) Content 0.1% (1000ppm) Chromium VI (Cr6+) Content 0.1% (1000ppm) Polybrominated Biphenyls (PBBs) 0.1% (1000ppm) Polybrominated Diphenyl Ehters (PBDEs) 0.1% (1000ppm)

The above limits were quoted from 2002/95/EC and amendment 2005/618/EC for homogeneous material.

Page 69: resource… · 1 ICP Test Report Certification Packet Company name : Littelfuse, Inc. Product Series: FUSE - BF1 58V Product #: 142.5631.xxx Series Issue Date: August 22, 2012 It

Number : TWNC00241669

Test Conducted

Page 4 of 9 Intertek Testing Services Taiwan Ltd.

8F., No. 423, Ruiguang Rd., Neihu District, Taipei 114, Taiwan, R.O.C. 全國公證檢驗股份有限公司 114台北市內湖區瑞光路 423號 8樓

Tel: (+886-2) 6602-2888.2797-8885 Fax: (+886-2) 6602-2400.6602-2401

(Ⅲ) Test Method: Test Item Test Method Reporting Limit

Cadmium (Cd) content

With reference to IEC 62321 edition 1.0:2008 in clause 8/9/10, by microwave digestion until the tested samples are totally dissolved and determined by ICP-OES.

2 ppm

Lead (Pb) content

With reference to IEC 62321 edition 1.0:2008 in clause 8/9/10, by microwave digestion until the tested samples are totally dissolved and determined by ICP-OES.

2 ppm

Mercury (Hg) content

With reference to IEC 62321 edition 1.0:2008 in clause 7, by microwave digestion until the tested samples are totally dissolved and determined by ICP-OES.

2 ppm

Chromium VI (Cr6+) content

With reference to IEC 62321 edition 1.0:2008 in annex C, by alkaline digestion and determined by UV-Vis spectrophotometer.

1 ppm

Polybrominated Biphenyls (PBBs)

With reference to IEC 62321 edition 1.0:2008 in annex A, by solvent extraction and determined by GC-MS and further HPLC-DAD confirmation when necessary.

5 ppm

Polybrominated Diphenyl Ethers (PBDEs)

With reference to IEC 62321 edition 1.0:2008 in annex A, by solvent extraction and determined by GC-MS and further HPLC-DAD confirmation when necessary.

5 ppm

Halogen Content With reference to EN 14582:2007 by calorimetric bomb with oxygen and determined by Ion Chromatograph.

50 ppm

Phthalates With reference to ASTM D3421-75, by solvent extraction and determined byGC-MSD or GC-FID

10 ppm

Hexabromocyclododecane(HBCDD)

With reference to USEPA 3540C, by solvent extraction and determined byGC-MSD

10 ppm

Remark: Reporting limit = Quantitation limit of analyte in sample

Page 70: resource… · 1 ICP Test Report Certification Packet Company name : Littelfuse, Inc. Product Series: FUSE - BF1 58V Product #: 142.5631.xxx Series Issue Date: August 22, 2012 It

Number : TWNC00241669

Test Conducted

Page 5 of 9 Intertek Testing Services Taiwan Ltd.

8F., No. 423, Ruiguang Rd., Neihu District, Taipei 114, Taiwan, R.O.C. 全國公證檢驗股份有限公司 114台北市內湖區瑞光路 423號 8樓

Tel: (+886-2) 6602-2888.2797-8885 Fax: (+886-2) 6602-2400.6602-2401

(Ⅳ) Measurement Flowchart: Test for Cd/Pb/Hg/Chromium (VI)/PBBS/PBDES Contents Reference Standard: IEC 62321 edition 1.0:2008

Remarks: *1: List of Appropriate Acid:

Material Acid Added for Digestion Polymers HNO3,HCl,HF,H2O2,H3BO3 Metals HNO3,HCl,HF Electronics HNO3,HCl,H2O2,HBF4

*2: If the result of spot test is positive, Chromium VI would be determined as detected.

Sample preparation

For different material, digest the sample with appropriate acid*1

Make up with deionized water

Cd/Pb/Hg

Analyzed by ICP-OES

Weigh sample and add alkaline solution

Definite temp. extraction

Make up with deionized water and add diphenyl-carbazide solution

Cool and filter the extract

Cr6+

Weigh sample and add organic solvent

By Soxhlet extraction or Solvent extraction

Concentrate the extract and make upwith organic solvent

PBBs/PBDEs

Analyzed by UV-VIS

Analyzed by GC-MSD

By spot test

Get 50cm2 sample

By boiling water extraction

Metal Polymers / electronics

Negative *2

Confirm the tested samples are totally dissolved

Take sample and immerse into Aqua Regia, start to strip plating layer

Stop the stripping procedure upon color change completely

Take the Aqua solution as plating component and stripped body as substrate component

For non-metal part For metal part

Page 71: resource… · 1 ICP Test Report Certification Packet Company name : Littelfuse, Inc. Product Series: FUSE - BF1 58V Product #: 142.5631.xxx Series Issue Date: August 22, 2012 It

Number : TWNC00241669

Test Conducted

Page 6 of 9 Intertek Testing Services Taiwan Ltd.

8F., No. 423, Ruiguang Rd., Neihu District, Taipei 114, Taiwan, R.O.C. 全國公證檢驗股份有限公司 114台北市內湖區瑞光路 423號 8樓

Tel: (+886-2) 6602-2888.2797-8885 Fax: (+886-2) 6602-2400.6602-2401

(Ⅳ) Measurement Flowchart:

Test for Halogen Content Reference Standard:EN 14582

Add absorbent in a combustion flask & place weighed sample in equipment

Fill oxygen into calorimetric bomb

Ignite then leave the bomb at room temperature

Transfer the absorbent into a volumetric flask

Make up with deionized water

Sampling/grinding or cutting

Analyzed by ion chromatography

Page 72: resource… · 1 ICP Test Report Certification Packet Company name : Littelfuse, Inc. Product Series: FUSE - BF1 58V Product #: 142.5631.xxx Series Issue Date: August 22, 2012 It

Number : TWNC00241669

Test Conducted

Page 7 of 9 Intertek Testing Services Taiwan Ltd.

8F., No. 423, Ruiguang Rd., Neihu District, Taipei 114, Taiwan, R.O.C. 全國公證檢驗股份有限公司 114台北市內湖區瑞光路 423號 8樓

Tel: (+886-2) 6602-2888.2797-8885 Fax: (+886-2) 6602-2400.6602-2401

(Ⅳ) Measurement Flowchart: Test For Phthalates Contents Reference Method: EN 14372: 2004

Sampling/grinding or cutting

Weigh sample and add organic solvent

By solvent extraction

Concentrate the extract and make up with organic solvent

Analyzed by GC-MSD

Page 73: resource… · 1 ICP Test Report Certification Packet Company name : Littelfuse, Inc. Product Series: FUSE - BF1 58V Product #: 142.5631.xxx Series Issue Date: August 22, 2012 It

Number : TWNC00241669

Test Conducted

Page 8 of 9 Intertek Testing Services Taiwan Ltd.

8F., No. 423, Ruiguang Rd., Neihu District, Taipei 114, Taiwan, R.O.C. 全國公證檢驗股份有限公司 114台北市內湖區瑞光路 423號 8樓

Tel: (+886-2) 6602-2888.2797-8885 Fax: (+886-2) 6602-2400.6602-2401

(Ⅳ) Measurement Flowchart:

Test For Hexabromocyclododecane (HBCDD) Reference Standard:USEPA 3540C

End of Report

Sampling/grinding or cutting

Weigh sample and add organic solvent

By soxhlet extraction

Concentrate the extract and make up with organic solvent

Analyzed by GC-MSD

Page 74: resource… · 1 ICP Test Report Certification Packet Company name : Littelfuse, Inc. Product Series: FUSE - BF1 58V Product #: 142.5631.xxx Series Issue Date: August 22, 2012 It

Number : TWNC00241669

Test Conducted

Page 9 of 9 Intertek Testing Services Taiwan Ltd.

8F., No. 423, Ruiguang Rd., Neihu District, Taipei 114, Taiwan, R.O.C. 全國公證檢驗股份有限公司 114台北市內湖區瑞光路 423號 8樓

Tel: (+886-2) 6602-2888.2797-8885 Fax: (+886-2) 6602-2400.6602-2401

Photo

Page 75: resource… · 1 ICP Test Report Certification Packet Company name : Littelfuse, Inc. Product Series: FUSE - BF1 58V Product #: 142.5631.xxx Series Issue Date: August 22, 2012 It

Test Report Number : TWNC00241668

Authorized By: On Behalf Of Intertek Testing Services Taiwan Limited

K. Y. Liang Director

This report shall not be reproduced except in full, without the written approval of the laboratory.

Page 1 of 9 Intertek Testing Services Taiwan Ltd.

8F., No. 423, Ruiguang Rd., Neihu District, Taipei 114, Taiwan, R.O.C. 全國公證檢驗股份有限公司 114台北市內湖區瑞光路 423號 8樓

Tel: (+886-2) 6602-2888.2797-8885 Fax: (+886-2) 6602-2400.6602-2401

Applicant: Littelfuse, S.A. de C.V. Date : Feb 01, 2012 Blvd. Fausto Z. Martinez #1800

Col. Magisterio Seccion 38 C.P. 26070 Piedra Negras, Coahuila, Mexico

Sample Description:

One (1) group of submitted samples said to be : Part Description : HOUSING GRAY Part Number : 353.2131.5150 Date Sample Received : Jan 20, 2012 Date Test Started : Jan 30, 2012

Test Conducted :

As requested by the applicant, for details please refer to attached pages.

Page 76: resource… · 1 ICP Test Report Certification Packet Company name : Littelfuse, Inc. Product Series: FUSE - BF1 58V Product #: 142.5631.xxx Series Issue Date: August 22, 2012 It

Number : TWNC00241668

Test Conducted

Page 2 of 9 Intertek Testing Services Taiwan Ltd.

8F., No. 423, Ruiguang Rd., Neihu District, Taipei 114, Taiwan, R.O.C. 全國公證檢驗股份有限公司 114台北市內湖區瑞光路 423號 8樓

Tel: (+886-2) 6602-2888.2797-8885 Fax: (+886-2) 6602-2400.6602-2401

(Ⅰ) Test Result Summary : Result (ppm)

Test Item Grey Plastic

Heavy Metal

Cadmium (Cd) content ND Lead (Pb) content 19 Mercury (Hg) content ND Chromium VI (Cr6+) content ND

Polybrominated Biphenyls (PBBs) Monobrominated Biphenyls (MonoBB) ND Dibrominated Biphenyls (DiBB) ND Tribrominated Biphenyls (TriBB) ND Tetrabrominated Biphenyls (TetraBB) ND Pentabrominated Biphenyls (PentaBB) ND Hexabrominated Biphenyls (HexaBB) ND Heptabrominated Biphenyls (HeptaBB) ND Octabrominated Biphenyls (OctaBB) ND Nonabrominated Biphenyls (NonaBB) ND Decabrominated Biphenyl (DecaBB) ND

Polybrominated Diphenyl Ethers (PBDEs) Monobrominated Diphenyl Ethers (MonoBDE) ND Dibrominated Diphenyl Ethers (DiBDE) ND Tribrominated Diphenyl Ethers (TriBDE) ND Tetrabrominated Diphenyl Ethers (TetraBDE) ND Pentabrominated Diphenyl Ethers (PentaBDE) ND Hexabrominated Diphenyl Ethers (HexaBDE) ND Heptabrominated Diphenyl Ethers (HeptaBDE) ND Octabrominated Diphenyl Ethers (OctaBDE) ND Nonabrominated Diphenyl Ethers (NonaBDE) ND Decabrominated Diphenyl Ether (DecaBDE) ND

Halogen Content Fluorine (F) ND Chlorine (Cl) ND Bromine (Br) 59698 Iodine (I) ND

Page 77: resource… · 1 ICP Test Report Certification Packet Company name : Littelfuse, Inc. Product Series: FUSE - BF1 58V Product #: 142.5631.xxx Series Issue Date: August 22, 2012 It

Number : TWNC00241668

Test Conducted

Page 3 of 9 Intertek Testing Services Taiwan Ltd.

8F., No. 423, Ruiguang Rd., Neihu District, Taipei 114, Taiwan, R.O.C. 全國公證檢驗股份有限公司 114台北市內湖區瑞光路 423號 8樓

Tel: (+886-2) 6602-2888.2797-8885 Fax: (+886-2) 6602-2400.6602-2401

(Ⅰ) Test Result Summary : Result (ppm)

Test Item Grey Plastic

Phthalates Di(2-ethylhexyl) Phthalate (DEHP) ND Dibutyl Phthalate (DBP) ND Benzyl Butyl Phthalate (BBP) ND

Others Hexabromocyclododecane (HBCDD) ND

Remarks: ppm = Parts per million based on weight of tested sample = mg/kg ND = Not detected

Responsibility of Chemist :Irene Chiou / Kevin Liu / Cathy Chen

Date Sample Received : Jan 20, 2012 Test Period : Jan 30, 2012 To Feb 01, 2012

(Ⅱ) RoHS Requirement:

Restricted Substances Limits

Cadmium (Cd) Content 0.01% (100ppm) Lead (Pb) Content 0.1% (1000ppm) Mercury (Hg) Content 0.1% (1000ppm) Chromium VI (Cr6+) Content 0.1% (1000ppm) Polybrominated Biphenyls (PBBs) 0.1% (1000ppm) Polybrominated Diphenyl Ehters (PBDEs) 0.1% (1000ppm)

The above limits were quoted from 2002/95/EC and amendment 2005/618/EC for homogeneous material.

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Number : TWNC00241668

Test Conducted

Page 4 of 9 Intertek Testing Services Taiwan Ltd.

8F., No. 423, Ruiguang Rd., Neihu District, Taipei 114, Taiwan, R.O.C. 全國公證檢驗股份有限公司 114台北市內湖區瑞光路 423號 8樓

Tel: (+886-2) 6602-2888.2797-8885 Fax: (+886-2) 6602-2400.6602-2401

(Ⅲ) Test Method: Test Item Test Method Reporting Limit

Cadmium (Cd) content

With reference to IEC 62321 edition 1.0:2008 in clause 8/9/10, by microwave digestion until the tested samples are totally dissolved and determined by ICP-OES.

2 ppm

Lead (Pb) content

With reference to IEC 62321 edition 1.0:2008 in clause 8/9/10, by microwave digestion until the tested samples are totally dissolved and determined by ICP-OES.

2 ppm

Mercury (Hg) content

With reference to IEC 62321 edition 1.0:2008 in clause 7, by microwave digestion until the tested samples are totally dissolved and determined by ICP-OES.

2 ppm

Chromium VI (Cr6+) content

With reference to IEC 62321 edition 1.0:2008 in annex C, by alkaline digestion and determined by UV-Vis spectrophotometer.

1 ppm

Polybrominated Biphenyls (PBBs)

With reference to IEC 62321 edition 1.0:2008 in annex A, by solvent extraction and determined by GC-MS and further HPLC-DAD confirmation when necessary.

5 ppm

Polybrominated Diphenyl Ethers (PBDEs)

With reference to IEC 62321 edition 1.0:2008 in annex A, by solvent extraction and determined by GC-MS and further HPLC-DAD confirmation when necessary.

5 ppm

Halogen Content With reference to EN 14582:2007 by calorimetric bomb with oxygen and determined by Ion Chromatograph.

50 ppm

Phthalates With reference to ASTM D3421-75, by solvent extraction and determined byGC-MSD or GC-FID

10 ppm

Hexabromocyclododecane(HBCDD)

With reference to USEPA 3540C, by solvent extraction and determined byGC-MSD

10 ppm

Remark: Reporting limit = Quantitation limit of analyte in sample

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Number : TWNC00241668

Test Conducted

Page 5 of 9 Intertek Testing Services Taiwan Ltd.

8F., No. 423, Ruiguang Rd., Neihu District, Taipei 114, Taiwan, R.O.C. 全國公證檢驗股份有限公司 114台北市內湖區瑞光路 423號 8樓

Tel: (+886-2) 6602-2888.2797-8885 Fax: (+886-2) 6602-2400.6602-2401

(Ⅳ) Measurement Flowchart: Test for Cd/Pb/Hg/Chromium (VI)/PBBS/PBDES Contents Reference Standard: IEC 62321 edition 1.0:2008

Remarks: *1: List of Appropriate Acid:

Material Acid Added for Digestion Polymers HNO3,HCl,HF,H2O2,H3BO3 Metals HNO3,HCl,HF Electronics HNO3,HCl,H2O2,HBF4

*2: If the result of spot test is positive, Chromium VI would be determined as detected.

Sample preparation

For different material, digest the sample with appropriate acid*1

Make up with deionized water

Cd/Pb/Hg

Analyzed by ICP-OES

Weigh sample and add alkaline solution

Definite temp. extraction

Make up with deionized water and add diphenyl-carbazide solution

Cool and filter the extract

Cr6+

Weigh sample and add organic solvent

By Soxhlet extraction or Solvent extraction

Concentrate the extract and make upwith organic solvent

PBBs/PBDEs

Analyzed by UV-VIS

Analyzed by GC-MSD

By spot test

Get 50cm2 sample

By boiling water extraction

Metal Polymers / electronics

Negative *2

Confirm the tested samples are totally dissolved

Take sample and immerse into Aqua Regia, start to strip plating layer

Stop the stripping procedure upon color change completely

Take the Aqua solution as plating component and stripped body as substrate component

For non-metal part For metal part

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Number : TWNC00241668

Test Conducted

Page 6 of 9 Intertek Testing Services Taiwan Ltd.

8F., No. 423, Ruiguang Rd., Neihu District, Taipei 114, Taiwan, R.O.C. 全國公證檢驗股份有限公司 114台北市內湖區瑞光路 423號 8樓

Tel: (+886-2) 6602-2888.2797-8885 Fax: (+886-2) 6602-2400.6602-2401

(Ⅳ) Measurement Flowchart:

Test for Halogen Content Reference Standard:EN 14582

Add absorbent in a combustion flask & place weighed sample in equipment

Fill oxygen into calorimetric bomb

Ignite then leave the bomb at room temperature

Transfer the absorbent into a volumetric flask

Make up with deionized water

Sampling/grinding or cutting

Analyzed by ion chromatography

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Number : TWNC00241668

Test Conducted

Page 7 of 9 Intertek Testing Services Taiwan Ltd.

8F., No. 423, Ruiguang Rd., Neihu District, Taipei 114, Taiwan, R.O.C. 全國公證檢驗股份有限公司 114台北市內湖區瑞光路 423號 8樓

Tel: (+886-2) 6602-2888.2797-8885 Fax: (+886-2) 6602-2400.6602-2401

(Ⅳ) Measurement Flowchart: Test For Phthalates Contents Reference Method: EN 14372: 2004

Sampling/grinding or cutting

Weigh sample and add organic solvent

By solvent extraction

Concentrate the extract and make up with organic solvent

Analyzed by GC-MSD

Page 82: resource… · 1 ICP Test Report Certification Packet Company name : Littelfuse, Inc. Product Series: FUSE - BF1 58V Product #: 142.5631.xxx Series Issue Date: August 22, 2012 It

Number : TWNC00241668

Test Conducted

Page 8 of 9 Intertek Testing Services Taiwan Ltd.

8F., No. 423, Ruiguang Rd., Neihu District, Taipei 114, Taiwan, R.O.C. 全國公證檢驗股份有限公司 114台北市內湖區瑞光路 423號 8樓

Tel: (+886-2) 6602-2888.2797-8885 Fax: (+886-2) 6602-2400.6602-2401

(Ⅳ) Measurement Flowchart:

Test For Hexabromocyclododecane (HBCDD) Reference Standard:USEPA 3540C

End of Report

Sampling/grinding or cutting

Weigh sample and add organic solvent

By soxhlet extraction

Concentrate the extract and make up with organic solvent

Analyzed by GC-MSD

Page 83: resource… · 1 ICP Test Report Certification Packet Company name : Littelfuse, Inc. Product Series: FUSE - BF1 58V Product #: 142.5631.xxx Series Issue Date: August 22, 2012 It

Number : TWNC00241668

Test Conducted

Page 9 of 9 Intertek Testing Services Taiwan Ltd.

8F., No. 423, Ruiguang Rd., Neihu District, Taipei 114, Taiwan, R.O.C. 全國公證檢驗股份有限公司 114台北市內湖區瑞光路 423號 8樓

Tel: (+886-2) 6602-2888.2797-8885 Fax: (+886-2) 6602-2400.6602-2401

Photo

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Report No.: MX11-0928-03 Date:2011-06-16

It is prohibited the total or partial reproduction of this document, as well as any modification or alteration in no of its parts without the previous authorization of Intertek Testing

Services de México, S.A. de C.V. On the contrary Intertek reserves the right of coming from legal form against that (it is) they are responsible (s). The results that appear in this report belong solely to (s) shows (s) analyzed (s).

1ª. Emisión Junio 2005, 1° Revisión Junio 26, 2009. ILTA/003/GENS-F8

Intertek Testing Services de México, S.A. de C.V. Poniente 134 No. 660, Col. Industrial Vallejo

C.P. 02300, Del. Azcapotzalco, México, D.F. Tel.: 50912150 www.intertek.com

TEST REPORT

APPLICANT Littelfuse, S.A. de C.V. Blvd. Fausto Z. Martínez 1800, Col. Magisterio Sección 38, Piedras Negras, Coahuila Ing. María Valdez SAMPLE DESCRIPTION

One (1) group of submitted samples said to be : Sample Description NP Item No. 3) Element Sn Plated Copper N/P 353.1119.4043 Country of Origin NP Buyer's Name NP Supplier's Name NP Date sample received 2011-05-05 Testing period 2011-05-09 to 2011-05-13 ******************************************************************************************** TEST CONDUCTED

As requested by the applicant, for details please refer to attached pages. ********************************************************************************************

CONCLUSION

Sample Number Testing item Conclusion Failed component Failed result

3 (Base)

Element Sn Plated Copper N/P 353.1119.4043

Pass See Result summary

--- ---

3 (Plated)

Element Sn Plated Copper N/P 353.1119.4043

Pass See Result summary

--- ---

********************************************************************************************

TEST CONDUCTED

Samples:

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Report No.: MX11-0928-03 Date:2011-06-16

It is prohibited the total or partial reproduction of this document, as well as any modification or alteration in no of its parts without the previous authorization of Intertek Testing

Services de México, S.A. de C.V. On the contrary Intertek reserves the right of coming from legal form against that (it is) they are responsible (s). The results that appear in this report belong solely to (s) shows (s) analyzed (s).

1ª. Emisión Junio 2005, 1° Revisión Junio 26, 2009. ILTA/003/GENS-F8

Intertek Testing Services de México, S.A. de C.V. Poniente 134 No. 660, Col. Industrial Vallejo

C.P. 02300, Del. Azcapotzalco, México, D.F. Tel.: 50912150 www.intertek.com

3) Base Element Sn Plated Copper N/P 353.1119.4043 3) Plated Element Sn Plated Copper N/P 353.1119.4043 TEST RESULT SUMMARY FOR RoHS DIRECTIVE :

TESTING ITEM Ω RESULT (ppm)

Limit (3) Base

(3) Plated

Cadmium (Cd) content ND ND 0,01% (100 ppm)

Lead (Pb) content 36,10 148,1 0,1% (1000 ppm)

Mercury (Hg) content ND ND 0,1% (1000 ppm)

Chromium (VI) (Cr6+) ND ND 0,1% (1000 ppm)

ppm = parts per million based on dry weight of sample. µg/cm2 = microgram per square centimeter. mg/kg WITH 50cm2 = milligram per kilogram with 50 square centimeter. < = less than. ND = Not detected. The above limits were quoted from 2002/95/EC and amendment 2005/618/EC for homogeneous material. These Accreditations only apply for the methods listed in such. Not accredited under EMA Ω.

Prepared and checked by: For Intertek Laboratory Manager

The Official Mexican Standard NOM-008-SCFI-1993 establishes like separator decimal the comma (,).

NOTE : DecaBDE IN POLYMERIC APPLICATIONS IS EXEMPTED ACCORDING TO ROHS DIRECTIVE AMENDMENT 2005/717/EC.

# =ACCORDING TO IEC 62321, A POSITIVE RESULT INDICATES THE PRESENCE OF Cr(VI) COATING. IT IS THE Cr(VI) CONCENTRATION DETECTED IN THE BOILING-WATER-EXTRACTION SOLUTION AND SHOULD NOT BE INTERPRETED AS THE Cr(VI) CONCENTRATION IN THE COATING LAYER OF THE SAMPLE. REMARK : AS REQUESTED BY THE APPLICANT, COATING WITH BASE MATERIAL OF TESTED COMPONENTS OF THE SAMPLE MX11-0928-03 WERE TESTED SEPARATED. Test method:

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Report No.: MX11-0928-03 Date:2011-06-16

It is prohibited the total or partial reproduction of this document, as well as any modification or alteration in no of its parts without the previous authorization of Intertek Testing

Services de México, S.A. de C.V. On the contrary Intertek reserves the right of coming from legal form against that (it is) they are responsible (s). The results that appear in this report belong solely to (s) shows (s) analyzed (s).

1ª. Emisión Junio 2005, 1° Revisión Junio 26, 2009. ILTA/003/GENS-F8

Intertek Testing Services de México, S.A. de C.V. Poniente 134 No. 660, Col. Industrial Vallejo

C.P. 02300, Del. Azcapotzalco, México, D.F. Tel.: 50912150 www.intertek.com

Sample Number Testing item Ω Testing method

Quality control Batch:

Analysis Date:

Analyzed By:

Reporting limit ppm

3 Chromium VI (Cr6+) content

With reference to USEPA 3060, by EPA 7196

QHU2010-61p73 2011-05-13 MELA 20,0

Sample Number Testing item Ω Testing method

Quality control Batch:

Analysis Date:

Analyzed By:

Reporting limit ppm

3 (Base) Lead (Pb) content With reference to USEPA 3050MOD, by EPA 6010 MET2010-40p129 2011-05-11 MARY 5,0 3 (Plated) Lead (Pb) content With reference to USEPA 3050MOD, by EPA 6010 MET2010-40p129 2011-05-11 MARY 50,0

Sample Number Testing item Ω Testing method

Quality control Batch:

Analysis Date:

Analyzed By:

Reporting limit ppm

3 (Base) Cadmium (Cd) content With reference to USEPA 3050MOD, by EPA 6010 MET2010-40p129 2011-05-11 MARY 2,0 3 (Plated) Cadmium (Cd) content With reference to USEPA 3050MOD, by EPA 6010 MET2010-40p129 2011-05-11 MARY 20,0

Sample Number Testing item Ω Testing method

Quality control Batch:

Analysis Date:

Analyzed By:

Reporting limit ppm

3 (Base) Mercury (Hg) content With reference to USEPA 7471 by USEPA 7471 MET2010-40p126 2011-05-10 RNC 0,25 3 (Plated) Mercury (Hg) content With reference to USEPA 7471 by USEPA 7471 MET2010-40p126 2011-05-10 RNC 2,5

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Report No.: MX11-0928-05 Date:2011-06-16

It is prohibited the total or partial reproduction of this document, as well as any modification or alteration in no of its parts without the previous authorization of Intertek Testing

Services de México, S.A. de C.V. On the contrary Intertek reserves the right of coming from legal form against that (it is) they are responsible (s). The results that appear in this report belong solely to (s) shows (s) analyzed (s).

1ª. Emisión Junio 2005, 1° Revisión Junio 26, 2009. ILTA/003/GENS-F8

Intertek Testing Services de México, S.A. de C.V. Poniente 134 No. 660, Col. Industrial Vallejo

C.P. 02300, Del. Azcapotzalco, México, D.F. Tel.: 50912150 www.intertek.com

TEST REPORT

APPLICANT Littelfuse, S.A. de C.V. Blvd. Fausto Z. Martínez 1800, Col. Magisterio Sección 38, Piedras Negras, Coahuila Ing. María Valdez SAMPLE DESCRIPTION

One (1) group of submitted samples said to be : Sample Description NP Item No. 5) N/P 353.1126.4043 Country of Origin NP Buyer's Name NP Supplier's Name NP Date sample received 2011-05-05 Testing period 2011-05-09 to 2011-05-13 ******************************************************************************************** TEST CONDUCTED

As requested by the applicant, for details please refer to attached pages. ********************************************************************************************

CONCLUSION

Sample Number Testing item Conclusion Failed component Failed result

5 (Base)

N/P 353.1126.4043 Pass

See Result summary --- ---

5 (Plated)

N/P 353.1126.4043 Pass

See Result summary --- ---

********************************************************************************************

TEST CONDUCTED

Samples:

Page 88: resource… · 1 ICP Test Report Certification Packet Company name : Littelfuse, Inc. Product Series: FUSE - BF1 58V Product #: 142.5631.xxx Series Issue Date: August 22, 2012 It

Report No.: MX11-0928-05 Date:2011-06-16

It is prohibited the total or partial reproduction of this document, as well as any modification or alteration in no of its parts without the previous authorization of Intertek Testing

Services de México, S.A. de C.V. On the contrary Intertek reserves the right of coming from legal form against that (it is) they are responsible (s). The results that appear in this report belong solely to (s) shows (s) analyzed (s).

1ª. Emisión Junio 2005, 1° Revisión Junio 26, 2009. ILTA/003/GENS-F8

Intertek Testing Services de México, S.A. de C.V. Poniente 134 No. 660, Col. Industrial Vallejo

C.P. 02300, Del. Azcapotzalco, México, D.F. Tel.: 50912150 www.intertek.com

5) Base N/P 353.1126.4043 5) Plated N/P 353.1126.4043 TEST RESULT SUMMARY FOR RoHS DIRECTIVE :

TESTING ITEM Ω RESULT (ppm)

Limit (5) Base

(5) Plated

Cadmium (Cd) content ND ND 0,01% (100 ppm)

Lead (Pb) content 61,51 ND 0,1% (1000 ppm)

Mercury (Hg) content ND ND 0,1% (1000 ppm)

Chromium (VI) (Cr6+) ND ND 0,1% (1000 ppm)

ppm = parts per million based on dry weight of sample. µg/cm2 = microgram per square centimeter. mg/kg WITH 50cm2 = milligram per kilogram with 50 square centimeter. < = less than. ND = Not detected. The above limits were quoted from 2002/95/EC and amendment 2005/618/EC for homogeneous material. These Accreditations only apply for the methods listed in such. Not accredited under EMA Ω.

Prepared and checked by: For Intertek Laboratory Manager

The Official Mexican Standard NOM-008-SCFI-1993 establishes like separator decimal the comma (,).

NOTE : DecaBDE IN POLYMERIC APPLICATIONS IS EXEMPTED ACCORDING TO ROHS DIRECTIVE AMENDMENT 2005/717/EC.

# =ACCORDING TO IEC 62321, A POSITIVE RESULT INDICATES THE PRESENCE OF Cr(VI) COATING. IT IS THE Cr(VI) CONCENTRATION DETECTED IN THE BOILING-WATER-EXTRACTION SOLUTION AND SHOULD NOT BE INTERPRETED AS THE Cr(VI) CONCENTRATION IN THE COATING LAYER OF THE SAMPLE. REMARK : AS REQUESTED BY THE APPLICANT, COATING WITH BASE MATERIAL OF TESTED COMPONENTS OF THE SAMPLE MX11-0928-05 WERE TESTED SEPARATED. Test method:

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Report No.: MX11-0928-05 Date:2011-06-16

It is prohibited the total or partial reproduction of this document, as well as any modification or alteration in no of its parts without the previous authorization of Intertek Testing

Services de México, S.A. de C.V. On the contrary Intertek reserves the right of coming from legal form against that (it is) they are responsible (s). The results that appear in this report belong solely to (s) shows (s) analyzed (s).

1ª. Emisión Junio 2005, 1° Revisión Junio 26, 2009. ILTA/003/GENS-F8

Intertek Testing Services de México, S.A. de C.V. Poniente 134 No. 660, Col. Industrial Vallejo

C.P. 02300, Del. Azcapotzalco, México, D.F. Tel.: 50912150 www.intertek.com

Sample Number Testing item Ω Testing method

Quality control Batch:

Analysis Date:

Analyzed By:

Reporting limit ppm

5 Chromium VI (Cr6+) content

With reference to USEPA 3060, by EPA 7196

QHU2010-61p73 2011-05-13 MELA 20,0

Sample Number Testing item Ω Testing method

Quality control Batch:

Analysis Date:

Analyzed By:

Reporting limit ppm

5 (Base) Lead (Pb) content With reference to USEPA 3050MOD, by EPA 6010 MET2010-40p129 2011-05-11 MARY 5,0 5 (Plated) Lead (Pb) content With reference to USEPA 3050MOD, by EPA 6010 MET2010-40p129 2011-05-11 MARY 41,67

Sample Number Testing item Ω Testing method

Quality control Batch:

Analysis Date:

Analyzed By:

Reporting limit ppm

5 (Base) Cadmium (Cd) content With reference to USEPA 3050MOD, by EPA 6010 MET2010-40p129 2011-05-11 MARY 2,0 5 (Plated) Cadmium (Cd) content With reference to USEPA 3050MOD, by EPA 6010 MET2010-40p129 2011-05-11 MARY 16,7

Sample Number Testing item Ω Testing method

Quality control Batch:

Analysis Date:

Analyzed By:

Reporting limit ppm

5 (Base) Mercury (Hg) content With reference to USEPA 7471 by USEPA 7471 MET2010-40p126 2011-05-10 RNC 0,25 5 (Plated) Mercury (Hg) content With reference to USEPA 7471 by USEPA 7471 MET2010-40p126 2011-05-10 RNC 2,5

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Test Report Number : TWNC00258877

Authorized By: On Behalf Of Intertek Testing Services Taiwan Limited

K. Y. Liang Director

This report shall not be reproduced except in full, without the written approval of the laboratory.

Page 1 of 5 Intertek Testing Services Taiwan Ltd.

8F., No. 423, Ruiguang Rd., Neihu District, Taipei 114, Taiwan, R.O.C.

全國公證檢驗股份有限公司 114 台北市內湖區瑞光路 423 號 8 樓

Tel: (+886-2) 6602-2888.2797-8885 Fax: (+886-2) 6602-2400.6602-2401

Applicant: Littelfuse, S.A. de C.V. Date : May 28, 2012 Blvd. Fausto Z. Martinez #1800

Col. Magisterio Seccion 38 C.P. 26070 Piedra Negras, Coahuila, Mexico

Sample Description:

One (1) group of submitted samples said to be : Part Description : TIN PLATED COPPER STRIP Part Number : 355.1115.2053 Date Sample Received : May 22, 2012 Date Test Started : May 23, 2012

Test Conducted :

As requested by the applicant, for details please refer to attached pages.

Page 91: resource… · 1 ICP Test Report Certification Packet Company name : Littelfuse, Inc. Product Series: FUSE - BF1 58V Product #: 142.5631.xxx Series Issue Date: August 22, 2012 It

Number : TWNC00258877

Test Conducted

Page 2 of 5 Intertek Testing Services Taiwan Ltd.

8F., No. 423, Ruiguang Rd., Neihu District, Taipei 114, Taiwan, R.O.C.

全國公證檢驗股份有限公司 114 台北市內湖區瑞光路 423 號 8 樓

Tel: (+886-2) 6602-2888.2797-8885 Fax: (+886-2) 6602-2400.6602-2401

(Ⅰ) Test Result Summary : Result (ppm)

Test Item (1) (2)

Heavy Metal

Cadmium (Cd) content ND ND Lead (Pb) content ND 344 Mercury (Hg) content ND ND

Chromium VI (Cr6+) content (mg/kg with 50cm2) Negative (<0.02)

Negative (<0.02)

Remarks: ppm = Parts per million based on weight of tested sample = mg/kg ND = Not detected < = Less than mg/kg with 50cm2 = milligram per kilogram with 50 square centimetre Negative = A negative test result indicated positive observation

was not found at the time of Test.

Tested Components (1) Silvery Plating Layer (2) Coppery Metal Base Material

Responsibility of Chemist :Irene Chiou / Kevin Liu / Cathy Chen

Date Sample Received : May 22, 2012 Test Period : May 23, 2012 To May 28, 2012

(Ⅱ) RoHS Requirement:

Restricted Substances Limits

Cadmium (Cd) Content 0.01% (100ppm) Lead (Pb) Content 0.1% (1000ppm) Mercury (Hg) Content 0.1% (1000ppm) Chromium VI (Cr6+) Content 0.1% (1000ppm)

The above limits were quoted from 2002/95/EC and amendment 2005/618/EC for homogeneous material.

Page 92: resource… · 1 ICP Test Report Certification Packet Company name : Littelfuse, Inc. Product Series: FUSE - BF1 58V Product #: 142.5631.xxx Series Issue Date: August 22, 2012 It

Number : TWNC00258877

Test Conducted

Page 3 of 5 Intertek Testing Services Taiwan Ltd.

8F., No. 423, Ruiguang Rd., Neihu District, Taipei 114, Taiwan, R.O.C.

全國公證檢驗股份有限公司 114 台北市內湖區瑞光路 423 號 8 樓

Tel: (+886-2) 6602-2888.2797-8885 Fax: (+886-2) 6602-2400.6602-2401

(Ⅲ) Test Method: Test Item Test Method Reporting Limit

Cadmium (Cd) content

With reference to IEC 62321 edition 1.0:2008 in clause 8/9/10, by microwave digestion until the tested samples are totally dissolved and determined by ICP-OES.

2 ppm

Lead (Pb) content

With reference to IEC 62321 edition 1.0:2008 in clause 8/9/10, by microwave digestion until the tested samples are totally dissolved and determined by ICP-OES.

2 ppm

Mercury (Hg) content

With reference to IEC 62321 edition 1.0:2008 in clause 7, by microwave digestion until the tested samples are totally dissolved and determined by ICP-OES.

2 ppm

Chromium VI (Cr6+) content

With reference to IEC 62321 edition 1.0:2008 in annex B, by boiling water extraction and determined by UV-Vis Spectrophotometer.

0.02 mg/kg with 50cm2

Remark: Reporting limit = Quantitation limit of analyte in sample

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Number : TWNC00258877

Test Conducted

Page 4 of 5 Intertek Testing Services Taiwan Ltd.

8F., No. 423, Ruiguang Rd., Neihu District, Taipei 114, Taiwan, R.O.C.

全國公證檢驗股份有限公司 114 台北市內湖區瑞光路 423 號 8 樓

Tel: (+886-2) 6602-2888.2797-8885 Fax: (+886-2) 6602-2400.6602-2401

(Ⅳ) Measurement Flowchart: Test for Cd/Pb/Hg/Chromium (VI) Reference Standard:IEC 62321 edition 1.0:2008

Remarks: *1: List of Appropriate Acid:

Material Acid Added for Digestion Polymers HNO3,HCl,HF,H2O2,H3BO3 Metals HNO3,HCl,HF Electronics HNO3,HCl,H2O2,HBF4

*2: If the result of spot test is positive, Chromium VI would be determined as detected.

End of Report

Sample preparation

For different material, digest the sample with appropriate acid*1

Make up with deionized water

Cd/Pb/Hg

Analyzed by ICP-OES

Weigh sample and add alkaline solution

Definite temp. extraction

Make up with deionized water and add diphenyl-carbazide solution

Cool and filter the extract

Cr6+

Analyzed by UV-VIS

By spot test

Get 50cm2 sample

By boiling water extraction

Metal Polymers / electronics

Negative *2

Confirm the tested samples are totally dissolved

Take sample and immerse into Aqua Regia, start to strip plating layer

Stop the stripping procedure upon color change completely

Take the Aqua solution as plating component and stripped body as substrate component

Page 94: resource… · 1 ICP Test Report Certification Packet Company name : Littelfuse, Inc. Product Series: FUSE - BF1 58V Product #: 142.5631.xxx Series Issue Date: August 22, 2012 It

Number : TWNC00258877

Test Conducted

Page 5 of 5 Intertek Testing Services Taiwan Ltd.

8F., No. 423, Ruiguang Rd., Neihu District, Taipei 114, Taiwan, R.O.C.

全國公證檢驗股份有限公司 114 台北市內湖區瑞光路 423 號 8 樓

Tel: (+886-2) 6602-2888.2797-8885 Fax: (+886-2) 6602-2400.6602-2401

Photo

Page 95: resource… · 1 ICP Test Report Certification Packet Company name : Littelfuse, Inc. Product Series: FUSE - BF1 58V Product #: 142.5631.xxx Series Issue Date: August 22, 2012 It

Test Report Number : TWNC00258878

Authorized By: On Behalf Of Intertek Testing Services Taiwan Limited

K. Y. Liang Director

This report shall not be reproduced except in full, without the written approval of the laboratory.

Page 1 of 5 Intertek Testing Services Taiwan Ltd.

8F., No. 423, Ruiguang Rd., Neihu District, Taipei 114, Taiwan, R.O.C.

全國公證檢驗股份有限公司 114 台北市內湖區瑞光路 423 號 8 樓

Tel: (+886-2) 6602-2888.2797-8885 Fax: (+886-2) 6602-2400.6602-2401

Applicant: Littelfuse, S.A. de C.V. Date : May 28, 2012 Blvd. Fausto Z. Martinez #1800

Col. Magisterio Seccion 38 C.P. 26070 Piedra Negras, Coahuila, Mexico

Sample Description:

One (1) group of submitted samples said to be : Part Description : Sn PLATED COPPER STRIP Part Number : 355.1115.3053 Date Sample Received : May 22, 2012 Date Test Started : May 23, 2012

Test Conducted :

As requested by the applicant, for details please refer to attached pages.

Page 96: resource… · 1 ICP Test Report Certification Packet Company name : Littelfuse, Inc. Product Series: FUSE - BF1 58V Product #: 142.5631.xxx Series Issue Date: August 22, 2012 It

Number : TWNC00258878

Test Conducted

Page 2 of 5 Intertek Testing Services Taiwan Ltd.

8F., No. 423, Ruiguang Rd., Neihu District, Taipei 114, Taiwan, R.O.C.

全國公證檢驗股份有限公司 114 台北市內湖區瑞光路 423 號 8 樓

Tel: (+886-2) 6602-2888.2797-8885 Fax: (+886-2) 6602-2400.6602-2401

(Ⅰ) Test Result Summary : Result (ppm)

Test Item (1) (2)

Heavy Metal

Cadmium (Cd) content ND ND Lead (Pb) content ND 211 Mercury (Hg) content ND ND

Chromium VI (Cr6+) content (mg/kg with 50cm2) Negative (<0.02)

Negative (<0.02)

Remarks: ppm = Parts per million based on weight of tested sample = mg/kg ND = Not detected < = Less than mg/kg with 50cm2 = milligram per kilogram with 50 square centimetre Negative = A negative test result indicated positive observation

was not found at the time of Test.

Tested Components (1) Silvery Plating Layer (2) Coppery Metal Base Material

Responsibility of Chemist :Irene Chiou / Kevin Liu / Cathy Chen

Date Sample Received : May 22, 2012 Test Period : May 23, 2012 To May 28, 2012

(Ⅱ) RoHS Requirement:

Restricted Substances Limits

Cadmium (Cd) Content 0.01% (100ppm) Lead (Pb) Content 0.1% (1000ppm) Mercury (Hg) Content 0.1% (1000ppm) Chromium VI (Cr6+) Content 0.1% (1000ppm)

The above limits were quoted from 2002/95/EC and amendment 2005/618/EC for homogeneous material.

Page 97: resource… · 1 ICP Test Report Certification Packet Company name : Littelfuse, Inc. Product Series: FUSE - BF1 58V Product #: 142.5631.xxx Series Issue Date: August 22, 2012 It

Number : TWNC00258878

Test Conducted

Page 3 of 5 Intertek Testing Services Taiwan Ltd.

8F., No. 423, Ruiguang Rd., Neihu District, Taipei 114, Taiwan, R.O.C.

全國公證檢驗股份有限公司 114 台北市內湖區瑞光路 423 號 8 樓

Tel: (+886-2) 6602-2888.2797-8885 Fax: (+886-2) 6602-2400.6602-2401

(Ⅲ) Test Method: Test Item Test Method Reporting Limit

Cadmium (Cd) content

With reference to IEC 62321 edition 1.0:2008 in clause 8/9/10, by microwave digestion until the tested samples are totally dissolved and determined by ICP-OES.

2 ppm

Lead (Pb) content

With reference to IEC 62321 edition 1.0:2008 in clause 8/9/10, by microwave digestion until the tested samples are totally dissolved and determined by ICP-OES.

2 ppm

Mercury (Hg) content

With reference to IEC 62321 edition 1.0:2008 in clause 7, by microwave digestion until the tested samples are totally dissolved and determined by ICP-OES.

2 ppm

Chromium VI (Cr6+) content

With reference to IEC 62321 edition 1.0:2008 in annex B, by boiling water extraction and determined by UV-Vis Spectrophotometer.

0.02 mg/kg with 50cm2

Remark: Reporting limit = Quantitation limit of analyte in sample

Page 98: resource… · 1 ICP Test Report Certification Packet Company name : Littelfuse, Inc. Product Series: FUSE - BF1 58V Product #: 142.5631.xxx Series Issue Date: August 22, 2012 It

Number : TWNC00258878

Test Conducted

Page 4 of 5 Intertek Testing Services Taiwan Ltd.

8F., No. 423, Ruiguang Rd., Neihu District, Taipei 114, Taiwan, R.O.C.

全國公證檢驗股份有限公司 114 台北市內湖區瑞光路 423 號 8 樓

Tel: (+886-2) 6602-2888.2797-8885 Fax: (+886-2) 6602-2400.6602-2401

(Ⅳ) Measurement Flowchart: Test for Cd/Pb/Hg/Chromium (VI) Reference Standard:IEC 62321 edition 1.0:2008

Remarks: *1: List of Appropriate Acid:

Material Acid Added for Digestion Polymers HNO3,HCl,HF,H2O2,H3BO3 Metals HNO3,HCl,HF Electronics HNO3,HCl,H2O2,HBF4

*2: If the result of spot test is positive, Chromium VI would be determined as detected.

End of Report

Sample preparation

For different material, digest the sample with appropriate acid*1

Make up with deionized water

Cd/Pb/Hg

Analyzed by ICP-OES

Weigh sample and add alkaline solution

Definite temp. extraction

Make up with deionized water and add diphenyl-carbazide solution

Cool and filter the extract

Cr6+

Analyzed by UV-VIS

By spot test

Get 50cm2 sample

By boiling water extraction

Metal Polymers / electronics

Negative *2

Confirm the tested samples are totally dissolved

Take sample and immerse into Aqua Regia, start to strip plating layer

Stop the stripping procedure upon color change completely

Take the Aqua solution as plating component and stripped body as substrate component

Page 99: resource… · 1 ICP Test Report Certification Packet Company name : Littelfuse, Inc. Product Series: FUSE - BF1 58V Product #: 142.5631.xxx Series Issue Date: August 22, 2012 It

Number : TWNC00258878

Test Conducted

Page 5 of 5 Intertek Testing Services Taiwan Ltd.

8F., No. 423, Ruiguang Rd., Neihu District, Taipei 114, Taiwan, R.O.C.

全國公證檢驗股份有限公司 114 台北市內湖區瑞光路 423 號 8 樓

Tel: (+886-2) 6602-2888.2797-8885 Fax: (+886-2) 6602-2400.6602-2401

Photo

Page 100: resource… · 1 ICP Test Report Certification Packet Company name : Littelfuse, Inc. Product Series: FUSE - BF1 58V Product #: 142.5631.xxx Series Issue Date: August 22, 2012 It

Test Report Number : TWNC00241458

Authorized By: On Behalf Of Intertek Testing Services Taiwan Limited

K. Y. Liang Director

This report shall not be reproduced except in full, without the written approval of the laboratory.

Page 1 of 9 Intertek Testing Services Taiwan Ltd.

8F., No. 423, Ruiguang Rd., Neihu District, Taipei 114, Taiwan, R.O.C. 全國公證檢驗股份有限公司 114台北市內湖區瑞光路 423號 8樓

Tel: (+886-2) 6602-2888.2797-8885 Fax: (+886-2) 6602-2400.6602-2401

Applicant: Littelfuse, S.A. de C.V. Date : Feb 01, 2012 Blvd. Fausto Z. Martinez #1800

Col. Magisterio Seccion 38 C.P. 26070 Piedra Negras, Coahuila, Mexico

Sample Description:

One (1) group of submitted samples said to be : Part Description : COLORANT NATURAL Part Number : 325.2131.0001 Date Sample Received : Jan 19, 2012 Date Test Started : Jan 19, 2012

Test Conducted :

As requested by the applicant, for details please refer to attached pages.

Page 101: resource… · 1 ICP Test Report Certification Packet Company name : Littelfuse, Inc. Product Series: FUSE - BF1 58V Product #: 142.5631.xxx Series Issue Date: August 22, 2012 It

Number : TWNC00241458

Test Conducted

Page 2 of 9 Intertek Testing Services Taiwan Ltd.

8F., No. 423, Ruiguang Rd., Neihu District, Taipei 114, Taiwan, R.O.C. 全國公證檢驗股份有限公司 114台北市內湖區瑞光路 423號 8樓

Tel: (+886-2) 6602-2888.2797-8885 Fax: (+886-2) 6602-2400.6602-2401

(Ⅰ) Test Result Summary : Result (ppm)

Test Item White Plastic Pellet

Heavy Metal

Cadmium (Cd) content ND Lead (Pb) content 20 Mercury (Hg) content ND Chromium VI (Cr6+) content ND

Polybrominated Biphenyls (PBBs) Monobrominated Biphenyls (MonoBB) ND Dibrominated Biphenyls (DiBB) ND Tribrominated Biphenyls (TriBB) ND Tetrabrominated Biphenyls (TetraBB) ND Pentabrominated Biphenyls (PentaBB) ND Hexabrominated Biphenyls (HexaBB) ND Heptabrominated Biphenyls (HeptaBB) ND Octabrominated Biphenyls (OctaBB) ND Nonabrominated Biphenyls (NonaBB) ND Decabrominated Biphenyl (DecaBB) ND

Polybrominated Diphenyl Ethers (PBDEs) Monobrominated Diphenyl Ethers (MonoBDE) ND Dibrominated Diphenyl Ethers (DiBDE) ND Tribrominated Diphenyl Ethers (TriBDE) ND Tetrabrominated Diphenyl Ethers (TetraBDE) ND Pentabrominated Diphenyl Ethers (PentaBDE) ND Hexabrominated Diphenyl Ethers (HexaBDE) ND Heptabrominated Diphenyl Ethers (HeptaBDE) ND Octabrominated Diphenyl Ethers (OctaBDE) ND Nonabrominated Diphenyl Ethers (NonaBDE) ND Decabrominated Diphenyl Ether (DecaBDE) ND

Halogen Content Fluorine (F) 290 Chlorine (Cl) 86 Bromine (Br) 33550 Iodine (I) ND

Page 102: resource… · 1 ICP Test Report Certification Packet Company name : Littelfuse, Inc. Product Series: FUSE - BF1 58V Product #: 142.5631.xxx Series Issue Date: August 22, 2012 It

Number : TWNC00241458

Test Conducted

Page 3 of 9 Intertek Testing Services Taiwan Ltd.

8F., No. 423, Ruiguang Rd., Neihu District, Taipei 114, Taiwan, R.O.C. 全國公證檢驗股份有限公司 114台北市內湖區瑞光路 423號 8樓

Tel: (+886-2) 6602-2888.2797-8885 Fax: (+886-2) 6602-2400.6602-2401

(Ⅰ) Test Result Summary : Result (ppm)

Test Item White Plastic Pellet

Phthalates Di(2-ethylhexyl) Phthalate (DEHP) ND Dibutyl Phthalate (DBP) ND Benzyl Butyl Phthalate (BBP) ND

Others Hexabromocyclododecane (HBCDD) ND

Remarks: ppm = Parts per million based on weight of tested sample = mg/kg ND = Not detected

Responsibility of Chemist :Irene Chiou / Kevin Liu / Cathy Chen

Date Sample Received : Jan 19, 2012 Test Period : Jan 19, 2012 To Feb 01, 2012

(Ⅱ) RoHS Requirement:

Restricted Substances Limits

Cadmium (Cd) Content 0.01% (100ppm) Lead (Pb) Content 0.1% (1000ppm) Mercury (Hg) Content 0.1% (1000ppm) Chromium VI (Cr6+) Content 0.1% (1000ppm) Polybrominated Biphenyls (PBBs) 0.1% (1000ppm) Polybrominated Diphenyl Ehters (PBDEs) 0.1% (1000ppm)

The above limits were quoted from 2002/95/EC and amendment 2005/618/EC for homogeneous material.

Page 103: resource… · 1 ICP Test Report Certification Packet Company name : Littelfuse, Inc. Product Series: FUSE - BF1 58V Product #: 142.5631.xxx Series Issue Date: August 22, 2012 It

Number : TWNC00241458

Test Conducted

Page 4 of 9 Intertek Testing Services Taiwan Ltd.

8F., No. 423, Ruiguang Rd., Neihu District, Taipei 114, Taiwan, R.O.C. 全國公證檢驗股份有限公司 114台北市內湖區瑞光路 423號 8樓

Tel: (+886-2) 6602-2888.2797-8885 Fax: (+886-2) 6602-2400.6602-2401

(Ⅲ) Test Method: Test Item Test Method Reporting Limit

Cadmium (Cd) content

With reference to IEC 62321 edition 1.0:2008 in clause 8/9/10, by microwave digestion until the tested samples are totally dissolved and determined by ICP-OES.

2 ppm

Lead (Pb) content

With reference to IEC 62321 edition 1.0:2008 in clause 8/9/10, by microwave digestion until the tested samples are totally dissolved and determined by ICP-OES.

2 ppm

Mercury (Hg) content

With reference to IEC 62321 edition 1.0:2008 in clause 7, by microwave digestion until the tested samples are totally dissolved and determined by ICP-OES.

2 ppm

Chromium VI (Cr6+) content

With reference to IEC 62321 edition 1.0:2008 in annex C, by alkaline digestion and determined by UV-Vis spectrophotometer.

1 ppm

Polybrominated Biphenyls (PBBs)

With reference to IEC 62321 edition 1.0:2008 in annex A, by solvent extraction and determined by GC-MS and further HPLC-DAD confirmation when necessary.

5 ppm

Polybrominated Diphenyl Ethers (PBDEs)

With reference to IEC 62321 edition 1.0:2008 in annex A, by solvent extraction and determined by GC-MS and further HPLC-DAD confirmation when necessary.

5 ppm

Halogen Content With reference to EN 14582:2007 by calorimetric bomb with oxygen and determined by Ion Chromatograph.

50 ppm

Phthalates With reference to ASTM D3421-75, by solvent extraction and determined byGC-MSD or GC-FID

10 ppm

Hexabromocyclododecane(HBCDD)

With reference to USEPA 3540C, by solvent extraction and determined byGC-MSD

10 ppm

Remark: Reporting limit = Quantitation limit of analyte in sample

Page 104: resource… · 1 ICP Test Report Certification Packet Company name : Littelfuse, Inc. Product Series: FUSE - BF1 58V Product #: 142.5631.xxx Series Issue Date: August 22, 2012 It

Number : TWNC00241458

Test Conducted

Page 5 of 9 Intertek Testing Services Taiwan Ltd.

8F., No. 423, Ruiguang Rd., Neihu District, Taipei 114, Taiwan, R.O.C. 全國公證檢驗股份有限公司 114台北市內湖區瑞光路 423號 8樓

Tel: (+886-2) 6602-2888.2797-8885 Fax: (+886-2) 6602-2400.6602-2401

(Ⅳ) Measurement Flowchart: Test for Cd/Pb/Hg/Chromium (VI)/PBBS/PBDES Contents Reference Standard: IEC 62321 edition 1.0:2008

Remarks: *1: List of Appropriate Acid:

Material Acid Added for Digestion Polymers HNO3,HCl,HF,H2O2,H3BO3 Metals HNO3,HCl,HF Electronics HNO3,HCl,H2O2,HBF4

*2: If the result of spot test is positive, Chromium VI would be determined as detected.

Sample preparation

For different material, digest the sample with appropriate acid*1

Make up with deionized water

Cd/Pb/Hg

Analyzed by ICP-OES

Weigh sample and add alkaline solution

Definite temp. extraction

Make up with deionized water and add diphenyl-carbazide solution

Cool and filter the extract

Cr6+

Weigh sample and add organic solvent

By Soxhlet extraction or Solvent extraction

Concentrate the extract and make upwith organic solvent

PBBs/PBDEs

Analyzed by UV-VIS

Analyzed by GC-MSD

By spot test

Get 50cm2 sample

By boiling water extraction

Metal Polymers / electronics

Negative *2

Confirm the tested samples are totally dissolved

Take sample and immerse into Aqua Regia, start to strip plating layer

Stop the stripping procedure upon color change completely

Take the Aqua solution as plating component and stripped body as substrate component

For non-metal part For metal part

Page 105: resource… · 1 ICP Test Report Certification Packet Company name : Littelfuse, Inc. Product Series: FUSE - BF1 58V Product #: 142.5631.xxx Series Issue Date: August 22, 2012 It

Number : TWNC00241458

Test Conducted

Page 6 of 9 Intertek Testing Services Taiwan Ltd.

8F., No. 423, Ruiguang Rd., Neihu District, Taipei 114, Taiwan, R.O.C. 全國公證檢驗股份有限公司 114台北市內湖區瑞光路 423號 8樓

Tel: (+886-2) 6602-2888.2797-8885 Fax: (+886-2) 6602-2400.6602-2401

(Ⅳ) Measurement Flowchart:

Test for Halogen Content Reference Standard:EN 14582

Add absorbent in a combustion flask & place weighed sample in equipment

Fill oxygen into calorimetric bomb

Ignite then leave the bomb at room temperature

Transfer the absorbent into a volumetric flask

Make up with deionized water

Sampling/grinding or cutting

Analyzed by ion chromatography

Page 106: resource… · 1 ICP Test Report Certification Packet Company name : Littelfuse, Inc. Product Series: FUSE - BF1 58V Product #: 142.5631.xxx Series Issue Date: August 22, 2012 It

Number : TWNC00241458

Test Conducted

Page 7 of 9 Intertek Testing Services Taiwan Ltd.

8F., No. 423, Ruiguang Rd., Neihu District, Taipei 114, Taiwan, R.O.C. 全國公證檢驗股份有限公司 114台北市內湖區瑞光路 423號 8樓

Tel: (+886-2) 6602-2888.2797-8885 Fax: (+886-2) 6602-2400.6602-2401

(Ⅳ) Measurement Flowchart: Test For Phthalates Contents Reference Method: EN 14372: 2004

Sampling/grinding or cutting

Weigh sample and add organic solvent

By solvent extraction

Concentrate the extract and make up with organic solvent

Analyzed by GC-MSD

Page 107: resource… · 1 ICP Test Report Certification Packet Company name : Littelfuse, Inc. Product Series: FUSE - BF1 58V Product #: 142.5631.xxx Series Issue Date: August 22, 2012 It

Number : TWNC00241458

Test Conducted

Page 8 of 9 Intertek Testing Services Taiwan Ltd.

8F., No. 423, Ruiguang Rd., Neihu District, Taipei 114, Taiwan, R.O.C. 全國公證檢驗股份有限公司 114台北市內湖區瑞光路 423號 8樓

Tel: (+886-2) 6602-2888.2797-8885 Fax: (+886-2) 6602-2400.6602-2401

(Ⅳ) Measurement Flowchart:

Test For Hexabromocyclododecane (HBCDD) Reference Standard:USEPA 3540C

End of Report

Sampling/grinding or cutting

Weigh sample and add organic solvent

By soxhlet extraction

Concentrate the extract and make up with organic solvent

Analyzed by GC-MSD

Page 108: resource… · 1 ICP Test Report Certification Packet Company name : Littelfuse, Inc. Product Series: FUSE - BF1 58V Product #: 142.5631.xxx Series Issue Date: August 22, 2012 It

Number : TWNC00241458

Test Conducted

Page 9 of 9 Intertek Testing Services Taiwan Ltd.

8F., No. 423, Ruiguang Rd., Neihu District, Taipei 114, Taiwan, R.O.C. 全國公證檢驗股份有限公司 114台北市內湖區瑞光路 423號 8樓

Tel: (+886-2) 6602-2888.2797-8885 Fax: (+886-2) 6602-2400.6602-2401

Photo

Page 109: resource… · 1 ICP Test Report Certification Packet Company name : Littelfuse, Inc. Product Series: FUSE - BF1 58V Product #: 142.5631.xxx Series Issue Date: August 22, 2012 It

Test Report Number : TWNC00242056

Authorized By: On Behalf Of Intertek Testing Services Taiwan Limited

K. Y. Liang Director

This report shall not be reproduced except in full, without the written approval of the laboratory.

Page 1 of 9 Intertek Testing Services Taiwan Ltd.

8F., No. 423, Ruiguang Rd., Neihu District, Taipei 114, Taiwan, R.O.C. 全國公證檢驗股份有限公司 114台北市內湖區瑞光路 423號 8樓

Tel: (+886-2) 6602-2888.2797-8885 Fax: (+886-2) 6602-2400.6602-2401

Applicant: Littelfuse, S.A. de C.V. Date : Feb 03, 2012 Blvd. Fausto Z. Martinez #1800

Col. Magisterio Seccion 38 C.P. 26070 Piedra Negras, Coahuila, Mexico

Sample Description:

One (1) group of submitted samples said to be : Part Description : COLORANT VIOLET Part Number : 325.7692.0810 Date Sample Received : Feb 01, 2012 Date Test Started : Feb 01, 2012

Test Conducted :

As requested by the applicant, for details please refer to attached pages.

Page 110: resource… · 1 ICP Test Report Certification Packet Company name : Littelfuse, Inc. Product Series: FUSE - BF1 58V Product #: 142.5631.xxx Series Issue Date: August 22, 2012 It

Number : TWNC00242056

Test Conducted

Page 2 of 9 Intertek Testing Services Taiwan Ltd.

8F., No. 423, Ruiguang Rd., Neihu District, Taipei 114, Taiwan, R.O.C. 全國公證檢驗股份有限公司 114台北市內湖區瑞光路 423號 8樓

Tel: (+886-2) 6602-2888.2797-8885 Fax: (+886-2) 6602-2400.6602-2401

(Ⅰ) Test Result Summary : Result (ppm)

Test Item Purple Plastic Pellet

Heavy Metal

Cadmium (Cd) content ND Lead (Pb) content ND Mercury (Hg) content ND Chromium VI (Cr6+) content ND

Polybrominated Biphenyls (PBBs) Monobrominated Biphenyls (MonoBB) ND Dibrominated Biphenyls (DiBB) ND Tribrominated Biphenyls (TriBB) ND Tetrabrominated Biphenyls (TetraBB) ND Pentabrominated Biphenyls (PentaBB) ND Hexabrominated Biphenyls (HexaBB) ND Heptabrominated Biphenyls (HeptaBB) ND Octabrominated Biphenyls (OctaBB) ND Nonabrominated Biphenyls (NonaBB) ND Decabrominated Biphenyl (DecaBB) ND

Polybrominated Diphenyl Ethers (PBDEs) Monobrominated Diphenyl Ethers (MonoBDE) ND Dibrominated Diphenyl Ethers (DiBDE) ND Tribrominated Diphenyl Ethers (TriBDE) ND Tetrabrominated Diphenyl Ethers (TetraBDE) ND Pentabrominated Diphenyl Ethers (PentaBDE) ND Hexabrominated Diphenyl Ethers (HexaBDE) ND Heptabrominated Diphenyl Ethers (HeptaBDE) ND Octabrominated Diphenyl Ethers (OctaBDE) ND Nonabrominated Diphenyl Ethers (NonaBDE) ND Decabrominated Diphenyl Ether (DecaBDE) ND

Halogen Content Fluorine (F) ND Chlorine (Cl) ND Bromine (Br) ND Iodine (I) ND

Page 111: resource… · 1 ICP Test Report Certification Packet Company name : Littelfuse, Inc. Product Series: FUSE - BF1 58V Product #: 142.5631.xxx Series Issue Date: August 22, 2012 It

Number : TWNC00242056

Test Conducted

Page 3 of 9 Intertek Testing Services Taiwan Ltd.

8F., No. 423, Ruiguang Rd., Neihu District, Taipei 114, Taiwan, R.O.C. 全國公證檢驗股份有限公司 114台北市內湖區瑞光路 423號 8樓

Tel: (+886-2) 6602-2888.2797-8885 Fax: (+886-2) 6602-2400.6602-2401

(Ⅰ) Test Result Summary : Result (ppm)

Test Item Purple Plastic Pellet

Phthalates Di(2-ethylhexyl) Phthalate (DEHP) ND Dibutyl Phthalate (DBP) ND Benzyl Butyl Phthalate (BBP) ND

Others Hexabromocyclododecane (HBCDD) ND

Remarks: ppm = Parts per million based on weight of tested sample = mg/kg ND = Not detected

Responsibility of Chemist :Irene Chiou / Kevin Liu / Cathy Chen

Date Sample Received : Feb 01, 2012 Test Period : Feb 01, 2012 To Feb 03, 2012

(Ⅱ) RoHS Requirement:

Restricted Substances Limits

Cadmium (Cd) Content 0.01% (100ppm) Lead (Pb) Content 0.1% (1000ppm) Mercury (Hg) Content 0.1% (1000ppm) Chromium VI (Cr6+) Content 0.1% (1000ppm) Polybrominated Biphenyls (PBBs) 0.1% (1000ppm) Polybrominated Diphenyl Ehters (PBDEs) 0.1% (1000ppm)

The above limits were quoted from 2002/95/EC and amendment 2005/618/EC for homogeneous material.

Page 112: resource… · 1 ICP Test Report Certification Packet Company name : Littelfuse, Inc. Product Series: FUSE - BF1 58V Product #: 142.5631.xxx Series Issue Date: August 22, 2012 It

Number : TWNC00242056

Test Conducted

Page 4 of 9 Intertek Testing Services Taiwan Ltd.

8F., No. 423, Ruiguang Rd., Neihu District, Taipei 114, Taiwan, R.O.C. 全國公證檢驗股份有限公司 114台北市內湖區瑞光路 423號 8樓

Tel: (+886-2) 6602-2888.2797-8885 Fax: (+886-2) 6602-2400.6602-2401

(Ⅲ) Test Method: Test Item Test Method Reporting Limit

Cadmium (Cd) content

With reference to IEC 62321 edition 1.0:2008 in clause 8/9/10, by microwave digestion until the tested samples are totally dissolved and determined by ICP-OES.

2 ppm

Lead (Pb) content

With reference to IEC 62321 edition 1.0:2008 in clause 8/9/10, by microwave digestion until the tested samples are totally dissolved and determined by ICP-OES.

2 ppm

Mercury (Hg) content

With reference to IEC 62321 edition 1.0:2008 in clause 7, by microwave digestion until the tested samples are totally dissolved and determined by ICP-OES.

2 ppm

Chromium VI (Cr6+) content

With reference to IEC 62321 edition 1.0:2008 in annex C, by alkaline digestion and determined by UV-Vis spectrophotometer.

1 ppm

Polybrominated Biphenyls (PBBs)

With reference to IEC 62321 edition 1.0:2008 in annex A, by solvent extraction and determined by GC-MS and further HPLC-DAD confirmation when necessary.

5 ppm

Polybrominated Diphenyl Ethers (PBDEs)

With reference to IEC 62321 edition 1.0:2008 in annex A, by solvent extraction and determined by GC-MS and further HPLC-DAD confirmation when necessary.

5 ppm

Halogen Content With reference to EN 14582:2007 by calorimetric bomb with oxygen and determined by Ion Chromatograph.

50 ppm

Phthalates With reference to ASTM D3421-75, by solvent extraction and determined byGC-MSD or GC-FID

10 ppm

Hexabromocyclododecane(HBCDD)

With reference to USEPA 3540C, by solvent extraction and determined byGC-MSD

10 ppm

Remark: Reporting limit = Quantitation limit of analyte in sample

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Number : TWNC00242056

Test Conducted

Page 5 of 9 Intertek Testing Services Taiwan Ltd.

8F., No. 423, Ruiguang Rd., Neihu District, Taipei 114, Taiwan, R.O.C. 全國公證檢驗股份有限公司 114台北市內湖區瑞光路 423號 8樓

Tel: (+886-2) 6602-2888.2797-8885 Fax: (+886-2) 6602-2400.6602-2401

(Ⅳ) Measurement Flowchart: Test for Cd/Pb/Hg/Chromium (VI)/PBBS/PBDES Contents Reference Standard: IEC 62321 edition 1.0:2008

Remarks: *1: List of Appropriate Acid:

Material Acid Added for Digestion Polymers HNO3,HCl,HF,H2O2,H3BO3 Metals HNO3,HCl,HF Electronics HNO3,HCl,H2O2,HBF4

*2: If the result of spot test is positive, Chromium VI would be determined as detected.

Sample preparation

For different material, digest the sample with appropriate acid*1

Make up with deionized water

Cd/Pb/Hg

Analyzed by ICP-OES

Weigh sample and add alkaline solution

Definite temp. extraction

Make up with deionized water and add diphenyl-carbazide solution

Cool and filter the extract

Cr6+

Weigh sample and add organic solvent

By Soxhlet extraction or Solvent extraction

Concentrate the extract and make upwith organic solvent

PBBs/PBDEs

Analyzed by UV-VIS

Analyzed by GC-MSD

By spot test

Get 50cm2 sample

By boiling water extraction

Metal Polymers / electronics

Negative *2

Confirm the tested samples are totally dissolved

Take sample and immerse into Aqua Regia, start to strip plating layer

Stop the stripping procedure upon color change completely

Take the Aqua solution as plating component and stripped body as substrate component

For non-metal part For metal part

Page 114: resource… · 1 ICP Test Report Certification Packet Company name : Littelfuse, Inc. Product Series: FUSE - BF1 58V Product #: 142.5631.xxx Series Issue Date: August 22, 2012 It

Number : TWNC00242056

Test Conducted

Page 6 of 9 Intertek Testing Services Taiwan Ltd.

8F., No. 423, Ruiguang Rd., Neihu District, Taipei 114, Taiwan, R.O.C. 全國公證檢驗股份有限公司 114台北市內湖區瑞光路 423號 8樓

Tel: (+886-2) 6602-2888.2797-8885 Fax: (+886-2) 6602-2400.6602-2401

(Ⅳ) Measurement Flowchart:

Test for Halogen Content Reference Standard:EN 14582

Add absorbent in a combustion flask & place weighed sample in equipment

Fill oxygen into calorimetric bomb

Ignite then leave the bomb at room temperature

Transfer the absorbent into a volumetric flask

Make up with deionized water

Sampling/grinding or cutting

Analyzed by ion chromatography

Page 115: resource… · 1 ICP Test Report Certification Packet Company name : Littelfuse, Inc. Product Series: FUSE - BF1 58V Product #: 142.5631.xxx Series Issue Date: August 22, 2012 It

Number : TWNC00242056

Test Conducted

Page 7 of 9 Intertek Testing Services Taiwan Ltd.

8F., No. 423, Ruiguang Rd., Neihu District, Taipei 114, Taiwan, R.O.C. 全國公證檢驗股份有限公司 114台北市內湖區瑞光路 423號 8樓

Tel: (+886-2) 6602-2888.2797-8885 Fax: (+886-2) 6602-2400.6602-2401

(Ⅳ) Measurement Flowchart: Test For Phthalates Contents Reference Method: EN 14372: 2004

Sampling/grinding or cutting

Weigh sample and add organic solvent

By solvent extraction

Concentrate the extract and make up with organic solvent

Analyzed by GC-MSD

Page 116: resource… · 1 ICP Test Report Certification Packet Company name : Littelfuse, Inc. Product Series: FUSE - BF1 58V Product #: 142.5631.xxx Series Issue Date: August 22, 2012 It

Number : TWNC00242056

Test Conducted

Page 8 of 9 Intertek Testing Services Taiwan Ltd.

8F., No. 423, Ruiguang Rd., Neihu District, Taipei 114, Taiwan, R.O.C. 全國公證檢驗股份有限公司 114台北市內湖區瑞光路 423號 8樓

Tel: (+886-2) 6602-2888.2797-8885 Fax: (+886-2) 6602-2400.6602-2401

(Ⅳ) Measurement Flowchart:

Test For Hexabromocyclododecane (HBCDD) Reference Standard:USEPA 3540C

End of Report

Sampling/grinding or cutting

Weigh sample and add organic solvent

By soxhlet extraction

Concentrate the extract and make up with organic solvent

Analyzed by GC-MSD

Page 117: resource… · 1 ICP Test Report Certification Packet Company name : Littelfuse, Inc. Product Series: FUSE - BF1 58V Product #: 142.5631.xxx Series Issue Date: August 22, 2012 It

Number : TWNC00242056

Test Conducted

Page 9 of 9 Intertek Testing Services Taiwan Ltd.

8F., No. 423, Ruiguang Rd., Neihu District, Taipei 114, Taiwan, R.O.C. 全國公證檢驗股份有限公司 114台北市內湖區瑞光路 423號 8樓

Tel: (+886-2) 6602-2888.2797-8885 Fax: (+886-2) 6602-2400.6602-2401

Photo

Page 118: resource… · 1 ICP Test Report Certification Packet Company name : Littelfuse, Inc. Product Series: FUSE - BF1 58V Product #: 142.5631.xxx Series Issue Date: August 22, 2012 It

Test Report Number : TWNC00258320

Authorized By: On Behalf Of Intertek Testing Services Taiwan Limited

K. Y. Liang Director

This report shall not be reproduced except in full, without the written approval of the laboratory.

Page 1 of 9 Intertek Testing Services Taiwan Ltd.

8F., No. 423, Ruiguang Rd., Neihu District, Taipei 114, Taiwan, R.O.C.

全國公證檢驗股份有限公司 114 台北市內湖區瑞光路 423 號 8 樓

Tel: (+886-2) 6602-2888.2797-8885 Fax: (+886-2) 6602-2400.6602-2401

Applicant: Littelfuse, S.A. de C.V. Date : May 29, 2012 Blvd. Fausto Z. Martinez #1800

Col. Magisterio Seccion 38 C.P. 26070 Piedra Negras, Coahuila, Mexico

Sample Description:

One (1) group of submitted samples said to be : Part Description : BF1 CLEAR COVER Part Number : 353.2140.1000 Date Sample Received : May 17, 2012 Date Test Started : May 19, 2012

Test Conducted :

As requested by the applicant, for details please refer to attached pages.

Page 119: resource… · 1 ICP Test Report Certification Packet Company name : Littelfuse, Inc. Product Series: FUSE - BF1 58V Product #: 142.5631.xxx Series Issue Date: August 22, 2012 It

Number : TWNC00258320

Test Conducted

Page 2 of 9 Intertek Testing Services Taiwan Ltd.

8F., No. 423, Ruiguang Rd., Neihu District, Taipei 114, Taiwan, R.O.C.

全國公證檢驗股份有限公司 114 台北市內湖區瑞光路 423 號 8 樓

Tel: (+886-2) 6602-2888.2797-8885 Fax: (+886-2) 6602-2400.6602-2401

(Ⅰ) Test Result Summary : Result (ppm)

Test Item Clear Orange Plastic

Heavy Metal

Cadmium (Cd) content ND Lead (Pb) content ND Mercury (Hg) content ND Chromium VI (Cr6+) content ND

Polybrominated Biphenyls (PBBs) Monobrominated Biphenyls (MonoBB) ND Dibrominated Biphenyls (DiBB) ND Tribrominated Biphenyls (TriBB) ND Tetrabrominated Biphenyls (TetraBB) ND Pentabrominated Biphenyls (PentaBB) ND Hexabrominated Biphenyls (HexaBB) ND Heptabrominated Biphenyls (HeptaBB) ND Octabrominated Biphenyls (OctaBB) ND Nonabrominated Biphenyls (NonaBB) ND Decabrominated Biphenyl (DecaBB) ND

Polybrominated Diphenyl Ethers (PBDEs) Monobrominated Diphenyl Ethers (MonoBDE) ND Dibrominated Diphenyl Ethers (DiBDE) ND Tribrominated Diphenyl Ethers (TriBDE) ND Tetrabrominated Diphenyl Ethers (TetraBDE) ND Pentabrominated Diphenyl Ethers (PentaBDE) ND Hexabrominated Diphenyl Ethers (HexaBDE) ND Heptabrominated Diphenyl Ethers (HeptaBDE) ND Octabrominated Diphenyl Ethers (OctaBDE) ND Nonabrominated Diphenyl Ethers (NonaBDE) ND Decabrominated Diphenyl Ether (DecaBDE) ND

Halogen Content Fluorine (F) ND Chlorine (Cl) 1768 Bromine (Br) ND Iodine (I) ND

Z

Page 120: resource… · 1 ICP Test Report Certification Packet Company name : Littelfuse, Inc. Product Series: FUSE - BF1 58V Product #: 142.5631.xxx Series Issue Date: August 22, 2012 It

Number : TWNC00258320

Test Conducted

Page 3 of 9 Intertek Testing Services Taiwan Ltd.

8F., No. 423, Ruiguang Rd., Neihu District, Taipei 114, Taiwan, R.O.C.

全國公證檢驗股份有限公司 114 台北市內湖區瑞光路 423 號 8 樓

Tel: (+886-2) 6602-2888.2797-8885 Fax: (+886-2) 6602-2400.6602-2401

(Ⅰ) Test Result Summary : Result (ppm)

Test Item Clear Orange Plastic

Phthalates Di(2-ethylhexyl) Phthalate (DEHP) ND Dibutyl Phthalate (DBP) ND Benzyl Butyl Phthalate (BBP) ND

Others Hexabromocyclododecane (HBCDD) ND

Remarks: ppm = Parts per million based on weight of tested sample = mg/kg ND = Not detected

Responsibility of Chemist :Irene Chiou / Kevin Liu / Cathy Chen

Date Sample Received : May 17, 2012 Test Period : May 19, 2012 To May 28, 2012

(Ⅱ) RoHS Requirement:

Restricted Substances Limits

Cadmium (Cd) Content 0.01% (100ppm) Lead (Pb) Content 0.1% (1000ppm) Mercury (Hg) Content 0.1% (1000ppm) Chromium VI (Cr6+) Content 0.1% (1000ppm) Polybrominated Biphenyls (PBBs) 0.1% (1000ppm) Polybrominated Diphenyl Ehters (PBDEs) 0.1% (1000ppm)

The above limits were quoted from 2002/95/EC and amendment 2005/618/EC for homogeneous material.

Z

Page 121: resource… · 1 ICP Test Report Certification Packet Company name : Littelfuse, Inc. Product Series: FUSE - BF1 58V Product #: 142.5631.xxx Series Issue Date: August 22, 2012 It

Number : TWNC00258320

Test Conducted

Page 4 of 9 Intertek Testing Services Taiwan Ltd.

8F., No. 423, Ruiguang Rd., Neihu District, Taipei 114, Taiwan, R.O.C.

全國公證檢驗股份有限公司 114 台北市內湖區瑞光路 423 號 8 樓

Tel: (+886-2) 6602-2888.2797-8885 Fax: (+886-2) 6602-2400.6602-2401

(Ⅲ) Test Method: Test Item Test Method Reporting Limit

Cadmium (Cd) content

With reference to IEC 62321 edition 1.0:2008 in clause 8/9/10, by microwave digestion until the tested samples are totally dissolved and determined by ICP-OES.

2 ppm

Lead (Pb) content

With reference to IEC 62321 edition 1.0:2008 in clause 8/9/10, by microwave digestion until the tested samples are totally dissolved and determined by ICP-OES.

2 ppm

Mercury (Hg) content

With reference to IEC 62321 edition 1.0:2008 in clause 7, by microwave digestion until the tested samples are totally dissolved and determined by ICP-OES.

2 ppm

Chromium VI (Cr6+) content

With reference to IEC 62321 edition 1.0:2008 in annex C, by alkaline digestion and determined by UV-Vis spectrophotometer.

1 ppm

Polybrominated Biphenyls (PBBs)

With reference to IEC 62321 edition 1.0:2008 in annex A, by solvent extraction and determined by GC-MS and further HPLC-DAD confirmation when necessary.

5 ppm

Polybrominated Diphenyl Ethers (PBDEs)

With reference to IEC 62321 edition 1.0:2008 in annex A, by solvent extraction and determined by GC-MS and further HPLC-DAD confirmation when necessary.

5 ppm

Halogen Content With reference to EN 14582:2007 by calorimetric bomb with oxygen and determined by Ion Chromatograph.

50 ppm

Phthalates With reference to EN 14372: 2004, bysolvent extraction and determined byGC-MS.

50 ppm

Hexabromocyclododecane(HBCDD)

With reference to USEPA 3540C, by solvent extraction and determined byGC-MSD.

10 ppm

Remark: Reporting limit = Quantitation limit of analyte in sample

Page 122: resource… · 1 ICP Test Report Certification Packet Company name : Littelfuse, Inc. Product Series: FUSE - BF1 58V Product #: 142.5631.xxx Series Issue Date: August 22, 2012 It

Number : TWNC00258320

Test Conducted

Page 5 of 9 Intertek Testing Services Taiwan Ltd.

8F., No. 423, Ruiguang Rd., Neihu District, Taipei 114, Taiwan, R.O.C.

全國公證檢驗股份有限公司 114 台北市內湖區瑞光路 423 號 8 樓

Tel: (+886-2) 6602-2888.2797-8885 Fax: (+886-2) 6602-2400.6602-2401

(Ⅳ) Measurement Flowchart: Test for Cd/Pb/Hg/Chromium (VI)/PBBS/PBDES Contents Reference Standard: IEC 62321 edition 1.0:2008

Remarks: *1: List of Appropriate Acid:

Material Acid Added for Digestion Polymers HNO3,HCl,HF,H2O2,H3BO3 Metals HNO3,HCl,HF Electronics HNO3,HCl,H2O2,HBF4

*2: If the result of spot test is positive, Chromium VI would be determined as detected.

Sample preparation

For different material, digest the sample with appropriate acid*1

Make up with deionized water

Cd/Pb/Hg

Analyzed by ICP-OES

Weigh sample and add alkaline solution

Definite temp. extraction

Make up with deionized water and add diphenyl-carbazide solution

Cool and filter the extract

Cr6+

Weigh sample and add organic solvent

By Soxhlet extraction or Solvent extraction

Concentrate the extract and make upwith organic solvent

PBBs/PBDEs

Analyzed by UV-VIS

Analyzed by GC-MSD

By spot test

Get 50cm2 sample

By boiling water extraction

Metal Polymers / electronics

Negative *2

Confirm the tested samples are totally dissolved

Take sample and immerse into Aqua Regia, start to strip plating layer

Stop the stripping procedure upon color change completely

Take the Aqua solution as plating component and stripped body as substrate component

For non-metal part For metal part

Page 123: resource… · 1 ICP Test Report Certification Packet Company name : Littelfuse, Inc. Product Series: FUSE - BF1 58V Product #: 142.5631.xxx Series Issue Date: August 22, 2012 It

Number : TWNC00258320

Test Conducted

Page 6 of 9 Intertek Testing Services Taiwan Ltd.

8F., No. 423, Ruiguang Rd., Neihu District, Taipei 114, Taiwan, R.O.C.

全國公證檢驗股份有限公司 114 台北市內湖區瑞光路 423 號 8 樓

Tel: (+886-2) 6602-2888.2797-8885 Fax: (+886-2) 6602-2400.6602-2401

(Ⅳ) Measurement Flowchart:

Test for Halogen Content Reference Standard:EN 14582

Add absorbent in a combustion flask & place weighed sample in equipment

Fill oxygen into calorimetric bomb

Ignite then leave the bomb at room temperature

Transfer the absorbent into a volumetric flask

Make up with deionized water

Sampling/grinding or cutting

Analyzed by ion chromatography

Page 124: resource… · 1 ICP Test Report Certification Packet Company name : Littelfuse, Inc. Product Series: FUSE - BF1 58V Product #: 142.5631.xxx Series Issue Date: August 22, 2012 It

Number : TWNC00258320

Test Conducted

Page 7 of 9 Intertek Testing Services Taiwan Ltd.

8F., No. 423, Ruiguang Rd., Neihu District, Taipei 114, Taiwan, R.O.C.

全國公證檢驗股份有限公司 114 台北市內湖區瑞光路 423 號 8 樓

Tel: (+886-2) 6602-2888.2797-8885 Fax: (+886-2) 6602-2400.6602-2401

(Ⅳ) Measurement Flowchart: Test For Phthalates Contents Reference Method: EN 14372: 2004

Sampling/grinding or cutting

Weigh sample and add organic solvent

By solvent extraction

Concentrate the extract and make up with organic solvent

Analyzed by GC-MSD

Page 125: resource… · 1 ICP Test Report Certification Packet Company name : Littelfuse, Inc. Product Series: FUSE - BF1 58V Product #: 142.5631.xxx Series Issue Date: August 22, 2012 It

Number : TWNC00258320

Test Conducted

Page 8 of 9 Intertek Testing Services Taiwan Ltd.

8F., No. 423, Ruiguang Rd., Neihu District, Taipei 114, Taiwan, R.O.C.

全國公證檢驗股份有限公司 114 台北市內湖區瑞光路 423 號 8 樓

Tel: (+886-2) 6602-2888.2797-8885 Fax: (+886-2) 6602-2400.6602-2401

(Ⅳ) Measurement Flowchart: Test For Hexabromocyclododecane (HBCDD) Reference Standard:USEPA 3540C

End of Report

Sampling/grinding or cutting

Weigh sample and add organic solvent

By soxhlet extraction

Concentrate the extract and make up with organic solvent

Analyzed by GC-MSD

Page 126: resource… · 1 ICP Test Report Certification Packet Company name : Littelfuse, Inc. Product Series: FUSE - BF1 58V Product #: 142.5631.xxx Series Issue Date: August 22, 2012 It

Number : TWNC00258320

Test Conducted

Page 9 of 9 Intertek Testing Services Taiwan Ltd.

8F., No. 423, Ruiguang Rd., Neihu District, Taipei 114, Taiwan, R.O.C.

全國公證檢驗股份有限公司 114 台北市內湖區瑞光路 423 號 8 樓

Tel: (+886-2) 6602-2888.2797-8885 Fax: (+886-2) 6602-2400.6602-2401

Photo

Page 127: resource… · 1 ICP Test Report Certification Packet Company name : Littelfuse, Inc. Product Series: FUSE - BF1 58V Product #: 142.5631.xxx Series Issue Date: August 22, 2012 It

Test Report Number : TWNC00258319

Authorized By: On Behalf Of Intertek Testing Services Taiwan Limited

K. Y. Liang Director

This report shall not be reproduced except in full, without the written approval of the laboratory.

Page 1 of 5 Intertek Testing Services Taiwan Ltd.

8F., No. 423, Ruiguang Rd., Neihu District, Taipei 114, Taiwan, R.O.C.

全國公證檢驗股份有限公司 114 台北市內湖區瑞光路 423 號 8 樓

Tel: (+886-2) 6602-2888.2797-8885 Fax: (+886-2) 6602-2400.6602-2401

Applicant: Littelfuse, S.A. de C.V. Date : May 29, 2012 Blvd. Fausto Z. Martinez #1800

Col. Magisterio Seccion 38 C.P. 26070 Piedra Negras, Coahuila, Mexico

Sample Description:

One (1) group of submitted samples said to be : Part Description : SOLDER DIN Part Number : 353.1590.0001 Date Sample Received : May 17, 2012 Date Test Started : May 19, 2012

Test Conducted :

As requested by the applicant, for details please refer to attached pages.

Page 128: resource… · 1 ICP Test Report Certification Packet Company name : Littelfuse, Inc. Product Series: FUSE - BF1 58V Product #: 142.5631.xxx Series Issue Date: August 22, 2012 It

Number : TWNC00258319

Test Conducted

Page 2 of 5 Intertek Testing Services Taiwan Ltd.

8F., No. 423, Ruiguang Rd., Neihu District, Taipei 114, Taiwan, R.O.C.

全國公證檢驗股份有限公司 114 台北市內湖區瑞光路 423 號 8 樓

Tel: (+886-2) 6602-2888.2797-8885 Fax: (+886-2) 6602-2400.6602-2401

(Ⅰ) Test Result Summary : Result (ppm)

Test Item Silvery Metal

Heavy Metal

Cadmium (Cd) content ND Lead (Pb) content ND Mercury (Hg) content ND Chromium VI (Cr6+) content (mg/kg with 50cm2) Negative (< 0.02)

Remarks: ppm = Parts per million based on weight of tested sample = mg/kg ND = Not detected < = Less than mg/kg with 50cm2 = milligram per kilogram with 50 square centimetre Negative = A negative test result indicated positive observation

was not found at the time of Test.

Responsibility of Chemist :Irene Chiou / Kevin Liu / Cathy Chen

Date Sample Received : May 17, 2012 Test Period : May 19, 2012 To May 28, 2012

(Ⅱ) RoHS Requirement:

Restricted Substances Limits

Cadmium (Cd) Content 0.01% (100ppm) Lead (Pb) Content 0.1% (1000ppm) Mercury (Hg) Content 0.1% (1000ppm) Chromium VI (Cr6+) Content 0.1% (1000ppm)

The above limits were quoted from 2002/95/EC and amendment 2005/618/EC for homogeneous material.

Page 129: resource… · 1 ICP Test Report Certification Packet Company name : Littelfuse, Inc. Product Series: FUSE - BF1 58V Product #: 142.5631.xxx Series Issue Date: August 22, 2012 It

Number : TWNC00258319

Test Conducted

Page 3 of 5 Intertek Testing Services Taiwan Ltd.

8F., No. 423, Ruiguang Rd., Neihu District, Taipei 114, Taiwan, R.O.C.

全國公證檢驗股份有限公司 114 台北市內湖區瑞光路 423 號 8 樓

Tel: (+886-2) 6602-2888.2797-8885 Fax: (+886-2) 6602-2400.6602-2401

(Ⅲ) Test Method: Test Item Test Method Reporting Limit

Cadmium (Cd) content

With reference to IEC 62321 edition 1.0:2008 in clause 8/9/10, by microwave digestion until the tested samples are totally dissolved and determined by ICP-OES.

2 ppm

Lead (Pb) content

With reference to IEC 62321 edition 1.0:2008 in clause 8/9/10, by microwave digestion until the tested samples are totally dissolved and determined by ICP-OES.

2 ppm

Mercury (Hg) content

With reference to IEC 62321 edition 1.0:2008 in clause 7, by microwave digestion until the tested samples are totally dissolved and determined by ICP-OES.

2 ppm

Chromium VI (Cr6+) content

With reference to IEC 62321 edition 1.0:2008 in annex B, by boiling water extraction and determined by UV-Vis Spectrophotometer.

0.02 mg/kg with 50cm2

Remark: Reporting limit = Quantitation limit of analyte in sample

Page 130: resource… · 1 ICP Test Report Certification Packet Company name : Littelfuse, Inc. Product Series: FUSE - BF1 58V Product #: 142.5631.xxx Series Issue Date: August 22, 2012 It

Number : TWNC00258319

Test Conducted

Page 4 of 5 Intertek Testing Services Taiwan Ltd.

8F., No. 423, Ruiguang Rd., Neihu District, Taipei 114, Taiwan, R.O.C.

全國公證檢驗股份有限公司 114 台北市內湖區瑞光路 423 號 8 樓

Tel: (+886-2) 6602-2888.2797-8885 Fax: (+886-2) 6602-2400.6602-2401

(Ⅳ) Measurement Flowchart:

Test For Cd/Pb/Hg/Chromium (VI) Reference Standard:IEC 62321 edition 1.0:2008

Remarks: *1: List Of Appropriate Acid:

Material Acid Added For Digestion

Polymers HNO3,HCl,HF,H2O2,H3BO3 Metals HNO3,HCl,HF Electronics HNO3,HCl,H2O2,HBF4

*2: If the result of spot test is positive, Chromium VI would be determined as detected.

End of Report

Sampling/grinding or cutting

For different material, digest the sample with appropriate acid*1

Make up with deionized water

Cd/Pb/Hg

Analyzed by ICP-OES

Weigh sample and add alkaline solution

Definite temp. extraction

Make up with deionized water and add diphenyl-carbazide solution

Cool and filter the extract

Cr6+

Analyzed by UV-VIS

By spot test

Get 50cm2 sample

Boiling water extraction

Metal Polymers / Electronics

Negative*2 Confirm the tested samples are totally dissolved

Page 131: resource… · 1 ICP Test Report Certification Packet Company name : Littelfuse, Inc. Product Series: FUSE - BF1 58V Product #: 142.5631.xxx Series Issue Date: August 22, 2012 It

Number : TWNC00258319

Test Conducted

Page 5 of 5 Intertek Testing Services Taiwan Ltd.

8F., No. 423, Ruiguang Rd., Neihu District, Taipei 114, Taiwan, R.O.C.

全國公證檢驗股份有限公司 114 台北市內湖區瑞光路 423 號 8 樓

Tel: (+886-2) 6602-2888.2797-8885 Fax: (+886-2) 6602-2400.6602-2401

Photo