manufacturer since 1873 selection of standard display of results pmove jog-wheel operation system...

WWW.PETROTEST.COMManufacturer since 1873

2

Softening-Point (RKA)

Breaking-Point (BPA)

Flash-Point (CLA)

Petrotest® Instruments GmbH & Co KG... is producing high quality laboratory instruments for the research of petroleum products under quality control according to ISO 9001.

A wide range of equipment for the determination of the physical behavior of bitumen is offered.

Users of these instruments are mainly: • Refi neries• Road Construction Companies• Roofi ng Felt Manufacturers • Producers of Protective Coating for Architecture• Material Testing Authorities • Research Sections of Universities and Independent Test Institutions

Penetrometer (PNR)

Bitumen Methods / Info .................................................................................. 3

Softening-Point (RKA) ............................................................................ 4 - 9

Tensile Properties (DDA, DD) ................................................................ 10 - 15

Penetration & Texture (PNR, Rheotex) ................................................... 16 -19

Breaking-Point (BPA) ............................................................................. 20 - 23

Stiffness (BBR) .............................................................................................. 24

Viscosity (DSR, RV) ............................................................................... 25 - 35

Aging (LOH, TFOT, RTFOT, RFT, PAV) .................................................. 36 - 40

Flash-Point (ABA, CLA, PMA) ................................................................ 41 - 51

Paraffi n Content ............................................................................................ 52

Water Content ......................................................................................... 53 - 55

Distillation ............................................................................................... 56 - 59

Density & Weight .................................................................................... 61 - 64

Sampling ........................................................................................................ 65

General Equipment Reference Material ..................................................................................... 66Miscellaneous Equipment .......................................................................... 67Tempering Equipment ......................................................................... 68 - 69

Tables of Contents

Keywords .................................................................................................... 71Order Numbers ................................................................................... 72 - 74Standards ................................................................................................... 75

Petrotest® Company ...................................................................... on the rear

ContentsContents

3

Bitumen MethodsBitumen Methods

Aging ...................................... [page 36-40]

Loss-On-Heat Method (LOH) ............... [36]To determine the volatility upon heating by measuring the loss in mass.Suitable for bitumen (asphalt), fl ux oil & bituminous binders.

Thin-Film-Oven Method (TFOT) ........... [36]To determine the effects of heat & air during conventional hot-mixing on a thin fi lm of semi-solid bitumen.Suitable for bitumen (asphalt), fl ux oil & bituminous binders.

Rolling Thin-Film-Oven Meth. (RTFOT) [38]To determine the resistance to hardening under infl uence of heat and air and the change in sample mass (Loss-on-Heat).Suitable for bitumen (asphalt) & bituminous binders.

Rotating Flask Method (RFT) ............... [39]To determine the effects of heat and air during conventional hot-mixing on a moving thin fi lm.Suitable for bituminous binders.

Pressure Aging Vessel Method (PAV) .. [40]To simulate the accelerated long-term aging, the type of in-service oxidative aging that occurs in binders during pavement service. Suitable for bitumen (asphalt) & bituminous binders.

Breaking-Point (FRAASS) ..... [20-23] To determine the temperature of any homogeneous road or industrial bitumen at which a bitumen tends to break rather than to fl ow when stressed.

Density & Weight ....................... [61-64]

Displacement Method ........................... [64]To determine the density or relative density with a balance.Suitable for hard pitches and asphalts with softening points above +70°C.

Hydrometer Method ............................... [62]To determine the density of samples at room temperature.Suitable for cutback asphalts.

Pycnometer Method .............................. [61]To determine the density and relative density by use of capillary-stopperd Gay-Lussac & Hubbard or bicapillary Lipkin Pycnometer.Suitable for petroleum products like liquid, semi-solid or solid bituminous materials, asphalt cements, and soft tar pitches by use of a pycnometer.

Distillation ..................................... [56-60]

Cut-Back & Road Tar Method ......... [56, 58]To measure the amount of the more volatile constituents.Suitable for cut-back asphaltic (bituminous) products and fl uxed bitumens.

Pitch Method........................................... [60]To identify the quality of pitch to avoid problems of fuming or instability in use.Suitable for hard and soft pitch.

Flash Point .................................... [41-51]To defi ne the hazards of fl ammable and combustible materials according to shipping and safety regulations. Therefore the tendency to form a fl ammable mixture with air is detected by measuring the fl ash-point temperature.

Abel Method (ABA) ........................... [48, 51]Suitable for closed cup tests within a range of +10 °C (+50 °F) to +110 °C (+230 °F) or -30 °C (-22 °F) to +110 °C (+230 °F).

Cleveland Method (CLA) .................. [41, 43]Suitable for open cup tests within a range of +79 °C (+175 °F) to +400 °C (+752 °F).

Pensky-Martens Method (PMA) ..... [44, 47]Suitable for closed cup tests within a range of +40 °C (+104 °F) to +360 °C (+680 °F).

General Equipment ................... [67-69]

Paraffi n Content .............................. [52]

Distillation Method................................. [52]To determine the paraffi n wax content.Suitable for bitumen and bituminous binder.

Penetration & Texture ............... [16-19]

Penetrometer Method ............................ [16]Cone-Penetration:To determinate the consistency of hot-applied, fuel-resistant joint sealants with or without being immersed in fuel or oil.Needle-Penetration:To measure the consistency of semi-solid and solid bituminous mixtures.Rod-Penetration:To measure the apparent viscosity (Bitumen No) of fi ller aggregates used in bituminous mixtures.

Texture Method ....................................... [18]To measure load forces as well as tensile stresses, which occur when a test body is pushed into the tested material or withdrawn.Suitable for bituminous materials, hot-applied pavement sealants & fi llers and cement.

Reference Fluids ............................. [66]

Sampling ............................................. [65]

Boring, Bottle, Grease, Thief, Tube Method [65]To take liquid, semi-solid or solid samples.Suitable for liquids, lubricating greases, soft waxes or soft bitumens similar to grease in consistency, waxes and soft solids.

Softening-Points ........................... [4-9]Ring & Ball Method .............................. [4, 8]To determine the temperature at which a substance attains a particular degree of softness.Suitable for bitumen & bituminous binders, fi ller aggregats used in bituminous mixtures, binders for paints and varnishes and resins derived from naval stores.

Wilhelmi Method ................................... [7, 9]To determine the temperature at which a hot casting substance used for road construction attains a particular degree of softness.Suitable for joint sealing compounds in road construction and thermoplastic materials for pavement marking.

Stiffness .............................................. [24]

Bending Beam Method (BBR) .............. [24]To determine the fl exural creep stiffness at low temperatures.Suitable for asphalt binders.

Tensile Properties (Ductility) . [10-15]

The Ductility or Elongation is measured by the distance to which a bitumen briquette will elongate before breaking when pulled apart.The Force-Ductility measures tensile properties of modifi ed bitumen on the basis of the performed force and the specimen strain.The Elastic Recovery of modifi ed bitumen is measured by the recoverable strain determined after severing an elongated briquette specimen.

Viscosity ......................................... [25-35]

Capillary Method (CFOV, RFV, ZCAV, CMVV, AIVV) ......... [31]To characterize the fl ow behavior and to determine the consistency by measuring the kinematic or dynamic viscosity.Suitable for liquid asphalts (bitumens), their distillation residues, road oils or asphalt cements.

Dynamic Shear Method (DSR) ............. [25]To measure the linear viscoelastic properties.Suitable for modifi ed or unmodifi ed (aged or unaged) asphalt binders

Engler Method ........................................ [30]Used for characterizing the consistency by measuring the fl ow properties to determinate the specifi c viscosity. Suitable for tar and their fl uid products.

Rotational Method (RV) ......................... [26]To determine the apparent viscosity at elevated temperatures.Suitable for asphalt.

Road Tar Method .................................... [27]To measure of the viscosity by determining the effl ux time of a warm sample, through a 10 or 4 mm orifi ce.Suitable for road tars, cutback asphalts and high-viscous bitumen emulsions with effl ux times in the range of 15 to 500 sec.

Saybolt Method ...................................... [28]To determine the Saybolt Universal Viscosity or the Saybolt Furol Viscosity by measuring the effl ux time of a sample.Suitable for lubricants, fuel oils and residual materials.

Water Content .............................. [53-55]

Distillation Method................................. [53]To determine the water content of a sample.Suitable for petroleum products, tars, and other bituminous materials.

4

Selection of Standard

Display of Results

PMoveJog-Wheel operation

system

Softening-Point - Ring & Ball Method - RKA 5 (automatic)

Bitumen and bituminous binders: ASTM D 36 - AASHTO T 53 EN 1427 (DIN 52 011, NF T66-008) IP 58 JIS K2207Filler aggregats in bituminous mixtures: EN 13179-1Wilhelmi-Option: DIN 1996-15 EN 1871-F

The RKA 5 instrument features a microprocessor technology combined with a smart jog-wheel operation system. It maintains program sequences for all relevant test standards and bath liquids as well as for user defi ned test conditions.

An infrared radiator along with a controlled magnetic stirrer ensure the optimum test conditions, the four-wire Pt-100 and the laser-based ball detection probe guarantee precise test results. A draft defl ector stabilizes ambient and homogeneous heating conditions, the lifting traverse simplifi es setup and handling of the test rack.

An optional automatical system leads and dispenses the balls to the specimens.

The test procedure is supported by intelligent software routines, at the end an automated test assessment is done. Heat gradients are precisely recorded and are available as printouts. Test results can be stored in the instrument and / or transferred via USB.

Keyboard or barcode scanner options are avaiable as input support.

Scope of ApplicationTo determine the temperature at which a substance attains a particular degree of softness.Suitable for bitumen & bituminous binders, fi ller aggregates used in bituminous mixtures, binders for paints and varnishes and resins derived from naval stores.

Summary of MethodTwo horizontal disks of a sample (cast in shouldered rings) are heated at a controlled rate in a liquid bath (up to 80°C in distilled water or silicone oil, above +80°C in glycerin or silicone oil) while each supports a steel ball. The softening-point is reported as the mean of the temperatures at which the two disks soften enough to allow each ball to fall a distance of 25 mm.

Softening-PointSoftening-Point

5

10-0888

10-0856 (& stirrer ring)

25-0910/1/2

10-0868

25-0920

Laser Scanner

Main Units

10-080010-0801

RKA 5 - Automatic Softening-Point Tester Ring and Ball MethodASTM D 36 - AASHTO T 53 - EN 1427 (DIN 52 011, NF T66-008) - IP 58 - JIS K2207 EN 13 179-1 (With optional accessories for: EN-1871-F (DIN 1996-15) or referee tests acc. IP & NF)Further for resins (ASTM E 28), paints and varnishes (ISO 4625-1 - BS 6782-6) and thermoplastic adhesives (EN 1238 (NF T76-106))Features:• Pmove® - innovative operation platform• large color display - visible from 10 m (30 ft.)• easy Firmware-upload via USB • compact ball detection system• Ready-to-Go unit for two simultaneous testsConsisting of:CPU:Up-to-date dual OMAP controller technology featuring a real-time DSP and a multimedia coprocessor, 4.7” full graphical color display, graphical menu guidance and intuitive user concept (Pmove®), help key (explanation of important device/ program features), Jog-Wheel operation (turn & push), large-area device status indicator (light ring), zooming temperature reading, device & data management via LAN, USB or RS232, extended statistical and database functionality, automatic assessment of results according to individual standards, printout on heat gradient conformity.Electronic device features:Automatic self check of sensors and system, multipoint calibration of temperature sensor (Pt-100), compact ball sensing system consisting of a precise 3D-adjustable laser scanner.Mechanical device features:Infrared radiator technology with temperature control, CERAN heat plate, standardized beaker with barcode imprint, test rack with slide bearing and single-hand fi xation, Pt-100 gold plated four-wire system (also available with calibration certifi cate), test rings, load balls, centering guides, stirring wheel, holding tong, mechanical ball centering system, software controlled stirrer system, transparent draft defl ector.Supplied with:10 rings (shouldered), 10 load balls, 1 gauge ball, 1 test rack with mechanical ball centering unit (standard type upon request), 1 glass-beaker bath (600ml) with barcode, 1 tongs (aluminum), 1 temperature probe (Pt-100) 1 test tube (as Pt-100 tray), 1 magnetic stirrer (ring shape), 1 pouring plate (brass)Note:Accessories like electromagnetic ball & centering unit, external USB-keyboard, barcode scanner, printer (USB, serial), memory stick, bath liquid and optional test accessories are not included.Technical Data: Test places : 2 (for simultaneous tests)Housing : stainless steel, two colored powder coatingInterface : 1 serial RS232, 3 USB, 1 LAN (LIMS)Dimensions : 230 x 470 x 460 cm (WxDxH), Weight: 10 kgPower supply : 230 V, 50/60 Hz, EU-plugPower supply : 115 V, 50/60 Hz, US-plug

Accessories25-091025-091125-0912

Keyboard - german layout, 86 keys, USB/PS2-connection - english layout, 86 keys, USB/PS2-connection - french layout, 86 keys, USB/PS2-connection

25-0920 Barcode-Scanner, USB

25-0919 Memory Stick, 2 GB, USB 2.0 (verifi ed for Petrotest®-units)

25-028225-0283

Impact Printer for single sheet & continuous paper, serial (For details see: General Equipment)Power supply : 220-240 V, 50/60 HzPower supply : 110-130 V, 50/60 Hz

25-090225-0903

Laser Printer (Mono), duplex, for single sheet, USB (For details see: General Equipment)Power supply : 220-240 V, 50/60 HzPower supply : 110-115 V

25-0930Receipt Impact Printer (POS) for paper rolls, serial (For details see: General Equipment)Power supply : 120/230 V, (AC converter output 7 V)

50-916051-9151

Bath Liquid, silicone oil M50, 1 kg, water clear, heat resistant up to approx. +200 °Cglycerin, 99% pure, 1 kg

10-0868 Service Kit - RKA 5 Consisting of 1 each: reference plug 20°C & 180°C, scanner & ball gauge, visor, USB-memory stick, SD card, scraper, plastic cleaner and tool set

10-084710-0848

Temperature Probe Pt-100 (glass), 5 certifi ed values at 0/+20/+40/+60/+80°C 7 certifi ed values at +30/+60/+90/+120/+180/+200°C


6

Electromagnetic Ball Dispense(comfortable Petrotest® setup)

Test Rack with: mechanical Petrotest® ball centering & dispense device(10-0840 and accessories)

Test Rack for use with: - ball centering guides (10-0841, 2x 10-0052)- in combination with electro-magnetic ball dispensers & guides (10-0851)

Standard Ball Centering Device(10-0841 & 2x 10-0052)

(a standard setup with centering guides, substitutional for 10-0840)

Petrotest® Ball Dispense & Centering Device (10-0840)

(convenient Petrotest® setup, included in standard delivery)

“Mechanical Ball Centering & Dispense Device” (included in the standard delivery)

10-0840 Test Rack - RKA 5-Dispensing Devicewith mechanical Petrotest® ball centering & dispensing device

Accessories10-0805 Load Balls, blackened steel

(Ø 9.5 mm, 3.5 g), pack of 10

“Manual Ball Dispense” Option (to be ordered as replacement for the incl. 10-0840)

10-0841 Test Rack - RKA 5-Centering Guideto be used with 2 ball centering guides

10-0052 Ball Centering Guide for shouldered rings

Accessories10-0049 Rings, shouldered,

nickel-plated brass, pack of 10

10-0805 Load Balls, blackened steel (Ø 9.5 mm, 3.5 g), pack of 10

“Electromagnetic Ball Dispense” Option 10-0851 Test Rack Kit -

RKA 5-Electromagneticfor electromagnetic ball dispensing Consisting of: 1 test rack for centering guides2 electromagnetic ball dispensers 2 test tubes, as ball dispenser holder2 ball centering guides

Spare Parts10-0052 Ball Centering Guide

10-0841 Test Rack - RKA 5-Centering Guideto be used with 2 ball centering guides & 2 ball dispensers

10-0850 Ball Dispenser, electromagnetic

17-0158 Test Tube, borosilicate glass (to hold the ball dispenser or Pt-100)


710-0052 & 10-0049

Load Balls (for RKA5 instruments only)

(10-0805 & 10-0877)

10-0051 & 10-0048

RKA with options

10-0079 & Rings

Modifi ed Test Rack with accessories similar to Wilhelmi Method (10-0860 & 10-0864)

10-0860

10-0864


“Wilhelmi-Method” Option (for manual or automatic ball detection) 10-0860 Test Rack Kit -

RKA 5-Wilhelmi - manual detection (EN 1871 / DIN 1996-15) used for Mastix determinationConsisting of: 1 test rack 1 ring with bayonet lock 10 load balls (Ø 15 mm, 13.9 g) 1 magnetic ball dispenser 1 temperature probe Pt-100, 1 glass beaker (1000 ml) 1 pouring plate (50 x 75 mm) 1 Allen key (2 mm)

10-0864 Test Rack Extension - RKA 5-Wilhelmi - automatic detection (similar to EN 1871 / DIN 1996-15) requires Test Kit 10-0860Consisting of: 1 rod (50 mm) 1 bottom plate, perforated 2 distance pieces (25 mm)

Spare Parts10-0075 Ring (Wilhelmi) with bayonet lock

10-0877 Load Balls (Wilhelmi), blackened steel (Ø 15 mm, 13.9 g), pack of 10

10-0906 Glass Beaker (Wilhelmi) (1000 ml) with barcode (as bath)

10-0846 Temperature Probe (Wilhelmi) Pt-100 (fi ts 10-0860 only)

10-0865 Ball Dispenser (Wilhelmi), magnetic

17-0237 Allen Key (2 mm)

10-0861 Test Rack - RKA 5-Wilhelmi for manual ball detection

Option “former referee tests acc. IP 58 & NF T66-008” 10-0048 Rings, tapered

(former IP & NF), pack of 1010-0051 Ball Centering Guide for tapered rings

(former IP & NF)

Spare Parts10-0049 Rings, shouldered,

nickel-plated brass, pack of 10 (acc. ASTM, ISO, EN, IP, NF)

10-0805 Load Balls, blackened steel (Ø 9.5 mm, 3.5 g), pack of 10

10-0079 Pouring Plate, brass, U-shape (50 x 75 mm) to fi ll the rings

10-0840 Test Rack - RKA 5-Dispensing Devicewith mechanical Petrotest® ball centering & dispensing device

10-0856 Glass Beaker (600 ml) with barcode (as bath)

50-5227 Magnetic Stirrer Ring (Ø 57 mm)

50-5317 Tongs for beaker (aluminum)

10-0849 Temperature Probe Pt-100 (glass)(also available certifi ed!)

17-0158 Test Tube, borosilicate glass (to hold the ball dispenser or Pt-100)

10-0888 Gauge-Ball - RKA 5for light barrier adjustment

8 50-5315

Ring & Ball Accessories

10-0281

10-0455


Scope of ApplicationTo determine the temperature at which a substance attains a particular degree of softness.

Suitable for bitumen & bituminous binders, fi ller aggregates used in bituminous mixtures, binders for paints and varnishes and resins derived from naval stores.

Summary of MethodTwo horizontal disks of a sample (cast in shouldered rings) are heated at a controlled rate in a liquid bath (up to +80 °C in distilled water or silicon oil, above +80 °C in glycerin or silicon oil) while each supports a steel ball. The softening-point is reported as the mean of the temperatures at which the two disks soften enough to allow each ball to fall a distance of 25 mm.

Softening-Point - Ring & Ball Method (manual)

Bitumen and bituminous binders: ASTM D 36 - AASHTO T 53EN 1427 (DIN 52 011, NF T66-008) - IP 58JIS K2207

Filler aggregats in bituminous mixtures: EN 13179-1(Wilhelmi-Option: see next page)

Main Units

10-028110-0284

Manual Softening-Point Tester, Ring & Ball MethodASTM D 36 - AASHTO T 53 - EN 1427 (DIN 52 011, NF T66-008) - IP 58 - JIS K2207 EN 13 179-1 (with optional accessories for referee tests acc. IP & NF)Further for resins (ASTM E 28), paints and vanishes (ISO 4625-1 - BS 6782-6)Features: • 2 simultaneous tests• electric heating• electric stirrerConsisting of:electric heater (800 W) in stainless steel housing with electronic power regulator, 4 heater rods, electric stirrer and support for two test ringsSupplied with: 10 shouldered rings, 10 load balls, 2 ball centering guides, 2 thermometers (precision made, 1 x ASTM 15C, 1 x ASTM 16C), 1 glass beaker (600 ml), 1 heater support board (bored, 50 mm / 2”), 1 pouring plate (brass), 1 mortar with pestleNote: Bath liquids & accessories acc. IP & NF referee tests are not included. Technical Data:Test places : 2Working range : approx. +25 to +200 °C Dimensions : 16 x 18.5 x 20.5 cm (W x D x H), Weight: 3 kgPower supply : 230 V, 50/60 Hz, 800 W, EU-plugPower supply : 115 V, 50/60 Hz, 800 W, US-plug

Options & Accessories50-5315 Tongs for beaker

50-9167 Bath Liquid, silicon oil, water clear, 1 kg, water clear, heat resistant up to approx. +250 °C, viscosity at +25 °C: 190 till 210 mPa·s

For former referee tests acc. IP 58 & NF T66-008:10-0048 Rings, tapered (former IP & NF), pack of 1010-0051 Ball Centering Guide for tapered rings (former IP & NF)

Thermometers

Precision Made

Offi cially Certifi ed

TypeRange

ASTM IP10-0061 10-0062 15C 60C -2 to +80 : 0.2 °C10-0063 10-0064 15F - +30 to +180 : 0.5 °F10-0065 10-0066 16C 61C +30 to +200 : 0.5 °C10-0067 10-0068 16F - +85 to +392 : 1.0 °F

Spare Parts10-0052 Ball Centering Guide

for shouldered rings

10-0055 Load Balls, steel (Ø 9.5 mm, 3.5 g), pack of 10

10-0049 Rings, shouldered, nickel-plated brass, pack of 10 (acc. ASTM, ISO, EN, IP, NF)

10-0455 Ring-Holder Assembly for 2 rings

10-0056 Glass Beaker (600 ml) as bath

10-0070 Mortar with pestle (ISO 4625, ASTM E 28)

10-0079 Plate, brass, U-shape (50 x 75 mm) as pouring plate to fi ll the rings

11-0138 Support Board for heater, glass ceramics, (150 x 150 x 4 mm), with center hole (Ø 50 mm / 2”)

11-0018 Heater Rod, 200 W, 115-230 V

11-001911-0029

Heating Element (4 heater rods)... 230 V, 50/60 Hz, 800 W ... 115 V, 50/60 Hz, 800 W

25-000425-0009

Control Module “M2” to regulate the heating power... 230 V, 50/60 Hz... 115 V, 50/60 Hz

25-004225-0043

Electric Stirrer with propeller blade... 230 V, 50/60 Hz, EU-plug... 115 V, 50/60 Hz, US-plug

9

Wilhelmi-Ring (10-0075)

10-0071

Scope of ApplicationTo determine the temperature at which a hot casting substance used in road construction attains a particular degree of softness.

Suitable for joint sealing compounds in road construction and thermoplastic materials for pavement marking.

Summary of MethodA horizontal disk of a sample casted in a ring supports a steel ball and is heated at a controlled rate in a liquid bath (up to +80°C in distilled water or silicon oil, above +80°C in glycerin or silicon oil).The softening-point is reported as the temperature at which the softening disk experiences a plastic deformation.

Softening-Point - Wilhelmi Method (manual)

Bituminous materials: DIN 1996-15 Thermoplastic materials: EN 1871-F

Main Unit

10-0071

Manual Softening-Point Tester, Wilhelmi MethodFeatures: • single test place• electric heating• electronic power regulatorConsisting of:electric heater (800 W) in stainless steel housing with electronic power regulator “M2”, 4 heater rods, laboratory stand (1 bar, 1 special clamp, 1 ring support)Supplied with: 1 Wilhelmi-ring, 10 load balls 2 thermometers (precision made, 1 x ASTM 15C, 1 x ASTM 16C), 1 glass beaker (1000 ml), 1 heater support board (bored, 50 mm / 2”), 1 pouring plate (glass)Technical Data:Test place : 1Working range : approx. +25 to +200 °C Dimensions / Weight : 16 x 18.5 x 20.5 cm (W x D x H), 3 kgPower supply : 230 V, 50/60 Hz, 800 W, EU-plug

Options & Accessories50-5315 Tongs for beaker

50-9167 Bath Liquid, silicon oil, water clear, 1 kg, heat resistant up to approx. +250 °C, viscosity at +25 °C: 190 till 210 mPa·s

For automatic tests see Ring & Ball-Apparatus RKA 5:10-0800 RKA 5 - Automatic Softening-Point Tester, Ring & Ball Method

10-0860 Test Rack Kit RKA 5-Wilhelmi - manual detection together with 10-0864 Test Rack Kit RKA 5-Wilhelmi - automatic detection

Thermometers

Precision Made


TypeRange

ASTM IP10-0061 10-0062 15C 60C -2 to +80 : 0.2 °C10-0063 10-0064 15F - +30 to +180 : 0.5 °F10-0065 10-0066 16C 61C +30 to +200 : 0.5 °C10-0067 10-0068 16F - +85 to +392 : 1.0 °F

Spare Parts10-0077 Load Balls (Wilhelmi), steel

(Ø 15 mm, 13.9 g), pack of 10

10-0075 Ring (Wilhelmi) with bayonet lock

10-0076 Ring-Holder (Wilhelmi)

10-0106 Beaker (1000 ml), glass, low shape, with spout, as bath

10-0057 Plate, glass (120 x 120 x 6 mm) as pouring plate to fi ll the rings

11-0138 Support Board for heater, glass ceramics, (150 x 150 x 4 mm)with center hole (Ø 50 mm / 2”)

11-0018 Heater Rod, 200 W, 115-230 V

11-0019Heating Element (4 heater rods)... 230 V, 50/60 Hz, 800 W

25-0004

Control Module “M2” to regulate to heating power... 230 V, 50/60 Hz


10

Temperature Probes

Molds

Scope of ApplicationThe Ductility or Elongation is measured by the distance to which a sample will elongate before breaking when two ends of a specimen briquette are pulled apart at a specifi ed speed and at a specifi ed temperature.It may be used for quality specifi cations.

The Force-Ductility measures tensile properties on the basis of the performed force and the specimen strain.A specimen briquette is pulled apart at a specifi ed speed and at a specifi ed temperature until the briquette ruptures or a specifi ed strain is achieved.

The Elastic Recovery is measured by the recoverable strain determined after severing an elongated briquette specimen. The specimens are pulled to a specifi ed distance at a specifi ed speed and at a specifi ed temperature.This is useful in confi rming that a material has been added to the asphalt to provide a signifi cant elastomeric characteristic.

Tensile Properties - Force-Ductilometer Method - DDA 3 (automatic)

Elongation: ASTM D 113 - AASHTO T 51 - JIS K2207 DIN 52 013 (IP 32, NF T 66-006)

Force-Ductility: EN 13589 - IP 520 EN 13703 - IP 515 - AASHTO T 300

Elastic Recovery: ASTM D 6084 EN 13398 (DIN V 52 021-1) - IP 516 (ASTM D 5892 - ASTM P 226)

With the ductility machines of the DDA 3 series the afore mentioned procedures can be performed automatically. Except for recovery tests, 3 tests can be performed simultaneously.

The drive is microprocessor controlled and uses a stepping motor and a feed rod. Both are located outside the tempering bath and therefore are not affected by corroding infl uences of the bath liquid.The tempering bath itself is double-walled with an outer water circulation system.The tractor cradle is made of stainless steel as well as the bath walls.

If extremely thin threads are measured, the built-in circulation pump for the inner bath can be switched off.

A very even and exact temperature can be obtained in the bath by the connection of a good coolant circulator and due to several temperature probes plus the transparent bath cover.

Traction speed, elongation and pauses can be pre-set on the control unit.During the whole test run the tensile force on each line is permanently measured. The maximum tensile force may be up to 300 Newton’s per line.

With the DDA 3 a minimum tensile force margin can be set. When a bitumen briquette ruptures and the tensile falls below this setting, the pertinent elongation will be stored and the machine will be stopped automatically after all three briquettes have broken.

There is a special program for recovery tests of polymer-modifi ed bitumen.The bitumen briquette will be expanded to a pre-set elongation, then the tractor (after a pause) returns to a position where no more stress is in the material, equivalent to the cut-up state of the specimen. If due to any recovery of the material a tension should occur, the tractor will move until there is a stress-free condition again.

The control unit is equipped with two RS232 interface. This allows to connect a serial printer and a PC to record all test parameters, the fi nal values on each test line as well as peaks with their pertinent elongation.Further, the DDA 3 has analog output sockets so that force/elongation curves can be drawn.

The ductility meters are also available as DD 3 in a basic version without force measurement. These models have a digital indication of the elongation only.

Tensile PropertiesTensile Properties

11

Software Diagram "Force"

Recovery Test

Elongation Test

Software Diagram "Recovery"

Printer Chart "Recovery"

Printer Chart

Located Points

DDACon-SoftwareA program for recording, saving and graphic presentation of DDA values.Replacing analog line recorder or serial data-printer, allows to control the DDA by PC, the data-transfer to MS EXCEL® or LIMS and simplifi es the download of fi rmware-upgrades.The sample status of up to 3 samples will be displayed simultaneously, indicating the traction distance or for Recovery-tests the percentage of relief and the total energy.Signifi cant points like the local minimum, maximum, turn-points of in- & decreasing fl anks and tangent-points can be determined automatically and displayed as diagram or chart.The numerical display of force or distance for a single point on the curve is possible, too.

Individual diagram areas can be increased, curves can be hidden or indicated numerically.Since every sample will be saved under an individual fi lename, it is possible to compare 3 samples of different tests with each other.The evaluated data can be exported as ASCII-fi les. They include information like the sample name, fi le name, user ID, date & time, duration, program, speed, temperature at start & end, status and distance & force.Printing of numerical or graphic evaluations, including relevant point like maxima and fracture are possible on a usual printer.

Main UnitsDDA 3 - Automatic Tensile Property Tester, Force-Ductilometer MethodDepending on the accessories suitable for: Elongation: ASTM D 113 - AASHTO T 51 - JIS K2207 - DIN 52 013Recovery : ASTM D 6084 - EN 13 398 - IP 516Force : EN 13 589 - IP 520 - EN 13 703 - IP 515 - AASHTO T 300 (obs.: ASTM D 5892, ASTM P 226, DIN V 52021-1, IP 32, NF T 66-006)Features: • 2 elongation & 2 recovery programs• variable traction speed up to 140 mm/min.• force detection by high resolution (10 mN) 300 N-sensors• automatic rupture detection above 20 mN is possible• constancy of speed and temperature at minor bath motion is better than demanded by the standards• without cooling coils, therefore easy to cleanConsisting of:Bath: for 3 simultaneous tests, made of stainless steel, double-walled and full insulated, closed cycle cooling system, circulation pump to be switched off, temperature probe, bath illumination and acrylic bath cover.Control Unit: with microprocessor, membrane keypad, analog output for 3 force-channel line-recorder, RS232-interfaces for printer & PC. Digital display (LCD) of: program, traction speed, distance, tensile force and temperature4 Programs: - Semi-Automatic Elongation for rupture forces below 20 mN

- Automatic Elongation for rupture forces of 20 mN to 300 N- Semi-Automatic Elastic Recovery for polymer modifi ed bitumen (in accordance with ASTM D 6084, EN 13 398 and other methods)- Automatic Elastic Recovery for polymer modifi ed bitumen (similar to ASTM D 6084 and other methods)

Serial Impact Printer: for single sheet & continuous paper (incl. data transmission cable)makes printouts of 3 test points with following parameters:program, traction speed, distance, tensile forces, temperatures, percentage of elastic recovery, energy (the result of integral) (not suitable for DDACon-software printouts)Note: External cooling device for fi lling the bath-jacket is required.

Windows® PC-Software DDACon is available.Technical Data : Working range : approx. -10 to +60 °C (depending on the cooler)Travel length : 100 cm or 150 cm (maximum)Test positions : 3 (in a 30 l or 45 l bath)Traction speed : Standard: 50 mm/min. / Variable: 2.5 to 140 mm/min.Tension force : 300 N (maximum)Connections for : line-recorder, serial printer, PC (RS232), cooler as tempering & fi lling device (Ø 8 mm)


12

10-0360 & 10-0364

10-0335 & 10-1333

25-0228

Printer Chart

10-0404

10-0380

Main Units

10-036010-0361

DDA 3/100 - for test length up to 100 cmSupplied with: 3 molds (acc. ASTM D 113, if not ordered otherwise), 3 mold-holders, 2 corrosion protection specimen, 2 contrast inlays and distance piecesTechnical Data: Travel length : 100 cm (maximum)Dimensions of Bath : 170 x 40 x 50 cm (W x D x H), weight: 70 kg Controller : 35 x 25 x 15 cm (W x D x H), weight: 6 kg Printer : 37 x 28 x 16 cm (W x D x H), weight: 5 kgPower supply : 220/240 V, 50/60 Hz, EU-plugPower supply : 115 V, 60 Hz, US-plug

10-036410-0365

DDA 3/150 - for test length up to 150 cm Supplied with: 3 molds (acc. ASTM D 113, if not ordered otherwise), 3 mold-holders, 2 corrosion protection specimen, 3 contrast inlays and distance piecesTechnical Data: Travel length : 150 cm (maximum)Dimensions of Bath : 220 x 40 x 50 cm (W x D x H), weight: 92 kg Controller : 35 x 25 x 15 cm (W x D x H), weight: 6 kg Printer : 37 x 28 x 16 cm (W x D x H), weight: 5 kgPower supply : 220/240 V, 50/60 Hz, EU-plugPower supply : 115 V, 60 Hz, US-plug

10-038010-0381

Circulator (for external & internal cooling & heating)Necessary as tempering & fi lling device for the DD/DDA bath jacket and for reaching a bath-temperature of approx. -10 to +60 °C (at +20 °C ambient temperature).Consisting of:Cooler with stainless steel bath. Thermostat with digital display, splash-proof keypad, heater, pump, RS232/RS485-interface, Pt-100-socket, programmer, over/under-temperature & low-level protection, adjustable pump-pressure, proportional cooling control.Supplied with: 1 bath cover, 1 drain tap, 1 junction line for temperature probeNote: Insulated hose matter is not included but recommended.

For details see: General Equipment Dimensions / Weight : 37 x 46 x 71 cm (W x D x H), 49 kgPower supply : 230 V, 50 Hz, EU-plugPower supply : 230 V, 60 Hz

25-0228 Hose-Set, insulated (Ø 8 mm, 2x 2 m, incl. fi ttings)

Data Evaluation

10-0404 PC Software - DDACon (Windows®)A program for recording, saving and graphic presentation of DDA values.Replacing analog line recorder or serial printer, allows to control the DDA by PC, the data-transfer to MS EXCEL® or LIMS and simplifi es the download of fi rmware-upgrades.Supplied with: 1 PC-data-cable, 1 USB/RS232-converter


13

10-0332

10-0335

10-1336 & 10-1337

10-0403 & DDA

18-0403

10-0379

Options and Accessories

10-033210-033510-1336

10-1337

Mold (4-piece), brass, for the preparation of bitumen briquettes ... according to EN 13 398 - IP 516 - DIN 52 013... according ASTM D 113 - AASHTO T 51... according to EN 13 589 - IP 520 - DIN EN 13 589 EN 13 703 - IP 515... according to ASTM D 6084 - AASHTO T 300

10-1333 Mold Holder (fi ts all petrotest ductility molds)

10-0379 Calibration Set - DDAConsisting of: 1 set of precision resistor plugs , 1 certifi ed thermometer DIN 12 775 (0 to +50 :0.1°C), 1 thermometer holder,1 digital stop watch, 1 tape-measure with mm-division3 weights with steel-rope & 1 pulley

10-038310-0384

Thermometer, for DDA/DD-calibration set... DIN 12 775, range 0 to +50 :0.1°C, precision made... DIN 12 775, range 0 to +50 :0.1°C, offi cially certifi ed (incl. in calibration set)

10-0403 Rack 80 x 25 x 42 cm (L x W x H) to place controller and printer behind the ductilometer

18-040318-0402

Circulator-Bath (for external & internal heating)Used for pre-tempering of samples (e.g. DD/DDA-molds)Note: It requires counter-cooling by a circulation cooler or thermostatic circulator for

applications near ambient temperatures. Hose matter is not included.For details see: General Equipment

Dimensions / Weight : 37.5 x 45 x 47.5 cm (W x D x H), 3.4 kgPower supply : 230 V, 50 Hz, EU-plugPower supply : 115 V, 60 Hz, US-plug

11-0181 Hose, silicon (Ø 8 mm, 8 m)

Spare Parts10-0377 Contrast Inlay

(6 x 170 x 550 mm) pack of 1

10-0406 Corrosion Protection Specimen (200 x 100 mm) pack of 2

11-0599 USB/RS232-Converter with 2 m cable (verifi ed for Petrotest®-units)For details see: General Equipment

25-0262 PC-Data Cable (O-modem)serial, (9 & 25-pin)


14

Molds in Bath

Themometer in Bath

Tensile Properties - Ductilometer Method - DD 3 (semi-automatic)

Elongation: ASTM D 113 - AASHTO T 51 - JIS K2207 DIN 52 013 (IP 32, NF T 66-006)

Elastic Recovery: ASTM D 6084 EN 13398 (DIN V 52 021-1) - IP 516(ASTM D 5892 - ASTM P 226)

Ductility gives an indication of the suitability of bituminous materials for specifi c applications such as road construction etc.

In order to determine the particular properties of polymer modifi ed bitumen, the method of elastic recovery has turned out to be more expedient.

Main Units

DD 3 - Semi-Automatic Tensile Property Tester, Ductilometer Method

Depending on accessories suitable for:Elongation : ASTM D 113 - AASHTO T 51 - JIS K2207 - DIN 52 013Recovery : ASTM D 6084 - EN 13 398 - IP 516(obs.: ASTM D 5892,ASTM P 226, DIN V 52021-1, IP 32, NF T 66-006)Features: • 1 elongation & 1 recovery program• variable traction speed up to 140 mm/min.• constancy of speed and temperature at minor bath motion is better than demanded by the standards• without cooling coils, therefore easy to cleanConsisting of:Bath: for 3 simultaneous tests, made of stainless steel, double-walled and full insulated, closed cycle cooling system, circulation pump to be switched off, bath illumination and acrylic bath cover.Control Unit: with microprocessor, membrane keypad, RS232-interface for printer Digital display (LCD) of: program, traction speed, distance2 Programs: - Semi-Automatic Elongation

- Semi-Automatic Elastic Recovery for polymer modifi ed bitumenSerial Impact Printer: for single sheet & continuous paper (incl. data transmission cable)makes printouts of 3 test points with following parameters: program, traction speed, distanceNote: External cooling device for fi lling the bath-jacket is required.

Technical Data : Working range : approx. -10 to +60 °C (depending on the cooler)Travel length : 100 cm or 150 cm (maximum)Test positions : 3 (in a 30 l or 45 l bath)Traction speed : Standard: 50 mm/min. / Variable: 2.5 to 140 mm/min.Connections for : serial printer, cooler as tempering & fi lling device (Ø 8 mm) Dimensions: Bath (100 cm travel length) : 170 x 40 x 50 cm (W x D x H), weight: 70 kg

Bath (150 cm travel length) : 220 x 40 x 50 cm (W x D x H), weight: 92 kgController : 35 x 25 x 15 cm (W x D x H), weight: 6 kg Printer : 37 x 28 x 16 cm (W x D x H), weight: 5 kg

10-035010-0351

DD 3/100 - for test length up to 100 cmSupplied with: 3 molds (acc. ASTM D 113, if not ordered otherwise), 3 mold-holders, 2 corrosion protection specimen, 2 contrast inlays, 2 distance pieces, 3 thermometers ASTM 63C, 3 thermometer-holdersPower supply : 220/240 V, 50/60 Hz, EU-plugPower supply : 115 V, 60 Hz, US-plug

10-035410-0355

DD 3/150 - for test length up to 150 cm Supplied with: 3 molds (acc. ASTM D 113, if not ordered otherwise), 3 mold-holders, 2 corrosion protection specimen, 3 contrast inlays, 3 distance pieces, 3 thermometers ASTM 63C, 3 thermometer-holdersPower supply : 220/240 V, 50/60 Hz, EU-plugPower supply : 115 V, 60 Hz, US-plug

Scope of ApplicationThe Ductility or Elongation is measured by the distance to which a sample will elongate before breaking when two ends of a specimen briquette are pulled apart at a specifi ed speed and at a specifi ed temperature.It may be used for quality specifi cations.

The Elastic Recovery is measured by the recoverable strain determined after severing an elongated briquette specimen. The specimens are pulled to a specifi ed distance at a specifi ed speed and at a specifi ed temperature.This is useful in confi rming that a material has been added to the asphalt to provide a signifi cant elastomeric characteristic.

Our ductilometers are also available as an automatic version with force measure-ment - DDA 3.


15

10-0335 & 10-1333

10-1336 & 10-1337

10-0332 & 10-1333

Thermometer & Holder

10-0403 & Ductilometer

10-0380

10-0399

10-038010-0381

Circulator (for external & internal cooling & heating)Necessary as tempering & fi lling device for the DD/DDA-bath jacket and for reaching a bath-temperature of approx. -10 to +60°C (at +20°C ambient temperature).Note: Insulated hose matter is not included but recommended.

For details see: General EquipmentDimensions / Weight : 37 x 46 x 71 cm (W x D x H), 49 kgPower supply : 230 V, 50 Hz, EU-plugPower supply : 230 V, 60 Hz


21-0697 Digital Stop WatchFor details see: General Equipment

Options & Accessories

10-033210-033510-1336

10-1337

Mold (4-piece), brass, for the preparation of bitumen briquettes ... according to EN 13 398 - IP 516 - DIN 52 013... according ASTM D 113 - AASHTO T 51... according to EN 13 589 - IP 520 - DIN EN 13 589 EN 13 703 - IP 515... according to ASTM D 6084 - AASHTO T 300

10-1333 Mold Holder (fi ts all petrotest ductility molds)

10-0399 Calibration Set - DDConsisting of: 1 set of precision resistor plugs , 1 certifi ed thermometer DIN 12 775 (0 to +50 :0.1°C), 1 thermometer holder,1 digital stop watch, 1 tape-measure with mm-division

10-0403 Rack 80 x 25 x 42 cm (L x W x H) to place controller and printer behind the ductilometer

18-040318-0402

Circulator-Bath (for external & internal heating)Used for pre-tempering of samples (e.g. DD/DDA-molds)Note: It requires counter-cooling by a circulation cooler or thermostatic circulator for

applications near ambient temperatures. Hose matter is not included.For details see: General Equipment



Thermometers (for DDA/DD-calibration set & DD-bath)

Precision Made


TypeRange

ASTM DIN10-0383 10-0384 - 12 775 0 to +50 : 0.1 °C10-0385 10-0386 63C - +8 to +32 : 0.1 °C

Spare Parts10-0377 Contrast Inlay

(6 x 170 x 550 mm) pack of 110-0406 Corrosion Protection Specimen

(200 x 100 mm) pack of 2


16

18-1120 + 18-1135 + 18-1160

Display

Plastic Properties - Penetrometer Method - PNR 12Bituminous MaterialsNeedle-Penetration: ASTM D 5 - EN 1426 JIS K2207 (DIN 52 010 - IP 49)

Rod-Penetration (Bitumen Number): EN 13179-2 - van der Baan

Hot-Applied Sealants & FillersCone-Penetration : ASTM D 5329 EN 13880-2

The PNR 12 belongs to the group of conventional gravity-penetrometers used for the determination of consistency of highly viscous and plastically workable stuff.A test body is precisely lowered to the surface of the material under test, and then sinks into the matter by its own weight during a defi ned test duration. This penetration, which is indicated in Penetration Units of 1/10 mm per unit or directly in millimeters, and allows a rating of the plasticity or consistency.

Main Units

18-1120

PNR 12 - Automatic Penetrometer, Bitumen MethodDepending on accessories suitable for:Needle-Penetration : ASTM D 5 - EN 1426 (DIN 52 010 - IP 49)Rod-Penetration : EN 13 179-2 - van der BaanCone-Penetration : ASTM D 5329 - EN 13 880-2Features:• manual positioning by Jog-Wheel operation• electronic positioning to a preset depth with Memory-function• automatic surface detection• fully automatic measurements of electrically conductive samples• fully automatic measurements of non-conductive samples (optional)• automatic data evaluation against limit values set• auto-start function• 16 user programs possible• magnifi er & extra bright LED-sample illuminationConsisting of:Microcomputer, graphical display, electronic distance measuring device, stepper motor for exact positioning, conductivity sensor, plastic housing with stable base plate and software for fully automatic measurements of electrically conductive samples, as well as of non-conductive samples using the optional patented Force-Sensor-Plunger.Software:Auto-Start function for program 1+2+316 program positions for user defi ned programsAutomatic surface detection: • by conductivity sensor (included)• with force sensor (Requires a Force-Sensor-Plunger - not included)Conversion of results:• NLGI-classifi cation ASTM D 217• Bitumen classifi cation EN 1426• Quarter- and Half-Scale Cone into Full-Scale Cone• Margarine C-value 80g and 160gSupplied with: 1 conductivity sensor, 1 leveling bulbTo be ordered separately: Accessories have to be selected in compliance with different test standards or samples (plunger, needle, cone etc.)!

Technical Data:Measuring range : 0 to 80 mmMax. test load : 2 kgResolution : 0.01 mm Test duration : 0.1 to 18000 seconds (preset standard duration: 5 seconds)Start delay : adjustable up to to max. of 600 sec. (10 minutes)Limit Indicator : audible alarm when test value falls outside preset valuesValue conversion : NLGI-class, EN-bitumen value, c-value, 1/4-cone to solid-cone, 1/2-cone to solid-cone Surface detector : for electrically conductive samples (optional for non-conductive samples)Data output : USB, LANBench space : 35 x 35 x 60 cm (WxDxH), weight 11 kgPower supply : 100/240 V, 50/60 Hz, EU-plug

Scope of ApplicationUsed to determine the plasticity of a wide range of materials, as well as for the evaluation of such theological characteristics as rheopexy and thixotropy.

Suitable for bituminous materials and hot-applied pavement sealants & fi llers.

Needle-Penetration:To measure the consistency of semi-solid and solid bituminous mixtures.Rod-Penetration:To measure the apparent viscosity (Bitumen N°) of fi ller aggregates used in bituminous mixtures.Cone-Penetration:To determine the consistency of hot-applied, fuel-resistant joint sealants with or without being immersed in fuel or oil.

Summary of MethodPenetration is the resistance which a material under specifi ed conditions of test provides against being pierced by a specifi cally shaped penetrator.Beside the confi guration of the penetrator used, prime importance attaches to such factors of temperature, time and load of test as are specifi ed by the different standard methods of test.A sample is fi lled in a specifi ed container and conditioned in a temperature bath. Then a standardized penetrator is vertically dropped on the specimen to measure the penetration depth. Higher values of penetration indicate softer consistency.

Penetration & TexturePenetration & Texture

17

Test Kit “Optional Hollow Cone - Filler” (18-2215)

Test Kit “Rod - Bitumen Number” (18-2370)

Test Kit “Needle - ASTM” (18-2220)

Test Kit “Needle - EN” (18-2221)

Temperature Sensor (18-1149)

Sensor-Plungers (18-1135/18-1136/18-1137)

Leveling Bulb “PNR”

Test Bodies18-2220 Test Kit - Needle - ASTM (ASTM D 5 - AASHTO T49 - JIS K2207)

3 standard needles, 2.5 g, brass/steel, precision made (18-1160)1 plunger, 47.5 g (18-0042)1 load weight, 50 g (18-0051)5 sample jars I, Ø 55 x 35 mm (18-0066)1 tempering bath (18-0065)

18-2221 Test Kit - Needle - EN (EN 1426 - IP 49) 3 standard needles, 2.5 g, brass/steel, precision made (18-1160)1 plunger, 47.5 g (18-0042)1 load weight, 50 g (18-0051)5 sample jars I, Ø 55 x 35 mm (18-0066)1 sample jar III, Ø 70 x 45 mm (18-0068)1 sample jar V, Ø 55 x 60 mm (18-0069)1 reduction ring, Ø 36 / 53 x 20 mm (18-0076)1 reduction ring, Ø 36 / 53 x 30 mm (18-0077)1 tempering bath with serpentine heat exchanger tube (18-0070)1 spacer plate for tempering bath (18-0091)1 thermometer holder (18-0094)1 thermometer ASTM 63C, -8/+32/0.1 °C (90-0106)1 thermometer ASTM 64C, +25/+55/0.1 °C (90-0107)Note! obs. IP 49 requires additionally: 150 g load weight (18-0052 & 18-0056) and thermometer ASTM 17C (21-0601)

18-2370 Test Kit - Rod - Bitumen Number (van der Baan) (EN 13 179-2)1 rod, Ø 8 mm, 15 g, aluminum (18-0251)1 sample jar, Ø 30 mm x 30 mm (18-0252)

18-2215 Test Kit - Optional Hollow Cone - Filler (ASTM D 5329-6/7 - EN 13 880-2)1 optional hollow cone, 102.5 g, brass/steel (18-0101)1 plunger, 47.5 g (18-0042)1 sample jar I, Ø 55 x 35 mm (18-0066)1 tempering bath, Ø 160 x 80 mm (18-0065)1 spacer plate for tempering bath (18-0091)

18-116018-116118-116318-1164

Standard Needle, 2.5 g... Precision Made (ASTM D 5 - AASHTO T 49 - EN 1426 - IP 49 - ISO / DIS 3997)... Works Certifi cate Petrotest® (ASTM D 5 - AASHTO T 49 - EN 1426 - IP 49 - ISO / DIS 3997)... Offi cially Certifi ed, with UKAS certifi cate (EN 1426 - IP 49)... Offi cially Certifi ed, with UKAS certifi cate (ASTM D 5 - AASHTO T 49 - EN 1426 - IP 49)


18-113518-1136

18-1137

Sensor-Plunger - Force a plunger with an extremely sensitive force sensor for the automatic surface detection underneath a layer of water. It activates the related the PNR 12 software automatically.Suitable for Bitumen-samples (<160 PU) and for PNR 12 only! For 1 additional weight:... 47.5 g ... 97.5 g

For up to 4 additional 50 or 100g weights:... 97.5 g extra long

18-120118-120018-120218-120318-1204

Additional Weights for sensor-plunger... 100 g ... 50 g ... 10 g ... 5 g ... 2 g

18-1145 Calibration Kit - PNR 12for distance calibration: 1 test ram & 4 gauge blocks (5 / 9 / 15 & 25 mm)for time calibration: 1 contact-rod & 1 stop watch (electric input)for temperature calibration: 2 reference-plug (+20°C & +90°C)

18-1149 Temperature Sensor with Pt-100 to monitor the sample-bath temperature

18-1144 Electronic Stop WatchDetails: General Equipment

25-028225-0283

Serial Impact Printer to record data like test results, duration of test, etc. without a PC.Details: General Equipment Power supply: 220/240 V, 50/60 HzPower supply: 110/130 V, 50/60 Hz

25-067025-0671

Circulator-Bath Set(for ex- & internal heating & cooling)Used for sample tempering (e.g. with tempering bath 18-0065, 18-0070).Details: General Equipment Power supply: 230 V, 50 Hz, EU-plugPower supply: 115 V, 60 Hz

18-040318-0402

Circulator-Bath (for external & internal heating)Used for sample tempering (e.g. with tempering bath 18-0065, 18-0070).Details: General Equipment Power supply: 230 V, 50 Hz, EU-plugPower supply: 115 V, 60 Hz

Thermometers (for sample tempering)

Precision Made


TypeRange

ASTM IP21-0601 21-0607 17C - +19 to +27 : 0.1 °C21-0621 21-0627 17F - +66 to +80 : 0.2 °C11-0087 11-0088 38C 78C +24 to +78 : 0.2 °C


18

18-1700 + Testbody

supplied with 18-1700

18-1721PNR Pro

Plastic & Elastic Properties - Texture Method - PNR 21

Main Units

18-170018-1701

PNR 21 - Rheotex Texture Analyzer

Features: User generated test programs include• automatic contact of the sample surface• alternating load tests or oscillating programs• program loops with constant load• pauses and no motion stages

Consisting of:testing machine for texture and consistency examinations, with splash water protected membrane control panel with LCD showing actual test parameters and measured values directly, control and programming software PNRCon (used to record measured values, their graphic display, as well as to save test results and test programs), RS232-interfaces for printer and PC connectionSupplied with: 1 clamping support (2 groove stones with bolds)

1 test cylinder (Ø 10 mm)1 PNRCon software (for Windows).

Note: Ordinary Pentium PC with printer and extended software PNRProor parallel printer are recommended.Further the Penetration Accessories of PNR 10 like needles, cones etc. can be used also.

Technical Data: Load & tensile force : 100 NewtonsResolution : up to 9 Newtons: 0.01 N / more than 9 Newtons: 0.1 NDisplacement : 100 mm (start position of measuring carriage is variable)Resolution : 0.01 mmTravelling speed : 0.1 - 8 mm/s ±0.1 %Pause mode : for delayed plunger releaseConnections for : PC (9-pin), serial printer (25-pin) Dimensions : 32 x 37.5 x 50 cm (W x D x H), weight: 11 kgPower supply : 115-230 V, 50/60 Hz, 0.4 A, EU-plugPower supply : 115-230 V, 50/60 Hz, 1.0 A, US-plug

The PNR 21 is a compact but highly fl exible texture analyzer, that demonstrates the forces, which occur when the properly chosen test body is pushed into the tested material or withdrawn.Especially due to its easy and convenient handling the apparatus allows a quick and economical examination of the plastic & elastic properties of pasty materials. PNR 21 Rheotex uses different test bodies. It depends on the measurement problem, whether a needle, a cone, a cylindrical or platelike ram is applied. These test bodies are mounted to a support-arm with force sensor which is attached to a vertically movable carriage.The load or tensile forces, which affect the force sensor, when the carriage moves up or down are indicated on a computer screen as a force/displacement diagram or as a displacement/time function.

The instrument permits to monitor curing and congealing reactions of adhesives, mortars etc. or to observe the behaviour of sealing matter and cements.

The creation of test programs is very easy. Either made directly on the instrument or by using PNRCon software and a PC with Windows.The use of a computer does not only enable a much easier and more extensive creation of test procedures, but also allows their storage and reloading.

Scope of ApplicationUsed to measure load forces as well as tensile stresses, which occur when a test body is pushed into the tested material or withdrawn.

Suitable for bituminous materials, hot-applied pavement sealants & fi llers and cement.

Summary of MethodA texture analyzer measures the forces, which occur when a test body is pushed with a pre-programmed speed into the tested material or pulled out.

The forces affecting the test body are measured and indicated in the form of a “displacement/force curve“ or as a“force/time function“This allows to determine information about the aging, the maturity or the curing, as well as the estimated subsequent processing of a sample.


19

18-0279

18-1721 PNR Pro

18-0255

18-1728

18-0251

The PNR 12 penetrometer measures the penetration depth in millimeters. The texture analyzer PNR 21-Rheotex measures load and tensile forces.

PNR 12 gives one solitary displacement value at the end of a test. PNR 21 provides a series of values, which can be shown as a force/displacement curve or as a diagram “force versus time“.

You will fi nd further information about the PNR-instruments and their available accessories in our Texture Testing-catalog.


Test Bodies18-0279 Test Needle - VICAT,

2 g, fl attened, Ø 1 x 50 mm (effective length 35 mm) stainless steel

18-0255 Test Ball, 6.3 g, Ø 6.3 mm (overall length with shaft 100 mm), brass

18-0045 Plunger (penetrometer clamping rod) 10 g, length 107 mm, aluminum, for test needle 18-0279, test ball 18-0255 and other penetrators

18-025118-1726

Test Cylinder, with plane end face15.0 g, Ø 8 mm, 40 mm effective length, aluminum21.8 g, Ø 10 mm, 100 mm overall length, aluminum

18-024718-0248

Platelike Test Ram - Adhesion10 cm² (Ø 35.7 mm)20 cm² (Ø 50.5 mm)

Options & Accessories18-1728 Test Kit - Adhesive Strength

with sample & ram temperature control and 3 easy-to-change sample containers. By use of a circulation thermostat (not included), the ram (Ø=3 mm or Ø=10 mm), the sample and the container can be heated up to the requested temperature, without that the test equipment gets into contact with the tempering fl uid.

18-1721 PNRPro Softwareoffering additional possibilities like simultaneous display of stored master curves and comparison of actual test curve, statistical analysis, storage of test series in a data base for comfortable comparison and their statistical evaluation, programmable zero setting for a defi ned program step (labelling), menu in English.

Circulator-Baths with intermediate bottom are used for - sample pre-tempering (e.g. Tempering Bath 18-0065) and / or - connection to small external units (e.g. Tempering Bath 18-0070 or Adhesive Strength Device 18-1728)

25-067025-0671

Circulator-Bath Set (for internal & external sample heating & cooling)Note: Insulated hose-set (25-0228) is included.

For details see: General EquipmentDimensions / Weight : (WxDxH) 57 x 37 x 42 cm, 13 kg (bath) / 23 x 36 x 38 cm, 23 kg (cooler)Power supply : 230 V, 50 Hz, EU-plugPower supply : 115 V, 60 Hz

18-040318-0402

Circulator-Bath ( for external & internal sample heating)Note: It requires counter-cooling by a circulation cooler or thermostatic circulator

for applications near ambient temperatures. Hose matter is not included.For details see: General Equipment



25-0228 Hose-Set, insulated (Ø 8 mm, 2 x 2 m, incl. fi ttings)

Spare Partsdepending on the used Test Kit

20

BPACon Permanent Bending

BPACon Glass Transition Temperature

BPA 5 (10-0457)

BPA 5 Bending Mechanism

Breaking-Point - FRAASS Method - BPA 5 (automatic)

Bitumen and bituminous binders: IP 80 - EN 12593 (DIN 52 012, NF T 66-026) - JIS K 2265

Easy to OperateDue to its principle of construction ”measuring the bending force of a steel plaque coated with the material to be examined“ and the use of thermoelectric elements for the cooling of the test chamber, the Automatic Breaking-Point Tester BPA 5 offers a series of outstanding advantages.The handling of the BPA 5 is very easy. The operator only needs to place the specimen on the plaque support and the BPA 5 automatically clamps and adjusts the test plaque.The large LC-display, visible up to 10 m distance, provides the operator with additional instructions during a test. When a test is completed, the fi nal result remains on the display until a new measurement is started.

VersatilityThe scope not only covers the examination of bitumen according to the conventional FRAASS Method but also allows the user to adapt the test procedure to particular conditions (e.g. research of glass transition temperatures) or to perform a permanent bending program.

With the Standardized-FRAASS-Test-Method the instrument detects a distinct variation of the bending force or a typical deformation of the force/temperature curve respectively. Just as if the BPA 5 user could look inside the material under test.

These striking force characteristics can even be recognized with diffi cult materials (such as certain kinds of bitumen), where ruptures of the bitumen coating cannot be observed visually.

In particular with Polymer-modifi ed Bitumen (PmB), the Permanent-Bending-Program is an interesting alternative to the conventional FRAASS method. The sample is cooled to a specifi ed temperature and then the number of bending strokes is counted which are necessary to cause a rupture.

This program, however, requires a PC with BPACon-software to remote-control the BPA 5, for storage and evaluation of the measured data. Thus, test proceedings (e.g. variation of the bending force) can be easily watched via a graphic diagram on the PC screen.

For samples with a very low breaking-point a Rapid-Test-Program is included. It cools with an accelerated rate of 2 K/min in the beginning and then changes to the standardized cooling rate during the actual test period.

In order to avoid unnecessary tests, with samples where the breaking-point is not known at all, the SEARCH-Mode, which is preset in the USER program, can be used benefi cially. The instrument works with a refrigeration rate of 2 K/min and makes a bending test every 2 Kelvin.

The BPA 5 also offers the possibility to change test parameters like bending speed, cooling rate or bending intervals and to store them as a USER-Defi ned-Program.

Scope of ApplicationTo determine the temperature at which a bitumen tends to break rather than to fl ow when stressed.Suitable for any homogeneous road or industrial bitumen.

Summary of MethodA thin fl at steel plaque, coated with the sample, is fl exed under specifi ed conditions at a descending series of temperatures.The FRAASS-Breaking-Point is the temperature at which the fi rst cracks appear in the coating.

Breaking-PointBreaking-Point

21

10-0460

Printer Test Chart

BPACon Standardized

Test

Data OutputAlthough not required, the connection of a serial printer is recommended.The user will receive a test result for each fl exion or any other interval (time or temperature according to the parameters set by the operator).

BPACon-SoftwareMost comfortable is the use of the BPA 5 together with a PC with BPACon-software. This software package (for Windows®) includes the Permanent-Bending-program. Further it permits to remote control the BPA 5 by PC, to create additional user-defi ned test programs and to store or reload them from a PC. The measured data can be easily saved and evaluated on a PC in numerical form and as well as a graphical diagram.BPACon is, for instance, mandatory to run Permanent-Bending-Tests or when Glass-Transition-Temperatures are determined, where the trend of the bending force versus the temperature drops and the recovery trend serves as the criteria for the material under test.

EconomicalThe BPA 5 is a very economical instrument. It uses Peltier-elements for the refrigeration of the test chamber. These solid-state cooling elements require a light auxiliary refrigerant only and thus avoid investing in a bulky and high energy consuming cooler.

Cooling Source Coolant Temperature

Achievable Breaking Point(at ambient temperature of +20 °C)

Tap Water +17 °C approx. -24 °CCirculation Cooler -10 °C approx. -36 °CCirculator -20 °C approx. -45 °C

Note: These coolers are designed to be opperated at ambient temperatures of approximately +5 to +40 °C. All mentioned values are basically detected at an ambient temperature of approx. +20 °C.

Main Units

10-046010-0461

BPA 5 Set - Fraass Method- Automatic Breaking-Point Tester with Circulation CoolerIP 80 - EN 12 593 - JIS K2207Consisting of:- Measuring and Control Unit:

Measuring head with bending mechanism, automatic fi xture and adjustment of test plaques; test chamber cooled by solid-state components (Peltier-elements), chamber ventilator, touch-key panel with large LC-display visible up to 10 m distance for measured values and user guidance for temperature pre-selction and test-plaque clamping.

- Programs: Standardized-FRAASS-Test RAPID-Test for very low breaking-points USER-Defi nable-Program SEARCH-Mode for samples with unknown breaking-point. In combination with a PC and BPACon-software: Permanent-Bending-Program. Further the graphic display and evaluation of the bending forces.

- Circulation Cooler: as auxiliary refrigeration of the Peltier-elements.Supplied with: 10 test-plaques (41 x 20 x 0.15 mm), 1 insulated hose-set (Ø 8 mm, 2 x 2 m)Note: serial printer or PC-software BPACon are recommended.Technical Data: Resolution : 10 mNWorking range : approx. -45 to +60 °C (due to external cooling)Cooling : Peltier-elements (internal) & circulation cooler (external)Connections for : serial printer, PC (RS232), cooler (Ø 8 mm) Dimensions BPA : 23 x 40 x 29/43 cm (W x D x H), weight: 15 kgDimensions Cooler : 23 x 36 x 38 cm (W x D x H), weight: 23 kgPower supply : 230 V, 50/60 Hz, 450 W, 2 A, EU-plugPower supply : 115 V, 60 Hz, 450 W, 4 A, US-plug

Technical DataOperating Range:approx. -45 to +60°C

Programs:• Standard-Program

(cooling rate of 1 K/min)for FRAASS-Breaking-Point

• RAPID-Program (cooling rate of 2 K/min)for very low breaking-points

• SEARCH-Mode to fi nd the approximated breaking-point

• USER-Defi nable-Program for program modifi cations

In connection with the PC-software BPACon:• Permanent-Bending-

Program for fatigue tests• Glass-Transition-Temperature • Graphic display and

evaluation of bending forces• LIMS ability

Interface:serial RS232 for printerserial RS232 for PC (USB-converter available)

Refrigeration: Peltier-elements counter-cooled by the circulation cooler

For special applications the BPA 5 can be delivered with an extended working range or a 1 mN-resolution.


22

10-0473

10-0474

25-0282

Plaques

11-0599

10-0233

12-1763


10-0473 PC Software - BPACon (Windows®)The program includes the Permanent-Bending-Test-Software and is used to store / modify and display curves of force for - Breakpoint-Tests - Permanent-Bending-Tests - Glass-Transition-Temperature-Test. It replaces the serial printer and makes it possible to start/stop the BPA 5 by PC, as well as to load self-defi ned test-programs.The progression in elasticity, plasticity, glass-transition-temperatures and of cause cracking will be displayed numerical or graphically in different scales. With special created curves of trends for bending or recovery force even very small, nearly not visible, breaks of the material can be found in an unknown high precision.Supplied with: 1 PC-data-cable, 1 USB/RS232-converter

10-0474 Calibration Set - BPA 5Consisting of:1 set of precision resistor plugs, 2 weights, 1 thermometer IP 42C (calibrated)

10-0475 Laboratory Stand for calibration set

10-0233 Tongs to handle stest-plaques

12-1763 Storage Box for spare parts and tools

10-050710-0506

BPM 5 - Melting ApparatusConsisting of:steplessly regulated red heater plate (11 x 9 cm) with thermometer socket; blue cooling plate (11 x 9 cm) (hose connections for a cooler in the rear); holder for a depositing panSupplied with: 1 thermometer ASTM 2C (-5 to +300 : 1 °C), 1 magnetic test-plaque holder (50 x 40 x 8 mm),1 cover hood for better tempering of the test-plaques, 1 T-shaped spirit-level,10 aluminum depositing pansNote: We suggest a connection in series with the BPA and its circulation coolerTechnical Data:Dimensions / Weight : 23 x 40 x 30 cm (W x D x H), 6,5 kgPower supply: 230 V, 50 Hz, EU-plugPower supply: 115 V, 60 Hz, US-plug

25-028225-0283

Serial Impact Printer to record data like test results, duration of test, etc. without a PC.For details see: General EquipmentPower supply : 220/240 V, 50/60 HzPower supply : 110/130 V, 50/60 Hz

Spare Parts10-0006 Test-Plaques, 10 pieces

(41 x 20 x 0.15 mm), steel

10-0016 Test-Plaques, 10 pieces (41 x 20 x 0.15 mm),steel, with works certifi cate

25-0228 Hose-Set, insulated (Ø 8 mm, 2 x 2 m)

25-0262 PC-Data-Cable (0-modem), serial, RS232 (9 & 25-pin)


25-0274 Printer-Data-Cable, serial (2 m)standard 25-pin


23

10-0507

10-0090

10-0000

10-0233

Breaking-Point - FRAASS Method (manual)

Bitumen and bituminous binders: IP 80 - EN 12 593 (DIN 52 012, NF T 66-026) - JIS K 2265

Main Unit10-0000 Manual Breaking-Point Tester, Fraass-Method

Consisting of:cooling apparatus (test tube, stopper and Dewar-fl ask with metal stand); bending apparatus with small stopper.Supplied with: 10 test-plaques (41 x 20 x 0.15 mm), 1 thermometer IP 42CNote: protection vessel for Dewar-fl ask and tongs on separate order.Technical Data: Dimensions : Ø 12 x 48 cm, weight: 3 kg


10-0090 Protection Vessel (Acryl) (inside Ø 125 x 245 mm) for Dewar-fl ask

10-0233 Tongs to handle test-plaques

10-050710-0506

BPM 5 - Melting ApparatusConsisting of:steplessly regulated red heater plate (11 x 9 cm) with thermometer socket; blue cooling plate (11 x 9 cm) (hose connections for a cooler in the rear); holder for a depositing panSupplied with: 1 thermometer ASTM 2C (-5 to +300 : 1 °C), 1 magnetic test-plaque holder (50 x 40 x 8 mm),1 cover hood for better tempering of the test-plaques, 1 T-shaped spirit-level,10 aluminum depositing pansNote: We suggest a connection in series with the BPA and its circulation coolerTechnical Data:Dimensions / Weight : 23 x 40 x 30 cm (W x D x H), 6,5 kgPower supply: 230 V, 50 Hz, EU-plugPower supply: 115 V, 60 Hz, US-plug

Spare Parts10-0002 Bending Apparatus

Consisting of:two concentric tubes fi tted with plaque-holding clips, curved spacer, crank-operated cone-and-peg mechanism, setting screw and rubber stopper

10-0003 Cone-and-Peg Mechanism, hardened and polished

10-0004 Setting Screw with a hardened tip

10-0006 Test-Plaques, 10 pieces (41 x 20 x 0.15 mm), steel

10-0008 Test-Tube

10-0009 Dewar-Flask (borosilicate glass), 1 litre, Ø 75 x 205 mm, without stand.

10-0010 Stopper (NBR-rubber), Ø 83/71 x 60 mm, bored twice (Ø 15 & 38 mm), to support the test-tube in the Dewar-fl ask and allow fi lling at the same time

10-0017 Thermometer IP 42C (-38 to +30 : 0.5 °C)

20-0106 Metal Stand for Dewar-fl ask


24

25-0240

StiffnessStiffness

Scope of ApplicationTo determine the fl exural creep stiffness of asphalt binders at low temperatures like ambient to -36°C

Summary of MethodDuring testing, a constant load (0 to 450 g) is applied to a asphalt beam for a selected duration. The defl ection of the beam is measured and monitored continuously by PC. Further the test parameters are set by the PC, which displays & prints a plot of load vs. defl ection and calculates the stiffness at the lowest temperature anticipated.For tests acc. ASTM D 6648 an auxiliary cooler is required to cool down the molds, so that the sample is stiff enough to be demolded without distortion.

Flexural Creep Stiffness - Bending Beam Rheometer Method - BBR (automatic)

AASHTO T313 (AASHTO TP1)

ASTM D 6648 (ASTM P 245)

EN 14771 (NF T66-062)

Superpave®: SHRP 1002 - SHRP B-002 (AASHTO TP1 - ASTM P 245)

Main UnitBBR - Automatic Bending Beam Rheometer Consisting of:Integrated programmable controller for controls and recording measured data.Linear-electromagnetic loading unit and incremental transducer.Compact tempering unit with heater and compressor cooling and powerful pressure/suction pump.Separate test bath with constant level maintenance. Freely selectable test temperatures.Own layout of test records.Technical Data: Load range : 0 to 1500 mN (accuracy class 0.1)Loading unit : max. lift 10 mm, max. force 2000 mNTemperature range : -40 to +200 °C : ±0.01 KBath volume : Tempering unit: approx. 4.9 l Test bath: approx. 11 lDimensions / weight : 95 x 48 x 75 cm (W x D x H), approx.80 kgNote: Requires molds, cooling bath (for sample preparation) and PC (no Laptop).

10-070010-0701

ASTM D 6648 - AASHTO T313 Superpave®: SHRP 1002 - SHRP B-002 - (AASHTO TP1 - ASTM P 245)Power supply : 230/240 V, 50/60 Hz, EU-plugPower supply : 115 V, 60 Hz, US-plug

10-070210-0703

EN 14771Power supply : 230/240 V, 50/60 Hz, EU-plugPower supply : 115 V, 60 Hz, US-plug

10-0706 Beam Casting Molds, aluminium (acc. AASHTO, ASTM, EN), pack of 5

10-0709 Beam Casting Mold, silicone, triple


10-0707 Calibration Kit - BBR Force (with works certifi cate)

10-0716 Calibration Kit - BBR Force (with DKD certifi cate)

10-0708 Calibration Kit - BBR Temperature (with works certifi cate)

10-0717 Calibration Kit - BBR Temperature (with DKD certifi cate)

25-024025-0241

Circulator (external & internal heating & cooling) (for ASTM D 6648 sample preparation)For details see: General EquipmentDimensions / Weight : 23 x 42 x 61 cm (W x D x H), 31 kgPower supply : 230 V, 50 Hz, EU-plugPower supply : 115 V, 60 Hz, US-plug

The U.S. Government funded Strategic Highway Research Program (SHRP) brought new rheology tools and procedures to the market to improve performance and commerce with Superpave® Performance Graded Binders.

25

ViscosityViscosity

Viscoelastic Properties - Dynamic Shear Rheometer Method - DSR II (automatic)

Superpave®: SHRP B-003 - SHRP 1007 - AASHTO T315 (AASHTO TP5) ASTM P 246

Paving grade: EN 12591 (NF T65-001)

Main Units

10-0770 DSR II - Automatic Dynamic Shear RheometerSHRP B-003 - SHRP 1007 - AASHTO T315 - ASTM P 246 - Superpave® - EN 12591A rheometer system confi gured for dynamic testing of asphalt and bitumen according the temperatures and frequencies specifi ed by SHRP and Superpave®.It offers precise and stable temperature control, a rapid sample equilibrium to settemperature, an automatic expansion compensation keeps the pre-set gap constant with temperature.Consisting of:1 rheometer with mechanical bearing and fl uid cell 1 cooling circulator with hose1 Windows-software SHRP for Superpave® specifi cation and grade determination 1 measuring plate (PU) Ø 8 mm (for average temperature tests)1 measuring plate (PU) Ø 25 mm (for high temperature tests)

Note: PC and Printer sets are required.Technical Data: Torque : 0.05 to 10 mNmTemperature Range : 5 °C to +80 °C (DSR)Heating / Cooling Rate : 2 °C / 1.5 °C (circulator)Power supply : 230 V, 50/60 Hz


10-077410-0775

Computer & Printer SetConsisting of:Windows©-software compatible minitower with DVD-ROM drive and USB-interface,TFT-monitor, keyboard, mouse and Inkjet color printerNote: Confi guration details upon requestPower supply: 230 V, 50/60 HzPower supply: 110 V, 60 Hz

A range of research-grade software is available to enable the following tests:• Oscillation as a function of time, temperature, frequency and shear stress• Viscosity as a function of shear rate, shear stress, temperature and time• Creep and Creep Recovery (for compliance measurement and analysis) including accumulated strain testing.• Time Temperature Superposition and Viscoelastic Analysis

Scope of ApplicationUsed to measure the viscoelastic properties of modifi ed or unmodifi ed (aged or unaged) asphalt binders in a temperature range of +5 to +80 °C.

Summary of MethodFor AASHTO MP1 tests a sample disc is confi ned between circular parallel plates and tested at a specifi c temperature.Dynamic shear is determined by applying a known torque to oscillate one of the plates and measuring the resulting strain.The phase angle, in radiants or degrees between the sinusoidal stress & strain, is measured, too. Resultant stress is measured in a strain control mode, while resultant strain in a stress control mode.

The measurement of the rheo-logical properties, or viscoelastic behavior, of binder, like range and degree of stiffness, elasticity, and relaxation times measured over the working temperatures, helps to improve the performance life of asphalt road systems.

Rheometers measure the rheo-logical data concerning the fl ow and the deformation behavior of substances by:

- Rotational tests for liquids:Flow curves (shear stress and shear rate), viscosity function, yield point, thixotropy (structuraldecomposition and regeneration), temperature behavior.

- Oscillatory tests for low viscous liquids to solids:

Viscoelastic behavioras an amplitude sweep as a function of the deformation or load (or shear stress); as a frequency sweep as a function of time (speed or frequency)

Time-dependent behavior (thixotropy, structural decomposition and regeneration)

Temperature-dependent behavior(glass-transition-temperature, melting-temperature, crystallization-temperature)

Jellifi cation and hardening behavior

- Creep and relaxation tests to investigate the viscoelastic behavior and material structure (e.g. molar mass distribution) of polymers

26

RV with spindle

ViscosityViscosity

Apparent Viscosity - Rotational Viscometer Method - RV (automatic)

Superpave®: SHRP 1006 - AASHTO T316 (AASHTO TP48) - ASTM D 4402 EN 13302

Main Units

10-060010-1600

RV - Digital Rotational Viscometer with Brookfi eld Thermosel

SHRP 1006 - AASHTO T316 - Superpave® - ASTM D4402 - EN 13 302Consisting of:measuring head (without spindle), temperature probe (Pt-100), digital display, RS232, parallel and anaolg output, stadia materialSupplied with: 1 carry caseNote: Spindle, viscosity standard, tempering unit (& controller for 115 V) are required.

The application PC-software is recommended.Technical Data: Working range : depending on spindle from 50 up to 3.3 million mPa·s Display of : torque, viscosity, shear rate, shear stress and temperatureSerial RS232 interface : for data transfer to PCParallel output : for printer Analog output : for torque (0-1 V) and temperature (0-4 V)Power supply : 230 V, 50 Hz, EU-plugPower supply : 115 V, 60 Hz, US-plug

10-0602 Spindle (Viscosity range: 50 to 170 000 mPa·s)Note: Since the viscosity range depends on the speed, the max. viscosity can only be

reached at the lowest speed!

10-0604 Spindle Extension, including link and coupling nut(only for test without Tempering Unit - RV)


10-060110-1601

Tempering Unit - RV(temperature controller with thermo-container)Temperature range: ambient to +300 °CPower supply: 230 V, 50 HzPower supply: 115 V, 60 Hz

10-1602 Tempering Controller - RV (for 115 V -Tempering Unit)

10-0603 PC-Software - RVprovides automatic data collection and instant fl ow curves (rheograms), for Windows®, data transfer cable included.

10-0605 Viscosity Standard 1000 cPs, 500 ml (for calibration at 10, 20, 30 rpm)

Scope of ApplicationUsed to determine the fl ow resistance, the dynamic and apparent viscosity, at elevated temperatures.(e.g. +38 to +260°C).

Suitable for bituminous binders.

Summary of MethodThe torque on a spindle rotating in a special thermostatically controlled sample holder containing a small sample of asphalt is used to measure the relative resistance to rotation.A factor is applied to the torque dial reading to yield the viscosity of the asphalt in millipascal seconds.

27

10-0312 with accessories

25-0001 / 25-0108

ViscosityViscosity

Apparent Viscosity - Effl ux Viscometer Method (manual)

Bitumen emulsions: EN 12846

Main Units

10-031210-0313

Effl ux (Road Tar) ViscometerEN 12 846Consisting of:electrically-heated single-place viscometer heating bath and ball valve supportSupplied with:2 test cups (with 4 mm and 10 mm orifi ce, 1 each),2 ball-tipped valve rods, 1 graduated (100 ml) receiver,1 set of 6 different stoppers.Note: Thermometers & Electronic Energy Regulator are required.Power supply : 230 V, 50/60 HzPower supply : 115 V, 50/60 Hz

25-000125-0108

Electronic Energy Regulator for heating coilsConsisting of:Potentiometer on/off switch, 10 A overload fuse; DIN-socket, 1.5 m cable with DIN-plug.Technical Data: Capacity : up to 2000 WWeight : 500 gDimension : 80 x 150 x 55 mm (W x D x H)Power supply : 230 V, 50/60 Hz, 2000 WPower supply : 115 V, 60 Hz


10-0295 Ball-Tipped Valve Rod for 2 mm orifi ce

10-1294 Test Cup, brass with 2 mm orifi ce

21-0697 Digital Stop WatchFor details see: General Equipment

Thermometer

Precision Made


TypeRange Dimensions (mm) /

Immersion (mm)DIN10-0317 10-0318 12 775 / E 0.1/0/50 0 to +50 : 0.1 °C10-0319 10-0320 12 775 / E 0.2/0/100 0 to +100 : 0.2 °C

Precision Made



Immersion (mm)ASTM IP11-0155 11-0156 8C 6C -2 to +400 : 1 °C 385 x Ø 7 / total21-0361 21-0362 - 8F +30 to +100 : 0.5 °F 340 x Ø 7 / 6521-0367 21-0368 - 8C 0 to +45 : 1 °C 340 x Ø 7 / 65

Spare Parts

10-132110-1323

Test Cup, brass, with... 4 mm orifi ce... 10 mm orifi ce

10-032210-0324

Ball-Tipped Valve Rod for... 4 mm orifi ce... 10 mm orifi ce

10-033710-0338

Electric HeaterMains: 230 V, 500 WMains: 115 V, 250 W

11-0130 Measuring Cylinder, 100 ml, graduated, with stand, glass, 1 ml subdivision, 254 mm high

10-0329 Stopper Set, NBR-rubberConsisting of:1x each for orifi ces

12 /15 mm (10-0325 pack of 10)6.5/15 mm (22-0082 pack of 10)5 /20 mm (22-0081 pack of 10)

1x for sample thermometer DIN44/30/bored Ø 8.6 mm (10-0326 slotted)

1x for sample thermometer ASTM / IP44/30/bored Ø 6 mm (10-0327 slotted)

1x for bath thermometer DIN14.5/20/bored Ø 8.6 mm (10-0328)

1x for bath thermometer ASTM / IP14.5/20/bored Ø 6 mm (16-0739)

Scope of ApplicationTo measure the viscosity by determining the effl ux time of a warm sample, through a 10 or 4 mm orifi ce.

Suitable for viscous bitumen emulsions, bituminous binders.

Summary of MethodThe viscometer cup is fi lled with the warm sample, then placed in the bath to settle at a specifi c temperature, before the ball valve is pulled. After the fi rst 25 ml of the sample ran out, the time for the next 50 ml will be determined.

28

21-0695

ViscosityViscosity

Saybolt Viscosity - Universal & Furol Method (semi-automatic)

Bituminous and Residual materials:ASTM D 88 - AASHTO T72 - FTM 791-304 (FTM 141A-4285)JIS K2207Bitumen and Residual materials at high temperatures: ASTM E 102

Universal and Furol viscometers are technically identical designs, except for orifi ce tips which differ in diameter.

Being built-in as interchangeable units in the viscometer, the orifi ce tips, Universal or Furol, can be universally used for all types of Saybolt viscosity measurements.

Main Units

21-050121-0502

Two-Tube Saybolt-Viscometer ASTM D 88 - AASHTO T72 - FTM 791-304 - JIS K2207ASTM E 102Consisting of:stainless steel housing with thermostatically controlled test bath, and electric stirrerSupplied with: 2 receiving fl asks, 60 ml2 pipettes with rubber suction bulb2 thermometer protection tube2 thermometer holders2 cork stoppers2 rubber suction bulbs3 lids for bath opening with Ø 51 mm1 orifi ce spanner1 tube cleaning plungerNote: Thermometers are not includedTechnical Data: Working range : +20 to +230 °C (+68 to +450 °F) Temperature Accuracy : ± 0.03 °C (± 0,05 °F)Power supply : 230 V, 50 Hz, EU-plugPower supply : 115 V, 60 Hz, US-plug.


21-0695 8-Channel Stop Watch(containing 8 individual stop watches)For details see: General Equipment

21-0697 Digital Stop Watch, For details see: General Equipment

21-0703 Filter Funnel No. 100, ASTM E 11

21-0713 Viscosity Tube Cap, ASTM E 102

21-0714 Displacement Ring, ASTM E 102

Scope of ApplicationUsed to determine the Saybolt Universal Viscosityof lubricants and distillates with effl ux times > 32 s orthe Saybolt Furol Viscosity of residual materials with effl ux times > 25 s. Further of petroleum products such as fuel oils and other residual materials having Saybolt Universal viscosities > 1000 s.

Summary of MethodThe effl ux time in seconds of a sample, fl owing through a calibrated orifi ce, is measured under carefully controlled conditions. The time is corrected by an orifi ce factor and reported as the viscosity of the sample at that temperature.

ASTM D 88 temperature range:+21 to +99 °C (70 to 210 °F)ASTM E 102 temperature range:+120 to +240 °C (248 to 464 °F)

29

21-0699

21-0693

ViscosityViscosity

Thermometer

Precision Made



Immersion (mm)ASTM IP

acc. ASTM D 8821-6000 — Set of 1 each: ASTM 17C, 18C, 19C, 20C, 21C, 22C

21-0601 21-0607 17C — +19 to +27 : 0.1 °C 275 x Ø 6.5 / total21-0602 21-0608 18C 23C +34 to +42 : 0.1 °C 275 x Ø 6.5 / total21-0603 21-0609 19C — +49 to +57 : 0.1 °C 275 x Ø 6.5 / total21-0604 21-0610 20C — +57 to +65 : 0.1 °C 275 x Ø 6.5 / total21-0605 21-0611 21C — +79 to +87 : 0.1 °C 275 x Ø 6.5 / total21-0606 21-0612 22C 24C +95 to +103 : 0.1 °C 275 x Ø 7 / total

21-0621 21-0627 17F — +66 to +80 : 0.2 °F 275 x Ø 6.5 / total21-0622 21-0628 18F 23F +94 to +108 : 0.2 °F 275 x Ø 6.5 / total21-0623 21-0629 19F — +120 to +134 : 0.2 °F 275 x Ø 6.5 / total21-0624 21-0630 20F — +134 to +148 : 0.2 °F 275 x Ø 6.5 / total21-0625 21-0631 21F — +174 to +188 : 0.2 °F 275 x Ø 6.5 / total21-0626 21-0632 22F 24F +204 to +218 : 0.2 °F 275 x Ø 7 / total

acc. ASTM E 102 21-0641 21-0646 77F — +245 to +265 : 0.5 °F 275 x Ø 6.5 / total21-0642 21-0647 78F — +295 to +315 : 0.5 °F 275 x Ø 6.5 / total21-0643 21-0648 79F — +345 to +365 : 0.5 °F 275 x Ø 6.5 / total21-0644 21-0649 80F — +395 to +415 : 0.5 °F 275 x Ø 6.5 / total21-0645 21-0650 81F — +445 to +465 : 0.5 °F 275 x Ø 6.5 / total

Reference MaterialThe factory certifi ed viscosity-oil-standards have been tested to perform according to the following list.Content: 470 ml/one pint acc. ASTM D 2162

Factory certifi ed Type

Saybolt Universal Seconds

SUS 100 °F (37.8 °C)Saybolt Universal Seconds

SUS 210 °F (98.9 °C)Saybolt Furol Seconds

SFS 122 °F (50 °C)

24-0606 S 20 96 mm²/s 24-0607 N 35 160 mm²/s24-0616 S 60 280 mm²/s24-0608 N 100 600 mm²/s24-0609 S 200 950 mm²/s 90 mm²/s24-0610 N 350 130 mm²/s24-0611 S 600 180 mm²/s 140 mm²/s24-0613 N 2000 420 mm²/s

For details see: General Equipment

Spare Parts

21-0675 Saybolt Viscosity Tubebrass, gold plated, interchangeable Universal- and Furol-orifi ces (1 ea.) including calibration certifi cate

21-0693 Receiving Flask, 60 ml capacity

21-0699 Oil Pipette with rubber suction bulb21-0700 Oil Withdrawal Tube

21-0701 Cleaning Plunger21-0704 Stopper, NBR-rubber (18/20) with loop

25-060725-0608

Heating Element HD 2000 W, 230 VHeating Element HD 1000 W, 115 V

30

ASTM testing

21-0695

21-0155 21-0157

ASTM calibration / IP testing

Specifi c Viscosity - Engler Method (semi-automatic)

Tar & Tar destillates: ASTM D 1665 - JIS K2208Bituminous emulsions: IP 212 (DIN 51 560)

Specifi c Viscosity Test Equipment - Engler Viscometeracc. ASTM : testing fl ask 50 ml, calibration fl ask 200 mlacc. IP : testing fl ask 200 ml, calibration fl ask 200 ml

Main Units

21-0030 Engler Viscometer

ASTM D 1665 - IP 212 - JIS K2208Consisting of:Basic instrument with gold plated test vessel, tempering bath with digital controller, heater 300 W with over-temperature protection, cooling coil for counter cooling.Supplied with: 1 Kohlrausch fl ask 200 ml (IP & ASTM)1 measuring fl ask, 50 ml (ASTM)3 thermometers (ASTM 23C - 25C)1 thermometer (ASTM 54C/18C)1 silicone stopper (bath thermometer holder)1 lifting table1 miniature spirit level1 m tubingTechnical Data: Working temperature : max. +100 °CStorage temperature : -10 to +70 °CRelative Humidity : to 90%Dimensions / Weight :32 x 26 x 55 cm (W x D x H), 8 kgPower supply : 230 V, 50 Hz, EU-plug




21-0158 Measuring Cylinder, 50:1 ml, Tol. +/-0.5 ml

Thermometer

Precision Made



Immersion (mm) / collarASTM IP21-0113 21-0114 23C – -18 to + 28 : 0.2 °C 212 x Ø 6 / 90 / Ø 821-0115 21-0116 24C – -39 to + 54 : 0.2 °C 237 x Ø 6 / 90 / Ø 821-0117 21-0118 25C – -95 to +105 : 0.2 °C 212 x Ø 6 / 90 / Ø 890-0103 90-1103 54C 18C -20 to +100.6 : 0.2 °C 310 x Ø 7 / total

Spare Parts21-0157 Kohlrausch Flask, 200 ml

(ASTM and IP)

21-0155 Measuring Flask, 50 ml (ASTM)

21-0113 Thermometer ASTM 23C



11-0395 Stopper, Silicone (14.5/20 / bored Ø 6 mm)

90-0103 Thermometer ASTM 54C/IP 18C

50-0001 Spirit Level - Miniaturevertical and horizontal, Dimension: 100 x 40 x 15 mm

50-5242 Lifting Table (Details: Gen. Equipment)

Scope of ApplicationUsed for characterising the consistency by measuring the fl ow properties to determinate the specifi c viscosity.

Suitable for tar and their fl uid products.

Summary of MethodThe time, in s, is measured for a fi xed volume of liquid material to fl ow through an effl ux tube under an accurately reproducible head and at a closely controlled temperature.The Engler specifi c viscosity is then calculated by dividing the effl ux time by the viscometer calibration factor as determined by making the same effl ux measurement for water.It does not determine absolute viscosity, but is an empirical fl ow test.

ViscosityViscosity

31

CFOV - type

22-0097

ViscosityViscosity

Kinematic Viscosity - Glass Capillary Methods (manual)

Liquid petroleum products (transparent & opaque):ASTM D 445 - IP 71-1 (DIN 51 550 - NF T60-100 - FTM 791-305)ISO 3104 - JIS K2283 (DIN 51 366 (CFOV) - DIN 51 372 (BS/IP-RFV))

Glass Capillary specifi cations: ASTM D 446 - IP 71-2 ISO 3105 - JIS K2207

Liquid asphalts (bitumens), road oils (under gravity):ASTM D 2170 - IP 319 - EN 12595 - DIN 52 007-1(FTM 791-305)

Kinematic Viscosity -Cannon-Fenske Opaque Viscometer Method - CFOV (manual)

CFOV - Cannon-Fenske Opaque Viscometer (CR-type) (length: 295 mm, required sample: ~ 12 ml)

Factory Certifi ed

Offi cially Certifi ed Size Constant

[cSt/s or mm2/s2]Viscosity Range [cSt or mm2/s]

22-0070 – Set (1 each) of25 - 600 0.002 - 20.0 0.4 - 20 000

22-0050 22-2050 25 0.002 0.4 - 222-0051 22-2051 50 0.004 0.8 - 422-0052 22-2052 75 0.008 1.6 - 822-0053 22-2053 100 0.015 3 - 1522-0054 22-2054 150 0.035 7 - 3522-0055 22-2055 200 0.1 20 - 10022-0056 22-2056 300 0.25 50 - 25022-0057 22-2057 350 0.5 100 - 50022-0058 22-2058 400 1.2 240 - 1 20022-0059 22-2059 450 2.5 500 - 2 50022-0060 22-2060 500 8.0 1 600 - 8 00022-0061 22-2061 600 20.0 4 000 - 20 000

Note: Holders, tempering bath, fi lling & cleaning equipment are required!

CFOV Accessories

22-0097 Holder "CFRV-CFOV" with suspension bracket (for factory certifi ed viscometers)

22-2065 Holder "CFOV" with suspension (for offi cially certifi ed viscometers)

22-0164 Stopper, NBR-rubber (18/20, bored Ø 6 mm)

22-0528 Stopper, solid rubber, Ø 2-6 mm, 20 mm high, pack of 10 (to close the viscometer tube)

22-0093 Conical Silicone Tubing (for suction of liquids)

23-0204 Suction Syringe, made of glass

Scope of ApplicationUsed to characterizes the fl ow behavior at +60°C (140°F) and +135°C (275°F).

Suitable for liquid asphalts (bitumens), their distillation residues and road oils at +60°C (140°F) or of asphalt cements at +135°C (275°F) with a viscosity from 6 to 100 000 cSt.

Kinematic Viscosity:[mm²/s = cSt]

Dynamic Viscosity: [mPa·s = cP]

Dynamic Viscosity: [dPa·s = P = poise]

Summary of MethodThe time is measured for a fi xed volume of the liquid to fl ow under gravity through the capillary tube, under an accurately reproducible head and at a closely controlled temperature.The kinematic viscosity is then calculated by multiplying the effl ux time in seconds by the viscometer calibration factor.The dynamic viscosity can be obtaint by multiplying the measured kinematic viscosity by the density of the liquid.

32

ZCAV - type

RFV - type

22-0278

RFV - type

22-0278

ViscosityViscosity

Kinematic Viscosity - Zeitfuchs Cross-Arm Viscometer Method - ZCAV (manual)

ZCAV - Zeitfuchs Cross-Arm Viscometers(length: 295 mm, required sample: ~ 3 ml)

Factory Certifi ed



– 22-0530 1 0.003 0.6 - 3– 22-0531 2 0.01 2 - 10– 22-0532 3 0.03 6 - 30– 22-0533 4 0.1 20 - 100– 22-0534 5 0.3 60 - 300– 22-0535 6 1 200 - 1 000– 22-0536 7 3 600 - 3 000– 22-0537 8 10 2 000 - 10 000– 22-0538 9 30 6 000 - 30 000– 22-0539 10 100 20 000 - 100 000


ZCAV Accessories22-0540 Holder - UNIVERSAL with suspension bracket (for ZCAV viscometer)22-0528 Stopper, solid rubber, Ø 2-6 mm, 20 mm high, pack of 10

(to close the viscometer tube)

Kinematic Viscosity - BS/IP Reverse Flow Viscometer Method - RFV (manual)

RFV - U-Tube Reverse Flow Viscometer (length: 275 mm, required sample: ~ 12 - 25 ml)

Factory Certifi ed



22-0220 – Set (1 each) of1 - 11 0.003 - 300 0.6 - 300 000

22-0200 22-2200 1 0.003 0.6 - 322-0201 22-2201 2 0.01 2 - 1022-0202 22-2202 3 0.03 6 - 3022-0203 22-2203 4 0.1 20 - 10022-0204 22-2204 5 0.3 60 - 30022-0205 22-2205 6 1 200 - 1 00022-0206 22-2206 7 3 600 - 3 00022-0207 22-2207 8 10 2 000 - 10 00022-0208 22-2208 9 30 6 000 - 30 00022-0209 22-2209 10 100 20 000 - 100 00022-0210 22-2210 11 300 60 000 - 300 000


RF - U-tube Accessories22-0278 Holder - RFV with suspension bracket (for BS/IP viscometer)22-0270 Pipette, 50 ml with stopper (to withdraw air by suction)22-0528 Stopper, solid rubber, Ø 2-6 mm, 20 mm high, pack of 10

(to close the viscometer tube)

33

22-0529 22-0528

22-0515 & 22-0516

AIVV - type

CMVV - type

ViscosityViscosity

Dynamic Viscosity - Vacuum Capillary Method (manual)ASTM D 2171 - IP 222 - EN 12596

Summary of MethodThe time is measured for a fi xed volume of the liquid to be drawn-up by vacuum through a capillary tube, under closely controlled conditions of vacuum and temperature. The viscosity in poises is calculated by multiplying the fl ow time in seconds by the viscometer calibration factor.

1 dPa·s = 1 P = poise1 Pa•s = 10 P = 10 poises

Dynamic Viscosity - Cannon-Manning Vacuum Viscometer Method - CMVV (manual)

CMVV - Cannon-Manning Vacuum Viscometer (length: 180 mm, required sample: ~ 6 ml)

Factory Certifi ed

Offi cially Certifi ed Size Viscosity Range

[Poise or dPa·s]

22-0500 – 4 0.036 - 0.822-0501 – 5 0.12 - 2.422-0502 – 6 0.36 - 822-0503 – 7 1.2 - 2422-0504 – 8 3.6 - 8022-0505 – 9 12 - 24022-0506 – 10 36 - 80022-0507 – 11 120 - 2 40022-0508 – 12 360 - 8 00022-0509 – 13 1 200 - 24 00022-0510 – 14 3 600 - 80 000


Dynamic Viscosity - Asphalt Institute Vacuum Viscometer Method - AIVV (manual)

AIVV - Asphalt Institute Vacuum Viscometer(length: 180 mm, required sample: ~ 3 ml)

Factory Certifi ed

Offi cially Certifi ed Size Viscosity Range

[Poise or dPa·s]

22-0520 – 25 42 - 80022-0521 – 50 180 - 3 20022-0522 – 100 600 - 12 80022-0523 – 200 2 400 - 52 00022-0524 – 400R 9 600 - 1 400 00022-0525 – 800R 38 000 - 5 800 000


CMVV & AIVV Accessories

22-0529 Holder - VV without suspension bracket(for CM- & AI-Vacuum-Viscometer) neoprene rubber, fi ts Ø 51 mm bath openings

22-0528 Stopper, solid rubber, Ø 2-6 mm, 20 mm high, pack of 10(to close the viscometer tube)

22-0515 Vacuum Manifold

22-0516 Digital Vacuum Regulator with pump, 240 V, 175 W horizontal orientation, non-mercury system, CE-approved

Scope of ApplicationUsed to characterizes the fl ow behavior at +60°C (140°F).

Suitable for: cutbacks and asphalt cements at 60°C (140°F) with a viscosity from 0.036 to over 200 000 P.

34

Reference Material

21-0695

22-0450

20-0030

ViscosityViscosity

Capillar Viscometer - Options & Accessories 22-0528 Stopper, solid rubber, Ø 2-6 mm, 20 mm high, pack of 10 (to close the viscometer tube)



20-003020-0040

Luminous BackgroundLarge fi eld lamp for convenient glare-free observation of the viscometers immersed in the thermostatic bath.Power supply: 220/250 V, 50/60 Hz, 22 WPower supply: 115 V, 50/60 Hz

Filling & Cleaning Devices

22-0270 Pipette, 50 ml with stopper (for fi lling of RFV-type)

23-0204 Suction Syringe, made of glass (for fi lling of CFOV-type)

22-0093 Conical Silicone Tubing (for suction of liquids)

10-0013 Water Jet Pump acc. to Hanff, made of glass

25-048525-0486

Vacuum-Pump with Mini-Compressor & AccessoriesConsisting of:1 oil-free diaphragm pump with fi lter1 hose (Ø 6 mm x 1 m, silicon, clear)1 T-piece connection (Ø 7.5 mm)1 Hoffmann-ClipTechnical Data:Max. capacity : 6 l/minEnd vacuum : 100 mbarOperating pressure : 2.4 bar (overpressure)Dimensions / Weight : 9 x 17 x 12 cm (W x D x H), 1.9 kgPower supply : 220/230 V, 50 Hz, EU-plugPower supply : 115 V, 60 Hz

20-009520-0096

Viscometer Tube Cleaner and Dryerwashes (with solvents) and dries (with pressurized air) up to six glass capillary tubes at a time.Note: Requires pressurized air source (150 psi maximum)Dimensions (L x W x H): 41 x 18 x 32 cm (7 kg) & solvent tank (15 kg)... with solvent container... without solvent container

22-0450 ViscoHanger - Universal Glass Capillary Viscometer StandAllows to hang-up all viscometer-types fi tted into holders with suspension (not ViscoClock - holders) to let the bath fl uid from into the detached leakage tray (stainless steel, chemical resistant).Dimensions (L x W x H): 51 x 28 x 49 cmAvailable holders with suspension:Cannon Fenske (22-0097), BS/IP Viscometer (22-0278), Ubbelohde (22-0155), Zeitfuchs Cross-Arm (22-0540)

Reference MaterialThe values listed in the following table are to be considered as nominal and approximate only (depending on the batch). The actual and exact data will be printed on the container-lable or on a separate certifi cate.Content: 470 ml / 1 pint Shelf life: 2 years

UKAS Type

Kinematic Viscosity [mm²/s = cSt] Dynamic Viscosity [mPa·s = cP]

certifi ed approx. 20°C68°F

25°C77°F

37.8°C100°F

40°C104°F

50°C122°F

60°C140°F

80°C176°F

99°C210°F

100°C212°F

24-0616 S 60 mm²/smPa·s

160140

120100

6051

5446

3529

−−

1311

7.96.4

7.76.3

24-0609 S 200 mm²/smPa·s

650570

460400

210180

180160

11092

−−

3226

1815

1814

24-0611 S 600 mm²/smPa·s

22001900

15001300

600520

520450

290250

−−

7361

3831

3630

24-0613 S 2 000 mm²/smPa·s

81007100

53004700

20001700

17001500

900780

−−

189160

9075

8672

24-0615 S 8 000 mm²/smPa·s

3500031000

2300020000

79007000

67005900

33002900

−−

591507

−−

240200

24-0618 S 30 000 mm²/smPa·s

−−

8100073000

2800024000

2300021000

110009700

−−

17441510

−−

660560

35

20-0150

20-0156

ViscosityViscosity

Tempering Bath

20-015020-0151

High Temperature Liquid BathConsisting of:digital temperature read-out, 7 test places (Ø 50 mm) and front window (270 x 285 mm)Note: Bath thermometers ASTM 47 / IP 35 or ASTM 110 are surgested.Technical Data: Working range : +5 °C above ambient (or cooling water) up to +150 °CConstant : 0.02 KIncreasement : 0.1 °C Stability : ±0.01° C and better (with water at +55 °C)Bath opening : 26 x 24 x 30 cm (W x D x H)Volume : 40 lDimensions / Weight : 59 x 35 x 56 cm (W x D x H), 41 kgPower supply : 230 V, 50/60 Hz, 1500 W, EU-plugPower supply : 115 V, 50/60 Hz, 1500 W

20-015620-015720-0158

Circulator (external & internal heating & cooling)Used for counter-cooling the Liquid BathSupplied with: 1 bath coverNote: Insulated hose-set (25-0228) is recommended.

For details see: General Equipment Dimensions / Weight : 27 x 46 x 57 cm (W x D x H), 30 kgPower supply : 230 V, 50 Hz, 1400 W, EU-plugPower supply : 230 V, 60Power supply : 115 V, 60 Hz

22-0164 Stopper, NBR-rubber (18/20, bored Ø 6 mm)

50-916150-9162

Bath Fluid Silicon Oil basedTemperature Range : approx. +10 to +200 °CColor : Water Clear 5 liters10 liters

Thermometers (acc. ASTM E 1)

Precision Made



Immersion (mm)ASTM IP90-0285 90-1285 74C 69C -55.6 to -53.9 : 0.05 °C 305 x Ø 7 / total90-0173 90-0252 73C 68C -41.4 to -38.6 : 0.05 °C 305 x Ø 7 / total90-0212 90-1212 126C 71C -27.4 to -24.6 : 0.05 °C 305 x Ø 7 / total90-0214 90-1214 127C 99C -21.4 to -18.6 : 0.05 °C 305 x Ø 7 / total90-0284 90-1284 72C 67C -19.4 to -16.6 : 0.05 °C 305 x Ø 7 / total90-0215 90-1215 128C 33C -1.4 to +1.4 : 0.05 °C 305 x Ø 7 / total90-0100 90-0250 44C 29C -80.0 to +20.0 : 1 °C 305 x Ø 7 / total90-0101 90-1101 45C 30C +23.6 to +26.4 : 0.05 °C 305 x Ø 7 / total90-0204 90-1204 118C − +28.6 to +31.4 : 0.05 °C 305 x Ø 7 / total90-0241 90-1241 28C 31C +36.6 to +39.4 : 0.05 °C 305 x Ø 7 / total90-0136 90-0253 120C 92C +38.6 to +41.4 : 0.05 °C 305 x Ø 7 / total90-0102 90-0251 46C 66C +48.6 to +51.4 : 0.05 °C 305 x Ø 7 / total90-0281 90-1281 29C 34C +52.6 to +55.4 : 0.05 °C 305 x Ø 7 / total90-0149 90-1149 47C 35C +58.6 to +61.4 : 0.05 °C 305 x Ø 7 / total90-0311 90-1311 − 100C +78.6 to +81.4 : 0.05 °C 280 x Ø 6.5 / total90-0240 90-1240 48C 90C +80.6 to +83.4 : 0.05 °C 305 x Ø 7 / total90-0217 90-1217 129C 36C +91.6 to +94.4 : 0.05 °C 305 x Ø 7 / total90-0137 90-0254 121C 32C +98.6 to +101.4 : 0.05 °C 305 x Ø 7 / total90-0196 90-1196 110C 93C +133.6 to +136.4 : 0.05 °C 305 x Ø 7 / total90-0315 90-1315 132C 102C +148.6 to +151.4 : 0.05 °C 305 x Ø 7 / total

Thermometers (High-Precision acc. DIN 12 771)

Precision Made



Immersion (mm)DIN22-0157 22-0158 − +18 to +24 : 0.01 °C22-0159 22-0160 − +36 to +42 : 0.01 °C22-0161 22-0162 − +50 to +60 : 0.01 °C

22-0163 Protective Sleeve for bath-thermometers

36

10-1117 (with Timer)

10-0117

AgingAging

Effect of Heat and Air - Loss-On-Heat Method - LOH (semi-automatic)

Semi-solid Bitumen: ASTM D 6 (AASHTO T 47) - JIS K2207 EN 13 303 (IP 45, NF T66-011) - IP 506

To determine the loss in mass of bitumen, after being heated. It is suitable to confi rm the presents of volatile components.

Effect of Heat and Air - Thin-Film-Oven Method - TFOT (semi-automatic)

Semi-solid Bitumen: ASTM D 1754 - JIS K2207 EN 12607-2 (NF T66-047) - IP 460-2

Simulating the combined effects of heat & air on a thin fi lm of bituminous binders during conventional hot-mixing.

Main Units

10-011710-0118

TFOT & LOH 4 - Semi-Automatic Thin-Film & Loss-On-Heat Oven

Depending on accessories suitable for:TFOT - Resistance to Hardening (Thin-Film-Oven-Test): ASTM D 1754 - JIS K2207 - EN 12 607-2 - IP 460-2LOH - Loss in Mass (Loss-On-Heat): ASTM D 6 (AASHTO T 47) - JIS K2207 - EN 13 303 - IP 506

Features: • for bitumen, fl ux oil & bituminous compounds• digital display of temperature with a 1°C resolution • overheat protection acc. to DIN 12 880 class 2• venting continuously variable• multi-purpose use due to removable gratings and motor switch-off

Consisting of:double-walled electrically heated convection type oven with illuminated stainless steel chamber, door with twin paned observation window (260 x 200 mm), safety thermostat with cut-off limit (thermal safety class 2), electronic PID-temperature controller with Pt-100 temperature probe and digital display of set point & actual values, continuously variable venting, switchable gear-motor assembly with axle (Ø 10 mm) to connect a horizontal rotating shelf.

Supplied with: 1 thermometer ASTM 13C, 1 thermometer support, 2 removable gratings

Note: Test equipment according to the standards is to be ordered separately!

Technical Data: Test places : acc. to the accessoriesTemperature max. : 300 °C (resolution: 1°C) (572 °F)Warming-up rate : 8 - 10 K/minAir change : 2 m³/h continuously variableRotating speed : 5- 6 rpmDimensions, interior : 403 x 370 x 380 mm (W x D x H), 57 literDimensions : 744 x 535 x 576 mm (W x D x H)Weight : approx. 50 kgPower supply : 220-250 V, 50/60 Hz, 6.5 A, EU-plugPower supply : 110-125 V, 50/60 Hz, 13 A

10-1117

TFOT & LOH 4/Ti - Semi-Automatic Thin-Film & Loss On Heat Oven with Timerlike TFOT & LOH 4 but additionally with: daily program timer (15 minutes intermittent) and high temperature-resolution (0.1°C)Power supply : 220-250 V, 50/60 Hz, 6.5 A, EU-plug

Scope of ApplicationUsed to confi rm volatile components in bitumen.

Measuring the combined effects of heat & air on a thin fi lm of bituminous binders.

Suitable for bitumen (asphalt), fl ux oil & bituminous binders.

Summary of MethodThe effects of heat and air are determined by physical tests measured before and after the oven treatment. Therefore a thin fi lm of a sample is heated in an constantly vented oven with a horizontal rotating shelf.

ASTM D 6 - EN 13 303 - IP 506:To determine the loss in mass a sample is weighed before and after being heated at a certain temperature for a specifi ed time. Requires a shelf with: 9 sample containers (metal, Ø 55 mm x 35 mm)

ASTM D 1754 - EN 12 607-2 - IP 460-2:Examine the loss in mass (by analytical balance) and the changed properties (by Viscosity, Penetration, Ductility or Softening-Point).Requires a shelf with: 4 sample containers (stainless steel, Ø 140 mm x 9.5 mm)

37

10-0123

10-0211

10-0212

10-0117 & 10-0211 (LOH)

10-0117 & 10-0212 (TFOT)

10-0117 & 10-0123 (TFOT & LOH)

AgingAging


10-0123 Test Kit - LOH & TFOT (Petrotest® modifi cation) ASTM D 6 - EN 13 303 - IP 506 and in analogy to ASTM D 1754 - EN 12 067-2 - IP 460-2Consisting of:1 rotating shelf, nickel-plated brass (Ø 266 mm x 3 mm), dual-purpose, 9 sample jars LOH, nickel-plated brass (Ø 55 mm x 35 mm), fl anged rim 3 sample dish TFOT, stainless steel (Ø 140 x 9.5 mm), fl at-bottom

10-0211 Test Kit - LOH ASTM D 6 - EN 13 303 - IP 506 Consisting of:1 rotating shelf, nickel-plated brass (Ø 266 mm x 3 mm), dual-purpose, 9 sample jars LOH, nickel-plated brass (Ø 55 mm x 35 mm), fl anged rim

10-0212 Test Kit - TFOT ASTM D 1754 - EN 12 067-2 - IP 460-2Consisting of:1 rotating shelf, cast aluminum (Ø 345 mm) 3 sample dish TFOT, stainless steel (Ø 140 x 9.5 mm), fl at-bottom

10-0128 Sample Dish, aluminum, (for TFOT - EN 12 607-2, IP 460-2)fl at-bottom (Ø 140 x 9.5 mm) (Ø 5½" x 3/8")

Thermometer

Precision Made



Immersion (mm)ASTM IP10-0126 10-0127 13C 47C +155 to +170 : 0.5 °C 155 x Ø 6.5 / total

Spare Parts18-0066 Sample Jar, nickel-plated brass

(Ø 55 mm x 35 mm), fl anged rim (for LOH - ASTM D 6, EN 13 303, IP 506)

10-0146 Sample Dish, stainless steel (Ø 140 x 9.5 mm) (Ø 5½" x 3/8") fl at-bottom (for TFOT - ASTM D 1754, EN 12 607-2, IP 460-2)

10-0150 Rotating Shelf - LOH & TFOT nickel-plated brass, dual-purpose, (Ø 266 mm x 3 mm), suitable for 9 LOH-sample jars (18-0066) or 3 TFOT-sample dishes (10-0128 / 10-0146)

10-0149 Rotating Shelf - TFOT cast aluminum (Ø 345 mm) suitable for4 TFOT-sample dishes (10-0128 / 10-0146)

10-0222 Thermometer Holder for shelf-axle

10-0242 Grating, chromium-plated steel (2 shelfs with supports)Dimensions (W x D): 387 x 365 mm

10-0243 Axle (Ø 10 mm) for rotating shelf

10-013410-0135

Gear-Motor for TFOT & LOH oven with connection-tube for shelf-axle, cable with plug and connectionsPower supply: 230 V, 50/60 HzPower supply: 115 V, 50/60 Hz

10-0244 Light bulb, 220 V, 15 W, E14

10-0245 Light bulb, 110 V, 15 W, E14

38

10-0619

AgingAging

Effect of Heat and Air - Rolling Thin Film Oven Test Method - RTFOT (semi-automatic)

Bitumen : ASTM D 2872 - Superpave® (AASHTO T 240) - JIS K2207Bituminous binders: EN 12607-1

Main Units

10-0619

RTFOT/ASTM - Semi-Automatic Rolling-Thin-Film Oven TesterASTM D 2872 - Superpave® - JIS K2207 - EN 12607-1

Features: • for semi-solid bitumen (asphalts)• digital display of temperature & settings • squirrel cage protected fan• venting continuously variable• fl owmeter control

Consisting of:double-walled illuminated heated convection type oven made of stainless steel, door with heat resistant twin paned glass window, safety thermostat and digital display, internal fan, symmetrical top and bottom vents, circular and vertical rotating 8-place aluminum rotating shelf, fl owmeter controlled air jet at the lowest point blows pre-heated air with a constant volume into each passing glass

Supplied with: 8 sample jars & 1 thermometer ASTM 13C

Note: Pressure reducer is recommended

Technical Data: Test places : 2 - 8Working temperature : +163 °C (325 °F)Rotating speed : 15 rpmAir volume : 4000 ml/minInside dimensions : 483 x 450 x 381 mm (W x D x H)Outside dimensions : 750 x 650 x 820 mmWeight : approx. 50 kgPower supply : 230 V, 50 Hz, 16 A, EU-plug

10-0621 Pressure Reducer with valve and manometer, 0.2 to 7 bar


25-048925-0490

Vacuum Pump with Mini-Compressor Consisting of:1 oil-free diaphragm pump with fi lter, 1 hose (Ø 6 mm x 1 m, silicon, clear), 1 T-piece connection (Ø 7.5 mm) 1 Hoffmann-ClipTechnical Data: Max. capacity : 11.5 l/minEnd vacuum : 240 mbarOperating pressure : 2 bar (overpressure)Dimensions : 9 x 20 x 13 cm (W x D x H), Weight: 2.2 kgPower supply : 220/230 V, 50 Hz, EU-plugPower supply : 110/115 V, 60 Hz, US-plug

16-0700 Air Volume Meter to calibrate the fl owmeter of the RTFOT-ovenTechnical Data:Type : drum-gasmeter for small quantities Range : 6 - 360 l/h Volume min. : 0.02 l readable Accuracy : ±0,2 %Drum volume : 3 l

Thermometer

Precision Made



Immersion (mm)ASTM IP10-0126 10-0127 13C 47C +155 to +170 : 0.5 °C 155 x Ø 6.5 / total

Spare Parts10-0625 Sample Jar, heat-resistant glass

(Ø 64 mm x 140 mm)50-5172 Hose-Clip, Hoffmann-type

Scope of ApplicationTo determine the effects of heat and air during conventional hot-mixing on a thin moving fi lm of semi-solid bitumen or bituminous binders.Indicating the resistance to hardening under infl uence of heat and air and the change in sample mass (Loss on Heat).

Suitable for bitumen (asphalt), fl ux oil & bituminous binders.

Summary of MethodThe effects of heat and air are determined by physical tests measured before and after the oven treatment. A moving fi lm of a sample is heated in an oven with a constant air fl ow and a vertical rotating shelf.

ASTM D 2872:The samples are cooled down in horizontal position in a metal rack. The change in sample mass (by analytical balance) and the changed properties of bitumen (by Ductility, Viscosity) are examined.

EN 12 607-1:The samples are cooled down in a desiccator.The change in sample mass (by analytical balance) and the changed properties of binders (by Penetration, Softening-Point, Viscosity).

39

10-2110

Glass-Set Bitumen

AgingAging

Effect of Heat and Air - Rotating Flask Method - RFT (semi-automatic)

Bituminous binders: EN 12607-3 (DIN 52 016, NF T66-048) - IP 460-3

Main Units

10-2110

RFT - Semi-Automatic Rotating Flask Testerin analogy to EN 12 607-3 (DIN 52 016, NF T66-048) - IP 460-3Features: • digital display of rotation speed, bath & steam temperature• adjustable dip-in depth• manual lift• timer

Consisting of:Rotary evaporator with double-walled stainless steel oil bath, manual lift, adjustable dip-in depth, electronic controlled rotation drive, LED of rotation speed, bath temperature, built-in timer, overtemperature cut-off.

Supplied with: 1 bitumen-glass-set incl. 1000 ml round fl ask

Technical Data: Test places : 1Working temperature : +20 to +210 °C Rotating speed : 20 - 280 rpmEvaporation volume : approx. 1000 ml/hBath volume : 4.5 lDimensions : 490 x 395 x 430 mm (W x D x H) (w/o. glassware)Weight : 17 kg (w/o. glassware)Power supply : 230 V, 50/60 Hz, 1300 W, EU-plug


25-048525-0486

Vacuum Pump with Mini-Compressor Consisting of:1 oil-free diaphragm pump with fi lter, 1 hose (Ø 6 mm x 1 m, silicon, clear), 1 T-piece connection (Ø 7.5 mm)1 Hoffmann-ClipTechnical Data: Max. capacity : 6 l/minEnd vacuum : 100 mbarOperating pressure : 2.4 bar (overpressure)Dimensions / Weight : 9 x 17 x 12 cm (W x D x H), 1.9 kgPower supply : 220/230 V, 50 Hz, EU-plugPower supply : 110/115 V, 60 Hz, US-plug

16-0773 Flowmeter 4 - 40 l/h, calibrated, with accessoriesConsisting of:1 fl owmeter (150 mm glass-tube, mm-scale and V-shaped metal fl oat) mounted on a tripod-stand with leveling screws and leveling bulb,1 hose (Ø 6 mm x 1 m, silicon, clear), 1 T-piece connection (Ø 7.5 mm) 2 angled hose connectionsNote: The correlation between scale readings and fl ow volumes are listed in the calibration sheet.

Technical Data: Range : 4 - 40 l/h Factory calibration : at +20 °C and 1000 mbar ambient pressure Dimensions / Weight : 180 x 180 x 230 mm (W x D x H), 1 kg

Thermometer

Precision Made



Immersion (mm)ASTM IP10-0065 10-0066 16C 61C +30 to +200 : 0.5 °C 395 x Ø 7 / total

Scope of ApplicationTo determine the effects of heat and air during conventional hot-mixing on a thin moving fi lm of bituminous binders.The loss in mass is used to determine the volatility upon heating.Suitable for bituminous binders.

Summary of MethodThe effects of heat and air are determined by physical tests measured before and after the rotation treatment. Therefore a moving thin fi lm of a sample is heated in an rotating fl ask of a rotary evaporator. The rotation shall prevent a surface hardening.

EN 12 607-3The samples are cooled down in a desiccator.The change in sample mass (by analytical balance) and the changed properties of binders (by Penetration, Softening-Point, Viscosity) are measured.

40

PAV

10-0146

AgingAging

Accelerated Aging - Pressure Aging Vessel Method - PAV (automatic)Accelerated long-term aging ASTM D 6521 - AASHTO R28 (AASHTO PP1) - EN 14769 Superpave® - SHRP 1001 - AASHTO M320 (AASHTO MP1) - (ASTM PS 36)

(Short-term aging/conditioning: see RTFOT- TFOT - RFT Methods)

Summary of MethodSamples aged by this method have previously been prepared in the condition they would be applied to the road.At fi rst a binder is aged using the RTFOT-Method (to simulate plant aging), than it is placed in TFOT stainless steel pans before beeing aged acc. PAV.

A fi lm of binder is heated to a specifi ed temperature, under a specifi ed air pressure for a given period of time to simulate the changes occurring to the binder within the pavement during use.Temperature range

• ASTM : +90°C to +110°C (+194 to +230°F)• EN : +80°C to +115°C

Main Units

10-072010-0722

PAV - Automatic Pressure Aging VesselASTM D 6521 - AASHTO R28 - EN 14 769 Superpave® - AASHTO M320 - SHRP 1001 Features: • Ready-to-Go Set • Bench Top Unit • Integral Vessel & Oven Design • ASME & CE Conform

Consisting of:Bench Top Unit: Integral vessel/oven design according to EEC pressure vessel directive 97/23 EC (incl. CE conformity declaration). Vertical stainless steel pressure vessel with encased band heaters and integral pressure measurement control and temperature control.Thermo Regulation: PID-controller with digital display, 2 Pt-100 temperature probes (one inside the vessel the other to control the heaters on the outside).Programmable Logic Controller (PLC): 2 serial communication ports, (1 connection for front panel display, 1 connection for phone, modem or Ethernet converter as remote control option)Process data like temperature & pressure are continually stored in regular intervals.User Interface: LCD (4 lines, 20 character); 4 Function-, 4 Cursor- & 1 Enter/Return-key.

Supplied with: 10 TFOT sample dishes (acc. AASHTO T 179) (Ø 140 x 9.5 mm) (Ø 5½” x 3/8”) 1 holder to place 10 samples inside the vessel

Note: Requires compressed air (min. 2.24 MPa / 325 psi / 23 bar) and an air pressure regulator.

Technical Data: Operating Pressure : max. 2.1 MPa (304 psi)Temperature Range : +80 to +115 °C Resolution : ±0.1°C Uniformity : ±0.5°CSetpoint Temperature : achievable in <120 min. (if pre-heated)Dimensions / Weight : 700 x 460 x 760 mm (WxDxH) / approx. 130 kgPower supply : 230 V, 50/60 Hz, 10 A, 1 Phase, EU-plugPower supply : 115 V, 50/60 Hz, 20 A, 1 Phase, US-plug


10-0725 Stand (Table), steel (Dimension: 560 x 915 x 660 mm (H x W x D))

10-0726 Compressed Air Reducer with connection to European pressure vessels, incl. hose.

10-0727 Remote Control Option allows user to access graphical displays, to retrieve data and remotely control and monitor one PAV-unit.Consists of: Windows®-PC, color-monitor, mouse, modem (details upon request)

50-0001 Miniature Spirit Level vertical and horizontal (Dimension: 100 x 40 x 15 mm)(to level the pan fi xture after PAV installation)

10-0146 Sample Dish, stainless steel (Ø 140 x 9.5 mm) (Ø 5½" x 3/8") fl at-bottom (acc. TFOT - ASTM D 1754, EN 12 607-2, IP 460-2)

Spare Parts

10-0724 Sample Dish (acc. AASHTO T 179) (Ø 140 x 9.5 mm) (Ø 5½” x 3/8”), pack of 10

Scope of ApplicationUsed to measure the accelerated aging (oxidation) by means of pressurized air and elevated temperature.It simulates the type of in-service oxidative aging that occurs in binders during pavement service.

Suitable for bitumen and bituminous (asphalt) or modifi ed binders.

41

Set-up with Skimmer

12-5700 & 12-5735 & 12-5754

Pt-100 resting in 12-5751

Set-up with Pt-100 weight & skimmer

Flash- & Fire-Point (open cup)Flash- & Fire-Point (open cup)

Flash- & Fire-Point - Cleveland Open Cup Method - CLA 5 (automatic)

Cleveland Method:Binder & Petroleum Products:Superpave® AASHTO T48 - ASTM D 92

Petroleum Products (except fuel oil)ASTM D 92 - JIS K2265-4 - GOST 4333 AASHTO T48 - FTM 791-1103IP 36 (BS 4689)ISO 2592 (EN 22592, DIN 51 376, NF T60-118)

The CLA 5 is a logical further development of the tried-and-tested automatic flash and fire point testing device CLA 4.

In addition to further improved device handling, this automatic equipment features modern electronics with a 5.7" color graphics display, jog-shuttle control and several USB interfaces.

The firmware enables intuitive device operation as well as sophisticated data administration and management of several languages.

Features

• Automatically lights test flame, relights if necessary during the test, suppresses gas source at end of test

• Built-in sensor for automatic barometric pressure correction

• Overheating detection with automatic heat shut-off during the test

• Pt-100 glass probe included, (stainless steel type optional)

• Manual testing, preset or individually set programs

• 2 Calibration modes: - dynamic calibration against certified ASTM-thermometer - sample Pt-100 calibration by correction table with

21 calibration points (preset every 20°C or user defined)

• Calibration protocol print out

• Jog-Shuttle operation (turn & push) with LED indication for operation (blue flashing), cooling down (red), failure (red flashing)

• Multi-language user support (English, French, German, others planned)

• Memory for 1000 tests, 20 operator names, 100 sample names, 21 test methods

• Message when result is out of specification

• Statistical result analysis (MIN, MAX, AVE, Repeatability)

• Password protection access for Service & Configuration level (supervisor master password)

• Easy firmware update and data handling via USB stick or import into EXCEL

Programs

The following programs are available:

2 ASTM Programs (1x Flash-, 1x Flash &Fire-Point)2 ISO Programs (1x Flash-, 1x Flash &Fire-Point)2 JIS Programs (1x Flash-, 1x Flash &Fire-Point)2 GOST Programs (1x Flash-, 1x Flash &Fire-Point)1 Bitumen Program1 Search run1 Calibration run (dynamic mode)10 User programs

Scope of ApplicationUsed to defi ne the hazards of fl ammable and combustible materials acc. to shipping and safety regulations.

Suitable for viscous materials having a fl ash-point between +79°C (175°F) and +400°C (752°F).

Summary of MethodThe temperature of the approximately 70 ml test specimen is increased rapidly at fi rst and then at a slower constant rate as the fl ash-point is approached. At specifi ed intervals a test fl ame is passed across the cup until the sample infl ames.Used to measure the tendency of the test specimen to form a fl ammable mixture with air.

The fl ash-point is the lowest liquid temperature at which the application of an ignition source causes the specimen vapors to ignite.

To determine the fi re-point, the test is continued until the application of the ignition source causes the test specimen to ignite and sustain burning for a minimum of 5 s.

42

12-5700

12-5753

12-5740

12-5750

12-0970

12-5735

12-5754

Main Units

12-570012-5701

CLA 5 - Automatic Flash- & Fire-Point Tester - Cleveland MethodPetroleum Products (except fuel oil) : ASTM D 92 - AASHTO T48 - FTM 791-1103

GOST 4333 - IP 36 - ISO 2592 - JIS K2265-4Binder, Petroleum Products : Superpave® (AASHTO T48, ASTM D 92)

Consisting of:- High-grade steel housing with two-color powder coating, electric heater with

overheat protection, gas flame applicator and gas supply regulation valve- Ionization sensor for detection of flash and fire points- Built-in barometric pressure sensor- Large 5.7'' QVGA color LCD (115 X 85 mm),

sample temperature indication 20 mm high, visible from up to 10 m distance- Splash-proof membrane key panel and Jog-shuttle for input of test parameters,

sample name and program selection- Menu operation with Jog-Shuttle with LED indication- Microprocessor electronics with test programs for flash and fire pointSupplied with:1 cup "CL" (heat resistant handle)1 temperature probe Pt-100 (glass) "CLA5"1 drip pan (for Pt-100 and skimmer)1 gas igniter with thermocouple, 1 electric igniter, 1 flame detection unit1 flame extinguisher cover, 1 tool set "CLA5"Technical Data: Temperature Range : +79 to +400 °C (+175 to +752°F)Display : 115 X 85 mm QVGA color LCD, °C or °F (selectable)Sensing System : Ionization MethodBarometric Pressure : automatic correction of the measured valuesSafety : overheat protection, automatic shut-offIgnition : Gas flame (electric ignition, automatic control)Gas Connection : for propane/butane or natural gas (max. 0.05 bar)Interface : 1x USB (front), 2 x USB (rear), 1x RS232Dimensions : 23 x 47 x 46 cm (WxDxH), Weight: 12 kgPower supply : 110/230 V, 50/60 Hz, EU-plug, approx. 600 Watt Power supply : 110/230 V, 50/60 Hz, US-plug

Options & Accessories12-5735 Draft Deflector - CLA 5

12-5749 Temperature Probe Pt-100 (Metal) - CLA 5 for sample temperature measurement

12-5754 Skimmer - CLA 5 for surface skin removal

12-5759 Service Kit - CLA 5 Consisting of: USB-Stick, storage card, 0-modem datacable

12-0970 Cup - CL-NIRO with heat resistant handle, approx. 70 ml (with filling mark), stainless steel Note! Flash-point results of stainless steel test inserts may deviate from standard results.

12-5756 Calibration Kit - CLA 5 - Flashpoint Detection Consisting of: 1 combi-resistor

12-5766 Calibration Kit - CLA 5 Temperature of Sample & Block Consisting of: 1 set of precision resistor plugs

50-9111 Reference Liquid, Flash-Point "ASTM D 92" (Flash Point: approx. +265°C), 250 ml


25-091025-091125-0912

Keyboard - german layout, 86 keys, USB/PS2-connection - english layout, 86 keys, USB/PS2-connection - french layout, 86 keys, USB/PS2-connection

25-028225-0283

Impact Printer (mono) for single sheets & continuous paper (instead of a PC)Power supply: 220-240 V, 50/60 HzPower supply: 100-130 V, 50/60 Hz

25-090225-0903

Laser Printer (Mono), duplex, for single sheet, USB (For details see: General Equipment)Power supply : 220-240 V, 50/60 HzPower supply : 110-115 V

25-0930Receipt Impact Printer (POS) (mono) for continuous paper Power supply: 120/230 V

Spare Parts12-0778 Electric Igniter

with connector cable and plugs

12-0952 Gas Igniter with thermocouple for monitoring the igniter flame

12-5740 Drip Pan, 20 ml, aluminum, pack of 10, to place under Pt-100 & skimmer

12-5750 Cup - CL, heat resistant handle <250°C, approx. 70 ml with fi lling mark, brass

12-5751 Temperature Probe Pt-100 (Glass) - CLA 5for sample temperature measurement

12-5753 Flame Detection Unit - CLA 5 for the detection of flash- & fire-points

12-5755 Flame Arrest Cover - CLA 5to extinguish the fire in the cup

12-5758 Tool Set - CLA 5Consisting of: 3 Allen keys


43

12-0710

12-0629

12-5750

12-2730 with 12-2735

12-0962


Flash- & Fire-Point - Cleveland Open Cup Method - CL 5 (semi-automatic)

Cleveland Method:Binder & Petroleum Products:

Superpave® AASHTO T48 - ASTM D 92

Petroleum Products (except fuel oil)

ASTM D 92 - JIS K2265-4 AASHTO T48 - FTM 791-1103IP 36 (BS 4689)ISO 2592 (EN 22 592, DIN 51 376, NF T60-118)

Scope of ApplicationUsed to defi ne the hazards of fl ammable and combustible materials used in shipping and safety regulations.

Suitable for viscous materials having a fl ash-point between +79°C (175°F) and +400°C (752°F).

Summary of MethodThe temperature of the approximately 70 ml test specimen is increased rapidly at fi rst and then at a slower constant rate as the fl ash-point is approached. At specifi ed intervals a test fl ame is passed across the cup until the sample infl ames.Used to measure the tendency of the test specimen to form a fl ammable mixture with air.

The fl ash-point is the lowest liquid temperature at which the application of an ignition source causes the specimen vapors to ignite.

To determine the fi re-point, the test is continued until the application of the ignition source causes the test specimen to ignite and sustain burning for a minimum of 5 s.

Main Units

12-273012-2731

CL 5 - Semi-Automatic Flash- & Fire-Point Tester, Cleveland MethodASTM D 92 - JIS K2265-4 - AASHTO T48 - FTM 791-1103 - Superpave®IP 36 (BS 4689)ISO 2592 (EN 22 592, DIN 51 376, NF T60-118)Consisting of: high-grade stainless steel housing with two-color powder coated, motor-driven arm with gas ignition device & control valve, electric heating, infi nitely variable electronic heater control, automatic overheat protection, re-cooling fan, thermometer holderSupplied with: 1 cup with handle1 thermometer ASTM 11C/IP 28C (precision made)Technical Data: Temperature range : approx. +79 to +400 °C (+175 to +752 °F)Ignition : gas Dimensions : 23 x 47 x 46 cm (W x D x H)Weight : 9 kgPower supply : 230 V, 50/60 HzPower supply : 115 V, 50/60 Hz

Options & Accessories12-2735 Draft Defl ector - CL (recommended for gas ignition tests)

12-2737 Flame Arrest Cover - CL

12-0629 Pre-Regulating Valve for gas supply with hose adapter, suitable for all types of burning gases

12-0970 Cup - CL-NIRO with handle, approx. 70 ml (with fi lling mark), standard size, stainless steelNote! Flash-point results of stainless steel test inserts may deviate from standard results.

12-0962 Cup - CL-DRAIN with handle and drainage, approx. 70 ml, made of brass


50-9111 Reference Liquid - ASTM D 92 (approx. +250 °C), 250 ml

Thermometer

Precision Made


TypeRange

ASTM IP12-0751 12-0752 11C 28C -6 to + 400 : 2°C

12-0753 12-0754 11F 28F +20 to + 760 : 5°F

Spare Parts12-5750 Cup - CL, heat resistant handle <250°C,

approx. 70 ml with fi lling mark, brass12-2734 Ignition Device with control valve

44

(12-1770)

PMA 4 F (12-1767) with Fire-Extinguishing Device(Test-Insert included)

Flash-Point (closed cup)Flash-Point (closed cup)

Scope of ApplicationUsed in shipping & safety regulations to defi ne fl ammable and combustible materials.

Suitable for liquids with a viscosity above 5.5 cSt at +40°C.

Summary of MethodThe fl ash-point determination of petroleum products is using:Method A:for distillate fuels (diesel, kerosene, heating oil, turbine fuels), new lubricating oils, paints, vanishes and other homogeneous liquids.

Method B:for residual fuel oils, cutback residual, used lubricating oils, non-homogeneous materials like mixtures of petroleum liquids & solids, surface-fi lm building petroleum liquids or liquids with a viscosity above 5.5 cSt at +40°C.

Method C:for biodiesel (FAME, B100). Electronic fl ash point detection required.

A brass test cup is fi lled to the inside mark with test specimen, fi tted with a cover and heated, while the specimen is stirred at specifi ed rates. An ignition source is directed into the test cup at regular intervals with simultaneous interruption of the stirring, until a fl ash is detected.

Flash-Point - Pensky-Martens Method - PMA 4 (automatic)

Bitumen & bituminous binders:

ASTM D 93 - IP 34-B - ISO 2719 AASHTO T73 - AASHTO T172 FTM 791-1102 - FTM 141-4293

PMA - Single Place Units

12-177012-1771

PMA 4 - Automatic Flash-Point Tester, Pensky-Martens MethodPensky-Martens Method: ASTM D 93-A&B - JIS K2265-3 FTM 791-1102 - FTM 141-4293 AASHTO T73-A&B - AASHTO T172-A&B IP 34-A&B (BS 2839) ISO 2719-A&B (EN 22719, DIN 51 758, NF M07-019) Biodiesel Method: ASTM D 93-C - ASTM D 6751 Limit Test (eatable oils &fats): ISO 15267 - BS 684-1.17

Features: - swivel-around multi-function-head - ONE TWIST- automatic barometric pressure correction- electric & gas igniter (with auto-relighting and safety shut-off)- suitable for Standard-tests (70 ml) & Milli-tests (2 - 15 ml)- PC-software

Consisting of:stainless steel housing with two-color powder coating, touch-key panel with large LC-display (visible in up to 10 m distance), swivel-mounted multi-function-head - ONE-TWIST, two RS232-interfaces for data printer and computer connection, different test-programs, data-transfer and software upgrading through bi-directional interface, automatic barometric pressure correction, automatic overheat protection, power controlled/monitored electric igniter, gas igniter with auto-relighting and safety shut-off, re-cooling fan.

PC-Software - FPPnet (Windows® compatible): A control & analysis program for easy handling, data storage and program transfer. Providing online display of sample & heater block temperature, gradient (also in an XY-diagram) and test status. Easy to read tableau indicating: sample no., sample name, °C/°F, expected fl ash point, program, status, found fl ash point, corrected fl ash point, corrected rounded fl ash point. Test results are stored together with all program and device parameters in one fi le. The simultaneous connection of different petrotest® fl ash point devices is possible. To simplify the device management they can be named individually.

Supplied with:1 cup “PM”1 cover “PM”1 multi-detector “PM”1 gas igniter1 electric igniter1 tong for cup1 tray for cup and multi-detector1 stirrer coupling1 PC-software “FPPnet”

Technical Data: Working temperature : +40 to +360 °C (+104 to +680 °F)Stirring Speed : 60 to 250 min-1 (adjustable)Ignition : gas and electric-type (both included)Sensing System : Differential-Thermocouple MethodAir Pressure : Automatic Barometric Pressure Correction of measured valuesSafety : Overheat protection, automatic ignition fl ame, fl ame arrest coverInterface : 1 RS232 (for printer) & 1 RS232 (for downloads on PC), USB-converter availableDimensions, Weight : 230 x 470 x 460 mm (W x D x H), approx. 12 kgPower supply: 115/230 V, 50/60 Hz, EU-plug Power supply: 115/230 V, 50/60 Hz, US-plug

12-176712-1768

PMA 4 F - Automatic Flash-Point Tester, Pensky-Martens Methodwith Fire-Extinguishing Device

Consisting of:like Standard Unit (12-1770), but with automatic fi re-suppression system for connection to an external Nitrogen- or Carbon Dioxide supply.Power supply: 115/230 V, 50/60 Hz, EU-plug Power supply: 115/230 V, 50/60 Hz, US-plug

Programs:5 ASTM-Programs4 ISO-Programs 2 Rapid-Heating-Programs2 Search-Programs 2 Customized-Programs, (user defi ned)

45

12-1509 with multi-detector

Chilled PMA 4 Sample Changer (12-2776) (Test Inserts & Cooler not included)

PMA 4 Sample Changer (12-2772)(Test Inserts not included)

PMA - 12-Place Units (with 12-place carrousel)

Automatic Flash-Point Tester, Pensky-Martens Method with Sample Changer(for Standards see Single-Place Unit)Features: - for up to 12 samples- suitable for Standard “PM” (72 ml) & Milli-test inserts “pPM” (< 15 ml)- PMA 4 with “Sample Changer”- fi rmwareConsisting of:PMA 4 in a high-grade stainless steel housing with two-color powder coating, touch-key panel and large LC-display, swivel-mounted multi-function-head - ONE-TWIST, two RS232-interfaces for data printer and computer connection, different test-programs, data-transfer and software upgrading through bi-directional interface, automatic barometric pressure correction, automatic overheat protection, power controlled/monitored electric igniter, gas igniter with auto-relighting and safety shut-off, re-cooling fan. (Optional with automatic fi re-suppression system)Sample Changer with 12-place carrousel, transfer arm with housing and positioning devices. (Optional with insulating cover and coolant circulator with insulated tubing.)PC-Software “FPPnet” (Windows® compatible): A control & analysis program for easy handling, data storage and program transfer. Providing online display of sample & heater block temperature, gradient (also in an XY-diagram) and test status. Easy to read tableau indicating: sample no., sample name, °C/°F, expected fl ash point, program, status, found fl ash point, corrected fl ash point, corrected rounded fl ash point. Test results are stored together with all program- and device parameters in one fi le. The simultaneous connection of different petrotest® fl ash point devices is possible. To simplify the device management they can be named individually.With the sample changer the software is able to use the result of the previous test as the estimated fl ashpoint for the next test automatically (important for unknown samples). With the included “Quick Run” option, the re-cooling time is optimized in relation to the next consecutive sample. Rationalization of up to 50% becomes possible. The full compliance with standards is ensured.Supplied with: 1 gas igniter, 1 electric igniter, 1 tong for cup, 1 stirrer coupling, 1 PC-software “FPPnet” (incl. “QuickRun”)To be ordered separately: cups, covers & multi-detectors (e.g. 12-0777 & 12-0787)Temperature Range: +40 to +360 °C (+104 to +680 °F)

12-277012-2771

PMA 4 S - with Sample ChangerPower supply: 115/230 V, 50/60 Hz, EU-plugPower supply: 115/230 V, 50/60 Hz, US-plug

12-277212-2773

PMA 4 FS - with Fire-Extinguishing Device & Sample ChangerPower supply: 115/230 V, 50/60 Hz, EU-plugPower supply: 115/230 V, 50/60 Hz, US-plug

12-277612-2777

PMA 4 SC - with Chilled Sample ChangerPower supply: 115/230 V, 50/60 Hz, EU-plugPower supply: 115/230 V, 50/60 Hz, US-plug

12-277812-2779

PMA 4 FSC - with Fire-Extinguishing Device & Chilled Sample ChangerPower supply: 115/230 V, 50/60 Hz, EU-plugPower supply: 115/230 V, 50/60 Hz, US-plug

Options & Accessories12-0782 Calibration Set - PMA/PM

Consisting of: 1 calibration cover, 1 thermometer ASTM 9C/IP 15C, 1 thermometer ASTM 10C/IP 16C

12-1760 Calibration-Device for Pt-100 in multi-detector

12-0793 Handle for permanent fi xing at the cup

12-1508 Draft Guard (recommended for gas ignition tests)

12-1509 Stand to hold 12 multi-detectors

12-0600 Tray for cup and multi-detectorNote: An option for all PMA 4 units built before 05/2004, since than allready included.



25-0804Computer with fl at screen monitor (detailed specifi cations upon request)Power supply: 230 V, 50 Hz

25-028225-0283


12-3788 PC-Software - FPPnet (Windows®): Instruments with ABACon & ABApro, TAGCon & TAGpro, PMANet software and the CLA4 can be up-dated. (Details upon request)


For more details see our catalogs:

Pensky-Martens Flash-Point TesterFlash-Point & Auto-Ignition Tester

46

12-0777

12-1790

12-1777

12-1763 & PMA accessories

25-0240


Test InsertsStandard Brass Test Equipment:12-0777 Standard Test Insert - PM (incl. in PMA4)

Consisting of: 1 cover and 1 cup (standard dimensions, made of brass)

12-0785 Standard Cup - PM, approx. 75 ml (with fi lling mark), made of brass

12-0786 Standard Cover - PM with shutter assembly, made of brass

12-0787 Standard Multi-Detector - PM with fl ash-point detector (thermocouple) and temperature probe, made of glass

Stainless Steel Test Equipment:12-1790 Test Insert - NIRO

Consisting of: 1 cover and 1 cup (standard dimensions, made of stainless steel)

12-1791 Cup - NIRO, approx. 75 ml (with fi lling mark), made of stainless steel

12-1792 Cover - NIRO with shutter assembly, made of stainless steel

12-0784 Multi-Detector - NIRO with fl ash-point detector (thermocouple) and temperature probe, made of stainless steel

Milli Test Equipment (for small sample amounts):

12-1777 Milli Test Insert - pPM Consisting of: 1 cover and 1 cup (sample quantity 2 to 15 ml, ideal 7 ml), made of brass

12-1785 Milli Cup - pPM, approx. 15 ml, made of brass12-1786 Milli Cover - pPM with shutter assembly, made of brass

12-1787 Milli Multi-Detector - pPM with fl ash-point detector (thermocouple) and temperature probe, made of stainless steel

Note! Flash-point results of NIRO & pPM test inserts may deviate from standard results.

Circulator (external & internal heating & cooling) Consisting of:Cooler with stainless steel bath, thermostat with digital display, splash-proof keypad, heater, pump, RS232-interface, over/under-temperature & low-level protection, adjustable pump-pressure, cooling control.Supplied with: 1 bath cover, 1 drain tapNote: Insulated hose-set (25-0228) is recommended.Technical Data: Working range : -28 to +200°CDisplay / Resolution : LED / 0.01 or 0.1 °CControl : --Heater capacity (115 V) : 2000 W (1000 W)Cooling capacity : 260 W at +20 °CPump-Pressure : 11-16 l/min, 450 mbarPump-Suction : --

Bath opening (WxDxH) : 12 x 14 x 14 cm Safety class : 3Bath fl uid (possible) : FL (Flammable Liquids)Volume : 4.5 lInterface (capability) : --Sockets for : hose (Ø 8 /10 mm)

25-024025-0241

Dimensions / Weight : 23 x 42 x 61 cm (W x D x H), 31 kgPower supply : 230 V, 50 Hz, EU-plugPower supply : 115 V, 60 Hz, US-plug

Reference Liquids Flash- & Fire-PointPart-No Standard Test Name Material Flash-Point approx. Size50-9110 * ASTM D 93 Pensky-Martens Gas Oil + 65 °C 255 ml50-9111 ASTM D 92 Cleveland Lubricant + 250 °C 250 ml50-9112 ASTM D 93 Pensky-Martens Lubricant + 198 °C 250 ml50-9113 * ASTM D 93 Pensky-Martens Diesel +74.5 °C 250 ml50-9114 * ASTM D 56 TAG + 47 °C 255 ml50-9024 * ASTM D 93, IP 34 Flash-Point Gas Oil approx. 56 to 80 °C 500 ml

* Note: These liquids require special shipment as hazadous goods, due to their low fl ash-point



12-0779 Gas Igniter with 20 cm hose

12-0781 Gas Supply Tubing, 1 meter

12-0788 Safety Detector to control gas igniter and external infl ammation

12-0790 Tong for safe hot test cup handling

12-0791 Stopper, brass (Ø 18 mm), to close the covers multi-detector opening

12-078012-1507

Stirrer Couplings, pack of 10for units built until 12/2001for units built since 1/2002

The pPM - CupThis is a special test insert with a volume of approx. 15 ml for cases, where a small sample volume is available only (Milli-Test-Insert).

Although this cup does not comply with the offi cial standards, experiments have shown that in many cases and even with a sample volume of only 2 ml, good reproducibility and test results can be achieved which agree well with those measuring strictly according to the standards.

The pPM-cup extends the application of the PMA 4 to a domain where only small sample quantities are available, e.g. cosmetics industry with very expensive perfume oils.

47

12-1669

12-0777

12-1650


Flash-Point - Pensky-Martens Method - PM 4 (semi-automatic)

Bitumen & bituminous binders:

ASTM D 93 - IP 34-B - ISO 2719AASHTO T73 - AASHTO T172FTM 791-1102 - FTM 141-4293

Main Unit

12-165012-1651

PM 4 - Semi-Automatic Flash-Point Tester, Pensky-Martens MethodFeatures: - easy to manipulate- automatic overheat protection- gas and electric igniterConsisting of: stainless steel housing with two-color powder coating, swivel-mounted head, automatic overheatprotection, electric heating, electronic heater control, electric stirrer 120 rpm (method A) and250 rpm (method B) and automatic stirrer shut-off during dipping of igniter, re-cooling fanSupplied with:1 cup “PM”, 1 cover “PM”, 1 handle for cup, 1 gas igniter, 1 electric igniter, 1 stirrer coupling, 1 thermometer ASTM 9C/IP 15C, 1 thermometer ASTM 10C/IP 16CNote: Stopper (12-0791) for thermometer opening is required.Technical Data: Working temperature : approx. +40 to +360 °C (+104 to +680 °F)Stirring Speed : 120 and 250 rpmIgnition : gas and electric-type (both included) Safety : overheat protection Interface : 1 RS232 (for printer) & 1 RS232 (for downloads on PC)Dimensions, Weight : 230 x 470 x 460 mm (W x D x H), approx. 10 kgPower supply : 230 V, 50/60 Hz, 850 WPower supply : 115 V, 50/60 Hz

Options & Accessories12-1669 Digital-Thermometer alternative for glass-thermometer.

Hold-key stops the display for easy storing of the fl ash-point, while the normal display runs further. Measuring Range: up to +400°C

12-1750 Digital Precision Barometer, 0 to 1300 mbar : 1 mbar12-1751 Case for barometer12-1752 Certifi cate for barometer - 5 measuring points12-1753 Certifi cate for barometer - 10 measuring points12-1754 Battery, 9V-Block, for barometer

12-0600 Tray for cup

12-0790 Tong for handling hot handleless test cups

12-1508 Draft Defl ector (recommended for gas ignition tests)


Test Insert12-0777 Standard Test Insert - PM (incl. in PM4)

Consisting of: 1 cup and 1 cover (standard dimensions, made of brass)

12-0785 Standard Cup - PM, approx. 75 ml, made of brass12-0786 Standard Cover - PM for standard cup with shutter assembly, made of brass12-0791 Stopper, brass (Ø 18 mm), to close the thermometer opening of the cover before use

ThermometerPrecision

MadeOffi cially Certifi ed

TypeRangeASTM IP

12-0657 12-0658 9C 15C -5 to + 110 : 0.5°C12-0659 12-0660 9F 15F +20 to + 230 : 1°F12-0661 12-0662 10C 16C +90 to + 370 : 2°C12-0663 12-0664 10F 16F +200 to + 700 : 5°F12-0665 12-0666 88C - +10 to + 200 : 1°C12-0667 12-0668 88F - +50 to + 392 : 2°F

Spare Parts12-0793 Handle for permanent fi xing at the cup

12-1507 Stirrer Couplings for units built since 1/2002, pack of 10

12-0778 Electric Igniter with connector cable and plugs


12-0781 Gas Supply Tubing, 1 meter

Scope of ApplicationUsed in shipping & safety regulations to defi ne fl ammable and combustible materials.

Summary of MethodA brass test cup of specifi ed dimensions, fi lled to the inside mark with test specimen and fi tted with a cover of specifi ed dimensions is heated, while the specimen is stirred at specifi ed rates. An ignition source is directed into the test cup at regular intervals with simultaneous interruption of the stirring, until a fl ash is detected.

48

12-0501


Flash-Point - ABA Method - ABA 4 (automatic)

Abel Method:IP 170 (BS 3442-2) - ISO 13 736 (NF M07-011) Equilibrium Method (Flashpoint):ISO 1523 - IP 492 (IP 304-1) - EN 924 Equilibrium Method (Flash/no Flash):ISO 1516 - IP 491 (IP 304-2)

Abel-Pensky Method:DIN 51 755-1 - NF M07-036 (DIN 53 213)Rapid Equilibrium-Simulation (Flashpoint):ISO 3679 (BS 6664-4, EN 456, NF T60-616)Rapid Equilibrium-Simulation (Flash/no Flash):ISO 3680 (BS 6664-3, DIN 55 680, NF T60-617)

Main Units

12-050112-0502

ABA 4 - Automatic Flash-Point Tester, Abel Method (air cooled)Abel Method: IP 170 - ISO 13 736 Equilibrium Method: ISO 1523 - IP 492 - EN 924(fl ash / no fl ash) ISO 1516 - IP 491with further accessories for:Abel-Pensky Method: DIN 51 755-1 - NF M07-036Rapid Equilibrium-Simulation: ISO 3679 - ISO 3680

Features: - swivel-around multi-function-head - ONE TWIST- automatic barometric pressure correction- equilibrium-simulation mode- rapid heating mode- 2 user defi nable test programs- Peltier element system- integrated fl ame sensor- PC-software

Consisting of:stainless steel housing with two-color powder coating, touch-key panel with large LC-display (visible in up to 10 m distance), swivel-mounted multi-function-head - ONE-TWIST, stirrer drive, two RS232-interfaces for data printer and computer connection, different test-programs, data-transfer and software upgrading through bi-directional interface, Peltier element system, automatic barometric pressure correction, automatic overheat protection, power controlled/monitored electric igniter, gas igniter with auto-relighting and safety shut-off.

PC-Software “FPPnet” (Windows® compatible): A control & analysis program for easy handling, data storage and program transfer. Providing online display of sample & heater block temperature, gradient (also in an XY-diagram) and test status. Easy to read tableau indicating: sample no., sample name, °C/°F, expected fl ash point, program, status, found fl ash point, corrected fl ash point, corrected rounded fl ash point. Test results are stored together with all program and device parameters in one fi le. The simultaneous connection of different petrotest® fl ash point devices is possible. To simplify the device management they can be named individually.

Supplied with:1 cup “ABA”1 cover “ABA”1 multi-detector “ABA”1 gas igniter1 electric igniter1 stopper1 tong for cup1 tray for cup and multi-detector1 stirrer coupling1 PC-software “FPPnet”

Technical Data: Working temperature : +10 to +110°C (air cooled) / -30 to +110°C (liquid cooled)Stirring speed : 0 and 100 rpm (adjustable)Ignition : gas and electric-type (both included)Sensing System : Differential-Thermocouple MethodAir Pressure : Automatic Barometric Pressure Correction of measured valuesSafety : Overheat protection, automatic ignition fl ame, automatic shut-offInterface : 1 RS232 (for printer) & 1 RS232 (for downloads on PC), USB-converter availableDimensions, Weight : 230 x 470 x 460 mm (W x D x H), approx. 8 kgGas supply : Propane/butane or natural gas, preset to max. 0.05 barPower supply : 115/230 V, 50/60 Hz, EU-Plug Power supply : 115/230 V, 50/60 Hz, US-Plug

Programs: (acc. to international standards)2x ISO-Standards 2x Rapid-Heating 2x Search Run 2x Equilibrium2x Rapid-Test Simulation 2x User Defi ned (preset to Abel-Pensky Method)

Scope of ApplicationThe Abel-Method describes the determination of the closed-cup fl ash-point of petroleum products and other liquids having fl ash-points between -30°C and +70°C.Further it may be used for fl ash point determination of petroleum products, black oils, bitumens, fl uxed bitumens, fl uidized and cut-back asphalts.

The Equilibrium-Method describes the determination of the closed-cup fl ash/no fl ash temperature of paints, varnishes, paint binders, solvents, adhesives, petroleum & related products between -30°C and +110°C.

The Abel-Pensky-Method describes the determination of the closed-cup fl ash-point of petroleum products and other combustible liquids having fl ash-points between -30 °C and +65 °C.

Summary of MethodFor the FLASH / NO FLASH determination ignition source is applied to a tempered sample to observe whether or not a fl ash occurs. Used to detect the ability to yield fl ammable vapors.

The FLASH-POINT is the lowest temperature at which the application of an ignition source causes the specimen vapors to ignite.

49

12-1508

12-1763

25-0382

12-0518

12-050312-0504

ABA 4 - Automatic Flash-Point Tester, Abel Method (liquid cooled)Abel Method: IP 170 - ISO 13 736 Equilibrium Method: ISO 1523 - IP 492 - EN 924(fl ash / no fl ash) ISO 1516 - IP 491with further accessories for:Abel-Pensky Method: DIN 51 755-1 - NF M07-036Rapid Equilibrium-Simulation: ISO 3679 - ISO 3680

Consisting of:see Standard Unit (12-0501), but with cooler connections for external liquid cooling.

Software (Windows®): see Standard Unit (12-0501)

Supplied with: see Standard Unit (12-0501)

Note: Circulation cooler (e.g. 25-0382) is required.

Technical Data: Working temperature : -30 to +110 °C (-22 to +230 °F)(if externally cooled)

Power supply : 230 V, 50/60 Hz, EU-plugPower supply : 115 V, 60 Hz, US-plug

Tempering Accessories

25-038225-0383

Circulation Cooler (for external cooling)Necessary for counter-cooling the Peltier element system (to let the TAG 4 reach a test-temperature of approx. -30 °C (at +20°C ambient temperature)).Supplied with: 1 insulated hose-set (Ø 8 mm, 2x 2 m)Note: For details see : General Equipment Dimensions / Weight : 23 x 36 x 38 cm (W x D x H), 23 kgPower supply : 230 V, 50/60 Hz, 3.5 A, EU-plugPower supply : 115 V, 60 Hz

25-0228 Insulating Hose Set for circulation coolerConsisting of: 2x 2 m hoses (Ø 8 mm), 4 hose clamps

12-0518 Insulating Hood as ice protection to protect the cover and shutter assembly from icing.Recommended for low temperature fl ash-point tests, made of Styrofoam®.

Options & Accessories12-0520 Calibration Set - ABA

Consisting of:1 calibration cover, 1 thermometer IP 74C, 1 thermometer IP 2C

12-1760 Calibration-Device for Pt-100 in multi-detector

50-9023 Reference Liquid (Kerosene) with certifi cate, 500 mlrange: approx. +35 °C to +60 °CNote: Requires special shipment as hazardous goods

12-1508 Draft Defl ector (recommended for gas ignition tests)

12-1509 Stand to hold 12 multi-detectors

12-0600 Tray for cup and multi-detectorNote: An option for all ABA 4 units built before 05/2004, since than allready included.



25-028225-0283


12-3788 PC-Software - FPPnet (Windows®): Instruments with ABACon & ABApro, TAGCon & TAGpro, PMANet software and the CLA4 can be up-dated. (Details upon request)


50

12-0600

12-0510(12-0512 & 12-0511 & 12-0513)

12-1512 & 12-0511 & 12-0513

12-1514(12-1516 & 12-1515 & 12-0577)

12-0514


Test InsertsStandard Test Equipment12-0510 Standard Test Insert - ABA (incl. in ABA 4)

Consisting of: 1 cup and 1 cover

12-0511 Standard Cup - ABA, 79 ml

12-0512 Standard Cover “ABA”, with shutter assembly

12-0513 Standard Multi-Detector - ABA, with fl ash-point detector (thermocouple) and temperature probe

12-1512 Cover - Abel-Pensky for older AP standards with shutter assembly for standard cup “ABA“ (without stirrer)

Rapidfl ash Simulation Test Equipment12-1514 Rapidfl ash Simulation Set

Consisting of: 1 rapidfl ash cup, 1 rapidfl ash cover, 1 stopper, 1 syringe and 1 multi-detector

12-1515 Rapidfl ash Cup12-1516 Rapidfl ash Cover, with shutter assembly

12-0577 Multi-Detector - pAB/pTA, for rapidfl ash-tests

12-1518 Syringe for sample introduction, 10 mlNote: Flash-point results of rapidfl ash simulation may deviate from standard results.

Milli Test Equipment (for small sample amounts), composed of:12-0575 Milli Cup - pAB, for sample quantity between 2 ... 15 ml, ideal 7 ml

12-0574 Milli Cover - pAB, with shutter assembly

12-0577 Multi-Detector - pAB/pTA for milli-tests, mit fl ash-point detector & temperature probeNote! Flash-point results of milli test inserts may deviate from standard results.

Reference Liquids Flash- & Fire-PointPart-No Standard Test Name Material Flash-Point approx. Size50-9110 * ASTM D 93 Pensky-Martens Gas Oil + 65 °C 255 ml50-9111 ASTM D 92 Cleveland Lubricant + 250 °C 250 ml50-9112 ASTM D 93 Pensky-Martens Lubricant + 198 °C 250 ml50-9113 * ASTM D 93 Pensky-Martens Diesel +74.5 °C 250 ml50-9114 * ASTM D 56 TAG + 47 °C 255 ml50-9024 * ASTM D 93, IP 34 Flash-Point Gas Oil approx. +56 to +80 °C 500 ml

* Note: These liquids require special shipment as hazadous goods, due to their low fl ash-point





12-1507 Stirrer Couplings, pack of 10


12-0790 Tong for safe hot test cup handling

12-0791 Stopper, brass (Ø 18 mm), to close the covers multi-detector opening before use

12-0600 Tray for cup and multi-detector,

51

12-2270 & 12-2279

not using a cooler

25-0248

with overfl ow protection if a cooler is connected


Flash-Point - ABEL Method - AB 5 (semi-automatic)

Abel Method:IP 170 (BS 3442-2) - ISO 13 736 (NF M07-011)

Main Unit12-2270 AB5 -Semi-Automatic Flash-Point Tester, ABEL Method

Abel Method : IP 170 - ISO 13 736Consisting of: stainless steel housing with spray painting surface, water bath with electric heater and cooling coil for elegant pre-cooling by external circulation cooler, funnel for cooling without circulation cooler, electric stirrer on pivotable head,energy regulator, multi-gas ignition, adustable feet.

Supplied with: 1 cup ABA, 1 cover AB with gas-igniter, 1 multi-gas igniter, 1 test cup tong, 1 thermometer IP 74C (for cup), 1 thermometer IP 75C (for bath)

Note: Circulation cooler (e.g. 25-0248) might be necessary.

Technical Data: Temperature range : -18 to +71 °C (-0.4 to +160 °F)Cooling : liquid cooled (external)Ignition : gas Safety : overheat protection, automatic shut-offStirrer : 30 ±5 rpmDimensions : 23 x 47 x 38 cm (W x D x H), weight: 9 kgPower supply : 230 V, 50/60 Hz

Options & Accessories12-2279 Overfl ow Protection (recommended when cooler connected)

12-2282 Insulating Hood - AB 5 to protect the cover and shutter assembly from icing. Recommended for low temperature fl ash-point tests, made of Styrofoam®

25-0248 Circulation Cooler (for external cooling)Necessary for counter-cooling the Peltier element system (to let the AB 5 reach a test-temperature of approx. -18 °C (at +20°C ambient temperature)).Required: 1 insulated hose-set (Ø 8 & 12 mm)Note: For details see : General Equipment 25-0382Dimensions / Weight : 23 x 36 x 38 cm (W x D x H), 23 kgPower supply : 230 V, 50/60 Hz, 3.5 A, EU-plug

25-0234 Insulating Hose Set for circulation coolerConsisting of: hose 1x 2 m each (Ø 8 & 12 mm), 4 hose clamps

12-1755 Digital Precision Barometer, 300 to 1100 mbar : 2 mbar

12-1751 Case for barometer

12-1752 Certifi cate for barometer with: 5 measuring points12-1753 Certifi cate for barometer with: 10 measuring points12-1754 Battery 9-V-Block, for barometer

50-9023 Reference Liquid (Kerosene) with certifi cate, 500 ml, range: approx. +35 °C to +60 °CNote: Requires special shipment as hazardous goods

Thermometer

Precision Made


TypeRange

ASTM IP

90-0306 90-1306 74C -35 to + 70 : 0.5 °C (for cup)

90-0247 90-1247 74F -35 to +160 : 1 °F (for cup)

90-0248 90-1248 75C -30 to + 80 : 0.5 °C (for bath)

90-0307 90-1307 75F -25 to +180 : 1 °F (for bath)

Spare Parts90-0306 Thermometer IP74C90-0248 Thermometer IP75C

12-0511 Cup - ABA12-2277 Cover - AB with shutter assembly

12-0790 Tongs for safe test cup handling

Scope of ApplicationThe Abel-Method describes the determination of the closed-cup fl ash-point of petroleum products and other liquids having fl ash-points between -30°C and +70°C.

Further it may be used for fl ash point determination of petroleum products, black oils, bitumens, fl uxed bitumens, fl uidized and cut-back asphalts.

52

Filtration Unit

Distillation Unit

17-0710

17-0802

Paraffi n ContentParaffi n Content

Scope of ApplicationA procedure for determination the paraffi n wax content of bitumen and bituminous binder.

Paraffi n Wax Content - Distillation Method - (manual)

Cut-Back Bitumen:EN 12606-1 (DIN 52 015) - IP 459-1

Main Unit

10-016010-0161

Paraffi n Wax Content ApparatusEN 12 606-1 (DIN 52 015) - IP 459-1

Consisting of:Distillation Unit: 1 distillation fl ask (100 ml) with stopper and protecting ring,

1 Erlenmeyer fl ask (100 ml) with bored rubber stopper, 1 glass vessel (Ø 140 x 75 mm)support stand, universal gas burner and adjustable table

Filtration Unit: 1 cooling bath (for direct cooling) with sockets for tempering unit, 1 suction fl ask (500 ml) with bored stopper, 1 water jet pump with U-tube vacuum meter and 2 meters tubing, 3 test tubes with spout, bored stopper, 3 special test tubes (NS 29/32) with splash bulb attachment, 1 bath thermometer (-30 ... +50:0.5 °C), 1 sample thermometer (-38 ... +50:1 °C), 1 congealing point thermometer (0 ... +100 °C) with sleeve stand

Note: Cooling bath requires counter-cooling.Power supply: 230 V, 50/60 Hz, EU-plugPower supply: 115 V, 50/60 Hz


17-071017-0711

Circulator (external & internal heating & cooling) programmable & regulated by Main-UnitFor counter-cooling the fi ltration cooling bath.Consisting of: Cooler with stainless steel bath. Thermostat with digital display, splash-proof keypad, heater, pump, RS232-interface, Pt-100-socket, programmer, over/under-temperature & low-level protection, adjustable pump-pressure, cooling control.Supplied with: 1 bath cover, 1 drain tap, 1 insulated hose-set (Ø 8 mm, 2x 2m)Note: For details see: General EquipmentDimensions / Weight: 31 x 42 x 66 cm (W x D x H), 38 kgPower Supply: 230 V, 50 Hz, EU-plugPower Supply: 230 V, 60 Hz

17-080217-0804

Circulation Air Oven14 l capacity, thermostatically-controlled between +60 and +200 °C, temperature constancy of +/- 2-3 K, includes time switch, thermometer for temperature inspection and perforated intermediate bottom.Dimensions (W x H x D): outside 31 x 38.5 x 47 cm / inside 19 x 20 x 36 cmWeight: 17 kg.Power supply: 230 V, 50/60 HzPower supply: 115 V, 50/60 Hz

25-047025-0471

Vacuum-Pump with Mini-Compressor (oil-free diaphragm pump with fi lter)Max. capacity: 6 l/minEnd vacuum: 100 mbarOperating pressure: 2.4 bar (overpressure)Dimensions / Weight: 9 x 17 x 12 cm (W x D x H), 1.9 kgPower supply: 220/230 V, 50 Hz, EU-plugPower supply: 110/115 V, 60 Hz

ThermometerPrecision

MadeStopper

(NBR-rubber) Type Range

16-0264 11-0030 DIN 12 775 -30 to -50 : 0.5°C (for bath)16-0313 10-0236 DIN 12 785 -38 to +50 : 1 °C (for sample)17-0010 — ISO 2207 0 to +100 : 0.5°C (congealing point)

Spare Parts10-0013 Water Jet Pump, Hanff, glass

10-0136 Vacuum Flask, 500 ml10-0239 Stopper for vacuum fl ask

10-0144 Distillation Flask (EN 12606-1), 100 ml10-0145 Protecting Ring for distillation fl ask10-0234 Stopper for distillation fl ask

10-0166 Receiver, Erlenmeyer Flask, 100 ml10-0235 Stopper for Receiver Erlenmeyer fl ask

10-0167 Test Tube with spout (EN 12606-1)

10-0168 Reagent Tube (standard taper NS 29/32)

10-0169 Splash Head (standard taper NS 29/32)

10-0170 U-Tube-Manometer 500-0-500 mm Acrylic tube on metal plate for wall mounting. Suitable for measuring pressures to 98 mbar with water or 1.33 bar with mercury fi lling. Note! Mercury is not included

10-0171 Round Filter Ø 110 mm, pack of 100

11-0110 Universal Gas Burner for butane, propane, town & natural gases

13-0923 Hose, 1 m (5x 1.5 mm, Silicon)

16-0925 Test Cup (DIN 12 338), 700 ml, glass

53

Dean & StarkASTM D 95 / ISO 3733

ASTM D 244

Water ContentWater Content

Water Content - Distillation Method - (manual)

Petroleum Products & Bituminous Materials (Dean & Stark App.)ASTM D 95 - JIS K2275 - AASHTO T55 - IP 74 (BS 4385)- ISO 3733 (DIN 51 582, DIN 1995)

DIN 1996-5

Emulsifi ed AsphaltsASTM D 244 - AASHTO T59 - IP 291 (BS 434)

EN 1428 (DIN 52 048, DIN 1995)

Main Unit

16-083016-1430

Water Content Determination Apparatus for Petroleum Products and Bituminous Materials (Dean & Stark)ASTM D 95 - JIS K2275 - AASHTO T55 - IP 74 Consisting of:- 1 fl ask (500 ml), standard taper (NS 29) - 1 glass trap (10 ml), standard taper (NS 29) - 1 refl ux condenser (400 mm), standard taper (NS 29)

Supplied with: - 1 electric heater (800 W), stainless steel housing - 1 heating board (center hole Ø 70 mm) - support rod (600 mm) with 4 adjustable clampsPower supply: 230 V, 50 Hz, EU-plugPower supply: 115 V, 60 Hz

16-183916-1452

Supplied with: - 1 heating mantle (565 W) & support ring for 500 ml fl ask - 1 electronic energy regulator (2000 W) - support rod (600 mm) with 4 adjustable clamps and base platePower supply: 230 V, 50 Hz, EU-plugPower supply: 115 V, 60 Hz

16-085016-1450

Water Content Determination Apparatus for Petroleum Products and Bituminous Materials (Extended Dean & Stark)ISO 3733 (DIN 51 582, DIN 1995) but also for: ASTM D 95 - JIS K2275 - AASHTO T55 - IP 74 - EN 1428Consisting of:- 3 fl asks (250, 500 and 1000 ml), standard taper (NS 29)- 3 glass traps (6, 10 and 25 ml), standard taper (NS 29)- 1 refl ux condenser (400 mm), standard taper (NS 29)

Supplied with: - 1 electric heater (800 W), stainless steel housing- 3 heating boards (center hole Ø 50, 70 and 89 mm) - support rod (600 mm) with 4 adjustable clampsPower supply: 230 V, 50 Hz, EU-plugPower supply: 115 V, 60 Hz

16-185016-1458

Supplied with: - 1 heating mantle (345 W) & support ring for 250 ml fl ask - 1 heating mantle (565 W) & support ring for 500 ml fl ask - 1 heating mantle (875 W) & support ring for 1000 ml fl ask - 1 electronic energy regulator (2000 W) - support rod (600 mm) with 4 adjustable clamps and base platePower supply: 230 V, 50 Hz, EU-plugPower supply: 115 V, 60 Hz

16-084416-1444

Water Content Determination Apparatus for Emulsifi ed AsphaltsASTM D 244 - AASHTO T59 - IP 291 - EN 1428 Consisting of:- 1 fl ask (500 ml), standard taper (NS 29)- 1 glass trap (25 ml), standard taper (NS 29)- 1 refl ux condenser (400 mm), standard taper (NS 29)

Supplied with: - 1 electric heater (800 W), stainless steel housing - 1 heating board (center hole Ø 70 mm) - support rod (600 mm) with 4 adjustable clampsPower supply: 230 V, 50 Hz, EU-plugPower supply: 115 V, 60 Hz

16-184416-1454


Scope of ApplicationFor the determination of water in petroleum products, tars, and other bituminous materials by the distillation method.

The test arrangement consists of a set of glassware and a suitable heater.As far as the standard taper joints fi t together, many other individual combinations are possible, dependent upon customer’s requirements.

Summary of MethodBituminous Material Methods: The material to be tested is heated under refl ux with a water-immiscible solvent, which co-distills with the water in the sample. Condensed solvent and water are continuously separated in a trap, the water settling in the graduated section of the trap and the solvent returning to the still.

Emulsifi ed Asphalts Methods: They are determining the water content of an emulsifi ed asphalt by refl ux distillation, using a water trap to measure the amount of water present in the emulsifi ed asphalt, as distinguished from either bitumen or petroleum solvent.

54

DIN 1996-5

Water ContentWater Content

16-084516-1445

Water Content Determination Apparatus for Bituminous MaterialsDIN 1996-5Consisting of:- 1 fl ask (500 ml), standard taper (NS 45) - 1 adapter, standard taper (NS 45 to NS 29) - 1 glass trap (10 ml), standard taper (NS 29) - 1 refl ux condenser (400 mm), standard taper (NS 29)

Supplied with: - 1 electric heater (800 W), stainless steel housing - 1 heating board (center hole Ø 70 mm) - support rod (600 mm) with 4 adjustable clamps Power supply: 230 V, 50 Hz, EU-plugPower supply: 115 V, 60 Hz

16-184516-1455


Glassware (Options & Accessories & Spares)

16-087816-0879

Liebig Refl ux Condenser NS 29 with special drip tip for easy counting of drops... 250 mm... 400 mm

16-0898 Drying Tube for ASTM D 4006

FlasksVolume Erlenmeyer fl ask

DIN 12 387with standard taper

Round fl ask DIN 12 348 with standard taper

Round fl ask DIN 12 394 with standard taper and side neck

[ml] NS 29/32 NS 45/40 NS 29/32 NS 45/40 NS 29/32 NS 45/40

250 16-0859 16-0862 16-0865 16-0869 16-0873 500 16-0860 16-0863 16-0866 16-0870 16-08741000 16-0861 16-0864 16-0867 16-0871 16-08752000*) 16-0868 16-0872 16-0876 16-0877

Adapter(NS 29 to 40) 16-0897 16-0897 16-0897

Sleves (PTFE) with

Gripping Ring(0.4 mm) multiple use

50-7027 50-7030 50-7027 50-7030 50-7027 50-7030

Rips(0.07 mm) pack of 10

50-7047 50-7050 50-7047 50-7050 50-7047 50-7050

The comfortable gripping ring type is not recommended in combination with taper clips.

TrapsOrder No. Size [ml] Measuring Tube End 0-Point16-0880 2 : 0.05 round at bottom

16-0901 5 : 0.05 round at bottom

16-0881 * 6 : 0.05 conical at tip

16-0882 * 6 : 0.05 with cock at cock

16-0883 * 6 : 0.05 round above bottom

16-0884 * 6 : 0.05 with cock above cock

16-0886 10 : 0.1 conical at tip

16-0887 10 : 0.1 round above bottom

16-0888 10 : 0.1 with cock above cock

16-0889 10 : 0.1 with cock at cock

16-0890 25 : 0.1 conical at tip

16-0891 25 : 0.1 round above bottom

16-0892 25 : 0.1 with cock above cock

16-0902 25 : 0.1 with cock at cock

* Can be used when 5 : 0.1 ml types are recommended.

*) Recommended for electrical heating of a 2000 ml fl ask:

• heating mantle (16-0825), • stand (16-0824), • electronic energy regulator (25-0001)

The sleeves are recommended for assembling the glassware. They prevent a sticking together and on the other hand assure tightness.

55

17-0802

25-0001 / 25-0108

Heating Mantle

Water Content Water Content

CylindersVolume [ml] Graduated cylinder (DIN 12 680) Mixing cylinder (DIN 12 685)

50 16-0899 100 11-0130 250 16-0820 17-0584 500 16-0705 16-07421000 26-0014 16-0675

Sample Thermometer DIN 12 784 with collar NS 14/23, Range 0 ... +250 : 1 °C

Precision Made insertation depth for fl ask with side neck

16-0893 120 mm 16-0873

16-0894 150 mm 16-0874

16-0895 160 mm 16-0875

16-0896 195 mm 16-0876 / 16-0877

Heating Mantles

Flask Size 250 ml

Flask Size 500 ml

Flask Size 1000 ml

Flask Size 2000 ml

Electronic Energy

Regulator

Power supply 230 V, 50 Hz 25-0706 25-0700 25-0702 16-0825 25-0001

115 V, 60 Hz 25-0707 25-0701 25-0703 16-0829 25-0108

Support Ring 25-0708 25-0704 25-0705 incl.

Support Stand(base plate, 750 mm rod, 2 adjustable clamps Ø 40 mm, 3 boss heads)

16-0824 16-0824 16-0824 16-0824

Heating Devices

11-013811-013911-0140

Heater Board, 150 x 150 x 4 mm ceramic, with a ... 50 mm Ø center hole... 70 mm Ø center hole... 89 mm Ø center hole

16-0898 Gas Heating Device Consisting of:universal gas burner, ring holder, wire net and support stand (base plate, 750 mm rod, 2 adjustable clamps Ø 40 mm, 3 boss heads)

17-080217-0804

Circulation Air Oven14 l capacity, thermostatically-controlled between +60 and +200 °C, temperature constancy of +/- 2-3 K, includes time switch, thermometer for temperature inspection and perforated intermediate bottom.Dimensions (W x H x D): outside 31 x 38.5 x 47 cm / inside 19 x 20 x 36 cmWeight: 17 kg.Power supply: 230 V, 50/60 HzPower supply: 115 V, 50/60 Hz

Spare Parts for Electric Heater11-0018 Heater Rod, 200 W, 115-230 V

11-001911-0029

Heater Plate, (with 4 heater rods)... 230 V, 50/60 Hz, 800 W... 115 V, 50/60 Hz, 800 W

25-000425-0009

Heater Module "m2" for sensitive regulation of heating energyPower supply: 230 V, 50/60 HzPower supply: 115 V, 50/60 Hz

56

DistillationDistillation

Scope of ApplicationThis procedure measures the amount of the more volatile constituents in cut-back asphaltic products. Suitable for the distillation of cut-back asphaltic (bituminous) products.

Summary of Method200 ml of a sample are distilled in a 500 ml fl ask at a controlled rate to a sample temperature of +360 °C (680°F) and the volumes of distillate obtained at a specifi c temperature are measured.

Distillation Analysis - Cut-Back Bitumen ASTM-Method (manual)

Cut-Back (Fluxed) Bitumen:ASTM D 402 - AASHTO T 79 - IP 27 (BS 4453) - EN 13358 (NF T66-003)

Main Unit10-0213 Distillation Apparatus - Cut-Back Bitumen (ASTM-type)

ASTM D 402 - AASHTO T 79 - IP 27 (BS 4453) - EN 13358 (NF T66-003)Consisting of:1 thermometer ASTM 8C (precision made) with holder (bored stopper)1 distillation fl ask (500 ml) 1 fl ask shield with two-part ceramic cover 1 ring support with wire gauze 2 support rods with clamps and base plates1 adjustable universal gas burner1 condenser tube (400 mm) with special jacket 1 cylindrical graduated receiver (100 : 1 ml) and connection material (adapter etc)

Thermometer

Precision Made


TypeRange Holder

(Stopper)ASTM IP

11-0155 11-0156 8C 6C -2 to +400 : 1 °C 10-0210

Spare Parts11-0130 Cylindrical Graduated Receiver

(100 ml : 1 ml division)

11-0503 Graduated Receiver (100 ml : 1 ml division, BS 658) with conical lower part (0 ... 10 ml) and base

10-0220 Adapter10-0217 Condenser Tube (400 mm)

10-0218 Condenser Jacket10-0204 Stopper for condenser tube,

DIN 12 871, NS 24/30, Ø 12 mm

10-0214 Connecting Tube, Silicon, 1 m (Ø 10 x 2 mm)

10-0210 Stopper, NBR, to hold thermometer, NS 29/30, bored Ø 6.5 mm

11-0155 Distillation Thermometer ASTM 8C/ IP 6C

10-0216 Distillation Flask (500 ml, Ø 102 mm) short-necked

10-0205 Flask Shield, stainless-steel with ceramic insulation and windows

10-0208 Insulating Cover, ceramic, 2-part

10-0178 Ring Support with wire gauze

11-0110 Universal Gas Burner for butane, propane, town & natural gas

57

Distillation Distillation

Distillation Analysis - Cut-Back Bitumen DIN-Method (manual)

Cut-Back (Fluxed) Bitumen:DIN 52 024

Main Unit10-0173 Distillation Apparatus - Cut-Back Bitumen (DIN-type)

DIN 52 024Consisting of:1 distillation thermometer (precision made)1 distillation fl ask (500 ml) 1 fl ask shield of stainless steel with windows and ceramic insulation1 two-part ceramic cover1 ring support 2 support rods with 3 boss heads, 1 clamp and 2 base plates1 Universal gas burner 1 glass condenser tube (360 mm)6 Erlenmeyer fl ask (100 ml) 1 base for 100 ml fl askand connection material (2 silicon stoppers (bored Ø 4 & 10 mm))

Thermometer

Precision Made


TypeRange Holder

(Stopper)DIN

10-0154 10-0155 12 779 0 to +360 : 1 °C 10-1298

Spare Parts10-0166 Erlenmeyer Flask (100 ml)

10-0175 Distillation Flask (500 ml)

10-0176 Condenser Tube (360 mm), glass

10-129810-1297

Stopper, silicon NS 27/30, bored... Ø 4 mm for thermometer... Ø 10 mm for side-neck

10-0177 Flask Shield, stainless-steel with ceramic insulation and windows


10-1178 Ring Support 11-0110 Universal Gas Burner for butane,

propane, town & natural gas

Scope of ApplicationThis procedure measures the amount of the volatile constituents and the residue in in cut-back asphaltic products. Suitable for the distillation of cut-back asphaltic (bituminous) products.

Summary of MethodA 200 g sample is distilled at a controlled rate up to +360 °C (680°F) into tared receivers.

The masses of distillate fractions and of the residue are determined at a specifi ed temperature.

58


Scope of ApplicationDistillation devices according to these standards are used for determination of boiling characteristics, asphalt residue, total distillate and fractions of bituminous materials, tar products and creosote at specifi ed distillation temperatures.

Suitable for the distillation of bituminous material, tar products and creosote.

Summary of MethodA 100 g sample is distilled at a controlled rate from a 300 ml fl ask into tared receivers.

The masses of distillate fractions at a series of specifi ed temperatures and of residue at the maximum specifi ed temperature are determined.

Distillation Analysis - Road Tar ASTM-Method (manual)

Road Tars:ASTM D 20 (ASTM D 246)

Main Unit10-0203 Distillation Apparatus - Road Tar Products (ASTM-type)

ASTM D 20 (ASTM D 246)Consisting of:1 distillation fl ask (diameter 86 mm) 1 thermometer ASTM 8C (precision made) 1 stopper to hold thermometer1 fl ask shield and two-part ceramic cover1 ring support with wire gauze 2 support rods with clamps and base plate1 adjustable universal gas burner1 condenser tube (360 mm) 6 receivers, and connection material (adapter etc.)

Thermometer

Precision Made


TypeRange

Holder(Stopper)ASTM IP

11-0155 11-0156 8C 6C -2 to +400 : 1 °C 17-0047

Spare Parts10-0166 Receiver Erlenmeyer Flask (100 ml)

10-0220 Adapter10-0207 Condenser Tube (360 mm long)

17-0047 Stopper, NBR, to hold thermometer, NS 29/30, bored Ø 6 mm


10-0206 Distillation Flask (Ø 86 mm) short necked

10-0205 Flask Shield, stainless-steel with ceramic insulation and 2 windows


10-0178 Ring Support with wire gauze

11-0110 Universal Gas Burner for butane, propane, town & natural gas

59

Distillation Distillation

Distillation Analysis - Road Tar DIN-Method (manual)

Road TarsDIN 52 027

Main Unit10-0152 Distillation Apparatus - Road Tar Products (DIN-type)

DIN 52 027Consisting of:1 heater housing of stainless-steel 1 universal gas burner 1 fractionation fl ask (500 ml) 1 thermometer (precision made) 1 Liebig condenser tube 400 1 condenser tube (600 mm) 6 receivers 1 support rod with 1 boss head, 1 clamp and 1 base plate and connection material (2 silicon stoppers (bored Ø 4 & 12 mm))



Thermometer

Precision Made


TypeRange Holder

(Stopper)DIN

10-0154 10-0155 12 779 0 to +360 : 1 °C 10-0298

Spare Parts10-0166 Erlenmeyer Flask (100 ml)

10-0153 Fractionating Flask (500 ml)

10-0156 Condenser Tube (600 mm, Ø 22 mm)

10-0157 Liebig Condenser Tube “400”(for cold tars to +170 °C)

10-029810-1297

Stopper, silicon, pack of 20, bored... Ø 4 mm, NS 30/32, for thermometer... Ø 12 mm, NS 22/25, for side-neck

10-0159 Heater Housing, stainless-steel, with holding ring and wire gauze


10-0158 Universal Gas Burner, special shape

Scope of ApplicationThis procedure measures the amount of the more volatile constituents in fl uxed bitumen. Suitable for the distillation of fl uxed bitumen (Road & Coal Tar).

Summary of Methodapprox. 250 g of a sample are distilled at temperature up to +350 °C. The reciver will be changed at +170°C, +270°C and +300°C.

60

Distillation Analysis - Pitch-Method (manual)

ASTM D 2569

Main Unit10-0179 Distillation Apparatus - Pitch

ASTM D 2569Consisting of:electric heater 800 W with high-capacity low-mass heater elements for precise energy input control, triac controller, heater carrier infi nitely adjustable in heightSupplied with:1 fl ask shield1 heater board1 ceramic insulation cover1 distillation fl ask Ø 86 mm1 thermometer ASTM 8C (-2 to +400 °C)2 stoppers1 condenser tube6 Erlenmeyer fl ask2 support rods2 clamps2 base plate2 boss head1 lifting tablePower supply: 230 V, 50/60 Hz

Thermometer

Precision Made


TypeRange

Holder(Stopper)ASTM IP

11-0155 11-0156 8C 6C -2 to +400 : 1 °C 17-004711-0157 11-0158 8F +30 to +760 : 2 °C

Spare Parts10-0166 Receiver Erlenmeyer Flask (100 ml)

10-0207 Condenser Tube (360 mm long)

17-0047 Stopper, NBR, to hold thermometer, NS 29/30, bored Ø 6 mm


10-1297 Stopper, silicon, pack of 20, boredØ 12 mm, NS 22/25, for side-neck

10-0206 Distillation Flask (Ø 86 mm) short necked

10-0205 Flask Shield, stainless-steel with ceramic insulation and 2 windows


11-0119 Support Board center hole Ø 80 mm glass ceramic (150 x 150 x 4 mm)

50-5242 Lifting Table (Details: Gen. Equipment)

Scope of ApplicationThis test method is used to identify the quality of pitch to avoid problems of fuming or instability in use.

Suitable for hard and soft pitch.

Summary of MethodA 100 g sample is distilled at a designated rate.

The weight of the destillate fractions at specifi ed temperatures and the time required to collect the main fraction are recorded.

The amount of distillate below +270 °C should be less than 2.0 %.


61

HubbardGay-Lussac

Lipkin

DensityDensity

Density, Relative Density - Pycnometer Method (manual)

Capillary-Stoppered Hubbard Pycnometer:ISO 3838 (DIS 3658) - JIS K2249ASTM D 70 - IP 190 (BS 4699) DIN 52 004 (DIN 1995)Capillary-Stoppered Gay-Lussac Pycnometer:ISO 3838 (DIS 3658) - JIS K2249IP 190 (BS 4699)

Graduated Bicapillary Lipkin Pycnometer:ISO 3838 (DIS 3658) - JIS K2249ASTM D 1481 - IP 189 (BS 4699)

Pycnometer26-0712 Lipkin-Pycnometer, 5 ml

Bitumen: ASTM D 1481 - IP 189 (BS 4699) ISO 3838 - JIS K2265 Suitable for very small sample amounts with a kinematic viscosity <50 cSt (mm²/s) at test temperature.

26-0721 Gay-Lussac-Pycnometer, 25 mlBitumen: ISO 3838 - JIS K2265 - IP 190 (BS 4699)Suitable for non-volatile liquids

26-0740 Hubbard Pycnometer, 24 mlBitumen : ASTM D 70 - ISO 3838 - JIS K2265

26-0741 Hubbard-Pycnometer, 25 mlBitumen : ASTM D 70 - IP 190 (BS 4699) ISO 3838 - JIS K2265 - DIN 52 004Suitable for solids or high viscous liquids.

Options & Accessories26-0790 Holder (for Lipkin-Pycnometer)

26-0791 Holder (for Gay-Lussac-Pycnometer)

26-0793 Clamp (for Gay-Lussac-holder 26-0791), polyethylene coated

26-0792 Holder (for Hubbard-Pycnometers 26-0740 and -0741)

26-0794 Clamp (for Hubbard-holder 26-0792)

Scope of ApplicationFor the determination of the density and relative density of petroleum products like liquid, semi-solid or solid bituminous materials, asphalt cements, and soft tar pitches by use of a pycnometer.

Capillary-StopperedGay-Lussac Pycnometer: suitable for non-volatile liquids.Hubbard Pycnometer: suitable for high viscous liquids or solids.Graduated BicapillaryLipkin Pycnometer: suitable for very small sample amounts with a kinematic viscosity <50 cSt (mm²/s) at test temperature.

Summary of MethodGraduated Bicapillary PycnometerThe liquids sample is drawn into the graduated pycnometer arms, and after it has reached equilibrium at the test temperature, the liquid levels are noted and the pycnometer weighed.

Capillary-Stoppered PycnometerThe mass of equal volumes of a sample and of water are compared. Equal volumes are ensured by the pycnometer beeing fi lled so as to overfl ow when placed in a bath at the test temperature until equilibrium is reached.

62

26-0010 / 26-0011

Hydrometer (example)

DensityDensity

Density, Relative Density - Hydrometer Method (manual)

Liquid Bitumen:ASTM D 3142

HydrometerASTM D 3142

Precision Made Hydrometer-Type Series Range : Div. Overall

LengthRef.

Temp.

26-0500

API Gravity(ASTM E 100)

1H-62 -1 to +11 : 0.1 °API

max. 330 mm

60 °F26-0501 2H-62 +9 to +21 : 0.1 °API

26-0502 3H-62 +19 to +31 : 0.1 °API

25-0503 4H-62 +29 to +41 : 0.1 °API

26-0603

ASTM Specifi c Gravity(ASTM E 100)

85H-62 0.800 to 0.850 : 0.0005 sp gr

max. 330 mm

60/60°F

26-0604 86H-62 0.850 to 0.900 : 0.0005 sp gr

26-0605 87H-62 0.900 to 0.950 : 0.0005 sp gr

26-0606 88H-62 0.950 to 1.000 : 0.0005 sp gr

26-0607 89H-62 1.000 to 1.050 : 0.0005 sp gr

26-0608 90H-62 1.050 to 1.100 : 0.0005 sp gr

Note: °F-type not available with certifi cate. Suitable hydrometer cylinder (26-0014)

Scope of ApplicationThe Hydrometer Method is suitable for determining the density of cutback asphalts which are liquid at room temperature by using a glass hydrometer.

For materials that are solid or semi-solid at room temperature, use Hubbard Pycnometer Method ASTM D 70

Summary of MethodThe sample is brought to the testing temperature and transferred to a cylinder at approximately the same temperature.The cylinder and its contents are placed in a constant temperature bath to avoid excessive temperature variation during the test. The appropriate hydrometer is lowered into the sample and allowed to settle.After temperature equilibrium, the hydrometer is read and the temperature of the sample is noted.The hydrometer reading is converted to the density at +15°C using standard tables.

Pycnometer & Hydrometer Tempering Equipment

26-001026-0011

Tempering Bath for determinations up to +60°C by pycnometer, hydrometer or viscometer.

Consisting of:Acrylic glass bath (foot print 280 x 430 mm, depth of the bath 300 mm) with cooling-coil.Thermostat with digital display, splash-proof keypad, heater, pump and over-temperature protection.

Supplied with:1 pycnometer bath cover with 4 openings (Ø 50.5 mm)1 hydrometer bath insert with clamps, 4 openings (Ø 55 mm) and 4 cylinders (Ø 54 x 300 mm)5 lids (20-0024) for the unused openings1 bath-thermometer, -2 to +105 :0.5 °C (incl. stopper)

Note: Bath is suitable for hydrometer with an overall length of maximal 275 mm or viscometers. Measurements at temperatures lower than +25 °C require a counter-cooling device, (e.g. Recirculating Cooler 25-0368 or 25-0373)

Technical Data: Testplaces : 4Working range : approx. +25 to +60 °C (without counter-cooling)Display / Resolution : LED / 0.1°CControl : PIDHeater capacity : 2000 W (115 V = 1000 W)Pump-Pressure capacity : 15 l/min, 340 mbarBath opening : 26 x 26 x 30 cm (W x D x H)Safety class / Bath fl uid : 1 / NFL (water / water-antifreeze-mix only)Volume : 30 lSockets for : hose (Ø 8 / 10 mm)Dimensions : 28 x 43 x 50 cm (W x D x H) Power supply : 230 V, 50 Hz, EU-plugPower supply : 115 V, 50/60 Hz

63

26-0017 / 26-0018

25-0368 / 25-0373

DensityDensity

26-001726-0018

Tempering Bath for determinations up to +150°C by pycnometer, hydrometer or viscometer

Consisting of:borosilicate glass bath jar with cooling-coil.Thermostat with digital display, splash-proof keypad, integrated heater, pump, RS232-interface, over-temperature- & low-level-protection

Supplied with:1 bath insert (heat protected stainless steel) with 4 openings (Ø 67 mm) and clamps4 pycnometer adapter rings (inside Ø 50.5 mm)4 hydrometer cylinders (Ø 65 x 420 mm)5 lids (20-0024) for the unused openings1 leakage protection vessel complete with temperature insulation

Note: Bath is suitable for hydrometer with an overall length of maximal 400 mm or viscometers. Measurements at temperatures lower than +25 °C require a counter-cooling device, (e.g. Recirculating Cooler 25-0368 or 25-0373)

Technical Data: Testplaces : 4Working range : approx. +25 to +150 °C (without counter-cooling)Display / Resolution : LED / 0.01°CControl : PIDHeater capacity : 2000 W (115 V = 1000 W)Pump-Pressure capacity : 15 l/min, 320 mbarSafety class / Bath fl uid : 3 / FL (Flammable Liquids possible)Volume : 20 lInterface : RS232Sockets for : hose (Ø 8 mm)Dimensions / Weight : 35 x 37 x 60 cm (W x D x H), 20 kg Power supply : 230 V, 50/60 Hz, EU-plugPower supply : 115 V, 50/60 Hz

25-036825-0373

Circulation Cooler (tap water replacement, external cooling) with insulated hoseFor counter-cooling the tempering baths.Consisting of:Cooler with tank, digital display, splash-proof keypad, integrated pump, liquid level indication, over-/low-temperature & low-level protection.Supplied with: 1 insulated hose-set (Ø 8 mm, 2x 2 m, incl. fi ttings)Note: For details see: General EquipmentDimensions / Weight : 32 x 50 x 60 cm (W x D x H), 48 kgPower supply : 230 V, 50 Hz, EU-plugPower supply : 115 V, 60 Hz

Bath-ThermometerPrecision

MadeOffi cially Certifi ed

TypeRangeASTM IP

13-0715 13-0716 12C 64C -20 to +102 : 0.2 °C13-0717 13-0718 12F 64F -5 to +215 : 0:5 °F21-0601 21-0607 17C +19 to +27 : 0.1 °C21-0621 21-0627 17F +66 to +80 : 0.2 °F21-0606 21-0612 22C 24C +95 to +103 : 0.1 °C21-0626 21-0632 22F +204 to +218 : 0.2 °F10-0385 10-0386 63C -8 to +32 : 0.1 °C10-0387 10-0388 63F +18 to +89 : 0.2 °F26-0036 26-0037 39C -1 to +38 : 0.1 °C26-0038 26-0039 39F +30 to +100 : 0.2 °C

DIN11-0022 bath 0 to +105 : 0.5°C10-0383 10-0384 12 775 0 to +50 : 0.1°C

Spare PartsBath up to +60°C

11-0030 Stopper, NBR-rubber, to hold bath thermometer (18/20 / bored Ø 7.5 mm)

11-0022 Bath Thermometer (0 to +105 : 0.5°C)

26-0004 Hydrometer Cylinder (Ø 54 mm x 300 mm)

Bath up to +150°C13-0565 Thermometer Protection Tube26-0026 Adaptor Ring, inside Ø 50.5 mm

for pycnometer holders

26-0014 Measuring Cylinder, borosilicate glass, 1000 : 10 ml with plastic stand asHydrometer Cylinder (Ø 65 x 420 mm)

64

25-0282

25-0418 & 25-0420

Scope of ApplicationThe Displacement Method for the determination of the density or relative density of hard pitches and asphalts with softening points above +70°C.

The Balance Method is suitable for determining quickly and accurately the density or relative density of petroleum products, such as gasoline, kerosene and gas oil, particularly when the quantities available for test are small.

Summary of MethodDisplacement Method:The sample is suspended from a thin wire and weighed, fi rst in air, then submerged in water at +25.0 °C. The relative density is calculated from these weights.

Balance Method:To determine the density at test temperature, a balance is measuring the buoyancy of a bob suspended from a thin wire and immersed in a liquid sample at ambient temperature.

Density, Relative Density - Displacement / Balance Method (semi-automatic)

Displacement Method:ASTM D 71 (IP 59-B)

Balance Method:DIN 51 757-2 (IP 59-A)

Main Unit

26-001926-0020

Digital Density Test Rig

Bitumen: ASTM D 71 (IP 59-B) Fuel/Oil: DIN 51 757-2 (IP 59-A)

Consisting of:1 digital balance with electronic computation module to convert measured boyance to density1 stand with platform for balance1 lift for test cylinderSupplied with: 1 test cylinder (120 ml)1 thermometer (+10 to +30:0.1 °C)1 underfl oor hook1 bob (10 ml)1 test weight, 100 g (for balance control)

Technical Data: Density measuring range : 0.0 to 2.1 g/qcm Resolution : 0.0001 g/qcm Balance weighing range : max. 320 g : 0.001 g Weighing plate : 135 x 135 mm, stainless steelInterface : RS232Dimensions / Weight : 35 x 37 x 60 cm (W x D x H), 20 kgPower supply : 110/230 V, 50/60 Hz, EU-plugPower supply : 115 V, 60 Hz, US-plug


25-028225-0283


Spare Parts25-0417 Thermometer for density-applications

(Range: +10 to +30 : 0.1 °C)25-0418 Test Cylinder, 120 ml

25-0420 Bob, 10 ml

DensityDensity

65

19-0041 19-0032

19-0039

19-0080

19-0051 / 19-0052

19-0056 / 19-0057

19-0011

19-0005

Scope of ApplicationSolid MaterialsThe boring sampling procedure is applicable for waxes, solid bitumens and other soft solids in barrels, cases, bags, and cakes when they cannot be melted and sampled as liquids.

Semi-Solid MaterialsThe grease sampling procedure is applicable for lubricating greases, soft waxes or soft bitumens similar to grease in consistency from kettles, drums, cans, tubes.

Liquid MaterialsThe tube sampling procedure is applicable for sampling liquids of 13.8 kPa (2 psia) RVP or less and semi-liquids in drums, barrels, and cans.The bottle sampling procedure may be used for sampling liquids of 101 kPa (14.7 psia) RVP or less in tank cars and storage tanks.The core thief sampling procedure is applicable for emulsifi ed asphalts and other semi-liquids in tank cars and storage tanks.

Sampling Devices (manual)

Bituminous binders, Sealants & Fillers:ASTM D 140 EN 58 - DIN 52001 (DIN 1996-2)

Petroleum Products: ASTM D 4057 - (AASHTO T 79)

Solid Materials

19-005119-0052

Sampling Auger with handle ASTM D 4057 - DIN 51 750-3 (ASTM D 270, DIN 53 242-3)to take samples of non-liquid materials from any specifi ed level, brass construction... effective length 30.5 cm... effective length 50.0 cm

Semi-Solid Materials

19-005619-0057

Grease Sampling Tube with handleASTM D 4057 - EN 58 - DIN 51 750-3 (ASTM D 270)to take samples from any specifi ed level of hard greases and waxes, brass... effective length 500 mm... effective length 1000 mm

Liquid Materials19-0005 Open-End Sampling Tube

EN 58 - DIN 51 750-2 - ISO 3170 brass, 102 cm long To take individual samples from smaller containers such as barrels, drums etc.

19-0011 Closed-End Sampling TubeEN 58 - DIN 51 750-2alloy steel, 300 cm long To take samples from any specifi ed level of larger containers such as barrels, drums etc.

19-0041 Sampling Bottle with metal cage, 1 lASTM D 4057 - EN 58 - DIN 51 750-2 - ISO 3170 (ASTM D 270) Sample bottle: glass, neck 29/32, height 200 mm, outside Ø 111 mmTo take samples from any specifi ed container level, except the bottom.

19-0032 Tank Sampling Thief (BACON-bomb) ASTM D 4057 - ASTM D 923 - DIN 51 750-2 - ISO 3170 - JIS C 2101 - JIS K2254 (ASTM D 270, DIN 53 242-1) for mineral oils and mineral oil products, insulating oils, special gasolines and solvent naphthas, light gas oils, fuel oils etc. Brass construction, nickel plated with automatically opening bottom valve, outer Ø 80 mm. Capacity approx. 1 liter. Without lowering chain and pull cord.To take samples from the bottom or any specifi ed container level.

19-0039 Valve Pull Cord, Perlon, 100 m

19-0080 Hand-Wheel with 30 m steel wire (Ø 1 mm) and snaphook Note! Only for non fl ammable samples, because the steel-rope may cause sparks.

SamplingSampling

66

Viscosity & Density

MTVM

MTVM - Calibration Fluid (Multi- and Single-Test Verifi cation Material)

50-9037 MTVM - Reference Liquid (Bitumen) with certifi cate (ISO 9001), 250 ml

Test Name Method Range Units Amount / Test

Softening Point IP 58 +36.8 to +44 °C 7.5 ml

Needle Penetration IP 49 +184 to +200 °C 130 ml

Viscosity & Density Oil StandardsSuitable for calibration of master viscometers and viscosity oil standards as described in ASTM D 445 & D 446.Certifi ed by UKAS under ISO 17 025 at all stated temperatures.The values listed in the following table are to be considered as nominal and approximate only (depending on the batch). The actual and exact data will be printed on the container-lable or on a separate certifi cate.Content: 500 ml Shelf life: 2 years

UKAScertifi ed Type

Kinematic Viscosity [mm²/s = cSt] Dynamic Viscosity [mPa•s = cP]

Density [g/ml]

Saybolt Viscosity

SUS SUS SFS

approx. 20°C68°F

25°C77°F

37.8°C100°F

40°C104°F

50°C122°F

60°C140°F

80°C176°F

98.9°C210°F

100°C212°F

37.8°C100°F

98.9°C210°F

100°C122°F

24-0601 N 0.4mm²/smPa•sg/ml

0.47240.31510.6670

0.45250.29980.6625

0.40750.26520.6507

0.40030.25970.6487


0.72750.51620.7096

0.69000.48680.7055

0.60750.42200.6948

0.59490.41230.6930


1.3271.024

0.7716

1.2360.91410.7679

1.0440.79160.7582

1.0160.76860.7565

0.90360.67670.7489

24-0603 S 3mm²/smPa•sg/ml

4.5263.689

0.8150

4.0023.248

0.8115

3.0222.425

0.8026

2.8902.315

0.8010

2.3991.905

0.7942

2.0291.597

0.7871

1.5191.174

0.7732

1.2050.91570.7599

1.1900.90340.7592

36.0


10.598.954

0.8455

8.9457.533

0.8421

6.1135.096

0.8336

5.7614.794

0.8322

4.5003.714

0.8254

3.6182.962

0.8188

2.5022.015

0.8053

1.8801.490

0.7927

1.8521.467

0.7920

45.9

24-0605 N 10mm²/smPa•sg/ml

20.5517.27

0.8403

16.8014.06

0.8370

10.678.841

0.8286

9.9498.229

0.8271

7.4256.094

0.8207

5.7424.675

0.8141

3.7352.992

0.8012

2.6872.120

0.7888

2.6412.081

0.7881


43.3237.16

0.8579

33.8928.97

0.8548

19.6316.62

0.8467

18.0215.23

0.8452

12.7010.65

0.8388

9.3607.792

0.8325

5.6454.627

0.8197

3.8543.112

0.8076

3.7743.046

0.8070

96.3


84.9472.59

0.8546

64.8255.17

0.8514

35.4929.93

0.8434

32.2927.19

0.8420

21.8518.26

0.8358

15.5312.88

0.8296

8.8237.208

0.8170

5.7614.639

0.8052

5.6344.533

0.8046

166.3


157.5135.6

0.8610

117.0100.4

0.8579

59.8550.87

0.8500

53.9245.75

0.8485

34.9429.43

0.8423

23.9120.00

0.8363

12.7710.52

0.8239

7.9756.477

0.8122

7.7816.314

0.8115

278.0


325.3281.6

0.8657

235.8203.4

0.8626

113.096.59

0.8548

100.785.94

0.8534

62.4752.93

0.8473

41.1134.58

0.8412

20.5617.05

0.8291

12.2410.01

0.8177

11.919.732

0.8171

524.0


637.6554.6

0.8698

450.2390.2

0.8668

204.1175.3

0.8591

180.2154.6

0.8577

107.691.65

0.8518

68.3457.80

0.8458

32.2026.85

0.8338

18.3215.07

0.8226

17.7814.61

0.8219

945.0 91.4


11891038

0.8726

822.0714.8

0.8696

355.0306.0

0.8619

311.1267.7

0.8606

179.3153.2

0.8546

110.593.79

0.8488

49.3641.31

0.8370

27.0022.30

0.8259

26.1421.57

0.8253

1645 129.0


21411875

0.8758

14561271

0.8728

601.9520.9

0.8654

523.9452.6

0.8639

293.2251.6

0.8581

175.5149.6

0.8523

74.5562.67

0.8407

39.1632.49

0.8297

37.8531.38

0.8290

182.9 138.4

24-0612 N 1 000mm²/smPa•sg/ml

43753847

0.8793

29172556

0.8764

11531002

0.8690

994.0862.5

0.8677

309.7461.9

0.8620

300265.2

0.8562

123.6104.4

0.8448

61.7251.47

0.8340

59.4949.58

0.8335

253.0

24-0613 S 2 000mm²/smPa•sg/ml

79467015

0.8828

52224595

0.8800

19831731

0.8727

17001481

0.8714

889.6770.3

0.8659

499.2429.4

0.8601

188.8160.3

0.8488

90.2575.65

0.8382

86.8072.70

0.8376

24-0614 N 4 000mm²/smPa•sg/ml

17966159570.8882

11627102960.8855

42163702

0.8780

35893147

0.8769

18111578

0.8713

981.2849.4

0.8657

345.9295.6

0.8547

155.4131.2

0.4420

149.1125.8

0.8436

24-0615 S 8 000mm²/smPa•sg/ml

35264314270.8912

22566200500.8885

79817034

0.8813

67485938

0.8800

33272910

0.8747

17601530

0.8692

588.8505.4

0.8584

252.5214.2

0.8482

241.4204.6

0.8476

24-0618 S 30 000mm²/smPa•sg/ml

79747713820.8951

27285242370.8883

22946203550.8871

109939693

0.8817

56234929

0.8765

17561521

0.8659

700.1599.3

0.8560

666.5570.0

0.8552

Reference MaterialReference Material

67

25-0930

21-0695

11-0599

18-1144

21-0697 (look can vary)

25-0282

50-5242

25-0902

A B 25-0918

Miscellaneous Equipment

21-0695 8-Channel Stop WatchContaining 8 individual stop watches.Each operated by a single button to run, stop or reset.Auto-power-off when no stop watches are running.After power-off individual values are kept in memory.All values can be reset together or per channel.9 V-Battery-block included. Expected life time approx. 6 months.The stop watch can be supplied with a calibration certifi cate.Dimensions (L x W x H): 195 x 112 x 46 mm

21-069721-0698

Digital Stop Watch7-digit LC display, max. 10 hours countdown with 1/100 sec. precisionquartz-controlled, water resistant, memory function, calendarNote: Lithium battery operated (battery lifetime 1 year)... precision made... certifi ed

18-1144 Electronic Stop Watch with electric start-inputPower supply: 100/240 V, 50/60 Hz

50-5242 Lifting Table, mechanical Base plate: 160 x 130 mm, Weight: 60 kg capacity

25-090225-0903

Laser Printer (Mono), duplex, for single sheet to record data like test results, duration of test, etc. Supplied with: 1 data transmission cable (USB A-B), 1 toner cartridge (black)Technical Data: Resolution : 1200 x 1200 dpiPaper size : A4 single sheet, 300 sheet paper tray Printing speed : 30 pages/min Ports : USB (2.0) type BDimensions :378 x 255 x 390 mm (WxDxH), weight 11.5 kgPower supply : 220-240 V, 50/60 HzPower supply : 110-115 V

25-0930

Serial Receipt Impact Printer (POS) for paper rolls with tear-off edge, paper auto loadingSupplied with: 1 data-cable (3 m) null-modem, 25-pin male /9-pin female (25-0927), 1 paper roll (25-0928)1 ink ribbon, black, for receipt-printer (25-0929),1 USB/RS232-adapter (13-1696)Technical Data: Line spacing : 24 / 40 colums, 144 / 180 dotsPaper roll size : 58 mm x Ø 60 - 80 mm Printing speed : approx. 2.5 lines/secPorts : serial (RS-232C), & parallelDimensions : 10.6 x 18 x 8.8 cm (WxDxH), weight 0.5 kgPower supply : 120/230 V, (AC converter output 7 V)

25-028225-0283

Serial Impact Printer for single sheet & continuous paper to record data like test results, duration of test, etc. Supplied with: 2 data cables (9-pin 25-0304, USB 25-0918), 1 ink ribbon (black)Technical Data: Line spacing : 80 characters per line (10 cpi)Page size (W x H) : 257 x 364 mm (sheet), 254 x 58 mm (roll)Ports : serial (9-pin), USB (1.1)Dimensions : 37 x 28 x 16 cm (WxDxH), weight 5 kgPower supply : 220/240 V, 50/60 HzPower supply : 110/130 V, 50/60 Hz

25-0274 Printer Data-Cable, serial (2 m), for manual & semi-automatc units

25-0304 Printer Data-Cable, serial (2 m), for automatic Petrotest® units

25-0284 Ink Ribbon, black, for serial impact printer

25-0918 Data-Cable, USB 2.0, type A to B (3 m)

25-0919 Memory Stick, 2 GB USB 2.0 (verifi ed for petrotest®-units) (details upon request)

11-0599 USB/RS232-Converter with 2 m cable (verifi ed for Petrotest®-units)connecting 1 serial port to the USB-port of a PC or Hub

General EquipmentGeneral Equipment

68

10-0380

17-0710

25-0240

20-0156

Tempering EquipmentCirculator (for external & internal cooling & heating) programmable (with accessories)Consisting of:Cooler with stainless steel bath, thermostat with digital display, splash-proof keypad, heater, pump, RS232/RS485-interface, Pt100-socket, programmer, over/under-temperature & low-level protection, adjustable pump-pressure, proportional cooling control.Supplied with: 1 bath cover, 1 drain tap, 1 junction line for temperature probeNote: Insulated hose matter is not included but recommended.Technical Data: Working range : -40 to +200°CDisplay / Resolution : VFD & LCD / 0.01°CControl : programmableHeater capacity (115 V) : 2000 W (1000 W)Cooling capacity : 680 W at +20 °CPump-Pressure : 22-26 l/min, 700 mbarPump-Suction : 22-26 l/min, 400 mbar

Bath opening (WxDxH) : 23 x 14 x 20 cm Safety class : 3Bath fl uid (possible) : FL (Flammable Liquids)Volume : 16 lInterface (capability) : RS232 (LIMS) / RS485Sockets for : hose (Ø 8 / 12 mm), Pt100, solenoid valve

10-038010-0381

Dimensions / Weight : 37 x 46 x 71 cm (W x D x H), 49 kgPower supply : 230 V, 50 Hz, EU-plugPower Supply : 230 V, 60 Hz

Circulator (external & internal heating & cooling) programmable & regulated by Main-UnitConsisting of: Cooler with stainless steel bath, thermostat with digital display, splash-proof keypad, heater, pump, RS232-interface, Pt100-socket, programmer, over/under-temperature & low-level protection, adjustable pump-pressure, cooling control.Supplied with: 1 bath cover, 1 drain tap, 1 insulated hose-set (Ø 8 mm, 2x 2m)Technical Data: Working range : -35 to +200°CDisplay / Resolution : VFD / 0.01°CControl : programmableHeater capacity (115 V) : 2000 W (1000 W)Cooling capacity : 450 W at +20 °CPump-Pressure : 22-26 l/min, 700 mbarPump-Suction : 22-26 l/min, 400 mbar

Bath opening (WxDxH) : 18 x 12 x 15 cm Safety class : 3Bath fl uid (possible) : FL (Flammable Liquids)Volume : 8 lInterface (capability) : RS232 (LIMS)Sockets for : hose (Ø 8 / 12 mm), Pt100, solenoid valve

17-071017-0711


Circulator (external & internal heating & cooling) Consisting of:Cooler with stainless steel bath, thermostat with digital display, splash-proof keypad, heater, pump, RS232-interface, over/under-temperature & low-level protection, adjustable pump-pressure, cooling control.Supplied with: 1 bath cover, 1 drain tapNote: Insulated hose-set (25-0228) is recommended.Technical Data: Working range : -28 to +200°CDisplay / Resolution : LED / 0.01 or 0.1 °CControl : --Heater capacity (115 V) : 2000 W (1000 W)Cooling capacity : 260 W at +20 °CPump-Pressure : 11-16 l/min, 450 mbarPump-Suction : --

Bath opening (WxDxH) : 12 x 14 x 14 cm Safety class : 3Bath fl uid (possible) : FL (Flammable Liquids)Volume : 4.5 lInterface (capability) : --Sockets for : hose (Ø 8 /10 mm), solenoid valve

25-024025-0241


Circulator (external & internal heating & cooling)Consisting of:Cooler with stainless steel bath, thermostat with digital display, splash-proof keypad, heater, pump, over-temperature & low-level protection.Supplied with: 1 bath coverNote: Insulated hose-set (25-0228) is recommended.Technical Data: Working range : -5 to +60°CDisplay / Resolution : LED / 0.1 °CControl : --Heater capacity : 1100 W Cooling capacity : 250 W at +2 °CPump-Pressure : 7 l/min, 300 mbarPump-Suction : --

Bath opening (WxDxH) : 15 x 8.5 x 15 cm Safety class : 1Bath fl uid (possible) : NFL (Non Flammable Liquids)Volume : 5 lInterface (capability) : --Sockets for : hose (Ø 8 mm)

20-015620-015720-0158

Dimensions / Weight : 27 x 46 x 57 cm (W x D x H), 30 kgPower supply : 230 V, 50 Hz, 1400 W, EU-plugPower supply : 230 V, 60 HzPower supply : 115 V, 60 Hz


VFD = Vacuum Flourescence DisplayLCD = Liquid Crystal Display

FL = Flammable LiquidsNFL = Non Flammable Liquids (e.g. water or water-antifreezemix)

6925-0228

18-0403

25-0670

25-0382

25-0368 / 25-0373

Circulation Cooler (tap water replacement, external cooling) with insulated hoseFor cooling or counter-cooling of instruments with no circulation pump (e.g. Peltier-cooling).Consisting of:Cooler with tank, digital display, splash-proof keypad, integrated pump, liquid level indication, over-/low-temperature & low-level protection.Supplied with: 1 insulated hose-set (Ø 8 mm, 2x 2 m, incl. fi ttings)Technical Data: Working range : -20 to +40 °CDisplay / Resolution : LED / 0.1°CControl : --Heater capacity (115 V) : -- (--)Cooling capacity : 600 W at +20 °CPump-Pressure : 40 l/min, 1000 mbarPump-Suction : --

Bath opening (WxDxH) : -- Safety class : 1Bath fl uid (possible) : NFL (Non Flammable Liquids)Volume : 5.5 - 8 lInterface (capability) : RS232Sockets for : hose (Ø 8 / 12 mm)

25-036825-0373

Dimensions / Weight : 32 x 50 x 60 cm (WxDxH), 48 kgPower supply : 230 V, 50 Hz, 4.6 A, EU-plugPower supply : 115 V, 60 Hz, 9.7 A

Circulation Cooler (for external cooling)Consisting of: Cooler with tank, digital display, pump and liquid level indication.Supplied with: 1 insulated hose-set (Ø 8 mm, 2x 2m)Technical Data: Working range : -20 to +40 °CDisplay / Resolution : digital / 0.1°CControl : --Heater capacity (115 V) : -- (--)Cooling capacity : 300 W at +15°CPump-Pressure : 12 l/min, 200 mbarPump-Suction : 12 l/min, 100 mbar

Bath opening (WxDxH) : -- Safety class : 1Bath fl uid (possible) : NFL (Non Flammable Liquids)Volume : 1.4 lInterface (capability) : -- Sockets for : hose (Ø 8 / 12 mm), Pt100

25-038225-0383

Dimensions / Weight : 23 x 36 x 38 cm (W x D x H), 23 kgPower supply : 230 V, 50/60 Hz, 3.5 A, EU-plugPower supply : 115 V, 60 Hz

Circulator-Bath Set (internal & external heating & cooling) with intermediate bottom & circulation coolerConsisting of: stainless steel bath with drain tap. Thermostat with digital display, splash-proof keypad, integrated heater, pump and over-temperature protection. Cooler with tank, Pt100, digital display, pump and liquid level indication.Supplied with: 1 intermediate bottom, 1 cooling-coil, 1 insulated hose-set (Ø 8 mm, 2x 2m)Technical Data: Working range : +5 to +100°CDisplay / Resolution : LED / 0.1°CHeater capacity (115 V) : 2000 W (1200 W)Bath Pump-Pressure : 15 l/min, 350 mbar Cooling capacity : 300 W at +15°CPump-Pressure : 20 l/min, 200 mbarPump-Suction : 17 l/min, 180 mbar

Bath opening : 36 x 30 x 20 cm (WxDxH)

Safety class : 1Bath fl uid : NFL (water / water-antifreezemix)Volume : 27 l (bath), 1.4 l (cooler)Interface : --Sockets for : hose (Ø 8 / 12 mm)

25-067025-0671

Dimensions / Weight : (WxDxH) 57 x 37 x 42 cm, 13 kg (bath) / 23 x 36 x 38 cm, 23 kg (cooler)Power supply : 230 V, 50 Hz, EU-plugPower supply : 115 V, 60 Hz

Circulator-Bath (for external & internal heating) with cooling-coil & intermediate bottomConsisting of: Stainless steel bath with adjustable intermediate bottom and cooling-coil, thermostat with digital display, splash-proof keypad, heater, pump, RS232-interface, over-temperature- & low-level-protection.Supplied with: 1 bath cover Ø 5 cm, 1 bath cover 20 x 20 cm, 1 thermometer (-2 to +105:0.5°C)Note: Requires counter-cooling for applications near ambient temperature.

Hose matter is not included.Technical Data: Working range : +20 to +150°CDisplay / Resolution : LED / 0.01°CControl : --Heater capacity (115 V) : 2000 W (1000 W)Cooling capacity : --Pump-Pressure : 15 l/min, 320 mbarPump-Suction : --

Bath opening (WxDxH) : 20 x 20 x 25 cmSafety class : 3Bath fl uid (possible) : FL (Flammable Liquids)Volume : 20 lInterface (capability) : RS232 (LIMS)Sockets for : hose (Ø 8 mm)

18-040318-0402

Dimensions / Weight : 37.5 x 45 x 47.5 cm (W x D x H), 3.4 kgPower supply : 230 V, 50 Hz, EU-plugPower supply : 115 V, 60 Hz




70

Tables of ContentsKeywords ....................... page 71Order Numbers ......... page 72-74Standards ...................... page 75

71

page

Abel Flash-Point ................................................................... 48-49, 51

Aging ............................................................................................ 36 - 40Accelerated Aging ...................................................................... 40Effect of Heat and Air ..................................................... 36, 38, 39Resistance to Hardening ............................................... 36, 38, 39Loss-On-Heat - LOH ................................................................... 36Rolling Thin Film Oven Test - RTFOT ....................................... 38Rotating Flask Test - RFT .......................................................... 39Moving Thin Film Test - RFT ..................................................... 39Pressure Aging Vessel - PAV .................................................... 40Thin-Film-Oven Test - TFOT ...................................................... 36

API Gravity Hydrometer .................................................................... 62

Apparent Viscosity ...................................................................... 26, 27

Asphalt Binder Analyzer ................................................. 38, 40, 41, 43

Asphalt Institute Vacuum Viscometer - AIVV ................................ 33

ASTM Specifi c Gravity Hydrometer ................................................ 62

Balance .............................................................................................. 64

Bending Beam Rheometer - BBR .................................................... 24

Bitumen Number ................................................................................ 16

Breaking-Point ............................................................................. 20, 23

Brookfi eld Viscometer - RV .............................................................. 26

BS/IP Reverse Flow Viscometer - RFV ........................................... 32

Cannon-Fenske Opaque Viscometer - CFOV ................................ 31

Cannon-Manning Vacuum Viscometer - CMVV ............................. 33

Cleveland Flash- & Fire-Point .................................................... 41, 43

Creep Stiffness .................................................................................. 24

Cut-Back Bitumen Distillation .................................................. 56, 57

Dean & Stark Distillation .................................................................. 53

Density, Relative Density Displacement / Balance ............................................................. 64Hydrometer .................................................................................. 62Pycnometer ................................................................................. 61

Distillation Cut-Back Bitumen ................................................................ 56, 57Paraffi n Wax Content ................................................................. 52Pitch ............................................................................................. 60Road Tar Products ................................................................ 58, 59Water Content ............................................................................. 53

Ductility ......................................................................................... 10, 14

Dynamic Shear Rheometer - DSR .................................................... 25

Dynamic Viscosity ............................................................................. 33

Effect of Heat & Air ........................................................................... 36

Elastic Properties ........................................................................ 10, 18

Equilibrium Method ..................................................................... 48, 49

Fire-Point (open cup) ................................................................. 41, 43

Flash-Point (closed cup) Pensky-Martens - PMA 4 ........................................................... 44Pensky-Martens - PM 4 .............................................................. 47Abel - ABA 4 .......................................................................... 48, 49Abel - AB 5 ................................................................................... 51

Flash-Point (open cup) Cleveland (COC) - CLA 5 ........................................................... 41Cleveland (COC) - CL 5 .............................................................. 43

Fraass-Method ............................................................................. 20, 23

Gay-Lussac Pycnometer ................................................................. 61

General Equipment ....................................................................... 67-69

Glass Capillary Viscosity Asphalt Institute Vacuum Viscometer - AIVV .......................... 33BS/IP Reverse Flow Viscometer - RFV .................................... 32Cannon-Manning Vacuum Viscometer - CMVV ...................... 33Cannon-Fenske Opaque Viscometer - CFOV ......................... 31U-Tube Reverse Flow Viscometer - RFV .................................. 32Zeitfuchs Cross-Arm Viscometer - ZCAV ................................ 32High Temperature Liquid Bath .................................................. 35

Gravity ................................................................................................. 62

Hubbard Pycnometer ....................................................................... 61

Hydrometer ......................................................................................... 62

Kinematic Viscosity ......................................................................... 31

Kraemer-Sarnow Softening-Point ..................................................... 9

page

Lipkin Pycnometer ............................................................................ 61

Loss-On-Heat - LOH .......................................................................... 36

Moving Thin Film - RFT .................................................................... 39

Paraffi n Wax Content ....................................................................... 52

Penetration ................................................................................... 16, 18

Penetrometer - PNR 12 ...................................................................... 16

Pensky-Martens Flash-Point ...................................................... 44, 47

Pitch Distillation ................................................................................. 60

Plastic Properties ........................................................................ 16, 18

Pressure Aging Vessel - PAV ........................................................... 40

Pycnometer ........................................................................................ 61

Reference Material ........................................................................... 66

Resistance to Hardening ...................................................... 36, 38, 39

Reverse Flow Viscometer - RFV ...................................................... 32

Rheometer Method Bending Beam - BBR ................................................................. 24Dynamic Shear - DSR ................................................................. 25Texture - PNR 21 ......................................................................... 18

Rheotex Texture Analyzer - PNR 21 ................................................ 18

Ring & Ball Softening-Point ........................................................... 4, 7

Road Tar Distillation .......................................................................... 58

Road Tar Viscometer ......................................................................... 27

Rolling Thin Film Oven Test - RTFOT .............................................. 38

Rotating Flask Test - RFT ................................................................. 39

Rotary Viscometer - RV ..................................................................... 26

Sampling Devices Closed-End Sampling Tube ...................................................... 65Grease Sampling Tube with handle ......................................... 65Open-End Sampling Tube ......................................................... 65Sampling Bottle with metal cage .............................................. 65Tank Sampling Thief (BACON) ................................................. 65

SHARP Method Bending Beam Rheometer - BBR ............................................. 24Dynamic Shear Rheometer - DSR ............................................ 25Pressure Aging Vessel - PAV .................................................... 40Rotational Viscometer - RV ....................................................... 26

Softening-Point Ring & Ball - RKA 5 ....................................................................... 4Ring & Ball ..................................................................................... 8Wilhelmi ..................................................................................... 7, 9

Stiffness .............................................................................................. 24

Superpave® ...................................................................... 38, 40, 41, 43

Tempering Devices ........................................................................... 68

Tensile Properties Ductilometer - DD 3 .................................................................... 14Force-Ductilometer - DDA 3 ...................................................... 10

Texture ......................................................................................... 18 - 19

Thin-Film-Oven Test - TFOT ............................................................. 36

U-Tube Viscometer - RFV ................................................................. 32

Vacuum Capillary Tubes .................................................................. 33

Viscoelastic Properties ..................................................................... 25

Viscosity Apparent Viscosity ............................................................... 26, 27Brookfi eld Viscometer - RV ....................................................... 26Dynamic Shear Rheometer - DSR ............................................ 25Dynamic Viscosity ...................................................................... 33Effl ux Viscometer ....................................................................... 27Engler Viscometer ...................................................................... 30Glass Capillary Viscometer ...................................................... 31Kinematic Viscosity .................................................................... 31Liquid Bath ................................................................................... 35Reference Material ...................................................................... 66Rotational Viscometer - RV ....................................................... 26Saybolt Viscometer ..................................................................... 28Specifi c Viscosity ........................................................................ 30Universal & Furol Method ........................................................... 28Vacuum Capillary Tubes ............................................................ 33Viscosity Liquid Bath ................................................................. 35

Water Content Distillation ............................................................... 53

Weight ................................................................................................. 64

Wilhelmi Softening-Point Method ..................................................... 8

Zeitfuchs Cross-Arm Viscometers - ZCAV .................................... 32

KeywordsKeywords

72

Order-NumbersOrder-Numbers

10-0000 .......................................2310-0002 ........................................2310-0003 ........................................2310-0004 ........................................2310-0006 ..................................22, 2310-0008 ........................................2310-0009 ........................................2310-0010 ........................................2310-0013 ..................................34, 5210-0016 ........................................2210-0017 ........................................2310-0048 ......................................7, 810-0049 .................................. 6, 7, 810-0051 ......................................7, 810-0052 ......................................6, 810-0055 ..........................................810-0056 ..........................................810-0057 ..........................................910-0061 ......................................8, 910-0062 ......................................8, 910-0063 ......................................8, 910-0064 ......................................8, 910-0065 ................................ 8, 9, 3910-0066 ................................ 8, 9, 3910-0067 ......................................8, 910-0068 .......................................8-910-0070 ..........................................810-0071 ..........................................910-0075 ......................................7, 910-0076 ..........................................910-0077 ..........................................910-0079 ......................................7, 810-0090 ........................................2310-0106 ..........................................910-0117 ........................................3610-0118 ........................................3610-0123 ........................................3710-0126 ...................................37-3810-0127 ...................................37-3810-0128 ........................................3710-0134 ........................................3710-0135 ........................................3710-0136 ........................................5210-0144 ........................................5210-0145 ........................................5210-0146 ..................................37, 4010-0149 ........................................3710-0150 ........................................3710-0152 ........................................5910-0153 ........................................5910-0154 ........................................5710-0154 ........................................5910-0155 ........................................5710-0155 ........................................5910-0156 ........................................5910-0157 ........................................5910-0158 ........................................5910-0159 ........................................5910-0160 ........................................5210-0161 ........................................5210-0166 .............................52, 57-6010-0167 ........................................5210-0168 ........................................5210-0169 ........................................5210-0170 ........................................5210-0171 ........................................5210-0173 ........................................5710-0175 ........................................5710-0176 ........................................5710-0177 ........................................5710-0178 ..................................56, 5810-0179 ........................................6010-0203 ........................................5810-0204 ........................................5610-0205 ............................ 56, 58, 6010-0206 ..................................58, 6010-0207 ..................................58, 6010-0208 ...................... 56, 58, 59, 6010-0210 ........................................56

10-0211 .......................................3710-0212 ........................................3710-0213 ........................................5610-0214 ........................................5610-0216 ........................................5610-0219 ........................................5610-0220 ........................................5610-0222 ........................................3710-0233 ..................................22, 2310-0234 ........................................5210-0235 ........................................5210-0236 ........................................5210-0239 ........................................5210-0242 ........................................3710-0243 ........................................3710-0244 ........................................3710-0245 ........................................3710-0281 ..........................................810-0284 ..........................................810-0285 ..........................................610-0288 ..........................................510-0295 ........................................2710-0298 ........................................5910-0312 ........................................2710-0313 ........................................2710-0317 ........................................2710-0318 ........................................2710-0319 ........................................2710-0320 ........................................2710-0322 ........................................2710-0324 ........................................2710-0329 ........................................2710-0332 ..................................13, 1510-0335 ..................................13, 1510-0337 ........................................2710-0338 ........................................2710-0350 ........................................1410-0351 ........................................1410-0354 ........................................1410-0355 ........................................1410-0360 ........................................1210-0361 ........................................1210-0364 ........................................1210-0365 ........................................1210-0377 ..................................13, 1510-0379 ..................................13, 1510-0380 ............................ 12, 15, 6810-0381 ............................ 12, 15, 6810-0383 ............................ 13, 15, 6310-0384 ............................ 13, 15, 6310-0385 ..................................15, 6310-0386 ..................................15, 6310-0387 ........................................6310-0388 ........................................6310-0403 ..................................13, 1510-0404 ........................................1210-0406 ..................................13, 1510-0455 ..........................................810-0460 ........................................2110-0461 ........................................2110-0473 ........................................2210-0474 ........................................2210-0475 ........................................2210-0480 ..........................................610-0506 ..................................22, 2310-0507 ..................................22, 2310-0600 ........................................2610-0601 ........................................2610-0602 ........................................2610-0603 ........................................2610-0604 ........................................2610-0605 ........................................2610-0619 ........................................3810-0621 ........................................3810-0625 ........................................3910-0700 ........................................2410-0701 ........................................2410-0702 ........................................2410-0706 ........................................24

10-0707 .......................................2410-0708 ........................................2410-0720 ........................................4010-0721 ........................................4010-0722 ........................................4010-0724 ........................................4010-0725 ........................................4010-0726 ........................................4010-0727 ........................................4010-0770 ........................................2510-0774 ........................................2510-0775 ........................................2510-0800 ......................................5, 910-0801 ..........................................510-0805 ......................................6, 710-0840 ......................................6, 710-0841 ..........................................610-0846 ..........................................710-0849 ..........................................710-0850 ..........................................610-0851 ..........................................610-0856 ..........................................710-0860 ......................................7, 910-0861 ..........................................710-0864 ......................................7, 910-0865 ..........................................710-0868 ..........................................510-0877 ..........................................810-0888 ..........................................710-0906 ..........................................710-1117 ........................................3610-1178 ........................................5710-1181 ..........................................510-1294 ........................................2710-1296 ........................................5710-1297 ............................ 57, 59, 6010-1298 ........................................5710-1321 ........................................2710-1323 ........................................2710-1333 ..................................13, 1510-1336 ..................................13, 1510-1337 ..................................13, 1510-1600 ........................................2610-1601 ........................................2610-1602 ........................................2610-2110 ........................................39

11-0018 ................................8-9, 5511-0019 .................................8-9, 5511-0022 ........................................6311-0029 ................................... 8, 5511-0030 ..................................52, 6311-0087 ........................................1711-0088 ........................................1711-0110 .............................52, 56-5811-0119 ........................................6011-0130 ............................ 27, 55, 5611-0138 ................................ 8, 9, 5511-0139 ....................................6, 5511-0140 ....................................6, 5511-0155 ...................... 27, 56, 58, 6011-0156 ...................... 27, 56, 58, 6011-0157 ........................................6011-0158 ........................................6011-0181 ...................... 13, 15, 19, 6911-0395 ........................................3011-0503 ........................................5611-0599 ................ 13, 22, 45, 49, 69

12-0282 .......................................4212-0283 ........................................4212-0378 ..........................................612-0501 ........................................4812-0502 ........................................4812-0503 ........................................4912-0504 ........................................4912-0509 ........................................5012-0510 ........................................5012-0511 ..................................50, 5112-0512 ........................................5012-0513 ........................................5012-0514 ........................................5012-0518 ........................................4912-0520 ........................................4912-0574 ........................................5012-0575 ........................................5012-0577 ........................................5012-0600 ...................... 45, 47, 49, 5012-0629 ........................................4312-0657 ........................................4712-0658 ........................................4712-0659 ........................................4712-0660 ........................................4712-0661 ........................................4712-0662 ........................................4712-0663 ........................................4712-0664 ........................................4712-0665 ........................................4712-0666 ........................................4712-0667 ........................................4712-0668 ........................................4712-0751 ........................................4312-0752 ........................................4312-0753 ........................................4312-0754 ........................................4312-0774 ........................................4512-0777 ..................................46, 4712-0778 ...................... 42, 46, 47, 5012-0779 ..................................46, 4712-0780 ........................................4612-0781 ............................ 46, 47, 5012-0782 ........................................4512-0784 ........................................4612-0785 ..................................46, 4712-0786 ..................................46, 4712-0787 ........................................4612-0788 ........................................4612-0790 ...................... 46, 47, 50, 5112-0791 ............................ 46, 47, 5012-0793 ..................................45, 4712-0795 ........................................4512-0952 ........................................4212-0962 ........................................4312-0970 ........................................4312-1030 ............................ 43, 47, 5112-1507 ............................ 46, 47, 5012-1508 ............................ 45, 47, 4912-1509 ..................................45, 4912-1512 .......................................5012-1514 ........................................5012-1515 ........................................5012-1516 ........................................5012-1518 ........................................5012-1650 ........................................4712-1651 ........................................4712-1669 ........................................4712-1750 ........................................4712-1751 ..................................47, 5112-1752 ..................................47, 5112-1753 ..................................47, 5112-1754 ..................................47, 5112-1755 ........................................5112-1760 ..................................45, 4912-1763 ...........22, 42, 43, 45, 47, 4912-1767 ........................................4412-1770 ........................................4412-1777 ........................................46

73

12-1785 .......................................4612-1786 ........................................4612-1787 ........................................4612-1790 ........................................4612-1791 ........................................4612-1792 ........................................4612-1795 ........................................4512-2270 ........................................5112-2277 ........................................5112-2279 ........................................5112-2282 ........................................5112-2730 ........................................4312-2731 ........................................4312-2734 ........................................4312-2735 ........................................4312-2737 ........................................4312-3788 ..................................45, 4912-5700 ........................................4212-5701 ........................................4212-5735 ........................................4212-5749 ........................................4212-5750 ..................................42, 4312-5751 ........................................4212-5753 ........................................4212-5754 ........................................4212-5755 ........................................4212-5756 ........................................4212-5758 ........................................4212-5766 ........................................42

13-0565 .......................................6313-0715 ........................................6313-0716 ........................................6313-0717 ........................................6313-0718 ........................................6313-0923 ........................................52

16-0264 .......................................5216-0313 ........................................5216-0675 ........................................5516-0700 ........................................3816-0705 ........................................5516-0742 ........................................5516-0773 ........................................3916-0820 ........................................5516-0824 ........................................5516-0825 ........................................5516-0829 ........................................5516-0830 ........................................5316-0844 ........................................5316-0845 ........................................5416-0850 ........................................5316-0859 ........................................5416-0860 ........................................5416-0861 ........................................5416-0862 ........................................5416-0863 ........................................5416-0864 ........................................5416-0865 ........................................5416-0866 ........................................5416-0867 ........................................5416-0868 ........................................5416-0869 ........................................5416-0870 ........................................5416-0871 ........................................5416-0872 ........................................5416-0873 ........................................5416-0874 ........................................5416-0875 ........................................5416-0876 ........................................5416-0877 ........................................5416-0878 ........................................5416-0879 ........................................54

16-0880 .......................................5416-0881 ........................................5416-0882 ........................................5416-0883 ........................................5416-0884 ........................................5416-0886 ........................................5416-0887 ........................................5416-0888 ........................................5416-0889 ........................................5416-0890 ........................................5416-0891 ........................................5416-0892 ........................................5416-0893 ........................................5516-0894 ........................................5516-0895 ........................................5516-0896 ........................................5516-0897 ........................................5416-0898 ..................................54, 5516-0899 ........................................5516-0901 ........................................5416-0902 ........................................5416-0925 ........................................5216-1430 ........................................5316-1444 ........................................5316-1445 ........................................5416-1450 ........................................5316-1452 ........................................5316-1454 ........................................5316-1455 ........................................5416-1458 ........................................5316-1839 ........................................5316-1844 ........................................5316-1845 ........................................5416-1850 ........................................53

17-0010 .......................................5217-0047 ..................................58, 6017-0158 ......................................6, 717-0237 ..........................................717-0584 ........................................5517-0700 ........................................2417-0701 ........................................2417-0702 ........................................2417-0703 ........................................2417-0706 ........................................2417-0707 ........................................2417-0708 ........................................2417-0709 ........................................2417-0710 ..................................52, 6817-0711 ..................................52, 6817-0716 ........................................2417-0717 ........................................2417-0802 ..................................52, 5517-0804 ..................................52, 55

18-0045 .......................................1918-0066 ........................................3718-0247 ........................................1918-0248 ........................................1918-0251 ........................................1918-0255 ........................................1918-0279 ........................................1918-0402 ................ 13, 15, 17, 19, 6918-0403 ................ 13, 15, 17, 19, 6918-1120 ........................................1618-1135 ........................................1718-1136 ........................................1718-1137 ........................................17

18-1144 .................................17, 6718-1145 ........................................1718-1149 ........................................1718-1160 ........................................1718-1161 ........................................1718-1163 ........................................1718-1164 ........................................1718-1200 ........................................1718-1201 ........................................1718-1202 ........................................1718-1203 ........................................1718-1204 ........................................1718-1700 ........................................1818-1701 ........................................1818-1721 ........................................1918-1726 ........................................1918-1728 ........................................1918-1732 ........................................1918-2200 ........................................1718-2213 ........................................1718-2215 ........................................1718-2370 ........................................17

19-0005 .......................................6519-0011 ........................................6519-0032 ........................................6519-0039 ........................................6519-0041 ........................................6519-0051 ........................................6519-0052 ........................................6519-0056 ........................................6519-0057 ........................................6519-0080 ........................................65

20-0030 .......................................3420-0040 ........................................3420-0095 ........................................3420-0096 ........................................3420-0106 ........................................2320-0150 ........................................3520-0151 ........................................3520-0156 ..................................35, 6820-0157 ..................................35, 6820-0158 ..................................35, 68

21-0030 .......................................3021-0113 ........................................3021-0114 ........................................3021-0115 ........................................3021-0116 ........................................3021-0117 ........................................3021-0118 ........................................3021-0155 ........................................3021-0157 ........................................3021-0158 ........................................3021-0361 ........................................2721-0362 ........................................2721-0367 ........................................2721-0368 ........................................2721-0501 ........................................2821-0502 ........................................28

21-0601 ........................... 17, 29, 6321-0602 ........................................2921-0603 ........................................2921-0604 ........................................2921-0605 ........................................2921-0606 ..................................29, 6321-0607 ............................ 17, 29, 6321-0608 ........................................2921-0609 ........................................2921-0610 ........................................2921-0611 ........................................2921-0612 ..................................29, 6321-0621 ............................ 17, 29, 6321-0622 ........................................2921-0623 ........................................2921-0624 ........................................2921-0625 ........................................2921-0626 ..................................29, 6321-0627 ............................ 17, 29, 6321-0628 ........................................2921-0629 ........................................2921-0630 ........................................2921-0631 ........................................2921-0632 ..................................29, 6321-0641 ........................................2921-0642 ........................................2921-0643 ........................................2921-0644 ........................................2921-0645 ........................................2921-0646 ........................................2921-0647 ........................................2921-0648 ........................................2921-0649 ........................................2921-0650 ........................................2921-0675 ........................................2921-0693 ........................................2921-0695 ...................... 28, 30, 34, 6721-0697 .....15, 27, 28, 30, 34, 59, 6721-0698 ........................................6721-0699 ........................................2921-0700 ........................................2921-0701 ........................................2921-0703 ........................................2821-0704 ........................................2921-0713 ........................................2821-0714 ........................................2821-6000 ........................................29

22-0050 .......................................3122-0051 ........................................3122-0052 ........................................3122-0053 ........................................3122-0054 ........................................3122-0055 ........................................3122-0056 ........................................3122-0057 ........................................3122-0058 ........................................3122-0059 ........................................3122-0060 ........................................3122-0061 ........................................3122-0070 ........................................3122-0093 ..................................31, 3422-0097 ........................................3122-0157 ........................................3522-0158 ........................................3522-0159 ........................................3522-0160 ........................................3522-0161 ........................................3522-0162 ........................................3522-0163 ........................................3522-0164 ..................................31, 35


74


22-0200 .......................................3222-0201 ........................................3222-0202 ........................................3222-0203 ........................................3222-0204 ........................................3222-0205 ........................................3222-0206 ........................................3222-0207 ........................................3222-0208 ........................................3222-0209 ........................................3222-0210 ........................................3222-0220 ........................................3222-0270 ..................................32, 3422-0278 ........................................3222-0450 ........................................3422-0500 ........................................3322-0501 ........................................3322-0502 ........................................3322-0503 ........................................3322-0504 ........................................3322-0505 ........................................3322-0506 ........................................3322-0507 ........................................3322-0508 ........................................3322-0509 ........................................3322-0510 ........................................3322-0515 ........................................3322-0516 ........................................3322-0520 ........................................3322-0521 ........................................3322-0522 ........................................3322-0523 ........................................3322-0524 ........................................3322-0525 ........................................3322-0528 ...................................31-3422-0529 ........................................3322-0530 ........................................3222-0531 ........................................3222-0532 ........................................3222-0533 ........................................3222-0534 ........................................3222-0535 ........................................3222-0536 ........................................3222-0537 ........................................3222-0538 ........................................3222-0539 ........................................3222-0540 ........................................3222-2050 ........................................3122-2051 ........................................3122-2052 ........................................3122-2053 ........................................3122-2054 ........................................3122-2055 ........................................3122-2056 ........................................3122-2057 ........................................3122-2058 ........................................3122-2059 ........................................3122-2060 ........................................3122-2061 ........................................3122-2065 ........................................3122-2200 ........................................3222-2201 ........................................3222-2202 ........................................3222-2203 ........................................3222-2204 ........................................3222-2205 ........................................3222-2206 ........................................3222-2207 ........................................3222-2208 ........................................3222-2209 ........................................3222-2210 ........................................32

23-0204 .................................31, 34

24-0601 .......................................6624-0602 ........................................6624-0603 ........................................6624-0604 ........................................6624-0605 ........................................6624-0606 ........................................6624-0607 ..................................29, 6624-0608 ..................................29, 6624-0609 ............................ 29, 34, 6624-0610 ..................................29, 6624-0611 ............................ 29, 34, 6624-0612 ........................................6624-0613 ............................ 29, 34, 6624-0614 ........................................6624-0615 ..................................34, 6624-0616 ............................ 29, 34, 6624-0617 ........................................6624-0618 ..................................34, 66

25-0001 .................................27, 5525-0004 ................................ 8, 9, 5525-0009 ................................ 8, 9, 5525-0042 ..........................................825-0043 ..........................................825-0108 ..................................27, 5525-0228 ...........12, 15, 19, 22, 49, 6925-0234 ........................................5125-0240 ............................ 24, 46, 6825-0241 ............................ 24, 46, 6825-0248 ........................................5125-0262 ........................................2225-0274 ........................................6725-0282 .......5, 17, 22, 45, 49, 64, 6725-0283 .......5, 17, 22, 45, 49, 64, 6725-0284 ........................................6725-0304 ..................................22, 6725-0338 ........................................1725-0368 ..................................63, 6925-0373 ..................................63, 6925-0382 ..................................49, 6925-0383 ..................................49, 6925-0417 ........................................6425-0418 ........................................6425-0420 ........................................6425-0470 ........................................5225-0471 ........................................5225-0485 ..................................34, 3925-0486 ..................................34, 3925-0489 ........................................3825-0490 ........................................3825-0607 ........................................2925-0608 ........................................2925-0670 ............................ 17, 19, 6925-0671 ............................ 17, 19, 6925-0700 ........................................5525-0701 ........................................5525-0702 ........................................5525-0703 ........................................5525-0704 ........................................5525-0705 ........................................5525-0706 ........................................5525-0707 ........................................5525-0708 ........................................5525-0804 ........................................4525-0902 .............................. 5, 42, 6725-0903 .............................. 5, 42, 6725-0910 ....................................5, 4225-0911 ....................................5, 4225-0912 ....................................5, 4225-0918 ........................................6725-0919 ....................................5, 6725-0920 ..........................................525-0930 .............................. 5, 42, 6725-0970 ........................................42

26-0004 .......................................6326-0010 ........................................6226-0011 ........................................6226-0014 ..................................55, 6326-0017 ........................................6326-0018 ........................................6326-0019 ........................................6426-0020 ........................................6426-0026 ........................................6326-0036 ........................................6326-0037 ........................................6326-0038 ........................................6326-0039 ........................................6326-0500 ........................................6226-0501 ........................................6226-0502 ........................................6226-0503 ........................................6226-0603 ........................................6226-0604 ........................................6226-0605 ........................................6226-0606 ........................................6226-0607 ........................................6226-0608 ........................................6226-0712 ........................................6126-0721 ........................................6126-0740 ........................................6126-0741 ........................................6126-0790 ........................................6126-0791 ........................................6126-0792 ........................................6126-0793 ........................................6126-0794 ........................................61

50-0001 .................................30, 4050-5172 ........................................3950-5227 ..........................................750-5242 ............................ 30, 60, 6750-5315 .......................................7-950-5317 ..........................................750-7027 ........................................5450-7030 ........................................5450-7047 ........................................5450-7050 ........................................5450-9023 ..................................49, 5150-9024 ..................................46, 5050-9037 ........................................6650-9110 ..................................46, 5050-9111 ...................... 42, 43, 46, 5050-9112 ..................................46, 5050-9113 ..................................46, 5050-9114 ..................................46, 5050-9151 ..........................................550-9160 ..........................................550-9161 ........................................3550-9162 ........................................3550-9167 .................................. 5, 8, 9

90-0100 .......................................3590-0101 ........................................3590-0102 ........................................3590-0103 ........................................3090-0136 ........................................3590-0137 ........................................3590-0149 ........................................3590-0173 ........................................3590-0196 ........................................3590-0204 ........................................3590-0212 ........................................3590-0214 ........................................3590-0215 ........................................3590-0217 ........................................3590-0240 ........................................3590-0241 ........................................3590-0247 ........................................5190-0248 ........................................5190-0250 ........................................3590-0251 ........................................3590-0252 ........................................3590-0253 ........................................3590-0254 ........................................3590-0281 ........................................3590-0284 ........................................3590-0285 ........................................3590-0306 ........................................5190-0307 ........................................5190-0311 ........................................3590-0315 ........................................3590-1101 ........................................3590-1103 ........................................3090-1149 ........................................3590-1196 ........................................3590-1204 ........................................3590-1212 ........................................3590-1214 ........................................3590-1215 ........................................3590-1217 ........................................3590-1240 ........................................3590-1241 ........................................3590-1247 ........................................5190-1248 ........................................5190-1281 ........................................3590-1284 ........................................3590-1285 ........................................3590-1306 ........................................5190-1307 ........................................5190-1311 ........................................3590-1315 ........................................35

99-0143 .......................................1999-0144 ........................................19

75

International StandardsInternational Standards

AASHTO AASHTO MP 1 (obs.) ..................................... 40AASHTO PP 1 (obs.) ...................................... 40AASHTO R 28 ................................................. 40AASHTO T 47 ................................................. 36AASHTO T 48 ........................................... 41, 43AASHTO T 51 ........................................... 10, 14AASHTO T 53 ............................................... 4, 8AASHTO T 55 ................................................. 53AASHTO T 59 ................................................. 53AASHTO T 72 ................................................. 28AASHTO T 73 ........................................... 44, 47AASHTO T 79 ........................................... 56, 65AASHTO T 172 ........................................... 44, 47AASHTO T 240 ................................................. 38AASHTO T 300 ................................................. 10AASHTO T 313 ................................................. 24AASHTO T 315 ................................................. 25AASHTO T 316 ................................................. 26AASHTO T 320 ................................................. 40AASHTO TP 1 (obs.) ..................................... 24AASHTO TP 5 (obs.) ..................................... 25AASHTO TP 48 (obs.) ..................................... 26

ASTM ASTM D 5 ................................................... 16ASTM D 6 ................................................... 36ASTM D 20 ................................................... 58ASTM D 36 ................................................. 4, 8ASTM D 70 ................................................... 61ASTM D 71 ................................................... 64ASTM D 88 ................................................... 28ASTM D 92 ............................................. 41, 43ASTM D 93 ............................................. 44, 47ASTM D 95 ................................................... 53ASTM D 113 ............................................. 10, 14ASTM D 140 ................................................... 65ASTM D 244 ................................................... 53ASTM D 246 (obs.) ........................................ 58ASTM D 402 ................................................... 56ASTM D 445 ................................................... 31ASTM D 446 ................................................... 31ASTM D 1481 ................................................... 61ASTM D 1665 ................................................... 30ASTM D 1754 ................................................... 36ASTM D 2171 ................................................... 33ASTM D 2569 ................................................... 60ASTM D 2872 ................................................... 38ASTM D 3142 ................................................... 62ASTM D 4057 ................................................... 65ASTM D 4402 ................................................... 26ASTM D 5329 ................................................... 16ASTM D 5892 (obs.) .................................. 10, 14ASTM D 6084 ............................................. 10, 14ASTM D 6521 ................................................... 40ASTM D 6648 ................................................... 24

ASTM E 102 ..................................................... 28

ASTM P 226 (obs.) .................................... 10, 14ASTM P 245 ..................................................... 24ASTM P 246 ..................................................... 25ASTM PS 36 (obs.) .......................................... 40

BS BS 434 (obs.) ................................................. 53BS 3442-2 (obs.) ........................................ 48, 51BS 4385 (obs.) ................................................. 53BS 4453 (obs.) ................................................. 56BS 4689 (obs.) ........................................... 41, 43BS 4699 (obs.) ................................................. 61

DIN DIN 1995 (obs.) ....................................... 53, 61DIN 1996-2 (obs.) ............................................ 65DIN 1996-5 ....................................................... 53DIN 1996-15 ................................................... 4, 9DIN 51 366 (obs.) ............................................. 31DIN 51 372 (obs.) ............................................. 31DIN 51 376 (obs.) ....................................... 41, 43DIN 51 550 (obs.) ............................................. 31DIN 51 560 (obs.) ............................................. 30DIN 51 582 (obs.) ............................................. 53DIN 51 757-2 .................................................... 64DIN 51 755-1 .................................................... 48DIN 52 001 ....................................................... 65DIN 52 004 ....................................................... 61DIN 52 010 (obs.) ............................................. 16DIN 52 011 (obs.) ........................................... 4, 8DIN 52 012 (obs.) ....................................... 20, 23DIN 52 013 ................................................. 10, 14DIN 52 015 (obs.) ............................................. 52DIN 52 016 (obs.) ............................................. 39DIN 52 024 ....................................................... 57DIN 52 027 ....................................................... 59DIN 52 048 (obs.) ............................................. 53DIN 55 680 (obs.) ............................................. 48DIN V 52 021-1 (obs.) ................................ 10, 14

DIS DIS 3658 (obs.) ................................................ 61

EN EN 58 ......................................................... 65EN 456 (obs.) .............................................. 48EN 924 ......................................................... 48EN 1426 ......................................................... 16EN 1427 ....................................................... 4, 8EN 1428 ......................................................... 53EN 1871-F ................................................... 4, 9EN 12 591 ......................................................... 25EN 12 593 ................................................... 20, 23EN 12 596 ......................................................... 33EN 12 606-1 ..................................................... 52EN 12 607-1 ..................................................... 38EN 12 607-2 ..................................................... 36EN 12 607-3 ..................................................... 39EN 12 846 ......................................................... 27EN 13 179-1 ................................................... 4, 8EN 13 179-2 ..................................................... 16EN 13 302 ......................................................... 26EN 13 303 ......................................................... 36EN 13 358 ......................................................... 56EN 13 398 ................................................... 10, 14EN 13 589 ......................................................... 10EN 13 703 ......................................................... 10EN 13 880-2 ..................................................... 16EN 14 769 ......................................................... 40EN 14 771 ......................................................... 24EN 22 592 (obs.) ........................................ 41, 43

FTM FTM 141-4293 ............................................ 44, 47FTM 141A-4285 (obs.) ..................................... 28FTM 791-1102 ............................................. 44,47FTM 791-1103 ............................................ 41, 43FTM 791-304 .................................................... 28FTM 791-305 (obs.) ......................................... 31

IP IP 27 ............................................................... 56IP 32 (obs.) .............................................. 10, 14IP 34-B ..................................................... 44, 47IP 36 ......................................................... 41, 43IP 45 (obs.) .................................................... 36IP 49 (obs.) .................................................... 16

IP 58 ............................................................. 4, 8IP 59-A (obs.) ................................................. 64IP 59-B (obs.) ................................................. 64IP 71-1 ............................................................ 31IP 71-2 ............................................................ 31IP 74 ............................................................... 53IP 80 ......................................................... 20, 23IP 170 ......................................................... 48, 51IP 189 ................................................................ 61IP 190 ................................................................ 61IP 212 ............................................................... 30IP 222 ............................................................... 33IP 291 ............................................................... 53IP 304-1 (obs.) . ................................................ 48IP 304-2 (obs.) ................................................. 48IP 459-1 ............................................................ 52IP 460-2 ............................................................ 36IP 460-3 ............................................................ 39IP 491 ............................................................... 48IP 492 ............................................................... 48IP 506 ............................................................... 36IP 515 ............................................................... 10IP 516 ......................................................... 10, 14IP 520 ............................................................... 10

ISO ISO 1516 ........................................................ 48ISO 1523 ........................................................ 48ISO 2592 .................................................. 41, 43ISO 2719 .................................................. 44, 47ISO 3104 ........................................................ 31ISO 3105 ........................................................ 31ISO 3679 ........................................................ 48ISO 3680 ........................................................ 48ISO 3733 ........................................................ 53ISO 3838 ........................................................ 61ISO 13736 .................................................. 48, 51

JIS JIS K 2207 ................... 4, 8, 10, 14, 28, 31, 36, 38JIS K 2208 ........................................................ 30JIS K 2249 ........................................................ 61JIS K 2265 ...................................... 20, 23, 41, 43JIS K 2275 ........................................................ 53JIS K 2283 ........................................................ 31

NF NF M 07-011 (obs.) .................................... 48, 51NF M 07-036 ..................................................... 48NF T 60-100 (obs.) ........................................... 31NF T 60-118 (obs.) ..................................... 41, 43NF T 60-616 (obs.) ........................................... 48NF T 60-617 (obs.) ........................................... 48NF T 65-001 (obs.) ........................................... 25NF T 66-003 (obs.) ........................................... 56NF T 66-006 (obs.) ..................................... 10, 14NF T 66-008 (obs.) ......................................... 4, 8NF T 66-011 (obs.) ........................................... 36NF T 66-026 (obs.) ..................................... 20, 23NF T 66-047 (obs.) ........................................... 36NF T 66-048 (obs.) ........................................... 39

SHRP SHRP 1001 ....................................................... 40SHRP 1002 ....................................................... 24SHRP 1006 ....................................................... 26SHRP 1007 ....................................................... 25SHRP B-002 ..................................................... 24SHRP B-003 ..................................................... 25

Superpave Superpave® .................. 24, 25, 26, 38, 40, 41, 43

(obs.) = obsolete

Ludwig-Erhard-Ring 13 · 15827 Dahlewitz - Germany · Tel.: +49 (0) 33708 / 56-300 · Fax: +49 (0) 33708 / 56-556E-Mail: [email protected] · Website: www.petrotest.com

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Petroleum Test Equipmentsince 1873

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98-1400 11/08

manufacturer since 1873 selection of standard display of results pmove jog-wheel operation system...

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