laboratory report for samples received 05/11/2006 · 2020-07-03 · laboratory report chris nitchie...

Laboratory Report

Chris Nitchie PO Number: None

Rizzo Associates LabiD: 10338

One Grant Street Date Received: 5/11/06

Framingham, MA 01701

Project: 1272420016

Attached please find results for the analysis of the samples received on the date referenced above.

Unless otherwise noted in the attached report, the analyses performed met the requirements of Resource Laboratories, LLC Quality Assurance Plan. The Standard Operating Procedures (SOP) are based upon USEPA SW-846, USEPA Methods for Chemical Analysis of Water and Wastewater, Standard Methods for the Examination of Water and Wastewater and other recognized methodologies. The results contained in this report pertain only to the samples as indicated on the chain of custody.

Resource Laboratories, LLC maintains certification with the agencies listed below.

We appreciate the opportunity to provide laboratory services. If you have any questions regarding the enclosed report, please contact the laboratory and we will be glad to assist you.

Sincerely, Resource. Laboratories, LLC

fl-1 t-a' , klA ..L-<

Susan Sylvester Date

Principal, General Manager

Total number of pages

New Hampshire Maine

Resource Laboratories, LLC Certifications

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Massachusetts M-NH902

124 Heritage Avenue #1 0 Portsmouth NH 03801 Voice: 603-436-2001 Fax: 603-430-2100

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Lab Number: Sample Designation: Date Sampled: Date Analyzed: Matrix: Instrument Dilution Factor: Analyst:

VOLATILE ORGANICS SW846 Method 50308/82608

dichlorodifluoromethane chloromethane vinyl chloride bromomethane chloroethane trichlorofluoromethane diethyl ether acetone 1,1-dichloroethene methylene chloride carbon disulfide methyl t-butyl ether (MTBE) trans-1 ,2-dichloroethene 1,1-dichloroethane 2-butanone (MEK) 2,2-dichloropropane cis-1 ,2-dichloroethene chloroform bromochloromethane tetrahydrofuran (THF) 1,1, 1-trichloroethane 1,1-dichloropropene carbon tetrachloride 1 ,2-dichloroethane benzene trichloroethene 1 ,2-dichloropropane bromodichloromethane dibromomethane 4-methyl-2-pentanone (MIBK) cis-1 ,3-dichloropropene toluene trans-1 ,3-dichloropropene 2-hexanone

SURROGATE STANDARDS

dibromofluoromethane toluene-DB 4-bromofluorobenzene

10338-01 B-5D-I 5/9/06 5/12/06 Water 1 LMM

Concentration

ug/L u u u u u u u u 2 u u u u

240 u u u u u

22 u u u u u u u u u u u u u u

Recovery (%)

109 104 101

Concentration Quantitation Limit

ug/L ug/L u 2 u 2 u 2 u 2 u 2 u 2 u 2 u 2 u 2 u 2 u 2 u 2 u 2 u 2 u 2 u 2 u 2 u 2 u 2 u 2 u 2 u 2 u 2 u 2 u 2 u 2 u 2 u 2 u 2 u 2 u 2 u 5 u 2

Quantitation Limit

ug/L 2 2 2 2 2 2

10 10

1 5 2 2 2 2

10 2 2 2 2

10 2 2 2 2 2 2 2 2 2

10 2 2 2

10

Acceptance Limits

(%) 78-114

88-110 86-115

1,1 ,2-trichloroethane 1 ,3-dichloropropane tetrachloroethene dibromochloromethane 1 ,2-dibromoethane chlorobenzene 1,1, 1 ,2-tetrachloroethane ethylbenzene m&p-xylenes a-xylene styrene bromoform isopropylbenzene 1,1 ,2,2-tetrachloroethane 1 ,2,3-trichloropropane n-propylbenzene bromo benzene 1 ,3,5-trimethylbenzene 2-chlorotoluene 4-chlorotoluene tert-butylbenzene 1 ,2,4-trimethylbenzene sec-butylbenzene 1 ,3-dichlorobenzene 4-isopropyltoluene 1 A-dichlorobenzene 1 ,2-dichlorobenzene n-butylbenzene 1 ,2-dibromo-3-chloropropane 1 ,2,4-trichlorobenzene hexachlorobutadiene naphthalene 1 ,2,3-trichlorobenzene

U =Below quantitation limit

RL Resource Laboratories, LLC



dichlorodifluoromethane chloromethane vinyl chloride bromo methane chloroethane trichlorofluoromethane diethyl ether acetone 1,1-dichloroethene methylene chloride carbon disulfide methyl t-butyl ether (MTBE) trans-1 ,2-dichloroethene 1, 1-dichloroethane 2-butanone (MEK) 2,2-dichloropropane cis-1 ,2-dichloroethene chloroform bromochloromethane tetrahydrofuran (THF) 1,1, 1-trichloroethane 1,1-dichloropropene carbon tetrachloride 1 ,2-dichloroethane benzene trichloroethene 1 ,2-dichloropropane bromodichloromethane dibromomethane 4-methyl-2-pentanone {MIBK) cis-1 ,3-dichloropropene toluene trans-1 ,3-dichloropropene 2-hexanone

SURROGATE STANDARDS

dibromofluoromethane

toluene-DB

4-bromofluorobenzene

10338-02 B-6A-D 5/9/06 5/15/06 Water 10 LMM

Concentration

ug/L u u

250 u u u u u

510 u u u

56 5200

u u

3500 u u u u u u u u

69 u u u

470 u

27 u u

Recovery

(%)

106

104

97


ug/L ug/L u 20 u 20 u 20 u 20 u 20 u 20 u 20

1700 20 940 20

u 20 u 20 u 20 u 20 u 20 u 20 u 20 u 20

u 20 u 20 u 20 u 20 u 20 u 20 u 20 u 20 u 20 u 20 u 20 u 20 u 20 u 20 u 50 u 20

Quantitation Limit

ug/L 20 20 20 20 20 20

100 100

10 50 20 20 20 20

100 20 20 20 20

100 20 20 20 20 20 20 20 20 20

100 20 20 20

100

Acceptance Limits

(%)

78-114

88-110

86-115

1,1 ,2-trichloroethane 1 ,3-dichloropropane tetrachloroethene dibromochloromethane 1 ,2-dibromoethane chlorobenzene 1,1, 1 ,2-tetrachloroethane ethylbenzene m&p-xylenes a-xylene styrene bromoform isopropyl benzene 1,1 ,2,2-tetrachloroethane 1 ,2,3-trichloropropane n-propylbenzene bromo benzene 1 ,3,5-trimethylbenzene 2-chlorotoluene 4-chlorotoluene tert-butylbenzene 1 ,2,4-trimethylbenzene sec-butylbenzene 1 ,3-dichlorobenzene 4-isopropyltoluene 1 A-dichlorobenzene 1 ,2-dichlorobenzene n-butylbenzene 1 ,2-dibromo-3-chloropropane 1 ,2,4-trichlorobenzene hexachlorobutadiene naphthalene 1 ,2,3-trichlorobenzene

U = Below quantitation limit





SURROGATE STANDARDS

dibromofluoromethane toluene-D8


10338-03 B-8A-D 5/9/06 5/12/06 Water 1 LMM

Concentration

ug/L u u 3 u u u u u

110 u u u u

430 u u u u u

59 u u u u u

13 u u u

330 u u u u

Recovery

(%)

108 102 99


ug/L ug/L u 2 u 2 u 2 u 2 u 2 u 2 u 2 6 2 u 2 u 2 u 2 u 2 u 2 u 2 u 2 u 2 u 2 u 2 u 2 u 2 u 2 u 2 u 2 u 2 u 2 u 2 u 2 u 2 u 2 u 2 u 2 u 5 u 2

Quantitation Limit

ug/L 2 2 2 2 2 2

10 10

1 5 2 2 2 2

10 2 2 2 2

10 2 2 2 2 2 2 2 2 2

10 2 2 2

10

Acceptance Limits (%)

78-114 88-110

86-115

1,1 ,2-trichloroethane 1 ,3-dichloropropane tetrachloroethene dibromochloromethane 1 ,2-dibromoethane chlorobenzene 1,1, 1 ,2-tetrachloroethane ethylbenzene m&p-xylenes a-xylene styrene bromoform isopropylbenzene 1,1 ,2,2-tetrachloroethane 1 ,2,3-trichloropropane n-propylbenzene bromo benzene 1 ,3,5-trimethylbenzene 2-chlorotoluene 4-chlorotoluene tert-butylbenzene 1 ,2,4-trimethylbenzene sec-butyl benzene 1 ,3-dichlorobenzene 4-isopropyltoluene 1 A-dichlorobenzene 1 ,2-dichlorobenzene n-butylbenzene 1 ,2-dibromo-3-chloropropane 1 ,2,4-trichlorobenzene hexachlorobutadiene naphthalene 1 ,2,3-trichlorobenzene



Lab Number: 10338-04 Sample Designation: B-9A-I Date Sampled: 5/9/06 Date Analyzed: 5/15/06 Matrix: Water Instrument Dilution Factor: 5 Analyst: LMM

VOLATILE ORGANICS SW 846 Method 50308/82608

Concentration Quantitation Limit Concentration Quantitation Limit

ug/L ug/L ug/L ug/L dichlorodifluoromethane u 10 1,1 ,2-trichloroethane u 10 chloromethane u 10 1 ,3-dichloropropane u 10 vinyl chloride u 10 tetrachloroethene u 10 bromomethane u 10 dibromochloromethane u 10 chloroethane 370 10 1 ,2-dibromoethane u 10 trichlorofluoromethane u 10 chlorobenzene u 10 diethyl ether u 50 1,1, 1 ,2-tetrachloroethane u 10 acetone 1300 50 ethyl benzene 40 10 1,1-dichloroethene u 5 m&p-xylenes 45 10 methylene chloride u 30 a-xylene 19 10 carbon disulfide 15 10 styrene u 10 methyl t-butyl ether (MTBE) u 10 bromoform u 10 trans-1 ,2-dichloroethene u 10 isopropylbenzene u 10 1,1-dichloroethane 670 10 1,1 ,2,2-tetrachloroethane u 10 2-butanone (MEK) 1100 50 1 ,2,3-trichloropropane u 10 2,2-dichloropropane u 10 n-propylbenzene u 10 cis-1 ,2-dichloroethene 31 10 bromo benzene u 10 chloroform u 10 1 ,3,5-trimethylbenzene u 10 bromochloromethane u 10 2-chlorotoluene u 10 tetrahydrofuran (THF) u 50 4-chlorotoluene u 10 1,1, 1-trichloroethane u 10 tert-butylbenzene u 10 1 ,1-dichloropropene u 10 1 ,2,4-trimethylbenzene u 10 carbon tetrachloride u 10 sec-butyl benzene u 10 1 ,2-dichloroethane u 10 1 ,3-dichlorobenzene u 10 benzene u 10 4-isopropyltoluene u 10 trichloroethene 18 10 1 A-dichlorobenzene u 10 1 ,2-dichloropropane u 10 1 ,2-dichlorobenzene u 10 bromodichloromethane u 10 n-butylbenzene u 10 dibromomethane u 10 1 ,2-dibromo-3-chloropropane u 10 4-methyl-2-pentanone (MIBK) 130 50 1 ,2,4-trichlorobenzene u 10 cis-1 ,3-dichloropropene u 10 hexachlorobutadiene u 10 toluene 68 10 naphthalene u 30 trans-1 ,3-dichloropropene u 10 1 ,2,3-trichlorobenzene u 10 2-hexanone u 50

SURROGATE STANDARDS Recovery Acceptance Limits

(%) (%) dibromofluoromethane 107 78-114 toluene-DB 102 88-110 4-bromofluorobenzene 99 86-115

Note: The sample pH was greater than 2, indicating inadequate preservation. U = Below quantitation limit




dichlorodifluoromethane chloromethane vinyl chloride bromo methane chloroethane trichlorofluoromethane diethyl ether acetone 1, 1-dichloroethene methylene chloride carbon disulfide methyl t-butyl ether (MTBE) trans-1,2-dichloroethene 1,1-dichloroethane 2-butanone (MEK) 2,2-dichloropropane cis-1,2-dichloroethene chloroform bromochloromethane tetrahydrofuran (THF) 1, 1, 1-trichloroethane 1,1-dichloropropene carbon tetrachloride 1,2-dichloroethane benzene trichloroethene 1,2-dichloropropane bromodichloromethane dibromomethane 4-methyl-2-pentanone (MIBK) cis-1,3-dichloropropene toluene trans-1,3-dichloropropene 2-hexanone

SURROGATE STANDARDS


toluene-DB


10338-05 B-128-1 5/9/06 5/15/06 Water 5 LMM

Concentration

ug/L

u u

52 u

190 u u

63 270

u u u

14 2900

120 u

830 u u

51 u u u u u

36 u u u

310 u

72 u u

Recovery

(%)

106

103

99

Quantitation Limit

ug/L

10 1,1,2-trichloroethane

10 1,3-dichloropropane

10 tetrachloroethene 10 dibromochloromethane 10 1,2-dibromoethane 10 chlorobenzene 50 1,1,1,2-tetrachloroethane 50 ethyl benzene

5 m&p-xylenes 30 a-xylene 10 styrene 10 bromoform 10 isopropyl benzene

10 1, 1,2,2-tetrachloroethane 50 1,2,3-trichloropropane 10 n-propylbenzene 10 bromo benzene 10 1,3,5-trimethylbenzene 10 2-chlorotoluene 50 4-chlorotoluene 10 tert-butylbenzene 10 1,2,4-trimethylbenzene 10 sec-butylbenzene . 10 1,3-dichlorobenzene 10 4-isopropyltoluene 10 1A-dichlorobenzene 10 1,2-dichlorobenzene

10 n-butylbenzene 10 1,2-dibromo-3-chloropropane 50 1,2,4-trichlorobenzene

10 hexachlorobutadiene 10 naphthalene 10 1,2,3-trichlorobenzene 50

Acceptance Limits

(%)

78-114

88-110

86-115


ug/L ug/L

u 10

u 10

u 10 u 10 u 10

u 10

u 10 400 10 300 10 130 10

u 10

u 10

u 10 u 10

u 10

u 10

u 10 u 10

u 10

u 10

u 10 u 10

u 10

u 10

u 10

u 10

u 10

u 10

u 10

u 10 u 10

u 30 u 10





dichlorodifluoromethane chloromethane vinyl chloride bromomethane chloroethane trichlorofluoromethane diethyl ether acetone 1,1-dichloroethene methylene chloride carbon disulfide methyl t-butyl ether (MTBE) trans-1 ,2-dichloroethene 1,1-dichloroethane 2-butanone (MEK) 2,2-dichloropropane cis-1 ,2-dichloroethene chloroform bromochloromethane tetrahydrofuran (THF) 1,1, 1-trichloroethane 1,1-dichloropropene carbon tetrachloride 1 ,2-dichloroethane benzene trichloroethene 1 ,2-dichloropropane bromodichloromethane dibromomethane 4-methyl-2-pentanone {MIBK) cis-1 ,3-dichloropropene toluene trans-1 ,3-dichloropropene 2-hexanone

SURROGATE STANDARDS

dibromofluoromethane toluene-DB


10338-06 NBW-L 5/9/06 5/12/06 Water 1 LMM

Concentration

ug/L u u u u u u u

100 u u u u u u u u u u u u u u u u u u u u u u u u u u

Recovery

(%)

107 102

96

Quantitation Limit

ug/L 2 1,1 ,2-trichloroethane 2 1 ,3-dichloropropane 2 tetrachloroethene 2 dibromochloromethane 2 1 ,2-dibromoethane 2 chlorobenzene

10 1,1, 1 ,2-tetrachloroethane 10 ethyl benzene

1 m&p-xylenes 5 a-xylene 2 styrene 2 bromoform 2 isopropylbenzene . 2 1,1 ,2,2-tetrachloroethane

10 1 ,2,3-trichloropropane 2 n-propylbenzene 2 bromobenzene 2 1 ,3,5-trimethylbenzene 2 2-chlorotoluene

10 4-chlorotoluene 2 tert-butylbenzene 2 1 ,2,4-trimethylbenzene 2 sec-butyl benzene 2 1 ,3-dichlorobenzene 2 4-isopropyltoluene 2 1 A-dichlorobenzene 2 1 ,2-dichlorobenzene 2 n-butylbenzene 2 1 ,2-dibromo-3-chloropropane

10 1 ,2,4-trichlorobenzene 2 hexachlorobutadiene 2 naphthalene 2 1 ,2,3-trichlorobenzene

10


78-114

88-110 86-115








SURROGATE STANDARDS



10338-07 NBW-U 5/9/06 5/12/06 Water 1 LMM

Concentration

ug/L u u u u u u u


Recovery (%)

108 102

98



Quantitation Limit ug/L

2 2 2 2 2 2

10 10

1 5 2 2 2 2

10 2 2 2 2

10 2 2 2 2 2 2 2 2 2

10 2 2 2

10


78-114

88-110 86-115

1,1 ,2-trichloroethane 1 ,3-dichloropropane tetrachloroethene dibromochloromethane 1 ,2-dibromoethane' chlorobenzene 1,1, 1 ,2-tetrachloroethane ethyl benzene m&p-xylenes o-xylene styrene bromoform isopropylbenzene 1,1 ,2,2-tetrachloroethane 1 ,2,3-trichloropropane n-propylbenzene bromobenzene 1 ,3,5-trimethylbenzene 2-chlorotoluene 4-chlorotoluene tert-butylbenzene 1 ,2,4-trimethylbenzene sec-butyl benzene 1 ,3-dichlorobenzene 4-isopropyltoluene 1 A-dichlorobenzene 1 ,2-dichlorobenzene n-butylbenzene 1 ,2-dibromo-3-chloropropane 1 ,2,4-trichlorobenzene hexachlorobutadiene naphthalene 1 ,2,3-trichlorobenzene





dichlorodifluoromethane chloromethane vinyl chloride bromo methane chloroethane trichlorofluoromethane diethyl ether acetone 1,1-dichloroethene methylene chloride carbon disulfide methyl t-butyl ether (MTBE) trans-1 ,2-dichloroethene 1,1-dichloroethane 2-butanone (MEK) 2,2-dichloropropane cis-1 ,2-dichloroethene chloroform bromochloromethane tetrahydrofuran (THF) 1,1, 1-trichloroethane 1,1-dichloropropene carbon tetrachloride 1 ,2-dichloroethane benzene trichloroethene 1 ,2-dichloropropane bromodichloromethane dibromomethane 4-methyl-2-pentanone (MIBK) cis-1 ,3-dichloropropene toluene trans-1 ,3-dichloropropene 2-hexanone

SURROGATE STANDARDS


toluene-DB 4-bromofluorobenzene

10338-08 ODW-L 5/9/06 5/12/06 Water 1 LMM

Concentration ug/L

u u u u u u u


Recovery

(%)

110 103

100


2 1,1 ,2-trichloroethane 2 1 ,3-dichloropropane 2 tetrachloroethene 2 dibromochloromethane 2 1 ,2-dibromoethane· 2 chlorobenzene

10 1,1, 1 ,2-tetrachloroethane 10 ethyl benzene

m&p-xylenes 5 a-xylene 2 styrene 2 bromoform 2 isopropyl benzene 2 1,1 ,2,2-tetrachloroethane

10 1 ,2,3-trichloropropane 2 n-propylbenzene 2 bromo benzene 2 1 ,3,5-trimethylbenzene 2 2-chlorotoluene

10 4-chlorotoluene 2 tert-butylbenzene 2 1 ,2,4-trimethylbenzene 2 sec-butyl benzene 2 1 ,3-dichlorobenzene 2 4-isopropyltoluene 2 1 A-dichlorobenzene 2 1 ,2-dichlorobenzene 2 n-butylbenzene 2 1 ,2-dibromo-3-chloropropane


10


78-114

88-110 86-115








SURROGATE STANDARDS



10338-09 ODW-U 5/9/06 5/12/06 Water 1 LMM

Concentration

ug/L u u u u u u u

29 u u u u u

27 u u 4 u u u u u u u u u u u u u u u u u

Recovery

(%)

108 102

99



Quantitation Limit

ug/L 2 2 2 2 2 2

10 10

5 2 2 2 2

10 2 2 2 2

10 2 2 2 2 2 2 2 2 2

10 2 2 2

10

Acceptance Limits

(%)

78-114 88-110

86-115

1,1 ,2-trichloroethane 1 ,3-dichloropropane tetrachloroethene dibromochloromethane 1 ,2-dibromoethane chlorobenzene 1,1, 1 ,2-tetrachloroethane ethyl benzene m&p-xylenes o-xylene styrene bromoform isopropyl benzene 1,1 ,2,2-tetrachloroethane 1 ,2,3-trichloropropane n-propylbenzene bromo benzene 1 ,3,5-trimethylbenzene 2-chlorotoluene 4-chlorotoluene tert-butylbenzene 1 ,2,4-trimethylbenzene sec-butylbenzene 1 ,3-dichlorobenzene 4-isopropyltoluene 1 A-dichlorobenzene 1 ,2-dichlorobenzene n-butylbenzene 1 ,2-dibromo-3-chloropropane 1 ,2,4-trichlorobenzene hexachlorobutadiene naphthalene 1 ,2,3-trichlorobenzene






SURROGATE STANDARDS



10338-10 P-20 5/9/06 5/12/06 Water 1 LMM

Concentration

ug/L u u

63 u u u u u 2 u u u

180 55 u u

420 u u u u u u u u

210 u u u u u u u u

Recovery

(%) 108 104

102



Quantitation Limit

ug/L 2 2 2 2 2 2

10 10

5 2 2 2 2

10 2 2 2 2

10 2 2 2 2 2 2 2 2 2

10 2 2 2

10

Acceptance Limits

(%) 78-114 88-110

86-115

1,1 ,2-trichloroethane 1 ,3-dichloropropane tetrachloroethene dibromochloromethane 1 ,2-dibromoethane chlorobenzene 1,1, 1 ,2-tetrachloroethane ethyl benzene m&p-xylenes a-xylene styrene bromoform isopropyl benzene 1,1 ,2,2-tetrachloroethane 1 ,2,3-trichloropropane n-propylbenzene bromo benzene 1 ,3,5-trimethylbenzene 2-chlorotoluene 4-chlorotoluene tert-butylbenzene 1 ,2,4-trimethylbenzene sec-butyl benzene 1 ,3-dichlorobenzene 4-isopropyltoluene 1 A-dichlorobenzene 1 ,2-dichlorobenzene n-butylbenzene 1 ,2-dibromo-3-chloropropane 1 ,2,4-trichlorobenzene hexachlorobutadiene naphthalene 1 ,2,3-trichlorobenzene






SURROGATE STANDARDS



10338-11 QB-4 5/9/06 5/12/06 Water 1 LMM

Concentration

ug/L u u u u u u u u u u u u u u u u u u u u u u u u u u u u u u u u u u

Recovery (%)

107

102 101


2 1,1 ,2-trichloroethane 2 1 ,3-dichloropropane 2 tetrachloroethene 2 dibromochlorometliane 2 1 ,2-dibromoethane 2 chlorobenzene

10 1,1, 1 ,2-tetrachloroethane 10 ethylbenzene

m&p-xylenes 5 o-xylene 2 styrene 2 bromoform 2 isopropyl benzene 2 1,1 ,2,2-tetrachloroethane

10 1 ,2,3-trichloropropane 2 n-propylbenzene 2 bromo benzene 2 1 ,3,5-trimethylbenzene 2 2-chlorotoluene

10 4-chlorotoluene 2 tert-butylbenzene 2 1 ,2,4-trimethylbenzene 2 sec-butylbenzene 2 1 ,3-dichlorobenzene 2 4-isopropyltoluene 2 1 A-dichlorobenzene 2 1 ,2-dichlorobenzene 2 n-butylbenzene 2 1 ,2-dibromo-3-chloropropane


10


78-114

88-110 86-115








SURROGATE STANDARDS


toluene-DB


10338-12 B-128-1-Dup 5/9/06 5/15/06 Water 5 LMM

Concentration

ug/L u u

50 u

180 u u

58 260

u u u

14 2800

110 u

800 u u

53 u u u u u

36 u u u

290 u

70 u u

Recovery

(%)

109

105 98

Quantitation Limit

ug/L 10 1,1 ,2-trichloroethane 10 1 ,3-dichloropropane 10 tetrachloroethene 10 dibromochloromethane 10 1 ,2-dibromoethane 10 chlorobenzene 50 1,1, 1 ,2-tetrachloroethane 50 ethyl benzene

5 m&p-xylenes 30 a-xylene 10 styrene 10 bromoform 10 isopropylbenzene 10 1,1 ,2,2-tetrachloroethane 50 1 ,2,3-trichloropropane 10 n-propylbenzene 10 bromo benzene 10 1 ,3,5-trimethylbenzene 10 2-chlorotoluene 50 4-chlorotoluene 10 tert-butylbenzene 10 1 ,2,4-trimethylbenzene 10 sec-butyl benzene 10 1 ,3-dichlorobenzet:e 10 4-isopropyltoluene 10 1 A-dichlorobenzene 10 1 ,2-dichlorobenzene 10 n-butylbenzene 10 1 ,2-dibromo-3-chloropropane 50 1 ,2,4-trichlorobenzene 10 hexachlorobutadiene 10 naphthalene 10 1 ,2,3-trichlorobenzene 50

Acceptance Limits

(%) 78-114

88-110

86-115


ug/L ug/L u 10 u 10 u 10 u 10 u 10 u 10 u 10

400 10 290 10 120 10

u 10 u 10 u 10 u 10 u 10 u 10 u 10 u 10 u 10 u 10 u 10 u 10 u 10 u 10 u 10 u 10 u 10 u 10 u 10 u 10 u 10 u 30 u 10




VOLATILE ORGANICS SW846 Method 5030B/8260B

dichlorodifluoromethane chloromethane vinyl chloride bromo methane chloroethane trichlorofluoromethane diethyl ether acetone 1,1-dichloroethene methylene chloride carbon disulfide methyl t-butyl ether (MTBE) trans-1 ,2-dichloroethene 1,1-dichloroethane 2-butanone (MEK) 2,2-dichloropropane cis-1 ,2-dichloroethene chloroform bromochloromethane tetrahydrofuran (THF) 1,1, 1-trichloroethane 1,1-dichloropropene carbon tetrachloride 1 ,2-dichloroethane benzene trichloroethane 1 ,2-dichloropropane bromodichloromethane dibromomethane 4-methyl-2-pentanone (MIBK) cis-1 ,3-dichloropropene toluene trans-1 ,3-dichloropropene 2-hexanone

SURROGATE STANDARDS


toluene-D8


10338-13 Trip Blank 5/9/06 5/12/06 Water 1 LMM

Concentration ug/L

u u u u u u u u u u u u u u u u u u u u u u u u u u u u u u u u u u

Recovery

(%)

107

101 100



Quantitation Limit

ug/L 2 2 2 2 2 2

10 10

1 5 2 2 2 2

10 2 2 2 2

10 2 2 2 2 2 2 2 2 2

10 2 2 2

10

Acceptance Limits

(%)

78-114

88-110

86-115

1,1 ,2-trichloroethane 1 ,3-dichloropropane tetrachloroethane dibromochloromethane 1 ,2-dibromoethane chlorobenzene 1,1, 1 ,2-tetrachloroethane ethyl benzene m&p-xylenes a-xylene styrene bromoform isopropyl benzene 1,1 ,2,2-tetrachloroethane 1 ,2,3-trichloropropane n-propylbenzene bromobenzene 1 ,3,5-trimethylbenzene 2-chlorotoluene 4-chlorotoluene tert-butylbenzene 1 ,2,4-trimethylbenzene sec-butyl benzene 1 ,3-dichlorobenzene 4-isopropyltoluene 1 A-dichlorobenzene 1 ,2-dichlorobenzene n-butylbenzene 1 ,2-dibromo-3-chloropropane 1 ,2,4-trichlorobenzene hexachlorobutadiene naphthalene 1 ,2,3-trichlorobenzene



Lab Number:

Sample Designation:

Date Sampled:

Date Extracted:

Date Analyzed:

Matrix:

Dilution Factor:

Analyst:

DIMETHYLFORMAMIDE

10338-01

B-5D-I

5/9/06

5/22/06

5/24/06

Water

1

AJD

Method Reference: EPA SW 846, 3rd Edition. Method 8270, modified.

dimethylformamide

SURROGATE STANDARDS

pyridine


Concentration

ug/L

u

Recovery

(%) 57

Quantitation Limit

ug/L

50

Acceptance Limits

(%) 40-125


Lab Number:

Sample Designation:

Date Sampled:

Date Extracted:

Date Analyzed:

Matrix:

Dilution Factor:

Analyst:

DIMETHYLFORMAMIDE

10338-02

B-6A-D

5/9/06

5/22/06

5/24/06

Water

1

AJD


dimethylformamide

SURROGATE STANDARDS

pyridine


Concentration

ug/L

890

Recovery

(%) 72

Quantitation Limit

ug/L

50

Acceptance Limits

(%) 40-125


Lab Number: Sample Designation:

Date Sampled: Date Extracted:

Date Analyzed:

Matrix:

Dilution Factor:

Analyst:

DIMETHYLFORMAMIDE

10338-03

B-8A-D

5/9/06 5/22/06

5/24/06

Water

1 AJD


dimethylformamide

SURROGATE STANDARDS

pyridine


Concentration

ug/L

480

Recovery

(%) 60

Quantitation Limit

ug/L

50

Acceptance Limits

(%) 40-125


Lab Number:

Sample Designation:

Date Sampled:

Date Extracted:

Date Analyzed:

Matrix:

Dilution Factor:

Analyst:

DIMETHYLFORMAMIDE

10338-04

B-9A-I

5/9/06

5/22/06

5/24/06

Water

1

AJD


d i methylfo rma 111 ide

SURROGATE STANDARDS

pyridine


Concentration

ug/L

u

Recovery

(%) 62

Quantitation Limit

ug/L

50

Acceptance Limits

(%) 40-125


Lab Number:

Sample Designation:


Date Analyzed:

Matrix:

Dilution Factor:

Analyst:

DIMETHYLFORMAMIDE

10338-05

B-128-1

5/9/06 5/22/06

5/24/06

Water

1 AJD


dimethylformamide

SURROGATE STANDARDS

pyridine


Concentration ug/L

1600

Recovery

(%) 72


50

Acceptance Limits

(%) 40-125


Lab Number: Sample Designation:


Date Analyzed:

Matrix:

Dilution Factor:

Analyst:

DIMETHYLFORMAMIDE

10338-06

NBW-L 5/9/06

5/22/06

5/24/06 Water

1 AJD


dimethylformamide

SURROGATE STANDARDS

pyridine


Concentration

ug/L

u

Recovery (%) 59


50


40-125


Lab Number:

Sample Designation:

Date Sampled:

Date Extracted:

Date Analyzed:

Matrix:

Dilution Factor:

Analyst:

DIMETHYLFORMAMIDE

10338-07

NBW-U

5/9/06

5/22/06

5/24/06

Water

1

AJD


dimethylformamide

SURROGATE STANDARDS

pyridine


Concentration

ug/L

u

Recovery

(%) 75

Quantitation Limit

ug/L

50

Acceptance Limits

(%) 40-125


Lab Number:

Sample Designation:


Date Analyzed: Matrix:

Dilution Factor:

Analyst:

DIMETHYLFORMAMIDE

10338-08 ODW-L

5/9/06 5/22/06

5/25/06 Water

1 AJD


dimethylformamide

SURROGATE STANDARDS

pyridine


Concentration ug/L

u

Recovery

(%) 69

Quantitation Limit

ug/L

50


40-125


Lab Number:

Sample Designation:

Date Sampled:

Date Extracted:

Date Analyzed:

Matrix:

Dilution Factor:

Analyst:

DIMETHYLFORMAMIDE

10338-09

ODW-U

5/9/06

5/22/06

5/24/06

Water

1

AJD


dimethylformamide

SURROGATE STANDARDS

pyridine


Concentration

ug/L

u

Recovery

(%) 67

Quantitation Limit

ug/L

50

Acceptance Limits

(%) 40-125


Lab Number:

Sample Designation:

Date Sampled:

Date Extracted:

Date Analyzed:

Matrix:

Dilution Factor:

Analyst:

DIMETHYLFORMAMIDE

10338-10

P-20

5/9/06

5/22/06

5/24/06

Water

1

AJD


dimethylformamide

SURROGATE STANDARDS

pyridine


Concentration

ug/L

u

Recovery

(%) 60

Quantitation Limit

ug/L

50

Acceptance Limits

(%) 40-125


Lab Number:

Sample Designation:

Date Sampled:

Date Extracted:

Date Analyzed:

Matrix:

Dilution Factor:

Analyst:

DIMETHYLFORMAMIDE

10338-11

QB-4

5/9/06

5/22/06

5/24/06

Water

1

AJD


dimethylformamide

SURROGATE STANDARDS

pyridine


Concentration

ug/L

u

Recovery

(%) 68

Quantitation Limit

ug/L

50

Acceptance Limits

(%) 40-125


Lab Number:

Sample Designation:

Date Sampled:

Date Extracted:

Date Analyzed:

Matrix:

Dilution Factor:

Analyst:

DIMETHYLFORMAMIDE

10338-12

8-128-1-Dup

5/9/06

5/22/06

5/24/06

Water

1

AJD


dimethylformamide

SURROGATE STANDARDS

pyridine


Concentration

ug/L

1700

Recovery

(%) 75

Quantitation Limit

ug/L

50

Acceptance Limits

(%) 40-125


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