kodak reports laboratories - science...your own in photography through the microscope, don't...

11
Kodak reports to laboratories on: identifying multicarbide phases by color photomicrography... high speed movie success stories ... some things you can do with oxidized cellulose Metallography in color Meet Mr. Foster. Charles S. Foster is our ace photomicrographer. Charlie's function with us is to dole out individualized advice on how most expeditiously to get where you want to go with a photomicrograph- ic or metallographic undertaking. Being the kind of chap he is, Char- lie's advice is likely to be highly per- sonalized. A year or two ago the chief metal- lographer in the Powder Metals Re- search Department at Firth Sterling Inc. in Pittsburgh thought he would ask Mr. Foster for a little help on the problem of identifying constitu- ents and phases in multicarbide mix- tures through photomicrography in color. Worked out fine. Recently that hard-boiled publication, Steel, carried a short illustrated article on the results. It may turn out to be something of a landmark in metal- lography. Time will tell. The technique is heat-tinting at 900 F for 5 minutes after careful -polishing and electrolytic etching in 5 % sodium carbonate. The various phases assume characteristic colors: grey for tungsten carbide grains, yellow for tantalum carbide, tan for the solution areas of tungsten car- bide plus titanium carbide, deep purple for the eta phase formed by carbon deficiency, blue for the co- balt matrix,_and so on. Though Mr. Foster is no metallurgist, he did prove helpful on the important mat- ters of illumination and filtering to record these color nuances repro- ducibly on Kodak Ektachrome Film, Daylight Type. Bulking large in making the proj- ect practical was the fact that this film can be processed on the spot to judge the results. Perhaps life is not really that sim- ple, but we like to think that in supe- rior creep properties, better service in jet engine blades, etc., Firth Ster- ling products are now or soon will be reflecting the knowledge gained through heat-tinting. Mr. Foster will be most happy to send you a reprint of the Steel article if you want to see color reproductions of Firth Sterling's heat-tinted carbides at 1500 diameters. Also, ifyou have problems of your own in photography through the microscope, don't hesitate to write him about them. His address: Eastman Kodak Company, Industrial Photo- graphic Division, Rochester 4, N. Y. High speed booklet For only $1713.50 one may pur- chase from any Kodak Industrial Dealer a Kodak High Speed Camera. Some of the best-known type- writers, diesel locomotives, ciga- rette lighters, oil-drilling bits, break- fast foods, circuit breakers, printing papers, auto tires, beet pickers, cas- serole dishes, power- looms, power tools, addressing machines, shot- guns, vacuum cleaners, airplanes, and adding machines are being manufactured today on the basis of information their makers learned or confirmed by buying a Kodak High Speed Camera and submitting their products or processes to its quick and glassy gaze. (On the more academic side, we know of at least one diverted biologist who used the camera to find out how holes in fluids appear and disappear when a missile passes through.) The subject is mentioned at this time because we have just published a new booklet which explains how the camera works and how it has performed some of its industrial research feats. For a copy of "High Speed Motion Picture Making in Industry," write Eastman Kodak Company, Industrial Photographic Division, Rochester 4, N. Y. Slightly degenerated cotton Instead of oxidizing cellulose as man has done from time immemorial to take the chill out of his bones, cook his dinner, and dispel his gloom, we have a trick of oxidizing it only to a 10% to 22% carboxyl level. This we do by treatment with nitrogen diox- ide. The product, called, surprising- ly enough, "oxidized cellulose," looks like this: It has the appearance and even some of the strength of ordinary cot- ton, along with some rather extraor- dinary properties. The most recent of these to come to light is its use in the diagnosis of congenital hyper- plasia (enlargement) of the adrenal gland in children. This comes about from the remarkable affinity of ox- idized cellulose for ACITH, which it absorbs quantitatively. ACTH is not detectable in the blood of nor- mal children but does appear where this affliction exists. After cortisone treatment, no ACTH is detectable. One advantage of oxidized cellulose in ACTH assay is that the concen- trates it yields are not toxic to the assay animal. This is not the debut of the stuff as a tool in the healing art. Its first flush of prominence a few years ago was based on the surgically useful fact that it has the physical attri- butes of cotton gauze, yet is wholly absorbed in the blood stream after fulfilling its mechanical function. Aside from its medical use, oxi- dized cellulose is an ion exchange medium, plucking cations out of aqueous solution to form metallic salts of cellulose. Plain cotton as far as the eye can see and the finger can feel, it bewitchedly vanishes into solution when popped into a 2% sodium hydroxide solution. When kept dry and cold-, however, it sur- vives indefinitely without change. Trimming the cellulose chains with 10 to 22 percent of carboxyls drives the price of cotton up to $62.25 per pound, FOB Kingsport, Tenn. If you are inter- ested in concentrating some ACTH, this may be a bargain for you right now, and, if you can develop some decent volume of demandfor it, we'll probably drop the price. For the cold facts, write Eastman Chemical Products, Inc., Chemical Divi- sion, Kingsport, Tenn. (Subsidiary of Eastman Kodak Company). A This is one of a series of reports on the many products and services with which the Eastman Kodak Company and its divisions are. . . serving laboratories everywhere

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Page 1: Kodak reports laboratories - Science...your own in photography through the microscope, don't hesitate to write him about them. His address: Eastman Kodak Company, Industrial Photo-graphic

Kodak reports to laboratories on:identifying multicarbide phases by color photomicrography... high speed moviesuccess stories ... some things you can do with oxidized cellulose

Metallography in color

Meet Mr. Foster. Charles S. Fosteris our ace photomicrographer.Charlie's function with us is to doleout individualized advice on howmost expeditiously to get where youwant to go with a photomicrograph-ic or metallographic undertaking.Being the kind of chap he is, Char-lie's advice is likely to be highly per-sonalized.A year or two ago the chief metal-

lographer in the Powder Metals Re-search Department at Firth SterlingInc. in Pittsburgh thought he wouldask Mr. Foster for a little help onthe problem of identifying constitu-ents and phases in multicarbide mix-tures through photomicrography incolor. Worked out fine. Recentlythat hard-boiled publication, Steel,carried a short illustrated article onthe results. It may turn out to besomething of a landmark in metal-lography. Time will tell.The technique is heat-tinting at

900 F for 5 minutes after careful-polishing and electrolytic etching in5% sodium carbonate. The variousphases assume characteristic colors:grey for tungsten carbide grains,yellow for tantalum carbide, tan forthe solution areas of tungsten car-bide plus titanium carbide, deeppurple for the eta phase formed bycarbon deficiency, blue for the co-balt matrix,_and so on. Though Mr.Foster is no metallurgist, he didprove helpful on the important mat-ters of illumination and filtering torecord these color nuances repro-ducibly on Kodak Ektachrome Film,Daylight Type.

Bulking large in making the proj-ect practical was the fact that thisfilm can be processed on the spot tojudge the results.

Perhaps life is not really that sim-ple, but we like to think that in supe-

rior creep properties, better servicein jet engine blades, etc., Firth Ster-ling products are now or soon willbe reflecting the knowledge gainedthrough heat-tinting.Mr. Foster will be most happy to send

you a reprint of the Steel article if youwant to see color reproductions of FirthSterling's heat-tinted carbides at 1500diameters. Also, ifyou have problems ofyour own in photography through themicroscope, don't hesitate to write himabout them. His address: EastmanKodak Company, Industrial Photo-graphic Division, Rochester 4, N. Y.

High speed bookletFor only $1713.50 one may pur-chase from any Kodak IndustrialDealer a Kodak High Speed Camera.Some of the best-known type-

writers, diesel locomotives, ciga-rette lighters, oil-drilling bits, break-fast foods, circuit breakers, printingpapers, auto tires, beet pickers, cas-serole dishes, power- looms, powertools, addressing machines, shot-guns, vacuum cleaners, airplanes,and adding machines are beingmanufactured today on the basis ofinformation their makers learnedor confirmed by buying a KodakHigh Speed Camera and submittingtheir products or processes to itsquick and glassy gaze. (On the moreacademic side, we know of at leastone diverted biologist who used thecamera to find out how holes influids appear and disappear when amissile passes through.)The subject is mentioned at this

time because we have just publisheda new booklet which explains howthe camera works and how it hasperformed some of its industrialresearch feats.For a copy of "High Speed Motion

Picture Making in Industry," writeEastman Kodak Company, IndustrialPhotographic Division, Rochester 4,N. Y.

Slightly degenerated cottonInstead of oxidizing cellulose as manhas done from time immemorial totake the chill out of his bones, cookhis dinner, and dispel his gloom, wehave a trick of oxidizing it only to a10% to 22% carboxyl level. This wedo by treatment with nitrogen diox-ide. The product, called, surprising-

ly enough, "oxidized cellulose,"looks like this:

It has the appearance and evensome of the strength of ordinary cot-ton, along with some rather extraor-dinary properties. The most recentofthese to come to light is its use inthe diagnosis of congenital hyper-plasia (enlargement) of the adrenalgland in children. This comes aboutfrom the remarkable affinity of ox-idized cellulose for ACITH, which itabsorbs quantitatively. ACTH isnot detectable in the blood of nor-mal children but does appear wherethis affliction exists. After cortisonetreatment, no ACTH is detectable.One advantage of oxidized cellulosein ACTH assay is that the concen-trates it yields are not toxic to theassay animal.

This is not the debut of the stuffas a tool in the healing art. Its firstflush of prominence a few years agowas based on the surgically usefulfact that it has the physical attri-butes of cotton gauze, yet is whollyabsorbed in the blood stream afterfulfilling its mechanical function.Aside from its medical use, oxi-

dized cellulose is an ion exchangemedium, plucking cations out ofaqueous solution to form metallicsalts of cellulose. Plain cotton as faras the eye can see and the finger canfeel, it bewitchedly vanishes intosolution when popped into a 2%sodium hydroxide solution. Whenkept dry and cold-, however, it sur-vives indefinitely without change.

Trimming the cellulose chains with 10to 22 percent of carboxyls drives theprice of cotton up to $62.25 per pound,FOB Kingsport, Tenn. Ifyou are inter-ested in concentrating some ACTH, thismay be a bargain for you right now, and,if you can develop some decent volumeofdemandfor it, we'll probably drop theprice. For the coldfacts, write EastmanChemical Products, Inc., Chemical Divi-sion, Kingsport, Tenn. (Subsidiary ofEastman Kodak Company). A

This is one of a series of reports on the many productsand services with which the Eastman Kodak Company andits divisions are. . . serving laboratories everywhere

Page 2: Kodak reports laboratories - Science...your own in photography through the microscope, don't hesitate to write him about them. His address: Eastman Kodak Company, Industrial Photo-graphic

INTRODUCTION TONUCLEAR ENGINEERINGby RAYMOND L. MURRAY, North Carolina

State College at RaleighThe FIRST and ONLY undergraduate text innuclear engineering, this new book gives an overallview of the nuclear energy field including prob-lems of radiation hazards, waste disposal andinstrumentation.INTRODUCTION TO NUCLEAR ENGINEER-ING has been developed and tested in the famouspioneering program in Nuclear Engineering of theNorth Carolina State College. It is designed tohelp meet the growing need for trained personnelin peacetime industrial research and production.416 pages * 5-5/8" x 8-3/8" * February 1954

ADVANCEDORGANIC CHEMISTRY

by E. EARL ROYALS, Emory UniversityThis book provides a practically useful integrationof descriptive fact and unifying theory at the ad-vanced level of organic chemistry. Discussions ofmechanisms and the applications of organic reac-tions to synthesis and degradation are not sep-arated; every effort is made to relate mechanisticconsiderations to the practical problems of syn-thesis and analysis.6" x 9" * 858 pages * February 1954

INTRODUCTION TOEXPERIMENTAL PHYSICSby WILLIAM B. FRETTER, University of Cali-

fornia, BerkeleyThis text presents for the first time a countlessnumber of small but invaluable details of tech-niques not found in texts, references, or journals.The procedures themselves have never before beenavailable except from widely diverse sources.

It is an authoritative description of various pro-cedures in current use in experimental physicsincluding numerous techniques common to mostexperiments in modern physics. The emphasis ison those procedures developed in recent years andparticular attention is given to atomic and nuclearphysics techniques. Particle detectors are discussedin some detail with comparative advantages givenand the various types of particle accelerators arediscussed.352 pages * 6" x 9" 0 January 1954

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Page 3: Kodak reports laboratories - Science...your own in photography through the microscope, don't hesitate to write him about them. His address: Eastman Kodak Company, Industrial Photo-graphic

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O NUCLEAR PHYSICS by Werner Heisenberg. This new work, by one of theoutstanding physicists of our time, begins with a short and fascinating historyof the views about atoms in antiquity and also of the development of atomictheory. With 18 halftone Illustrations and 32 line illustrations. $4.75

O ESSAYS IN SCIENCE by Albert Einstein. The world of science as thedistinguished physicist sees it. Abridged. $S2.75

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o HARWELL This book presents the first connected story to be published ofthe work and problems of the British Atomic Energy Research Establishment.Harwell, from its inception in 1946 until the end of 1951. $3.75

O ENCYCLOPEDIA OF ATOMIC ENERGY by Frank Gaynor. More than 2,000entries defining and explaining concepts and terms in nuclear physics andatomic energy makes this volume a vital handbook for all those concernedwith atomic science. Illustrations, charts, tables. $7.50

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O THE ATOM STORY by J. G. Feinberg. The first complete and balanced bookon the atom in the language of the layman. Hitherto, books on the subjectintended for the ordinary reader have largely stressed one phase of nuclearenergy: the bomb. Dr. Feinberg does, of course, discuss the bomb, past andfuture, In its fullest detail; but places it In its proper perspective In relationshipto the complete atomic picture. $4.75

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Page 4: Kodak reports laboratories - Science...your own in photography through the microscope, don't hesitate to write him about them. His address: Eastman Kodak Company, Industrial Photo-graphic

Jlltronomer3 - P4sici3L - teclronic (Znjineer3

ASTRONOMICAL PHOTOELECTRIC PHOTOMETRYEdited by

Frank Bradshaw WoodFlower and Cook Observatories, University of Pennsylvania

6 x 9 inches, 141 pages, 40 illustrations, clothboundPrice $3.75 Special price to AAAS members $3.25

The papers in this symposium, presented in somewhat abbreviated form at the AAAS Meeting inPhiladelphia, will help those wishing to enter this field, especially in the design and construction ofequipment. The material-and the bibliography included with the first paper-will also prove invaluableto those actively working in the field. Although the number of contributors is limited, the papers coverdevelopments around the world.

Dr. Linnell, who covers direct current techniques, constructed a photoelectric photometer still in useat the Boyden station in South Africa, and while at Harvard used this in the study of the faint and'un-usual eclipsing variable, UX Ursae Majoris. His present work involves the development of techniquesusing subminiature tubes.

Dr. Hall-alternating current techniques-is co-discoverer of the phenomenon of the polarization ofthe light of certain stars, and was the first astronomer to demonstrate the value of refrigeration of photo-cells.

Dr. Blitzstein constructed the first pulse-counting photometer for astronomical use and applied it tothe observation of eclipsing variables.

Although Dr. Bengt Stromgren of the Yerkes and McDonald Observatories reviewed foreign devel-opments at the Philadelphia meeting, this volume includes papers written by MM. Lellemand and Len-ouvel on work at the Observatoire de Haute Provence and by R. 0. Redman, Director, and G. G.Yates of the Observatory at Cambridge University.

Dr. Walraven of Leiden describes the work with servomechanisms carried out by him at the UnionObservatory in Johannesburg.

Dr. Whitford, who supplies the critical summary and evaluation of future developments, has beenconsidered an outstanding authority in this field for many years. His introduction of the constant deflec-tion method using electrometer tube techniques marked a major advance.

TABLE OF CONTENTSThe Use of Direct-Current Techniques in Photoelectric Photometry of Stars-Albert P. Linnell, Amherst CollegeObservatory-i. Alternating-Current Techniques and Sources of Error in Photoelectric Photometry of Stars-JohnS. Hall, The Equatorial Section of the U. S. Naval Observatory1-4. The Use of Pulse-Counting Techniques inPhotoelectric Photometry of Stars-William Blitzstein, Flower and Cook Observatories, University of Pennsyl-vania-64. Photoelectric Installation of the Observatoire de Haute Provence, A. Lallemand, Observatoire de Paris-88. Photoelectric Installation at the Observatoire de Haute Provence, F. Lenouvel, Observatoire de HauteProvepce, St. Michel, Bas$es Alpes, Fvancq-.89 Th4e PWrfopnance of TwQ Pulse-CousAting Stellar Photometers,R. 0. Redman and G. G. Yates, Cambridge University Observatory-93. On the Use of Servomechanisms in Photo-electric Photometry of Stars, Th. Walraven, Leiden Observatory, Southemn Station, Johannesburg-114. Limits ofSensitivity and Precision Attainable by Photoelectric Methods, Critical Sunmmary and Comparison of Varioug Tech-niques, A. E. Whitford, Washburn Observatory, University of Wisconsjn-126.

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14A SCIENCE, Vol. 119

Page 5: Kodak reports laboratories - Science...your own in photography through the microscope, don't hesitate to write him about them. His address: Eastman Kodak Company, Industrial Photo-graphic

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Page 6: Kodak reports laboratories - Science...your own in photography through the microscope, don't hesitate to write him about them. His address: Eastman Kodak Company, Industrial Photo-graphic

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|SIMtlIBIIIH POSITIONSWNTE IIISIIIIjHI$jjIMIIIIIHIIRIIBacteriologist, Ph.D., employed in large metropolitan area desiresacademic appointment in smaller city. Box 40, SCIENCE. X

Bacteriologist: Ph.D. 434 years Assistant Professor, MedicalSchool. Clinical laboratory and industrial experience. Publications.Desires academic or industrial position. Available after June 30.Box 70, SCIENCE. X

Biochemist-Physiologist, Ph.D. five years teaching experiencein biochemistry, physiology, endocrinology. Assistant professor.Research experience endocrine control enzyme activity, cellularbiochemistry, isotopes (A.E.C. fellowships). Desire position withopportunity for research. Woman, 36. Box 72, SCIENCE. X

Biologist, M.A.; Genetics, embryology, physiology. Research ex-perience: genetics, embryological histochemistry. AvailableSeptember 1954, prefer north central states, teaching, research orboth. Box 67, SCIENCE. 3/19

Botanist; Ph.D. 7 years teaching plant physiology, biology, bio-chemistry, radioactive tracers; publications; desires teaching orresearch; Midwest. Box 64, SCIENCE. X

Biophysicist; Ph.D. '52. Presently engaged by university in fulltime research capacity, desires teaching position with time forresearch and possibility of permanency. Willing to organize bio-physical curriculum. Box 62, SCIENCE. X

Field biology: botany, ecology, soils, science education, phyto-pathology. Ph.D. Box 57, SCIENCE. X

Microbiologist-Chemist. Ph.D. 1950. Training in enzyme chem-istry, vitamin and cofactor studies, bacterial metabolism, chroma-tography. Interested in academic or industrial position with re-search opportunities. Age 30, Married. Box 65, SCIENCE. X

Plant research desired, teaching considered. Possess M.S. withtraining in botany, bacteriology, genetics, chemistry, and elec-tronics. Box 63, SCIENCE. X

Pharmacologist: Ph.D. Two years industrial experience. Desiresresearch and/or teaching position in pharmacology, toxicology, ornutrition. Box 68, SCIENCE. X

(a) Pharmacologist; Ph.D.; now engaged in post-doctoral re-search; university medical school; interested in position involvingresearch in pharmacology, teaching or industrial institution. (b)Bacteriologist; M.S.; four years, chief bacteriologist, pharmaceuti-cal company; three years, research bacteriologist, university medicalschool. Science department, Medical Bureau (Burneice Larson,Director) Palmolive Building, Chicago. X

Physiologist-PhD. June 1954. Experienced psychophysiologicalresearch; background endocrinology, pharmacology; publications.Desires academic position. Box 71, SCIENCE. X

Virologist: Ph.D. extensive research experience all phases of tissueculture, virus diseases of humans and domestic animals, desiresresponsible position industry or university; any locality. Box 73,SCIENCE. X

Virologist-background in bacteriology and immunology, M.S.with 3 years graduate work plus 3 years research experience. Ex-cellent references. Box 66, SCIENCE. X

18A

tllllHllllllllllllllllllPOSITIONS OPEN ||||||||llllllllllIII

ANNOUNCEMENTThe ELECTRON MICROSCOPESOCIETY OF AMERICA'S

FREEPLACEMENT SERVICE

for Electron Microscopists and EmployersSociety Placement Officer-Dr. John H. L. Watson

Edsel B. Ford Institute for Medical Research2799 lVest Grand Blvd., Detroit 2, Michigan

Biochemist, Ph.D.; administrative ability, to head new depart-ment; pharmaceutical research laboratories Midwest. Please writeScientific Personnel Service, 122 South Michigan Ave., Chicago. X

(a) Chemist; research position with medical school department ofobstetrics-gynecology; Ph.D. or M.S. (b) Chief statistician andadministrative officer; bureau of public health statistics; outsideU. S.; $6400-$7400. (c) Fellow in pediatric allergy; physicianwith year or two training in pediatrics, particularly interestedbasic research and allergy or Ph.D. with similar interests; largeteaching hospitaL (d) Pharmacologist; experienced anticonvulsants,hypotensive drugs, anticholinergics; M.D. preferred, Ph.D. eligible;duties: testing new drugs; capable organizer required; $10,000.(e) Physician to serve as director of clinical research: senior ap-pointment; pharmaceutical company: East. S3-2 Science Depart-ment, Medical Bureau (Burneice Larson, Director) PalmoliveBuilding, Chicago. X

Instructor to teach general biology, plant morphology, economicbotany and mycology; Ph.D. required, salary $4250.00 for 9months and $1,000 additional for fourth quarter after first year;active research interest desired; opening at small western univer-sity. Box 69, SCIENCE. 3/26; 4/9

C4emI*/

Openings exist in the Vermont1 49mtlt~ State Department of Health for

graduate biologist and chemist.Experience of one year or Master's degree preferred butnot required. Liberal personnel policies, including excel-lent retirement plan. Write to Personnel Officer, Depart-ment of Health, 115 Colchester Ave., Burlington, Vt.

COLLEGE OF ARTS AND SCIENCEBAGHDAD, IRAQ.

Applications are invited for appointments as pro-fesser, or assistant professor in the Department ofPhysics. The stipends will depend upon the rankand qualifications of appointees. (From ID 1800to 3000 per annum plus living allowance of ID. 164per annum and transportation for two persons.ID. 1 is equivalent to $2.80). Full particulars maybe obtained from Dean A. A. Duri, College of Artsand Science, Baghdad, Iraq. (Send applications byair mail).

Graduate assistantships in teaching and research available in Sep-tember, 1954. Load 12 or 6 hours per week. Remainder of timeavailable for graduate work leading to master's degree. Stipendsrange from $550.00 to $1900.00. Chemistry Department, HowardUniversity, Washington 1 D. C. 3/12

$1800 stipend for 12 months beginning early June for qualifiedgraduate student. All work in reproductive physiology and behaviorwould count toward Ph.D. in Anatomy or Psychology. Communi-cate William C. Young, University of Kansas. 3/X2. 19

SCIENCE, Vol. 119

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