jej entered - hwbdocuments.env.nm.gov chemical...jun 08, 2017 · final determination was that the...

... '

' JEJ ENTERED

June 8, 2017

John E. Kieling

Chief, Hazardous Waste Bureau New Mexico Environment Department

2905 Rodeo Park Drive East, Building 1

Santa Fe, NM 87505

RE: Response to NMED's Letter dated 5/15/17

Dear Mr. Kiellng:

Advanced Chemical Treatment, Inc. (ACTreatment) EPA ID# NMD002208627 would like to respond to the request for additional information in the letter dated June 15, 2017 regarding the release of hazardous waste that occurred on March 9, 2017.

1. Identify the exact location of the spill. Include:

a. If the spill was located within a trailer, The initial spill was within the trailer that held two 55-gallon metal drums.

b. If the spill was contained by the trailer or if any contamination occurred outside the trailer, Liquid material did leak from the bottom of the trailer as well as the trailer door. The material had spilled onto the asphalt of the parking area and pooled in the collection sump located in front of dock 2.

c. If the spill was confined to the trailer, provide an explanation for the samples taken Sampling was conducted in the asphalt, but not within the trailer after the spill clean-up was complete. Samples were taken at 4/t., 25 ft., and 48ft. from the dock each at a depth of 2.5 inches and 6 inches respectively.

2. Include a map clearly showing the location of the spill as well as the sampling locations. Please refer to Appendix A for a map that indicates the sampling locations and location of the spill.

3. The incident report lists the material spilled as 0002 but the manifest lists both 0002 and 0004. Identify all constituents and applicable RCRA codes associated with the spill.

Two containers from Line item 1 from the manifest leaked in the trailer and does have an EPA waste code of both 0002 & 0004. Total constituents from the profile include:

Activated carbon {20-59%) Arsenic (1-5%) Phospine (0-1%) Phosphorus (1-5% Water (30%)

Please refer to Appendix B for a copy of the manifest and waste profile sheet

4. Identify the cause of the container leak and how long the container was at the facility before the leak was discovered. The 55-gaf/on poly lined metal drums had an additional poly insert, but had degraded. Final determination was that the materials were being added to the drums with an elevated temperature causing the drum liners to degrade and leak. The trailer was accepted for processing the afternoon of March 7, 2017 and partial process of the trailer was conducted on March 8th, 2017. The spill was identified prior to the start of the business day March 9th, 2017. No external leaking of containers or presence of spillage was noticed on March gth, 2017. The first indication of a spill was noticed by an employee while opening the warehouse up for the day on the morning of March 9, 2017@ 705 AM.

s. Fully describe how and where this waste was managed and disposed. Note that this waste and any associated wash water must be included in the Facility's waste generation volume.

The leaking containers were immediately pulled from the trailer and over packed by our warehouse technicians. Spill containment procedures were conducted and all recovered materials were containerized, labeled (as ACT Treatment as the generator), and marked. The remaining 10 drums on line item 1 were also over packed and sent to an alternate facility for disposal. The waste and associated clean-up materials were manifest as ACT Treatment and will be counted against our generator volume.

6. Include the laboratory chemical analyses conducted on the samples and the rationale for the selected

analyses.

Refer to Appendix C for a copy of the analytical report from Hall Environmental. The rational for the selected analyses is EPA Method 6010B: TCLP Metals to check for elevated arsenic levels and SM4500-H+B: PH to check for any abnormal pH levels.

7. The incident report indicates that 7 to 10 gallons leaked from a drum; however, the volume recovered was not included. Include the total recovered volume.

The total recovered volume of materials was estimated to be between 6-7 gallons plus debris and materials generated during the spill response and clean up phases. All spill material was placed into the over packs with the drums that were sent to an alternate facility for disposal.

If N MED requires further information please contact myself or Krista Harsono at 619-571-5737 or [email protected] and I will respond in a timely manner.

e rey Smith

General Manager

Advanced Chemical Treatment

Enclosures

cc: P. Paduano, Advanced Chemical Transport/Treatment

K. Harsono, Advanced Chemical Transport/Treatment

'

Appendix A

Mop that indicates the sampling locations and location of the spill

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0 Sample tocations 4, 25, and 48 feet from Dock 2

.-Spill Pattern Locations

L.---·--- -- -- ··-··-··-··--·-·---·-··---- .-L·--··-··-·

Facility Evacuation Routes Advanced Chetnica\ Treatment

6137 Edith Blvd. NE Albuquerque, NM 87107

October 1011\. 2014

Scale: 1 inch equals 50 feet

100 •

ES=Emergency Shower F•Fire Extinguisher SP=Spill Kil pS.iP•Jll Station FA=First Aid Kit

P'imary ::."acua11on Roule

Secondary :::'.vti.cuat;on Route

N

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Appendix B

Hazardous Waste Manifest & Waste Profile Sheet

Please print or tvoe. IFonn de&l!lfled b' use on elite (12-pitdt) twewriter.I Form Approved. OMB No. 2060-0039 . UNIFORMw··~.....,,., 1~w,.rlDNumbar 12. Pr t of 13. ~enB'o,~ePhone . ra·cr9crb59s s FLE · WASTE MAM!FEST . ••·•• 000002816 -620-6842

·- - treGIES CORP. ll'tneralor'l lllll Md11111 l"""''mit man ,,_ng lllllllell/

10420 RESEARCH ROAD SE ALBUQUE'i!;U~~~l123 01111eralofa Phone: I

I IL Transporttr 1 !)Om~~me · AcMin'Cled C real Transport Inc. (SV) u.e. EPA 11 Num1r CAR00007Q540

I . 7. Tl'lnaporter 2 Company Name U.S.EPAIDNumber

I a. ...... ..... n~. 1 ..,.mrent U.S. EPA ID Nunar

6133 Ecliih Blvd NE NMD002:208627 Albuquerque, NM 87107 FadW '1 PhojOS-349-5220 I 9e. Sb. U.S. DOT Oescriplloll (Including Prcpar Shipping Name, Hawd Class, ID Nwnller, 10. CClnlain«I 11. Total 12. llnll 13. Waste Code1 HM and Packing Group !If anvil No. Type Quandl'J WlMll.

'tit.Ii-· --. vva111e c;orrO&tve 11qu1as, lOXIC, n.o.s. OM p LIW-' ..,.,., .. ~x (ARSENIC, PHOSPHOROUS), 8 (6.1). PGll (0002)

I f.. S''l'10 ~ w iii x rn:~. '""'~ft, n;u:araous warsre, SOiia, n.o.s. , ... ·--· ·-

' DF p LJW4

<:I CONTAMINATED PPE), g I PGlll (0004) ~I

3.

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14. Sp11e11IHBndlnghtm1C11on11ngl\llllftlU/1l.I. W ~ ,.

1) ERG#154; RC8077 BOA- 11.- . reject Number 120446 Dacument#: 0143015 2)ERG#171; RC8078 SOA- l, l) Q.f .SS" EMERGENCY CdNTACT: HENRY ROMERO 0 5)5..620-6642 15. GENERATOll'l/OFFEftOR'I CERTIFICATION: I herabydlClant lhatlhe conlen1s of Ihle ~menh.re illy and aoo11111et/ desclilacllbow by the proper shW!ng lllllt. and are Cll11181ftld, piickagad,

m•ked 11d labellll/placald8if, and are In all l8llllllls In PKJP81' oondllon forlrnporl 8'lll0rdin9 ID appllaablt 111111maftonal anonlllonil ~owmmental reaulaGolls. If export shlp111entand I am the Plitnery l:xpmtar, I certify ltllt the C011t1n11 of Ihle can11Qnmtnl oonform ID tie lilHTB al !hi tUached EPAAl:knal.4adg111nt of Conunt. I ulltlfy 1hal Iha wa1t11 m!nlmlzation ltalamant ldantllad ln 40 CFR 282.27(1) {It I em a largelJUlnllly ____ -· (It) (II I am umall !lllll'lllW.tl1neratol)ls lrut. ~·

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Ii= ITranapor!er 1 PrinllC111YPem NlllllB rJ ~n11111n1 ll'!UIJll I.MY Year

~ J1uJam11 - ..... I \ a..-..J (J A-Mo. 101.1°" !Ji :f Tran8f1c~ar z rn111e1111yp1(1 NBrne \ ·- I a91( r l'IJQtllll lllY 1Blll'

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r ··--1aa. oracrapancy lndlcallan Space D Qiardlly 0Type 0Resldue 0Part1al Rejection ~FulReiec:t!on Mllllht Rellllence fUnber.

j!: 19b.A!temrllllF)f!'!arGan~r) S7' II 'fS"' f( M I-LS $ 'g~ UAEFA.lll~mbei ~VT!!OOIOOOO d US.~ 11'"' .&.~ > "'" · I l •

~ FecllhhPhooa: .,.,~\ '1~1 .. I,,.. "7t1t. I ~ 18c. l!lgllatureolAltarnatnaGllly'l'Jl'GllMIKll'J . 1¥1Dll!ll Day veer

~ I I I ! 19. Halllldooa waste Report MlllSgement Metkod Clldaa O.t., codn for ham!aus wa•te lrelJlmanl, d&ijma~ ind recyding •Y11tlme)

!t r r. ,~ l "_, ......... ,,,_..._. ______ .. ____ , ..... P11ntaa1 rtJlllO Name :11111111ure 1VIOHll1 Dey Y11r

I I I I EPA form 8700·22 (Rev. 3-115) Previous edHloos are obsclale. DESIGNATED FACILITY TO DESTINATION STATE (If REQUIRED)

6133 Edith Blvd. NE Albuquerque, NM 87107 Phone: (505) 349-5220 Fax: (505) 344-7986

A. GENERATORlllFORMATION G.n1rat01 Neme: MllllllQ Addr-:

Site Pick-up Addraee;

SOLAERO TECHNOLOGIES CORP. 10420 RESEARCH ROAD SE ALBUQUERQUE, NM87123 1D420 RESEARCH ROAD SE ALBUQUERQUE, NM 87123

GENERATOR WASTE PROFILE SHEET

Profile Number: RC8077 Gen1rator US EPA IC: NMR000002816

Phone: 505·250.8288 Fax:

Emalt

Tec;twi!cal Ccnlact: HENRY ROr.IERO 1111&: Ml\IN CONTACT Name of Waste Proeass Generating

1'GA CARBON-ARSENIC WASTE • DO NOT RECERTIFY PER JAS REMOVAL OF CARBON FROM TO.lQC GAS ABSORBERS

NAICS CODE: 334413 Form Code :W002

B. PHYSICAL CHARACTEIU8TICS OFWASTEAT 25C OF77F

Physical State: SLUDGE I S Color: BLACK Clarity: CLEAR

Source Code: G13

Phase Separation MULTI Odor: NONE Number of L.fiyers:

PH: 1 - 7 Specific 1 • 1.2 SP.GR. Gravity:

Flash Point > 200 F (F):

BTU Value: 100- 500 B1U/LB

C. Chem lcal Com position I UHC's Range

BASED UPON: ANAL YTICAL(INCLUD!D) D GENERATOR KNOWLEDGE 00 D. MEfALS Total(PPM) EP Toxicity (mg/I)

ACTIVAlEO CARBON 20 - 59 % ARSENIC 1 - 5 % PHOSPHINE 0 . 1 o/1 PHOSPHOROUS ,......_,SPHOR1C ACID! 1 • 5 % WATER 30 - 30 %

F. Shipping Information:

YEB Exempted NO DOT Hamrdous r.taterial

Proper Shipping NS11e:

HamrdCIHe: 8 ID#: UN2922 PG; II

RQ, UN2!122, Waste Corrosive lquids, toxic, n.o.s. (ARSENIC, PHOSPHOROUS}, 8 (6.1 ), PGll (0002)

Anticipated Volume (Unls): 32 OM

Per: MONTH

0. &peclll lflndllng Instructions:

STABILIZAilON

H. GENERATOR'S CER11FICATION:

"590 MG/L. Arseolc: < 100 M01L. Barlurn:

< .5 MG/L. Cedmium: < 5 MGIL Chromium: < 15 MGl'L !Aid:

< .2 MGJl Ml!wry:

< 5 MG/L SI~ er: < MGIL Copper: < MGIL Nlckel: < MGIL Zinc: < MGIL 1l11Elum:

,. MG/L Chromium, Hexavalent < 1 MG.IL Selenium:

E OTHER COM PONEffl'S O>GDIZER: N Elf'LOSIVE: N SHOCK SENSITIVE: N 11RES: N PYROPHORIC: N RADIOAC11VE: N E><EMPT RAD: N EnilOLOGICAL: N

REAC11VE SULFIDES PPM N REAC11VE CV ANIOES PPM N WA1=R/AIR REAC11VE Y THERMALLY UNSTABLE N 1SCA REG PCB WASTE: N COMPRESSED GASSES: N CERCLAISUPERFUND; N PESTICIDE l\WJtJFAClURING WASTE: N

HALOGENATI:O ORGANIC COMPOUNDS PER 411 CPR 2158, APPENDIX 111 DEE!RIS N <500 PPM VOC 1111 generated NO

Subject to NESH.AP Regulallcns us EPA Hmardous Waste y

US EPA Hamrdoua Wasle Codes:

; DOOl2,0004

I h1reby certify that 1111 Information In thll 111d 1111 the attached documents la complete and accurate, and lhat all kl\CIMI or suspected hamrds have been disclosed. I lunhsr certify that eny samplas submitted wih this prollle are l'll!l'llSBntetiveof the waate to be shipped and n taken In accordance with SW 8411 er other approved proceds1111. I agree to notify Advanced Chemical Treatment In 'Mltlng Wien the process genaratlng thle waato tlraam changes or v.llen I have reason lo bellev e the data contained her&ln Is not complete .id accurate.

Tiiie. ___________ _ Date. ____ _

Appendix C

Analytical Report from Hall Environmental

HALL ENVIRONMENTAL ANALYSIS LABORATORY

March 15, 2017

Kris Gwash

Advanced Chemical Transport Alb 6137 Edith Blvd NE

Albuquerque, NM 87107 TEL: (719) 466-9328

FAX

RE: T I 097 Leak

Dear Kris Gwash:

Hall Environmental Analysis Laboratory

490 I Hawkins NE Albuquerque, NM 87109

TEL: 505-345-3975 FAX. 505-345-4107 Website: www.hallenvironmental.com

OrderNo.: 1703483

Hall Environmental Analysis Laboratory received 6 sample(s) on 3/9/2017 for the analyses presented in the following report.

These were analyzed according to EPA procedures or equivalent. To access our accredited tests please go to www.hallenvironmental.com or the state specific web sites. In order to properly interpret your results it is imperative that you review this report in its entirety. See the sample checklist and/or the Chain of Custody for information regarding the sample receipt temperature and preservation. Data qualifiers or a narrative will be provided if the sample analysis or analytical quality control parameters require a flag. When necessary, data qualifers are provided on both the sample analysis report and the QC summary report, both sections should be reviewed. All samples are reported, as received, unless otherwise indicated. Lab measurement of analytes considered field parameters that require analysis within 15 minutes of sampling such as pH and residual chlorine are qualified as being analyzed outside of the recommended holding time.

Please don't hesitate to contact HEAL for any additional information or clarifications.

ADHS Cert #AZ0682 -- NMED-DWB Cert #NM9425 -- NMED-Micro Cert #NMO 190

Sincerely,

~·

Andy Freeman

Laboratory Manager

4901 Hawkins NE Albuquerque, NM 87109

Analytical Report

Lab Order 1703483

Hall Environmental Analysis Laboratory, Inc. Date Reported: 311512011

CLIENT: Advanced Chemical Transport Alb Client Sample ID: 2.5-1 (Dock)

Project: T 1097 Leak Collection Date: 3/9/2017 11 :30:00 AM

Lab ID: 1703483-001 Matrix: SOIL Received Date: 3/9/2017 12:06:00 PM

Analyses Result PQL Qua I Units DF Date Analyzed Batch

MERCURY, TCLP Analyst: pmf

Mercury ND 0.020 mg IL 3/14/2017 2:21 :08 PM 30661

EPA METHOD 60108: TCLP METALS Analyst: pmf

Arsenic ND 5.0 mg/I.. 3/13/201711:21:11 PM 30640 Barium ND 100 mg/I.. 3/13/2017 11 :21 :11 PM 30640

Cadmium ND 1.0 mg/I.. 3113/2017 11 :21 :11 PM 30640

Chromium ND 5.0 mg/L 3/13/201711:21:11 PM 30640

Lead ND 5.0 mg/L 3/13/201711 :21:11 PM 30640

Selenium ND 1.0 mg/L 3/13/201711:21:11 PM 30640

Silver ND 5.0 mg/L 3/13/2017 11 :21 :11 PM 30640

SM4500-H+B:. PH Analyst: JRR

pH 7.34 pH Units 3/13/2017 3:31:00 PM R41334

Refer to the QC Summary report and sample login checklist for flagged QC data and preservation information.

Qualifiers: Value exceeds Maximum Contaminant Level. B Analyte detected in the associated Method Blank

D Sample Diluted Due to Matrix E Value above quantitation range

H Holding times for preparation or analysis exceeded J Analyte detected below quantitation limits Page 1 of Io ND Not Detected at the Reporting Limit p Sample pH Not In Range

R RPD outside accepted recovery limits RL Reporting Det.ection Limit

s % Recovery outside of range due to dilution or matrix w Sample container temperature is out of limit as specified

Analytical Report

Lab Order 1703483

Hall Environmental Analysis Laboratory, Inc. Date Reported: 311s12011

CLIENT: Advanced Chemical Transport Alb Client Sample ID: 6-1 (Dock)

Project: T l 097 Leak Collection Date: 3/9/2017 11 :30:00 AM




Mercury ND 0.020 mg/L 3/1412017 2:22:54 PM 30661

EPA METHOD 60108: TCLP METALS Analyst pmf

Arsenic ND 5.0 mg IL 3/13/2017 11 :36:23 PM 30640 Barium ND 100 mgll 3/13/201711:36:23 PM 30640

Cadmium ND 1.0 mg/L 3/131201711:36:23 PM 30640 Chromium ND 5.0 mg/L 31131201711:36:23 PM 30640

Lead ND 5.0 mg/L 3113/2017 11 :36:23 PM 30640 Selenium ND 1.0 mg/L 3/1312017 11 :36:23 PM 30640

Silver ND 5.0 mg/L 3/13/2017 11 :36:23 PM 30640

SM4500-H+B: PH Analyst: JRR

pH 8.11 pH Units 311312017 3:31 :00 PM R41334

Refer to the QC Summary report and sample login checklist for flagged QC data and preservation infonnation.



H Holding times for preparation or analysis exceeded J Analyte detected below quantitation limits Page 2 of Io ND Not Detected at the Reporting Limit p Sample pH Not In Range

R RPO outside accepted recovery limits RL Reporting Detection Limit


Analytical Report Lab Order 1703483

Hall Environmental Analysis Laboratory, Inc. Date Reported: 311sr2011

CLIENT: Advanced Chemical Transport Alb Client Sample ID: 2.5-2 (Middle)

Project: T 1097 Leak Collection Date: 3/9/2017 11:30:00 AM


Analyses Result PQL Qual Units DF Date Analyzed Batch


Mercury ND 0.020 mg/L 3/14/2017 2:28:13 PM 30661


Arsenic ND 5.0 mg/L 3/13/201711:38:06 PM 30640 Barium ND 100 mg/L 3/13/2017 11 :38:06 PM 30640 Cadmium ND 1.0 mg/L 3/13/2017 11 :38:06 PM 30640

Chromium ND 5.0 mg/L 3/13/201711:38:06 PM 30640 Lead ND 5.0 mg/L 3/13/2017 11 :38:06 PM 30640 Selenium ND 1.0 mg/L 3/13/2017 11 :38:06 PM 30640

Silver ND 5.0 mg/L 3/13/2017 11 :38:06 PM 30640

SM4500-H+B: PH Analyst JRR

pH 7.98 pH Units 3/13/2017 3:31 :00 PM R41334




H Holding times for preparation or analysis exceeded Analyte detected below quantitation limits Page 3 of 10 ND Not Detected at the Reporting Limit p Sample pH Not Jn Range

R RPD outside accepted recovery limits RL Reporting Detection Limit

s % Recovery outside ofrange due to dilution or matrix w Sample container temperature is out of limit as specified

Analytical Report

Lab Order 1703483

Hall Environmental Analysis Laboratory, Inc. Date Reported; 311s12011

CLIENT: Advanced Chemical Transport Alb Client Sample ID: 6-2 (Middle)





Mercury ND 0.020 mg IL 3/14/2017 2:30:01 PM 30661

EPA METHOD 60108: TCLP METALS Analyst: pmf

Arsenic ND 5.0 mg/L 3114/2017 3:57: 15 PM 30640 Barium ND 100 mg/L 3/14/2017 3:57:15 PM 30640 Cadmium ND 1.0 mg IL 3/14/2017 5:01:36 PM 30620 Chromium ND 5.0 mg/L 3114/2017 3:57:15 PM 30640 Lead ND 5.0 mg/L 3/14/2017 3:57:15 PM 30640 Selenium ND 1.0 mglL 3/14/2017 3:57:15 PM 30640 Sliver ND 5.0 mg IL 3/14/2017 3:57:15 PM 30640


pH 9.13 pH Units 3/1312017 3:31:00 PM R41334




H Holding times for preparation or analysis exceeded J Analyte detected below quantitation limits Page 4 of l 0 ND Not Detected at the Reporting Limit p Sample pH Not In Range



Analytical Report Lab Order 1703483

Hall Environmental Analysis Laboratory, Inc. Date Reported: 3/1s12011

CLIENT: Advanced Chemical Transport Alb Client Sample ID: 2.5-3 (Clean)



Analyses ·Result PQL Qual Units DF Date Analyzed Batch


Mercury ND 0.020 mg/L 3/14/2017 2:31:49 PM 30661


Arsenic ND 5.0 mg/L 3/13/2017 11 :50:21 PM 30640

Barium ND 100 mg/L 3113/2017 11 :50:21 PM 30640 Cadmium ND 1.0 mg/L 3/13/201711:50:21 PM 30640

Chromium ND 5.0 mg/L 3/131201711:50:21 PM 30640 Lead ND 5.0 mg/L 3/13/2017 11:50:21 PM 30640 Selenium ND 1.0 mg/L 3/13/2017 11 :50:21 PM 30640

Silver ND 5.0 mg/L 3/131201711:50:21 PM 30640


pH 8.80 pH Units 3/13/2017 3:31:00 PM R41334

Refer to the QC Summary report and sample login checklist for flagged QC data and preservation infonnation.



H Holding times for preparation or analysis exceeded J Analyte detected below quantitation limits Page S of l O ND Not Detected at the Reporting Limit p Sample pH Not Jn Range



Analytical Report

Lab Order 1703483

Hall Environmental Analysis Laboratory, Inc. Date Reported: 3/15/2017

CLIENT: Advanced Chemical Transport Alb

Project: T l 097 Leak

Lab ID: 1703483-006 Matrix: SOIL

Analyses Result PQL

MERCURY, TCLP

Mercury ND 0.020

EPA METHOD 60108: TCLP METALS

Arsenic ND 5.0

Barium ND 100

Cadmium ND 1.0

Chromium ND 5.0

Lead ND 5.0

Selenium ND 1.0

Silver ND 5.0

SM4500-H+B: PH

pH 8.63

Client Sample ID: 6-3 (Clean)

Qua I

Collection Date: 3/9/2017 11 :30:00 AM

Received Date: 3/9/2017 12:06:00 PM

Units DF Date Analyzed Batch

Analyst: pmf

mg/L 3/14/2017 2:33:37 PM 30661

Analyst pmf

mg/L 3/13/2017 11 :52:04 PM 30640

mg/l 311312017 11 :52:04 PM 30640

rng/L 3/13/2017 11 :52:04 PM 30640

mg/L 3/13/201711 :52:04 PM 30640

mg/l 3/13/2017 11 :52:04 PM 30640

mg/L 3/13/201711:52:04 PM 30640

mg/L 3/13/2017 11 :52:04 PM 30640

Analyst: JRR

pH Units 3/13/2017 3:31:00 PM R41334




H Holding times for preparation or analysis exceeded J Analyte detected below quantitation limits Page 6 of l 0 ND Not Detected at the Reporting Limit p Sample pH Not In Range

R RPO outside accepted recovery limits RL Reporting Detection Limit


QC SUMMARY REPORT WO#: 1703483

Hall Environmental Analysis Laboratory, Inc. 15-Mar-17

Client: Advanced Chemical Transport Alb

Project: T 1097 Leak

Sample ID MB-30661 SampType: MBLK TestCode: MERCURY, TCLP

Client ID: PBW Batch ID: 30661 RunNo: 41367

Prep Dale: 3113/2017 Analysis Date: 3/14/2017 SeqNo: 1296438 Units: mg/L

Analyte Result PQL SPK value SPKRefVal %REC Lowlimit Highlimit %RPD RPDLimil Qual Mercury ND 0.020

Sample ID LCS-30661 SampType: LCS TestCode: MERCURY, TCLP

Client ID: LCSW Batch ID: 30881 RunNo: 41367

Prep Date: 311312017 Analysis Date: 3/14/2017 SeqNo: 1296439 Units: mg/L

Analyte Result POL SPKvalue SPK Ref Val l{.REC Lowlimit Hlghlimit %RPO RPDUmit Qual Mercury ND 0.020 0.005000 0 95.5 80 120

Sample ID 1703483·002AMS SampType: MS TestCode: MERCURY, TCLP

Client ID: 6·1 (Dock) Batch ID: 30661 RunNo: 41367

Prep Date: 3/13/2017 Analysis Date: 3/1412017 SeqNo: 1296442 Units: mg/L

Analyte Result PQL SPKvalue SPK Ref Val %REC Lowlimit Hlghllmit %RPO RPDLimit Qua I Mercury ND 0.020 0.005000 0 97.7 75 125

Sample ID 1703483·002AMSD SampType: MSD TestCode: MERCURY, TCLP

Client ID: 6·1 (Dock) Batch ID: 30661 RunNo: 41367


Analyte Result PQL SPK value SPKRefVal %REC Lowlimit Highlimit o/oRPD RPO Limit Qua I Mercury ND 0.020 0.005000 0 98.9 75 125 0 20

Qualifiers:

Value exceeds Maximum Contaminant Level. B Analyte detected in the associated Method Blank


H Holding times for preparation or analysis exceeded J Analyte detected below quantitation limits Page 7 of10 ND Not Detected at the Reporting Limit P Sample pH Not In Range


S % Recovery outside ofrange due to dilution or matrix W Sample container temperature is out of limit as specified




Project: T l097Leak

Sample ID MB-30640 SampType: MBLK TestCode: EPA Method 60108: TCLP Metals

Client ID: PBW Batch ID: 30640 Run No: 41345

Prep Date: 3110/2017 Analysis Date: 3113/2017 SeqNo: 1295668 Units: mgll

Analyte Result PQL SPK value SPK Ref Val %REC Lowlimit Highlimit %RPD RPDLimit Qual

Arsenic ND 5.0 Barium ND 100

Cadmium ND 1.0

Chromium ND 5.0

Lead ND 5.0

Selenium ND 1.0

Silver ND 5.0

Sample ID LCS-30640 SampType: LCS TestCode: EPA Method 6010B: TCLP Metals

Client ID: LCSW Batch ID: 30640 Run No: 41345

Prep Date: 3/1012017 Analysis Date: 3/13/2017 Seq No: 1295669 Units: mgll

Analyte Result PQL SPK value SPKRefVal %REC Lowlimit Highlimit %RPD RPDLimit Qual Arsenic ND 5.0 0.5000 0 99.7 80 120

Barium ND 100 0.5000 0 100 80 120

Cadmium ND 1.0 0.5000 0 102 80 120

Chromium NO 5.0 0.5000 0 97.7 80 120 Lead ND 5.0 0.5000 0 93.5 80 120 Selenium ND 1.0 0.5000 0 98.0 80 120 Silver ND 5.0 0.1000 0 101 80 120

Sample ID 1703483-001AMS SampType: MS TestCode: EPA Method 60108: TCLP Metals

Client ID: 2.S-1 (Dock) Batch ID: 30640 RunNo: 41345

Prep Date: 3110/2017 Analysis Date: 3'13/2017 SeqNo: 1295673 Units: mgfl

Analyte Result POL SPK value SPK Ref Val %REC Lowlimit Highlimit %RPO RPDLimit Qua I Arsenic ND 5.0 0.5000 0.02447 99.6 75 125 Barium ND 100 0.5000 0.4949 101 75 125 Cadmium ND 1.0 0.5000 0.001620 102 75 125

Chromium ND 5.0 0.5000 0.004310 94.4 75 125

Lead ND 5.0 0.5000 0 90.6 75 125

Selenium ND 1.0 0.5000 0 95.3 75 125

Silver ND 5.0 0.1000 0 100 75 125

Sample ID 1703483-001 AMSD SampType: MSD TestCode: EPA Method 60108: TCLP Metals

Client ID: 2.6-1 (Dock) Batch ID: 30640 Run No: 41345

Prep Date: 3/1012017 Analysis Date: 3113/2017 SeqNo: 1295674 Units: mglL

Analyte Result PQL SPK value SPK Ref Val %REC Lowlimit Highlimit %RPO RPDLimit Qual

Arsenic ND 5.0 0.5000 0.02447 101 75 125 0 20

Qualifiers:



H Holding times for preparation or analysis exceeded Analyte detected below quantitation limits Page 8of10 ND Not Detected at the Reporting Limit p Sample pH Not fn Range

R RJ>D outside accepted recovery limits RL Reporting Detection Limit

s % Recovery outside of range due to dilution or matrix w Sample container temperature is out oflimit as specified




Project: T 1097 Leak

Sample ID 1703483-001AMSO SampType: MSD TestCode: EPA Method 6010B: TCLP Metals

Client ID: 2.5-1 (Dock) Batch ID: 30640 RunNo: 41345


Analyte Result PQL SPKvalue SPKRefVal YoREC Lowlimil Highlimit %RPO RPDLimit Qual

Barium ND 100 0.5000 0.4949 101 75 125 0 20

Cadmum ND 1.0 0.5000 0.001620 102 75 125 0 20

Chromium ND 5.0 0.5000 0.004310 94.3 75 125 0 20

Lead ND 5.0 0.5000 0 90.8 75 125 0 20

Selenium ND 1.0 0.5000 0 95.9 75 125 0 20

Silver ND 5.0 0.1000 0 99.9 75 125 0 20

Qualifiers:



H Holding times for preparation or analysis exceeded Analyte detected below quantitation limits Page 9 oflO ND Not Detected at the Reporting Limit P Sample pH Not In Range


S % Recovery outside of range due to dilution or matrix W Sample container temperature is out of I imit as specified

QC SUMMARY REPORT Hall Environmental Analysis Laboratory, Inc.

Client:

Project:

Advanced Chemical Transport Alb

T 1097Leak

Sample ID 1703483-001ADUP SampType: DUP

Client ID: 2.5-1 (Dock) Batch ID: R41334

Prep Date: Analysis Date: 3/13/2017

TestCode: SM4500-H+B; pH

RunNo: 41334

SeqNo: 1295186 Units: pH Units

WO#:

Analyte Result PQL SPK value SPK Ref Val ¥.REC Lowlimit Highlimit %RPD RPDLimit

pH 7.40

Qualifiers:



1703483

15-Mar-17

Qua I

H Holding times for preparation or analysis exceeded J Analyte detected below quantitation limits Page 10 of l 0 ND Not Detected at the Reporting Limit P Sample pH Not In Range


S % Recovery outside ofrange due to dilution or matrix W Sample container temperature is out of limit as specified

Hall En~tronmental Ana/yJis Laboratory 4901 Hawkins NE

:-:

HALL ENVIRONMENTAL ANALYSIS LABORATORY

Albuquerque. NM a1109 Sample Log-In Check List TEL: 505-345-3975 FAX: 505-3,5-4107

Website: 1vww.hallenvironmental.com

Client Name: Advanced Chemical Tran Work Order Number: 1703483 RcptNo: 1

Received by/date:. _ ~~-· ___ (~/~----- .... ----------·· ·-·.----

Logged By: Llnd11a)J.,angln 3/9/2017 12:06:00 PM

completedBy: L1ndsayM7'g1n 3191201112:r1aPM

Reviewed By: ~-t-0-U _ ___jc~rd 'i)Cl r~-Chain of Custodv

1. Custody seals Intact on sample bottles?

2. ls Chain of Custody complete?

3. How was the sample delivered?

l:JNl.1D. 4. Was an attempt made to cool the samples?

5. Were an samples received at a temperature of >O• C to 6.o•c

Yes D Yes ~

~

Yes~

Yes 0

No D No 0

No D

No l!lJ

Not Present ~

Not Present 0

NAO

NA D Sam Plea were cgl!ected th• 11me dg and ch!lled.

6. Sa11"1>ie(s) in proper contalner(s)?

7. Sufffelent sample volume for Indicated test(s)?

8. Are samples (except VOA and ONG) properly preserved?

g_ Wes preservative added to bottles?

10. VOA 11lals have zero headspace?

11. Were any sample containers received broken?

12. Does p1pe1WOrk match bottle labels? (Note discrepancies on chain of custody)

13. Are matrices correctly identified on Chain of Custody?

14. ls It clear what analyses were requested?

15. Were all holding times able to be met? (If no, notify customer fOr authorization.}

Special Handling Of aoplicableJ

16. Was client notified of all discrepancies with this order? .----- ·--··-· ' Person Notifiad:

By Whom:

Regarding;

Cliant Instructions: :

17. Additional remarks:

18. Coolerlnf9rmation

Yes ~ No 0

Yes ~ No 0 Yes ~ No 0 Yes D No~ NA D

Yet! D No 0 No VOA Vials ~

Yes D No~ # of preserved bottles checked

Yes ~ No 0 for pH: (<2 or> 12 unius noted)

Yes ~ No 0 Adjusted?

Yes ~ NoO

Yes ~ No 0 Checked by:

Yes D No D

Date

Via: D eMall 0 Phone D Fax D In Person

i Cooler No Temp "C Condition Seal Intact Seal No Seal Date Signed By

1 25.EI Good Not Present

Pagel of I

Chain~of-Custody Record Tum-Around Time:

Client: ,.. - ..- .--.. "']'j ostandard 6Rush Project Name;

Y..tJl7 a.lf1:. NM ([ qt:7 z I Project#: Tt~ ·.

~#Jf 7 ema11 or r-axTP. &:f'IMe:eJeCTJ"Ul,@.,&!f jProject Manager;

QA/QC Package:

S'"'Standard o Level 4 (Full Validatf:on} ~

Accreditation

o NELAP 0 Other

D EDD (Type)

Date I Time: I Matrix Sample Request lD

·ao 15'.•'

"rJ' Jq

-· ~---- ····--------.--- ~

Container Type and#

...-..-

H HALL ENVJ:RONMENTAL ANALYSIS LABORATORY

www.hallen11ironmentaLcom

4901 Hawkins NE - Albuquerque, NM.87109

T~ 505:-34~915 F.ax: .505-345.41: 07

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Time I Remarks:

11 nea;!mlf)f, samples:subm.illied to.Hell Eiwironn-oe<llsl nir&; bi.> i;;ubo::n1rBCled ID cJlheo' acaalhed lalxx'alories.. Tm seNeS :as notM;e af.1hl~.poej!lbilty. Arly wb-eonl!ttlC:!Ed dl!!a will ·be elealt>] nol:llted Qll th9 ai~l eport

jej entered - hwbdocuments.env.nm.gov chemical...jun 08, 2017 · final determination was that the...

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