instrumental anal ce course outline sprinig 2012
DESCRIPTION
INSTURMTALTRANSCRIPT
United Arab Emirates University Instrumental Analysis -chem. Eng.Faculty of Science CHEM. 3707Department of Chemistry Spring Semester, 2011/2012
Course Outlines
Course Title Instrumental analysis for chemical engineering
Credit Hours 2 (1 Lecture + 1 Lab)
Teaching
Hours
1 Lecture + 3 hours Laboratory
Instructor Dr. Mohammed A. [email protected] phone # (03) 713-6136office location: building 81, 1st floor, room # 101
Course
Description
This course deals with the fundamental concept and
applications of instrumental techniques in chemical analysis.
The course covers some spectroscopic, electro analytical and
chromatographic methods of analysis.
Objectives By completing this course, the student should be able to:
1. Develop an understanding of basic principles of
instrumentation currently available.
2. use the instrumentation to solve analytical problems.
3. Develop an understanding of the potentials and
limitations of different instrumental analytical techniques.
4. Select a proper instrumental technique for a given
analytical problem.
5. Perform standard instrumental laboratory procedures.
6. Complete assigned tasks by self-reliance, discipline, and
responsibility.
Instruction
Methods
A combination of Lectures, exercises, classroom
demonstrations including videotaping, Computer programs and
Overhead transparencies will be used through out the course.
Text Book Daniel Harris “Quantitative Chemical Analysis”, 8th Edition
(2010), Freeman publishing
Reference
Books
1. Willard, H. H.; Merrit, L. Jr., Dean, J. A., and Settle, F. A., Jr.
"Instrumental Methods of Analysis", 7th edition. Wadsworrth,
1998.
2. Christian G.D. "Analytical Chemistry", 5th Edition, John Wiley,
(1994).
3- Principles of Instrumental Analysis" Skoog D. A., Holler, F. J.
and Nieman T. A. 5th edition, 1997, Saunders College
Publishing
Practical part The practical part is covered by the book titled "Chemistry
Experiments for Instrumental Methods" by Sawyer D. et al.,
John Wiley and Sons Inc. 1984, additional supplementary
materials will be provided as well.
Web Sites
Some interesting Web sites include:
www.anachem.nmu.se/jumpstation.htm
www.scimedia.com/chem-ed/analytic/ac-basic.htm
www.scimedia.com/chem-ed/courses/equil/toc.htm
www.scimedia.com/chem-ed/analytic/ac-meths.htm
www.chemweb.com
Assessments Students evaluation will be based on the following weights
Theoretical 75%
Activities (assignments, reports, exams, quizzes and classroom
interaction) 30%
Midterm Exam 15%
Final Exam 30%
Practical 25%
Reports and lab activities 15%
Final Exam 10%
Total 100%
Office Hours Sunday 12:00 – 01:00 (Maqam)
Tuesday 12:00 – 01:00 (maqam), 3:00-4:00 (Jimi)
Thursday: By previous appointment
Contents Overview
Introduction to instrumental Analysis 1 week
Chapter 18 Fundamentals of Spectrophotometry 2 weeks
Chapter 20 Spectrophotometers 1 week
Chapter 19 Applications of Spectrophotometry 1 week
Chapter 21 Atomic Spectroscopy 1 week
Chapter 15 Electrodes and Potentiometry 1 week
Chapter 17 Electroanalytical Techniques 1 week
Chapter 23 An Introduction to Analytical Separations 2 weeks
Chapter 24 Gas Chromatography 1week
Chapter 25 High-Performance Liquid Chromatography 1 week
Chapter 22 Mass spectrometry 1week
Chapter 27 Gravimetric and combustion analysis 1 week
Chapter 28 Sample Preparation 1 week
Supplementary
Material
Thermal Analysis 1 week