infralum ft - 02 ft (mid)ir spectrometer certification fourier transform spectrophotometer

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InfraLum FT - 02 InfraLum FT - 02 FT (Mid)IR Spectrometer FT (Mid)IR Spectrometer CERTIFICATION CERTIFICATION FOURIER TRANSFORM SPECTROPHOTOMETER FOURIER TRANSFORM SPECTROPHOTOMETER

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Page 1: InfraLum FT - 02 FT (Mid)IR Spectrometer CERTIFICATION FOURIER TRANSFORM SPECTROPHOTOMETER

InfraLum FT - 02InfraLum FT - 02

FT (Mid)IR SpectrometerFT (Mid)IR Spectrometer

CERTIFICATIONCERTIFICATION

FOURIER TRANSFORM SPECTROPHOTOMETERFOURIER TRANSFORM SPECTROPHOTOMETER

Page 2: InfraLum FT - 02 FT (Mid)IR Spectrometer CERTIFICATION FOURIER TRANSFORM SPECTROPHOTOMETER

DEVICE LAYOUTDEVICE LAYOUT

LightSource

Interferometer Focusing Optics

Sample Compartment

Detector

Page 3: InfraLum FT - 02 FT (Mid)IR Spectrometer CERTIFICATION FOURIER TRANSFORM SPECTROPHOTOMETER

PRINCIPLE OF PRINCIPLE OF OPERATIONOPERATION

Permanently aligned “Double Cats Eye” interferometer ensures stability and durability.

1 – Light source2 – Heat shield3-4 – Focusing spherical mirrors 5 – Diaphragm6 – “Double Cats Eye” interferometer 7 – Flat mirror8, 9,11 – Toric mirrors10 – Sample Compartment12 – Detector

Page 4: InfraLum FT - 02 FT (Mid)IR Spectrometer CERTIFICATION FOURIER TRANSFORM SPECTROPHOTOMETER

ADVANTAGEADVANTAGESS

high throughput

high photometric accuracy

high selectivity

simultaneous analysis of several components

variability of accessories

Page 5: InfraLum FT - 02 FT (Mid)IR Spectrometer CERTIFICATION FOURIER TRANSFORM SPECTROPHOTOMETER

ROUTINE MEASUREMENTROUTINE MEASUREMENT

Take a Sample

Fill a Cell

Placethe Cell

Measure

Complete a Report

Condition the Sample

Page 6: InfraLum FT - 02 FT (Mid)IR Spectrometer CERTIFICATION FOURIER TRANSFORM SPECTROPHOTOMETER

ROUTINE MEASUREMENTROUTINE MEASUREMENT

Take a Sample

Fill a Cell

Placethe Cell

Measure

Complete a Report

Condition the Sample

Page 7: InfraLum FT - 02 FT (Mid)IR Spectrometer CERTIFICATION FOURIER TRANSFORM SPECTROPHOTOMETER

ROUTINE MEASUREMENTROUTINE MEASUREMENT

Take a Sample

Fill a Cell

Placethe Cell

Measure

Complete a Report

Condition the Sample

Page 8: InfraLum FT - 02 FT (Mid)IR Spectrometer CERTIFICATION FOURIER TRANSFORM SPECTROPHOTOMETER

ROUTINE MEASUREMENTROUTINE MEASUREMENT

Take a Sample

Fill a Cell

Placethe Cell

Measure

Complete a Report

Condition the Sample

Calcium gluconate transmission spectrum

Page 9: InfraLum FT - 02 FT (Mid)IR Spectrometer CERTIFICATION FOURIER TRANSFORM SPECTROPHOTOMETER

ROUTINE MEASUREMENTROUTINE MEASUREMENT

Take a Sample

Fill a Cell

Placethe Cell

Measure

Complete a Report

Condition the Sample

Comparison with the standard spectrum

Page 10: InfraLum FT - 02 FT (Mid)IR Spectrometer CERTIFICATION FOURIER TRANSFORM SPECTROPHOTOMETER

MAIN APPLICATIONSMAIN APPLICATIONS

Functional group analysis Unknown substance identification Pharmaceuticals identification (RF

Pharmacopoeia) Oil content in water and in soil (DIN) Oil-in-water pollutant source identification

Page 11: InfraLum FT - 02 FT (Mid)IR Spectrometer CERTIFICATION FOURIER TRANSFORM SPECTROPHOTOMETER

MAIN APPLICATIONSMAIN APPLICATIONS

Environmental Monitoring Air and emission measurement Determination of water oil polluters Detection of the presence of

ozone-destructing substance Concentration of oil in water

measurement Petrochemistry Fractional composition of oils Oil-type analysis Benzene content in gasoline Octane number, cetane number

Determination of gas composition Testing the composition of polymer

films and coatings

Industry

Pharmacology Determination of the authenticity of

medicine preparations using IR reference standards

Quality control of medicine preparations using IR reference standards

Quality assurance of organic raw materials

Forensic investigations At expert laboratories for

qualitative analysis: drugs, medicine, pigments, gas and etc. sample identification

Page 12: InfraLum FT - 02 FT (Mid)IR Spectrometer CERTIFICATION FOURIER TRANSFORM SPECTROPHOTOMETER

AIR POLLUTANTS CONTROLAIR POLLUTANTS CONTROL

Pollutant Detection limit, mg/m3

Carbon monoxide 0,11

Carbon dioxide 0,034

Water 0,18

Hydrogen chloride 0,11

Ammonia 0,033

Sulfur dioxide 0,25

Multi-component analysis of typical industrial air pollutants.

Multi-pass gas cell, L = 2,1 m.

Page 13: InfraLum FT - 02 FT (Mid)IR Spectrometer CERTIFICATION FOURIER TRANSFORM SPECTROPHOTOMETER

OIL CONTENT IN WATER AND IN SOILOIL CONTENT IN WATER AND IN SOIL

DIN 38409 H18

and Certificate of validation M 01-39-2000

Measured content range: from 0.025 to 50 mg/l

Automatic calculation based on absorption peaks

2925. 2960, 3055 cm-1

Quartz cell, L = 4 cm

Page 14: InfraLum FT - 02 FT (Mid)IR Spectrometer CERTIFICATION FOURIER TRANSFORM SPECTROPHOTOMETER

OIL POLLUTANT IDENTIFICATIONOIL POLLUTANT IDENTIFICATION

Identification of oil-in-water pollution source by Department of Ecology rule No 241

Automatic calculation based on 12 absorption peaks (1600, 1375, 1310, 1170, 1030, 970, 870, 810, 770, 750, 720, 695 cm-1).

Sealed Cell, NaCl, L=0.04-0.10 mm

Page 15: InfraLum FT - 02 FT (Mid)IR Spectrometer CERTIFICATION FOURIER TRANSFORM SPECTROPHOTOMETER

HHC IDENTIFICATIONHHC IDENTIFICATION

Comparison of the measured spectrum with the prohibited halogenated hydrocarbons database using Euclidian distance.

Sample: C2F4Br2

Gas cell, KBr, L=10 cm

Page 16: InfraLum FT - 02 FT (Mid)IR Spectrometer CERTIFICATION FOURIER TRANSFORM SPECTROPHOTOMETER

PHARMACEUTICALS PHARMACEUTICALS IDENTIFICATIONIDENTIFICATION

Comparison of the measured spectrum with the RF Pharmacopoeia database using Euclidian distance.

Sample: Calcium Gluconate

Demountable cell,

Nujol Suspension.

Page 17: InfraLum FT - 02 FT (Mid)IR Spectrometer CERTIFICATION FOURIER TRANSFORM SPECTROPHOTOMETER

PERFUME RAW MATERIALS QCPERFUME RAW MATERIALS QC

4000 3000 2000 1000

100

80

60

40

20

0

Волн. число

ПропусканиеDetermination of contaminant in perfume raw materials.

Sample: CH3-(CH2)10-(CH2-CH2O)2-OSO3Na

Demountable cell, CaF2, L=0.05 cm.

Black - a standard sample

Red - a contaminated sample.

Page 18: InfraLum FT - 02 FT (Mid)IR Spectrometer CERTIFICATION FOURIER TRANSFORM SPECTROPHOTOMETER

HARDWEARHARDWEAR

Parameter Specification

Optical System Single Beam Optics

Interferometer Proprietary “Double Cats Eye” interferometer, Sealed and Desiccated

Beam Splitter Multi-layer Coated KBr plate

Light Source High Temperature Ceramic

Detector Pyroelectric (LiTaO3 or DTGS)

Scanning speed 1.6; 2; 3.2; 5 mm/sec

Page 19: InfraLum FT - 02 FT (Mid)IR Spectrometer CERTIFICATION FOURIER TRANSFORM SPECTROPHOTOMETER

HARDWEARHARDWEAR

Parameter Specification

Size 580х515х295 mm

Weight 37 kg

Power Requirements ~ 110/220 V, 50/60 Hz

Operating ConditionsTemperature: 10oC to 35oC, Humidity: Below 80%

Typical analysis time 60 sec

Data acquisition and processing

PC data station, Laptop

Page 20: InfraLum FT - 02 FT (Mid)IR Spectrometer CERTIFICATION FOURIER TRANSFORM SPECTROPHOTOMETER

SPECIFICATIONSSPECIFICATIONS

Parameter Specification

Spectral resolution 0.5, 1, 2, 4, 8, 16 cm-1

Spectral range 6 500 350 cm-1

Wavenumber accuracy ± 0.02 cm-1

Noise level of 100% transmission line (spectral range: 200050 cm-1; resolution: 4 cm-1)

< 0.08 %