icp test report certification packet/media/files/littelfuse/... · 2015-03-07 · 2 . table 1: list...

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1 ICP Test Report Certification Packet Company name: Littelfuse, Inc. Product Series: Ultra-low Capacitance Protection Array Product #: SP1001-xxJTG Issue Date: August 13, 2013 It is hereby certified by Littelfuse, Inc. that there is neither RoHS (EU Directive 2011/65/EU, recasting 2002/95/EC)-restricted substance nor such use, for materials to be used for unit parts, for packing/packaging materials, and for additives and the like in the manufacturing processes. In addition, it is hereby reported to you that the parts and sub-materials, the materials to be used for unit parts, the packing/packaging materials, and the additives and the like in the manufacturing processes, are all composed of the following components. Issued by: <Global EHS Engineer> (1) Parts, sub-materials and unit parts This document covers the Unidirectional TVS Array for ESD Protection RoHS-Compliant series products manufactured by Littelfuse, Inc. Raw Materials Used Please see Table 1 (2) The ICP data on all measurable substances Please see appropriate pages as identifed in Table 1 Remarks. Form 585-047 Rev. A 2/21/06

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ICP Test Report Certification Packet

Company name : Littelfuse, Inc. Product Series: Ultra-low Capacitance Protection Array Product #: SP1001-xxJTG Issue Date: August 13, 2013 It is hereby certified by Littelfuse, Inc. that there is neither RoHS (EU Directive 2011/65/EU, recasting 2002/95/EC)-restricted substance nor such use, for materials to be used for unit parts, for packing/packaging materials, and for additives and the like in the manufacturing processes. In addition, it is hereby reported to you that the parts and sub-materials, the materials to be used for unit parts, the packing/packaging materials, and the additives and the like in the manufacturing processes, are all composed of the following components.

Issued by:

<Global EHS Engineer>

(1) Parts, sub-materials and unit parts This document covers the Unidirectional TVS Array for ESD Protection RoHS-Compliant series products manufactured by Littelfuse, Inc. < Raw Materials Used

Please see Table 1 (2) The ICP data on all measurable substances Please see appropriate pages as identifed in Table 1

Remarks:.

Form 585-047 Rev. A 2/21/06

2

Table 1: List of Raw Materials covered by this report

Total Parts Raw Material Part Number Raw Material Description Page(s) 1 A194 Leadframe (A194 Alloy) 3-15 2 2200D Adhesive 16-31 3 NA IC Wafer 32-38 4 NA Gold Bonding Wire 39-51 5 EME-G600 Epoxy Molding Compound 52-60 6 Sn 100 A Tin Plating 61-70

SignaturetidForQueEtionPlease with scs

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The following sample(s)

Sample Submitted BySample DescriptionStyl€/ltqm No.Sample Receiving DateTesting Pedod

HENKEL CORPORATIONADHESIVE2200D2013t05t07201 3 | 05 I 07 1 0 201 3 | 05 | I 0

Test Rqsu[(8)

No. : CE/20'1350843 Date : 2013/05/10 Paae : 1 of 8

IRVINE. CALIFORNIA, 92606 U, S, A.

was/were submitted and identified by/on behalfofthe applicant a5 :

: Please refer to next page(s).

ReportHENKECORPORATION

A'w4)

6, dol-r.1r ts $.d b' rB co!:4 rba b BGomDrc.m mio s6acr"d ,ol s'€do rc ,o rr daulnts 3-bidb1ft3dc!iai1o$,o F4 .aja o'ts

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SCS rarvaf Lic O,t,n* tt.,a r, n t ,O r..OMdbo'd..sG€Gdp

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PART

Report No. : CE/2013s0843 Date : 2Ol3/O5/lO Pase : 2 of 8

ooRPoRATTON tm[ltlI,BOREE ROAD, IRVINE. CALIFORNIA, 92606 U. S. A.

No.1 : GRAY PASTE

T€€t lton(g) Unit Me{hod MDL ResultNo.l

CadmiLn (e) mg/Kg With reference to IEC 62321: 2008 andoerformed bv ICP-AES.

2 n.d.

Lead (PD) mg/Kg With reference to IEC 62321:2008 andperformed by ICP{ES.

2 n.d.

Mercun(Hs) mdkg With reference to IEC 62321: 2008 andperfomed by |CP4ES.

2 n.d.

Eexavaent Chromium Cr(Vl) mgikS With reference to IEC 62321 : 2008 andperformed by UV-VIS.

2 n.d.

Hexabn(HBCDIdiaster€HBCDC(cAs N55-6 (1:13237

mocyclododecaneD and all major)isomers identif ied (a-F HBoDD, y- HBCDD)

,.: 25637-99 and 319+423751-7,13423740$,52-8)

mgikg With reference to US EPA 3540Cm€thod. Analysis wEs performed byGCA{S.

5 n.d.

BBP (BNo.: 85

nzyl butyl phthalate) (CASt&7)

% With reference to EN 14372. AnalysiswEs performed by GC/MS.

0.003 n.o.

DEHP Iphthala

)i- (2-ethylhexyl)3) (CAS No.: 117-E1-7)

o With Eferenc€ to EN 14372. Analysiswas performed by GC/MS.

0.003 n.d.

DIDP (N o . : 2 6

i-isodecyl phthalate) (CAS61-4G0)

With reference to EN 14372. Analysiswas performed by GC/MS.

0.01 n.d.

DINP (No.: 28

i-isononyl phthalate) (CASi53-12-0)

% with reference to EN'14372. Analysiswas perfomed by GC/MS.

0.01 n.d.

DNOPNo.: 1 1

Di-n-ociyl phthalate) (CAS'-84-0)

% With reference to EN 14372. Analysis,ras performed by GC/MS.

0.003 n.d.

DBP (Tu-7+2

butyl phthalate) (CAS No.: with reference to EN 14372. Analysiswas perfomed by GC/MS.

0.003 n.d.

][ltrtlt

Teslt ReportHENKEL CORPORATION'14OOO JAMBOREE ROAD,

No. : CE/201350843 Date : 2013'/05/10P a g e : 3 o f 8

IRVINE. CALIFORNIA, 92606 U. S- A.lll|||[Iultutt]ll

T€6t ltem(s) Unit Mothod MDL ResultNo.l

Sum ol PBBs mg/Kg

With reference to IEC 62321: 2008 andperfomed by GC/MS.

n.d.l\ronobl'mobiphenyl mg/Kg 5 n.d.Dibrombiphenyl mg/Kg n.d.Tribrcn)biphenyl mg/K(l 5 n.d.Tetrabrmobiphenyl mg/Kg 5 n.d.Pentabl )mobiphonyl mg/Kg n.d.Hexabrmobiphenyl mg/Kg n.d.Heptab )mobiphenyl mg/Kg 5 n . d .Oclab( nobiphenyl mg/Kg 5 n . d .Nonabnmobiphenyl mg/Kg 5 n . d .Decabi mobiphenyl mg/Kg 5 n.d.Sum ol PBOEs mg/Kg n.d.Ivlonobrmodiphenyl ethe. mgKg 5 n.d.Dibromdiphenyl ether mgKg 5 n.o.Triblor rdiphenyl ether mgikgTetrabr modiphenyl ether mgftg 5 n-d.Pentabrmodiphenyl ether mg/kg n.d.Hexabrmodiphenyl ether mgftg 5 n.d.Heptab)modiphenyl ether mg/Kg 5 n.d.Octabnnodiphenyl ether mg/Kg n . d .

Nonabrmodiphenyl €ther mg/Kg 5 n . d .

Der-abrmodiphenyl €ther mg./Kg 5 n.d.

Note :1. mE/kg = ppm : O.1wt% = lOOOppm2. n.b. = Not Detected3. MPL = Method Detection Limit4. " ; " = Not Regulated

d b n i h r b r m d F d a o r N

b a l - a M d o i f t o - r . ^ r o p i d / - a a p o w s o r .c o a . b a y u a t u d , r ; , o i ' c a 4 c a B i s s o k @ . ' ' d €

SGS awan L id

M.r$4 ot rF scs Gdt

Test Report No. : CE/2013/50843 Date : 2013i/05/10 Paoe : 4 of I

HENKEL CORPORATION14OOO JAMBOREE ROAD, IRVINE, CALIFORNIA, 92606 U, S, A,

r)

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2')

These samples were dissolved totally by pre-conditioning method according to belowflowchart.( Cf* test method excluded)

Name ofthe percon who m€de me€surement: ClimbgreatYangName of the p€rgon in charg€ of mea6urement: Troy Chang

Cutling / Preparation

Add appropriate amountof digestaon rcagent

Acid digestion by suitable aciddeDended on different samolematerial (as below table)

Microwave digestion withHNO3/HCI/HF

Heat to appropriatetemperature to extract

Cool, filter digestatethrough fllter'1) Alkal iFusion

2) HClto dissolve

Add diphenyl-carbaz idefor color development

measure the absorbanceat g0 nm by Uv-vls

Samole Material Dioestion Acid

Seel, copper, aluminum, solder Aaua reqia. HNO3, HCl. HF. H,O,

Glass HNO./HF

Gold, platinum, palladium, ceramic Aqua reqiaSilver HN03

Plastic H"SO.. H"O". HNO". HCI

Others Added appropdate reagent to totaldigestion

Note" : (1) For non-metiallic material,(2) For metallic material, add

add alkaline digestion reagent and heatto 90-95t.pure water and heat to boiling.

irlLd,SlLE*tsStiE8lBst5 6 5 r , l d n L L " ' r d k t l l ! ! i r l K i \ l

sGsTest ReportHENKEL CORPORATION,14OOO JAMBOREE ROAD,

No.:CE/20'1950843Date : 2013/05/10 P a g e . 5 o f 8

IRVINE, CALIFORNIA, 92606 U. S. A

I

I

PBB/PBoE analytical FLOW CHART

Name of the pe6on who made measurement Roman WongName ofthe person in charge ofmeasuremenl Troy Chang

Scteen analysis

Filter

Analysis byGC/MS

lssue Report

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First testing prcces6 ---->

Odiona! screen Process ....

Confirmatonprocess -.>

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t . t t t . i , , . . . . . f r r , , , , r t ! i ' ' I

Sample exfactiorvSoxhlet method

Concentrate/D iluteExtracted solution

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Prk Ner:oacd,raqan/+illriSll**ffi Unfifi339ts336 102)??99 3279

Test Report No. : CE/2013/50843 Date : 2013/0y10 Page : 6 of 8

HENKEL CORPORATION14OOO JAMBOREE ROAD,

fll ]t]tfl|ltr ]

II

IRVINE, CALIFORNIA, 92606 U, S, A.

Data

Analyticalflow chart of phthalate content

Name ofthe person who made measurement Roman WongName of the person in charge of measurement Troy Chang

l l*f. '#f.x;3i-538ru*{1.'l"s"P,'.f,]:1s'1'nt.9'#*';3;;Ti:. ',q:l 'h:"-;:.,,"".;a*"^"-,-i.:"'"0.*+-.'"c.*.' i , - i , id . "ma* . *nn- " ; i ' ;d : iw iecamsh i 'o . so; ;;i;; o-s€(,rc' tu,ahbm@s,o.rd6 raiz:nndoo :6; i' dot-sdfidscn ;:";'l#i_i*1".;'i?fi.g.::a;;r; i:;'*in,i'a|'d- o'os1o shdi' m d tu€aF'o !

SGs.\!rnrld e '',? S!i;qtft',; f nr,tl dr &wra*c'q ras€i/irir!fisrt;*6&fi*l1r33t'

Concentrate/Dilute Extracted solution

Analysis was performed by GC/[4S

Test Report No. : CE/2013i/50843 Date : 2013/05/10 Page : 7 of I

HENKEL CORPORATION14OOO JAMBOREE ROAD,

HBCDD analytic.l flow chari

Name of the Derson who made mea6urement: Roman WongName of the per6on in charge of measurement Troy Chang

||J []tt][tttlllIRVINE, CALIFORNIA, 92606 U. S, A.

II

a d 6 a . ( u o n ( o n d o o a - s n 6 i d , i { l b - € m s r

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b a u i i q d o i n o m s ^ d . > m 3 r r E r; ; $ i r y ; ; u ; . f t ; d a ' ; j ' d i a i d a 3 i i o a r . 6 -Ji 6; otuni s sbrd r'. '6.8 r@

scsra,an-id r,.";,|x1{'truitr*,. i f;#%91$39r,!"iJati!!l!S3!31( *I"'3f""ljo -" *^'tr"rts"*+6gn*s"*

Sample e)draction by soxhlet method

Concentrate/Dilute Exfacted solution

SGSTest Report No. : CE/20'1350843 Date: 2013/0t10

HENKEL CORPORATION14OOO JAMBOREE ROAD. IRVINE, CALIFORNIA, 92606 U. S. A-

P a g e : 8 o f 8

' The tested sample / part b ma*ed by an afiow it ifs shown on the photo. '

|| l t]]t ||illlll

cE/2013/s0843

' " EndofReport ' t

slb€d b roe and Coid(oiero, E6dD ;bh6 ,mh$d r€b ' r r osmmarss d u $ ' do ' $ . 630dIndno rd rs r - dd E -@a ;_ !o ob | @ ' * e ' | m . € b ' . o a | f 6 .Co-rrfr A,r ,.ffho €d a €un lo

Pe( N€w Ta os c tv, ra wai / till i j$rrd+FElie$33Bf!€€6 102)2299 3?9

SignatureFor QuePlease

No. : CEi2013l50840 Date : 20 1 3/05/1 0

HENKEL CORPORATIONl4OOO JAMBOREE ROAD, IRVINE, CALIFORNIA, 92606 U. S. A.

The following sample{s} was/weJe submitted and identified by/on behalfofthe applicant as :

Test Report

Sample Submitted BySample Descriptionstyle/ltem No.Sarnple Receiving DateTesting Period

P a g e : 1 o f 4

u]l['t]]l [[l[l]!

HENKEL CORPORATIONADHESIVE22mO2013t05t072013t05n7 ro 2013n5/10

with

Test Request d

T66t Method

feat R€ault(s)

As specified by client, to test Halogen-Fluorine,the submitted samole.

Chlorine, Bromine, lodine in

: With reference to BS EN 1,1582:2007.

: Pleas€ refer to next page(s)-

d i t i$ ; im. 'omi&-m s , .0 . , . r ro -s m k d tda 'o - f sakKf f ; . l1 , : ;_*^ " . . * * . ,1 " - , . : . " . * * -

,d,&ih Eilmbid $ iry, 'd.mit€r oi €nd F dd di islss ds

r , m , b . r s , - 6 d D d ! B , j r " o . ' - \ l s c o - @ f t i t o s s : u e b ' i r c E c r € d : ! : . d o r s ' d eT b r d d ' @ d . . e ' f t - ; ; r j ' i o - n s : r ' i d r e ' e * m

F / " " . . - ' - " . .

* ' : ; ; ; ; ; ; ; i : l a ; o . ; ; 6 ; , : f ' . r o d " e ' t u o . o o " d-nb.d.ni.M!6s@rE 6.f5-hN- nf 616r'401'3r3'd\ btoe-tu{bn6

6 q+ i4 { 1 } B i '

Test ReportHENKEL CORPORATION14OOO JAMBOREE ROAD,

TeSt Regultls)

PART NAME No,l

No. : CE/201350840 Date:2013/0110

IRVINE. CALIFORNIA, 92606 U. S. A,

: GRAY PASTE

Paget 2 ol 4

|||]l||lt ||!ttn

Tost ltem(s) Unlt Method MDLR€6ultNo.l

HalogenHalogen-Fluorine (F)(C,AS No.: 14762-94-8)

msikgWith reference to BS EN'14582:2007. Analysis wasperfomed by lC.

50 n.d.

Hafogen-Chlorine (Cl)(CAS No.: 22537-15-1)

50 n.d.

Halogen-Eromine (Br)(CAS No.: 10097-32-2)

50 n.d.

Halogenlodine (l)(CAS No.: 1436244-8)

50 n.o,

Ndte :

1. mg/kg = PPmi 0.'1wt% ='1000PPm

2 n.d = Not Detected

3 MDL = Mothod Detection Limit

r o d . o l d $ n _ € d 6 r E @ { o or o 3 r i i s d o n r r . $ c a o 6 r ' M rco-prq A\ Jarho d.i@ro'. rd9.1o !Eu.nd M 6 @1d 6

ar r ts bd mFr d. m\ ro r 3 *mcae bnd

sc,c,awa,r1d e,{r.'!+1.r{!r,,,! jr.,.r | ,':dg",ocjii3&1ili,B8%Itjg5!3" }Y-':fjt:'" -

Test ReportHENKEL CORPORATION14OOO JAMBOREE ROAD.

No. : CE201350840 Dale | 201305/10

IRVINE, CALIFORNIA. 92606 U. S, A.

Analtrtical flow chart of halogen contant

Name of the person who made measurement: Rita ChenName ofthe pe6on in charge of measurement: Troy Chang

Page: 3 of 4

|l] tl] ||lltn

I

I

Sample pret€alryrent / Separation

Weighting and putting sample in cell

Orygen Bomb Combustion / Absorption

Dihlion to fixed volume

Analysis was p€rformed by lC

Ilest ReportHqNKEL CORPORATION14OOO JAMBOREE ROAD, IRVINE, CALIFORNIA, 92606 U. S. A.

No. : CEl201350840 Date : 2013/0t10 Page: 4 of 4

||]ltI]fittttll

' The tested sample/ part is marked by an arow if if3 shown on the photo.,

" End of Repod "

s0840

scs r.r ndn L,Lr ;.,,ikki+.lt!,.,,rs.,..rl f#%.,iliifj:*Y.k1B,6itl!355!!9,' ]il"'35 ,',ffit-

Signature plidForOuesionPle€se 6!t[ wjth SGSwww.tw.sal-om

trtNl tI|t ||lrrll

Test Report No. I CEl2013/50844 Date : 2013/0t10 Paoe : 1 of 4

HENKEL CORPORATION14OOO JAMBOREE ROAD, IRVINE, CALIFORNIA, 92606 U. S, A,

The following a.mple{s) was/were submitted and idontified by/on behatf of the applicant as :

Sample Submitted BySample OescdptionStyl€/ltem No.Sample Receiving DateTesling Period

HENKEL CORPORATIONADHESIVE220002013t05t072013t05t07 1 0 201 3to5t 1 0

T€€l R6ult(5) : Please refer to next page(s).

| D d r c 5 d m m 6 o l E i G r y 6 i l o ' o ' 4 f o i q { | 6 d a d i ' ! d a ' ' . ' | d @t o : l u i g d o n | s . € c ! e : | ' B r

scsriwanLd i',,{r*iill{!v,;rAr1}.r I L*'io'.1,'."3#.#1-kff,iil9!*!!31' X;"-#1,:"' " *" / sirt'o'i1r6*$Er'{ts33!r

-NW4E

Test Report No. : CE/2013/50844 Date : 2013/05/10 Paoe : 2 of 4

HENKEL CORPORATION'14OOO JAMBOREE ROAD,

Test Rosultls)

PART MME No.1

IRVINE. CALIFORNIA, 92606 U. S, A

: GRAY PASTE

|l] |||ll[tt] l

Nole :1. mg/kg = ppm ;0.1M% = 1000ppm2. n.d. = Not Detected3. MDL = Method Detection Limit4. "-"=NotRegulated

PFOS Refe.ence InfoJmation : POPS - (EU) 7572010Outlawing PFOS as substances or preparations in concentrations above 0.001% (1oppm), in semi-finishedproducts or adicles or parts at a level above 0.1%(1000ppm), in textiles or other coated matedals above 1pg/m'

T€at ltem(s) Unit Method MDLRe€ultNo.l

Perf luorooc,tane sulf onates(PFOS-Acid, Metal Salt, Amid€)

mg/Kg With reference to US EPA 3550C:2007. Analysis was perfomed byLC/MS.

1 0 n.d.

PFOA (CAS No.: 335-67-1) mg/Kg With reference to US EPA 3550C12007. Analysis wa6 performed byLC/|V]S.

'10 n.o.

' , - 4 n r 6 ,' o ' r l -

e t u F / ' s d e ' a d _r c a U a n * D ' o a . c r 6 . o iGn t il,i unidho.iad di''d o. ro'i.ry d raciEa@" d ft" *d-, -.

!ilLiELul4*LdE!1iE$&33trSCS raLwaf Ltd a t ltri u jt l{ It f rE !:;l

Test Report No. : CEl2013/50844 Date: 2013/0t10 Paoe : 3 of4

HENKEL CORPORATIONl4OOO JAMBOREE ROAD, IRVINE, CALIFORNIA, 92606 U, S. A.

lllt[ttl][]||I

PFOA/PFOS analytlcal floty cha.t of lJltrasonlc axtractlon (LC/MS) procedu.eI Name of the person who made measur€ment Roman Wongr Name ofthe person in charge of measurement Troy Chang

Sample extraclion by Ultrasonic extraction(Refe.ence method: US EPA 3550C)

b ,u i ns r , r casc t r soqa t u ' q t smo@'@roa . . o . r ' . aco@ry tu! uEfto,'od .rro,at on io,bsryd hki .bior rhaFtumora

i +38 - € r da d b d s%m063 b d

scs Tawan Lrd t,6ia*fi l{1|,} ii R r} rl

Test Report No. : C92013,/50844 Date: 20'13/0t10 Page : 4 of4

HENKEL CORPORATION14OOO JAMBOREE ROAD, IRVINE, CALIFORNIA, 92606 U. S. A,

' The testgd sample / part is marked by an arow if ifs shown on the photo, .

*' End of Report '*

tIlIttI|tt][tttt|l

t r idmi d rha t f f i d G,f t ;dd on, ad 'do;e I mie db ' uin*tr rom .src6 no a I dE o(u:6 G

-h ' dd,nd 6-nd ba 6

co@a tu' f 'sd cd rhizi on .op4 c hki 5tr oi .h6 6.6. r o' o

s6srawanLrd ec&*l+&utrurn,ral i,'.Syo"jii8Jiri!i,Bt%I*Ag:!9'lfl*'S""Lr'''"'-/s+dst*r6@nEk*x

50844

Signature tidForQuePlease with scs

om

Test Report No. : Cg201zC1068F Date:201101/18

(2) As specified by client, to test Halogen-Fluorine' Chlorine, Bromine, lodine

contents in the submitted sample.

Please refer to next page(s)

Please refer to next Page(s)

Page: 1 of 7

ul[!ll]lllllllllR. O. C.

EPISIL TECHNOLOGIES INC.HO. :, IHUOVNTIOI\I NO 1, SCIENCE BASED INDUSTRIAL PARK, HSIN'CHU. TAIWAN,

The following sanple(s) was/wete submitted and identified by/on bohelf of the client asl

Sample DescriptaonStyl€/ltem No.Sample Receiving DateTesting Pedod

IC WAFERAI PROCESS20121121O72012t 12107't o 2012t 121 18

: (1) As specified by client, with eference to RoHS Directive 201'1/65/EU Annex llto

ditermine cadmium, Lead, Mercury, Cr(vl), PBBS, PBDES contents in the

submitted sampl6.

Test Requ6tod

Test irothod

Test R€ult(s)

chr|ltcd L$otrbrt - Tratd

ffi ffi *m{#ffi lfffi ffi ,ffi #xtffi u'ffi H*,_r-..W'ffffiI , . e " r c a z * r p ' ' M t o r z r r v - r " " t " " . - - .

; ; ; " * * - -

F.rw4)

s1[d lorrrl

Test ReportEPISIL TECHNOLOGIESNO. 3, INNOVATION RD

tNc..1, SCIENCE BASED INDUSTRIAL PARK, HSIN-CHU, TAIWAN'

No. : CEi201ZC1068F Date:2013/01/18 Page,2 ol7

[ll]llltlfll |rilltR. O. C.

T.st Result{sl

PART NAME NO.1 MULTICOLOR WAFER

Te6t ltem(s) Unit Method MOLRe9ultNo.1

2 n.d.Cadmium (Cd) mg/Kg With reference to lEu bz'ztt z\No 1l

perfonned bY ICP-AES

Wiif iETerence to tEc 02321 : 2008 andperfomed by ICPdES

2 n.d.Lead (Pb) mg/kg

2 n.d.Mercury (Hg) mgKg With reference to IEU bzJz l: zuuo arN

Dedormed by ICP.AES.2 n.d,

Hexavalent Chromium Cr(Vl) mg/kg With reference to lE(; ozJzl: zuuo anuperfomed bY W-VIS

,aar""jwith reference to lEc 62321:pedormed by Gc/Ms.

n.d.Sum of PgBs n.d.MonoblomobiPhenyl n.o-DibromobiPhenyl 5 n.d.iribromobiPhenyl 5 n.d.TarabomobiPhenYl 5 n.d.FEiFtromouipnenyt 5 n,o-tri-affiftb'phen/ n.d.flauromooiptrenyt 5 n.d.-ctabromobiPhenyl 5 n.d.N6-abromobiphenyl n.d.JFbromobiphenyl n.d.sum of PBDES n.o-M-onobromodiptrenytetner 5 n.o.Dibromodiphenyl ether 5 n.d.ii6romodiphenyl ether

5 n.d.FrabromodiPhenYlether 5

5

n.d.fltabromodiphenylether n.d.FilxabromodiPtrenYtetner n.d.FEotaoromodiPnenyl etner 5 n.d.OctabromodiPhenyl ethet n.d.tbna-onabromodiPhenYlether 5 n.d.DFbromodiphenyl ether

mlffi ,m, *i'ml ",!*g$i*'wi,H*r"---=

Test Report No. : CE/20'12C1068F Date : 2013/01/18 Page: 3 of 7

EptstL TEoHNOLOGTES tNC. l[lllllllllllll llNO. 3, INNOVATION RD 1, SCIENCE BASED INDUSTRIAL PARK. HSIN-CHU, TAIWAN, R, O. C.

Teat ltem(s) Unit method MDLReaultNo.1

HalogenHalogen-Fluodne (F)(CAS No.: 14762-9+8)

mg/xg With reference to BS EN 1458212007.Analysis was pedormed by lC-

50 n-d.

Halogen€hlorine (Cl)(CAS No.: 22537-'191)

50 n.d.

Halogen-Bromine (Br)(CAS No.: 10097-32-2)

50 n.d-

Halogenlodine (l)(CAS No.: 14362-4?|€)

50 n.d.

Note :1. mg/kg = ppm ; 0.1wt% = '1000ppm

2. n.d. = Not Detected3. MDL = Method Detection Limit4 - " - "=No tRegu la ted

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Test ReportEPISIL TECHNOLOGIESNO- 3, INNOVATION RD

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tNc.1, SCIENCE BASEO INOUSTRIAL PARK,HSIN-CHU, TAIWAN, R, O.

Paget 4 ol7

tltfilfl lllllllllc.

No. : CE/2012/C1068F Date:2013i/0' l /18

TheSe samDles werc disEolved( cft test method excluded )

Name of the person who madg

totally by pre-conditioning method according to below iow chan-

measurement Climbgreat Yang

ICP-AES

Sample Ma€rial 0igestionAcid

S-teel, copper, aluminum, solder Aqua regia, HNO3, HCl, HF, HrO,

Glass HNO/HF

Gold, plallnum, Palladium, ce€mic Aqua regia

Silver HNO3

Plastic HrSOr, HrOr, HNO3, HCI

Ohers Ad-G-dEFFEpriate reagent to totaldioastion

ffi ffi gffi imffi ffi trffi ffi $ffi ffi :m"$*t:ffi :#"----.=*Note" : (1) For non_metallic material' add alkaline digestion reagent and

i2i For metallic material' add pure water and heat to boiling'heat to 90-95"C

of measurement: TroY Chang

cf.

Add appropriate amount of

digestion reagenttaid digestion by suitable aciddepended on diffe€nt samplematerial (as below table)

Heat io appropnate

tomperature to extfacl

Cool, filter digestate

through filterAlkaliFusionHClto dissolve

Add diphenyl-cabazide for

color development

at 540 nm bY uV-VlS

Test Report No. : CE/2012C1068F

EPISILTECHNOLOGIES INC.NO. 3, INNOVATION RD 1, SCIENCE

Date : 2013/01/18

BASED INOUSTRIAL PARK, HSIN-CHU' TAIWAN' R' O.

Page: 5 of 7

ll|llll$lllllll!c.

I

I

PBB/PBDE analytlcal FLOW CHART

Name of the person who macle measurement: Roman Wong

Name of the pe6on in charge of measurement: Troy Chang

First testing Process -----'

Optional screen Process "..confirmatjon process - '>

r " " " " ' : " " " " " " " " :! l screen analysis l :: r ' :i , , . . . . , , , ' . . . t . . . ' ' ' . . . . . ' r

Concentrate/DiluieExtracted solution

t

I Sample ext€ctiorv II Soxhlet method I---_T_-

Scr€en analysis

lssue Report

I Filter I

I Analy6isbyco/Ms I

ffi*gmgmw*u#mffiffi

Test Report No. : Cg2012l/Cl068F

EPISIL TECHNOLOGIES INC.NO. 3, INNOVATION RD 1, SCIENCE

Date:2013/01/18

BASED INDUSTRIAL PARK, HSIN-CHU, TAIWAN, R. O, C'

Analytlcal flow chart of halogen content

1) tSnE of the person who nEde fiEasurement Rita Chen2) NanE of the person in charge of rEasu.erEnt Troy Chang

Page: 6 of 7

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Sanple p€treatment / Sepa€tion

Weighting ard putting safiple in cell

Oxygen Bomb Conbustion / Absorption

Dilution to fixed volunE

Analysis w€6 perfonned bY lC

Test Report No. i CEi20lZClCl68F Date : 20'13/01/18 Pager 7 of 7

tm[n$ u||c.EPISIL TECHNOLOGIES INC.

ruo. i, nlovnior no 1, sctENcE BASED INDUsTRIAL PARK' HslN-cHU' TAIwAN R o'

* The tested samplo / part is mark6d by an aJrcw if ifs shown on the photo '

" 'EndofReport "-

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&m of PBXa rtlrc wtr| llh.lr|ca b IEC da'2l 2m8. drdb.rilral lw 6a-lls N.D.

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P.drb.firodlfi{.ryt aih.. mer(o wlt| rdaltrica b IEC 6232'12004. erdr.ftr.isl h, all:-lls N.O.

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H.tsalJomodM ath.r mgre wth |a d*roa to l€C 62}21 2O8, a|ldE lo.|nd b, (lc-MS N.D.

O.r.lfqrlo({phart drar mcre Wlt| rlbsE lo tEC 6A|2lfr6. ardr!..t!mrl l* Aa"tllA N.0.

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tlot : (.) mg/to . pF ; (o.lwtL. ImopomlG) N.D. . Not Dobctcrt(c) OL. i,Ldrod D.bcton Llmlt(d) I . aFi-T..rl

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r.ld|. S hat$3rl

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2) Nalt| d Ura pa|!o|l rfio mad. da.rurlrn nt Ah Chene3) Nar|l oa tl. partoi ln atiargD of neldrrrEnft f,ey Chaio

by lcP-AEs

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1) Alkdl Fu.iona Hc| b dllsoi/.

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Test Report

SGS LABOfiA'K)RY SERVICES (M) SDN. BHD.

B.So"(HONS) Ar,nCSENTOR LAB MANAGERtd.drbcldrt.rl.

No. CTSAArzdl(Byl2.K l8fl|l* lh. : 19t11/2t12 P.fp: 13 ol 13gtA n l. Ct3S^rlz|trua/T.r|d(|

fia$cd llor clrrrt ol Phthahtc co. .||t

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Adytlt ur. Farlomid ly CCi[s

Test Report No.:KA/2013/30818Date : 2013i/03i/13 Page: 1 of9

SUMITOMO BAKELITE SINGAPORE PTE CO., LTD.NO. 1 SENOKO SOUTH ROAD. SINGAPORE 758069

The following sample(s) was/werc 3ubmitted and identified by/on behatf of the ctient as :

Sample DescripljonStyl€/ltem No.Sample Receiving DateTesting PeriodSampb Submitted By

EPOXY II,IOLDING COMPOUNDEME.G6OO TYPE2013n3n72013n3n7 rO 20 13t03t13SUMITOIVIO BAKELITE SINGAPORE PTE CO., LTD.

Test Re6ult(s) Please refer lo ne{ page(s).

{ r y ' ! F d ! . q { Q i ! r ' , dii. i ;o;nd" i-.at e cmEd& d b B a.*d c-d!*' d$n]; indd o;dai;ldhde q.+e' d.@$bt *!@5 @^"a4{@!!!@ih s"d ior

ddrcnc6m'I&d.-j!-bjdloi!#aidco"db*l-e|e' 'Ddn!"rid- n.,.r ddi.d b@h byh -d--"k";ih.€s'*eb.tunFnv3tidi!6nh.roedkr€re; d-e .'M $. i my. re c.;pi," n"-* a*.-" n. a*..d;ind b GFe;.-pt h tur i

| ' , m . o J r ) L

-

W4iy\

3Emd no. .rd oo balrdfaOS Trlw.n Llmb.d

Test Report No.:KA/2013/30818 Date:2013 03/13 Page:2 of 9

SUMITOMO BAKELITE SINGAPORE PTE CO., LTD,NO, 1 SENOKO SOUTH ROAD, SINGAPORE 758069

Te3t Re3uld3l

PART NAME NO.1

Test lbm (6): Unit t ethod IIDL Result

Cadmium (Cd) m9Kg With reference to IEC 62321:2008 andperformed by ICP-AES.

2 n.d.

Lead (Pb) m(yKg With reference to IEC 62321: 2008 andperformed by ICP-AES.

2 n.d.

Mercury (Hg) m9/K9 With reference to IEC 62321 : 2008 andperfo.med by ICP-AES.

2 n.d.

HeEvalent Chromium Cr(Vl) byalkaline e{raction

ms&s with relerence lo lEc 6232'1 : 2008 andperfomed by uV-VlS.

2 n.d.

Sum of PBBs

mgKg With reference to IEC 62321: 2008 andperformed by GC/MS.

n,d,Ivlonobromobiphenyl 5 n.d.Dibromobiphenyl 5 n.d.Tribromobipheryl 5 n.d.Terabomobiphenyl 5 n.d.Pentabromobiphenyl 5 n.d.Ho€bromobiph€nyl 5 n.d.Heptabromobiphenyl n.d.Oclabromobipheryl 5 n.d.Nonabromobiphenyl 5 n,d,Decabromobiph€nyl 5 n.d.Sum of PBDES

mg/Kg With reference to IEC 62321: 2008 andperformed by GC/MS.

n.d.Monobomodipheny' elher 5Dibromodiphenyl elher 5 n.d.Tribromodiphenyl ether 5 n,d,Tetrabromodiphenyl eth€r 5 n.d-Pentabromodiphenyl ether 5 n.d.He)€bromodiphenyl elher 5 n.d.

H€ptabromodiphenyl ether 5 n.d.Cctabromodipherryl elher n.d.Nonabromodiphenyl elher 5 n,o,Decabromodiphenyl ethef 5 n.d.

r& d&nhd n hs.d by h cohts4 dld b e qmd coid !oi! d 5.d.|dMh6da@nd6DbldbTluidre bu.. ddi.dddh !ry h

. i t i 4 c . F i r l r 1 y a b a q . d e f

. 'dd.d.5rrb.4r!s1rc*.u

BLACK EPOXY IJOLDING COMPOUND

Test ReportSUMITOMO BAKELITE SINGAPORE PTE CO.. LTD.NO. 1 SENOKO SOUTH ROAD, SINGAPORE 758069

No. : KA/201 3i/308 1 8 Date:201303/13Page | 3 ofg

Test ]tem (s): Unit Method iIDL Re3ultNo. l

Antimorry (Sb) ngftg With reference to US EPA llethod 3052forAntimony Content. Analysis waspertomed by ICP-AES.

2 n.d.

Perfl uorooctane sultonates(PFOS - Acid, Melal Salt, Amide)

mg/tg With reference to US EPA 3550C: 2007.Analysis was perfomed by LC/MS.

1 0 n.d,

PFOA (CAS No.:33S ) msfts With reference to US EPA 3550C: 2007.Analysis was performed by LC/MS.

1 0 n.d.

HalogenHalogen-Fluorine (F)(CAS No.: 014762-94-8)

mg/Kg With reference to BS EN 1458212007.Analysis was per{ormed by lC.

50 n.d.

Ha|ogen-unbnne (ut)(CAS No.:022537-1$1)

mg/rg With reference to BS EN 14582:2007.Analysis was performed by lC.

50

Halogen-Bromine (Br)(CAS No.: 010097-32-2)

mgikS With rcference to BS EN 14582:2007.Analysis was performed by lC,

50 n.o.

Halogen-lodine (l)(CAS No.: 014362-4.4-8)

mS./kg With reference to BS EN 1 4582:2007.Analysis was perfomed by lC.

50 n.d.

Note : .t. mgrkg = ppm : 0.1M%= 1000ppm2. n.d. = Not Detected3. IVIDL = I\rethod Deteclion Limit4.'-" = Not Regulated

PFOS Refe.ence lnturnation : POP8 . {EU} 7572010Outlawing PFOS as subslances or preparalions in concentrations above 0.001% (1oppm), in semi-finished products oradicles or parts at a levelabove 0.1ol6(1000ppm), in te{iles or other coated materhls above '1!g/m'.

e r E @ E i i e

dddhhr &dn66 .ujd b r d5 d wwrsad.l4!40@b!!!84

Test ReportSUMITOMO BAKELITE SINGAPORE PTE CO.. LTD.NO. 1 SENOKO SOUTH ROAD, SINGAPORE 758069

No. rKA/201380818 Date:20130313 Page:4of 9

1) These samphs wft dislEd ioblly by pe-@ndilioning melhod a@rding io bdMflowctun' (C6+ tesl

2) Name ol ihe peEd who made heasuendt Alex Chang

3) Name of ihe pesn in chaqe of measurement Ray Chang

steer, @ppor, aruminum, 3ord.r ,qu€ 6gia, HNO 3, HC, NF, HrCl

Gold, darinud, pall.dium, 6Bdk

No!._ : O ) For non-mslattic maiand add atkathe dio€ston reag€nt and heat ro 90-€5 f .(2) For meiallic haledal, add pure wabr and heat 10 boiling.

iddcbdn&@mhB rsjdbr

Acid digeslion by suilabl€ aci(i

depended on difeEnl sample

mabdal (a3 bd@ bble)

Micro$aw dig€slion witl

HNO3/HCUHF,dd appropd ale a mount

Me.sue lhe absorban@

I .d6rc ,b r r

No.:KA/2013/30818Dale : 2013n3h3 P a g e : 5 o f g

" " " " " " " " " ' i " " " " " , " " "J Sample extraction/ I

Soxhlet method I

I Concentrate/Dilute II Exlracted solution I_ - - - - - - - - - - - - - - -

I Filter I

i

Analysis by GC/[,lS

6mr.t'lls, .!4 r si 49ti{l! .r tlGiy ebid ro iB G6dr tudtun! d s.B

*dit hn d@notu. abl.d ro tm@t' indio' d h' tmc d iB illtff

n!/r.*c.@3b|iy*bi!ddlnd

Test ReportSUMITOMO BAKELITE SINGAPORE PTE CO., LTD.NO. 1 SENOKO SOUTH ROAD, SINGAPORE 758069

PBBTPBDE analytical FLOW CHART1) Nam€ ofthe o€rson who made measurementr Anson Tsao

2) Nam€ ofthe p€rson in charge of measuremenl Ray Chang

First testing process

Oplional screen process

Confirmalion process

Test Report No.:M/2013/30818Date:2013/03/13P a g e : 6 o f g

SUltllTOlrO BAKELITE SINGAPORE PTE CO., LTD.NO. 1 SENOKO SOUTH ROAD, SINGAPORE 758069

1) These samples we|e dissolved totally by p|e-conditioning melhod accoding to below

2) Name of the peGon who made measurement Alex Chang3) Name of the pe6on in chaEe of m€asurement Ray Chang

Flow Chart of digestion for lho glgments analysis peformed by ICP-AES

t 3 1 . r r f i - a r s ,

Sample M€asurcment

Acid digestion by suitable acid depend€d on diff€€nl sample material{as betowtable)

2) HClto dissolve

Steel, copper, aluminum, solder Aqua regia HNOI. HCI HF, HrO,

Glass ftNo3/HF

Gold, 9lalinum, palladium, ceranic Aqua regia

Silver HNO3

H2SO4 HrOr, HNOr, HCI

Any acid to total digeslion

I a i d , ' n r

Test Report No-:KA/2013/30818Date : 201 3/03/1 3 Page : 7 of g

SUII4ITOI\4O BAKELITE SINGAPORE PTE CO,, LTD.NO. 1 SENOKO SOUTH ROAD, SINGAPORE 758069

Analytical flow chart of PFOA/PFOS content

1) Name of the person who made measurement Anson Tsao

2) Name ofthe person in charge of measuremenl: Ray Chang

sbiqdb 6 c. i .Er cqdi4! d s4

I , . u o o u a a

Test ReportSUMITOMO BAKELITE SINGAPORE PTE CO.. LTD.NO. 1 SENOKO SOUTH ROAD, SINGAPORE 758069

No. rKA/201380818Date :201t03/13 Page :8 ofg

y sbid b 6 cad cofd r qn' d sqiftj!ry.!$c!r^!E{4o@!!!!l@

it.dErtsdlr!y*b 6 obh lid

Analytical flow charl of halogen content

1) Name of the person who made measurement Jean Hung

2) Name of the p€rson in charge of measurement Ray Chang

Sample picture and rsport number

Weighting and putting sample in cell

Orygen Bomb Combustion /Absoption

Dilution to fixed volume

Analysis was perfomed by lC

l , e i o t n , n r

Test ReportSUI/lITOMO BAKELITE SINGAPORE PTE CO., LTD.NO, 1 SENOKO SOUTH ROAD, SINGAPORE 758069

No. : KA/2013/30818Date:201303/13Page: I of9

' The tested sample / parl is ma*ed by an anow if it's shown on the pholo. '

*' End of Report "'

y eqd 6 iB c6d,r coden. or s.o

]ddidm r-u.r ddmd 6.6n. My hnta $L artsns b riv tr b i! c id and

30818