icp test report certification packet/media/electronics... · ltttelfuse phtls., tnc. lima tech...

60
1 ICP Test Report Certification Packet Company name: Littelfuse, Inc. Product Series: Nano (Silver or Gold plated) Product #: 456xxx Series Issue Date: January 17, 2013 It is hereby certified by Littelfuse, Inc. that there is neither RoHS (EU Directive 2002/95/EC, and its recast 2011/ 65/EU)-restricted substance nor such use, for materials to be used for unit parts, for packing/packaging materials, and for additives and the like in the manufacturing processes. In addition, it is hereby reported to you that the parts and sub-materials, the materials to be used for unit parts, the packing/packaging materials, and the additives and the like in the manufacturing processes, are all composed of the following components. Issued by: <Global EHS Engineer> (1) Parts, sub-materials and unit parts This document covers the Nano RoHS-Compliant series products manufactured by Littelfuse, Inc. Raw Materials Used Please see Table 1 (2) The ICP data on all measurable substances Please see appropriate pages as identifed in Table 1 RemarksPb (lead) contained in the high temperature melting solder > 85% and is categorized as exempt under section 7a of the RoHS Annex. Form 585-047 Rev. A 2/21/06

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Page 1: ICP Test Report Certification Packet/media/electronics... · LTTTELFUSE PHtLS., tNC. Lima Tech Center, SEZ, Lipa, Malvar, Batangas The following sample(s) was/veere submitted and

1

ICP Test Report Certification Packet

Company name : Littelfuse, Inc.

Product Series: Nano (Silver or Gold plated)

Product #: 456xxx Series

Issue Date: January 17, 2013

It is hereby certified by Littelfuse, Inc. that there is neither RoHS (EU Directive 2002/95/EC, and its

recast 2011/ 65/EU)-restricted substance nor such use, for materials to be used for unit parts, for

packing/packaging materials, and for additives and the like in the manufacturing processes.

In addition, it is hereby reported to you that the parts and sub-materials, the materials to be used

for unit parts, the packing/packaging materials, and the additives and the like in the manufacturing

processes, are all composed of the following components.

Issued by:

<Global EHS Engineer>

(1) Parts, sub-materials and unit parts

This document covers the Nano RoHS-Compliant series products manufactured by

Littelfuse, Inc.

< Raw Materials Used

Please see Table 1

(2) The ICP data on all measurable substances

Please see appropriate pages as identifed in Table 1

Remarks:

Pb (lead) contained in the high temperature melting solder > 85% and is categorized as

exempt under section 7a of the RoHS Annex.

Form 585-047 Rev. A 2/21/06

Page 2: ICP Test Report Certification Packet/media/electronics... · LTTTELFUSE PHtLS., tNC. Lima Tech Center, SEZ, Lipa, Malvar, Batangas The following sample(s) was/veere submitted and

2

Table 1: List of Raw Materials covered by this report

Total Parts Raw Material Part Number Raw Material Description Page(s) 1 909-422 Body 3-10

2 910-259 (same as 910-238) Cap – Silver plated 11-18

3 910-554 (same as 910-275) Cap – Gold plated 19-24

4 087266 Anaerobic Adhesive 25-34

5 11-0010 (687xxx) Element-Pure Ag1000 35-40

6 079xxx Element 41-45

7 692323 Solder 46-51

8 425809 Ink 52-60

Page 3: ICP Test Report Certification Packet/media/electronics... · LTTTELFUSE PHtLS., tNC. Lima Tech Center, SEZ, Lipa, Malvar, Batangas The following sample(s) was/veere submitted and

Test Report Number : TWNC00285767

Authorized By: On Behalf Of Intertek Testing Services Taiwan Limited

K. Y. Liang Director

*THJ0285767* Page 1 of 8

Intertek Testing Services Taiwan Ltd. 8F., No. 423, Ruiguang Rd., Neihu District, Taipei 114, Taiwan, R.O.C.

全國公證檢驗股份有限公司 114台北市內湖區瑞光路 423號 8樓

Tel: (+886-2) 6602-2888.2797-8885 Fax: (+886-2) 6602-2410

Applicant: Littelfuse Philippines Inc. Date : Nov 19, 2012 LIMA Technology Center, Lipa City,

Malvar, Batangas

Sample Description:

One (1) group of submitted samples said to be : Part Description : Body Part Number : 909-422 Date Sample Received : Nov 12, 2012 Date Test Started : Nov 13, 2012

Test Conducted :

As requested by the applicant, for details please refer to attached pages.

Page 4: ICP Test Report Certification Packet/media/electronics... · LTTTELFUSE PHtLS., tNC. Lima Tech Center, SEZ, Lipa, Malvar, Batangas The following sample(s) was/veere submitted and

Number : TWNC00285767

Test Conducted

*THJ0285767* Page 2 of 8

Intertek Testing Services Taiwan Ltd. 8F., No. 423, Ruiguang Rd., Neihu District, Taipei 114, Taiwan, R.O.C.

全國公證檢驗股份有限公司 114台北市內湖區瑞光路 423號 8樓

Tel: (+886-2) 6602-2888.2797-8885 Fax: (+886-2) 6602-2410

(Ⅰ) Test Result Summary : Result (ppm)

Test Item White Plastic

Heavy Metal

Cadmium (Cd) content ND Lead (Pb) content ND Mercury (Hg) content ND Chromium VI (Cr6+) content ND

Polybrominated Biphenyls (PBBs) Monobrominated Biphenyls (MonoBB) ND Dibrominated Biphenyls (DiBB) ND Tribrominated Biphenyls (TriBB) ND Tetrabrominated Biphenyls (TetraBB) ND Pentabrominated Biphenyls (PentaBB) ND Hexabrominated Biphenyls (HexaBB) ND Heptabrominated Biphenyls (HeptaBB) ND Octabrominated Biphenyls (OctaBB) ND Nonabrominated Biphenyls (NonaBB) ND Decabrominated Biphenyl (DecaBB) ND

Polybrominated Diphenyl Ethers (PBDEs) Monobrominated Diphenyl Ethers (MonoBDE) ND Dibrominated Diphenyl Ethers (DiBDE) ND Tribrominated Diphenyl Ethers (TriBDE) ND Tetrabrominated Diphenyl Ethers (TetraBDE) ND Pentabrominated Diphenyl Ethers (PentaBDE) ND Hexabrominated Diphenyl Ethers (HexaBDE) ND Heptabrominated Diphenyl Ethers (HeptaBDE) ND Octabrominated Diphenyl Ethers (OctaBDE) ND Nonabrominated Diphenyl Ethers (NonaBDE) ND Decabrominated Diphenyl Ether (DecaBDE) ND

Page 5: ICP Test Report Certification Packet/media/electronics... · LTTTELFUSE PHtLS., tNC. Lima Tech Center, SEZ, Lipa, Malvar, Batangas The following sample(s) was/veere submitted and

Number : TWNC00285767

Test Conducted

*THJ0285767* Page 3 of 8

Intertek Testing Services Taiwan Ltd. 8F., No. 423, Ruiguang Rd., Neihu District, Taipei 114, Taiwan, R.O.C.

全國公證檢驗股份有限公司 114台北市內湖區瑞光路 423號 8樓

Tel: (+886-2) 6602-2888.2797-8885 Fax: (+886-2) 6602-2410

(Ⅰ) Test Result Summary : Result (ppm)

Test Item White Plastic

Halogen Content Fluorine (F) ND Chlorine (Cl) ND Bromine (Br) ND Iodine (I) ND

Remarks: ppm = Parts per million based on weight of tested sample = mg/kg ND = Not detected

Responsibility of Chemist :Irene Chiou / Kevin Liu / Cathy Chen

Date Sample Received : Nov 12, 2012 Test Period : Nov 13, 2012 To Nov 15, 2012

(Ⅱ) RoHS Limits:

Restricted Substances Limits

Cadmium (Cd) Content 0.01% (100ppm) Lead (Pb) Content 0.1% (1000ppm) Mercury (Hg) Content 0.1% (1000ppm) Chromium VI (Cr6+) Content 0.1% (1000ppm) Polybrominated Biphenyls (PBBs) 0.1% (1000ppm) Polybrominated Diphenyl Ehters (PBDEs) 0.1% (1000ppm)

The above limits were quoted from Annex II of 2011/65/EU for homogeneous material.

Page 6: ICP Test Report Certification Packet/media/electronics... · LTTTELFUSE PHtLS., tNC. Lima Tech Center, SEZ, Lipa, Malvar, Batangas The following sample(s) was/veere submitted and

Number : TWNC00285767

Test Conducted

*THJ0285767* Page 4 of 8

Intertek Testing Services Taiwan Ltd. 8F., No. 423, Ruiguang Rd., Neihu District, Taipei 114, Taiwan, R.O.C.

全國公證檢驗股份有限公司 114台北市內湖區瑞光路 423號 8樓

Tel: (+886-2) 6602-2888.2797-8885 Fax: (+886-2) 6602-2410

(Ⅲ) Test Method: Test Item Test Method Reporting Limit

Cadmium (Cd) content

With reference to IEC 62321 edition 1.0:2008 in clause 8/9/10, by microwave digestion until the tested samples are totally dissolved and determined by ICP-OES.

2 ppm

Lead (Pb) content

With reference to IEC 62321 edition 1.0:2008 in clause 8/9/10, by microwave digestion until the tested samples are totally dissolved and determined by ICP-OES.

2 ppm

Mercury (Hg) content

With reference to IEC 62321 edition 1.0:2008 in clause 7, by microwave digestion until the tested samples are totally dissolved and determined by ICP-OES.

2 ppm

Chromium VI (Cr6+) content

With reference to IEC 62321 edition 1.0:2008 in annex C, by alkaline digestion and determined by UV-Vis spectrophotometer.

1 ppm

Polybrominated Biphenyls (PBBs)

With reference to IEC 62321 edition 1.0:2008 in annex A, by solvent extraction and determined by GC-MS and further HPLC-DAD confirmation when necessary.

5 ppm

Polybrominated Diphenyl Ethers (PBDEs)

With reference to IEC 62321 edition 1.0:2008 in annex A, by solvent extraction and determined by GC-MS and further HPLC-DAD confirmation when necessary.

5 ppm

Halogen Content With reference to EN 14582:2007 by calorimetric bomb with oxygen and determined by Ion Chromatograph.

50 ppm

Remark: Reporting limit = Quantitation limit of analyte in sample

Page 7: ICP Test Report Certification Packet/media/electronics... · LTTTELFUSE PHtLS., tNC. Lima Tech Center, SEZ, Lipa, Malvar, Batangas The following sample(s) was/veere submitted and

Number : TWNC00285767

Test Conducted

*THJ0285767* Page 5 of 8

Intertek Testing Services Taiwan Ltd. 8F., No. 423, Ruiguang Rd., Neihu District, Taipei 114, Taiwan, R.O.C.

全國公證檢驗股份有限公司 114台北市內湖區瑞光路 423號 8樓

Tel: (+886-2) 6602-2888.2797-8885 Fax: (+886-2) 6602-2410

(Ⅳ) Measurement Flowchart: Test for Cd/Pb/Hg/Chromium (VI)/PBBS/PBDES Contents Reference Standard: IEC 62321 edition 1.0:2008

Weigh sample and add organic solvent

By Soxhlet extraction or Solvent extraction

Concentrate the extract and make upwith organic solvent

PBBs/PBDEs

Analyzed by GC-MSD

Sample preparation

Take sample and immerse into Aqua Regia, start to strip plating layer

Stop the stripping procedure upon color change completely

Take the Aqua solution as plating component and stripped body as substrate component

For non-metal part For metal part

Make up with deionized water and add diphenyl-carbazide solution

Cr6+

Analyzed by UV-VIS

By spot test

Get 50cm2 sample

By boiling water extraction

Negative *2

Substrate Plating

Weigh sample and add alkaline solution

Definite temp. extraction

Cool and filter the extract

Cr6+

For different material, digest the sample with appropriate acid*1

Make up with deionized water

Cd/Pb/Hg

Analyzed by ICP-OES

Confirm the tested samples are totally dissolved

Page 8: ICP Test Report Certification Packet/media/electronics... · LTTTELFUSE PHtLS., tNC. Lima Tech Center, SEZ, Lipa, Malvar, Batangas The following sample(s) was/veere submitted and

Number : TWNC00285767

Test Conducted

*THJ0285767* Page 6 of 8

Intertek Testing Services Taiwan Ltd. 8F., No. 423, Ruiguang Rd., Neihu District, Taipei 114, Taiwan, R.O.C.

全國公證檢驗股份有限公司 114台北市內湖區瑞光路 423號 8樓

Tel: (+886-2) 6602-2888.2797-8885 Fax: (+886-2) 6602-2410

(Ⅳ) Measurement Flowchart: Remarks: *1: List of Appropriate Acid:

Material Acid Added for Digestion Polymers HNO3,HCl,HF,H2O2,H3BO3 Metals HNO3,HCl,HF Electronics HNO3,HCl,H2O2,HBF4

*2: If the result of spot test is positive, Chromium VI would be determined as detected.

Page 9: ICP Test Report Certification Packet/media/electronics... · LTTTELFUSE PHtLS., tNC. Lima Tech Center, SEZ, Lipa, Malvar, Batangas The following sample(s) was/veere submitted and

Number : TWNC00285767

Test Conducted

*THJ0285767* Page 7 of 8

Intertek Testing Services Taiwan Ltd. 8F., No. 423, Ruiguang Rd., Neihu District, Taipei 114, Taiwan, R.O.C.

全國公證檢驗股份有限公司 114台北市內湖區瑞光路 423號 8樓

Tel: (+886-2) 6602-2888.2797-8885 Fax: (+886-2) 6602-2410

(Ⅳ) Measurement Flowchart: Test for Halogen Content Reference Standard:EN 14582

End of Report

This report is made solely on the basis of your instructions and/or information and materials supplied by you. It is not intended to be a recommendation for any particular course of action. Intertek does not accept a duty of care or any other responsibility to any person other than the Client in respect of this report and only accepts liability to the Client insofar as is expressly contained in the terms and conditions governing Intertek's provision of services to you. Intertek makes no warranties or representations either express or implied with respect to this report save as provided for in those terms and conditions. We have aimed to conduct the Review on a diligent and careful basis and we do not accept any liability to you for any loss arising out of or in connection with this report, in contract, tort, by statute or otherwise, except in the event of our gross negligence or wilful misconduct.

Add absorbent in a combustion flask & place weighed sample in equipment

Fill oxygen into calorimetric bomb

Ignite then leave the bomb at room temperature

Transfer the absorbent into a volumetric flask

Make up with deionized water

Sampling/grinding or cutting

Analyzed by ion chromatography

Page 10: ICP Test Report Certification Packet/media/electronics... · LTTTELFUSE PHtLS., tNC. Lima Tech Center, SEZ, Lipa, Malvar, Batangas The following sample(s) was/veere submitted and

Number : TWNC00285767

Test Conducted

*THJ0285767* Page 8 of 8

Intertek Testing Services Taiwan Ltd. 8F., No. 423, Ruiguang Rd., Neihu District, Taipei 114, Taiwan, R.O.C.

全國公證檢驗股份有限公司 114台北市內湖區瑞光路 423號 8樓

Tel: (+886-2) 6602-2888.2797-8885 Fax: (+886-2) 6602-2410

Photo

Page 11: ICP Test Report Certification Packet/media/electronics... · LTTTELFUSE PHtLS., tNC. Lima Tech Center, SEZ, Lipa, Malvar, Batangas The following sample(s) was/veere submitted and

scsTest Report No.: LB12-01094C March 5, 2012 Page 1 of 4

LTTTELFUSE PHtLS., tNC.Lima Tech Center, SEZ,Lipa, Malvar, Batangas

The following sample(s) was/veere submitted and identified bylon behalt ol the client as:

Product Name

SGS Samplg Number

Recelved Date

Test Perlorming Date

T6sl Perlormed

Test Requested

Test llethod

Ted n6sult(5)

C,oncluslon

Cap 910-259 / Base

LB12-01094.004

FebrJary 21 ,2012

F€bruary 21,20121o March 5,2012

SGS Philippines subcontracted the testing ot sampte(s) setecl€d byapplicant with following results

Selected test(s) as requested by client.

Please reler to next page(s).

Please refer 1o next page(s).

Based on the perfomed tests on submitted sample(s), the results ofLead, Cadmium, Hexavalent chromium and l\,,lercury complywithlhe RoHS Dnective 2002/95/EC and iis subsequeni amendments.

This reportwillbe kepl on file for six months from the date ol issue.

Signed for and on behalt olSGS PHILIPPINES, INC.

I'EDEN L. PENEYHALaboralory Operalions Manager

''Thl! docum i. r*ru.d by th. co o.ny rbt.cr ro r|3 6s.6r cddirro. ot s.rur6 pndod oqlEl, fl.ihbb oh 6qu6d 4 ac6*lbl. .l

q, jAttolr@!-d!gtE$&!b Alidtllon b dren lo lh.limil.lion ol lirbihy, hd.nnit€rion and iurl.dtclld ls.u6.Ll|md lh€Eh.Any hordor or lhrs [email protected] b advr$d lh.l Inromalron @nlarn.d hrs r.rr€.1. lh. comps9. llndino! .r rh. rim ol n5 inr6m 16 on,y.nd $$rn rh. llnrt ol clr.nr'3 lmrMrron., r, dy. Ih. comFny s $1. repoFiblllry i! ro irs clk anrl $is rlocun.d do. nor .rcnr.l.p.nb. ro . lnn$crbn r6m 4rcrdhg .rr rrsrf rrgrtu .nd obrrg.t nt!. This d*[email protected] ..nnor b. Eproduc€d.EDt In turr, Tlnoul prrd rrnl.n .D9.mr ot rh. conp.ny, any unrurhdi2.d ,ledrid, l6rgery orrhb ddmnr l. unl.wlul .nd ofi.nd.6 n.v b. .Mur.d ro rh. tull.3r 6rem or !i. r.w. unre.t o$.frr$ !r.r€d rh. 63ulr. llwn l. rhleb31 Ep..r dr onry ro rho 3flpr.(3) l.!r.d *d ech *mpl€l.) .E Br.in.d td 50 rlrys dly--

Page 12: ICP Test Report Certification Packet/media/electronics... · LTTTELFUSE PHtLS., tNC. Lima Tech Center, SEZ, Lipa, Malvar, Batangas The following sample(s) was/veere submitted and

SGSTest Report No.: LB12'01094C March 5.2012 Page 2 ol4

Sample Number : LB11-01094.004Physlcal Das€ription : Base material of silver colored metalItem / Batch Numb€r : fl/A

RoHS Dlreclive 2002/95/EC

Tesl ltem(s) unit Itothod iIDL n6sult

Cadmium (Cd) mg/Kg IEC 62321: 2008 applicationof modified digestion by

surlace etching andperfomed by ICP-AES.

2 ND

Lead (Pb) MEKg 2 ' | 19

Mercury (Hg) mg/Kg 2 ND

Hexavalent Chromium C(Vl)

with reference to lEc 62321:2008 and perfomed byBoiling water extraction

Method.#

Negative

Nole :1 mg/kg = ppm ; 0.1wt% = lOOOppm2. ND = Not Detected

3. MDL = lllethod Det€ction Limit

4. " = Oualitative analysis (No Unit)

5. # = a. Posilive means the presence ol CrVl on the tested areasb. Negative means the. absence of CrVl on the tested areas

The detecGd concentration in boiling-water'extraction solulion is equalor grealer than 0 02 mg/kgwith 50 cm2lesled a€as.

6. Analyses were subcontracted to SGS Taiwan, Ltd

"Thr. dddd l. L.$.d by lh. c.np.ny.uq.cr b ib G.w.r condhiont or s{vid F.hl€rr oErlal' daiLbl' M '€qFr or 'c.sibl6 '1|w.;iffi rd ;dmdhim;nd, lor.l€.lbnic lom.l dodmnl.! .ubier io rmr and cddllle! tor Elecrrdnic o6'unstt tlffi;ffi. .ddmtt.hll.ntbn i3 dlM io ih. lidrd|6 d li.birilir, lnd.mnilicarbh tnd jrtudlctlon blA rt'lln€d rhs"n'G;Etdor ot thti d*um t. stv6d thd intoma on 6nl.tned heM r.lt.cl' rh. comtfy . rhdinss n $. n. ol 1l! Int Mxro onryi"iii'njlrL.ii.Ir"iiciii'ii:i"ai""rroninmv.r*conprny'sotggpon.|bi|ityB6n.c|Btandni,rrii r, i, i.*.ir"; r-.

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iict dn dor ory to thr *nde{.) i.d.d and sicn *mpl43) ae ra.lmd lot 60 day3 dlv "

Page 13: ICP Test Report Certification Packet/media/electronics... · LTTTELFUSE PHtLS., tNC. Lima Tech Center, SEZ, Lipa, Malvar, Batangas The following sample(s) was/veere submitted and

sGsTest Report No.: LB12-01094C March 5,2012 Page 3 of 4

"[email protected]'sbi€dtoit.G*n|cohdtr|dro|s.d'cepdnbd.y.l|.a|' '.||.b|.onftqed4*e.llb|..|bm.mo $d. ior a.dbdc ;;"i oiiii'i"G nrr; i" r"-"

"nd cdin'om ror Ererbnic D*!-mnt' 'r;lXi:,tr:tr;:;#T##ir;;.]';r;i#K-:|'"dd"'r;:iqiirFi:l-a.,b"F-1'i^ljll:i:d-:i"11':,::,.11t'1*Ll'""iffiT:i:';:#gtffi+ffi1ffffi1Y,i#il.;',r;&!.-i4iq,ss-4i"idl**lS:1r..,*.,';':"':ll*'S'*iJJtrf,llifll;

ATALYSIS FLOWCHARTOF HEAVY METALS

Pb,cd,Hg

Negalive

Addinq 1,5-diph€nylcalbazide lor

Adding 1.5-

the prssence o, Cl6+.

*"".'"-"-'*ffiJi ; iiriial ii" cip-v" ma"ril $' tme or n' inte*nrron orvAnv bldd ol lhh docurenl i..ci"j i-r,;nil r'r'" iiirJii cr".rt r"a*rr."' ,r -v. rr'. c"."iiis ;r; ;'po*ibi rv E t6 iddffr 'hi'r tni! do@mnr da' nor orod e

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iij5;;;ift;.;ii;ih;; iqJirixrca jna :i,ctr mmpr.{st *' r'rai^'d rs 60 d+ onrv "

Page 14: ICP Test Report Certification Packet/media/electronics... · LTTTELFUSE PHtLS., tNC. Lima Tech Center, SEZ, Lipa, Malvar, Batangas The following sample(s) was/veere submitted and

SGSTest Report

Sample Photo (As Becaived):

-l , .;

ffi ffi********#*'ni'fr ftiijffili.l-ifi,r$','fi'l,"r"r"g"'""''.'o""*""iGi6ii,"a.'i*mda..a.--o

fiJi'- rli iri,;i;;i p,r* *,'n"..pFi"-r or rr* co'p'nv G'" Jnrut*i:ao rtte'nton ro's*v c t,hF d.cumnr i: unr.wrur.nd one."".."v - p-*'*"iJi# iiiriili iir-"i'r'"ini i*

-u"it'" ott''fri* 't'r€d th' E3urtr shdn r' rhr'

iili "ii,-'i

*ri' -rv r. rn" *.ptel') b3r.d .hd .uch *mpq.' * t'r'i*d rot 60 d'va dry "

No.: LB12-010S4C March 5, 2012

LB12-01094.004

. . .End ol Report.. .

Page 4 of 4

,

Page 15: ICP Test Report Certification Packet/media/electronics... · LTTTELFUSE PHtLS., tNC. Lima Tech Center, SEZ, Lipa, Malvar, Batangas The following sample(s) was/veere submitted and

SGTest Heport

LITTELFUSE PHII..S., INC.Lima Tech Center, SEz,Lipa, Malvar, Batangas

The following sample(s) was/we

No.:1812-01094A March 5, 2012 Page 1 ot 4

Product Name

SGS Sample Numbel

Recelved Date

Test Performing Date

T€st Perfurmed

Te€t Requested

Test Method

Tqrt R.eult(s)

conclugion

re submitled and identilied bylon behalf of the client as:

Cap 910'259 / Plaling

L812,01094.002

Fehtuary 21 , 2012

February 21 , 2012 to lllarch 5, 2012

SGS Philippines subconlracted lhe tesling ol sample(s) selected byapplicant wilh following results

Selecled teg(s)as requested by client.

Please reler to next Page(s)

Please refer 10 next page(s).

Based on the perlormed tests on submitted sample(s)' the results ofLead, Cadmium, Hexavalent chromium and l\rercury complywlththe RoHS Dkective 2oo2l95/Eo and its subsequent amendments

This repod will be kept on file lor six months from the dale of issue'

Signed lor and on behalf olSGS PHILIPPINES, INC.

i,EDEN L. PENEYRALaboratory Operations Manager

W**********;ff 'ffi 'ffi "lt#ffi.'lro. ro . ln@ctron i,om erc.r,'"g ar $"n .gn'" .- o"lis.iioniijiai'iit"i'*iarn ao-'dr' rhr! docu@nr dnnot b' dPrcdued

lillii,iiririiir,iii,r p"- *r*n.pp;o,.ror $.b.6Fnv. A'-v un.uthd'ed 'rb'r'n r'!sv d I'r'rrurion oi rh' @nr' or'ppe Bnroiii- i"l,iir r.

"^r.h"r -o onein* .o te o.*,neo 6in" tuttert inor a m l*

-uni*" ott'ryr!' sraGrr rh' E urB lhdn In rhi!

ili .-,ia i"t"i .itv io tt "

-.pre{.l blt.d and 3irch '.mpre{t .ro Etain'd ro' 60 dtve onrv -

Page 16: ICP Test Report Certification Packet/media/electronics... · LTTTELFUSE PHtLS., tNC. Lima Tech Center, SEZ, Lipa, Malvar, Batangas The following sample(s) was/veere submitted and

sGsTest Report No.:1812-01094A Llarch 5, 2012

Sample NumberPhygical DescriplionItom / Balch Numbor

: LB11-01094.002: Plating layer ot siMer colored metal

PaOe 2 ol 4

RoHS Dlrectlve 2002/95/EC

Test ltem(s) Unlt Method MDL Rg€ult

Cadmium (tu) mgKg IEC 62321: 2006 applicationol modified digestion by

surface etching andperformed by ICP-AES.

ND

Lead (Pb) m9Kg 2 1 8

Mercury (Hg) mg/kg 2 N O

Hexavalent Chromium C(Vl)

wilh reference to lEc 62321:2008 and performed byBoiling water extraction

Method.#Negalive

Nole :1 .

2.

6.

3.4.5.

mdks=ppm ; 0.1M%= 1000ppmND = Not DetectedMDL = Method Detection Limit" = Qualitative analysis (No Unit)# = a. Positive means the presence ot CrVl on the tested areas

b. Negative moans the absence of CrVl on lhe tested areasThe detected concentration in boiling-waterexlraction solulion is equalor greaterthan 0.02 mg/kgwith 50 cm, tested arcas.Analys€s were subcontracled to SGS Taiwan, Ltd

"Th|.do.uEnt'.isU.dbylh6conp..|y{bt.dto|l.Gffi|c.nditi43.|sa|rn.hHdn6''swr.-Mn.d. .nd .;dhbnr.nin .nd, tor .l.crDni. lod.l doon.n€t sbFcl lo T.ds and coildl m tor EloclDnlc Docutrsllt .rd=ffiffiEelmdrnn. An.dbn rs dwn ro rE hhn rq or rr.bnhyi Ind.nn'r'cdris $d lo,r.drctron r.!s d.fimd rh'orn.Atrv h.ld.rcr rr'r. ddmnr |! .dvi!.d rh.r i dnrnbn conl.h.d h.Ed re{ 13 rh€ compdf! lindinc. .t ft. rlm. oi it inrorF.rlm onlv$; thl. rh. linir. ol cll.d. Instdcll@ il anv. Th. c.nptrv. ..1. E$ondbiritv i. ro lB dldl and lhii d.cumln d4. nol .&.e.r.r.nb. ro . t aEdm tdn osrcl.lno .ll $.k noms .nd ouigrlion. unrL. th. lrn{ctd [email protected].. Thlt d@umnl @hnol b. Eptodu.€daslr h tul. wirhod Fir fhbn .DDroEl ol lh€ comlt'ry. any u..ulhdP.d rlt 6lion. rolg v d l.llni@uon or rh. 6tunr d .r0€.6n6 orrhi. ircumi Le onk*rur .nd onqiJ€.. na h. lE;urod ro I'. tur6d.rrdr or rh. rtu. unr6's orh.fris lr.red rh. E.ulr! lhoan In rhr'r.3r dpon rd.f onry io rh. umpl4.) l6red lnd 3uch smpk{!) aE eitin.d L. 50 d.vr dlv "

Page 17: ICP Test Report Certification Packet/media/electronics... · LTTTELFUSE PHtLS., tNC. Lima Tech Center, SEZ, Lipa, Malvar, Batangas The following sample(s) was/veere submitted and

SGSTest Report No.: LB12-01094A March 5,2012 Page 3 of 4

-rhrs docuNm r. r$u.d by rn coi'e.ny{q.d16|ts6d.6rcmdnid.ds.niepn.d.w!"1:g*'^"ll,:ljf_*,L#llil-.ff;".?Hi;;i.;;;ilifr.i:iG.ffi1','iril-rl{;ro*-"1.;-?,tr"L':y1:.i*:n"l'i*",,lt,.lm,Lmg[,i:ffir,or*. as*-y r'or*. or f i"1o"u1-, i1 "01*ifiir..iit pgifi31:*a?.i1"-?TJ?l'i;g:T"'"" ,1;1":l1;":L'f.ff#i*:1"',:g* -' -- - -"-* ---;;'

;; ;sEibinry B d idc|dt and th'' d@un'nr do nor "on'Er'.ni wirhin uF lrdr. .t clLr{. h.lMlion* r Dv rh. com

rcr"r"o "r rm, ,rsnu _" -ircxi-i ".0., in" t*joo" ae"*,r.rt! !aTAt?lT:f-:fj:,::

. ndw i l h i n l l Fhdao l c | | . t { ' . h . lM l i on * fDy ' | n .@mpony lE|3ha dn $dr trghl!.nd oblgn

lLiii ri-rn ut'"i,i -- "ltun

Drd.r or rh comr..v. Anv un.urhonad :rr*'rron'!i-a r" u mt'u pa- "ltun

!F .d.r .t rh€hi;ru|rnr b ddfl .nd otidlr.E md ie

; i;'#;;":; ;i .i*rr-. t".s.'v * t"rn"*I- or rh' @'r'nr o.pp'dfr' oliiJr ilei"iJiiiil iiirii inr."r .i.n! or $e r*.-unre$ or'*i* 3r'rcd $' t'sh' shdn in rhr'

ANALYSIS FLOWCHART OF HEAVY METALS

Pb,cd,Hg

Posilive

Negative

Sample l,leasursmenl

Heating ro90-95'C

Totat Digestion

Adding 1,5-

the presence ol Cr6+.

rhl. d@umnr i. |lnlstul .ndi$ ;;;;ii.i;i;iift;;iii,:r-ii.r.al"r .i,.t *.pcr'r *. Erah'd t" 60 d'v" onrv

Page 18: ICP Test Report Certification Packet/media/electronics... · LTTTELFUSE PHtLS., tNC. Lima Tech Center, SEZ, Lipa, Malvar, Batangas The following sample(s) was/veere submitted and

SGSTest Report

Samole Photo (As Receiv€dl:

. .1

No.: LB12-01094A March 5,2012

LB12-01094.002

. . .End of Report . . .

Pege 4 ol 4

,

_Thi.documnrl.Lltu.dbyrh.conrF.yebl.cltoir'c6.6lcddrtro:ols.Blc.pnni.dderl..J,{.ll.br.onrqdd'*dbl€al

swsaod.m' .nd d;di'dn ih ;nd. ror €t.cr'o.ic remt [email protected]. sbFd to rons ond c6ndn'oN ror Er4'6hrc DaltrFr. .rffifi.-..de,mdltl'DAl.d|oh|ldRsnbrhe[frildIdo|||.bi|ity'indefrn|l|c.llon.ndjUrisdrn, h-adc-;Alh-b d-;umnr te.dvl*d |hlr intorndion cont.ln.d h.6on rd|4rs tho comp.nv's thdh$ .l lh. fine oi llt ld.mnlion onry

d; firhh $e rrmh. ol clionfs lEtruc{d3, il dy. The c.mp-v. tot. @tohslhllllv i5 lo ilr cllenr .nd rhb dod@nr d63 nol 'roMale

@nr6 ro a r,rEctid rbm.eE,.in0 . lhsir ndhl..nd obislt'bn3 uid€r irF tEn*iclio. docum-l3, Thi3 documnr o.nor b. EpEdued;ed h tu[. withdt sior wnM .!!bEt ot th. comp€ny. ary un.urh4rz€d .lt r.rion, lorgdy q l.l.iicari.n or rh6 6@nr or .pp..Bne orirri i*,*ii r'

";r"fu"r -a oll.iricr nd bo rrca;u|ad b $. tulr.lr .nFi or rh€ l$. unr€.s orhwis. .rded $' E!uh' 'hdn r' rhis

ro.r Epod ELr only ro the spl6(!) I6red lnd 3uch e.mpL{s) .E Et h6d td 60 d.y3 onlv."

Page 19: ICP Test Report Certification Packet/media/electronics... · LTTTELFUSE PHtLS., tNC. Lima Tech Center, SEZ, Lipa, Malvar, Batangas The following sample(s) was/veere submitted and

Test Report Number : TWNC00285774

Authorized By: On Behalf Of Intertek Testing Services Taiwan Limited

K. Y. Liang Director

*THJ0285774* Page 1 of 6

Intertek Testing Services Taiwan Ltd. 8F., No. 423, Ruiguang Rd., Neihu District, Taipei 114, Taiwan, R.O.C.

全國公證檢驗股份有限公司 114台北市內湖區瑞光路 423號 8樓

Tel: (+886-2) 6602-2888.2797-8885 Fax: (+886-2) 6602-2410

Applicant: Littelfuse Philippines Inc. Date : Nov 19, 2012 LIMA Technology Center, Lipa City,

Malvar, Batangas

Sample Description: One (1) group of submitted samples said to be : Part Description : Cap Part Number : 910-275 Date Sample Received : Nov 12, 2012 Date Test Started : Nov 13, 2012

Test Conducted :

As requested by the applicant, for details please refer to attached pages.

kbacila
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/ 910-554
Page 20: ICP Test Report Certification Packet/media/electronics... · LTTTELFUSE PHtLS., tNC. Lima Tech Center, SEZ, Lipa, Malvar, Batangas The following sample(s) was/veere submitted and

Number : TWNC00285774

Test Conducted

*THJ0285774* Page 2 of 6

Intertek Testing Services Taiwan Ltd. 8F., No. 423, Ruiguang Rd., Neihu District, Taipei 114, Taiwan, R.O.C.

全國公證檢驗股份有限公司 114台北市內湖區瑞光路 423號 8樓

Tel: (+886-2) 6602-2888.2797-8885 Fax: (+886-2) 6602-2410

(Ⅰ) Test Result Summary : Result (ppm)

Test Item (1) (2)

Heavy Metal

Cadmium (Cd) content ND ND

Lead (Pb) content ND ND Mercury (Hg) content ND ND

Chromium VI (Cr6+) content (mg/kg with 50cm2) Negative (< 0.02)

(#)

Negative (< 0.02)

(#)

Remarks: ppm = Parts per million based on weight of tested sample = mg/kg ND = Not detected < = Less than mg/kg with 50cm2 = milligram per kilogram with 50 square centimetre Negative = A negative test result indicated positive observation

was not found at the time of Test. # = Due to the insufficient sample area, reduced total sample

surface of 25 cm2 was used and the dilution factor was adjusted accordingly.

Tested Components (1) Coppery metal base material (2) Golden plating layer

Responsibility of Chemist :Irene Chiou / Kevin Liu

Date Sample Received : Nov 12, 2012 Test Period : Nov 13, 2012 to Nov 16, 2012

(Ⅱ) RoHS Limits:

Restricted Substances Limits

Cadmium (Cd) Content 0.01% (100ppm) Lead (Pb) Content 0.1% (1000ppm) Mercury (Hg) Content 0.1% (1000ppm) Chromium VI (Cr6+) Content 0.1% (1000ppm)

The above limits were quoted from Annex II of 2011/65/EU for homogeneous material.

Page 21: ICP Test Report Certification Packet/media/electronics... · LTTTELFUSE PHtLS., tNC. Lima Tech Center, SEZ, Lipa, Malvar, Batangas The following sample(s) was/veere submitted and

Number : TWNC00285774

Test Conducted

*THJ0285774* Page 3 of 6

Intertek Testing Services Taiwan Ltd. 8F., No. 423, Ruiguang Rd., Neihu District, Taipei 114, Taiwan, R.O.C.

全國公證檢驗股份有限公司 114台北市內湖區瑞光路 423號 8樓

Tel: (+886-2) 6602-2888.2797-8885 Fax: (+886-2) 6602-2410

(Ⅲ) Test Method:

Test Item Test Method Reporting Limit

Cadmium (Cd) content

With reference to IEC 62321 edition 1.0:2008 in clause 8/9/10, by microwave digestion until the tested samples are totally dissolved and determined by ICP-OES.

2 ppm

Lead (Pb) content

With reference to IEC 62321 edition 1.0:2008 in clause 8/9/10, by microwave digestion until the tested samples are totally dissolved and determined by ICP-OES.

2 ppm

Mercury (Hg) content

With reference to IEC 62321 edition 1.0:2008 in clause 7, by microwave digestion until the tested samples are totally dissolved and determined by ICP-OES.

2 ppm

Chromium VI (Cr6+) content

With reference to IEC 62321 edition 1.0:2008 in annex B, by boiling water extraction and determined by UV-Vis Spectrophotometer.

0.02 mg/kg with 50cm2

Remark: Reporting limit = Quantitation limit of analyte in sample

Page 22: ICP Test Report Certification Packet/media/electronics... · LTTTELFUSE PHtLS., tNC. Lima Tech Center, SEZ, Lipa, Malvar, Batangas The following sample(s) was/veere submitted and

Number : TWNC00285774

Test Conducted

*THJ0285774* Page 4 of 6

Intertek Testing Services Taiwan Ltd. 8F., No. 423, Ruiguang Rd., Neihu District, Taipei 114, Taiwan, R.O.C.

全國公證檢驗股份有限公司 114台北市內湖區瑞光路 423號 8樓

Tel: (+886-2) 6602-2888.2797-8885 Fax: (+886-2) 6602-2410

(Ⅳ) Measurement Flowchart: Test For Cd/Pb/Hg/Chromium (VI) Reference Standard:IEC 62321 edition 1.0:2008

For different material, digest the sample with appropriate acid*1

Make up with deionized water

Cd/Pb/Hg

Analyzed by ICP-OES

Confirm the tested samples are totally dissolved

Sample preparation

Take sample and immerse into Aqua Regia, start to strip plating layer

Stop the stripping procedure upon color change completely

Take the Aqua solution as plating component and stripped body as substrate component

Cr6+

Make up with deionized water and add diphenyl-carbazide solution

Analyzed by UV-VIS

By spot test

Get 50cm2 sample

By boiling water extraction

Negative *2

Substrate Plating

Page 23: ICP Test Report Certification Packet/media/electronics... · LTTTELFUSE PHtLS., tNC. Lima Tech Center, SEZ, Lipa, Malvar, Batangas The following sample(s) was/veere submitted and

Number : TWNC00285774

Test Conducted

*THJ0285774* Page 5 of 6

Intertek Testing Services Taiwan Ltd. 8F., No. 423, Ruiguang Rd., Neihu District, Taipei 114, Taiwan, R.O.C.

全國公證檢驗股份有限公司 114台北市內湖區瑞光路 423號 8樓

Tel: (+886-2) 6602-2888.2797-8885 Fax: (+886-2) 6602-2410

Remarks: *1: List Of Appropriate Acid:

Material Acid Added For Digestion

Polymers HNO3,HCl,HF,H2O2,H3BO3 Metals HNO3,HCl,HF Electronics HNO3,HCl,H2O2,HBF4

*2: If the result of spot test is positive, Chromium VI would be determined as detected.

End of Report

This report is made solely on the basis of your instructions and/or information and materials supplied by you. It is not intended to be a recommendation for any particular course of action. Intertek does not accept a duty of care or any other responsibility to any person other than the Client in respect of this report and only accepts liability to the Client insofar as is expressly contained in the terms and conditions governing Intertek's provision of services to you. Intertek makes no warranties or representations either express or implied with respect to this report save as provided for in those terms and conditions. We have aimed to conduct the Review on a diligent and careful basis and we do not accept any liability to you for any loss arising out of or in connection with this report, in contract, tort, by statute or otherwise, except in the event of our gross negligence or wilful misconduct.

Page 24: ICP Test Report Certification Packet/media/electronics... · LTTTELFUSE PHtLS., tNC. Lima Tech Center, SEZ, Lipa, Malvar, Batangas The following sample(s) was/veere submitted and

Number : TWNC00285774

Test Conducted

*THJ0285774* Page 6 of 6

Intertek Testing Services Taiwan Ltd. 8F., No. 423, Ruiguang Rd., Neihu District, Taipei 114, Taiwan, R.O.C.

全國公證檢驗股份有限公司 114台北市內湖區瑞光路 423號 8樓

Tel: (+886-2) 6602-2888.2797-8885 Fax: (+886-2) 6602-2410

Photo

Page 25: ICP Test Report Certification Packet/media/electronics... · LTTTELFUSE PHtLS., tNC. Lima Tech Center, SEZ, Lipa, Malvar, Batangas The following sample(s) was/veere submitted and

Test Report Number : TWNC00285781

Authorized By: On Behalf Of Intertek Testing Services Taiwan Limited

K. Y. Liang Director

*THJ0285781* Page 1 of 10

Intertek Testing Services Taiwan Ltd. 8F., No. 423, Ruiguang Rd., Neihu District, Taipei 114, Taiwan, R.O.C.

全國公證檢驗股份有限公司 114台北市內湖區瑞光路 423號 8樓

Tel: (+886-2) 6602-2888.2797-8885 Fax: (+886-2) 6602-2410

Applicant: Littelfuse Philippines Inc. Date : Nov 19, 2012 LIMA Technology Center, Lipa City,

Malvar, Batangas

Sample Description:

One (1) group of submitted samples said to be : Part Description : Anaerobic Adhesive Part Number : 087266 Date Sample Received : Nov 12, 2012 Date Test Started : Nov 13, 2012

Test Conducted :

As requested by the applicant, for details please refer to attached pages.

Page 26: ICP Test Report Certification Packet/media/electronics... · LTTTELFUSE PHtLS., tNC. Lima Tech Center, SEZ, Lipa, Malvar, Batangas The following sample(s) was/veere submitted and

Number : TWNC00285781

Test Conducted

*THJ0285781* Page 2 of 10

Intertek Testing Services Taiwan Ltd. 8F., No. 423, Ruiguang Rd., Neihu District, Taipei 114, Taiwan, R.O.C.

全國公證檢驗股份有限公司 114台北市內湖區瑞光路 423號 8樓

Tel: (+886-2) 6602-2888.2797-8885 Fax: (+886-2) 6602-2410

(Ⅰ) Test Result Summary : Result (ppm)

Test Item Green Liquid

Heavy Metal

Cadmium (Cd) content ND Lead (Pb) content ND Mercury (Hg) content ND Chromium VI (Cr6+) content ND

Polybrominated Biphenyls (PBBs) Monobrominated Biphenyls (MonoBB) ND Dibrominated Biphenyls (DiBB) ND Tribrominated Biphenyls (TriBB) ND Tetrabrominated Biphenyls (TetraBB) ND Pentabrominated Biphenyls (PentaBB) ND Hexabrominated Biphenyls (HexaBB) ND Heptabrominated Biphenyls (HeptaBB) ND Octabrominated Biphenyls (OctaBB) ND Nonabrominated Biphenyls (NonaBB) ND Decabrominated Biphenyl (DecaBB) ND

Polybrominated Diphenyl Ethers (PBDEs) Monobrominated Diphenyl Ethers (MonoBDE) ND Dibrominated Diphenyl Ethers (DiBDE) ND Tribrominated Diphenyl Ethers (TriBDE) ND Tetrabrominated Diphenyl Ethers (TetraBDE) ND Pentabrominated Diphenyl Ethers (PentaBDE) ND Hexabrominated Diphenyl Ethers (HexaBDE) ND Heptabrominated Diphenyl Ethers (HeptaBDE) ND Octabrominated Diphenyl Ethers (OctaBDE) ND Nonabrominated Diphenyl Ethers (NonaBDE) ND Decabrominated Diphenyl Ether (DecaBDE) ND

Page 27: ICP Test Report Certification Packet/media/electronics... · LTTTELFUSE PHtLS., tNC. Lima Tech Center, SEZ, Lipa, Malvar, Batangas The following sample(s) was/veere submitted and

Number : TWNC00285781

Test Conducted

*THJ0285781* Page 3 of 10

Intertek Testing Services Taiwan Ltd. 8F., No. 423, Ruiguang Rd., Neihu District, Taipei 114, Taiwan, R.O.C.

全國公證檢驗股份有限公司 114台北市內湖區瑞光路 423號 8樓

Tel: (+886-2) 6602-2888.2797-8885 Fax: (+886-2) 6602-2410

(Ⅰ) Test Result Summary : Result (ppm)

Test Item Green Liquid

Halogen Content Fluorine (F) ND Chlorine (Cl) ND Bromine (Br) ND Iodine (I) ND

Phthalates Di(2-ethylhexyl) Phthalate (DEHP) ND Dibutyl Phthalate (DBP) 77 Benzyl Butyl Phthalate (BBP) ND

Others Hexabromocyclododecane (HBCDD) ND

Remarks: ppm = Parts per million based on wet weight of tested sample =

mg/kg ND = Not detected

Responsibility of Chemist :Irene Chiou / Kevin Liu / Cathy Chen

Date Sample Received : Nov 12, 2012 Test Period : Nov 13, 2012 To Nov 15, 2012

(Ⅱ) RoHS Limits:

Restricted Substances Limits

Cadmium (Cd) Content 0.01% (100ppm) Lead (Pb) Content 0.1% (1000ppm) Mercury (Hg) Content 0.1% (1000ppm) Chromium VI (Cr6+) Content 0.1% (1000ppm) Polybrominated Biphenyls (PBBs) 0.1% (1000ppm) Polybrominated Diphenyl Ehters (PBDEs) 0.1% (1000ppm)

The above limits were quoted from Annex II of 2011/65/EU for homogeneous material.

Page 28: ICP Test Report Certification Packet/media/electronics... · LTTTELFUSE PHtLS., tNC. Lima Tech Center, SEZ, Lipa, Malvar, Batangas The following sample(s) was/veere submitted and

Number : TWNC00285781

Test Conducted

*THJ0285781* Page 4 of 10

Intertek Testing Services Taiwan Ltd. 8F., No. 423, Ruiguang Rd., Neihu District, Taipei 114, Taiwan, R.O.C.

全國公證檢驗股份有限公司 114台北市內湖區瑞光路 423號 8樓

Tel: (+886-2) 6602-2888.2797-8885 Fax: (+886-2) 6602-2410

(Ⅲ) Test Method: Test Item Test Method Reporting Limit

Cadmium (Cd) content

With reference to IEC 62321 edition 1.0:2008 in clause 8/9/10, by microwave digestion until the tested samples are totally dissolved and determined by ICP-OES.

2 ppm

Lead (Pb) content

With reference to IEC 62321 edition 1.0:2008 in clause 8/9/10, by microwave digestion until the tested samples are totally dissolved and determined by ICP-OES.

2 ppm

Mercury (Hg) content

With reference to IEC 62321 edition 1.0:2008 in clause 7, by microwave digestion until the tested samples are totally dissolved and determined by ICP-OES.

2 ppm

Chromium VI (Cr6+) content

With reference to IEC 62321 edition 1.0:2008 in annex C, by alkaline digestion and determined by UV-Vis spectrophotometer.

1 ppm

Polybrominated Biphenyls (PBBs)

With reference to IEC 62321 edition 1.0:2008 in annex A, by solvent extraction and determined by GC-MS and further HPLC-DAD confirmation when necessary.

5 ppm

Polybrominated Diphenyl Ethers (PBDEs)

With reference to IEC 62321 edition 1.0:2008 in annex A, by solvent extraction and determined by GC-MS and further HPLC-DAD confirmation when necessary.

5 ppm

Halogen Content With reference to EN 14582:2007 by calorimetric bomb with oxygen and determined by Ion Chromatograph.

50 ppm

Phthalates With reference to EN 14372: 2004, bysolvent extraction and determined byGC-MS.

50 ppm

Hexabromocyclododecane(HBCDD)

With reference to USEPA 3540C, by solvent extraction and determined byGC-MS.

10 ppm

Remark: Reporting limit = Quantitation limit of analyte in sample

Page 29: ICP Test Report Certification Packet/media/electronics... · LTTTELFUSE PHtLS., tNC. Lima Tech Center, SEZ, Lipa, Malvar, Batangas The following sample(s) was/veere submitted and

Number : TWNC00285781

Test Conducted

*THJ0285781* Page 5 of 10

Intertek Testing Services Taiwan Ltd. 8F., No. 423, Ruiguang Rd., Neihu District, Taipei 114, Taiwan, R.O.C.

全國公證檢驗股份有限公司 114台北市內湖區瑞光路 423號 8樓

Tel: (+886-2) 6602-2888.2797-8885 Fax: (+886-2) 6602-2410

(Ⅳ) Measurement Flowchart: Test for Cd/Pb/Hg/Chromium (VI)/PBBS/PBDES Contents Reference Standard: IEC 62321 edition 1.0:2008

Weigh sample and add organic solvent

By Soxhlet extraction or Solvent extraction

Concentrate the extract and make upwith organic solvent

PBBs/PBDEs

Analyzed by GC-MSD

Sample preparation

Take sample and immerse into Aqua Regia, start to strip plating layer

Stop the stripping procedure upon color change completely

Take the Aqua solution as plating component and stripped body as substrate component

For non-metal part For metal part

Make up with deionized water and add diphenyl-carbazide solution

Cr6+

Analyzed by UV-VIS

By spot test

Get 50cm2 sample

By boiling water extraction

Negative *2

Substrate Plating

Weigh sample and add alkaline solution

Definite temp. extraction

Cool and filter the extract

Cr6+

For different material, digest the sample with appropriate acid*1

Make up with deionized water

Cd/Pb/Hg

Analyzed by ICP-OES

Confirm the tested samples are totally dissolved

Page 30: ICP Test Report Certification Packet/media/electronics... · LTTTELFUSE PHtLS., tNC. Lima Tech Center, SEZ, Lipa, Malvar, Batangas The following sample(s) was/veere submitted and

Number : TWNC00285781

Test Conducted

*THJ0285781* Page 6 of 10

Intertek Testing Services Taiwan Ltd. 8F., No. 423, Ruiguang Rd., Neihu District, Taipei 114, Taiwan, R.O.C.

全國公證檢驗股份有限公司 114台北市內湖區瑞光路 423號 8樓

Tel: (+886-2) 6602-2888.2797-8885 Fax: (+886-2) 6602-2410

(Ⅳ) Measurement Flowchart: Remarks: *1: List of Appropriate Acid:

Material Acid Added for Digestion

Polymers HNO3,HCl,HF,H2O2,H3BO3 Metals HNO3,HCl,HF Electronics HNO3,HCl,H2O2,HBF4

*2: If the result of spot test is positive, Chromium VI would be determined as detected.

Page 31: ICP Test Report Certification Packet/media/electronics... · LTTTELFUSE PHtLS., tNC. Lima Tech Center, SEZ, Lipa, Malvar, Batangas The following sample(s) was/veere submitted and

Number : TWNC00285781

Test Conducted

*THJ0285781* Page 7 of 10

Intertek Testing Services Taiwan Ltd. 8F., No. 423, Ruiguang Rd., Neihu District, Taipei 114, Taiwan, R.O.C.

全國公證檢驗股份有限公司 114台北市內湖區瑞光路 423號 8樓

Tel: (+886-2) 6602-2888.2797-8885 Fax: (+886-2) 6602-2410

(Ⅳ) Measurement Flowchart: Test for Halogen Content Reference Standard:EN 14582

Add absorbent in a combustion flask & place weighed sample in equipment

Fill oxygen into calorimetric bomb

Ignite then leave the bomb at room temperature

Transfer the absorbent into a volumetric flask

Make up with deionized water

Sampling/grinding or cutting

Analyzed by ion chromatography

Page 32: ICP Test Report Certification Packet/media/electronics... · LTTTELFUSE PHtLS., tNC. Lima Tech Center, SEZ, Lipa, Malvar, Batangas The following sample(s) was/veere submitted and

Number : TWNC00285781

Test Conducted

*THJ0285781* Page 8 of 10

Intertek Testing Services Taiwan Ltd. 8F., No. 423, Ruiguang Rd., Neihu District, Taipei 114, Taiwan, R.O.C.

全國公證檢驗股份有限公司 114台北市內湖區瑞光路 423號 8樓

Tel: (+886-2) 6602-2888.2797-8885 Fax: (+886-2) 6602-2410

(Ⅳ) Measurement Flowchart:

Test For Phthalates Contents Reference Method: EN 14372: 2004

Sampling/grinding or cutting

Weigh sample and add organic solvent

By solvent extraction

Concentrate the extract and make up with organic solvent

Analyzed by GC-MSD

Page 33: ICP Test Report Certification Packet/media/electronics... · LTTTELFUSE PHtLS., tNC. Lima Tech Center, SEZ, Lipa, Malvar, Batangas The following sample(s) was/veere submitted and

Number : TWNC00285781

Test Conducted

*THJ0285781* Page 9 of 10

Intertek Testing Services Taiwan Ltd. 8F., No. 423, Ruiguang Rd., Neihu District, Taipei 114, Taiwan, R.O.C.

全國公證檢驗股份有限公司 114台北市內湖區瑞光路 423號 8樓

Tel: (+886-2) 6602-2888.2797-8885 Fax: (+886-2) 6602-2410

(Ⅳ) Measurement Flowchart:

Test For Hexabromocyclododecane (HBCDD) Reference Standard:USEPA 3540C

End of Report

This report is made solely on the basis of your instructions and/or information and materials supplied by you. It is not intended to be a recommendation for any particular course of action. Intertek does not accept a duty of care or any other responsibility to any person other than the Client in respect of this report and only accepts liability to the Client insofar as is expressly contained in the terms and conditions governing Intertek's provision of services to you. Intertek makes no warranties or representations either express or implied with respect to this report save as provided for in those terms and conditions. We have aimed to conduct the Review on a diligent and careful basis and we do not accept any liability to you for any loss arising out of or in connection with this report, in contract, tort, by statute or otherwise, except in the event of our gross negligence or wilful misconduct.

Sampling/grinding or cutting

Weigh sample and add organic solvent

By soxhlet extraction

Concentrate the extract and make up with organic solvent

Analyzed by GC-MSD

Page 34: ICP Test Report Certification Packet/media/electronics... · LTTTELFUSE PHtLS., tNC. Lima Tech Center, SEZ, Lipa, Malvar, Batangas The following sample(s) was/veere submitted and

Number : TWNC00285781

Test Conducted

*THJ0285781* Page 10 of 10

Intertek Testing Services Taiwan Ltd. 8F., No. 423, Ruiguang Rd., Neihu District, Taipei 114, Taiwan, R.O.C.

全國公證檢驗股份有限公司 114台北市內湖區瑞光路 423號 8樓

Tel: (+886-2) 6602-2888.2797-8885 Fax: (+886-2) 6602-2410

Photo

Page 35: ICP Test Report Certification Packet/media/electronics... · LTTTELFUSE PHtLS., tNC. Lima Tech Center, SEZ, Lipa, Malvar, Batangas The following sample(s) was/veere submitted and

Intertek Consumer Goods GmbH · Würzburger Straße 152 · 90766 Fürth ·

Durch die DAkkS nach DIN EN ISO/IEC 17025 akkreditiertes Prüflaboratorium Die Akkreditierung gilt für die in der Urkunde aufgeführten Prüfverfahren.

Intertek Consumer Goods GmbH Tel.: +49 911 74075 0 Sitz Fürth Geschäftsführer Würzburger Straße 152 Fax: +49 911 74075 30 Amtsgericht Fürth, HRB 5756 Kay Grönhardt 90766 Fürth, Germany [email protected] USt-IdNr. DE169317871 Rainer Mast

Polyfil AG Gina Gregorio Oberallmendstrasse 20A 6300 Zug / Switzerland

Fürth, 2012-12-19 Test report No. FUHL1236923 Testing of a material sample according to the RoHS directive 2011/65/EC Sample description: Ag1000 wire; part no. 4500236620; batch 13891141 Arrival in lab: 2012-012-04; Period of XRF analysis incl. sample preparation and photo documentation: 2012-12-07 – 2012-12-10 Head of Inorganic Lab: Claudia List Copying this test report is permitted only in agreement with the contracted lab. The test results refer only to the tested item. This report consists of 6 page(s). The test methods signed with * are not listed in the attachment of the accreditation certificate.

Conclusion based on tested item Test order Status testing according to the RoHS directive 2011/65/EC conform° ° Please see overview of test results - Test results see next pages -

Page 36: ICP Test Report Certification Packet/media/electronics... · LTTTELFUSE PHtLS., tNC. Lima Tech Center, SEZ, Lipa, Malvar, Batangas The following sample(s) was/veere submitted and

Page 2 of 6 page(s) of our test report No. FUHL1236923 dated 2012-12-19

Sample description: Ag1000 wire; part no. 4500236620; batch 13891141

Intertek Consumer Goods GmbH Tel.: +49 911 74075 0 Sitz Fürth Geschäftsführer Würzburger Straße 152 Fax: +49 911 74075 30 Amtsgericht Fürth, HRB 5756 Kay Grönhardt 90766 Fürth, Germany [email protected] Ust-IdNr. DE169317871 Rainer Mast

nM = non Metal M = Metal cM = composite Material List of component parts:

Sample No. Part No. Material Description

236923 1 M Ag1000 wire; part no. 4500236620; batch 13891141

Page 37: ICP Test Report Certification Packet/media/electronics... · LTTTELFUSE PHtLS., tNC. Lima Tech Center, SEZ, Lipa, Malvar, Batangas The following sample(s) was/veere submitted and

Page 3 of 6 page(s) of our test report No. FUHL1236923 dated 2012-12-19

Sample description: Ag1000 wire; part no. 4500236620; batch 13891141

Intertek Consumer Goods GmbH Tel.: +49 911 74075 0 Sitz Fürth Geschäftsführer Würzburger Straße 152 Fax: +49 911 74075 30 Amtsgericht Fürth, HRB 5756 Kay Grönhardt 90766 Fürth, Germany [email protected] Ust-IdNr. DE169317871 Rainer Mast

Comment

LOD = Limit of Detection

BL = Below Limit OL = Over Limit X = Inconclusive, further test necessary σ = Standard deviation CS = Composite sample

Remark: Results were obtained by EDXRF for primary screening. Additional chemical testing using ICP (for Cd, Pb), AAS (for Hg), IC-UC/VIS (for CrVI) and GC/MS (for PBBs/PBDEs) are recommended, if the concentration exceeds the below warning value according to IEC 62321. Element Unit non - metal metal

Cd mg / kg BL ≤ (70-3σ) < X < (130+3σ) ≤ OL BL ≤ (70-3σ) < X < (130+3σ) ≤ OL Pb mg / kg BL ≤ (700-3σ) < X < (1300+3σ) ≤ OL BL ≤ (700-3σ) < X < (1300+3σ) ≤ OL Hg mg / kg BL ≤ (700-3σ) < X < (1300+3σ) ≤ OL BL ≤ (700-3σ) < X < (1300+3σ) ≤ OL Br mg / kg BL ≤ (300-3σ) < X -- Cr mg / kg BL ≤ (700-3σ) < X BL ≤ (700-3σ) < X

Element Unit composite material

Cd mg / kg LOD < X < (150+3σ) ≤ OL Pb mg / kg BL ≤ (500-3σ) < X < (1500+3σ) ≤ OL Hg mg / kg BL ≤ (500-3σ) < X < (1500+3σ) ≤ OL Br mg / kg BL ≤ (250-3σ) < X Cr mg / kg BL ≤ (500-3σ) < X

Page 38: ICP Test Report Certification Packet/media/electronics... · LTTTELFUSE PHtLS., tNC. Lima Tech Center, SEZ, Lipa, Malvar, Batangas The following sample(s) was/veere submitted and

Page 4 of 6 page(s) of our test report No. FUHL1236923 dated 2012-12-19

Sample description: Ag1000 wire; part no. 4500236620; batch 13891141

Intertek Consumer Goods GmbH Tel.: +49 911 74075 0 Sitz Fürth Geschäftsführer Würzburger Straße 152 Fax: +49 911 74075 30 Amtsgericht Fürth, HRB 5756 Kay Grönhardt 90766 Fürth, Germany [email protected] Ust-IdNr. DE169317871 Rainer Mast

1. XRF screening Method: XRF according to IEC 62321:2008*

Sample No. Part No. Pb Hg Cd Crtotal Br Status 236923 1 BL BL BL BL -- conform

Comment: Elements RoHS-limit value Lead (Pb) 1000 mg/kg Mercury (Hg) 1000 mg/kg Cadmium (Cd) 100 mg/kg Chromium VI (Cr VI) 1000 mg/kg Polybrominated Biphenyle (PBBs) 1000 mg/kg Polybrominated Diphenyl ether (PBDEs) 1000 mg/kg

- Flow charts see next page(s) -

Page 39: ICP Test Report Certification Packet/media/electronics... · LTTTELFUSE PHtLS., tNC. Lima Tech Center, SEZ, Lipa, Malvar, Batangas The following sample(s) was/veere submitted and

Page 5 of 6 page(s) Test procedure

Intertek Consumer Goods GmbH Tel.: +49 911 74075 0 Sitz Fürth Geschäftsführer Würzburger Straße 152 Fax: +49 911 74075 30 Amtsgericht Fürth, HRB 5756 Kay Grönhardt 90766 Fürth, Germany [email protected] Ust-IdNr. DE169317871 Rainer Mast

YES

YES

YES

YES

YES

NO

NO NO

NO

NO

samples

metallic materials,

polymer materials,

electronics (PCB / component)

mechanical

sample preparation

mechanical

sample preparation

screening by XRF ?

sample uniform ?

screening procedure

by XRF

chemical test procedure (verification)

various methods (please see verification test

procedure below)

meets limits ?

further testing ?

meets limits ?

pass

entity based conforming

sample

fail

entity based non conforming

sample

pass

entity based conforming

sample

fail

entity based non conforming

sample

non-destructive

sample preparation

Page 40: ICP Test Report Certification Packet/media/electronics... · LTTTELFUSE PHtLS., tNC. Lima Tech Center, SEZ, Lipa, Malvar, Batangas The following sample(s) was/veere submitted and

Page 6 of 6 page(s) Verification test procedure

Intertek Consumer Goods GmbH Tel.: +49 911 74075 0 Sitz Fürth Geschäftsführer Würzburger Straße 152 Fax: +49 911 74075 30 Amtsgericht Fürth, HRB 5756 Kay Grönhardt 90766 Fürth, Germany [email protected] Ust-IdNr. DE169317871 Rainer Mast

Sample Preparation

Sample Measurement

Sample solvent extraction

Concentration/ Dilution of extraction

solution

Filtration

GC/MS

DATA

Acid digestion with microwave / hotplate

Filtration

Residue

Total digestion

Solution

ICP-OES/AAS

DATA

Non-metallic material

Alkaline extraction Adding extraction

solution

Alkaline extraction Heating to 90~95°C

for extraction

Filtration and pH adjustment

Adding 1,5-diphenylcarbazide

for color development

UV-VIS or IC-UV/VIS

DATA

Metallic material

Spot test

Boiling water extraction

Adding 1,5-diphenylcarbazide

for color development

A red color indicates the presence of Cr6+ If necessary, confirm

with UV-VIS or IC-UV/VIS

DATA

Pb/Cd/Hg PBBs/PBDEs Cr6+

Positive

Negative

Page 41: ICP Test Report Certification Packet/media/electronics... · LTTTELFUSE PHtLS., tNC. Lima Tech Center, SEZ, Lipa, Malvar, Batangas The following sample(s) was/veere submitted and

Test Report Number : TWNC00293764

Authorized by: On Behalf of Intertek Testing Services Taiwan Limited

K. Y. Liang Director

*THJ0293764* Page 1 of 5

Intertek Testing Services Taiwan Ltd. 8F., No. 423, Ruiguang Rd., Neihu District, Taipei 11492, Taiwan, R.O.C.

全國公證檢驗股份有限公司 11492 台北市內湖區瑞光路 423 號 8 樓

Tel: (+886-2) 6602-2888.2797-8885 Fax: (+886-2) 6602-2410

Applicant: Littelfuse Philippines Inc. Date : Jan 14, 2013 LIMA Technology Center, Lipa City,

Malvar, Batangas

Sample Description:

One (1) group of submitted samples said to be : Part Description : Element (Silver Strip Sn Plated) Part Number : 079026 Date Sample Received : Jan 07, 2013 Date Test Started : Jan 08, 2013

Test Conducted :

As requested by the applicant, for details please refer to attached pages.

Page 42: ICP Test Report Certification Packet/media/electronics... · LTTTELFUSE PHtLS., tNC. Lima Tech Center, SEZ, Lipa, Malvar, Batangas The following sample(s) was/veere submitted and

Number : TWNC00293764

Test Conducted

*THJ0293764* Page 2 of 5

Intertek Testing Services Taiwan Ltd. 8F., No. 423, Ruiguang Rd., Neihu District, Taipei 11492, Taiwan, R.O.C.

全國公證檢驗股份有限公司 11492 台北市內湖區瑞光路 423 號 8 樓

Tel: (+886-2) 6602-2888.2797-8885 Fax: (+886-2) 6602-2410

(Ⅰ) Test Result Summary: Result

Test Item Unit Test Method Silvery metal

RL

Heavy Metal

Cadmium (Cd) content ppm

With reference to IEC 62321: 2008, by microwave digestion and determined by ICP-OES.

ND 2

Lead (Pb) content ppm

With reference to IEC 62321: 2008, by microwave digestion and determined by ICP-OES.

34 2

Mercury (Hg) content ppm

With reference to IEC 62321: 2008, by microwave digestion and determined by ICP-OES.

ND 2

Chromium VI (Cr6+) content mg/kg with 50 cm2

With reference to IEC 62321: 2008, by boiling water extraction and determined by UV-Vis Spectrophotometer.

Negative 0.02

Remarks: ppm = parts per million based on weight of tested sample = mg/kg

ND = Not detected

RL = Reporting Limit, Quantitation limit of analyte in sample mg/kg with 50cm2 = milligram per kilogram with 50 square centimeter

Negative = A negative test result indicated positive observation was not found at the time of Test. When the spot test showed a negative result, the boiling water extraction procedure shall be used to verify the result.

Responsibility of Chemist: Kevin Liu/ Irene Chiou Date Sample Received : Jan 07, 2013 Test Period : Jan 08, 2013 To Jan 11, 2013 (Ⅱ) RoHS Limits: Restricted Substances Limits

Cadmium (Cd) content 0.01% (100ppm) Lead (Pb) content 0.1% (1000ppm) Mercury (Hg) content 0.1% (1000ppm) Chromium VI (Cr6+) content 0.1% (1000ppm) The above limits were quoted from Annex II of 2011/65/EU for homogeneous material.

Page 43: ICP Test Report Certification Packet/media/electronics... · LTTTELFUSE PHtLS., tNC. Lima Tech Center, SEZ, Lipa, Malvar, Batangas The following sample(s) was/veere submitted and

Number : TWNC00293764

Test Conducted

*THJ0293764* Page 3 of 5

Intertek Testing Services Taiwan Ltd. 8F., No. 423, Ruiguang Rd., Neihu District, Taipei 11492, Taiwan, R.O.C.

全國公證檢驗股份有限公司 11492 台北市內湖區瑞光路 423 號 8 樓

Tel: (+886-2) 6602-2888.2797-8885 Fax: (+886-2) 6602-2410

(Ⅲ) Measurement Flowchart: Test For Cd/Pb/Hg/Chromium (VI) Reference Standard:IEC 62321 edition 1.0:2008

Sampling/grinding or cutting

For different material, digest the sample with appropriate acid*1

Make up with deionized water

Cd/Pb/Hg

Analyzed by ICP-OES

Weigh sample and add alkaline solution

Definite temp. extraction

Make up with deionized water and add diphenyl-carbazide solution

Cool and filter the extract

Cr6+

Analyzed by UV-VIS

By spot test

Get 50cm2 sample

Boiling water extraction

Metal Polymers / Electronics

Negative*2 Confirm the tested samples are totally dissolved

Page 44: ICP Test Report Certification Packet/media/electronics... · LTTTELFUSE PHtLS., tNC. Lima Tech Center, SEZ, Lipa, Malvar, Batangas The following sample(s) was/veere submitted and

Number : TWNC00293764

Test Conducted

*THJ0293764* Page 4 of 5

Intertek Testing Services Taiwan Ltd. 8F., No. 423, Ruiguang Rd., Neihu District, Taipei 11492, Taiwan, R.O.C.

全國公證檢驗股份有限公司 11492 台北市內湖區瑞光路 423 號 8 樓

Tel: (+886-2) 6602-2888.2797-8885 Fax: (+886-2) 6602-2410

Remarks: *1: List of Appropriate Acid: Material Acid Added for Digestion Polymers HNO3,HCl,HF,H2O2,H3BO3 Metals HNO3,HCl,HF Electronics HNO3,HCl,H2O2,HBF4

*2: If the result of spot test is positive, Chromium VI would be determined as

detected.

End of Report

This report is made solely on the basis of your instructions and/or information and materials supplied by you. It is not intended to be a recommendation for any particular course of action. Intertek does not accept a duty of care or any other responsibility to any person other than the Client in respect of this report and only accepts liability to the Client insofar as is expressly contained in the terms and conditions governing Intertek's provision of services to you. Intertek makes no warranties or representations either express or implied with respect to this report save as provided for in those terms and conditions. We have aimed to conduct the Review on a diligent and careful basis and we do not accept any liability to you for any loss arising out of or in connection with this report, in contract, tort, by statute or otherwise, except in the event of our gross negligence or wilful misconduct.

Page 45: ICP Test Report Certification Packet/media/electronics... · LTTTELFUSE PHtLS., tNC. Lima Tech Center, SEZ, Lipa, Malvar, Batangas The following sample(s) was/veere submitted and

Number : TWNC00293764

Test Conducted

*THJ0293764* Page 5 of 5

Intertek Testing Services Taiwan Ltd. 8F., No. 423, Ruiguang Rd., Neihu District, Taipei 11492, Taiwan, R.O.C.

全國公證檢驗股份有限公司 11492 台北市內湖區瑞光路 423 號 8 樓

Tel: (+886-2) 6602-2888.2797-8885 Fax: (+886-2) 6602-2410

Photo

Page 46: ICP Test Report Certification Packet/media/electronics... · LTTTELFUSE PHtLS., tNC. Lima Tech Center, SEZ, Lipa, Malvar, Batangas The following sample(s) was/veere submitted and

Test Report Number : TWNC00285770

Authorized By: On Behalf Of Intertek Testing Services Taiwan Limited

K. Y. Liang Director

*THJ0285770* Page 1 of 6

Intertek Testing Services Taiwan Ltd. 8F., No. 423, Ruiguang Rd., Neihu District, Taipei 114, Taiwan, R.O.C.

全國公證檢驗股份有限公司 114台北市內湖區瑞光路 423號 8樓

Tel: (+886-2) 6602-2888.2797-8885 Fax: (+886-2) 6602-2410

Applicant: Littelfuse Philippines Inc. Date : Nov 19, 2012 LIMA Technology Center, Lipa City,

Malvar, Batangas

Sample Description:

One (1) group of submitted samples said to be : Part Description : Solder (Pb is ≥ 90%) Part Number : 692323 Date Sample Received : Nov 12, 2012 Date Test Started : Nov 13, 2012

Test Conducted :

As requested by the applicant, for details please refer to attached pages.

Page 47: ICP Test Report Certification Packet/media/electronics... · LTTTELFUSE PHtLS., tNC. Lima Tech Center, SEZ, Lipa, Malvar, Batangas The following sample(s) was/veere submitted and

Number : TWNC00285770

Test Conducted

*THJ0285770* Page 2 of 6

Intertek Testing Services Taiwan Ltd. 8F., No. 423, Ruiguang Rd., Neihu District, Taipei 114, Taiwan, R.O.C.

全國公證檢驗股份有限公司 114台北市內湖區瑞光路 423號 8樓

Tel: (+886-2) 6602-2888.2797-8885 Fax: (+886-2) 6602-2410

(Ⅰ) Test Result Summary : Result (ppm)

Test Item Silvery Metal

Heavy Metal

Cadmium (Cd) content ND

Lead (Pb) content 910679 Mercury (Hg) content ND Chromium VI (Cr6+) content (mg/kg with 50cm2) Negative (< 0.02)

Remarks: ppm = Parts per million based on weight of tested sample = mg/kg ND = Not detected < = Less than mg/kg with 50cm2 = milligram per kilogram with 50 square centimetre Negative = A negative test result indicated positive observation

was not found at the time of Test.

Responsibility of Chemist :Irene Chiou / Kevin Liu

Date Sample Received : Nov 12, 2012 Test Period : Nov 13, 2012 To Nov 15, 2012

(Ⅱ) RoHS Limits:

Restricted Substances Limits

Cadmium (Cd) Content 0.01% (100ppm) Lead (Pb) Content 0.1% (1000ppm) Mercury (Hg) Content 0.1% (1000ppm) Chromium VI (Cr6+) Content 0.1% (1000ppm)

The above limits were quoted from Annex II of 2011/65/EU for homogeneous material.

Page 48: ICP Test Report Certification Packet/media/electronics... · LTTTELFUSE PHtLS., tNC. Lima Tech Center, SEZ, Lipa, Malvar, Batangas The following sample(s) was/veere submitted and

Number : TWNC00285770

Test Conducted

*THJ0285770* Page 3 of 6

Intertek Testing Services Taiwan Ltd. 8F., No. 423, Ruiguang Rd., Neihu District, Taipei 114, Taiwan, R.O.C.

全國公證檢驗股份有限公司 114台北市內湖區瑞光路 423號 8樓

Tel: (+886-2) 6602-2888.2797-8885 Fax: (+886-2) 6602-2410

(Ⅲ) Test Method: Test Item Test Method Reporting Limit

Cadmium (Cd) content

With reference to IEC 62321 edition 1.0:2008 in clause 8/9/10, by microwave digestion until the tested samples are totally dissolved and determined by ICP-OES.

2 ppm

Lead (Pb) content

With reference to IEC 62321 edition 1.0:2008 in clause 8/9/10, by microwave digestion until the tested samples are totally dissolved and determined by ICP-OES.

2 ppm

Mercury (Hg) content

With reference to IEC 62321 edition 1.0:2008 in clause 7, by microwave digestion until the tested samples are totally dissolved and determined by ICP-OES.

2 ppm

Chromium VI (Cr6+) content

With reference to IEC 62321 edition 1.0:2008 in annex B, by boiling water extraction and determined by UV-Vis Spectrophotometer.

0.02 mg/kg with 50cm2

Remark: Reporting limit = Quantitation limit of analyte in sample

Page 49: ICP Test Report Certification Packet/media/electronics... · LTTTELFUSE PHtLS., tNC. Lima Tech Center, SEZ, Lipa, Malvar, Batangas The following sample(s) was/veere submitted and

Number : TWNC00285770

Test Conducted

*THJ0285770* Page 4 of 6

Intertek Testing Services Taiwan Ltd. 8F., No. 423, Ruiguang Rd., Neihu District, Taipei 114, Taiwan, R.O.C.

全國公證檢驗股份有限公司 114台北市內湖區瑞光路 423號 8樓

Tel: (+886-2) 6602-2888.2797-8885 Fax: (+886-2) 6602-2410

(Ⅳ) Measurement Flowchart: Test For Cd/Pb/Hg/Chromium (VI) Reference Standard:IEC 62321 edition 1.0:2008

Sampling/grinding or cutting

For different material, digest the sample with appropriate acid*1

Make up with deionized water

Cd/Pb/Hg

Analyzed by ICP-OES

Weigh sample and add alkaline solution

Definite temp. extraction

Make up with deionized water and add diphenyl-carbazide solution

Cool and filter the extract

Cr6+

Analyzed by UV-VIS

By spot test

Get 50cm2 sample

Boiling water extraction

Metal Polymers / Electronics

Negative*2 Confirm the tested samples are totally dissolved

Page 50: ICP Test Report Certification Packet/media/electronics... · LTTTELFUSE PHtLS., tNC. Lima Tech Center, SEZ, Lipa, Malvar, Batangas The following sample(s) was/veere submitted and

Number : TWNC00285770

Test Conducted

*THJ0285770* Page 5 of 6

Intertek Testing Services Taiwan Ltd. 8F., No. 423, Ruiguang Rd., Neihu District, Taipei 114, Taiwan, R.O.C.

全國公證檢驗股份有限公司 114台北市內湖區瑞光路 423號 8樓

Tel: (+886-2) 6602-2888.2797-8885 Fax: (+886-2) 6602-2410

(Ⅳ) Measurement Flowchart:

Remarks: *1: List of Appropriate Acid: Material Acid Added for Digestion Polymers HNO3,HCl,HF,H2O2,H3BO3 Metals HNO3,HCl,HF Electronics HNO3,HCl,H2O2,HBF4

*2: If the result of spot test is positive, Chromium VI would be determined as

detected.

End of Report

This report is made solely on the basis of your instructions and/or information and materials supplied by you. It is not intended to be a recommendation for any particular course of action. Intertek does not accept a duty of care or any other responsibility to any person other than the Client in respect of this report and only accepts liability to the Client insofar as is expressly contained in the terms and conditions governing Intertek's provision of services to you. Intertek makes no warranties or representations either express or implied with respect to this report save as provided for in those terms and conditions. We have aimed to conduct the Review on a diligent and careful basis and we do not accept any liability to you for any loss arising out of or in connection with this report, in contract, tort, by statute or otherwise, except in the event of our gross negligence or wilful misconduct.

Page 51: ICP Test Report Certification Packet/media/electronics... · LTTTELFUSE PHtLS., tNC. Lima Tech Center, SEZ, Lipa, Malvar, Batangas The following sample(s) was/veere submitted and

Number : TWNC00285770

Test Conducted

*THJ0285770* Page 6 of 6

Intertek Testing Services Taiwan Ltd. 8F., No. 423, Ruiguang Rd., Neihu District, Taipei 114, Taiwan, R.O.C.

全國公證檢驗股份有限公司 114台北市內湖區瑞光路 423號 8樓

Tel: (+886-2) 6602-2888.2797-8885 Fax: (+886-2) 6602-2410

Photo

Page 52: ICP Test Report Certification Packet/media/electronics... · LTTTELFUSE PHtLS., tNC. Lima Tech Center, SEZ, Lipa, Malvar, Batangas The following sample(s) was/veere submitted and

Test Report Number : TWNC00253636

Authorized By: On Behalf Of Intertek Testing Services Taiwan Limited

K. Y. Liang Director

This report shall not be reproduced except in full, without the written approval of the laboratory.

Page 1 of 9 Intertek Testing Services Taiwan Ltd.

8F., No. 423, Ruiguang Rd., Neihu District, Taipei 114, Taiwan, R.O.C. 全國公證檢驗股份有限公司 114台北市內湖區瑞光路 423號 8樓

Tel: (+886-2) 6602-2888.2797-8885 Fax: (+886-2) 6602-2400.6602-2401

Applicant: Littelfuse Philippines Inc. Date : Apr 24, 2012 LIMA Technology Center, Lipa City,

Malvar, Batangas

Sample Description: One (1) group of submitted samples said to be : Part Description : Black Ink Part Number : 425809 Date Sample Received : Apr 19, 2012 Date Test Started : Apr 19, 2012

Test Conducted :

As requested by the applicant, for details please refer to attached pages.

Page 53: ICP Test Report Certification Packet/media/electronics... · LTTTELFUSE PHtLS., tNC. Lima Tech Center, SEZ, Lipa, Malvar, Batangas The following sample(s) was/veere submitted and

Number : TWNC00253636

Test Conducted

Page 2 of 9 Intertek Testing Services Taiwan Ltd.

8F., No. 423, Ruiguang Rd., Neihu District, Taipei 114, Taiwan, R.O.C. 全國公證檢驗股份有限公司 114台北市內湖區瑞光路 423號 8樓

Tel: (+886-2) 6602-2888.2797-8885 Fax: (+886-2) 6602-2400.6602-2401

(Ⅰ) Test Result Summary : Result (ppm)

Test Item Black Paste

Heavy Metal

Cadmium (Cd) content ND Lead (Pb) content ND Mercury (Hg) content ND Chromium VI (Cr6+) content ND

Polybrominated Biphenyls (PBBs) Monobrominated Biphenyls (MonoBB) ND Dibrominated Biphenyls (DiBB) ND Tribrominated Biphenyls (TriBB) ND Tetrabrominated Biphenyls (TetraBB) ND Pentabrominated Biphenyls (PentaBB) ND Hexabrominated Biphenyls (HexaBB) ND Heptabrominated Biphenyls (HeptaBB) ND Octabrominated Biphenyls (OctaBB) ND Nonabrominated Biphenyls (NonaBB) ND Decabrominated Biphenyl (DecaBB) ND

Polybrominated Diphenyl Ethers (PBDEs) Monobrominated Diphenyl Ethers (MonoBDE) ND Dibrominated Diphenyl Ethers (DiBDE) ND Tribrominated Diphenyl Ethers (TriBDE) ND Tetrabrominated Diphenyl Ethers (TetraBDE) ND Pentabrominated Diphenyl Ethers (PentaBDE) ND Hexabrominated Diphenyl Ethers (HexaBDE) ND Heptabrominated Diphenyl Ethers (HeptaBDE) ND Octabrominated Diphenyl Ethers (OctaBDE) ND Nonabrominated Diphenyl Ethers (NonaBDE) ND Decabrominated Diphenyl Ether (DecaBDE) ND

Page 54: ICP Test Report Certification Packet/media/electronics... · LTTTELFUSE PHtLS., tNC. Lima Tech Center, SEZ, Lipa, Malvar, Batangas The following sample(s) was/veere submitted and

Number : TWNC00253636

Test Conducted

Page 3 of 9 Intertek Testing Services Taiwan Ltd.

8F., No. 423, Ruiguang Rd., Neihu District, Taipei 114, Taiwan, R.O.C. 全國公證檢驗股份有限公司 114台北市內湖區瑞光路 423號 8樓

Tel: (+886-2) 6602-2888.2797-8885 Fax: (+886-2) 6602-2400.6602-2401

(Ⅰ) Test Result Summary : Result (ppm)

Test Item Black Paste

Halogen Content Fluorine (F) ND Chlorine (Cl) 610 Bromine (Br) ND Iodine (I) ND

Phthalates Di(2-ethylhexyl) Phthalate (DEHP) ND Dibutyl Phthalate (DBP) ND Benzyl Butyl Phthalate (BBP) ND

Others Hexabromocyclododecane (HBCDD) ND

Remarks: ppm = Parts per million based on wet weight of tested sample =

mg/kg ND = Not detected

Responsibility of Chemist :Irene Chiou / Kevin Liu / Cathy Chen

Date Sample Received : Apr 19, 2012 Test Period : Apr 19, 2012 To Apr 24, 2012

(Ⅱ) RoHS Requirement:

Restricted Substances Limits

Cadmium (Cd) Content 0.01% (100ppm) Lead (Pb) Content 0.1% (1000ppm) Mercury (Hg) Content 0.1% (1000ppm) Chromium VI (Cr6+) Content 0.1% (1000ppm) Polybrominated Biphenyls (PBBs) 0.1% (1000ppm) Polybrominated Diphenyl Ehters (PBDEs) 0.1% (1000ppm)

The above limits were quoted from 2002/95/EC and amendment 2005/618/EC for homogeneous material.

Page 55: ICP Test Report Certification Packet/media/electronics... · LTTTELFUSE PHtLS., tNC. Lima Tech Center, SEZ, Lipa, Malvar, Batangas The following sample(s) was/veere submitted and

Number : TWNC00253636

Test Conducted

Page 4 of 9 Intertek Testing Services Taiwan Ltd.

8F., No. 423, Ruiguang Rd., Neihu District, Taipei 114, Taiwan, R.O.C. 全國公證檢驗股份有限公司 114台北市內湖區瑞光路 423號 8樓

Tel: (+886-2) 6602-2888.2797-8885 Fax: (+886-2) 6602-2400.6602-2401

(Ⅲ) Test Method: Test Item Test Method Reporting Limit

Cadmium (Cd) content

With reference to IEC 62321 edition 1.0:2008 in clause 8/9/10, by microwave digestion until the tested samples are totally dissolved and determined by ICP-OES.

2 ppm

Lead (Pb) content

With reference to IEC 62321 edition 1.0:2008 in clause 8/9/10, by microwave digestion until the tested samples are totally dissolved and determined by ICP-OES.

2 ppm

Mercury (Hg) content

With reference to IEC 62321 edition 1.0:2008 in clause 7, by microwave digestion until the tested samples are totally dissolved and determined by ICP-OES.

2 ppm

Chromium VI (Cr6+) content

With reference to IEC 62321 edition 1.0:2008 in annex C, by alkaline digestion and determined by UV-Vis spectrophotometer.

1 ppm

Polybrominated Biphenyls (PBBs)

With reference to IEC 62321 edition 1.0:2008 in annex A, by solvent extraction and determined by GC-MS and further HPLC-DAD confirmation when necessary.

5 ppm

Polybrominated Diphenyl Ethers (PBDEs)

With reference to IEC 62321 edition 1.0:2008 in annex A, by solvent extraction and determined by GC-MS and further HPLC-DAD confirmation when necessary.

5 ppm

Halogen Content With reference to EN 14582:2007 by calorimetric bomb with oxygen and determined by Ion Chromatograph.

50 ppm

Phthalates With reference to EN 14372: 2004, by solvent extraction and determined by GC-MS.

10 ppm

Hexabromocyclododecane(HBCDD)

With reference to USEPA 3540C, by solvent extraction and determined by GC-MSD.

10 ppm

Remark: Reporting limit = Quantitation limit of analyte in sample

Page 56: ICP Test Report Certification Packet/media/electronics... · LTTTELFUSE PHtLS., tNC. Lima Tech Center, SEZ, Lipa, Malvar, Batangas The following sample(s) was/veere submitted and

Number : TWNC00253636

Test Conducted

Page 5 of 9 Intertek Testing Services Taiwan Ltd.

8F., No. 423, Ruiguang Rd., Neihu District, Taipei 114, Taiwan, R.O.C. 全國公證檢驗股份有限公司 114台北市內湖區瑞光路 423號 8樓

Tel: (+886-2) 6602-2888.2797-8885 Fax: (+886-2) 6602-2400.6602-2401

(Ⅳ) Measurement Flowchart: Test for Cd/Pb/Hg/Chromium (VI)/PBBS/PBDES Contents Reference Standard: IEC 62321 edition 1.0:2008

Remarks: *1: List of Appropriate Acid:

Material Acid Added for Digestion Polymers HNO3,HCl,HF,H2O2,H3BO3 Metals HNO3,HCl,HF Electronics HNO3,HCl,H2O2,HBF4

*2: If the result of spot test is positive, Chromium VI would be determined as detected.

Sample preparation

For different material, digest the sample with appropriate acid*1

Make up with deionized water

Cd/Pb/Hg

Analyzed by ICP-OES

Weigh sample and add alkaline solution

Definite temp. extraction

Make up with deionized water and add diphenyl-carbazide solution

Cool and filter the extract

Cr6+

Weigh sample and add organic solvent

By Soxhlet extraction or Solvent extraction

Concentrate the extract and make upwith organic solvent

PBBs/PBDEs

Analyzed by UV-VIS

Analyzed by GC-MSD

By spot test

Get 50cm2 sample

By boiling water extraction

Metal Polymers / electronics

Negative *2

Confirm the tested samples are totally dissolved

Take sample and immerse into Aqua Regia, start to strip plating layer

Stop the stripping procedure upon color change completely

Take the Aqua solution as plating component and stripped body as substrate component

For non-metal part For metal part

Page 57: ICP Test Report Certification Packet/media/electronics... · LTTTELFUSE PHtLS., tNC. Lima Tech Center, SEZ, Lipa, Malvar, Batangas The following sample(s) was/veere submitted and

Number : TWNC00253636

Test Conducted

Page 6 of 9 Intertek Testing Services Taiwan Ltd.

8F., No. 423, Ruiguang Rd., Neihu District, Taipei 114, Taiwan, R.O.C. 全國公證檢驗股份有限公司 114台北市內湖區瑞光路 423號 8樓

Tel: (+886-2) 6602-2888.2797-8885 Fax: (+886-2) 6602-2400.6602-2401

(Ⅳ) Measurement Flowchart:

Test for Halogen Content Reference Standard:EN 14582

Add absorbent in a combustion flask & place weighed sample in equipment

Fill oxygen into calorimetric bomb

Ignite then leave the bomb at room temperature

Transfer the absorbent into a volumetric flask

Make up with deionized water

Sampling/grinding or cutting

Analyzed by ion chromatography

Page 58: ICP Test Report Certification Packet/media/electronics... · LTTTELFUSE PHtLS., tNC. Lima Tech Center, SEZ, Lipa, Malvar, Batangas The following sample(s) was/veere submitted and

Number : TWNC00253636

Test Conducted

Page 7 of 9 Intertek Testing Services Taiwan Ltd.

8F., No. 423, Ruiguang Rd., Neihu District, Taipei 114, Taiwan, R.O.C. 全國公證檢驗股份有限公司 114台北市內湖區瑞光路 423號 8樓

Tel: (+886-2) 6602-2888.2797-8885 Fax: (+886-2) 6602-2400.6602-2401

(Ⅳ) Measurement Flowchart:

Test For Phthalates Contents Reference Method: EN 14372: 2004

Sampling/grinding or cutting

Weigh sample and add organic solvent

By solvent extraction

Concentrate the extract and make up with organic solvent

Analyzed by GC-MSD

Page 59: ICP Test Report Certification Packet/media/electronics... · LTTTELFUSE PHtLS., tNC. Lima Tech Center, SEZ, Lipa, Malvar, Batangas The following sample(s) was/veere submitted and

Number : TWNC00253636

Test Conducted

Page 8 of 9 Intertek Testing Services Taiwan Ltd.

8F., No. 423, Ruiguang Rd., Neihu District, Taipei 114, Taiwan, R.O.C. 全國公證檢驗股份有限公司 114台北市內湖區瑞光路 423號 8樓

Tel: (+886-2) 6602-2888.2797-8885 Fax: (+886-2) 6602-2400.6602-2401

(Ⅳ) Measurement Flowchart: Test For Hexabromocyclododecane (HBCDD) Reference Standard:USEPA 3540C

End of Report

Sampling/grinding or cutting

Weigh sample and add organic solvent

By soxhlet extraction

Concentrate the extract and make up with organic solvent

Analyzed by GC-MSD

Page 60: ICP Test Report Certification Packet/media/electronics... · LTTTELFUSE PHtLS., tNC. Lima Tech Center, SEZ, Lipa, Malvar, Batangas The following sample(s) was/veere submitted and

Number : TWNC00253636

Test Conducted

Page 9 of 9 Intertek Testing Services Taiwan Ltd.

8F., No. 423, Ruiguang Rd., Neihu District, Taipei 114, Taiwan, R.O.C. 全國公證檢驗股份有限公司 114台北市內湖區瑞光路 423號 8樓

Tel: (+886-2) 6602-2888.2797-8885 Fax: (+886-2) 6602-2400.6602-2401

Photo