icdd workshop 1 and 3 sample preparation group d
TRANSCRIPT
ICDD Workshop 1 and 3Sample Preparation
Group D
Aluminum peaks
??
Specimen holder cavity surface diffracting.
10 20 30 40 50 60
Counts
0
50000
100000
150000 Bauxite JM long time
Peak List
00-029-0041; Al ( O H )3
00-021-1307; Al O ( O H )
00-024-0072; Fe2 O3
00-003-0251; Fe +3 O ( O H )
00-005-0586; Ca C O3
00-004-0551; Ti O2
00-001-0562; Ti O2
Position [°2Theta]
10 20 30 40 50 60
Counts
0
50000
100000
150000
Bauxite JM long time
Ref. Code Compound Name Chemical Formula
00-029-0041 Gibbsite Al ( O H )3
00-021-1307 Bohmite, syn Al O ( O H )
00-024-0072 Hematite Fe2 O3
00-003-0251 Goethite Fe +3 O ( O H )
00-005-0586 Calcite, syn Ca C O3
00-004-0551 Rutile Ti O2
00-001-0562 Anatase Ti O2
10 20 30 40 50 60
Counts
0
5000
10000 Vaseline ZBH
Peak List
00-004-0364; C H3 ( C H2 )16 C O O H
Ref. Code Compound Name
Chemical Formula
00-004-0364
Stearic acid C H3 ( C H2 )16 C O O H
Position [°2Theta]10 20 30 40 50 60
Counts
0
5000
10000 Vaseline ZBH
10 20 30 40 50 60
Counts
0
5000
10000
D1127S1a
Peak List
00-006-0142; C12 H22 O11
Position [°2Theta]10 20 30 40 50 60
Counts
0
5000
10000
D1127S1a
Ref. Code Compound Name Chemical Formula
00-006-0142 Sucrose C12 H22 O11
10 20 30 40 50 60
Counts
0
10000
20000
Do112B2a test1
Peak List
00-024-1977; C12 H22 O11
Position [°2Theta]10 20 30 40 50 60
Counts
0
10000
20000
Do112B2a test1
Ref. Code Compound Name Chemical Formula
00-024-1977 Sucrose C12 H22 O11
10 20 30 40 50 60
Counts
0
2000
4000
6000 D0603P2c
Peak List
00-005-0586; Ca C O3
00-033-0310; Ca S O4 ·0.5 H2 O
00-003-0083; 2 Ca S O4 · H2 O
Position [°2Theta]
10 20 30 40 50 60
Counts
0
2000
4000
6000 D0603P2c
Ref. Code Compound Name Chemical Formula
00-005-0586 Calcite, syn Ca C O3
00-033-0310 Bassanite, syn Ca S O4 ·0.5 H2 O
00-003-0083 Calcium Sulfate Hydrate 2 Ca S O4 · H2 O
10 20 30 40 50 60
Counts
0
500
1000
D0603P5
Peak List
00-002-0667; plaster of paris; 2 Ca S O4 · H2 O
00-002-0629; Ca C O3
Position [°2Theta]10 20 30 40 50 60
Counts
0
500
1000
D0603P5
Ref. Code Compound Name Chemical Formula
00-002-0667 plaster of paris 2 Ca S O4 · H2 O
00-002-0629 Calcite Ca C O3
10 20 30 40 50 60
Counts
0
2000
4000
6000
8000 D0603P3b
Peak List
00-005-0586; Ca C O3
00-041-0224; Ca S O4 ·0.5 H2 O
00-041-0225; Ca S O4 ·0.62 H2 O
Position [°2Theta]
10 20 30 40 50 60
Counts
0
2000
4000
6000
8000
D0603P3b
Ref. Code Compound Name Chemical Formula
00-005-0586 Calcite, syn Ca C O3
00-041-0224 Bassanite, syn Ca S O4 ·0.5 H2 O
00-041-0225 Calcium Sulfate Hydrate Ca S O4 ·0.62 H2 O
10 20 30 40 50 60
Counts
0
10000
20000
D0112B2c
Peak List
00-024-1977; C12 H22 O11
Position [°2Theta]
10 20 30 40 50 60
Counts
0
10000
20000
D0112B2c
Ref. Code Compound Name Chemical Formula
00-024-1977 Sucrose C12 H22 O11
10 20 30 40 50 60
Counts
0
20000
40000
60000
D1127S2a
Peak List
00-024-1977; C12 H22 O11
Position [°2Theta]10 20 30 40 50 60
Counts
0
20000
40000
60000
D1127S2a
Ref. Code Compound Name Chemical Formula
00-024-1977 Sucrose C12 H22 O11
10 20 30 40 50 60
Counts
0
20000
40000
60000
80000 D0518G1b
Peak List
00-033-0311; Ca S O4 ·2 H2 O
Position [°2Theta]
10 20 30 40 50 60
Counts
0
20000
40000
60000
80000 D0518G1b
Ref. Code Compound Name Chemical Formula
00-033-0311 Gypsum, syn Ca S O4 ·2 H2 O
10 20 30 40 50 60
Counts
0
2000
4000
6000
8000
D0518PS1a
Peak List
00-024-0027; Ca C O3
00-033-0310; Ca S O4 ·0.5 H2 O
00-021-0167; Ca S O4 ·x H2 O
00-036-0426; Ca Mg ( C O3 )2
Position [°2Theta]10 20 30 40 50 60
Counts
0
2000
4000
6000
8000
D0518PS1a
Ref. Code Compound Name Chemical Formula
00-024-0027 Calcite Ca C O3
00-033-0310 Bassanite, syn Ca S O4 ·0.5 H2 O
00-021-0167 Calcium Sulfate Hydrate Ca S O4 ·x H2 O
00-036-0426 Dolomite Ca Mg ( C O3 )2
10 15 20 25 30 35 40 45 50 55 602Theta (°)
0
10000
40000
90000
Inte
nsity
(co
unts
)
Blue 2c
Red 1b
Ni Abs edge
Wow!!IntenseNaCl (200)
(111)
From group AExample of artifacts in data
Don’t forget that you can use Halite (NaCl) as a template to determine your beam “footprint” on your specimen holders.