heino markku june 18 enf web
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Application driven materials R&D - from deep science to real business
Dr. Markku Heino, Spinverse Ltd.
Programme Coordinator
Tekes Functional Materials Programme
Advanced materials and manufacturing
boosting solar energy and batteries
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Menu
Functional Materials Programme in short
New Technologies on
Solar energy
Advanced manufacturing
Energy storage
Spinverse
Key player in Nanotech
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Tekes Functional Materials Programme Overview
Programme includesOver 100 companies andall relevant Finnish researchorganizations
International collaboration with40 countries in the top Germany,Japan, Sweden, UK and USA
Duration: 2007-2013
Programme volume:ca. 150M EUR, of which Tekesaccounts for 70 M EUR
Project portfolio as of 01.01.201331 (56) research projects26 (80) company projects
We are developing new applications and competiveadvantage through materials technologyfor the Finnish industry
Renewing Finnish industry & creating new competences
More information:www.tekes.fi/en/materials
Materials Processing
Applications
http://www.tekes.fi/eng/materialshttp://www.tekes.fi/eng/materials -
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International
cooperation
Commercialization
Environmental andlife cycle issues
Value Chains
Four corner stones
in Functional Materials Programme
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Functional Materials - Four Focus areasBased on strategy work done 2009-2010
Biomaterials for medical use
- Close to market
Material and processing solutionsleading to cost-effective mass-manufacturable intelligent structures
Responsive materials
Externally controllable materials enabling
new applicationsNovel materials for energy technologies
Materials for solar energy, batteries andsupercapacitors
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New business areas
Application driven multi-disciplinary research onmaterials and manufacturing
Research projects
Univers i ty dr iven co nsor t ia
Corporate projectsCompany d r iven - app l icat ion related
Health
& BioICT Forest &
Chemical
Metals &
EngineeringConsumerProducts
Energy &
Construction
RAM ALEBOND
NoMaLi
Nanocom
K3MatNanorata Happirahti
UVEMA2
BioFace FUNKIS
FATE-DEFEXCALD
KIVI NNNN
NN NN NN NNNN NN NN NN NNNN NN NN NN NNNN
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Creating new competences, value networksand base for business
Solar energySolar thermal collectors and systems
High-performance photovoltaics
Energy storage
Novel batteries, materials & manufacturing
Building cluster (research/business)
Printed electronics/Adv. manufacturing
Focus on piloting and new applications
Energy efficient manufacturing
Bringing Finnish R&D & high-techtowards global business
Bio-based materialsConcrete building blocks for bioeconomy
Nanocellulose industrialization & applications
Green from inside
Life-cycle thinking
Energy and material efficiency
Biomedical
Tissue regeneration, implants, drug release
Transfer from research to clinical appl.
Functional materials & coatings
Enabling novel applications & approaches
Controlled/tailorable properties
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Solar energyemerging technologiesExamples of company projects
Target-oriented / need-based R&D
Materials & manufacturing & application know-how
Coating technologies in key role
Own technology basis, solutions, IPR
Fast commercialization to industrial applications
Aiming for global value chains
Enabling energy-efficient manufacturing,
integration to building environment+ new solutions for a variety of applications
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Full-aluminium direct-flow solar-thermal absorbersCase Savosolar
SOLARCO R&D project Selective three-layer absorption coatings (MEMO)
Industrial coating process
New collector design
Aluminium based collector developed & commercialized
High optical performance
Excellent heat resistance
Product launched in Munich at theIntersolar Fair in June 2011Best Technology Award
Contact: Jari Varjotie, Savosolar
Contact: Kaj Pischow
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Nano coating technology
Functional Materials Summer Festival, 29.-30.5.
Al or Cu substrate
TiAlSiN
TiAlON
SiO2
PECVD
PVD
The Savosolar patented absorber coating MEMO, is a three layer nano-coating deposited by PVD
and PE-CVD processes. MEMO coatings can be exposed in air to several hundred degree without
any degradation of the optical and mechanical properties surpassing the limitations of the
competing products.
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Competitive Advantage
Savosolar Confidential
Cu or Al substrate
100
PVD: TiAl Si Nx
PVD: TiAlSiOxNy
PECVD: SiO2
45
60
Patented optical vacuum nano coating Top class optical properties
high efficiency
Extremely good angle modifier - over 90% absorbtance still with120 degree angle
Stability in high temperatureslonger life time
Possibility to use in CSP solutions up to 700 Co
Only company in the world able to coat completeabsorbers up to size of 18m2 (3m x 6m)
Enables the use of direct flow absorber design with highlyefficient selective optical coating
Coating capacity 1 million sqm/a
Patented coating process
Direct flow design in theabsorber -
Minimizes heat losses
Maximizes energy yield
Long life time specialaluminium alloy
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Savosolar Collectors in Office Buiding
Solar thermal with district heating15 Savosolar direct flow collectors
Simulated energy production 20 000 kWh/a
Collector annual energy yield 667 kWh/m2, efficiency 56%
Savosolar Confidential
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Ruukki Roof Integrated Collector
Savosolar Confidential
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Architecturally integrated solar-thermal collectorsCase: Aurubis Finland Oy
Nordic Solar system
Solar thermal collectors fully integrated intoprepatinated copper faade architecturedesigned as fixed parts of the faade and roof
First commercial application: Pori swimming hall
R&D Project: Diffusion & adhesion coatings
Piloting the concept
The pilot has provided 280-450 kWh/m2
per year, depending on the prepatinated
copper.Temperature provided by the collectors is
well suitable e.g. for preheating of
domestic hot water.
Contact: Petri Konttinen
http://www.aurubis.com/en/public-relations/press-releases-news/aurubis-finland-oy-innovation-provides-new-freedom-for-design/
Photo: Esa Kyyr
http://www.aurubis.com/en/public-relations/press-releases-news/aurubis-finland-oy-innovation-provides-new-freedom-for-design/http://www.aurubis.com/en/public-relations/press-releases-news/aurubis-finland-oy-innovation-provides-new-freedom-for-design/http://www.aurubis.com/en/public-relations/press-releases-news/aurubis-finland-oy-innovation-provides-new-freedom-for-design/http://www.aurubis.com/en/public-relations/press-releases-news/aurubis-finland-oy-innovation-provides-new-freedom-for-design/http://www.aurubis.com/en/public-relations/press-releases-news/aurubis-finland-oy-innovation-provides-new-freedom-for-design/http://www.aurubis.com/en/public-relations/press-releases-news/aurubis-finland-oy-innovation-provides-new-freedom-for-design/http://www.aurubis.com/en/public-relations/press-releases-news/aurubis-finland-oy-innovation-provides-new-freedom-for-design/http://www.aurubis.com/en/public-relations/press-releases-news/aurubis-finland-oy-innovation-provides-new-freedom-for-design/http://www.aurubis.com/en/public-relations/press-releases-news/aurubis-finland-oy-innovation-provides-new-freedom-for-design/http://www.aurubis.com/en/public-relations/press-releases-news/aurubis-finland-oy-innovation-provides-new-freedom-for-design/http://www.aurubis.com/en/public-relations/press-releases-news/aurubis-finland-oy-innovation-provides-new-freedom-for-design/http://www.aurubis.com/en/public-relations/press-releases-news/aurubis-finland-oy-innovation-provides-new-freedom-for-design/http://www.aurubis.com/en/public-relations/press-releases-news/aurubis-finland-oy-innovation-provides-new-freedom-for-design/http://www.aurubis.com/en/public-relations/press-releases-news/aurubis-finland-oy-innovation-provides-new-freedom-for-design/http://www.aurubis.com/en/public-relations/press-releases-news/aurubis-finland-oy-innovation-provides-new-freedom-for-design/http://www.aurubis.com/en/public-relations/press-releases-news/aurubis-finland-oy-innovation-provides-new-freedom-for-design/http://www.aurubis.com/en/public-relations/press-releases-news/aurubis-finland-oy-innovation-provides-new-freedom-for-design/http://www.aurubis.com/en/public-relations/press-releases-news/aurubis-finland-oy-innovation-provides-new-freedom-for-design/http://www.aurubis.com/en/public-relations/press-releases-news/aurubis-finland-oy-innovation-provides-new-freedom-for-design/http://www.aurubis.com/en/public-relations/press-releases-news/aurubis-finland-oy-innovation-provides-new-freedom-for-design/http://www.aurubis.com/en/public-relations/press-releases-news/aurubis-finland-oy-innovation-provides-new-freedom-for-design/http://www.aurubis.com/en/public-relations/press-releases-news/aurubis-finland-oy-innovation-provides-new-freedom-for-design/http://www.aurubis.com/en/public-relations/press-releases-news/aurubis-finland-oy-innovation-provides-new-freedom-for-design/http://www.aurubis.com/en/public-relations/press-releases-news/aurubis-finland-oy-innovation-provides-new-freedom-for-design/ -
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Final result
11.2.2013 Petri Konttinen 16
Nordic Solar thermal collectors are invisible from the outside, i.e. this part of thefaade looks the same as the rest of 1000 m2 of Aurubis Nordic Green Living faade.
Photo Esa Kyyr
Impact: Nordic Solar can be fully architecturally integrated into different copperfacades and roofs. It alloys a variety in forms, sizes and patinas, and gives architectand constructor much wider opportunities than conventional solar thermal collectors.
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Roll-to-roll ALD Coating TechnologyCompany project 1: Beneq
First industrial R2R ALD equipment WCS 500 developed/commercialized Customer: Astral lab/ Lappeenranta University of Technology (Prof. Cameron)
Available for: Application development, industrial scale trials, piloting, R&D
.........................................................................................................................
EU dimension: Now Beneq in 2 EU projects utilizing this technology & know how:
R2R CIGS http://r2r-cigs.com/
Aim: to develop cost-effective processes and technologies
for high volume production of flexible solar modules
Zn(O:S) buffer layer for CIGS & next generation R2R ALD equipment for this application
PLIANT (Process Line Implementation for Applied Surface Nanotechnologies)
Aim: spatial device for flat surfaces, atmospheric (non-vacuum)
Contact: Sampo Ahonen, Beneq ALD = Atomic Layer Deposition
http://r2r-cigs.com/http://r2r-cigs.com/http://r2r-cigs.com/http://r2r-cigs.com/ -
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Driving forces for the R2R ALD technologyCase Beneq
15.8.2013
Market is driven to flexible products
Life time demand needs high moisture barriers,ALD thin film is the best known barrier
Barrier production cost has to be under 2$/m2
ALD CIGS buffer layer increases efficiencyover 2% units
Flexible lightning, PV and display productsare at market already
source Sony
Source Fraunhofer ISE
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A paradigm shift
1915.8.2013 Beneq 2012
Single wafer ALD
Semiconductor
Productivity: > 1 to 10s m2/hour
CoO: 10 to 1s $/m2
Roll-to-roll ALD
Packaging, photovoltaics,lighting, flexible electronics
Productivity: >10s m2/hourCoO: 1 to 0.1s $/m2
Large-area (batch) ALD
Solar, optical, lighting, medical
6
1.2 x 1.2 m
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Thin-film inorganic moisturebarrier on polymer substrate
2015.8.2013 Beneq 2012
Requirement for water vapor transmission rate(WVTR) of 10-6g/(m2day)
source:Holst centersource SonySource Fraunhofer ISE
Flexible photovoltaics Flexible display Flexible OLED lighting
equals over over one month!
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Coating Technology for TCO GlassCompany project 2: Beneq
TCO (transparent conductive oxide) coatings for photovoltaics
Thin layer of Fluorine-doped tin oxide on glass to collect currentfrom PV cells high transparency & conductance needed
Continuos deposition method for TCO and low-e coatings on flat
glass developed based on Beneqsproprietary aerosol techniquenAERO
Co-operation with Glaston(glass handling technology)
Industrial manufacturing line
built and commercialized
October 2012
Heating
21Beneq 2012 -CONFIDENTIAL
Loading
Annealing*
Cooling
nAERO TCO coating sheet resistance 8...15 /square transmission > 83% haze < 0.5% or up to 20%
In collaboration with:
* Heat strengthening available as option
Contact: Sampo Ahonen, Beneq
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Added valuefor glass manufacturers and processors
Turnkey solution for production of TCO TCO glass for a-Si, a-Si/c-Si and CdTe cell manufacturers
Economical and efficient production
Cost savingsand optimized performance for PV manufacturers
Pyrolytic FTO hard coating with proven performance
Low cost with optimized properties
Next generation of TCO combined with new features
October 2012 Beneq 2012 - CONFIDENTIAL 22
nAEROenabling TCO production
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SiON barrier layer
Reduces reflection and suppressesinterference in reflected light
Serves as Na diffusion-blocking interlayer
TCO coating
SnO2:F (FTO)
Optimized properties
Adjustable film properties
Transmittance > 83 %
Sheet resistance 8 15 /
Haze < 0.5% or 10 20%
October 2012 Beneq 2012 - CONFIDENTIAL 23
TCO film properties
Barrier layer
SiH4, NH3, N2O
N2
TCO layer
MBTC, TFA, MeOH
N2, O2, H2O
TCO film
Front glass
Semiconductor
Back electrode
Barrier layer
Incoming light
1Total transmission including low iron glass substrate, haze compensated2Keithley 2400 General Purpose SourceMeter with Alessi CPS-05 contact probe station
Measuredproperties
Haze
Averagetransmittance400-1000 nm1
Sheetresistance
Coatingthickness
Product 1 10 % 82.2 % 8.7 (/)2 970 nm
Product 2 < 1 % 84.4 % 13 (/)2 550 nm
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nAERO coating technology benefits
nAERO vs. CVD+ nAERO is pyrolytic hard coating comparable to APCVD
+ Robust equipment, technology and process
+ High coating growth rate
(up to 200 nm/s at 600 C, APCVD < 100 nm/s)
+ High material yield (up to 30%, APCVD 10-15%)+ Lowest Cost-of-Ownership
nAERO vs. PVD
+ nAERO TCO is stable at high temperatures+ nAERO enables haze control
+ Attractive Cost-of-Ownership
+ Possible to combine with heat strengthening
Touch the Future
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Canatu 2013, Confidential and proprietary 26
Touch the Future
CompanyAalto University spin-off with 20 employees, 150
patents on new materials, manufacturing, devices, designs and pilotmanufacturing in Finland
ProductsUnique NanoBudfilms and components with excellent
optoelectronic performance for flexible and formable electronics such as
PV, Lig htin g, Disp lays andLog ic
ProcessUnique, low cost, environmentally friendly, high yield, Roll-2-Roll
Direct Dry Printingmanufacturing
StatusBuilding manufacturing and supply chain to enable the large scaleproduction targeting first volume sales in Q4 2013
FutureWorlds foremost supplier of energy and electronics products
anywhere on anything
Canatu
Contact: David Brown
Examples of Research Projects: Dos Janne Halme Aalto University
http://e/Users/David_P_Brown/Desktop/Qii%20Promo%20Video.movhttp://localhost/var/www/apps/conversion/tmp/scratch_8/CanaTouchCompilation6b(short).wmvhttp://localhost/var/www/apps/conversion/tmp/scratch_8/CanaTouchCompilation6b(short).wmvhttp://e/Users/David_P_Brown/Desktop/Qii%20Promo%20Video.mov -
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Robust dye-sensitized solar cells printed on metal
-
e-
--
-
+
Dye
1.5 nm
TiO210 30 nm
3I-I3-
e-
e-
Pt
TCO
TCO 0.5 1 m
Glass 2
3 mm
Glass
Electrolyte
5 20 m
5 20 m
G24i
Fraunhofer ISE
KIST
Dyesol
Examples of Research Projects: Dos. Janne Halme, Aalto University
Examples of Research Projects
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High-Efficiency Solar Cells (Solar III-V)
Development of dilute nitride
semiconductor materials for
multi-junction solar cell systems
Concentrated photovoltaics (CPV)utilizing whole solar spectrum &minimizing size to createhigh efficiency (45-50%)
More information - Project Coordinator:
Prof. Mircea Guina, Tampere University of Technology
Examples of Research Projects
Examples of research projects
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Battery Materials
NOVEL ELECTRODE FABRICATION METHODS FOR LITHIUM ION BATTERY
Leader: Prof. Maarit Karppinen, Aalto University New environmentally-friendly, safe, cheap chemicals & methods for manufacturing
Optimization of LTO material for Li-ion battery application
Development of water-based printing methods for environmentally-friendly and economicmanufacturing of LTO-LFP (Li4Ti5O12-LiFePO4) batteries
TUBULAR NANOCARBONS FOR LITIUM ION BATTERY (LIB) ELECTRODESLeader: Prof Esko I. Kauppinen, Aalto University
Nanocarbons: CNT, CNB & CNFs to increase the electron conductivity at electrodes
Good results; further evaluation by partner (TOYOTA Central R&D Labs.; confidental)
Li ion partnering
with Carbon
nanobud...
Examples of research projects
Example of battery materials research
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CHOICES FOR ELECTRODE MATERIALS
Li1-xFePO4CATHODE(pos. electrode)
Olivine structure (not layered)
Safe, cheap, environmentally benign
excellent for large-scale applications
Stable, constant voltage (3.4 V),
excellent cyclability, fast to charge
Problems: low electrical conductivity,
water-related stability issues
LiFePO4 LiCoO2 Li4Ti5O12
Li4+yTi5O12ANODE(neg. electrode)
Spinel structure Li[Li1/6
Ti5/6
]2
O4
No protective SEI (solid-electrolyte interface)layer
formed/neededsafe
Stable, constant voltage (1.55 V), no volume
change, fast to charge
Problems: low electrical conductivity,
water-related stability issues
traditional
cathode
Example of battery materials research
NMP
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WATER-BASED BINDERS
in electrode manufacturing
[Presently: PVDF (polyvinyldifluoride) binder + NMP!!!(N-methylpyrrolidone) solvent]
Cheap
Non-toxic solvent
Environmentally friendly
Compatible with printing machine
Walkisprinting machine
NMP
Sachtleben: - electrode materialsSunChemical: - binder chemicalsWalki: - printing technologyEuropeanBatteries: - battery testing
Li ion battery research value chain
http://upload.wikimedia.org/wikipedia/commons/f/f1/N-Methylpyrrolidone_Structural_Formulae.png -
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A! Aalto UniversityDepartment of Chemistry
First litium mine in Europe
[LiAl(SiO3)2spodumen]
Li-ion battery manufacturing
Li-ion battery material research
End-user of batteries
TiO2& Li4Ti5O12
Battery chemicals
Battery recycling
Coating of electrodes
Inorganic Chemistry + Physical Chemistry
University
Consortium
Chydenius
Battery testing
Li ion battery research value chain
http://www.akkuser.fi/index_main.htmhttp://www.cargotec.fi/cms/cargocms20.nsf/Documents/9168BB8641A157FFC2256FDB003E3CC7?OpenDocument&lang=2http://www.sunchemical.com/http://www.europeanbatteries.com/ -
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Energy Storage - Large Format Li Ion BatteriesCase: European Batteries
Developed and commercialized novel
large format Li ion batteries
- Materials, cell technology, manufacturing
- High energy density per weight, safety & reliability- For energy, industrial & vehicle applications
LiFePO4(LFP) technology
- performance, safety, reliability
Contact: Mika Rsnen, European Batteries
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European BatteriesAdvanced Lithium Ion Batteries forIndustrial and Marine Application
Launch of the the second Full Hybrid Ferry byCMAL in UK May 23rd 2013: advantage: 25% -50% saving in energy consumption (customersannouncement)
Automated forlkifts in an automated warehousein US: advantage 22/7 365 days operation formany years without maintenance breaks(2 x 1 hour chargeing time per day).
High energy density 4X energy per weight compared to lead-acid
Lighter and smaller systems, completely new applications
Long cycle and calendar life
15X than lead-acid
5X than NiMH or 2X most Li-ion chemistries
Safe and stable
Free of the safety problems of the most Li-ion chemistries
Optimal for demanding applications
Environmentally friendly and recyclable battery technology
Vertical integration from cell manufacturing to System Integration
Main Characteristics
Customer Cases
FROM CELL TO MODULE AND FULL SYSTEM:
2,50
2,75
3,00
3,25
3,50
0% 20% 40% 60% 80% 100% 120%
Discharge Capacity, %
0.2C
0.5C
1.0C
2.0C
3.0C
4.0C
Voltage, V
Competitice Advantages Achieved
Contact: Mika Rsnen
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Lithium-Ion Battery manufacturing value chain
Lithium-carbonatemanufacturing
Industrial grade Li2CO3
Battery grade Li2CO3
Lithium-saltsManufacturing (e.q.LiF, LIPF6, LiBF4,LiBOB)
Battery grade cathode materialmanufacturing
Industrial grade salts
C-precursorsFePO4 or other active material base
ElectrolytesManufacturing
Organic carbonates and estersas electrolyte solvents
Lithium-ioncellmanufacturing
Separators,Anode-materials,binders, binder solvents,and additivesAl- and Cu-foils,cover-materials and tabs,Auxiliary process materials
Lithium-ionpackmanufacturing
BMSTMSIOFramesPackingCablingChargersSystem integration
MINING ANDCONCENTRATIONCOMPANIES
ACTIVE BATTERY MATERIAL MANUFACTURERS(AND OTHER MATERIAL MANUFACTURERS) CELLMANUFACTURESINTEGRATORS
OTHER BATTERYMATERIAL MANUFC
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Efficient Recycling of BatteriesCase: AkkuSer Oy
AkkuSer - collecting and recycling rechargeable
batteries and accumulators from the EU since 2006.
Their Dry Process separates valuable metals from rechargeable batteries -identified by element, crushed, sorted and supplied to industry as a raw material.-> refined using chemical and other methods.
The process makes it possible to reuse more than 90 percent of batteries
www.akkuser.fi/video
Development of energy-efficient chemical processing for used alkalinebatteries
High recovery rate (will raise > 80 percent)
Cost efficient and safe method compared to smelting
In pilot phase
New company started: Recalkaline Oy, www.recalkaline.fi
Contact: Jarmo Pudas, AkkuSer (& Recalkaline)
http://www.akkuser.fi/videohttp://www.recalkaline.fi/http://www.recalkaline.fi/http://www.akkuser.fi/video -
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Functional Materials ProgrammeMaking future visions reality
Kari Lehkonen, klplgraphics (http://www.kpl.fi)
See also video: http://www.youtube.com/watch?v=wfNvjySHqYk
http://www.kpl.fi/http://www.youtube.com/watch?v=wfNvjySHqYkhttp://www.youtube.com/watch?v=wfNvjySHqYkhttp://www.kpl.fi/ -
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Conclusions
Critical new technologies and solutions developed- Ready for use!
Combining
Application needs
Materials and nanotechnology
Energy efficient manufacturing
From research to business
Value networks recognized - Research & business
Active international cooperation &Building Finnish competence
Good results - Fast commercialization
Concrete building blocks for Sustainable Economy- already today!
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Contact information
Programme manager: Markku Lms, [email protected]
Programme coordination: Markku Heino, Spinverse [email protected]
Further information: www.tekes.fi/eng/materials
Visit our Nanotech Finland booth!
http://www.tekes.fi/eng/materialshttp://www.tekes.fi/eng/materials -
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Key player in NanotechGrowth Technology New markets
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We are building the future
- together with extensive expert networks
3 * place for confidentiality clauses
150 Meur,2007-2013
140 Meur,2007-2013
79 Meur,2011-2015
60 Meur,2011-2016
Innovation programs in Nano/Cleantech areacoordinated by Spinverse
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Examples of our expert services
3
Visit Spinverse booth in the Exhibition
R&D project & program building: Spinverse has assisted in building e.g.
ENIAC JU project, Processes for MEMS by Inkjet Enhanced TechnologiesPROMINENT; Okmetic Ltd. + consortium; 9.4 Mgranted,also project coordination managed by Spinverse
Sustainable Bioenergy Solutions for Tomorrow - joint PPP programof FIBIC & CLEEN Oy: participants are small and large forest, energy,technology and consultancy companies (21) and universities /
research institutions (13), budget 16 MDemos/piloting: Spinverse coordinates the full-scale Fuel Cell demoto be built in Vuosaari Harbour, Helsinki in 2013.
Technology commercialisation: Spinverse assisting Prof. Michael Graetzelto define a commercialisation path for new solar cell technology (ERC-POC)
Go-to-new Markets: Spinverse assisting Nanotech company Beneqto enter Russian Market
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