groundwater monitoring well sampling (second …1130 ug/1 (np/sdws of 300 and 50 ug/1,...
TRANSCRIPT
8 9
Rollins
December 18, 1987
Mr. Russ HartProject ManagerCERCLA Enforcement SectionU.S. EPA Region V
| 230 S. Dearborn Street| Chicago, IL 60604
RE: Groundwater Monitoring Well Sampling (Second Round) at theMaster Disposal Service Landfill
Dear Mr. Hart:
j Rollins Environmental Services (FS), Inc. (RES-FS) will perform thesecond round of groundwater sampling as required by the MDSL Work
! Plan. We anticipate performing this activity during the next period of• low groundwater level conditions (refer to the site map, submittedj 11/24/87, for sampling locations).
RES-FS has evaluated the analytical data from the first round ofmonitoring well samples to determine the number of samples and type ofanalyses necessary for the second round of sampling. Table 1 lists thefirst round of monitoring well samples collected in September, 1987. Theorganic and inorganic partial data packages are included as AttachmentsA and B, respectively.
RES-FS' evaluation of the first round analytical data indicated thefollowing, with respect to organic compounds (see Table 2):
Sample 30-01 contained 1,1-dichloroethene at a concentration of 18ug/l (detection limit 5 ug/1).
Sample 32-01 contained chloroethane at a concentration of 43 ug/1(detection limit 10 ug/1) and acetone at a concentration of 39 ug/1(detection limit 10 ug/1).
Sample 33-01 contained chloroethane at a concentration of 13 ug/1(detection limit 10 ug/1); acetone at a concentration of 16 ug/1(detection limit 10 ug/1) and benzene at a concentration of 8 ug/1(detection limit 5 ug/1).
EPA Region 5 Records Ctr.
232493
Mr. Russ HartDecember 18, 1987Page 2
Sample 37-01 contained acetone at a concentration of 30 ug/1(detection limit 10 ug/1).
Sample 41-01 contained acetone at a concentration of 41 ug/1(detection limit 10 ug/1).
Sample 42-01 contained trans 1,2-dichloroethene at a concentrationof 11 ug/1 (detection limit 5 ug/1).
Sample 44-01 contained acetone at a concentration of 43 ug/1(detection limit 10 ug/1).
Sample 46-01 contained acetone at a concentration of 76 ug/1(detection limit 10 ug/1).
Sample 47-01 contained acetone at a concentration of 49 ug/1(detection limit 10 ug/1).
Sample 49-02 contained toluene at a concentration of 360 ug/1(detection limit 250 ug/1). It should be noted that the high (250ug/1) detection limit for this sample is a result of a 50-fold dilutionfactor required for analysis of the sample. Additionally, sample 49-02 was a duplicate sample of sample 49-01, which contained tolueneat a concentration of 15 ug/1, well below the detection limit of 250ug/1 associated with these samples.
One semi-volatile compound was detected in the first round ofmonitoring well samples. The compound; bis(2-ethylhexyl)phthalatewas found in sample 30-01 at a concentration of 26 ug/1, in sample43-01 at a concentration of 36 ug/1 and in sample 49-01 at aconcentration of 48 ug/1. The detection limit for these threesamples was 10 ug/1. No other semi-volatile compounds weredetected in any of the monitoring well samples.
No pesticide/PCB compounds were detected in any of the monitoringwell samples.
The review of the groundwater monitoring well analytical data indicatedthe following, relative to inorganic compounds identified in the samples(see Table 3):
Sample 30-01 contained iron at a concentration of 470 ug/1, inexcess of the National Primary/Secondary Drinking Water Standards(NP/SDWS) of 300 ug/1 and manganese at a concentration of 92 ug/1(NP/SDWS of 50 ug/1).
Sample 33-01 contained iron at a concentration of 12500 ug/1(NP/SDWS of 300 ug/1) and manganese at a concentration of 219ug/1 (NP/SDWS of 50 ug/1).
Mr. Russ HartDecember 18, 1987Page 3
Sample 39-01 contained iron at a concentration of 1980 ug/1(NP/SDWS of 300 ug/1) and manganese at a concentration of 68 ug/1(NP/SDWS of 50 ug/1).
Sample 40-01 contained manganese at a concentration of 1320 ug/1(NP/SDWS of 50 ug/1).
Sample 42-01 contained the following inorganic compounds:
-barium at 1190 ug/1 (NP/SDWS of 1000 ug/1)-iron at 16500 ug/1 (NP/SDWS of 300 ug/1)-manganese at 82 ug/1 (NP/SDWS of 50 ug/1).
Sample 45-01 contained manganese at a concentration of 144 ug/1(NP/SDWS of 50 ug/1).
Sample 48-01 contained manganese at a concentration of 105 ug/1(NP/SDWS of 50 ug/1).
Sample 49-01 contained iron at a concentration of 26200 ug/1(NP/SDWS of 300 ug/1) and manganese at a concentration of 1140ug/1 (NP/SDWS of 50 ug/1).
Sample 49-02 (a duplicate sample of 49-01) contained iron at aconcentration of 11000 ug/1 and manganese at a concentration of1130 ug/1 (NP/SDWS of 300 and 50 ug/1, respectively.)
Sample 50-01 contained iron at a concentration of 12700 ug/1(NP/SDWS of 300 ug/1).
All groundwater monitoring well samples displayed Total Dissolved Solids(TDS) concentrations above the NP/SDWS of 500 mg/1 except thefollowing samples: 31-01, 34-01, 36-02, 43-01 and 46-01. (Refer to Tablethree for specific concentrations.)
RES-FS proposes to modify the sampling plan for the second round ofgroundwater monitoring well samples to exclude the analysis of all semi-volatile and PCB/Pesticide compounds.
The second round of sample collection and analysis therefore will includethe following parameters:
CLP Volatiles (including the target alcohols)CLP InorganicsConventional ParametersField measurements of; pH, Specific Conductance andTemperature.
The proposal to modify the sampling plan is based on the followingrationale:
Mr. Russ HartDecember 18, 1987Page 4
The only semi-volatile compound identified in any of the first roundsamples was a phthalate, which are found in virtually all rubberand plastic products. Therefore, the presence of phthalates at thelow ug/1 (ppb) concentrations found in three of the MDSLgroundwater samples are probably attributed to field and/orlaboratory contamination.
No PCBs or pesticides were found in any of the samples.
If you have any questions, please do not hesitate to call.Sincerely,
ROLLINS ENVIRONMENTAL SERVICES (FS), INC.
Rick SmithAssistant National Technical Director
Jeffrey M. BakerProject Manager
Attachments
JMB:bc
cc: Dennis Kugle, WDNRMike McCauley, Quarles & BradyDr. Kim Anderson, A. O. Smith Corp. - w/o attachmentsAaron Hardt, Rexnord, Inc. - w/o attachmentsTom Rutkowski, Briggs & Stratton Corp. - w/o attachmentsDave Quast, A. O. Smith Corp. - w/o attachmentsErnest McClellan, Plast-O-Meric - w/o attachmentsNancy Peterson, Quarles & Brady - w/o attachments
TABLE 1
Master Disposal Service Landfill
Groundwater Monitoring Well Sample Summary
Sampling Series Number 1
SAMPLENUMBER
WELLNUMBER
AQUIFERSAMPLED
DATESAMPLED
GW-030-01GW-031-01GW-032-01GW-033-01GW-034-01GW-035-01GW-036-01GW-036-02GW-037-01GW-038-01GW-039-01GW-040-01GW-041-01GW-O42-01GW-O43-01GW-044-01GW-045-01GW-046-01GW-047-01GW-048-01GW-049-01GW-049-02GW-050-01
MW-44MW-46MW-45MW-31MW-49MW-05MW-50MW-50MW-51MW-43MW-47MW-53MW-48MW-01MW-56MW-55MW-54MW-42MW-41MW-40MW-10MW-10MW-09
A-lA-3A-2A-lA-2A-lA-2A-2A-3A-3A-2A-lA-3A-lA-3A-2A-lA-3A-2A-lA-lA-lA-2
9/25/879/25/879/25/879/26/879/26/879/26/879/26/879/26/879/26/879/26/879/26/879/26/879/26/879/26/879/27/879/27/879/27/879/27/879/27/879/27/879/27/879/27/879/27/87
Please refer to Site Map for well locations.
1ABLE JMASTfR DISPOSAL SERVICE LANDFILLINORGANIC A N A L Y T I C A L SUMMARYGRUUNDUATER SAMPLING(PAGE 1 OF 2)
SAMPLE IDENTIFICATION NUMBER (1)
PARAMETER 3001
ALUMINUMANTIMONYARSENICBARIUMBERYLLIUMCADMIUMCALCIUM 67400CHROMIUMCOBALTCOPPERIRON 470**LEADMAGNESIUM 37600MANGANESE 92**MERCURYNICKELPOTASSIUM 6420SELENIUMSILVER
SODIUM 35400THALLIUMVANADIUMZINC
DISSOLVED IRONRESIDUE, FILT. (TOS) (mg/l) 550"
3101 3201 3301
678
8.226200 69200 153000
15
12500**
23000 126000219"
138264000 64300
20000 195000 227000
22
141270 1200** 1800**
3401 3501 3601
16
43600 38000 25900
300 116
28900 40500 2140021
13800 12900 16600
380 1200** 1300**
DETECTION3602 3701 3801 3901 4001 4101 LIMIT (2)
266 2006010
215 2005
5.3 529100 35400 62800 90900 103000 276000 5000
13 1050255
125 1980** 1005
23700 31200 37200 37600 500068** 1320** 15
0.244 CO
18500 70800 5000510
16000 29500 19000 33700 18500 51200 50001050
62 20
100280 1400" 670** 580" 680** 650" 10
NOTE: ** DENOTES CONCENTRATION OF PARAMETER EXCEEDS PRIMARY/SECONDARY DRINKING WATER REGULATIONS STANDARDSUNITS ARE EXPRESSED AS ug/l UNLESS OTHERWISE NOTED
(1) ID NUMBER REPRESENTS LAST 5 DIGITS OF THE NOMENCLATURE NOL-GU OXX-XX(2) CONTRACT REQUIRED DETECTION LIMITS
UBLE 3MASTER DISPOSAL SERVICE LANDFILLINORGANIC ANALYTICAL SUMMARYGROUNDUATER SAMPLING(PAGE 2 OF 2)
SAMPLE IDENTIFICATION NUMBER (1)
PARAMETER
ALUMINUMANTIMONYARSENICBARIUMBERYLLIUMCADMIUMCALCIUMCHROMIUMCOBALTCOPPERIRONLEADMAGNESIUMMANUtNESEMERCURYNICKELPOTASSIUMSELENIUMSILVERSODIUMTHALLIUMVANADIUMZINC
DISSOLVED IRONRESIDUE. FILT. (TDS) (*a/l)
4201 4301 4401 4501
203 224
1190** 649
240000 55100 288000 8140013 27
16500**
157000 26700 3060082** 144**
588380 5810 418000
246000 9920 205000
24
1992100" 390 2000** 920**
4601 4701 4801 4901
652 359
•
99000 54900 101000 25700020
54253 26200**
40000 170000105** 1140**
10234200 63300 65600
67400 86100 6150 303000
66 421
370 600** 1600** 2400**
4902
300
9.725100018
11000"
1680001130"
10366500
304000
682
2400"
DETECTION5001 LIMIT (2)
654
7.1133000
12700**
11600028
426220
U2000
40
115UOO"
200601020055
500010502551005
5000150.24050005105000105020
10010
UNITS EXPRESSED AS ug/l UNLESS OTHERWISE NOTED(1) 10 NUMBER REPRESENTS LAST 5 DIGITS OF THE NOMENCLATURE MDL-GU OXX-XX(2) CONTRACT REQUIRED DETECTION LIMITS
TABLE 3HASTER DISPOSAL SERVICE LANDFILLORGANIC ANALYTICAL SUMMARYGROUND WATER MONITORING WELL SAMPLING(PAGE 1 OF 2)
SAMPLE IDENTIFICATION NUMBER (1)
PARAMETER 3001 3101 3201 3301 3401 3501 3601 3602 3701 3801
CHLOROETHANE 43 13
ACETONE 39 16 30
1.1 DICHLOROE THANE 18
BENZENE 8**
BIS(2 ETHYLHEXYDPHTHALATE 26
TABLE 2MASTER DISPOSAL SERVICE LANDFILLORGANIC ANALYTICAL SUMMARYGROUND WATER MONITORING WELL SAMPLING(PAGE 2 OF 2)
PARAMETER 4201 4301 4401 4501 4601 4701 4801 4901 4902 5001
ACETONE 43 76 49
T 1,2-DICHLOROETHENE 11
TOLUENE 360
BIS(2-ETHYLHEXYL)PHTHALATE 36 48
DETECTION3901 4001 4101 LIMIT (2)
10
41 10
5
5
10
DETECTIONLIMIT (2)
10
5
250 (3)
10
NOTE: * DENOTES COMPOUND DETECTED IN THE METHOD BLANK" DENOTES CONCENTRATION OF PARAMETER EXCEEDS PRIMARY/SECONDARY DRINKING WATER REGULATIONS STANDARDS
UNITS EXPRSSED AS ug/l UNLESS OTHERWISE NOTED
(1) ID NUMBER REPRESENTS LAST 5 DIGITS OF THE NOMENCLATURE MDL-GW OXX-XX(.') CONTRACT REQUIRED DETECTION LIMITS(3) DETECTION LIMIT FOR SAMPLE INCREASED TO 250 BECAUSE OF 50-FOLD DILUTION FACTOR (5 FOR UNDILUTED SAMPLES)
ATTACHMENT A
MASTER DISPOSAL SERVICE LANDFILL
PARTIAL ANALYTICAL DATA PACKAGE
ORGANIC COMPOUNDS
LABORATORY NAME: ETC/TOXICON
LAB SAMPLE 10 NO: 4184-181SAMPLE MATRIX: WATEROATA RELEASE AUTHORIZED BY
ORGANICS ANALYSIS DATA SHEET(PAGE 1)
CASE NO: 4184flC REPORT NO: 4184CONTRACT NO: 0\ \DATE SAMPLE RECEIVED
VOLATILE COMPOUNDS
•9/29/87
CONCENTRATION: LOWDATE EXTRACTED/PREPARED:DATE ANALYZED: 18/43/87CONC/OIL FACTOR: 1.PERCENT MOISTURE: (NOT DECANTED)
PH
CAS NUMBER74-87-174-8J-*7S-81-47S-88-J75-89-247-44-175-15-875-35-47S-JS-J154-48-i47-44-3187-84-278-f J-J71-S5-454-23-5188-85-475-27-4
CHLOROMETHANEBROMOMETHANEVINYL CHLORIDECHLOROETHANEHETHYLENE CHLORIDE . . . .ACETONECARBON OlSULFIDC1. l-DICHLOROETHENE . . . .1.1-OZCHLOROETHANC . . . .
TRANS-1.2-OICHLOROETHENE .CHLOROFORM1.2-OICHLOROETHANE . . . .2-BUTANONE1. 1. 1-TRICHLOROETHANE . .CARBON TETRACHLORIOE . . .VINYL ACETATEIROMOOICHLOROMETHANE . . .
UG/L181818181185S
ItS55185S185
UUUuJuuu
uuuf6uuuu
CAS NUMBER78-87-518861-82-471-81-4124-48-179-88-571-43-218841-81-S118-75-87S-25-2188-18-15*1-78-4127-18-479-34-5188-88-3188-98-7188-41-4188-42-5
UG/L1.2-OICHLOROPROPANE . . .TRANS-1.3-OICHLOROPKOENE .TRICHLOROETHENEOIBROMOCHLOROMETHANE . . .1,1,2-TPICHLOROETHANE . .BENZENECIS-1.3-OICHLOROPROPENE .2-CHLOROETHYLVINYLETHER .
BROHOFORH4-HETHYL-2-PENTANONE . . .2-HEXANONCTETRACHLOROETHENE . . . .1.1.2.2-TETRACHLOROETHANETOLUENECHLOROBENZENEETHYLBENZENESTYRENETOTAL XYLENES
18S18
UUUuuuuuuuuuuuuuuu
8 - COMPOUND WAS DETECTED IN THE 8C BLANK.J - REPORTED VALUE IS LESS THAN THE DETECTION LIMIT.U - COMPOUND ANALYZED FOR BUT NOT DETECTED. THE REPORTED
VALUE IS THE MINIMUM ATTAINABLE DETECTION LIMIT FORTHE SAMPLE.
SEE PAGE 1A FOR COMPLETE DEFINITIONS OF THE DATA
REPORTING 8UALIFIERS.FORM I
4 1 8 4 3 0 3 4 9
Laboratory Name: ETCToxicon
Case No: 4184
Sample Number
Organics Analysis Data Sheet
CAS Number
67-63-0
71-36-3
78-92-2
Compound Name
Isopropyl Alcohol
N-Butjl Alcohol
sec-Butyl Alcohol
ConcentrationILf/L
300U
200U
200U
U Tndir«t<-f rftrnpr^r^ w^ ynalyrpj fly frit aft <jfftftfd_ Pi-pnn rtv minimum Aftrt-tinn limit fnrlhe tample with the U(e.g. 10U) baled on necessary coaxmratioa'dihaioo action. (This is not necessarily the instrument detection limit)The footnote should read: U-Compotmd was analyzed for but not detected The number is me minimum attainabledetection limit for the sample.
J TnH>r«tM m <yim«t<^ vabe. This flaj U ued timer wbea »«rimMing a coQcentratioQ for tentatively identified compoundswhere a 1:1 rappmc it asmpfd or »bf" mf "ift» ipe^r»l <<»« inHirjit«l thg presence of« componad ttm meets me ideati-ficatkm criteria bm the ronlt is VM than the edlWdeteaiooliiM If limit of detection is10 (JLgft. and a ooncenraion of 3 u{/L is calculated, report as 3J.
4 1 8 4 30350
3 I - ' ' ' - I ! .
Organics Analysis Data Sheet(Page 2)
Semivolatile Compounds
_oncentration Q.OVV) Medium /Circle One)
Date Extracted 'Prepared
•ate Analyred
Conc/Dil Factor:
'ercent Moisture (Decanted).
GPC Cleanup DY«s DNo
Separaiory Funnel E*iraciion
Continuous Liquid - Liquid Extraction DYes
CASNumber
ug/for ug/Kg(CirctoOfM)
108 95-2UI-44-495-57-8541-73-1106-46-7100-51-695-50-195-48-739638-32-9106-44-5621-64-767-72-198-95-378-59-188-75-5105-67-965-85-0111-91-1120-63-212O-82-191-2O-3106-47-887-68359-50791-57-677-47-488-06-29595-491-58-788 74-4131-11-3208 96-899 09 2
*henol6(S<-2-Crttoroe(nvf (Ether
2-Chlorophenol1. 3-Dichlorobenzene1 . 4-DtchtorobefueneBenzyl Alcohol1. 2-Dichforobcnzen*2-Methytph«noltx*(2 <hloroicopropv<tEth«r
4-M«thylpr»enoiN-Nitnno-Oi-n-Propy1»mir»«Heicachloro«trujntNitrobenzene(sophorone2-NHroohenoi
2. 4-Oim«tnytpn«nO<
Beruoic Acidbisf^-CnloroethoKYlMetftant2. 4-DKhloroph«nol1. 2. 4-Trichkxo6eozeneNapntn«(«ne4-Chlofo»nitin«S«ucMorobui»dt«n«4 • Chloro- 3 • Mcthylphenol2-Metfty<n«phthal«ntHe ucMorocyclopentadierw2. 4. 6-Trichloroprtenol2. 4. 5-Trtchtofophenol2-CMoron»phth«lertc2 NitroaniltrteDimethyl PhihalateAcenaphthylene3-Niiroamline
/Cu.//>&10 ttIn,,.10k/Ok(m-ir\uL(flulUUi\nuIOuIDuWK,I/]U
/(VWin
inu.'(I*IOu.If)*m*10*ffa/<vlUr-/OiA
ftu(CllA
SOU
IDu.IfilA
5m
CASNumber
606-20-284-66-2
86-73-7
86-30-6
3-32-91-28-500-02-732-64-921-14-2
005-77-3
00-01-634-52-1
01-S5-318-74-17-86-55-01-820-12-7
84-74-2206-44-029-00-0
15-687H-94-16-55-3
117^1-7218-01-9117-84-0205-99-2207-08-9J032-8193-39-553-703191-24-2
!. 4-Dinrtropr»«nol
4-NitropNenol
2. 4-D<n(trotolu«n«
!,.6-Oinhrotolu«ne
4 -Chlof oph«riy(-pn«ny««th*r
UNruoanilin*
Oiethylphtrujujte
Fluorcnt
N-Nitrocodipf>enyujmine (1)
Phenanthrtnc
Anthracene
3 atytb* rvrytph t K» late3. 3'BerucKilAnrtvaccne
ChryMoc
0<-n-Octy< Prttrujlate
. 2. 3-Cd>Pyren«
Oibenrd8«nio(g.
ug/I or ug/Kg(CircU One
$4*
fiuKM\fi\HI(Oit-
IOu.3bffiu.
ll
flu
Wtf.IC]\f-
(1 >-C»TX>1 b* i«p*r»t«d fr
FCH r^ I
4 1 8 485
' - • - "*::
^SF . ; - - •• :' . i ' .~ 'd ' : ' . f =, i":.4 ; = *
:it:'.f ''.iff'
i:-, A n a l y s i s D a t a Sheet(Paqe 3)Pestu ides/PCBs
[Lc»j Rpd;ui (Circle onei
Date Anaiy.-ed: 07-Dct-B7Conc/DiJ Factor;Percent Hoisture(decinted) HR
6PC Cleanup Ye; MSeparator Funnel Eitractior.Continuous Liquid-Liquid Extra:tisr
CAS [ug/L] or uNuiber
319-84-6 ftlphi-BHC 0.05 U319-85-7 Beti-BHC 0.05 U319-B6-6 Delti-BHC 0.05 U58-89-9 GaiH-BHC (Lindine) 0.05 U76-«4-8 Heptachlor 0.051)109-00-2 Aldrin 0.05 U1024-57-3 Heptichlor Epoiidr . 0.05 U959-98-8 Endosulfin I 0.05 U60-57-1 Jieldrin 0.1 U72-55-9 4,4'-DD£ 0.1 U72-20-8 Endrin 0.1 U33213-65-9 Endosulfifi II 0.1 U72-54-B 4,4'-DDD 0.1 U1-31-07-B Endosulfin Sulfite 0.1 U50-29-3 4,4 ' -BDT 0.1 U72-43-5 Kethojychlor 0.5 U53494-70-5 Endrin Ketont 0.1 U57-74-9 CMordanc 0.5 U8001-35-2 Touphene 1U12674-11-2 ftroclor-1016 0.5 U11104-28-2 flroclor-1221 0.51)11141-16-5 Aroclor-1232 0.5 U',3469-21-9 Aroclor-1242 0.5 U12672-29-6 ArDclor- i :4B 0.5 U11097-69-1 Aroclor-1254 ID11096-82-5 Aroclor-1260 1U
Vi = Voluie of eitract injected tul)Vs = Voluie of utter eitracted (illMs - Meiqht of saiple extracted (g)Vt ; Vo'.uie of total e i t ract (ul)
Vs = 1000 or Ms Vt 100CO Vi - 3.0
Fori 1
4 1 8 4 3 0 3 5 2
Laboratory Name ETC/Toxic on
• No
Organics Analysis Data Sheet(Page 4)
Tentatively Identified Compounds
Sample
CASMumtwr Compouod N««TM Frwction
1.. _&[££_
15
•**v16..
6..
2O..
1..
«..
!7..
10
NFA denotes no fraction analyzedNCF denotes no compound foundUnk denotes unknownmw denotes probable molecular weight
4 1 8 4 3 0 3 5 3
• . "EE
LABORATORY NAME. ETC/TOXICON
LAB SAMPLE 10 NO: 41B4-1«2SAMPLE MATRIX: WATER
DATA RELEASE AUTHORIZED BY
418*4184
ORGANICS ANALYSIS DATA SHEET
(PAGE 1)CASE NO:AC REPORT NO:CONTRACT NO:
DATE SAMPLE RECEIVED: •9/29/87
VOLATILE COMPOUNDS
CONCENTRATION: LOU
DATE EXTRACTED/PREPARED:DATE ANALYZED: l«/«3/«7
CONC/DIL FACTOR: 1.PERCENT MOISTURE: <NOT DECANTED)
PH
CAS NUMBER
74-S7-3 CHLOROMETHANE
74-11-9 BROMOHETHAME
7S-B1-4 VINYL CHLORIDE
78-••-3 CHLOROETHANE
7S-»»-2 HETHYLENE CHLORIDE . . .
47-44-1 ACETONE
7S-1S-* CARBON DISULFIDE . . . .7S-3S-4 1.1-OICHLOROETHENE . . .
7S-3S-3 1.1-OZCHLOROCTHANC . . .154-49-S TRANS-1.2-OICHLOROETHENE47-44-3 CHLOROFORM
l»7-«4-2 1.2-OICHLOROETHANE . . .7«-fl-l 2-BUTANOME
71-5S-* 1.1.1-TRICHLOROETHANE .
54-23-4 CARiON TETRACHLORIOC . .
i«8-«S-4 VINYL ACETATE
7S-27-* BROHOOICHLOROMETHAME . .
UG/L
!•!•!•119
1
!•
UUUUJUUUUUUU
UUU
CAS NUMBER7t-«7-S
1041-*2-4
124-4B-1
71-43-2
UG/L
7S-2S-2
S»l-7t-4
7t-34-S
•3*
1,2-OICHLOROPROPANE . . .TRANS-1,3-OICNLOROPROENE .
TRICHLOROETHENEOIBROP10CHLOROMETHANE . . .
1. 1.2-TRICHLOROETHANE . .BENZENECIS-1,3-OICHLOROPROPENE .
2-CHLOROETHYLVINVLETHER .
BROMOFORM4-HETHYL-2-PENTANONE . . .
2-HEXANONETETRACHLOROETHENE . . . .1.1.2.2-TETRACHLOROETHANE
TOLUENECHLOROBENZENEETHYLBENZENESTYREMETOTAL XYLENES
UUUUUUUUUUUJUUUUUU
B - COWPOUND WAS DETECTED IN THE «C BLANK.J - REPORTED VALUE IS LESS THAN THE DETECTION LIMIT.U - COMPOUND ANALYZED FOR BUT NOT DETECTED. THE REPORTED
VALUE IS THE MINIMUM ATTAINABLE DETECTION LIMIT FORTHE SAMPLE.
SEE PAGE 1A FOR COMPLETE DEFINITIONS OF THE DATAREPORTING QUALIFIERS.
FORM X
4 1 8 4 3 Q 3 6 9
Laboratory Name: ETC/Toxicon
rase No: 4184
Sample Number
Organics Analysis Data Sheet
CAS Number
67-63-0
71-36-3
78-92-2
Compound Name
Isopropyl Alcohol
N-Butyl Alcohol
sec-Butyl Alcohol
Concentration|i|/L
300U
200U
200U
*n*\ym\ fnr V^t |y^ faV&t4 Rgpflrt ** minimum Aftrt-Ann limit finr rtie tamplf with the 11(e.j. 10U) bued on aaxssxy concentntjoo/dilntka actkm. (This it not necessarily the Instrument detection limit)The footnote tV»iM read: U-Compouad wts totlyzed for bat not dftMfd. The number is the minimum attainabledetection limit for the sample.
an «timatM vihie. Thii flag bused dflier when e«timwhere a 1:1 response it assumed or when me mass qxctral data indicated fcc prae vt fif a nxnrK^ml *!*** "<m *»» M«*»-ficatioo criteria bot me resali bless than me fpecified detection limit but greater than iero(&f. 101). If limit of detection is10 m^L and a concentration of 3 (ig/L u cakiilatcd , report a§ 3J.
4 1 8 4 3 0 3 7 0
t . « : • • , N.
Concentration
Date Extracted
Date Analyzed
Cone/Oil Factor
CASNumber
"- • , ' -
Organics Ana(P
Semivolat
(Lovv^) Medium (Circle One)
'Pn»par»»d "-.'/^/(fO
!
tf (Decanted)
ug/lorug/Kg(Circle One)
nenol
S<-2-ChloroethvHEther
-Chloropn«r>ol
. 3-0«chlorobe>u«ne
. 4-Dichlorobenzent
entyl Alcohol
. 2-Dichloroberuenc
-Methytph*nol
is(2 <htor oisopropyDEther
-Mriy«ph«nol
- Nitroso-Oi -n -Propyte mine
exacMoroethant
rtroberuene
tophoron*
-Nrtroohenol
. 4-Dimetriy<pn*nol
teruoic Acid
is( • 2 -CMoroethocylMcthan*
. 4-Dknlorophenol
. 2, 4-Trich(orobeoz0ne
Uphtnakn«
•Chloroanilirw
<« xachlorobat«di«n«
-Chloro-3-M«rty1prwnol
,-Metfiy(n«phth«len*
tecicMorocvclopemadienc
!. 4. 6-Trich>orophenol
!. 4. 5-Tricnloroprtenol
! -CMoronaphifxalene
-Nitroaniline
iimethyl Phth»l»ie
icenaphthylene
lOu./fib.
10 uta*.10uiot^lrn~/AM.IQuiGaIDlA
lOuiffuIC^.Ifik
lUb-wiA
inu.lOt*./On.iDtttfi\fiQlL
IUK
(Oit-iQp.
/Ou.ft(A
(OtA56(\
K)&(C)IA.
lysis Data Sheetage 2)
ile Compounds
GPC Cleanup QYes D
Separatory Funnel Ext
Continuous Liquid - Li
CASNumber
3-32-9
1-28-5
00-02-7
32-64-9
21-14-2
606-20-2
8446-2
7005->2-3
86-73-7
00-01-6
534-52-1
86-30-6
01-55-3
118-74-1
87-86-5
85-01-6
120-12-7
84-74-2
206-44-0
129-00-0
J5-687
• 1-94-1
i6-5S-3
117-61-7
218-01-9
117-84 -O
205-99-2
207-08-9
JO-32-8
193 39 S
>3 703
191 24 2
SB r-pl- S ,:M'~.r
/TiO^ i'v ; j / C /
No
raction QYes
quid Extraction DYes
ug/torug/Kg(Circle One
Acenaphthene
[. 4-Otnrtroprienol
4-Nrtropr«enol
>ibeniofuran
!.4.0initrotoluene
L.6-Oinitrotoluene
Oiethytphthalate
4 -Chlorophenyl-prtenYlether
Fluor erw
4-Nrtroarufioe
4. 6-Oiniiro-2-Methylpherx>l
N-Nrtro$od»phertyUmir»e (1 )
4-Bromoohenyl-phenyletNer
Kexachbxobenzene
Pentachtorophenol
PNenantKren*
AnthraceneDi-n-Buty(phta«Ut«:luoranthene
Pyrerw
Butytoeruylp^^Ute
3. 3°-0«taorob«ruid<ne
B«ruo(aVknthrac«ne
Cxs(2-Ethy{f>eKyt)Ptnrxal«ie
ChryMrw
Di-n-Octyl Phthalate
Ber\io(b)Fluor>ntfier>e
Benzo(k f 1 ixxant Sene
B*nto<i)PvTene
Inoenotl. 2. 3-cdJPyene
O.bcnaa h)Antfv«cene
B«n»o(g. h. iJPeivlene
/^k&*5*14.
\C)kinuIfiu.ibu(Ci(0*
f^AS4U
lUuiCi*.
(C/u.50t\
iC/ii(fluIQujfiu
iOlL
J&uJ0(j
/(Ju.IfitIfJtA.
10iC}\r
IfJl*^IDiiLs'fnu.
lr,«.
(1) Cannot CM
4 1 8 4 30371
•I:'
0-ga-;:s Aralysis Data Sheet("age 3)Pesticides/PCBs
C;-:er.t'iti3r: [Leu] KedSite Ejfaitei'Presare::Sate Ar^rreJ: 07-Oct-E?Cone -'til factor:Fe-cent Hcistir
i Circle :ae)2'-Sep-B7
1
GPC Cleanup Yes [«]-NoSeparatary Fur.nel Eitraction Ves
us liquid-Liquid Eitrichon [ij Yes
CASNuiber
[ug/L] or ug/Cg
319-84-i Alph»-BHC ........................ 0.05 U319-85-7 Beti-BHC ........................ 0.05 U319-86-8 Delti-BHC ........................ 0.05 U58-69-9 Baiw-BHC (Lindint) ............. 0.05 U76-44-8 Heptachlor ...................... 0.05 U309-00-2 Aldnn .......................... 0.05 U1024-57-3 H«pt«hlor Epoiide ............... • 0.05 U959-98-8 Endosulfin I .................... 0.05 U60-57-1 Diildrin ........................ 0.1 U72-55-9 4,4'-DDE ........................ 0.1 U72-20-8 Endrin ........................ 0.1 U33213-65-9 Endosulfin II ................... 0.1 U72-54-8 4,4'-DBD ........................ 0.1 U1-11-07-8 Endosulfan Sulfite ............... 0.1 U50-29-3 4,4'-DDT ........................ 0.1 U72-43-5 Bethoxychlor .................... 0.5 U
53494-70-5 Endrin Ketone ................... 0.1 U57-74-9 Chlordwe ....................... 0.51)
8001-35-2 Touplwm ....................... 1U12674-11-2 ftroclor-1016 .................... 0.5 U11104-28-2 ftroclor-1221 .................... 0.5 U11141-16-5 Aroclor-1232 .................... 0.5 U53.469-21-9 Aroclor-1242 .................... 0.5 U12b^-29-6 Arcclor-1248 .................... 0.5 U110»?-69-l Araclor-1254 .................... 1 U11096-82-5 Aroclor-1260 .................... 1U
»i = Volutf of fitrtct injected (ul)Vs = Volute of »»ter eitricted (§1)Ms = Height of staple eitracted Iq)Vt - Voluie of total eitract (ul)
Vs = 1000 or Is Vt - 10000 Vi = 3.0
Fors 1
4 1 8 4 3 0 3 7 2
Lat>o. aio.y Name ETC/To* icon
e No
Organics Analysis Data Sheet(Page 4)
Tentatively Identified Compounds
S»»nple Number
CASCompound Nam* Fr»ctkxt
1- VGA
4.
S.
I"
li:-•i.. 51U
£Jc»
14..
I,...
17..
2O..
26.
28.
29.
3O
NFA denotes no fraction analyzedNCF denotes no compound foundlink denotes unknownmw denotes probable molecular weight
4 1 8 4 3 0 3 7 5
SAMPLE NUMBERMDLGU932*!
LABORATORY NAME: ETC/TOXICON
LAB SAMPLE ID NO: 4184-11*SAMPLE MATRIX: MATERDATA RELEASE AUTHORIZED BY
ORGAN ICS ANALYSIS DATA SHEET
(PAGE 1>CASE NO.
REPORT NO:CONTRACT NO.DATE SAMPLE RECEIVED: 49/29/87: frx///K/>-^—^/Lv*-/L/
41844184
VOLATILE COMPOUNDS
CONCENTMATION: LOWDATE EXTRACTED/PREPARED:
DATE ANALYZED: l«/*S/«7
CONC/OIL FACTOR. 1.PERCENT MOISTURE: <NOT DECANTED)
PH
CAS NUMBER
74-87-J74-83-97S-81-4
7S-M-375-89-2
47-44-1
75-15-871-3S-4
75-35-3154-48-547-44-3
187-84-278-93-371-55-4
54-23-5188-85-47S-27-4
CHLOROHETHANEBROMOMETHANE
VINYL CHLORIDECHLOROETHANEHCTHYLENC CHLORIDE . . . .
ACETONE
CARBON DISULFIOE
1. 1-OICHLOROETHENE . . . .
1. 1-OICHLOROETHANE . . . .
TRANS-1.2-OICHLOROETHENE .CHLOROFORM
1,2-DICHLOROETHANE . . . .
2-BUTANONE
1. 1. 1-TRICHLOROETHANE . .CARBON TETRACHLORIOE . . .VINYL ACETATEBROMOOICHLOROMETHANE . . .
UG/L!• U!• U!• U43S U39
UUUJUUJUU
18 US U
CAS NUMBER
78-87-518«41-«2-479-81-4
124-48-1
79-88-S
71-43-218841-81-S118-75-8
7S-25-2188-1*-!S91-78-4
127-18-4
79-34-S1*8-88-3
188-98-7188-41-4
148-42-S
ue/L1,2-OICHLOROPROPANE . . .TRANS-1.3-OICHLOROPROENE .TRICHLOROETHENEOUROMOCHLOROMETHANE . . .1,1,2-TRICHLOROETHANE . .BENZENCCIS-1.3-DICHLOROPROPENE .
2-CHLOROETHYLVINYLETHEM .
BROMOFORM4-METHYL-2-PENTANONE . . .
2-HEXANONC
TETRACHLOROETHENE . . . .1.1.2. 2-TETRACHLOROETHANE
TOLUENE
CHLOROBENZENEETHYLBENZENESTYRENETOTAL XYLENES
UUUUUUUUUUUUUUUUUU
J - REPORTED VALUE IS LESS THAN THE DETECTION LIMIT.
U - COMPOUND ANALYZED FOR BUT NOT DETECTED. THE REPORTEDVALUE IS THE MINIMUM ATTAINABLE DETECTION LIMIT FOR
THE SAMPLE.
SEE PAGE 1A FOR COMPLETE DEFINITIONS OF THEREPORTING aUALIFIERS.
DATA
FORM I
4 1 8 4 3 0 5 3 4
Labora to ry Name: ETC/Toxicon
Case No: 4184
Sample Numtxr
Organics Analysis Data Sheet
CAS Number
67-63-0
71-36-3
78-92-2
Compound Name
Isopropjl Alcohol
N-Butyl Alcohol
sec-Butyl Alcohol
Concentrationut/L
300U
200U
200U
U Tiviirant oompoood was analyzed for but oat detected. Report the minimum detection limit for the sample with the U(e.g. 10U) based on necessary concentntioo/dihttkm action. (TO* is oot necessarily the instrument detection limit)The footnote should read: U-Compound was analyzed for but oot detected. The number is the minimum attainabledetection limit for me sample.
value. This flag is used either when T^ ation for tentatively identified compoundswhere a 1: 1 response is assumed or when the mass spectral data indicated the presence of a compound dot meets the identi-fcation criteria but die result is less than the specified detection limit but greater than zero (e£. 101). If limit of detection is10 Hf/L and a concentration of 3 H£/L is calculated, report as 3J.
4 1 8 4 3 0 5 3 5
LABORATORY NAME
CASE NO
ETC/TOKICON
418*NUMBER
ORGANIC* ANALYSIS DATA SHEET
(PAGE 2)
SEMIVOLATILE COMPOUNDS
CONCENTRATION: LOW
DATE EXTRACTED/PREPARED: l*/17/87
DATE ANALYZED: It/28/87
CONC/OIL FACTO*: 1.PERCENT hOISTURE: <DECANTED)
GPC CLEANUP YES X NO
SEPARATORY FUNNEL EXTRACTION YES
CONTINUOUS LlaUIO-LIOUID EXTRACTION YES
CAS NUMBER
1*8-95-2 PHENOL
111-44-4 BIS<2-CHLORO€THYL)ETHER .
9S-57-S 2-CHLOROPHENOL$41-73-1 1.3-OICHLOROBENZENE . . .
1*4-44-7 1.4-OICHLOROBENZENE . . .
l**-Sl-4 BENZYL ALCOHOL
9S-S*-1 1,2-OICHLOROBENZENE . . .
95-48-7 2-METHYLPHENOL39438-32-9 •15<2-CHLOROI50PROPYL)ETHER
1*4-44-5 4-METHYLPMEMOL
421-44-7 N-NITROSO-DI-N-PROPYLAMINE
47-72-1 HEXACHLOROCTKANE
98-95-3 NITROiENZEMC
78-59-1 ISOPHOROME88-75-i 2-NITROPHEMOU
1*5-47-9 2. 4-01METHYLPHENOL . . . .
4S-8S-* IENZOIC ACID
111-91-1 ° BXS<2-CHLOROETHOXY)METHANE
;2*-83-Z 2. 4-OICHLOROPHENOL". . . .
128-82-1 1,2,4-TRICHLOROIENZENE . .
91-2*-3 NAPHTHALENE
1*4-47-8 4-CHLOROANILINC87-48-3 HEXACHV.OROBUTAOIENE . . .
S9-S8-7 4-CHLORO-3-METHYLPHENOL .
91-57-4 2-HETHYLNAPHTHALENE . . .77-47-4 HEXACHLOROCYCLOPENTAOIENE
88-*4-2 2.4, 4-TRICHLOROPHENOL . .
95-7S-4 2.4.S-TRICHLOROPHENOL . .
91-58-7 2-CHLORONAPHTHALEME . . .88-74-4 2-NITROANILINC
131-11-3 DIMETHYL PHTHALATC . . . .
2*8-94-8 ACCNAPHTHYLEME
99-«9-2 3-NXTROANILXNC
UG/I
1*181*1*1*1*1*
181*1*
181*18
181*1*
581*1*181*1*1*1*
1*1*1*
5*1*
581818
5*
UUUuuuuuuuuuuuuuuuuuuuuuuuuuuuuuu
CAS NUMBER83-32-9
51-28-518*-*2-7
132-44-9
121-14-2
4*4-2*-2
84-44-2
7885-72-384-73-7
l*8-l*-4
534-52-1
84-3*-4
181-55-3
118-74-1
87-84-5
8S-*l-8
128-12-7
84-74-2
284-44-*
129-**-*
85-48-791-94-1
54-55-3117-81-7
218-*l-9117-84-*
2*5-99-2
2*7-*8-9
5*- 32-8193-39-S
5 3-7*- 3
191-24-2
ACENAPHTHENE
2. 4-OINITROPHENOL . . . .
4-NXTROPHENOLDliCNZOFURAN
2.4-DINXTROTOLUENE . . . .
2.4-DXNXTROTOLUENE . . . .
OIETHYLPHTHALATE
4-CHLOROPHENYL-PHENYLETHEMFLUORENE
4-NXTROANILINC
4. 4-OINZTRO-2-METHYLPHENOL
N-NXTROSOOXPHENYLAMINE <1>
4-BROMOPHENYL-PHENYLETHER
HEXACHLOROBENZENE . . . .
PENTACHLOROPHENOL . . . .
PHENANTHRENE
ANTHRACENEOI-N-BUTYLPHTHALATE . . .
FLUORANTHENE
PYRENEBUTYLBENZYLPHTHALATE . . .
3. 3'-DXCHLOROBENZIOINE . .
BENZO(A) ANTHRACENE . . . .B X S < 2-ETHYLHEXYL > PHTHAL ATE
CHRYSENEOI-N-OCTYL PHTHALATE . . .
BENZO(B>FLUORANTHENE .
BENZO<H>FLUORANTH£NE . . .
BENZO< A) PYRENEXNOENO<1'2. 3-CD>PYRENE . .
DXBENZ<A.H> ANTHRACENE . .
BENZO<6. H.DPERYLENE . . .
UG/l1*S*
• •1*1*1*1*1*1*5*5*1*1*1*5*1*1*1*1*1*1*2*1*1*1*1*1*1*
1*1*1*18
UUU
uuuuuuuuuuuuuuuuuuuuuuuuuuuuu
<1> - CANNOT BE SEPARATED FROM OIPHENYLAMXNEFORM X
4184 30536
s-r
A n a l y s i s Eiti(Page 31Pestiudes/PCBs
C:nceitrat:Dn: [Lou] ''ediLi (Circle one)[ate [it'a:l.ei,frepa'ed: 29-Sep-87Date fir-:,-red: 07-Cct-B?Cor-:/Dil factor: 1rercer,t "oistjreldeiJited; NR
BPC Cleanup Yes [«HoSeparatory Funnel Extraction YesContinuous Liquid-Liquid E«trir.tii?n [i] Yes
CAS [ug/L] or ug/Kq
319-B*-6 Alptu-BHC ........................ 0.05 U319-85-7 Beti-BHC ........................ 0.05 U319-B6-B Delti-BHC ........................ 0.05 U58-B9-9 Saiti-BHC (Lindinr) ............. 0.05 U7fc-M-B HepUchlor ...................... 0.05 U309-00-2 ftldrin .......................... 0.05 U1024-57-3 Heptichlor Epoiide ............... 0.05 U959-9B-8 Endosulfin I .................... 0.05 U60-57-1 Ditldrin ........................ ' 0.1 U72-55-9 4,4'-DOE ........................ 0.1 U72-20-8 Endrin ........................ 0.1 U33213-45-9 Endosulfin II ................... 0.1 U72-54-B 4,4'-ODD ........................ 0.1 U1-31-07-8 Endosulfin Sulfitf ............... 0.1 U50-29-3 4,4'-DOT ........................ 0.1 U72-43-5 Hethwychlor .................... 0.5 U53494-70-5 Endrin Kttoni ................... 0.1 U57-74-9 Chlordine ....................... 0.5 U8001-35-2 Toxiphene ....................... 1U12674-11-2 Aroclor-1016 .................... 0.5 U11104-28-2 Aroclor-1221 .................... 0.5 U11141-16-5 Aroclor-1232 .................... 0.5 U53469-21-9 Aroclor-1242 .................... 0.5 U12672-29-6 Aroclor-1248 .................... 0.5 U11097-t9-l Aroclor-1254 .................... 1 U1109t-B2-5 Aroclor-1260 .................... ID
Vi = Voiuie of titrtct injected (ul)Vs = VoluM of «it»r extracted (il)Ms - Height of saiple eitrie ted (g)Vt - Voluie of totil eitrict (ul)
Vs = 1000 or Ms - Vt = 10000 Vi = 3.0
Fon 1
4 1 8 4 3 0 5 3 7
I i t . , ' .1:. • •
Case No
Organics Analysis Data Sheet(Page 4)
-"]Tan ta lively ld«ntif««d Compounds
CASNumb** Compound Frvction
of cjg/kg)
,40..
11.. (foeIf* n£31
•14..
IS..
1(053/>«k \ /
li.
M.
,24..
'25..
NFA denotes no fraction analyzedNCF denotes no compound foundUnk denotes unknownmw denotes probable molecular weight
4 1 8 4 3 0 5 3 8
LABORATORY NAME. ETC/TOXICON
LAB SAMPLE 10 NO: 4184-95
SAMPLE MATRIX: MATER
OATA RELEASE AUTHORIZED BY
»184
418*
OROANICS ANALYSIS OATA SHEET
(PAGE 1>
CASE NO.
\ . 8C REPORT NO.CONTRACT NO:DATE SAMPLE RECEIVED:
VOLATILE COMPOUNDS
•9/29/87
CONCENTRATION: LOUDATE EXTRACTED/PREPARED:DATE ANALYZED. l*/*3/87CONC/OIL FACTOR: 1.PERCENT MOISTURE: (NOT DECANTED)
PH
CAS NUMBEI74-87-374-B3-975-81-475-88-375-89-247-44-175-15-875-35-475-35-3154-48-547-44-3187-84-278-93-371-55-454-23-5188-85-475-27-4
t IKCHLOROMETHAKE 14BROMOHETHANE . 14VINYL CHLORIDE 14CHLOROETHANE 13HETHYLENE CHLORIDE . . . . !ACETONE . 14CARBON DISULFIOE1. 1-OICHLOROETHENE . . . .1, 1-DICHLOROETHANC . . . .TRANS-1. 2-DXCHLOROETHENE .CHLOROFORM1.2-OICHLOROETHANE . . . .2-BUTANONE 11. 1. 1-TRICHLOROETHANE . .CARBON TETRACHLORIOE . . .VINYL ACETATE 1BROMOOICHLOROHETHANC .. . <
i/L
> U> U> U1\ uk
uuuuuu
/*uu
» ui u
CAS NUMBER78-87-S1*841-82-479-81-4124-48-179-88-571-43-2
18841-81-5118-75-875-25-2188-18-1591-78-4127-18-479-34-5188-88-3188-98-7188-41-4188-42-5
UG/L
1.2-OrCHLOROPROPANC . . .
TRANS-1,3-OICHLOROPROENE .
TRICHLOROETHENE
DIBROMOCHLOROMETHANE . . .
1.1.2-TRICHLOROETHANE . .
BENZENE
CIS-1,3-DICHLOROPROPENE .
2-CHLOROETHYLVINYLETHE* .
BROHOFORH
4-HETHYU-2-PENTANONE . . .
2-HEXANONC
TETRACHLOROETHENE . . . .
1,1.2.2-TETRACHLOROETHANE
TOLUENE
CHLOROBENZENE
ETHYLBENZENE
STYRENE
TOTAL XYLENES
1*5
UUuUu
uuuuuuuuuuuu
B - COMPOUND WAS DETECTED IN THE «C BLANK.
U - COMPOUND ANALYZED FOR BUT NOT DETECTED. THE REPORTED
VALUE IS THE MINIMUM ATTAINABLE DETECTION LIMIT FOR
THE SAMPLE.
SEE PACE 1A FOR COMPLETE DEFINITIONS OF THE OATAREPORTING aUALIFIERS.
FORM I
4 1 8 4 3 0 2 1 1
Labora to ry Name: ETC/Toxicon
Case No: 4184
Sample Number
Organics Analysis Data Sheet
CAS Number
67-63-0
71-36-3
78-92-2
Compound Name
Isopropjl Alcohol
N-Butyl Alcohol
sec-Butyl Alcohol
Concentration«/L
300U
200U
200U
Tiviir-yti-^ compound wts analyzed for but not <V-*fft"^ Report me mmimnm detection limit for the sample with the U(e.g. 10U) based on necessary couccmiation/dfluDOC action. fTha is not necessarily me instrument detection limit)The footnote shook! read: U-Compoond wts analyxcd for bat not detected. The lumber is the minimum attainabledetection limit for me sample.
**«"«*<"£ • <^nv*ntr«ri«i far tentarivdy Mearificd eompopndl1:1 rcipontf ii ngnmrf qr «wn fte T»^H sffftt^ «<ia W8""*! **• i*" 1* rf« gnmMind tfat ma^a the idgnri.
fication criteria but flie resabis lea than (be ipedfled detection limit bot|reaiermaniero(e4. 101). If limit of detection is10 \if/L and a concentntioa of 3 HJ/L is calcuUMd. report ax 3J.
4 1 8 4 3 0 2 1 2
LABORATORY NAMECASE NO
E T C / T O X I C O N4184
NL-HBER
ORGANICS ANALYSIS DATA SHEET(PAGE 2)
SEHIVOLATXLE COMPOUNDS
CONCENTRATION: LOWDATE EXTRACTED/PREPARED: *9/3««/B7DATE ANALYZED: l*/*S/87CONC/OIL FACTOR: 1.PERCENT MOISTURE: <DECANTEO>
GPC CLEANUP YES X NOSEPARATORY FUNNEL EXTRACTION YESCONTINUOUS LIBUIO-LI9UIO EXTRACTION YES
CAS NUMBER1*8-95-2 PHENOL111-44-4 §IS<2-CHLOROETHYL>ETHER .9S-S7-8 2-CHLOROPHCNOL5*1-73-1 1.3-OICHLOROiENZENC . . .166-44-7 1.4-DICHLOROBENZENE . . .l**-51-4 BENZYL ALCOHOL9S-S*-l 1,2-OICHLOROBENZENE . . .95-48-7 2-hETHVLPHEHOL39638-32-9 BIS<2-CHLOROISOPROPYL>ETHER1*4-44-! 4-METHYLPHENOL421-44-7 N-NITROSO-DI-N-PROPYLAMINE47-72-1 HEXACHLOROETHANC
98-9S-J NITROBENZENE7B-59-1 ISOPHORONE•B-7J-§ 2-NITROPHENOL
16S-47-9 2.4-DIHETHYLPHENOL . . . .45-85-6 BENZOIC ACID111-91-1 BIS<2-CHLOROETHOXY>METHANE12*-83-2 2.4-OICHLOROPHENOL . . . .126-82-1 1.2,4-TRICHLOROBENZENE . .9l-2*-3 NAPHTHALENE . . '1*6-47-8 4-CHLOROANILINE
87-68-3 HEXACHLOROBUTADIENE . . .S9-S*-7 4-CHLORO-3-METHYLPHENOL .91-57-4 2-HETHYLNAPHTHALENE . . .77-47-4 HEXACHLOROCYCLOPENTADIENE88-*4-2 2. 4, 4-TRICHLOROPHENOL . .95-95-4 2,4,5-TRICHLOROPHENOL . .91-58-7 2-CHLORONAPHTHALENE . . .88-74-4 2-NXTROANILINC131-11-3 DIMETHYL PHTHALATE . . . .2*8-94-8 ACENAPHTHYLENE99-*9-2 3-NITROANILINE
UG/L
!•1*!•1816!•18181816161616161616S6161616161616161616165616S616165*
UUUUUUUUUUUUUUUUUUUUUUUUUUUU
UU
UUU
CAS NUMBER83-32-951-28-51*8-82-7132-44-9121-14-2464-28-284-44-2766S-72-384-7J-71*6-16-4534-52-184-36-41*1-55-3118-74-187-84-18S-61-8126-12-784-74-2264-44-6129-66-68S-48-791-94-154-55-3117-81-7218-61-9117-84-62*5-99-22*7-*8-95*-32-B193-39-553-76-3191-24-2
ACENAPHTHENE2.4-DINITROPHENOL . . . .4-NITROPHENOLOIBENZOFURAN2,4-OINITROTOLUENE . . . .2.4-DXNXTROTOLUENE . . . .OIETHYLPHTHALATE4-CMLOROPHENYL-PHENYLETHCR
FLUORENC4-NITROANILINE4. 4-OINITMO-2-METHYLPHENOLN-NITROSOOIPHENYLAMINE <1>4-BROHOPHENYL-PHENYLETHERHtXACHLOROBENZENE . . . .PEKTACHLOROPHENOL . . . .PHENANTHRENEANTHRACENEDI-N-BUTYLPHTHALATE . . .FLUORANTHENEPYRENEBUTYLBENZYLPHTHALATE . . .3.3'-OICHLOROBENZIOINE . .8ENZO<A)ANTHRACENE . . . .BIS<2-ETHYLHEXYL> PHTHALATECHRYSENEOI-N-OCTYL PHTHALATE . . .BENZO(B>FLUORANTHENE . . .BENZOOOFLUORANTHENE . . .BENZO<A)PYRENEINOENO<1.2.3-CO>PYRENE . .DIBENZ<A.H>ANTHRACENE . .BENZCMG. H, DPERYLENE . . .
UG/L16 U
UU
56561616161616165*5*161616ft*16161616161626161616161*1*1*1*1*
UUUUUUUUUUUUUUUUUUUUUUUUUUUU
16 U
<1> - CANNOT BE SEPARATED FROM 01PHENYLAMINE
FORM X
4 1 8 4 3 0 2 1 3
tin dtr-Cd'.E NC
Festicides/F'i&s
Concentration: [Lou] llediut (Circle one)Date Extracted/Prepared: 2?-Sep-87Date Analyzed: 06-OCT-87Conc/Dil Factor: 5Percent Hoisturefdlecanted) NR
EPC Cleanup Ves (x]-NoSsparjtory Fu-nsl Extraction YesContinuous Liquid-Liquid Extraction [i] Yes
CAS [uq/L] or us/KgNuiber
319-84-6 Alphi-BHC 0.25 U319-85-7 Beti-BHC 0.25 U319-Bt-B Delta-rHC 0.25 U58-69-9 Gifu-BHC (Lindine) 0.25 U74-M-E Heptachlor 0.25 U309-00-2 flldnn 0.25 U1024-57-3 Heptachlor Epoiide 0.25 U959-98-8 Endosulfin I 0.25 U60-57-1 Oitldrin ''o.5U72-55-9 4,4'-DDE 0.5 U72-20-B Endrin 0.51)33213-65-9 Endosulfin II 0.5 U72-54-8 4,4'-DDD 0.5 U1-31-07-B Endosulfin Sulfile 0.5 U50-29-3 4,4'-DDT 0.5 U72-43-5 nethoxychlor 2. U53494-70-5 Endrin Ketone 0. U57-74-9 Chlordin* 2. U8001-35-2 Toxaphene U12674-11-2 Aroclor-1016 2. U11104-28-2 Aroclor-1221 2.5 U11141-16-5 Aroclor-1232 2.5 U53469-21-9 Aroclor-1242 2.5 U12i72-29-(- «roclor-124B 2.5 U11C97-69-1 flroclor-1254 5U11096-82-5 Aroclor-1260 5U
Vi = Voluie of extract injected (ul)Vs - Volute of niter extracted (illIK = Height of saiple extracted (g)Vt -- Voluie of total extract (ul)
Vs = 1000 or Ms - Vt = 50000 Vi - 3.0
Fora ]
4184 30214
o.r f lo. , N.,,nc _KI'-''J^ ; i ;''";; _
Case No
Organics Analysis Data Sheet(Page 4)
Sample fJ, j . r \ t>--
Tentatively Identified Compounds
CASCompouod Nam* Fraction
RT of
(ug/jfor ug/Vg)
1..2-oC,
/r
tf*7V
•7..
I.UkkUnit
W
ILnLUnic
An u .IB
17.
/Xnk: A
121..
23..
24..
25..
26..
27..
29..
30..
NFA denotes no fraction analyzedNCF denotes no compound foundUnk denotes unknownmw denotes probable molecular weight
4 1 8 4 3 0 2 1 5
MOLl-w? 34*1
LABORATORY NAME: ETC/TOXICON
LAS SAMPLE 10 NO: 4114-94SAMPLE MATRIX: WATER
DATA RELEASE AUTHORIZED •
ORGANICS ANALYSIS DATA SHEET
(PAGE 1)
CASE NO:
8C REPORT NO:
CONTRACT NO:
DATE SAMPLE RECEIVED.4l41844184
•f/29/87
VOLATILE COMPOUNDS
CONCENTRATION: LOW
DATE EXTRACTED/PREPARED:
DATE ANALYZED: l«/*3/87
CONC/DIL FACTOR: 1.
PERCENT MOISTURE: (NOT DECANTED)
PH
CAS MUNICH
74-87-1 CHLOROMETHANE
74-83-9 BROHOMETHANE
71-4U-4 VINYL CHLORIDE
7S-88-J CHLOROETHANE
71-89-2 METHYLENE CHLORIDE . . .
67-44-1 ACETONE
7S-1S-* CARBON OISULFIDE . . . .
71-31-4 1.1-DICHLOROETHENt . . .
71-15-1 1.1-DICHLOROETHANE . . .
1S4-48-1 TRAM1-1.2-OKHLOROETHENE
47-44-1 CHLOROFORM
1*7-84-2 1.2-OICHLOROETHANC . . .
71-93-3 2-1UTANOWE71-S»-* 1,1,1-TRICHLOROETHANE .
14-23-1 CARBON TETRACHLORIOE . .
1*8-81-4 VINYL ACETATE
71-27-4 BROHODICHLOROHETHAME . .
CAS NUMBER
!•
18
18
1
18
1
18
1
UUUUUUUUUUUU
UUUU
79-81-4
124-48-1
71-43-218841-81-1
118-71-8
71-21-2
191-78-4
127-18-4
79-34-1
188-88-3
188-41-4
188-42-1
1.2-DICHLOROFROPANE . . .
TRAN1-1.1-DXCHLOROPROENE .
TRICHLOROETHENE
OIBROHOCHLOROMETHANE . . .
1.1.2-TRICHLOROETHANE . .
BENZENE
CIS-1,3-OICHLOROPROPENE .2-CHLOROETHYLVZNYLETHER .
BROMOrOMH4-HETHYL-2-FENTANONE . . .
2-HEXANONETETRACHLOROETHCNE . . . .
1.1.2.2-TCTRACHLOROETHANE
TOLUENE
CHLOROBENZENE
ETHYLBENZENE
STYRENC
TOTAL XYLENE1
UG/L1SsS11s
UUUUUUUUUUUUUUUUUU
8 - COMPOUND WAS DETECTED IN THE BC BLANK.U - COMPOUND ANALYZED FOR BUT NOT DETECTED. THE REPORTED
VALUE IS THE MINIMUM ATTAINABLE DETECTION LIMIT FORTHE SAMPLE.
SEE PAGE 1A FOR COMPLETE DEFINITIONS OF THE DATA
REPORTING B.UALIFIER1.FORM I
4184 30248
Laboratory Name: ETC/Toxicon
Case No: 4184
Sample Number
10 3o
Organics Analysis Data Sheet
CAS Number
67-63-0
71-36-3
78-92-2
Compound N>me
Isopropyl Alcohol
N-Butyl Alcohol
sec-Butyl Alcohol
Concentrationjif/L
300U
200U
200U
U Tnduf*»f romrrtnvl jygg analyzed fOT but <VM <Vtf"1*'l_ RCBOft me minimum ijf^p'tfffq Imiit f(jf (he f«^p^f with |he U(e.(. 10U) based on necesvy concentntioB/dlhitian acttoo. CThit U not neccsvilymeuistnuneatdetoctiooUinil)The footnote timid rod: U-Compoond was analyzed for but not detected. The number is the mimmom tftriubfe
tvahe, Thb flat Un^ richer when e«tinudnj a cooceai«k)n for tentatively identiWoCPC till ICSDOQ3C IS ftSSD^QfiQ Of WuCO ^DC ^DAU tDOCt^H ullft IPolCJtPo QIC DI QCOCC OK ft C^^-UHMtlQ t&flt ^ftOCO u9C lOCflO"ficaion oteia but the result it less than tb« g>edfled detoetioo limit but greater man rero (04.101). If limit of detection ii10 \iffL and a concentration of 3 u$/L is calnilitfrrt, report at 3J.
4 1 8 4 3 0 2 4 9
r, .t
Case Mo
Concentration: (Low") Medium
Date Extracted'Prepared
Date Analyzed: Icldrhl
Organics Analysis Data Sheet(Page 2)
Semivolatile Compounds
(Circle One)
N'jrn be r
Cone/Oil Factor:
Percent Moisture (Decanted).
GPC Cleanup QYes ONo
Separatory Funnel Extraction QYes
Continuous Liquid • Liquid Extraction QYes
CASNumber
ug/torug/Kg(Cwcle One)
CASNumber
108 95-2111-44-495-57-8541-73-1106-46-7100-51-695-50-195-48-739638-32-9106-44-5621-64-767-72-198-95-378-59-188-75-5105-67-965-85-0111-91-1120-83-212O-82-191-20-3106-47-887-68-3S9-SO-791-57-677-47-488-06-295-95-491-58-788-74-4131-11-3208 96-899-O9 2
Phenolois<-2 -CWoroeth/HEther2-CM<xoprvtrtol1. 3-Oichlorobenz«ne1. 4-OichlorobenzeneBenzyl Alcohol1. 2-Dicnforob*n»ne2-M^hylprwnolbi«(2-chloroisopropyl)EtrMr4-M*thy1ph«nolN-Nrtroso-Oi-n-PropylamineHexacMoroethaneNrtrobenzeneIsophoront2-Nitropnenol2. 4-DimethylphenolBeruoic Acidbis( • 2 -CMoroethoxYlMemant2. 4-OicriloropHenol1. 2, 4-TrichlorotenuneNaphtha l«n«4-CMoroaniline
He Kachtorobutadiene4-Chloro-3-M«thY<phenol2-Methy<naphthaltnt
2. 4. 6-Trichlorophenol2. 4. 5-Tnchkxophenol2 -Chloronaphthalent2-N<iroanilineDimethyl PhthalateAcenaphTtiyleoe3-Nilroaniline
/0U./Ok10 utoi,.10k10k.{nt~\F\VL(fluluaIDulOuIDu}£Hifiu/Qb-
WfA
/nu.feklOu.IDum±tOfilUt<Ity.10*/Ou
S'tu(CliA
56*ID*IQlA
s»*
ug/lorwg/Ke(Circle One
83-32-951-28-5100-02-7132-64-9121-14-2606-20-284-66-27005-72-316-73-7100-01-6534.52-186-30-6101-55-3118-74-117-86-StS-01-8120-12-784-74-2206-44-0129-OOX)15-68-711-94-1>6-55-3117-81-7218-01-9117-84-0iOS-99-2207-08-9J032-8193 39 5i3-703191 24-2
Acenaphthene!. 4-Dinhroph«nol
4-Nitrophenol>ibemofuran!.4-Oinitrotoluene
2..6-Oinitrotolu«n«Oiethylphthalate4-Chlorophenyl-phenytether:luor»ne4-NrtroanilirM4. 6-Oinhro-2-Methy(ph«nolN-NrtrosodiphenyUmine (1)
Hexachloroberu«n«PtntachlorophenolPhencnthreneAnthraceneOt-n-Butylphthalate:luorinthenePyreneBjtytt>eruY<phthat«te
3. 3''0tchlorober\tid4neB*<uo(i (Anthracenebu(2-Ethy«h«xYl)Prrtn*l«teChrysene0«-n-Octy< PhthafateBento(b)FluoranmeneBeniotk)Fluoranth«neBen«o(a)Pvr«neIndenotl. 2. 3<dlPyreneOcbenita h(Antht jceneB«nro(g. h. iJPerylene
IVlt'faStu
IfOkIfiu\hu./ham*-10*
fsKsou
IVutot*(flu.
Si*
IQ"[fiu
!QUnulOh
WuJeu
/(JU./QL\OtA-
IQu.mirId1*'//)t^inu^mi*.fn«.
(l)-Cannoi b«
fO'4 1 8 4 3027S
a=e No: 4164
Orqanics flnalysis Data Sheet(Page 3)Pesticides/PCBs
Conce"trjt.jc'-: [Lou] fledju* (Circle one)Date Extracted/Prepared; 29-Sep-B7Date Analyzed: Oi-Oct-B7Conc'Dil Factor: 1Percent Hoisture(decanted) UR
BFC Clej-'.p Yes [0-MoSeparatory Funnel Extraction YesContinuous Liquid-Liquid Extraction [x] Yes
CAS [ug.'L] or ug/KgNuibtr
319-84-6 Alph»-BHC 0.05 U319-85-7 I»U-BHC 0.05 U319-86-8 OelU-BHC 0.05 U58-89-9 6a«u-BHC (Lindane) 0.05 U76-44-8 HepUchlor 0.05 U309-00-2 Aldrin 0.05 U1024-57-3 Heptichlor Epoxidi 0.05 U959-98-8 EndosultM I 0.05 U60-57-1 Dieldrin 0.1 U72-55-9 4,4'-DD€ 0.1 U72-20-8 Endrin 0.1 U33213-65-9 Endosulfin II 0.1 U72-54-8 4,41-ODD 0.1 U1-31-07-8 Endosulfin Sulf»te 0.1 U50-29-3 4,4'-Dl>T 0.1 U72-43-5 Bethoiychlor 0.5 U53494-70-5 Endrin K«ton« 0.1 U57-74-9 Chlord»n« 0.5 U8001-35-2 To»»phM» ID12674-11-2 Aroclor-1016 0.5 U11104-28-2 Aroclor-1221 0.5 U11141-16-5 Aroclor-1232 0.5 U534A9-21-9 Aroclor-1242 0.5 U12672-29-6 ftroclor-1248 0.5 U11097-69-1 Arodor-1254 I D11096-82-5 Aroclor-1260 1U
Vi = Volutt of extract injected (ul)Vi = Volute of »*ter extracted 111)N« - Mfiqht o< staple ext racted (g)Vt -- Voluw of total ex t rac t lull
Vs -- 1000 or Hs Vt = 10000 = 3.0
For§
4 1 8 4 3 0 2 5 1
Lai aio' y f ; . < : • • • . - I: • •_ ' '.'.
~ - - ;pNo
Organics Analysts Data Sheet(Page 4}
Sample
Tentatively Identified Compounds
;ASCompound N«m« Fraction
RT«n < i tion
(fl/j/orog/kg)^
/. .
•- .
1O..
IV. 51*?
16..
19..
21..
I..
24..
i..
-5..
29
NFA denotes no fraction analyzedNCF denotes no compound found'nk denotes unknown.nw denotes probable nrxDlecular weight
4 1 8 4 3 0 2 5 2
LABORATORY NAME: ETC/TOXICON
LAB SAMPLE ID NO: 4184-112
SAMPLE MATRIX: HATERDATA RELEASE AUTHORIZED BY
418*4184
ORCANICS ANALYSIS OATA SHEET
(PAGE 1)
CASE NO:*C REPORT NO:CONTRACT NO:
DATE SAMPLE RECEIVED:
VOLATILE COMPOUNDS
•9/29/87
CONCENTRATION: LOW
DATE EXTRACTED/PREPARED:
DATE ANALYZED: l»/»S/87
CONC/DIL FACTOR: 1.
PERCENT MOISTURE: (NOT DECANTED)
PH
CAS NUMBEI74-87-374-83-f75 -81-*
7S-88-375-89-247-44-17S-U-*7S-3S-*75-35-3154-48-547-44-3187-84-278-93-371-SS-4S4-23-I188-85-475 -27-*
I
CHLOROMETHANEiROHOMETHANEVINYL CHLORIDECHLOROETHANCMETHYLENE CHLORIDE . . . .ACETONECARBON OISULFIDE1. 1-OICHLOROETHENE . . . .1. 1-OICHLOROCTHANC . . . .TRAMS-1.2-OICHLOROETHEMC .CHLOROFORM1,2-OICHLOROETHANE . . . .2-BUTANONE1, 1, 1-TRICHLOROETHANE . .CARBON TETRACHLORIDE . . .VINYL ACETATEBROMOOICHLOROMETHANE . . .
UO
14
1114
14
1
14
1
1<
/L
1 U• U1 U) U> u» u
uuuuuuuuu
I U
K U
CAS NUMBER78-87-K!••& 1-82-479-81-4124-48-179-M-571-43-218841-Ol-f'118-75-87S-2S-2188-18-1591-78-4127-18-479-34-S1*8-88-3188-98-7188-41-4188-42-5
UO/L
1.2-DICHLOROPROPANE . . .TRAN5-1.3-DICHLOROPROENE .TRICHLOROETHENEOIBROMOCHLOROHETHANE . . .1.1,2-TRICHLOROETHANE . .BENZENE
CIS-1.3-DICHLOROPROPENE .2-CHLOROETHYLVINYLETHER .BROMOFORN
4-MCTHYL-2-PENTANONE . . .2-HEXANONt
TETRACHLOROETHENE . . . .1.1.2.2-TETRACHLOROETHANETOLUENE
CHLOROBENZENCETHYLBENZENCSTYRENETOTAL XYLENCf
18S1*!•I10SS•SS
uuuuuuuuuuuuuuuuuu
U - COMPOUND ANALYZED FOR BUT NOT DETECTED. THE REPORTEDVALUE IS THE MINIMUM ATTAINABLE DETECTION LIMIT FORTHE SAMPLE.
SEE PAGE 1A FOR COMPLETE DEFINITIONS OF THE DATA
REPORTING QUALIFIERS.FORM I
4 1 8 4 3 0 5 7 5
Laboratory Name: ETC/Toxicon
Case No: 4184
Sample Number
Organics Analysis Data Sheet
CAS Number
67-63-0
71-36-3
78-92-2
Compound Name
Isopropyl Alcohol
N-Butyl Alcohol
sec-Butyl Alcohol
ConcentrationHi/L
300U
200U
200U
U Tnrticata c^T^tld "$ "ulyr^ fnr Hit rift AnmtA Bqvwt die minimum detection limit fog the mnple with me U(e.f . 10U) based on necessary concenlratioo/dilutJoo action. (Tto u »ot necessarily me instromem detection limit)Tbt footnote sbookl read: U-Compouod was analyzed for but not detected. The amber u the minimum inainabtedetection limit for the sample.
an fttim*fA value. This flag U used either when »p«Mring s coocentratioa far tentatively identified compounds1:1 fSpOMf U Igynffi Or TOPI fcC man lp«?rrf 4at> i~«^*4 i*«> pn^mr^ rf • nnmpmnd
featioo criteria btttbercsott is less than the speared det^^ If limit of detection is10 H4/L and a concentntion of 3 U£/L is calculated, report as 3J.
4 1 8 4 3 0 5 7 6
_ase No
_:or>centration
Date Extracted'Prepared
Organics Analysis Data Sheet(Page 2)
Semivolatile Compounds
Medium (Circle One)
S»mplo N
>ate Analy7ed (tin 1X1
Conc/Dil Factor:
'ercent Moisture (Decanted).
GPC Cleanup OYes DNo
Separaiory Funnel Extraction QYes
Continuous Liquid • Liquid Extraction QYes
CAS wQ/lorug/KgNumber (Circle One
106 95 2111-44-4
95 57-8
Ml -73-1
106-46-7
100-51-6
95-50-195-48-739636-32-9106-44-5621-64-767-72-198-95-378-59-188-75-5105-67-965-85-0111-91-1120-83-2120-82-191-20-3106-47-887-68-359-50-791-57-677-47-488-06-29595-491 58-788-74-4131-11-3208 96 899-09 2
Phenolbis<-2-Chtoroethyl|Ether2-Chlorophenol1 . 3-Dichlorobentene1. 4-DtchloroberueneSeruyi Alcohol1 . 2-Dichloroberuene2-Methylph«nolbts(2-chloroiMpropy1|ElH«r4-Methy<ph«nolN-Nitroso-Di-n-PropvUmirteHexachloroethaneNitrobenzeneUophofooe2-NiuopSenol2. 4-Dimethy<phenolBenioic Acidbi«( • 2 -Chtef oetnoxylMetna ne2. 4.Qichlorophenol1. 2. 4-TricMorobenzeneNaphthalene4-CMoroenitineHecacMorobuiadierte4-Chloro-3-Methy1pl>enol2-Memyl naphthaleneHeuchtorocyclopentadien*2. 4. 6-Trichloropnenol2. 4. 5-Tr<hloropKenol2 -CMoronaphthalene2-Nitroan<lineDimethyl PhthalateAcen«Dhthytene
3-NiIfoanilir>«
/On.rf}*10 itIn*.10u
/Ot^/nt~/rttciQuJuu.lf)ulOulOuIC^iQuIQ^
Wttinu.feuiOu.ID*m±lf)U
lOu.lOif-Ifo/OlA.
rou(flu
5t><*IDlA.
I0t*5»i\
CAS ug/lorug/KgNumber (Circle One
83-32-951-28-5100-02-7132-64-9121-14-2606-20-28446-27005-72-386-73-7100-01-6534-52-186-30-6101-55-3118-74-18746-585-01-8120-12-7W-74-2206-44-0129-00-0»5-68-7M-94-1>6-553117-81-7218-01-9117-84-0205-99-2207-08-9J032-819339553-70-3191-24-2
Acenaphtrtene2. 4-Dinhrophenol4-Nitrophenol>iber\zofuran!. 4-Oinmoioluene!. 6-Oinhrotoluene
Oiethytpnthatate4-Chlorophen)1-pnenyletherRuorene4-Nttroaniline4. 6-Oinhro-2-MethYlpnenolN-NitrosodiphenyUmine (1 )4-Bromapneny1-pn*nytetherHexachlorobenzenePentachtefophenol^wriantTifer eA nTflrar^tfi*
Ot-n-SutylpHthatateFluorinthenePyreneBurylbemytphtha late3. 3'-0«Morober\zidine
Be<uo(< (Anthracene
bt*2-Ethy!hexy<)Prrthalate
CNy»ene
Oi-n-Octy4 Phthatate
B«rua(b)Fluor«nthene
Benzo(V)Fluoranthe<%e
BennXalPYTArw
lr«Jeno(1.2. 3<d»Py^ne
Oib«rvi(a hJAnthracerie
6«nio(g. h. i)PeTY<eoe
IVlA.'fa
54 U\n\*.lf)u/PU./huin*-fOif
5^ A
ft 14jOu.faIfiu.
*>«On
ftiufQuIf) Li
((?'')buJ»a
lOu./fluHJISL
(Ou./ntrifltL,
Ifivinu.ip<~In*.
(1 r-Canr>oi be
F 0'
4 1 8 4 3 0 5 7 77 - 8 5
-I
late E:tra:tf;:;Frepa'?;: :5-Ee;-6?
Cnnc/Dil Factor:Percent M:r=tLreH!s:arls:J'
Njiber
'ralvs;s Data it-pet
6PC r.!eanuf Yes [i]-NoSeparator; Fur..iel Eitrjction YesI:"*:.'u:u5 Liqs;iiJ-Li5i;ii! Estraction [>} Yes
or
319-B5-7
"19-Bt-B5B-89-9
309-OC-21024-57-3959-98-860-57-1
72-55-972-20-9
33213-65-972-54-81-31-07-850-29-372-43-553494-70-5
57-74-98001-35-212674-11-211104-28-2
11141-16-55*469-21-9
I'l'^-ei-l11C96-B2-?
Beti-BHCDelU-BHC
HeptjcMor
AldrinHeptachlor Eponde
4, 4' -DDE
Erdosulfin II4,4'-JIDll ,.,
Endoiulftn Sulfite4,4'-D|)T
Endnn Ketone
Aroclor-1016Aroclor-1221Aroclor-1232Aroclor-1242
ftroclor-1254
Arodor-1260
0.05 U0.05 U0.05 U0.05 U0.05 U0.05 U0.05 U0.05 U0.1 U0.1 U0.1 U0.1 U0.1 U0.1 U0.1 U0.5 U0.1 U0.5 UI D
0.5 U0.5 U0.5 U0.5 U0.5 U
1 U1 U
Vs =
Vi = Volui* of eitrict injected lul)Vs = Volute of «ater eitricted (il)Us : Height of saiple eitricted lq|Vt -- Volute of total eitract (ul)
1POO or Ms - Vt =
Fort I
10000 Vi = 3.0
4 1 8 4 3 0 5 7 8
Name ETC/Toxicon
e No
Organics Analysis Data Sheet{Page 4)
Tentatively Identified Compounds
Sample t>
'?/Vk*)03>SQ
CASNumb** Compound N«ITM Fraction
Estimated
1..
5..
7..
O..531
1C,
17.
1ft
UFA denotes no fraction analyzedNCF denotes no compound foundUnk denotes unknownmv denotes probable molecular weight
4 1 8 4 3 0 5 7 9
LABORATORY NAME: ETC/TOXICONLAB SAMPLE ID NO: 4184-9*
SAMPLE MATRIX: WATER
DATA RELEASE AUTHORIZED BY:
ORGANICS ANALYSIS DATA SHEET<PAGE 1>
CASE NO: 4194•C REPORT NO: 4184
CONTRACT NO: Q\ «-fDATE SAMPLE RECEIVED:
,
*9/:9/87
VOLATILE COMPOUNDS
CONCENTRATION: LOUDATE EXTRACTED/PREPARED:DATE ANALYZED: l«/»3/67
CONC/OIL FACTOR: t.
PERCENT MOISTURE: <NOT DECANTED)PH
CAS NUMBEP
74-87-3
74-83-f7S-81-4
7S-»#-3
7S-tt-247-44-1
7S-1S-8
7S-3S-*
7S-3I-3
154-4*-S
47-44-3l»7-»*-2
78-»3-»
71-SS-*
S4-23-Sl*8-«S-4
7S-27-4
1
CHLOROMETHANE
BROMOMETHANE
VINYL CHLORIDE
CHLOROETHANE
METHYLENE CHLORIDE . . . .
ACETONECARBON OISULFIOE
1. 1-DICHLOROETHEME . . . .
1, i-OICHLOROETHANE . . . .
TRAN3-1,2-DZCHLOROETHENE .
CHLOROFORM
1.2-OICHLOROETHANE . . . .
2-BUTANONE1.1. 1-TRICHLOROETHANE . .
CARBON TETRACHLOMIDE . . .
VINYL ACETATE
•RQMOOICHLOROMETHANC . . .
uc14
14
14
14
1
11
1
1
!
i/L
1 U> U> Ui u
> u» u
uuuuuu06uu
> uI U
CAS NUMBER
7«-i7-S
1M41-82-4
7f-*l-4
124-48-1
79-M-S71-43-2
1««41~*1-S
llt-75-8
71 -25 -2
1M-1*-1
S»t-78-4
127-18-*79-34-S
1*6-88-318t-»»-7
14>«-41-4
l»*-42-S
U6/L1,2-DICHLOROPROPANC . . .TRANS-1.J-OICHLOROPROENE .
TRICHLOROETHENEDIBROHOCHLOROMETHANE . . .1.1.2-TRICHLOROETHANE . .
BENZENECIS-t.3-OICHLOROPROPENE .2-CHLOROETHYLVINYLETHER .BROMOFORM
4-METHVL-2-PENTANONE . . .
2-HEXANONETETRACHLOROETHENE . . . .
1-1,2.2-TETRACHLOROETHANC
TOLUENECHLOROBENZENEETHYLBENZENESTYRENE
TOTAL XVLENES
S14
UUuuuuuuuuuuuuuuuu
B - COMPOUND WAS DETECTED IN THE 8C BLANK.U - COMPOUND ANALYZED FOR BUT NOT DETECTED. THE REPORTED
VALUE IS THE MINIMUM ATTAINABLE DETECTION LIMIT FORTHE SAMPLE.
SEE PAGE 1A FOR COMPLETE DEFINITIONS OF THE DATAREPORTING BUALIFIERS.
FOR* Z
4184 30321
Laboratory Name: ETC/Toxicon
Case No: 4184
Sample Nurabtr
Organics Analysis Data Sheet
CAS Number
67-63-0 ,
71-36-3
78-92-2
Compound Name
Isopropyl Alcohol
N-Butyl Alcohol
sec-Butyl Alcohol
Concentrationut/L
300U
200U
200U
U Indicates compound was analyzed for but not 'Vifficil Report the minimntn detection limit for tbe sample with the U(e-t-lOU) based on necesory cotKcxumxrtdihitkn actioo. (This is not necessarily the instnuneat detection limit)The footnote should read: U-Compound was analyzed for bat not detected. Tbe namber U tbe minimum ctainabledetection limh for the «»mpi<»
J i*Atr***f tn xti""** value. This flag 1s used eits«- when *<m««<i a ooncentiation for tentatively identified compoundswhere a 1:1 response U assumed or wben (he mass spectnl data indicated (he prueace of a compound that meets the ideoti-fication criteria but the result is less man the specified detecdoe limb but greater than zero (ej. 1QJ). If limit of detection is10 nt/L and a cooceamrioo of 3 n«/L is calculated, report as 3J.
4 1 8 4 3 0 3 2 2
LdlMV
Case
r.:S a f ~M p I *
Concentration fLow) Medium
Date Ertracted'Prepared
Date Analyzed
Conc/Dil Factor:
Organics Analysis Data Sheet(Page 2}
Semivolatile Compounds
(Circle One) GPC Cleanup OYes ONo
CASNumber
idoif^l
r-
r* (Oeci«ntff<l) . . .
ug/lor ug/Kg(Circle One)
•henol*s(-2-Chloroethyt)Ether
-Chlorophenol. 3-Dichlorobenzene. 4-Oichlorobenzenetetuyt Alcohol
. 2-Dichlorobenzene
-MethyJphenol
i«<2 -chloroisopropyt)Eirter-Methylphenol
1 • Nitroso-Oi -n-PropylaminetexachloroethaneJrtrobenzene
wphorone
!-Nitroph«nolt. 4-Oimethvlpnenolleruoic Acid
» j< • 2 -ChtoroethoxylMethane
1. 4-Dichlorophenol. 2. 4-Tf tchlofooeniene
Naphthalene
l-Chloroartiline
•feKachlorobutadiene
l-Chlofo-3-Metrtytph«no«
l-Methytnaphthalent•«« uchlorocyclopentadtene
2. 4. 6-Trichlorophenol2. 4. 5-Tr«chkxophenol2-Ch(<xon«phthalen«
2-NitroanilineDimethyl Phthalate
Acenaphthyiene
/OIL//)nID uIn*.10klOl/nt-10*.ID*lu*lf)i*lOu10*10kifltL
/Ok-
%tt
in*.10*ip*ID*
lf)tL10*to*.lup-in*.
ftu(fitA
J*MID*
Continuous Liquid - Liquid Extraction OYes
CAS ug/lor ug/KgNumber (Circle One3-32-91-28-50X3-02-7
32-64-921-14-2
606-20-284-66-2
005-72-386-73-7
00-01-6534-52-1
86-30-6
01-55-318-74-1
I7-66-S
85-01-8120-12-7
84-74-2
206-44-0129-00-055-687M-94-1
>6-55-3117-81-7
218-01-9117-84-0205-99-2207-08-9
5032-819339553-703191 24-2
Acenaphtherte!. 4-Oinhrophenol
4-NitropNeno(liberuofuran
:.4-Dinitrotoluene!..6-D«nitroiotLiene
OiethyiphthalateJ /U | t . » . .
Fluorene
4-Nhroaniline4. 6-Oinitro-2-MethY<pr)enolN-Niuosodipt>enYl*iT»ine (1 j
4-Bromopheny(-phenytether
KeucMocobenzenePentacMoropnenoi
PhenamhreneAnthraceneOt-n-8uty»phthaujte
FluoramhenePyreneBatytt>eriiYU>hthalate3. 3'-Oichkxoberu;id<ne
Benzo(( uxnthr ace nebij(2 -EthyJSe cyHPhtha late
ChryseneOi-n-Octyl Phthalate
Benzo(b)Fl uora nthene
BenzotkjFluorantheneBenzo(a)PyTene
lnderto(1 . 2. 3-cd)Pyf eneDibenfla huVnthraceoeB«n;o(g h ip«ryleoe
IQiL
'diA
54uJIOJ*.(flu\f)LLin*(Otf-(Ot*
?4*9fiA
I(Mk*fflu
x>«(OnffilL
I(~)LI/f)bL
(flittun
afrtl
to*.lOt^JfJu.(fami>-iflbL,Ifii 'ink. _Ipls-
in*. _
(11 -Cjn
4 1 8 4 3 0 3 2 5
Analysis Data Sheet(Page 3)Pestuides/PCBs
Cor,cer,tr»tian: [Lou] Hediui (Circle ore)Pate E«tra:ted/Frepared: 29-Sep-87Date A."iiv;ed: 07-Oct-B7Conc/Dil Factor: 1Percent Roistu^decanteiJ) "R
6PC Cleanup Yes [i]-HoSeparatery Funnel Extraction YesContinuous liquid-Liquid Eitractian [x] Yes
CASNuiber
319-84-6319-85-7J19-86-858-89-976-44-8309-00-21024-57-3959-98-B60-57-172-55-972-20-833213-65-972-54-81-31-07-850-29-372-43-553494-70-557-74-98001-35-212674-11-211104-28-211141-16-553469-21-912672-29-6110*7-69-111096-B2-5
Alph»-BHCBeta-WCBelta-IHC£jiia-BHC (Lindint)
Aldrin
Endosulfin I
4I4'-00£
Endosulfin I]4)4'-DDD
4f4--DOTHethoiychlor
Aroclor-1016Uroc lor- 1221flroclor-1232Aroclor-1242Aroclor-1248Arorlor-1254Aroclor-1260
[uq/L] or ug/Kq
0.05 U0.05 U0.05 U0.05 U0.05 U0.05 U0.05 U0.05 U0.1 U0.1 U0.1 U0.1 U0.1 U0.1 U0.1 U0.5 U0.1 U0.5 U
1 U0.5 U0.5 U0.5 U0.5 U0.5 U
1 U1 U
Vi = Voluie of titnct injected (ul)Vs : Volui* of Mter e.tricted (illUs : Height of saiple eitracted (q)Vt -- Voluie of total extract lull
Vs - 1000 or Ms Vt = 10000 Vi = 3.0
Fon 1
4 1 8 4 3 0 3 2 4
L o' a io ' y
••-No
Organics Analysis Data Sheet(Page 4)
Tentatively Identified Compounds
Ei
Sample Number
CASNumber
1
*-
I-
t
S
»
f
*a.
10
•is
>4
S--
1ft
7
.•
19
•0
>1
•?»-
•J
?*
«J«J7.
M
M
10
Compound N«m«
Wo/.
UM*
UlOt.
*
Fraction
^/«r/i£
5f^,t/f4
RT orTSon^^Numbjr/
51563^
E*tim«t*d^Cooc«ntntiofl(ug/yor ug/kg)
15i-l
NFA denotes no fraction analyzedNCF denotes no compound foundInk denotes unknownmw denotes probable molecular weight
4184 30325
_ - S E R
LABORATORY NAME: ETC/TOXICON
LAB SAMPLE ID NO. 4184-188SAMPLE MATRIX: WATERDATA RELEASE AUTHORIZED •'
ORGANICS ANALYSIS DATA SHEET(PAGE 1)
CASE NO: 4184X fiC REPORT NO. 41B4
CONTRACT NO: Q)^DATE SAMPLE RECEIVED:
VOLATILE COMPOUNDS
CONCENTRATION: LOW
DATE EXTRACTED/PREPARED:
DATE ANALYZED: 18/83/87
CONC/OIL FACTOR: 1.
PERCENT MOISTURE: (NOT DECANTED)
PH
CAS NUMiER
74-87-1 CHLOROMCTHANC
74-81-* IROMOHCTHANC
7S-81-4 VINYL CHLORIDE
75-88-3 CHLOROCTHANC
7S-8»-2 METHYLENE CHLORIDE . . .
47-44-1 ACETONC
75-15-8 CARBON OISULFIDE . . . .
7S-35-4 1.1-OICHLOROETHENE . . .
75-35-3 1,1-DICHLOROCTHANC . . .
1S4-48-S TRANS-1,2-DICHLOROETHENE
47-44-1 CHLOROFORM
1*7-84-2 1,2-OICHLOROETHANC . . .
78,-tl-l 2-tUTANQNE
71-55-4 1. I. 1-TRXCHLOROCTHAME .
54-23-5 CARtON TETRACHLORIOE . .
188-85-4 VINYL ACETATE
71-27-4 BROMODICHLOROMETHANE . .
UG
11
11
14
14
S
14
1
1
'
»/L
1 UI U> Ur u> 0
> uuuuuuufOuu
1 U
1 U
CAS NUMBER78-87-S18841-82-47»-8l-4124-48-17»-88-S71-43-218841-81-S118-75-87S-2S-2188-18-1Sfl-78-4127-18-471-34-S188-88-3188-98-7188-41-4188-42-5
UG/L1.2-OICHLOROPROPANC . . .
TRANS-1. 1-OICHLOROPROENE .
TRICHLOROETHENE
DIBROMOCHLOROHETHANE . . .1,1,2-TRICHLOROETHANC . .
BENZENE
CI5-1.3-DICHLOROPROPENE .
2-CHLOROETHYLVINYLETHER .
•ROMOFORN4-METHYL-2-PENTANONE . . .
2-HEXANONC
TETRACHLOROETHENE . . . .1,1.2.2-TETRACHLOROETHANE
TOLUENECHLOROBENZENC
ETHYLBENZENE
STYRENE
TOTAL XYLENES
18
f18
18
S18
UUUuuuuuuuuuuuuuuu
B - COMPOUND WAS DETECTED IN THE 8C BLANK.
U - COMPOUND ANALYZED FOR BUT NOT DETECTED. THE REPORTED
VALUE IS THE MINIMUM ATTAINABLE DETECTION LIMIT FOR
THE SAMPLE.
SEE PACE 1A FOR COMPLETE DEFINITIONS OF THE DATA
REPORTING QUALIFIERS.
FORH I
4 1 8 4 3 0 3 3 5
Labora tory Name: ETC/Toxicon
Case No: 4184
Sample Numt>«r
Organics Analysis Data Sheet
CAS Number
67-63-0
71-36-3
78-92-2
Compound Name
Isopropyl Alcohol
N-Butyl Alcohol
sec-Butyl Alcohol
Concentrationm/L
300U
200U
200U
U TifrtVTt tnmpnpuA was analyzed for but *w* ^"^f'lrt Repot the mini mm detection i""** for the sample with tfae U(e.g. 10U) baaed on necessary coocattmJon/dflution action. CThis is not necessarily the insirument detection limit)The footnote should read: U-Compoand was snalyzed for bat not detected. The number is me minimum attainabledetection Hmit for tbe *<"n«**
J Indicates U estimated Vibe. ™f H«|t ^t Tf^* ^^Iff •*•• »«ri'««*<«e • moontr^lnH for t«itarivriy M«irifWM mmpnnfK<«where a 1:1 response is assumed or when the man speed! data indicated me presence of a compound mat meets me ideial-fcation criteria but merenb bless than me spedfW detection limit bnt ideate than KTO (e.j. 1QJ). Iflimitofdetectioots10 m/L and a concentration of 3 uj/L is calculated, report as 3J.
4 1 8 4 30336
La!, . 'a : . , r, ,- ..
Case No V-.
Organics Analysis Data Sheet
(Page 2)
Semivolatile Compounds
Sample
Concentration (Low) Medium (Circle One)^-^ .rA+A
Date Extracted'Prepared
Date Analyzed
Conc/Dd Factor.
Percent Moisture (Decanted).
GPC Cleanup QYes ONo
Separatory Funnel Extraction QYes
Continuous Liquid - Liquid Extraction QYes
CASNumber
ug/lerug/Kfl CAS
106-95-2111-44-4
95-57-8541-73-1106-46-7
100-51-695-50-195-48-739638-32-9106-44-5621-64-767-72-1
98-95-378-59-188-75-5105-67-965-85-0
111-91-1120-83-2120-82-191-20-3106-47-887-68-3S9-SO-791-S7-677-47-4
88-06-295-95-4
91-58-7 j88 74.4
131-11-320896-899-09 2
Phenolbis< - 2 -Cnioroeth yOEtrter
2-CMorophenol1 . 3-Oich(oroberuene
1 . 4-OicMorobenzentBeruyl Alcohol1 . 2-Oichtorobtnzene2-M«thy10henol
bis(2-chloroisopropY<)Ether4-MethytphtnolN-Nitroso-Di-n-PropyUmirw
HcKachloroethanc
NitrobenzeneIsophoront2-Nrtrophtnol2. 4-Oimethy(phenolBenzok Acidbis< - 2 -Ch(oro«tnoxYlM«th«ne
2. 4-Oichlorophenol1. 2. 4-TrkhloroberueneN«phtK»krt«
4-O>loro«r«ilineHe ucniorobut»diene4-Chloro-3-Methy1p'*"0<2-M«tny<n«phthaltnc
H«uchlorocyctopent>diene2. 4. 6 Trichlorophenol2. 4. S-Trichkxopnenol2 - CMorooi (fvi l«ne2-NiUoanilineDimethyl Ptithalate
Acenaphthylene3 Niuoarnlirv*
/Ou.//)k10 u
tOt*.10ulot*.(rit-/OM.
IQuilf)ulOuIDu/^KifiuIO(>-
^ttinu.10/Ou.ID*m±in &10*Ito.IfofOa
ftu\CitA
&nlOlA.fOlA
SttA.
Number (Circle One83-32-951-28-5100-02-7132-64-9121-14-2606-20-284-66-27005-77-316-73-7100-01-8534-52-116-30-6101-55-3118-74-1
17-86-585-01 -8120-12-7
84-74-2206-44-0129-00-0(5-68-711-94-1
>6-55-3117-81-7
218-01-9117-84-0205-99-2207-08-9MX 32 -819339-553-70-3191-24-2
Acenaphthene:. 4-Dinitrophenol
4-NrtrophenolJibennfuran
!. 4-Dinhrotoluene2, 4-D<nctroTofueneDJethvlprrtfialate
Fluor ene4-NhroamTirw
4. 6-OMtro-2-M«thYtpheno<
N-Nttro«o*phenvUmine (1 )JO h 4 IS* 4**tt* ~ *** OT«OP"* cvyi -pn* n ywv\c*
PtnuchtorophtnolPhencmhr«n.i
^nirvwcwncOi-n-ButytphthalateFluonnthenePyrene8ury(benry(phtna(ate3. 3'-Ochloroberuidine
8«Mo(«)Ajntv«cenetw(2 -Ethytrtexy()Prnhataie
Chryien*0<-n-Octyl PruhaUte8«nn(b)FluorantheneBenttXk |FI uorantnene
Beozo(«)PyTenelndeno(1.2. 3-cd)PyreneDiberuta h)Antnracene
8en/o(g. h. iJPerylene
IVk£JtA
50 U
10k[Ob.lf)u.(hy.(Otf-(0^
to*SSU
10kftOj*fflu.
&*QL,
'faIQitIfiu
IP"WuJou
/OlA.
lf)U
lOi*.lOu.fay-
it)itstnu. _
In*
4 1 5 4
Or;ar, i :« A n a l y s i s D a t a Sheet
iFage 3)
Pes t i c ides /PCBs
CDrcentratiDn: [Lcm] Kediui ;[;r:i; or,?'
[a'.e E . t ' ac ' .e^ r reoared : :s-le:-z~
ji'.s A - a i , : ? d : O ' -Oc t -B?
C o n c ' D i i F a c t o r : ;
Fer;ent Hcusture;de:intei!i NR
6PC Cleanup Y»s [«]-Ho
Separatory Funnel [inaction Yes
Continuous Liquid-Liquid Eitract ion [i] Yes
CA5Nulter
[uq/L] or ug/Kg
I19-B4-6 Alphi-BHC ........................ 0.05 U
319-B5-7 Beta-BHC ........................ 0.05 U
Ii9-Bi-8 DelU-BHC ........................ 0.05 U
58-69-9 Gana-BHC (Lindane) ............. 0.05 U
76-44-8 Heptachlor ...................... 0.05 U
109-00-2 Aldrin .......................... 0.05 U
1C24-57-3 Heptachlor Eponde ............... 0.05 U
959-98-8 Endosulfan I .................... . 0.05 U
60-57-1 Dieldrin ........................ 0.1 U
72-55-9 4,4'-DOE ........................ 0.1 U
72-20-8 Endrin ........................ 0.1 U
33211-65-9 Endosulfui II ................... 0.1 U
72-54-B 4,4'-DDD ........................ 0.1 U
1-31-07-B Endosultan Sulfate ............... 0.1 U5C-29-3 4 ,4 ' -DDT ........................ 0.1 U
72-43-5 Nethoxychlor .................... 0.5 U
53494-70-5 Endrin Ketone ................... 0.1 U57-74-9 Chlordant ....................... 0.5 U
8001-35-2 Touphene ....................... 1 U
12674-11-2 ftroclor-1016 .................... 0.5 U
11104-2B-2 ftroclor-1221 .................... 0.5 U
11141-16-5 Arodor-1232 .................... 0.5 U
53469-21-9 Aroclor-1242 .................... 0.5 U
12672-29-t Aroclor-1248 .................... 0.5 U
KO'T-69-1 Aroclor-1254 .................... 1 U
11096-82-5 f t r c c l o r - 1 2 6 0 . . . . . . . . . . . . . . . . . . . . 1 U
Vi = Volute of eitratt injected lul)Vs ; Voluie of Mter extracted (•!)Ms - Height of saiple eitracted Ig)Vt = Volute of total eitract (ul)
Vs • 1000 or Vt 10000 Vi s 3.0
Fori I
4 1 8 4 3 0 3 3 8
La
«•- No
Organics Analysis Data Sheet(Page 4)
Sample Numf>«>r
Tentatively Identified Compounds
CASNumber Compound N«m« Fraction
RT ( E*tim«t«dc«<ur«tionpf ug/kg)
2.
10..
51 fo n
16..
»..
3 .24..
5..
27..I
|».'TO.
NFA denotes no fraction analyzedNCF denotes no compound found;nk denotes unknownmw denotes probable molecular weight
4 1 8 4 30339
LABORATORY NAME: ETC/TOXICON
LAB SAMPLE ID NO. 4184-113SAMPLE MATRIX: WATER
DATA RELEASE AUTHORIZED BY
ORGANICS ANALYSIS DATA SHEET(PAGE 1>
CASE NO: 4184
8C REPORT NO. 4184CONTRACT NO: O l4^
DATE SAMPLE RECEIVED: 89/29/87
VOLATILE COMPOUNDS
SAMPLE NUMBERMOLGW93701
3-s'/
CONCENTRATION: LOU
DATE EXTRACTED/PREPARED:
DATE ANALYZCO: 18/85/87
CONC/OIL FACTOR: 1.
PERCENT MOISTURE. (NOT DECANTED)
PH
CAS NURSE*
74-87-3 CHLOROMETHANE
74-83-» BROMOHETHANE
75-81-* VJNYL CHLORIDE
75-88-3 CHLOROETHANE
75-89-2 HETHYLENC CHLORIDE . . .
47-44-1 ACETONE75-15-8 CARBON DISULFIOE . . . .
7S-3S-4 1.1-DICHLOROCTHENE . . .75-35-3 1-1-OICHLOROETHANE . . .
156-68-5 TRANS-1.2-OICHLOROETHENE47-44-3 CHLOROFORM
187-84-2 1.2-DICHLOROETHANC . . .78-93-3 2-BUTANONE
71-SS-A 1,1.1-TRICHLOROETHANE .56-23-5 CARBON TETRACHLORIDE . .188-85-4 VINYL ACETATE75-27-4 BROMODICHLOROHETHANE . .
Ufi
i«1114
11
1
3<
1
1
>/L
» U
• U
> U
> U
L J
>
U
U
U
U
U
U
U
U
U
» U
1 U
CAS NUMBER
7S-87-S
18861-82-*
79-81-4
124-48-1
71-88-S
71-43-218861-81-5
118-75-8
75-25-2
181-18-1
Stl-78-6
127-18-4
7f-34-S
188-88-3
188-98-7
188-41-4
188-42-5
UG/L1,2-DICHLOROPROPANE . . .
TRANS-1. 1-DICHLOROPROENE .TRICHLOROETHENEOIBROMOCHLOROftETHAME . . .
1.1,2-TRICHLOROETHANE . .
BENZENECIS-l,3-DICHLOROPROPENE .
2-CHLOROETHYLVINVLETHER .IROMOFORM
4-NETHYL-2-PENTANONE . . .
2-HEXANONETETRACMLOROETHENE . . . .
1.1,2.2-TETRACHLOROETHANE
TOLUENE
CHLOROBENZENEETHYLBENZENE
STYRENETOTAL XYLENES
1851818S185§55S
UUUUUUUUUUUUUUUUUU
J - REPORTED VALUE IS LESS THAN THE DETECTION LIMIT.
U - COMPOUND ANALYZED FOR BUT NOT DETECTED. THE REPORTEDVALUE IS THE MINIMUM ATTAINABLE DETECTION LIMIT FORTHE SAMPLE.
SEE PAGE 1A FOR COMPLETE DEFINITIONS OF THE DATA
REPORTING 8UALIFIERS.FORM I
30539
Labora tory Name: ETC/Toxicon
Case No: 4184
Sample N
Organics Analysis Data Sheet
CAS Number
67-63-0
71-36-3
78-92-2
Compound Name
Isopropyl Alcohol
N-Butyl Alcohol
sec-Butyl Alcohol
ConcentrationHf/L
300U
200U
200U
U in^irat** compound was analyzed for but not detected. Report the minimum detection limit for the sample with the U(e.g. 10U) based on necessary concenntion/dihilioD action. (This is not necessarily the instrument detection limit)The footnote sbould read: U-Gompound was analyzed for but not detected. Tbe number is the minimum attamabledetection limit for the sample.
J itrfintr* an *~pima»H value. This flag is used either when *frim«fing a ooncentnboo for tentatively Jdeatified compoundswhere a 1:1 response is ««pi*«««< or Men the mass spectral data <ndw-a*^ (he presence of a compound that meets the identi-ffcation criteria but tbc result is tess than the specified detection limit but greater than zero (e.|. 101). If limit of detection is10 |igft. and a concentration of 3 iig/L is calculated, report as JJ.
4 1 8 4 3 0 5 9 0
alxr <•<:."
Jase No i .J
Organics Analysis Data Sheet(Page 2)
Semivolatile Compounds
S« •••
Joncentration: fLovvj Medium
Oate Extracted'Prepared *' ^ -
Date Analyzed f.
(Circle One)
Cone/Oil Factor:
'ercent Moisture (Decanted).
GPC Cleanup OYes QNo
Separaiory Funnel Extraction QYes
Continuous Liquid - Liquid Extraction DYes
CASNumber
ug/lorug/Kg CAS ug/lorug/Kg(Circle One) Number (Circle One
/(CV
/0*fV?i~70&10
/AM.
Atti/<%/ty/0«/tfk.//7fc)$:Wtt//7^*/?««•/&kID*Ift*IftfiIfa.10*10*-iO\A.
S~614[OlA
5tq10*ICltA
3-32-91-28-500-02-7
32-64-921-14-2
606-20-284-66-2
005-72-36-73-7
00-01-634-52-1
86-30-6
01-55-318-74-1
87-86-585-01-8
20-12-784-74-2206-44-0129-00-0J5-68791-94-1
.6-55-3117-81-7
218-01-9117-64-020599-2207X»-9»32 8
193 395
J3-70-3191-24-2
Acenaphthvne1. 4-OinKrophenol
4-Nitrophenot>iberuofu'an
!.4-Oinhrotoluene! , .6 -OinKrotoluene
Oiethyiphthalate> -Chlorophenyl-phenylether
Fluorene4-Nitroaninne4. 6-Oinitr9-2-MettTy(phenol
N-NitrocodiphenyUmine (1 )
4-BromopSenvf-phenv<ether
HeuchlorooenzentPentachlorophenolPrteramhreneAmhr»c*ne04-n-ButyIphttxalate
Fluor* nthenePyreneButvtt>«<VYV>tK«iate3. 3'-OtcMorobenzidine3eozo(i)Amtv«cen«
txX2 -Ethy1heKyl)PriTtvaliwChryseneOi-n-Octyl PttttxalateBenzo(b)Fluoranthene
Benzofk)Fiuorantt>eneBerucXatPyrene
IrxJenotV 2. 3-cd)PyeneOibcnili h)Anthracer>e
Benio(g. h. ()P«rY««r>e
IQiiSfa54 u
I/9K(hit.lf)u.(i)u(f)lt-
fOt*ft A
&<4IUlLhi*
(OutJ*f
JHulf>k
iQuf)u
'Id'1]0u.
JtutVu.jf)(jL
lUljL
\0u.(f}tfid'*']T)i*s(f?AtlUl*i n^ __
f O' m I
4 1 8 4 3 0 5 9 17/85
H e .
Concen t r a t io r : [ Lc» j Hediui i C i r r l e aD a t e Ex t . -ac te i ' f ' epare i ! : :?-Sep-B'"a te H?a ;» :ed : 0 7 - G c t - E "Canc/d i F a c t o r : 1Percen t Hc is tare lde:anted i HP
BP: Cleanup Yes [iHoSeparately Fan-el Eitract:;r. Yes[:•'.:•..c.s L iuu id -L iQu iS [ - . ; ract ;o- [x ] Yes
CAS [u5 /L ] o- ug /KcNuliier
319-B4-6 Alphi-BHC O.C5 U
319-85-7 Beti-BHC 0.05 U
319-86-8 DelU-BHC 0.05 U
58-89-9 GaiM-BHC (Lindine) 0.05 U
76-44-8 Heptachlor 0.05 U
309-00-2 ftldnn 0.05 U
1024-57-3 Heptachlor Epciide 0.05 U959-9B-B Endosulfan I . 0.05 U60-57-1 Dieldrin 0.1 U72-55-9 4.4'-OD€ 0.1 U72-20-B Endrin 0.1 U33213-65-9 Endosulfan II 0.1 U72-54-B 4,4'-DDD 0.1 U1-31-07-8 Endosulfan Sulfate 0.1 U50-29-3 4,4'-DDT 0.1 U72-43-5 Kethoxychlor 0.5 U53494-70-5 Endrin Ketone 0.1 U57-74-9 Chlordane 0.5 UB001-35-2 Toiaphene 1U12674-11-2 Arodor-1016 0.5 U11104-28-2 Aroclor-1221 0.5 U11141-16-5 Aroclor-1232 0.5 U53469-21-9 Aroclor-1242 0.5 U12672-29-6 Aroclor-1248 0.5 U11097-69-1 Aroclor-i:54 1 U
11096-82-5 Aroclor-1260 1 U
Vi = Voluie of eitract in jected lullVs - Volute of viter extracted (•!)Us - Height of saiple eitricted (g)Vt - Volute of total ex t rac t lull
Vs = 1000 or Us = Vt = 10000 Vi = 3.0
Fori
4 1 8 4 3 0 5 9 2
abo ra io ry N a m e f c - T C / T u x i c o n
e No
Organics Analysis Data Sheet(Page 4)
Tentatively Identified Compounds
Sample
Number Compound Nam*C(tim«t«d**&*ntr«tioo
(ug/rr ug/kg)
n
l«DiO K. 531 15
603 *5uioic
/OZT-
1C
ms/^nil- h/4? 11
la
ss
,».129.
NFA denotes no fraction analyzedNCF denotes no compound foundUnk denotes unknownmw denotes probable molecular weight
4 1 8 4 3 0 5 9 3
' . i M - - fc E c
:•«.? 38*:
LABORATORY NAME: ETC/TOXICON
LAB SAMPLE 10 NO: 4184-1*3
SAMPLE MATRIX: WATERDATA RELEASE AUTHORIZED BY:
ORGANICS ANALYSIS DATA SHEET
<PA&E 1)
CASE NO: «1B4
8C REPORT NO: 41B4
CONTRACT NO: 0/4*1DATE SAMPLE RECEIVED: »»/29/87
VOLATILE COMPOUNDS
CONCENTRATION: LOW
DATE EXTRACTED/PREPARED:
DATE ANALYZED: l*/«3/87
CONC/DIL FACTOR: 1.
PERCENT MOISTURE: (NOT DECANTED)
PH
CAS NUMBER
74-87-374-83-»7S-81-47S-**-3
7S-*»-247-44-1
7S-1S-*7S-3S-4
7S-3S-3
154-49-S47-44-3
l*7-*4-278-»3-371-SS-4
S4-23-Sl*8-*S-4
78 -27-4
UC/L CAS NUMBERCHLOROMETHANE !• U 78-87-S
8ROHOMETHANE 1* U l**41-*2-4
VINYL CHLORIDE !• U 7f-«l-4CHLOROETHANE !• U 124-48-1METHYL ENE CHLORIDE . . . . 2 J 7»-**-S
ACETONE
CARBON1* U 71-43-2
DISULFIOE
1. 1-DICHLOROETHENE . . . .
1, 1-OICHLOROETHANE . . . .TRANf-1. 2-OXCHLOROETHENE .CHLOROFORM
1.2-OICHLOROETHANE . . . .
2-BUTANOME 14
U 1**41-*1-S
U ll*-7S-8U 7S-2S-2U 1*8-1*-1
U i«l-78-4
U 127-18-4
» jKl 7»-34-S1. 1, 1-TRICHLOROETHANE . . S U 1*8-88-3
CARBON TETRACHLORIDE ... S U l*8-9*-7
VINYL ACETATE 1* U 1M-41-4
BROHODICHLOROMETHAME ... i U 1M-42-S
UO/L
flifri
1,2-OICHLOROPROPANE . . .
TRANS-1, 3-OICHLOROPROENE .TRICHLOROETHENCDIBROMOCHLOROMETHANE . . .1.1.2-TRICHLOROETHANE . .
BENZENECIS-1.3-OICHLOROPROPENE .2-CHLOROETHYLVINYLETHCR .
BROMOFOM4-METHYL-2-PEHTANONC . . .
2-HEXANONETETRACHLOROCTHENE . . . .
1.1.2.2-TETRACHLOROETHANE
TOLUENE
CHLOROBENZENE
ETHYLBENZENE
STYREMETOTAL XVLENES
1*
U
U
U
U
U
U
U
U
U
UU
U
UU
U
U
U
U
8 - COMPOUND WAS DETECTED IN THE K BLANK.J - REPORTED VALUE IS LESS THAN THE DETECTION LIMIT.U - COMPOUND ANALYZED FOR BUT NOT DETECTED. THE REPORTED
VALUE IS THE MINIMUM ATTAINABLE DETECTION LIMIT FORTHE SAMPLE.
SEE PAGE 1A FOR COMPLETE DEFINITIONS OF THE DATAREPORTING 8UALIFIERS.
FORM I
4 1 8 4 3 0 3 8 9
Labora tory Name: ETC/Toxicon
Case No: 4184
Samplf N u m b e r
Organics Analysis Data Sheet
CAS Number
67-63-0
71-36-3
78-92-2
Compound Name
Isopropjl Alcohol
N-Butyl Alcohol
sec-Butyl Alcohol
ConcentrationILK/L
300U
200U
200U
U lnrfir-«<>^ compound was analyzed for tat not detected. Repot the minimum detection limit for the sample with die U(e.j. 10U) based on necessary concentration/dilution action. (Thisitnot necessarily the iimruinent detection limit)The footnote ibould read: U-Compound w« analyzed for but not detected. The amber U the minimum aoinibledetectioa ^mit for the sample.
j Indicates an estimated vitoe. Thk fig to uaed either when qrimariat' muxuuaioo for tenativdy identified compoundswhere a 1:1 response is assumed or when the mass Mfi U il 4f*\ iM^**^ the presence of a compound that meets the identi-ficatkn criteria bat the result is less than *e tpecifM dettctkn Umb tat greater than zoo (e . 101). If limuof detectioois10 \itfL and a concentration of 3 m/L U catailansd. report a§ U.
4 1 8 4 30390
Case f. :
Organics Analysis Data Sheet(Page 2)
Sa-MpL. •
rf.O _<:-. .
Concentration
Date Ertracted'Prepared
Date Analyzed
Conc/Dil Factor
Medium
Semivolatite Compounds
(Circle One) GPC Cleanup QYes ONo
CASNumber
i ° / t If!, ' ' 1r* (O»c^nt<»*l) .
ug/lorug/Kg(Circle One)
nenol
i$<-2-Chloroethyl)£ther-Cnlorophenol. 3-Dicnlorobentene. 4-Oicnlorobenteneenzyl Alcohol, 2-Dichlorobentene-Methytphenot««(2-chlorotsopropy1|E(her•Metfiytphenol-Nitfoso-Oi-n-PropyUminelexachloroethant(itrotenzenecopnoron*-Nitrophenol. 4-Dimethylph*nolleruoic Acid•2-CMofoetnocylMetnene. 4-Oichloropnenol. 2. 4-Trichloroberuene<aphm*(«ae-Oil&roeniline
<e (Achlorobutftdienel-CMoro-3-Melhylprtenol-Memylnaphthalene
». 4. 6-TricMorophenol!. 4. 5-TricMoroprtenol!-Chloronaphthalen«!-NitroenilineJ.mcthyi Ptitnadie»^en»phtriy1«r%e
/Ok./flk.10 uIn^lOu)Ck./ni~If)*.IfiuIQUL
lOulOu1C*.I HitID*.
527Uinu,10*10*ID*Ifiiflf)H.lOu./Ul/~\ur-/On.
$i(AIfilA
50t\10*IfilA
Continuous Liquid • Liquid Extraction QYes
CAS ug/lorug/KgNumber (Crcle One3-32-91-28-500-02 -732-64-921-14-2
606-20-284-66-27005-72-386-73-700-01-6
534-52-186-30-601-55-318-74-1
87-86-515-01 -8120-12-7M-74-2206-44-0129-00-0)5-687J1-94-1.6-55-3117-81-7218-01-9117-84-0205-99-2207-08-9>032-8193 39553-70-3191-24-2
Acenaphtftene2. 4-Dinrtroprienol4-NrtropNenol>ibenzo(uran
:. 4.0inrtroto(uene2. 6-OinhrotoloeneDiethylphthalftte
Fluor ene4-NrtroaniliM4. 6-Otohro-2-Wethv<pn«nolN-Nitrosodipneny(amine (1)4-Bromophenyf-phenvtetrterHeuchlorobenzertePentMhlorophenolPhenanthrentAnthnoeneOi-n-6utv<prithalateFluomnthenePyreneBut/ft* ruy(pritn«t«t«3. 3'-O<hioroberu«dineBeoiota lAnthracenetx*2 -Ethy<t>eKy<)PhttulateOvYieneDi-n-OctyH PhtnalateBemo(b|Fluor*nthene8«fUo(k|Fluorantt>ene8enzo(a)PvTeneIndenotV 2. 3-cdWerKOibeoflj. h)Anthr«cen«Bento(g. h. iJPeryleo*
I0uS"dt<Wu
in*(Huin*IUUL(f)t?.
(0(fUK
senjUuto*(flu.
SHifOn(fiu
10"fhu[Q\L
Wuyu
to*./n^'if (fi-lp*lOif-ffjf^/(/i*-^in*.
In* ..
rxji be tep«r«i«d ff
( o< 4 1 8 4 3 0 3 9 17 85
L d Z Z r a ' 7 ' t
Cdse N-:inc.
analysis Cat* Sheet(Page 3)Peshcides/PCBs
Concentration: [Lo»] tediut (Circle one)Date E«tracteJ/?repa'BS: 29-5ep-B7Date Anal.red: 07-Dct-S7Conc'Dil Factor: 1Percent rlcusture'decanted! HR
6PC Cleanup Yes [.HoSeparatory Funnel Extraction YesContinuous Liquid-Liquid Extraction [i] Yes
CAS [ug/L] or ug/KgNufber
319-B4-4 Alphi-BHC 0.05 U319-85-7 Beti-BHC 0.05 U319-B6-B D*Hi-BHC 0.05 U5B-B9-9 Sa»ia-BHC (Lmdane) 0.05 U74-44-B Heptachlor 0.05 U309-00-2 Aldnn 0.05 U1024-57-3 Htptachlor Epoiide . 0.05 U959-98-6 Endosulfan 1 0.05 U40-57-1 Dieldrin 0.1 U72-55-9 4,4'-OM 0.1 U72-20-8 Endrin 0.1 U33213-65-9 Endosulfw II 0.1 U72-54-B 4,4'-BDD 0.1 U1-31-07-B Endosulfan Sulfite 0.1 U50-29-3 4,4'-ODT 0.1 U72-43-5 Htthoxychlor 0.5 U53494-70-5 Endrin Ketone 0.1 U57-74-9 CMord»n« 0.5 U8001-35-2 Toiapheni IU12674-11-2 Aroclor-1016 0.5 U11104-28-2 Aroclor-1221 0.5 U11141-16-5 Aroclor-1232 0.5 U53469-21-9 Aroclor-1242 0.5 U12672-29-6 ftroclor-1248 0.5 U11097-69-1 Arodor-1254 1 U11096-82-5 Aroclor-1260 IU
Vi = Volute of titract injected (ul)Vs * Volute of water eitracted (•!)Us - Height of saiple extracted (9)Vt -- Volute of total eitract (ul)
Vs = 1000 or Us ; Vt - 10000 Vi - 3.0
Fort I
4 1 8 4 3 0 3 9 2
_abo'aiofy Name
e No .
LTC/To.\ i c
Organics Analysis Data Sheet(Page 4)
Tentatively Identified Compounds
Sample Ncxnl>er
CASCompound NMTM Fraction
[ug/rer ug/kg)
1..
3..
6..
7..
1O..
.*..
37
16..
16..
17..
16..
19..
21..
as
29.
JO.
NFA denotes no fraction analyzedNCF denotes no compound foundUnk denotes unknownmv denotes probable molecular weight
4 1 8 4 3 0 3 9 3
LABORATORY NAME: CTC/TOXICON
LAI SAMPLE ID NO: 4184-111SAMPLE MATRIX: WATER
CATA RELEASE AUTHORIZED IV
OftCANICS ANALYSIS OATA SHEET(PACE 1)
CASE NO. 4184BC REPORT NO: 4184
CONTRACT NO: 0) C\DATE SAMPLE RECEIVED
VOLATILE COMPOUNDS
99/29/87
CONCENTRATION: LOUDATE EXTRACTED/PREPARED:DATE ANALYZED: 14/49/87CONC/DIL FACTOR: 1.PERCENT MOISTURE: <NOT DECANTED)
PH
CAS NUtltER
74-87-1 CHLOROMCTHAMC
74-81-9 BROHOHETHANE
7S-81-4 VINYL CHLORIDE
75-88-3 CHLOROETHANE
75-89-2 METHYLENE CHLORIDE . . .
47-44-1 ACETONE
75-15-8 CARBON OISULFIOE . . . .
75-35-4 1.1-OICHLOROETHENE . . .
75-35-3 1,1-DICHLOROETHAMC . . .154-48-5 TRAN5-1.2-OICHLOROETHENC47-44-3 CHLOROFORM
187-84-2 1.2-OICHLOROETHANC . . .7t-93-3 2-iUTANOHt71-SI-4 1.1.1-TRICMLOROETHANE .
54-23-5 CARBON TETRACHLORIOC . .188-85-4 VINYL ACETATE
75-27-4 BROMODICHLOROHETHANC . .
»/LUUUUUUUUUUUUUUUUU
CAS NUMBER78-87-B1884 1-82-4
79-81-4124-48-1
79-88-571-43-218841-81-5118-75-8
75-25-2188-18-1
591-78-4127-18-4
79-34-5188-88-3188-98-7188-41-4
188-42-5
UO/L1.2-DICHLOROPROPANC . . .TRANS-1.3-OICNLOROPROENE .TRICHLOROETHENEDIIROMOCHLOROHETHANC . . .
1.1,2-TRICHLOROETHANE . .BENZENECIS-1.3-OICHLOROPROPENE .
2-CHLOROETHYLVINYLETHER .BROMOFORH4-METHYL-2-PENTANONC . . .
2-HEXANONE
TETRACHLOROETHENE . . . .
1.1.2,2-TETRACHLOROETHANETOLUENECHLOROBENZENE
ETHYLBENZENESTYRENE
TOTAL XYLENES
1*
UUUUUUUUUUUUUUUUUU
U - COMPOUND ANALYZED FOR BUT NOT DETECTED. THE REPORTED
VALUE IS THE MINIMUM ATTAINABLE DETECTION LIMIT FORTHE SAMPLE.
SEE PAGE 1A FOR COMPLETE DEFINITIONS OF THE DATAREPORTING BUALIFIERS.
FORM I
4 1 8 4 305 62
laboratory Name: ETC/Toxicon
Tase No: 4184
Sample Number
Organics Analysis Data Sheet
CAS Number
67-63-0
71-36-3
78-92-2
Compound Name
Isopropjl Alcohol
N-Butyl Alcohol
sec-Butyl Alcohol
ConcentrationRt/L
300U
200U
200U
U Indicate pntnpnnnj w^ •tmljmM fnr Hit TV* AetrftrA Pepnrt thg minimnin (toegtjnn limit for the tample wilh the U(e,j. 10U) bond on necessary concamdoa/dHutioo actioa. (This U not necessarily the instrument detection limit)The footnote should read: U-Compoond was analyzed for but not detected. The number is the minimum attainabledetection i>mit for the sample.Tndir^»t «n ,-aim,*** valiy. Thq fl«g lt njrj fitter mAtm f^jntiri^ • mnrrntntvm fnr tentatively MenrififtH enmpninxl*
where • 1:1 response U assumed or when the mass spectral data indicated me presence of a compound that meets the identi-fcattan criteria but the result is less than the specified detection limit but greater than zero (e . 10J). Iflimitofdetectioais10 \i%L and a coocentration of 3 U£/L is calculated, report as 3J.
4 1 8 4 3 0 5 6 3
LABORATORY NAME ETC/TOXICOH
CASE NO *18»NUMBER
ORGANIC* ANALYSIS DATA SHEET
<PAGE 2>
SEHIVOLATILE COMPOUNDS
CONCENTRATION: LOUDATE EXTRACTED/PREPARED: lt/17/87
DATE ANALYZED: lt/28/B7CONC/DIL FACTOR: 1.PERCENT hOISTURE: (DECANTED)
GPC CLEANUP YES X NO
SEPARATORY FUNNEL EXTRACTION YESCONTINUOUS LiaUID-LiaUID EXTRACTION YES
CAS NUMBERltB-»*-2 PHENOL111-44-4 BIS<2-CHLOROETHYL>ETHER .tS-§7-8 2-CHLOROPHENOL5*1-73-1 1,3-OICHLOROBENZENE . . .
186-46-7 1.4-OICHLOROBENZENC . . .
ltt-Sl-6 BENZYL ALCOHOL»S-St-l 1.2-OXCHLOROBENZENE . . .
95-48-7 2-HETHYLPHENOL39638-32-9 BI*<2-CHLOROISOPROPYL>ETHER
lt6-44-S 4-HETHYLPHEMOL621-64-7 W-NITROSO-D1-H-PROPYLAHINE47-72-1 HEXACHLOROETMAME98-TS-J MITROBEMZCME
78-S9-1 ISOPHORONC88-75-1 2-NITROPHCNOLltS-67-9 2.4-OIHETHYLPHENOL ....
65-8S-t iENZOIC ACID111-91-1 BIS<2-CHLOROETHOXY>HETHAMt
12t-B3-2 2.4-DICHLOROPHENOL . . . .
128-82-1 1.2. 4-TRICHLORO»EHZE*e . .91-2t-l NAPHTHALENEl«A-47-t 4-CHLOROANILINE
87-68-3 HEXACHLOROIUTAOIEHE . . .S»-S»-7 4-CHLORO-3-NETMYLPHENOL .
11-S7-6 2-METHYLNAPHTHALENE . . .77-47-4 HEXACHLOROCYCLOPENTAOIENE88-«6-2 2.4.A-TRICHLOROPHENOL .' .
»S-»S-4 2,4.S-TRICHUOROFHENOL . .
f1-58-7 2-CHLORONAPHTHALENE . . .88-74-4 2-NITROAMILINE
131-11-3 OIHETHVU PHTHALATE . . . .
288-96-8 ACENAPHTHVLENC»*-«»-2 J-NITROANILINE
UG/L CAS NUMBER UG/L
it U 83-32-9 ACENAPHTHENE It U
it U 51-28-5 2.4-DINITROPHENOL . . . . St Uit U ltt-t2-7 4-NITROPHENOL St UIt U 132-64-9 OIBENZOFURAM It U
It U 121-14-2 2.4-OINITROTOLUENE . . . . It UIt U 6t6-2t-2 2.6-OINITROTOLUENE . . . . It U
it U 84-66-2 OIETHYLPHTHALATE It Uit U 7ttS-72-3 4-CHLOROPHENYL-PHENYLETHER It UIt U 86-73-7 FLUORENE It Uit U ltt-it-6 4-NITROANILINE 5t U
it U 534-52-1 4.6-DIN1TRO-2-NETHYLPHENOL St Uit U 86-3t-6 N-NITROSOOIPHCNYLAHINE <1> It Uit U ltl-SS-3 4-BROHOPHENYL-PHENYi.ETHER it U
it U 118-74-1 HEXACHLOROBENZENE . . . . It Uit U 87-86-5 PENTACHLOROPHENOL . . . . St U
it U 8S-tl-8 PHENANTHREME It USt U 12t-12-7 ANTHRACENE it Uit U 84-74-2 OI-N-BUTYLPHTHALATE ... It U
it U 2t6-44-t FLUORANTHCNC it UIt U 129-tt-t PYRENE It Uit U 8S-68-7 8UTYLBENZYLPHTHALATE ... It Uit U 91-94-1 3.3'-OICHLOROtENZIOINE . . 2t U
It U 56-55-3 BENZO(A)ANTHRACENE . . . . It Uit U 117-81-7 BIS(2-ETHYLHEXYL>PHTHALATE It UIt U 21B-tl-9 CHRYSENE It UIt U 117-8»-t OI-N-OCTYL PHTHALATE . . It UIt U 2tS~99-2 BENZO(B)FLUCRANTHENE . . It USt U 2t7-t8-9 BENZO<K>FLUORANTHENE ... It Uit U St-32-8 8ENZO(A)PYRENE It U
St U 193-39-5 INOENOd. 2. 3-CO) PYRENE . It Uit U S3-7t-3 OIBENZ(A,H)ANTHRACENE . . It U
It U 191-24-2 BENZO<O.H. DPERYLENE ... It U
St U
<1> - CANNOT BE SEPARATED FROM DIPHENYLAHINEFORM I
30564
3)PpsticidM/PCBs
[1.3*] Sediut (Circle one! 6PC Cleanup Y« [*]-No
''Prepared: T'-Sep-E? Separa'.ory Fjrre! Extraction IPS
•'J-t'E' Cr'ii.-jDus L;5t;d-Liquj(! Ext'ac'.ior [s] >'es
•: 1•e!i?:art;j) Nfi
CAS [ag/L] or uoHuiber
319-84-4 Alpha-BHC 0.05 U
319-85-7 B*tj-BHC 0.05 U
319-Bi-B Dflta-BHC 0.05 U
58-89-9 Sana-BHC (Lindant) 0.05 U
74-M-B Htptachlor 0.05 U
309-00-2 Aldrin 0.05 U
1024-57-3 HepticMor Epo«ide 0.05 U959-9B-B Endosulfan I 0.05 U40-57-1 Oitldrin 0.1 U
72-55-9 M'-DDE «.l U72-20-8 Endrin 0.1 U
33213-45-9 Endosulfifl H 0.1 U72-54-8 4,4'-ODD 0.1 U1-31-07-8 Endosulfin Sulfitt 0.1 U50-29-3 4,4'-DDT 0.1 U72-43-5 Bethoiychlor 0.5 U
53494-70-5 Endrin Kftmc 0.1 U57-74-9 Chlordan* 0.5 UB001-35-2 Toxaphmt 1U12474-11-2 Aroclor-1014 0.51)
11104-28-2 Aroclor-1221 0.5 U11141-14-5 Aroclor-1232 0.5 U53469-21-9 Aroctor-1242 0.5 U
12672-29-4 Aroclor-1248 0.5 U11C97-49-1 ftroclor-1254 1 U
r-S Aroclor-1240 1U
Vi : Vcluie of ritrict in;rcteil lul)Vs = Voluii of Mter tttricttd (•!)Ms - Nrjght of saipl? eitractfd (9)Vt ^ Volute of total extract (ul)
Vs - 1000 or Us = Vt - 10000 Vi - 3.0
Fori I
4 1 8 4 3 0 5 6 S
Laboraio.y
eNo
Organics Analysis Data Sheet(Page 4}
Simple Number
Tentatively Identified Compounds
CAS
1
3
s
7
aft
10
._,19
,4
IS
1C
17
1*19
21
27.
23
28
„
28
24
in
Compound N«rTM
Wd^
^J^fS
•
Fraction
ttft
fX^ft
B^g
Estimated
(ug/tW ug/kg)v /
• -«...,
NFA denotes no fraction analyzedNCF denotes no compound foundlink denotes unknownmw denotes probable molecular weight
4 1 8 4 3 0 5 6 6
LABORATORY NAME: CTC/TOXICON
LAB SAMPLE 10 NO: 4184-93SAMPLE MATRIX: WATER
DATA RELEASE AUTHORIZED •Y:|c/4
ORGANICS ANALYSIS DATA SHEET(PAGE 1>
CASE NO:•C REPORT NO:CONTRACT NO:DATE SAMPLE RECEIVED: 89/29/87
. - / * / /
• / jj
41B44164
VOLATILE COMPOUNDS
CONCENTRATION: LOWDATE EXTRACTED/PREPARED:DATE ANALYZED: l«/*3/B7CONC/OIL FACTOR: 1.PERCENT MOISTURE: KNOT DECANTED)
CAS NUMBER74-87-374-83-975-81-475-88-375-89-247-44-175-15-875-35-475-35-3154-48-S47-44-3187-84-278-93-371-55-454-23-5188-85-475-27-4
CHLOROMETHANCBROMOMETHANEVINYL CHLORIDECHLOROETHANEMETHYLENE CHLORIDE . . . .ACETONECARBON OISULFIDE1,1-DICHLOROETHENE . . . .1, 1-DICHLOROETHANE . . . .TRANS-1. 2-DICHLOROETHENE .CHLOROFORM1,2-OICHLOROETHANE . . . .2-BUTANONE1, 1, 1-TRICHLOROETHANE . .CARBON TETRACHLORIOE . . .VINYL ACETATEBROMOOICHLOROMETHANE . . .
UG/L18 U18 U18 U18 US U18 U
1
UUUUUU<tuuu
18 US U
CAS NUMBER78-87-518841-82-479-81-4124-48-179-88-S71-43-218841-81-5118-75-875-2S-2188-18-1S91-78-4127-lt-*79-34-S
188-88-3188-98-7188-41-4188-42-5
UG/L1.2-OICHLOROPROPANE . . .TRANS-1. 3-DICHLOROPROENE .TRICHLOROETHENEDIBROMOCHLOROMETHANE . . .1. 1,2-TRICHLOROETHANE . .BENZENECIS-1.3-OICHLOROPROPENE .2-CHLOROETHYLVINYLETHER .BROMOFORH4-HETHYL-2-PENTANONE . . .2-HEXANONETETRACHLOROETHENE . . . .1.1.2.2-TETRACHLOROETHANETOLUENECHLOROBENZENEETHYLBENZENESTYRENETOTAL XYLENES
UUUUUUUUUUUUUUUUUU
B - COMPOUND WAS DETECTED IN THE «C BLANK.U - COMPOUND ANALYZED FOR BUT NOT DETECTED. THE REPORTED
VALUE IS THE MINIMUM ATTAINABLE DETECTION LIMIT FORTHE SAMPLE.
SEE PAGE 1A FOR COMPLETE DEFINITIONS OF THE DATAREPORTING 9UALIFIERS.
FORM I
4 1 8 4 3 0 1 6 9
Labora to ry Name: ETC/Toxicon
Case No: 4184
Sample Numb«r
Organics Analysis Data Sheet
CAS Number
67-63-0
71-36-3
78-92-2
Compound Name
Isopropyl Alcohol
N-Butyl Alcohol
sec-Butyl Alcohol
ConcentrationM/L
300U
200U
200U
indicates compound was analyzed for but not detpctgL Report the minimum detection limit for me sample with me U(e.j. 10U) y*1 on necessary concentration/dilution action. (Tnis is oot necessarily me instrument detection limit)The footnote should read; U-Compouad was analyzed for but not detected. The number U me minimum attainabledetection limit for the sample.Indicates an estimated vtlue. This flag Is used either when estimating * ccwxttration for lentativtly klentified compoond*where a 1:1 response it assnmed or when the mass tpectnl data inrliratcd me presence of a compound mat meets tfaeidenti-fkatioo criteria but the result is less dun me spedfied detection limit bat greater man zero (e . 101). If limit of detection ii10 ng/L and a coocentratioa of 3 u^/L is calculated, report as 3J.
4 1 8 4 30170
LABORATORY NAME
CASE NO
ETC /TOXICON4184
ORGANICS ANALYSIS DATA SHEET
(PAGE 2)
SEHIVOLATILE COMPOUNDS
CONCENTRATION: LOWDATE EXTRACTED/PREPARED: 99/39/97DATE ANALYZED: 18/85/87CONC/OIL FACTOR: 1.PERCENT MOISTURE: (DECANTED)
GPC CLEANUP YES X NOSEPARATORY FUNNEL EXTRACTION YESCONTINUOUS LIQUIO-LiaUIO EXTRACTION YES
CAS NUMBER188-95-2 PHENOL111-44-4 i!S<2-CHLOROETHYL>ETHER .95-57-8 2-CHLOROPHENOLS41-7J-1 1.3-DICHLOROBENZENC . . .184-44-7 1,4-OICHLOROBENZENE . . .188-S1-4 •CMZVL ALCOHOL9S-S8-1 1.2-OICHLOROBENZENE . . .95-48-7 2-HETHYLPHENOL39438-32-9 BIS<2-CHLOROISOPROPYL>ETHER184-44-5 4-HETHYLPHENOL421-44-7 N-NITROSO-OX-N-PROPYLAHINE47-72-1 HCXACHLOROETHANC98-9i-3 NITROtENZENC7i-§t-l ISOPHORONC•S-7S-S 2-NITROPHENOL185-47-9 2, 4-0IMETHYLPHENOL . . . .45-85-8 iENZOIC ACID111-91-1 •IS<2-CHLOROETHOXY)HETHANC12«-83-2 2.4-OICHLOROPHENOL . . . .128-82-1 1.2.4-TRXCHLOROBENZENE . .91-28-3 NAPHTHALENE1*4-47-1 4-CHLOROANILINE87-48-3 HEXACHLOROBUTADIENE . . .S9-S8-7 4-CHLORO-3-HETHYLPHENOL .91-57-4 2-HETHYLNAPHTHALENE . . .77-47-4 HEXACHLOROCYCLOPENTAOIENE88-84-2 2,4.4-TRICHLOROPHENOL . .9S-9S-4 2,4,5-TRICHLOROPHENOL . .11-58-7 2-CHLORONAPHTHALENE . . .88-74-4 2-NITROANILINE131-11-3 OIHETHYL PHTHALATE . . . .288-94-8 ACENAPHTHYLEME99-89-2 3-NITROAMILIME
U6/L1*191919191918181818181818181818S8181818181818181818185818S81818• 8
UUUUUUUUUUUUUUUUUUUUUUUUUUU
UU
UUUU
CAS NUMBER83-32-9S1-2B-S188-82-71 32-44- V121-14-2484-28-284-44-27885-72-384-73-7188-18-4S34-S2-184-38-4181-55-3118-74-187-84-S85-81-8128-12-784-74-2284-44-8127-88-885-48-791-94-154-55-3117-81-7218-81-9117-84-82*5-99-22*7-«<e-958-32-8193-39-553-78-3191-24-2
UG/L
ACENAPHTHENE 18 U2.4-DINITROPHENOL . . . . 58 U4-NITROPHENOL 58 UDIBENZOFURAN 18 U2.4-OINITROTOLUENE . . . . 18 U2.4-DXNITROTOLUENE . . . . 18 UDIETHYLPHTHALATE 18 U4-CHLOROPHENYL-PHENYLETHER 18 UFLUORENE 18 U4-NITROANILINE 58 U4.4-DINITRO-2-HETHYLPHENOL 58 UN-NITROSOOIPHENYLAHINE (!) 18 U4-BROHOPHENYL-PHENYLETKEM 18 UHEXACHLOROBENZEME . . . . 18 UPENTACHLOROPHENOL . . . . 58 UPHENANTHRENE 18 UANTHRACENE 18 UDX-N-BUTYLPHTHALATE ... 18 UFLUORANTHENE 18 UPYRENE 18 UBUTYLBENZYLPHTHALATE ... 18 U3.3'-OICHLOROBENZIOINE . . 28 UBENZO<A)ANTHRACENE . . . . 18 UBIS<2-ETHYLHEXYL>PHTHALATE 18 UCHRYSENE 18 UOI-N-OCTYL PHTHALATE ... 18 UBENZO(t>FLUORANTHENE ... 18 UBENZO<K)FLUORANTHENE ... 18 UBENZO(A>PYRENE 18 UINOENO<1,2.3-CD)PYRENE . . 18 UOIIENZ(A,H)ANTHRACENE . . 18 UIENZCXO. H, DPERYLENE ... 18 U
(i) - CANNOT BE SEPARATED FROM OIPHENYLAHINEFORH I
4 1 8 4 30171
N::
Organic* Analysis Data Sheet(Pige 3)Peshcides/PCBs
[arcentritio": [Lo»] Sediui (CKcle one)Site E'tractei.'Prepared: 29-Sep-B7Date Analyred: 06-Oct-87Conc/Di! Factor: 1Percent Ncisture(decanted) MR
6FC Clejr.us Yes [«]-NoSeparjlcTy Funnel Extrjction YesContinuous Liquid-Liquid Eitractian [x] Yes
CASNutber
[ug/U or ug/Kg
31T-84-4 Alphi-BHC ........................ 0.05 U319-85-7 Beti-BHC ........................ 0.05 U319-B6-B Delt*-BHC ........................ 0.05 U58-89-9 SaiM-BHC (Lindine) ............. 0.05 U76-44-8 HepUchlor ...................... 0.05 U309-00-2 Aldrin .......................... 0.05 U1024-57-3 Heptichlor Epo>id« ............... 0.05 U959-98-fl Endosulfin I .................... 0.05 U60-57-1 Dieldrin ........................ 0.1 U72-55-9 4,4'-OK ........................ 0.1 U72-20-8 Endrin ........................ 0.1 U33213-65-9 Endosulfin II ................... 0.1 U72-54-B 4,4'-DDD ........................ 0.1 U1-31-07-8 Endosulf»n SulUte ............... 0.1 U50-29-3 4,4 -DOT ........................ 0.1 U72-43-5 BethoiycMor .................... 0.5 U53494-70-5 Endrin Ketont ................... 0.1 U57-74-9 Chlordint ....................... 0.5 U8001-35-2 Tosiphene . . . . . . . . . . . . . . . . . . . . . . . I D12674-11-2 Arodor-1016 .................... 0.5 U11104-28-2 Aroclor-1221 .................... 0.5 U11141-16-5 Arodor-1232 .................... 0.5 U?TSfc9-2l-9 Aroclor-1242 . . . . . . . . . . . . . . . . . . . . 0 .5112t72-29-6 R r c c l o r - 1 2 4 B .................... 0.5 U11097-69-1 Aroclor-1254 . . . . . . . . . . . . . . . . . . . . 1 U11096-82-5 Aroclor-1260 . . . . . . . . . . . . . . . . . . . . 1U
Vs -
Vi = Volu»e of eitrict injected |ul)Vs -- Volute of »Jter eitrtcted (il)Ms - Height of s»ple eitrtcted |g)Vt - Volute o1 total extract (ul)
1000 or Us - Vt -
Fon I
10000 Vi • 3.0
4 1 8 4 3 0 1 7 2
Labofaio.y Name
Organics Analysis Data Sheet(Page 4)
Sample
Tentatively Identified Compounds
CASNumber Compouod N««n« Numbw
Etlirnat*dtration
ug/or ug/kg)
1C
5.
7.
^_ 5*1 /o
|16.
6.
I 2O.
ST.
to
NFA denotes no fraction analyzedNCF denotes no compound foundUnk denotes unknownmw denotes probable molecular weight
4 1 8 4 3 0 1 7 5
LABORATORY NAME:
LAB SAMPLE 10 NO:SAMPLE MATRIX:
ETC/TOXICON
4184-94
WATER
ORGANICS ANALYSIS DATA SHEETIfAGE 1>
/ -
DATA RELEASE AUTHORIZED BY:
CASE NO: 4184
ac REPORT NO: 41B4
CONTRACT NO: C(4^
DATE SAMPLE RECEIVED:
VOLATILE COMPOUNDS
CONCENTRATION: LOW
DATE EXTRACTED/PREPARED:
DATE ANALYZED: 18/83/87
CONC/OIL FACTOR: 1.
PERCENT MOISTURE: <NOT DECANTED)
PH
CAS NUMBER
74-87-3 CHLOROMETHANE74-83-9 BROMOHCTHANE
75-81-4 VINYL CHLORIDE75-88-3 CHLOROETHANE75-89-2 HETHYLENC CHLORIDE . . .
67-64-1 ACETONE75-15-8 CARBON DISULFIDE . . . .7S-3S-4 1, 1-DICHLOROETHEME . . .
7S-3S-3 1,1-OICHLOROETHANE . . .
1S6-68-S TRANS-1.2-OICHLOROETHENE67-44-3 CHLOROFORM
187-84-2 1.2-DICHLOROETHANE . . .71-93-3 2-BUTANONE71-SS-4 1.1,1-TRICHLOROETHANC .
54-23-5 CARBON TETRACHLOMIDE . .188-85-4 VINYL ACETATE
75-27-4 BROHOOICHLOROHETHANC . .
uc/18
18
18
18
f
41
18
5
5
18|
L
U
U
U
U
U
U
U
U
U
U
U
B\J
U
U
U
U
eft
CAS NUMBER
78-87-5
18861-82-4
79-81-4
124-48-1
79-88-5
71-43-2
18861-41-*
118-75-8
7S-2S-2
188-18-1
591-78-4
127-18-4
79-34-5
188-88-3
188-98-7
188-41-4
188-42-i
b1
1.2-OICHLOROPROPANE . . .
TRANS-1.3-DZCHLOROPROENE
TRICHLOROETHENEOIBROMOCHLOROHETHANE . . .
1.1.2-TRICHLOROETHANE . .BENZENECXS-1, 3-OICHLOROPROPENE .2-CHLOROETHYLVINYLETHER .•ROMOFORM
4-METHYL-2-PENTANONE . . .
2-HEXANONE
TETRACHLOROETHENE . . . .
1. 1.2. 2-TETRACHLOROETHANE
TOLUENE
CHLOROBENZENE
ETHYLBCNZENE
STYRENETOTAL XYLENE4
UO/LSs5555518518
18
518
UUUUUUUUUUU
UUUUUUU
B - COMPOUND WAS DETECTED IN THE 8C BLANK.U - COMPOUND ANALYZED FOR BUT NOT DETECTED. THE REPORTED
VALUE IS THE MINIMUM ATTAINABLE DETECTION LIMIT FORTHE SAMPLE.
SEE PACE 1A FOR COMPLETE DEFINITIONS OF THE DATA
REPORTING 8UAHFIERS.
FORM I
4 1 8 4 3 0 1 8 4
a b o r a t o r y Name: ETOToxicon
ase No: 4184
Sample Number
Organics Analysis Data Sheet
CAS Number
67-63-0
71-36-3
78-92-2
Compound Name
Isopropyl Alcohol
N-Butjl Alcohol
sec-Butyl Alcohol
ConcentrationHf/L
300U
200U
200U
U Itviiratff compound was analyzed for but not detected. Report me mfaimntti detection i™** for the t*r*f with the U(e.g. 10U) based on necessary concentration/dilution action. (This is not necessarily the instrument detection limit)The footnote should read: U-Compound was analysed for bat not detected. The number is the minimum attainabledetection limit for the sample.
j Tndif^t^t m i>etim«t«< vame. This flag is used either when »y<m«tint a concentration for tencttivety identified compoundswhere a 1:1 response is «««imH or when me m»*i medial data <m*i^«t««i the presence of a compound that meets the identi-fcarioa criteria but the result is less man the tpedfleddelectkmu^nit bat greater than zero (e . 10J). Iflimitofdetoctioais10 \ig/L and a concentration of 3 )ig/L is c?ir"latH. report as U.
4 1 8 4 3 0 1 8 5
LA90BA*:R* NAME
CASE NO
ETC / TOXIC ON
4184
ORGANIC* ANALYSIS DATA SHEET(PACE 2)
/a-
SEHIVOLATILE COMPOUNDS
CONCENTRATION: LOWDATE EXTRACTED/PREPARED: *9/3*/87DATE ANALYZED: l*/*5/87
CONC/OIL FACTOR: t.PERCENT MOISTURE: (DECANTED)
GPC CLEANUP VES X NOSEPARATORY FUNNEL EXTRACTION YESCONTINUOUS LIBUlO-LiaUID EXTRACTION YES
CAS NUHIER1*8-95-2 PHENOL111-44-4 iIS<2-CHLOROETHYL>ETHER .9S-S7-B 2-CHLOROPHENOL541-73-1 I.3-DXCHLOROBENZENE . . .1*4-44-7 1,4-OXCHLORQBENZENE . . .l**-Sl-4 BENZYL ALCOHOL9S-S8-1 1.2-OICHLOROBENZENE . . .95-48-7 2-HETHYLPHENOL39438-32-9 BX5(2-CHLOROXSOPROPYL>ETHER184-44-5 4-HETHYLPHENOL621-44-7 N-NXTROSO-DX-N-PROPYLAHXNE47-72-1 HEXACHLOROCTHANC98-95-3 NITROBENZENE78-59-1 ISOPHORONE••-75-5 2-NITROPHENOL185-47-f 2,4-DIhETHYLPHENOL . . . .65-BS-8 BENZOIC ACID111-91-1 BI§<2-CHLOROETHOXY>METHANE128-83-2 2.4-OICHLOROPHENOC . . . .128-82-1 1,2.4-TRICHLOROBENZENE . .91-28-3 NAPHTHALENE1*4-47-8 4-CHLOROANILINE87-68-3 HEXACHLOR08UTAOIENC . . .S9-5*-7 4-CHLORO-3-PIETHYLPHENOL .91-S7-4 2-HETHYLNAPHTHALENE . . .77-47-4 HEXACHLOROCYCLOPENTADIENE8B-«*-2 2.4,6-TRICHLOROPHENOL . .95-95-4 2. 4,5-TRICHLOROPHENOL . .91-S8-7 2-CHLORONAPHTHALENE . . .88-74-4 2-NITROANXLINE131-11-3 DIMETHYL FHTHALATE . . . .2*8-96-8 ACCNAPHTHYLEMC99-*9-2 3-NITROANILINE
UG/L1*1*1*1*1*1*181*1*1*181*
1*1*1*1*5*1*18!•!•1818181*181*5*
185*18185*
U
UUUU4iHUUUU
UUUUUUUU
UUUUUUUUU
U
UUUUU
CAS NUMBER83-32-9Sl-28-5188-82-71 32-64- V
01*121-14-2WK-28-2•4-66-27885-72-3•6-73-7188-18-6S34-S2-184-38-61*1-55-3ll«-7»-l•7-86-585-* 1-8128-12-784-74-2286-44-8129-88-885-68-7•l-?4-l56-55-3117-81-721B-*l-9117-84-82*5-99-22*7-*8-9S*-32-8193-39-553-7*-3191-24-2
UC/LACENAPHTHENE 1* U2.4-OINITROPHENOL . . . . 58 U4-NITROPHENOC 5* UOIBENZOFURAN 1* U2.4-OINITROTOLUENE . . . . 1* U2.4-OINXTROTOLUCNE . . . . 1* UOIETHYLPHTHALATE 18 U4-CHLOROPHENYL-PHENYLETHER 18 UFLUORENE 18 U4-NXTROANXLINC 58 U4.6-OXN1TRO-2-HETKYLPHENOL 58 UN-NITROSOOIPHENYLAHINE <1) 18 U4-SROMOPHENYL-PHENYLETHER 18 UHEXACHLOKOBENZENE . . . . 18 UPENTACHLOROPHENOL . . . . 58 UPHENANTHRENC 18 UANTHRACENE 18 UOI-N-tUTYLPHTHALATE ... 18 UFLUORANTHENE 18 UPYRENC 18 UBUTVLBENZYLPHTHALATE ... 18 U3.3'-OICHLOROBENZIOINE . . 28 UBENZO<A>ANTHRACENE . . . . 18 UBXS(2-ETHYLHEXYL)PHTHALATE 18 UCHRYSENE 1* UOI-N-OCTYL PHTHALATE ... 18 UBENZO<B>FLUORANTHENE . . 18 UBCNZOOOFLUORANTHENE . . . 1 8 UBENZO(A)PYRENE 18 UINDENO<1.2. 3-CD)PYRENE . . 18 UDIBENZ(A.H)ANTHRACENE . . 18 UBENZO(G.N. DPERYLENE ... 18 U
(1) - CANNOT BE SEPARATED FROM OIPHENYLAHINEFORM X
4 1 8 4 3 0 1 8 6
. 3 . - a .
fipjiysis Pa
iPage 7)Pesticides/Fx&s
DateDate Analyred: Oi-Dct-B"Conc/Dil Factor:Percent Hoistjreldecar.tei)
r'-5ep-«7
NR
af; CleanLC Yes [»]-MoSffji-itcry Fuin?, EifiCtJO" YfSContinuous Liquid-Liquid Eitriction [x] Yes
CftS tug'L] ar uq/KqNuiber
319-84-b ftlphi-BHC 0.05031S-85-7 Btta-BHC 0.05 U319-86-8 Delti-BHC 0.05 U5B-B9-9 Bauj-BHC (Lindane) 0.05 U76-44-8 Heptachlor 0.05 U309-00-: Aldrin 0.05 U10?4-57-3 Heptichlor Epoxide 0.05 U959-98-8 Endosullan I 0.05 U60-57-1 Oieldrin 0. U72-55-9 4,4'-OOE 0. U72-20-8 Endrin 0. U33213-65-9 Endosulfan II 0. U72-54-8 4,4'-DDO 0. U1-31-07-8 Endosulfan Sulfate 0. U50-29-3 4,4'-DDT 0.1 U72-43-5 Bethoxychlor 0.5 U53494-70-5 Endrin Ketone 0.1 U
57-74-9 CMordane 0.5 U8001-35-2 Toiaphtni 1U12674-11-2 Rroclor-1016 0.5 U11104-2B-2 Aroclor-1221 0.5 U11141-16-5 Aroclor-1232 0.5 U5:«69-2l-9 Aroclor-1242 0.5 U:267:-:9-t Aroclor-1248 C.5 U11097-69-1 Aroclor-1254 1 U11096-B2-5 Aroclor-1260 1U
vs :
Vi = VoluK of extract injected lullVs * Voluie of Mater extracted (il)Ms - Height of saiple eitricted Ig)Vt ; Voluie of total extract l u l l
1000 or Vt --
Fort I
10000 Vi - 3.0
41 84 3 0 1 8 7
I ».. .r - > r,
Co'^c No _.
Orvjanics Analysis Data Sheet(Page 4)
Tentatively Identified Compounds
CASNumber Compound Nwn« Fraction
Ectim«t«dgac«fitrction
(ug/tfor ug/Vg)
~Tiri (6
3.
*•
6.
I..
>..
11.. II8
. frf-7 (138
//nt Ib16.. lit
5t)1353
/intI..
I..
6..
27..
9..
30..
NFA denotes no fraction analyzedNCF denotes no compound foundUnk denotes unknownmw denotes probable molecuJar weight
4 1 8 4 3 0 1 8 8
LABORATORY NAME
LAB SAMPLE 10 NO:SAMPLE MATRIX:
ETC/TOXICOH4184-1*6WATER
DATA RELEASE AUTHORIZED
41844184
ORGAN1CS ANALYSIS DATA SHEET(PAGE 1)
CASE NO.flC REPORT NO.CONTRACT NO:DATE SAMPLE RECEIVED:
VOLATILE COMPOUNDS
•9/29/B7
CONCENTRATION: LOUDATE EXTRACTED/PREPARED:DATE ANALYSED: l»/»3/B7CONC/DIL FACTOR. 1.PERCENT MOISTURE: <NOT DECANTED)
PH
CAS NUMBER74-17-1 CHLOROMETHANE74-BJ-* •ROMOnETHANC7J-81-4 VINYL CHLORIDE75-M-3 CHLOROETHANE7S-«l-2 METHYLENE CHLORIDE . . .47-44-1 ACETONE7S-is-« CARBON DISULFIOE . . . .7S-3S-* 1.1-OICHLOROETHENE . . .7S-3S-3 1.1-01CHLOROETHANE . . .134-48-S TRANS-1,2-OICHLOROETHENE47-44-J CHLOROFORMl«7-«4-2 1,2-DICHLOROETHANE . . .78-13-1 2-iUTANONE71-SS-4 1.1.1-TRICHLOROETHANE .S4-23-S CARBON TETRACHLORIDC . .l«8-tS-4 VINYL ACETATE75-27-4 BROM001CHLOROMETHANE . .
UO/L CAS NUMBER181*!•!•2!•SSi11SI19SS18i
U 78-87-SU l**41-«2-4U 7f-»l-*U 124-48-1J 7f-0-SU 71-43-2U 1041-V1-SU ll«-7S-8
U 7S-2»-2IM-lt-l
U S»l-78-4U 127-18-4J&1 7T-34-1U !••-••- 1U l»8-f«-7U 1M-41-4U l**-42-S
"Ail*
UG/L1.2-DICHLOROPROPANE . . .
TRANS-1. 3-OICHLOROPROENE .TRICHLOROETHENEOUROMOCHLOROMETHANE . . .1. 1. 2-TRICHLOROETHANE . .•ENZENECIS-1.3-OICHLOROPROPENE .2-CHLOROETHYLVINYLETHER .BROMOFORH
4-METHYL-2-PENTANONE . - .2-HEXANONETETRACHLOROETHENE . . . .1.1.2.2-TETRACHLOROETHANETOLUENECHLOROBENZENEETHYLBENZENESTYRENETOTAL XYLENES
UUUUUUUUUUUUUUUUUU
I - COMPOUND WAS DETECTED IN THE «C BLANK.J - REPORTED VALUE IS LESS THAN THE DETECTION LIMIT.U - COMPOUND ANALYZED FOR BUT NOT DETECTED. THE REPORTED
VALUE IS THE MINIMUM ATTAINABLE DETECTION LIMIT FORTHE SAMPLE.
SEE PAGE 1A FOR COMPLETE DEFINITIONS OF THE DATAREPORTING QUALIFIERS.
FORM I
4 1 8 4 3 0 4 4 7
Labora to ry Name: ETC/Toxicon
"ase No: 4184
Sample N u m b e r
Organics Analysis Data Sheet
CAS Number
67-63-0
71-36-3
78-92-2
Compound Name
Isopropyl Alcohol
N-Butyl Alcohol
sec-Butyl Alcohol
ConcentrationHt/L
300U
200U
200U
U Indicates compound was analyzed for but not detected. Report me minimum detection limit for the sample with the U(e.g. 10U) based on necessary cooceatntioQ/dilutioo action. (This U cot necessarily the instrument detection limit)The footnote shook! read: U~Compound was analyzed for but not detected. The number is the minimum attainabledetection limit for the sample.
an »ttim«t«d vitnf Thfr flag U iM«d atha- «h«i i»«fini«riin i cnnceaftarioB for lentafivriy MamTied compound!where a 1:1 response is assumed or wtiea me mass spectral data indicated the presence of a compound mat meets me identi-fication criteria but the result is less than me specified detection limit but greater manxero(e^. 10J). If limit of detection is10 vffL and a concentiation of 3 u</L is calculated, report as 3J.
4 1 8 4 3 0 4 4 8
LABORATORY NAME
CASE NO
ETC/TOXICON
4184
ORGANICS ANALVS1S DATA SHEET<PAGE 2)
SEMIVOLATILE COMPOUNDS
CONCENTRATION: LOW
DATE EXTRACTED/PREPARED: 89/38/B7DATE ANALYZED: 18/84/87CONC/OIL FACTOR: 1.PERCENT MOISTURE: (DECANTED)
GPC CLEANUP VES X NOSEPARATORY FUNNEL EXTRACTION YESCONTINUOUS LIQUID-LIQUID EXTRACTION YES
CAS NUMBER188-95-2 PHENOL111-44-4 BIS<2-CHLO*OETHYL)ETHEB .95-57-8 2-CHLONOPHENOL541-73-1 1.3-OICHLOROIENZENE . . .184-44-7 1,4-DICHLOROBENZENE . . .188-51-4 BENZYL ALCOHOL95-58-1 1,2-OICHLOROBENZENE . . .95-48-7 2-HETHYLPHENOL39438-32-9 8IS<2-CHLOROISOPROPYL>ETHER1*6-44-5 4-METHYLPHENOL621-44-7 N-NITROSO-DI-N-PROPYLAHINE47-72-1 HEXACHLOROETHANE98-95-3 NITROBENZENE78-59-1 ISOPHORONE88-7S-S 2-NIT MO PHENOL185-47-9 2.4-OIHETHYLPHENOL . . . .45-85-8 BENZOIC ACID111-91-1 BIS<2-CHLO»OETHOXY>METHANE128-83-2 2.4-OICHLOROPHENOL . . . .129-82-1 1,2,4-TRICHLOROBENZENE . .91-28-3 NAPHTHALENE1*4-47-8 4-CHLOROANIL1NE87-48-3 HEXACHLOROBUTAOIENE . . .59-54-7 4-CHLORO-3-METHYLPHENOL .91-57-4 2-METHYLNAPHTHALENE . . .77-47-4 HEXACHLOROCYCLOPENTADIENE88-84-2 2.4.4-TRICHLOROPHENOL . .95-95-4 2.4,S-TRICHLOROPHENOL . .91-58-7 2-CHLORONAPHTHALENE . . .88-74-4 2-NITROANILINE131-11-3 DIMETHYL PHTHALATE . . . .288-94-8 ACENAPHTHYLEME99-89-2 3-NITROANILXNE
UG/L1*1818181818181818181818181818185818181818181818181818581858181858
UUUUUUUUUUUUUUU
UUUUUUUUUUUUUUUUUU
CAS NUMBER83-32-9il-28-S188-82-7132-44-9121-14-2484-28-284-44-27885-72-384-73-7188-18-4534-52-184-38-4181-55-3118-74-187-84-585-81-8128-12-784-74-2284-44-8129-88-88S-48-791-94-154-55-3117-81-7
218-81-9
117-84-8
285-99-2
287-88-9
58-32-8193-39-553-78-3191-24-2
ACENAPHTHENE2,4-OINITROPHENOL . . . .
4-NITROPHENOLOIBENZOFURAN2.4-OINITROTOLUENE . . . .2.4-OINITROTOLUENE . . . .OIETHYLPHTHALATE4-CHLOROPHENYL-PHENYLETMERFLUORENE4-NITROANILINE4,4-DINITRO-2-METHYLPHENOLN-NITROSOOXPHENYLAMINE <1>4-BROMOPHENYL-PHENYLETHERHEXACHLOROBENZENE . . . .PENTACHLOROPHENOL . . . .PHENANTHRENCANTHRACENEOZ-N-BUTYLPHTHALATE . - .FLUORANTHENEPYRENEBUTYLiENZYLPHTHALATE . . .3.3'-DICHLOROBENZIOINE . .
BENZO(A)ANTHRACENE . . . .BIS<2-ETHYLHEXYL>PHTHALATE
CHRYSENEOI-N-OCTYL PHTHALATEBENZO<B>FLUORANTHENE . .BENZO(K>FLUORANTHENE . . .BENZO(A>PYRENEINOENOM-2. 3-CD> PYRENEDIBENZ<A.H)ANTHRACENE . .BENZO<G,H. DPERYLENE . .
UG/L18 U58581818181818185858
18
18
1858
18
1818
18
1818
28
18
18
18
1*18
18
18
18
18
UUUUU
UUUUUUU
UUUUU
UUU
UUU
U
U
U
U
U
U
U
18 U
<1> - CANNOT BE SEPARATED FROM OIPHENYLAMINE
FORM I
4184 30449
fi-.s Data sheet
ir«e 3iPest ic i ies /PCBs
trat ion: [Lo»] Redui ( C i r c l e one)
ilricWtPrepirei: 25-3ep-67lite A m a z e d : 0 7 - O c t - 6 7Conc/Di l Fac tor : 5Percent Hc is ture ldecante i i Nft
6PL Cifjnup Yes [«]-NoS e p a r a t o r y Funnel [ i t ract ionCor t inuous liquid-Liquid E i t rac t io r [ i)
CAS [ug/L] or uq/KgNuiber
I19-B4-6 fllphi-BHC 0.25 U319-B5-7 Beti-BHC 0.25 U319-86-8 Delti-BHC 0.25 U58-89-9 6uii-BHC (lindane) 0.25 U76-4<-B Heptachlor 0.25 U309-00-2 ftldrin 0.25 U1024-57-3 Heptithlor Epo«ide 0.25 U959-98-fl EndosuHan I 0.25 U60-57-1 Oieldnn 0.5 U72-55-9 4,4'-DDE 0.5 U72-20-B Endrin 0.5 U33213-65-9 Endosulfin II 0.5 U72-54-8 4,4'-DDD 0.5 U1-31-07-8 Endosulfan Sulfitt 0.5 U50-29-3 4,4 ' -DDT 0. U72-43-5 H»tho»ychlor 2. U53494-70-5 Endrin Kftont 0. U57-74-9 Chlordane 2. UB001-35-2 Touphtnt U12674-11-2 Aroclor-1016 2. U11104-28-2 Aroclor-1221 2.5 U11141-16-5 Aroclor-1232 2.5 U53469-21-9 Aroclor-1242 2.5 U12672-29-6 Aroclor-1248 2.5 U11097-6'-! Aroclor-1254 5U11096-B2-5 Aroclor-1260 5 U
Vs =
Vi : Volute of otract injected lul)Vs : Voluii of vatcr eitracted dl)Ms - Height of saiple eitracted (g)Vt = VoluM of total e.trict lul)
1000 or Us = Vt -
Fort I
50000 Vi • 3.0
4 1 8 4 3 0 4 5 0
• J1 ,: , \ j r ; , t -
No
Organics Analysis Data Sheet(Page 4)
Tentatively Identified Compounds
I Sample Nurntxv I
yjuur^Jo ioi I
NFA denotes no fraction analyzedNCF denotes no compound foundInk denotes unknownmw denotes probable molecular weight
4 1 8 4 30451
E N •;_ 5 E -
" .r• < J 3
LABORATORY NAME: ETC/TOXICON
LAB SAMPLE ID NO: 4184-7*
SAMPLE MATRIX: WATEROATA RELEASE AUTHORIZED «Y
ORGANICS ANALYSIS DATA SHEET(PAGE 1)
CASE NO: «18»
QC REPORT NO: 4184CONTRACT NO:
DATE SAMPLE RECEIVED: •7/23/87
VOLATILE COMPOUNDS
CONCENTRATION: LOWDATE EXTRACTED/PREPARED:
DATE ANALYZED: 18/82/87CONC/OIL FACTOR: 1.PERCENT MOISTURE: (NOT DECANTED)
PH
CAS NUMBER74-87-3 CHLOROMETHANE74-83-7 BROMOHETHANE
75-81-4 VINYL CHLORIDE75-88-J CHLOROETHANE75-87-2 MCTHYLENE CHLORIDE . . .47-44-1 ACETONE
75-15-9 CARiON DISULFIOC . . . .
75-35-4 1.t-OICHLOROCTHENC . . .
75-35-1 1.1-OICHLOROETHANC . . .154-48-5 TRANS-1.2-OICHLOROETHENE47-44-1 CHLOROFORM
l»7-»4-2 1.2-OICHLOROETHANC . . .
78-73-3 2-IUTANONC71-SS-4 I.1.i-TRICHLOROETHANE .
S4-23-5 CARION TETRACHLORIDC . .
l«e-«5-4 VINYL ACETATE75-27-4 IROMOOICHLORCMETHAWC . .
181818S
UG/L18 U
UUUUUUUUUUU
1
18
•
UUUuu
CAS NUMBER78-87-518841-82-4
77-81-4124-48-177-88-S71-43-2
UO/L
118-75-871-25-2188-18-1571-78-4
127-18-4
77-34-5188-88-3
188-78-7188-41-4188-42-1
1,2-OICHLOMOPROPANE . . .TRANS-1.3-OICHLOROPROENE .
TRICHLOROETHENEDIBROMOCHLOROMETHANE . . .1.1.2-TRICHLOROETHANC . .BENZENECIS-1.3-OICHLOROPROPENE .
2-CHLOROETHYLVINYLETHER .BROMOFORM4-METHYL-2-PENTANONE . . .
2-HEXANONETETRACHLOROETHENE . . . .1.1,2.2-TETRACHLOROETHANE
TOLUENECHLOROBENZENE
ETHYLBENZENE
STVRENETOTAL XYLENES
18f18
18
51855555
U
uuuuuuuuuuuuuuuuu
U - COMPOUND ANALYZED FOR BUT NOT DETECTED. THE REPORTEDVALUE IS THE MINIMUM ATTAINABLE DETECTION LIMIT FORTHE SAMPLE.
SEE PAGE 1A FOR COMPLETE DEFINITIONS OF THE DATAREPORTING 8UALXFIERS.
FORM I
4184 30103
L a b o r a t o r y Name: ETC/Toxicon
Case No: 4184
Sample Numb«r
Organics Analysis Data Sheet
40 -ir~)
CAS Number
67-63-0
71-36-3
78-92-2
Compound Name
Isopropyl Alcohol
N-Butyl Alcohol
sec-Butyl Alcohol
Concentrationug/L
300U
200U
200U
U tivliryti*; compound WS$ analymd for but DOt 4t9&t4. RcpOTl DC minimntn detection litnit for the Sample with mt U(e.g. 10U) Nm^l on necesssy n»i»<fjiii<uyi/iiiiyfvy) icdoo. (Thjj U not necosjrfly me iostnuaent detectioQ limit)
I wts SDiIyzed for but not 4ficrtfi1 The number is me «"ini«num MQidbleThe footnote ihould read:detection limit for the ample.
viJoe. This flv U nwd eiflier wbco ffttm^tiy t cooceafaaioo for texiBdvtly identified compounds1-1 nH^rmtr If fyfamrA or »<Un ft>g m»q fpertrri <to» itntiftW«1 Ihe prMencg rf • componfld flat meett flie ideali-
rtcanoo criteria but the remit b less than the Kpecified detectioa limit but greater msn zero (e . 101). If limit of detection is10 U£/L aad a cooceatntioa of 3 ug/L is calculated, report « 31.
4 1 8 4 3 0 1 0 4
L A B O R A T O R Y NAHE E T C / T
CASE NO «18»
•* r _ E N _ - £ E R
ORGAMC5 ANALYSIS DATA SHEET<PAGE 2>
SEMIVOLATILE COMPOUNDS
CONCENTRATION: LOW
DATE EXTRACTED/PREPARED: *9/3*/87DATE ANALYZED: l*/*5/87
CONC/DIL FACTOR: 1.
PERCENT MOISTURE: (DECANTED)
GPC CLEANUP YES X NOSEPARATORY FUNNEL EXTRACTION YESCONTINUOUS LIQUID-LIQUID EXTRACTION YES
CAS NUN0ER1*8-95-2 PHENOL
111-44-* 8IS<2-CHLOROETHYL>ETHER .
95-57-8 2-CHLOROPHENOL
S41-73-1 1,3-OICHLOROBENZENE . . .1*4-44-7 1,4-DICHLOROBENZENE . . .
1*9-51-* iENZYL ALCOHOL95-59-1 1,2-DICHLOROBENZEME . . .
95-41-7 2-HETHYLPHENOL39438-32-9 BIS(2-CHLOROISOPROPYL)ETHER
1*4-44-5 4-METHYLPHENOL
421-44-7 N-NITROSO-OI-N-PROPYLAMINE47-72-1 HEXACHLOROETHANE
9B-9S-3 NITROBENZENE
71-59-1 XSOPHORONE88-75-5 2-NITROPHENOL
185-47-9 2,4-OIMETHYLPHENOL . . . .45-85-9 tENZOIC AC 10
111-91-1 BIS<Z-CHLOROETHOXY>METHANE129-«3-2 2,4-OICHLOROPHENOL . . . .129-82-1 1,2.4-TRICHLOROBENZENE . .
91-29-3 NAPHTHALENE
1*4-47-8 4-CHLOROANILINE
87-48-3 HEMACHLORQBUTADIENE . . .S9-S9-7 4-CHLORO-3-METHYLPHENOL .
91-57-4 2-HETHYLNAPHTHALENE . . .77-47-4 HEXACHLOROCVCLOPENTAOIENE
68-94-2 2,4.4-TRICHLOROPHENOL . .7S-7S-4 2.4,5-TRICHLOROPHENOL . .91-S8-7 2-CHLORONAPHTHALENE . . .88-74-4. 2-NITROANILINE
131-11-3 DIMETHYT. PHTHALATE . . . .
2*8-94-8 ACENAPHTHYLENE99-*9-2 3-NITROANILINE
UG/L1*1*
1*
1*
1*1*
!•1*
1*
1*
18
1*
18i*1*
1*
5*1*
1*1*
1*
1*
1919
19
19
19S*19
59
19
19
59
U
U
U
U
UU
U
U
U
U
U
U
UU
U
UU
U
UU
U
U
U
U
U
U
UU
U
U
U
UU
CAS NUMBED
83-32-9
51-28-5199-92-7
132-44-9
121-14-2494-29-2•4-44-27995-72-384-73-7
199-19-4534-52-1
84-39-4
191-55-3118-74-1
87-84-5•5-91-8128-12-784-74-2
294-44-9129-99-985-48-791-94-1
54-55-3117-81-7218-81-9
117-84-9295-99-22*7-*B-9
59-32-8193-39-5
53-79-3191-24-2
ACENAPHTHENE2. 4-DINITROPHENOL . . . .4-NXTNOPHENOLOIBENZOFURAN2,4-OINITROTOLUENC . . . .2.4-OINITRQTOLUENE . . . .
DIETHYLPHTHALATE4-CHLOROPHENYL-PHENYLETHER
FLUORENE4-NITROANILINE
4. 4-OINITW-2-HETHYLPHENOLN-NITROSOOIPHENYLAMINE <1>4-BROMOPHENYL-PHENYLETHCR
HEXACHLOROBENZENC . . . .PENTACHLOROPHENOL . . . .PHENANTHRENE
ANTHRACENEDI-N-BUTYLPHTHALATE . . .
FLUORANTHENE
PYRENEBUTYLBENZYLPHTHALATE . . .3, 3'-OICHLO«OBENZIOINE . .BEN20(A>ANTHRACENE . . . .BIS(2-ETHYLMEXYL)PHTHALATECHRYSENEDI-N-OCTYL PHTHALATE . . .BENZO<B>FLUORANTHENE . . .BENZO(H)FLUORANTHENE . . .BENZO(A)PYRENE
INOENO<1.2. 3-CO)PYRENE . .OIBENZ<A.H>ANTHRACENE . .
BENZO<G. H, DPERYLENE . . .
UG/L19
59
59
1919
19
19
19
19
59
59
1919
19
59
1919
19
1919
19
2919
34
19
19
19
1*1*19
19
19
U
U
U
UU
U
UU
U
UU
U
U
UU
UU
UU
U
U
U
U
U
U
U
U
U
U
UU
<1> - CANNOT BE SEPARATED FROM 01PHENYLAMINE
FORM I
4184 30105
Ld'r'i';', Hit;: -.".':-.. ::r
Case No: 4;=4
r j'.r-ies. !n;.
Organ:cs Analysis Data Sheet(Page 3)Peshcides/PC&s
Concentration: [Lou] Mefliui (Cir:le eDate Eitracted/Preparefi: 2'-Sep-87Bite Rnaly:ed; 06-0ct-fl7Conc/Dil Factor: 1Percent Moistureldecantedj NR
6FC C'.ea-u: Yes («]-NoSeparator* Funnel tstrac'ion YesCcntinuoi.3 Liquid-Liquid Extractian [«] Yts
CASNuiber
[uq/L] or ug/Kg
319-84-6 Alphi-BHC 0.05 U319-B5-7 B»tJ-BHC 0.05 U319-B6-8 Ddti-BHC 0.05 U53-89-9 Saiii-BHC ILjndine) 0.05 U76-44-8 HepticMor 0.05 U309-00-2 Aldrin 0.05 U1074-57-3 HeptKhlor Epoiide . 0.05 U959-98-8 Endosulfin I 0.05 U60-57-1 Dieldrin 0.1 U72-55-9 4,4'-DDE 0.1 U72-20-8 Endrin 0.1 U33213-65-9 Endosulfin 11 0.1 U72-54-8 4,4'-DDB 0.1 U1-31-07-8 Endosulfjn Sulfite 0.1 U50-29-3 4,4 ' -DDT 0.1 U
72-43-5 Hethoxychlor 0.5 U53494-70-5 Endrin Kftont 0.1 U57-74-9 Chlord»ne 0.5 U8001-35-2 Touphene 1U12674-11-2 flroclor-1016 0.5 U11104-28-2 Aroclor-1221 0.5 U11141-16-5 Aroclor-1232 0.5 Uf3U!?-:i-9 Aroclor-1242 0.5 U12672-29-6 flroclor-1248 C.5 U11097-69-1 Aroc!or -1254 1 U
11096-82-5 Aroclor-1260 1 U
Vi = Voluw of utract injected (ul)Vs - Voluie of Niter ext racted (•!)Ms - Weight of saiple e x t r a c t e d (q)Vt = Voluie of total eitract (ul)
Vs - 1000 or Ms - Vt = 10000 Vi = 3.0
Fori
4 1 8 4 3 0 1 0 6
NoSsr
Organics Analysis Data Sheet(Page 4}
i I
f I
CASNumber
Tentatively Identified Compounds
Compound Fr»cl»ooCctim«t«d
np*"f"**<w*(ug/jf<x ug/kg)
1O.
Sorrai 13,3.
I.
L 35iftffe
24
27.
30
NFA denotes no fraction analyzedNCF denotes no compound foundUnk denotes unknownmw denotes probable molecular weight
4 1 8 4 3 0 1 0 7r- - i
LABORATORY NAME: ETC/TOKICON
LAI SAMPLE ID NO. 4184-BV
SAMPLE MATRIX: HATER
DATA RELEASE AUTHORIZED BY\Jt.
ORCANICS ANALYSIS DATA SHEET
'<PAGE 1)
CASE NO: 4184
•C REPORT NO: 4184
CONTRACT NO: O}^^
DATE SAMPLE RECEIVED.
VOLATILE COMPOUNDS
»9/23/87
CONCENTRATION: LOWDATE EXTRACTED/PREPARED:DATE ANALYZED: l»/»2/87
CONC/DIL FACTOR: 1.PERCENT MOISTURE: <NOT DECANTED)
PH
CAS NUMBER74-87-374-83-975-81-475-88-37S-*9-247-44-175-15-875-35-4
75-35-3156-68-567-64-3187-84-278-93-371-55-454-23-518B-8S-475-27-4
CHLOROMETHANEBROMOMETHANCVINYL CHLORIDECHLOROETHANEMETHYUENE CHLORIDE . . . .ACETONECARBON OISULFIOE1. 1-DICHLOROETHENE . . . .1. 1-OICHLOROETHANE . . . .TRANS-1.2-DICHLOROETHEME .CHLOROFORM1.2-OICHLOROETHANE . . . .2-BUTANONE1. 1, 1-TRICHLOROETHANC . .CARBON TETRACHLORIDE . . .VINYL ACETATE
BROMOOICHUOROMETHANC - . .
UG/L18 U18 U18 U18 U5 U43
1
UU
UUUUUUU
18 U• U
CAS NUMBER71-87-51*841-82-471-81-4124-48-17V-88-571-43-21*861-81-5118-75-875-2S-2181-18-1591-78-4127-11-479-34-51*8-88-3188-98-71*8-41-4188-42-5
UG/L1.2-OZCHLOROPROPANC . . .TRANS-1,3-OICHLOROPROENE .TRICHLOROETHENCOIBHOMOCHLOROHETHANE . . .1.1,2-TRICHLOROETHANE . .BENZENECIS-1.3-OICHLOROMOPENE .
2-CHLOROETHYLVINYLETHER .
IROMOFOdM
4-METHYL-2-PEMTANONE . . .2-HEXANONETETRACHLOROETHENE . . . .1.1.2.2-TETRACHLOROETHANETOLUENECHLOROBENZENEETHYLBENZENESTYRENETOTAL XYLENES
51*
UUUUUUUUUUUUUUUUUU
U - COMPOUND ANALYZED FOR BUT NOT DETECTED. THE REPORTEDVALUE IS THE MINIMUM ATTAINABLE DETECTION LIMIT FORTHE SAMPLE.
SEE PAGE 1A FOR COMPLETE DEFINITIONS OF THE DATAREPORTING BUALIFIERS.
FORM I
4 1 8 4 3 0 0 8 4
Laboratory Name: ETC/Toxicon
Case No: 4184
Sample Nurabtr
/o
Organics Analysis Data Sheet
CAS Number
67-63-0
71-36-3
78-92-2
Compound Name
Isopropjl Alcohol
N-Butyl Alcohol
sec-Butyl Alcohol
ConcentrationHt/L
300U
200U
200U
U Tndif^t^ mtnpnufyj IM^ »TnlyTH fnr Ht ~^ AftrftrA Pgi«t **• minimum d*«Mtinn limit fnr th» tarn pig with thg II(e.g. 10U) based on necessary concentradoo/dihition action. (This is not necessarily die instrument detection limit)The footnote should real U-Compound was analyzed for but not detected. The number is the minnnnm attainabledetection limit for me sample.
J T«<<irat»« «n fft^mttfA vahw. This flag U used either when >t*im«t<n£ a conctntration for teutatively identified compoondiwhere a 1:1 response is assumed or when the mass spectral data indicated me presence of a compound that meets the ideod-fication criteria but the result is less than die specified detection limit but greater man tero (&g. 1QJ). If limit of detection U10 iig/L and a concentration of 3 U&/L is calculated, report at 3J.
4 1 8 4 3 0 0 8 5
LABORATORY NAME
CASC NO:
ETC/TOXICON
418*
OUGANICS ANALYSIS DATA SHEET(PAGE 2)
SEMIVOLATILE COHPOUNOS
CONCENTRATION: LOWDATE EXTRACTED/PREPARED: 89/38/87DATE ANALYZED: 18/85/87CONC/OIL FACTOR: 1.PERCENT MOISTURE: (DECANTED)
CPC CLEANUP YES X NOSEPARATORY FUNNEL EXTRACTION YESCONTINUOUS LIQUID-LieUIO EXTRACTION YES
CAS NUMBER188-95-2 PHENOL111-44-4 BX5(2-CHLOROETHYL>ETHEK .9S-S7-8 2-CHLOROPHENOLS41-73-1 1.3-DICHLOROBENZENE . . .184-44-7 1.4-OICHLOROBENZENE . . .188-51-4 BENZYL ALCOHOL95-58-1 1.2-OXCHLOROBENZENE . . .95-48-7 2-hETHYLPHENOC39438-32-9 BIS(2-CHLOROISOPROPYL)ETHER186-44-5 4-METHYLPHENOL421-64-7 N-NITROSO-DI-N-PROPYLAMINE47-72-1 HEXACHLOROCTHANC98-95-3 NITROiENZEMC7S-S9-1 ISOPHOROMC88-75-S 2-NITROPHENOL185-47-9 2.4-OIMETHYLPHENOL . . . .45-85-8 KNZOIC ACID111-91-1 §IS(2-CHLOROETHOXY)METHANE
128-83-2 2. 4-OICHLOKOPHENOL . . . .
128-82-1 1.2.4-TKXCHLOROBENZENC . .
91-28-3 NAPHTHALENE184-47-8 4-CHLOROANILINE•7-48-3 HEXACHLOROBUTAOIENC . . .59-58-7 4-CHLOHO-3-HETHYLPHENOL .91-57-4 2-HETHYLNAPHTHALENE . . .77-47-4 HEXACHLOROCYCLOPENTADIENE88-86-2 2.4.4-TRICHLOROPHENOL . .95-95-4 2.4,S-TRICHLOROPHENOL . .91-58-7 2-CHLORONAPHTHALENE . . .88-74-4 2-NITROANILINC131-11-3 DIMETHYL PHTHALATE . . . .298-94-8 ACENAPHTHYLENC99-89-2 3-NXTMOANILINC
UG/L
!•!•1*1*!•!•
!•
!•!•!•!•1*
!•!•!•!•S»!•1*181*!•1818!•!•185818S81818S8
UuUuuuuuuuuuuuuuuuuuuuuuuuuuuuuuu
CAS NUMiER
83-32-9Sl-28-5188-82-7132-44-9121-14-2484-28-284-44-27885-72-384-73-7188-18-4534-52-184-38-4181-5S-3118-74-187-84-58S-81-8128-12-784-74-2284-44-8129-88-885-48-791-94-1S4-SS-3117-81-7218-81-9117-84-82*5-99-2287-«8-958-32-8193-39-553-78-3191-24-2
ACENAPHTHENE2.4-OINITROPHENOL . . . .4-NITROPHENOLDliENZOFURAN2.4-OINITROTOLUENE . . . .2.A-DINITROTOLUENC . . . .DIETHYLPHTHALATE4-CHLOROPHENYL-PHENYLETHERFLUORENC4-NITROANXLXNC4,6-OINITRO-2-METHYLPHENOLN-NITROSODIPHENYLAHINt <1>
4-iROMOPHENYL-PHENYLETHERHEXACHLOROIENZENE . . . .PENTACHLOROPHENOL . . . .PHENANTHRENEANTHRACENEOX-N-BUTYLPHTHALATE . . .
FLUORANTHENEPYRENE•UTYL8ENZYLPHTHALATE . . .3.3--OICHLOROBENZIDINE . .BENZO<A>ANTHRACENE . . . .BIS(2-ETHYLHEXYL >PHTHALATECHRYSENEOI-N-OCTYL PHTHALATE . . .•EN20(B)FLUORANTHENE . . .BENZO(K)FLUORANTHENE . . .BENZO<A)PYRENEINOENOd, 2. 3-COPYRENE
OIIENZ<A,H>ANTHRACENE . .8ENZO(G.H. DPERYLENE . . .
UG/L
18 U
U
U
58
58
18
18
18
18
18
18
58
58
18
18
18
58
18
18
18
18
18
18
28
18
1818
18
18
18
18
18
18
U
U
U
U
U
U
uuuuuuuuuuuuuuuuuuuuuuu
<1> - CANNOT BE SEPARATED FROM DIPHENYLAHXNE
FORH X
4184 3C086
I r e .Case Nc: MB*
Organic* Analysis Data Sheet(Page 3)PestKjdes/PCBs
Co^ce^'ation: [Lo»] Kediui (Circle on?)Date Eitractei/rrepared: I^-Sep-B7Date Anal/red: OtrOct-B7Conc/DiI Factor: 1Percent Koisture(decanted) NR
Cleave fes [«Hot;', Fur.nel Extraction Yes
Continuous Liquid-Liquid Extraction [i] Yes
CASNuiber
319-84-6319-85-7319-86-858-89-976-44-8309-00-21024-57-3959-98-860-57-172-55-972-20-B33213-65-972-54-81-31-07-850-29-372-43-553494-70-557-74-98001-35-212674-11-211104-28-211141-16-5
11096-B2-5
[ug/l] or
Alphi-BHCBet»-BHCDelta-BHCGaiia-BHC (Lindane)Heptachlor
Heptachlor Epoiide.Endosulfan IDieldrin
EndrinEndosulfin II
Endosulfan Sulfate.4,4'-DOTflethoxychlorEndrin KetoneCMordaneToxapheneAroclor-1016Aroclor-1221Aroclor-1232Aroclor-1242Aroclor-1248Aroclor-1254Aroclor-1260
0.05 U0.05 U0.<K U0.05 U0.05 U0.05 U0.05 U0.05 U0.1 U0.1 U0.1 U0.1 U0.1 U0.1 U0.1 U0.5 U0.1 U0.5 U
1 U0.5 U0,5 U0.5 U0.5 U0.5 U
1 U1 U
Vi = VoIuM of (itract injected lullVs - Voluit of »ater extracted (il)Us : Height of saiple extracted (glVt - Volute of total extract l u l l
Vs - 1000 or Hs = Vt = 10000 Vi = 3.0
Fori I
4184 30087
Name CTC/ToxLicon
e No
Organics Analysis Data Sheet(Page 4)
S»mple Number
Tentatively Identified Compounds
CASNumbw Compound N«m« Fraction
Ettirrva1*d
1..
UIOIC 5111/lJtC SI?
/ 1/ I
16..
»-
12
NFA denotes no fraction analyzedNCF denotes no compound foundUnk denotes unknownmw denotes probable molecular weight
4184 3C088
H
LABORATORY NAME: ETC/TOXICON
LAt SAMPLE ID NO: 4184-188SAMPLE MATRIX: WATER
DATA RELEASE AUTHORIZED BY
4184
4184
OftGANICS ANALYSIS DATA SHEET
(PAGE 1)
CASE NO:
8C REPORT NO:
CONTRACT NO:
OATE SAMPLE RECEIVED:
VOLATILE COMPOUNDS
•9/29/87
CONCENTRATION: LOUOATE EXTRACTED/PREPARED.
OATE ANALYZED: 18/03/87
CONC/OIL FACTOR: i.
PERCENT MOISTURE: (NOT DECANTED)
PH
CAS NUMBER
74-87-3 CHLOROMETHANE
74-83-9 BROMOHETHANE7S-81-4 VINYL CHLORIDE75-88-3 CHLOROETHANE
7S-89-2 METHYLENE CHLORIDE . . .
47-44-1 ACETONE
75-15-8 CARBON OISULFIOE . . . .
7S-3S-4 i.1-OICHLOROETHENE . . .
7S-3S-J 1.I-DICHLOROETHANE . . .
154-48-5 TRANS-1.2-OICHLOROETHEME
47-44-3 CHLOROFORM
l«7-«4-2 1,2-DICHLOROETHANE . . .
78-93-3 2-kUTANONC
71-55-4 1. I. 1-TRICHLOROETHANE .
54-23-5 CARBON TETKACHLORIOC . .l»B-»S-4 VINYL ACETATE7S-27-4 BROMOOICHLOROMETHANE . .
IK
14
14
14
14
i
14
1
1
i/L
> U
> U
» U
> U
L J
» U
U
U
U
U
U
U
jfoU
U
» U
1 U
CAS NUMBER
78-87-5
18841-82-4
79-81-4
124-48-1
79-88-5
71-43-2
18841-81-5118-75-8
7S-25-2
188-18-1
591-78-4
127-1B-4
79-34-S
188-88-3
188-98-7
188-41-4
188-42-5
UG/L1,2-OICHLOROPROPANE . . .
TRANS-1,3-OICHLOROPROENt .
TRICHLOROCTHENEOIBROMOCHLOROMETHANE . . .
1.1.2-TRICHLOROETHANE . .
BENZENE
CIS-1,3-DICHCOROPROPENE .2-CHLOROETHYLVINYLETHER .
8MOHOFOMH
4-t4ETHYL-2-PENTANONe . . .
2-HEXANONETETRACHLOROETHENE . . . .
1.1.2.2-TETRACHLOROETHANE
TOLUENE
CHLOMOBENZENE
ETHYL BENZENE
STYRENETOTAL XYLENES
18
S!•18S18
UUUUUUUUUUUUUUUUUU
8 - COMPOUND WAS DETECTED IN THE 8C BLANK.
J - REPORTED VALUE IS LESS THAN THE DETECTION LIMIT.
U - COMPOUND ANALYZED FOR BUT NOT DETECTED. THE REPORTEDVALUE IS THE MINIMUM ATTAINABLE DETECTION LIMIT FOR
THE SAMPLE.
SEE PAGE 1A FOR COMPLETE DEFINITIONS OF THE DATAREPORTING 8UALIFIERS.
FORM I
4 1 8 4 3 0 5 0 2
Labora to ry Name: ETC/To»icon
Case No: 4184
Sample Number
Organics Analysis Data Sheet
CAS Number
67-63-0
71-36-3
78-92-2
Compound Name
Isopropyl Alcohol
N-Butyl Alcohol
sec-Butyl Alcohol
Concentrationat/L
300U
200U
200U
U Indira*** ryunpounj yg rulymf fry *•'* "<* **«rtrf- *q*»* ft"* minimnm (toeeriftn liiqtt fnr the «mplg with Ae U(e.g. 10U) bised on necessary conce&tntioo/dilntkja action. (This is not necessarily the instrument detection limit)The footnote ttould read: U-Compound was analyzed for but not detected. The number is the minimum atninibiedetection Emit for the ample,
"I *«n'm«t*H vfhifi Thtf fl«f It nttnl rifafr mtv-ti tim«rin£ « n.kfiHi Jlvai fnr b-ntafivriy Mgnrifiad eompoundlwhere a 1: 1 response is •««"""*< or when the mas* spectral data !»««'•»**«< me presence of a compound that meets the identi-ffcation criteria but the resnltb less man the jpedfied detection limit but greater than rero (e . 1QJ). If limit of detection is10 (if/L and a concentration of 3 n</L is calculated, report at 3J.
4 1 8 4 3 0 5 0 3
Case No
Organics Analysis Data Sheet
(Page 2)
Semivolatile Compounds
Sample N
Coi-Kentranon: U-O" ) Medium (Circle One)
)ate Extracted'Prepared
Jate Analyzed
Conc/Dil Factor
GPC Cleanup DYes QNo
CASNumber
10 \ t > } % 7
\r* 'n*eAnt*d)
ug/lorug/Kg(Circle One)
tienol
<s< • 2 -ChloroethyHEther
-Chloropnenol
. 3-Dtchlorobenzene
. 4-Dtcnlorobenzene
ienzyl Alcohol
. 2-Dichlorooerutnt
-Methylphenol
is(2 -cnloroisopropyOCtner
•Methytpnenoi
l-Nitroso-D«-n-Propytam«ne
(exacMoroethant
(itrobenztne(opnoron*
•Nhrgphenot
.. 4-Dimethy{pn*nol
lenzoic Acid
><s<-2-Ch<oroetnoxYlM«itujne
. 4-Dichlorophenol
. 2, 4-TrichkxoberueneNaphtha t«f>«
l-ChloroaiMline
He tachlorobutadtenc
l-Chloro-3-Methylpnenolt -M«tt\v4naphth«lent
4e xacMorocvclopentadient
I. 4. 6-Trichloropnenol
J. 4. S-Tochforopneno!
! -Chloronaphthalene
!-NitroanilineDimethyl Phthalite
B£Cnaphthy1«r>e
lOu./DM10 uIn,*.10k/Of^//o<-/Aw.lOu1$IDulOulOuIQl
mi*lyi.^(4
IDlA.
IQi*
ID*
I/)U
lOlt.{Dtfi-\u*-tOlA.
ftulf)lA
56*1lOu.
Continuous Liquid • Liquid Extraction QYes
CAS ug/lorug/KgNumber (Circle One3-32-9
1-28-5
00-02-7
32-649
21-14-2
606-20-2
84-66-2
7005-72-306-73-7
00-01-6
534-52-1
86-30-6
01-55-3118-74-1
8746-5
85-01-6
120-12-7
84-74-2
206-44-0
129-00-0J5^87
M-94-1
>6-553
117-81-7 1
218-01-9
117-84-0
20599-2
207-08-9
>0-32-8
193 395
53-70-3
191-24-2
Aceaiphtheoe
!. 4-Dinhrophenol
4-NilropSenolJibenzofuran
2.4-Oinitroiolu«ne
t. £-Oinhroto<uene
Oiethytphthalate
4-Chloropnenyl-phenytethef
Fluor ene
4-Nhroanifine
4. 6-Oinhro-2-Wethy1pnenol
N-Nrtrosodiphenytamine (1 )
4-Bromopheny<-pheny(ether
Kexachlorobenzent
'entachlorophe not
Phenanthrene
AnthnKene
Di-n-ButytphthalateFluoranrnene
PyreneBurytt>«azy{phtKalate
3. 3'-DtcMoraberuid<ne
Benn(t>Anthr*cene
t>n(2-Ethy(h«Ky<)Pmhalate
ChryMne
Oi-n-Octyt Pntnalate
Berujofrfluoranthene
Beniotli)Fluoranth«ne
B«nzo(a)Pyrene
InderxXL 2. 3-cd)P¥'«n«Otbenfli hlAnihcacene8enio(g. h. i)Perylene
IVK.$4**>4u
//Ok(fluin*./flu(Ot*fO*
3*KS9(4
IV*Mb.
(flu.*>«
Qu(0k
Qu
hulQh -JOu
Jeu/OU.Iflu
]QlA.
lOu.(Hlr
lO1^
ID1*'
/fl^n)tIn*. .
4 1 6 4
,,-: Sc.
Analysis Data S'leet(Paqe 3]Peshudes/PCBs
!Lo«] Nediui (Circle one) Bc: Ciei-ur ves [«}-1oCi'f E»ti-ac>.e:;s'e;a''e(i: 29-Sep-fl7 Separator-, "uirel Extraction VesSite a-a!,:ei: C?-Dct-B7 Crrti-u:.Conr/Dil Factor: 1Percent 'ois'-jreideca'ted) NR
CflS [ua'L] or u»/Nuiber
319-B4-6 Alphi-BHC 0.05 U319-B5-7 Beti-BHC 0.05 U319-B6-8 D«lt«-BHC 0.05 U58-69-9 Eana-BHC (Lindanc) 0.05 U76-44-B Keptachlor 0.05 U309-00-2 Aldrin 0.05 U1024-57-3 Keptachlor Epoxide 0.05 U959-9B-B Endosulfan 1 0.05 U60-57-1 Diildrin 0.1 U72-55-9 4,4'-DDE 0.1 U72-20-8 Endrin 0.1 U33213-65-9 Endosulfan II 0.1 U72-54-8 4,4'-DDO 0.1 U1-31-07-8 Endosulfan Sulfatt 0.1 U50-29-3 4,4'-DDT 0.1 U72-43-5 Bethoiychlor 0.5 U53494-70-5 Endrin Kftone 0.1 U57-74-9 Chlordane 0.5 UB001-35-2 Toiapheni 1 U
12674-11-2 Aroclor-lOU 0.5 U11104-28-2 Aroclor-1221 0.5 U11141-16-5 Aroclor-1232 0.5 U53469-21-9 Aroclor-1242 0.5 U12672-29-6 Aroclor-1248 0.5 U11C97-69-1 Aroclor-1254 I l l11C96-82-5 Aroclor-1260 ID
Vi = Volute of extract injected (ul)Vs = VoluH of Hittr eitricted (illUs = Height of sa«ple eitracted (g)Vt = Voluit of total extract (ul)
Vs = 1000 or Ns * Vt = 10000 Vi = 3.0
Fon 1
4184 30505
abo'ato'y Name
e No
Organics Analysis Data Sheet(Page 4)
Sample Numt>e»
Tentatively Identified Compounds
CASNumber Compound N«m« Fnjction
E»tim«t»dtr«tionug/hg)
5.
•..
7..
(3
i::::18.
*9 ._.
77.
NFA denotes no fraction analyzedNCF denotes no compound foundUnk denotes unknownmw denotes probable molecular weight
4 1 8 4 3 0 5 0 6
LABORATORY NAME ETC/TOXICON
LAB SAMPLE XO NO: 4184-92
SAMPLE MATRIX: WATERDATA RELEASE AUTHORIZED BY
ORGANICS ANALYSIS DATA SHEET(PAGE 1)
CASE NO. 4184flC REPORT NO: 4184
v, DATE SAMPLE RECEIVED: 89/29/87
VOLATILE COMPOUNDS
CONCENTRATION: LOWDATE EXTRACTED/PREPARED:DATE ANALYZED: 18/83/87CONC/OIL FACTOR: 1.PERCENT MOISTURE: <NOT DECANTED)
PH
CAS NUMBER74-17-374-83-975-81-475-88-375-89-247-44-175-15-875-35-475-35-3156-48-547-44-1187-84-271-93-371-55-4S4-23-S188-85-475-27-4
CHLOROMETHANEBROMOMETHANCVINYL CHLORIDECHLOROETHANEHETHYLENE CHLORIDE . . . .ACETONECARBON DISULFIOE1.1-DICHLOROETHENE . . . .1. t-OICHLOROETHANE . . . .TRANS-l-2-OICHLOROETHENE .CHLOROFORM1,2-OICHLOROETHANE . . . .2-BUTANONE1. 1. 1-TRICHLOROETHANE . .CARBON TETRACHLORIOE . . .VINYL ACETATEBROMOOICHLOROMETHANC . . .
UG/L18 U18 U18 U18 U5 U74
1
UUUUUU
*>UU
18 US U
CAS NUMBER71-17-518*41-82-479-81-4124-41-179-88-571-43-218841-81-5118-75-175-25-2188-18-1591-71-4127-11-479-34-S188-18-3188-98-7188-41-4188-42-5
UG/L1,2-OICHLOROPROPANE . . .TRANS-1, 3-OICHLOROPROENC .TRICMLOROETHENEOIBROMOCHLOROMETHANE . . .1. 1. 2-TRICHLOROETHANE . .BENZENECIS-1.3-OICHLOROPROPENE .2-CHLOROETHYLVINYLETHE* .BROMOFORM4-METHYL-2-PENTANONE . . .2-HEXANONCTETRACHLOROETHEME . . . .1. 1.2.2-TETRACHLOROETHANETOLUENECHLOROBENZENEETHYLBENZENESTYRENETOTAL XYLENES
S18
UUUUUUUUUUUUUUUUUU
8 - COMPOUND WAS DETECTED IN THE «C BLANK.
U - COMPOUND ANALYZED FOR BUT NOT DETECTED. THE REPORTEDVALUE IS THE MINIMUM ATTAINABLE DETECTION LIMIT FOR
THE SAMPLE.
SEE PAGE 1A FOR COMPLETE DEFINITIONS OF THE DATAREPORTING 9.UALIFIERS.
FORM I
4 1 8 4 3 0 1 4 5
Laboratory Name: ETC/Toxicon
Case No: 4184
Sample Number
Organics Analysis Data Sheet
CAS Number
67-63-0
71-36-3
78-92-2
Compound Name
Isopropyl Alcohol
N-Butyl Alcohol
sec-Butyl Alcohol
Concentrationm/L
300U
200U
200U
U Tt>Mw-«f>^ compound was analyzed for but not tfrtTT*^- Report the minirnnm detection limit for tbe sample with tbe U(e.t> 10U) based on necessary concauratioo/dilution action. (This is not necessarily die instrument detection limit)The footnote should read: U-Gompound was analyzed for but not detected. Tbe number is the minimum attainabledetection i»mh for the *a*if^
J Ttirlirjfr!* an Mrim«t»rt vain* Thh fl«« U MM< ritVr m^ien Mfimaring « concgntrarinn for tentarivdy ktenrifiad compoondtwhere a 1:1 re^ncmjf is assumed or wheo me *"••• iueclJil <*•*• iiv<ir«t<«j the presence of a compound that meets die ideoti-ficatioa oilcria but tbe result bless than the specified detection limit but greaier than zero (e^TlQI). If limit of detection is10 ug/L and a concentration of 3 jig/L is raimiatoii^ report as 31.
4 1 8 4 3 0 1 4 4
Case No: 4184
Organic? Arjlysis Data Sheet(Page 31Peshudes/PCBs
Cor-ceJ-tration: [Lo»] flediui (CircleDate Extracted/Prepared: 29-5ep-B7Date Analyzed: 06-Oct-87Con;/Di! Factor: 1Percent Roisture(decanted) NR
Gf'C Cleans Yes [x]-NoSerarat:ry Funnel titrac'.ior fesContinusus Liquid-Liquid Extrjcticn [s] Yes
CAS [ug/L] or u;/Nuiber
319-84-6 «!ph«-BHC 0.05 U319-85-7 Beta-BHC 0.05 U319-86-fl Oelta-BHC 0.05 U58-89-9 EaiH-BHC (Lindani) 0.05 U74-44-8 HepUchlor 0.05 U309-00-2 ftldrin 0.05 U1024-57-3 Heptachlor Epo«id« . 0.05 U959-98-8 Endosulf»n I 0.05 UiO-57-1 Dieldnn 0.1 U72-55-9 4,4'-DDE 0.1 U72-20-8 Endrin 0.1 U33213-45-9 Endosulf«n II 0.1 U72-54-8 4,4'-DDD 0.1 U1-31-07-8 Endosulfan Sulfjte 0.1 U50-29-3 4,4'-DDT 0.1 U
72-43-5 HtthoiycMor 0.5 U53494-70-5 Endrin Kttoot 0.1 U57-74-9 Chlordani 0.5 UB001-35-2 Toiaphen* 1 U
12674-11-2 flrodor-1016 0.5 U11104-28-2 Aroclor-1221 0.5 U11141-16-5 ftroclor-1232 0.5 U53469-21-9 ftroclor-1242 0.5 Ul?672-29-6 «rcclor-i:48 0.5 U11097-69-1 flroclor-1254 1U11096-82-5 Aroclor-1260 Ill
Vi - VoluM of extract injected (ul)Vs = Voluit of Mter extracted [•!)Us - Keiqht of saiple extracted (q)Vt = Volute of total extract l u l l
Vs = 1000 or N$ Vt = 10000 Vi •- 3.0
For* I
4 1 8 4 3 0 1 4 5
ETC/Toxucon
eNo
Organic* Analysis Data Sheet(Page 4)
ample Numbcf I
X4WU001 I
Tentatively Identified Compounds
ncAsNumber Compound Nam* Frvction Numbw
Ertirrutcd
6"
6..
|..
11:10.
**it /£>
19..
i;:::11
uwk. 3/032
/on ITfStr.-i.oit. lozi 11
tan M90
UlOC I2/15 12.
NFA denotes no fraction analyzedNCF denotes no compound foundUnk denotes unknownmw denotes probable molecular weight
4 1 8 4 3 0 1 4 6
LABORATORY NAME: ETC/TOXICON
LAB SAMPLE 10 NO: 4184-91
SAMPLE MATRIX: WATER
DATA RELEASE AUTHORIZED BY
• 184
4184
OKGANICS ANALYSIS DATA SHEET
<PAGE 1)
CASE NO:
aC REPORT NO:
CONTRACT NO. (
DATE SAMPLE RECEIVED:
VOLATILE COMPOUNDS
•9^23/87
CONCENTRATION: LOW
DATE EXTRACTED/PREPARED:
DATE ANALYZED: l*/*2/fl7
CONC/DIL FACTOR: 1. PH
PERCENT MOISTURE: <NOT DECANTED*
CAS NUMBER74-17-374-83-97S-81-475-88-375-89-247-44-17S-1S-87S-3S-47S-3S-3154-48-k47-44-3187-84-278-93-371-1S-454-23-f188-8S-'47S-27-4
CHLOROHETHANEBROHOHETHANCVINYL CHLORIDECHLOROETHANEHETHYLENE CHLORIDE . . . .ACETONECARBON OISULFIOE1.1-OICHLOROETHEME . . . .i. 1-OICHLOROETHANC . . . .TRANS-1.2-DICHLOROETKENE .CHLOROFORM1,2-OICHLOROETHANE . . . .2-BUTANONE1. 1. l-TRICHLOROETHANE . .CARBON TETRACHLORIOE . . .VINYL ACETATEBROMOOICHLOROMETHANC . . .
U6/L18 U18 U18 U18 Ui U4V
1
UUUUUUUUU
18 US U
CAS NUMBER78-87-S18841-82-479-81-4124-48-179-88 -S71-43-218841-81-S118-7S-87S-25-2188-18-1S91-78-4127-18-479-34-S188-88-3188-98-7188-41-4188-42-5
UG/L
1.2-OICHLOROPROPANE . . .
TRANS-1.3-OICHLOROPROENE .
TRICHLOROETHENE
OIBROMOCHLOROMETHANE . . .
1.1.2-TRICHLOROETHANE . .
BENZENECIS-1,3-OICHLOROPROPENE .
2-CHLOROETHYLVINYLETHER .
BROHOFORH
4-METHYL-2-PENTANONE . . .
2-HEXANONC
TETRACHLOROETHENE . . . .
1.1.2.2-TETRACHLOROETHANE
TOLUENE
CHLOROBENZENE
ETHYLBCNZENE
STYRENE
TOTAL XYLENES
18
S18
1*S
18
UUUUUUUUUUUUUUUUUU
U - COMPOUND ANALYZED FOR BUT NOT DETECTED. THE REPORTED
VALUE IS THE MINIMUM ATTAINABLE DETECTION LIMIT FOR
THE SAHPLE.
SEE PAGE 1A FOR COMPLETE DEFINITIONS OF THE DATA
REPORTING 8UALIFIERS.
FORM I
4 1 8 4 30121
Labora to ry Name: ETC/Toxicon
Case No: 4184
Sample Number
Organics Analysis Data Sheet
CAS Number
67-63-0
71-36-3
78-92-2
Compound Name
Isopropyl Alcohol
N-Butyl Alcohol
sec-Butyl Alcohol
Concentrationut/L
300U
200U
200U
compound wit analyzed for bat not drtpcleiL Report me minimim detection limit for me sample with the U(e.g. 10U) based on necessity concentration/dilution action. (This is not necessarily the instrument detection limit)The footnote should read: U-Compooad was analyzed for but not detected. The number U me minimum attainabledetection limit for the ample.TnrficjtM M >tfim»^ v^hif T^jf flgg <f ny^ ^ftg «*X« i^nnritu • cnnegntnrinn fnr tentatively idgnrified componndawhere a 1:1 response U teamed or when (he mats spectral dati 1**'** me presence of a compound that meets the ideati-ffcatioQcriteria but the result Is less man the specified detection limit but greater than zero (e . IQJ). If limit of detection U10 w/L and a coocentratkc of 3 n^L is calailated, report as M.
4 1 8 4 3 0 1 2 2
LABORATORY NAHECASE NO
ETC/TOX1CON
ORGANICS ANALYSIS DATA SHEET(PAGE 2)
SEHIVOLATILE COMPOUNDS
CONCENTRATION: LOWDATE EXTRACTED/PREPARED: *9/3*/B7DATE ANALYZED: l*/*S/87CONC/DIL FACTOR: i.PERCENT MOISTURE: <DECANTED)
6PC CLEANUP YES X NOSEPARATORY FUNNEL EXTRACTION YESCONTINUOUS LiaUID-LIBUIO EXTRACTION YES
CAS NUMBER
1*8-95-2 PHENOL111-44-4 IIS(2-CHLOROETHYL)ETHER .95-57-8 2-CHLOROPHENOL541-73-1 1,3-OICHLOROBENZENE . . .1*4-44-7 1,4-DICHtOROBENZEWE . . .l**-51-4 BENZYL ALCOHOL9S-S*-1 1.2-OICHLOROBENZENE . . .95-48-7 2-METHYLPHENOL39438-32-9 BIS<2-CHLOROISOPROPYL>ETHER1*6-44-1 4-METHYLPHENOL421-44-7 N-NITROSO-OI-N-PROPYLAHINE47-72-1 HEXACHLOROETHANE98-9S-I NITROBENZENE78-59-1 ISOPHORONEB8-7S-S 2-NITROPHENOL
1*5-47-* 2. 4-OIHETHYLPHENOi. . . . .6S-BS-* BCNZOIC ACID111-91-1 BIS<2-CHLOROETHOXY>HETHANE124-83-2 2.4-OICHLOROPHENOC . . . .129-82-1 1-2.4-TRICHLOROBENZENC . .91-2*-3 NAPHTHALENE1*4-47-8 4-CHLOROANILINE87-48-1 HEXACHLOROBUTAOIENE . . .S9-S*-7 4-CHLORO-3-METHYLPHENOL .91-57-4 2-METHYLNAPHTHALENE . . .77-47-4 HEXACHLOROCYCLOPENTADIENE88-**-2 2.4.4-TRXCHLOROPHENOL . .95-95-4 2,4.5-TRICHLOROPHENOL . .91-58-7 2-CHLORONAPHTHALENE . . .88-74-4 2-NITROAMILINE131-11-3 DIMETHYL PHTHALATE . . . .2*8-96-8 ACENAPHTHWENE99-*9-2 3-NITROANILINE
UG/L
1*
1*i*l*l*i*
l*l*l*l*l*l*l*1*l*l*
S*1*1*1*1*1*1*1*1*1*1*S*1*
S*1*1*I*
U
U
U
U
U
U
U
U
U
U
U
U
U
U
U
U
U
U
U
U
U
U
U
U
U
U
U
U
U
U
U
U
U
CAS NUMBER
•3-32-*
S 1-28-5
l**-*2-7132-44-*
121-14-2
4*4-2*-2
•4-44-2
7**5-72-3
•4-73-7
l**-l*-4534-52-1
•4-3*-4
1*1-55-3
118-74-1
•7-84-S
•$-•!-•
12*-12-7
•4-74-2
2*4-44-*
12*-**-*•1-48-7
*l-»4-l
54-55-3
117-81-7
218-*l-»
117-84-*
2*5-99-2
2*7-*8-9
S*-32-8
193-39-5
53-7*-3
191-24-2
ACENAPHTHENE2,4-OINITROPHENOL . . . .4-NITROPHENOLD1BENZOFURAN2,4-DINITROTOLUENE . . . .2.4-OINITROTOLUENE . . . .
DIETHYLPHTHALATE4-CHLOROPHENYL-PHENYLETHERFLUORENE4-NITROANILINE
4.4-OINITRO-2-METHYLPHENOLN-NXTRO&OOXPHENYLANXNE <1>4-BROMOPHENYL-PHENYLETHERHEXACHLOROBENZENE . . . .PENTACHLOROPHENOL . . . .PHENANTHRENEANTHRACENEOX-N-BUTYLPHTHALATE . . .FLUORANTHENEPYRENCBUTYLBENZYLPHTHALATE . . .3,3'-OICHLOROBENZIOINE . .8ENZO(A)ANTHRACENE . . . .BIS<2-ETHYLHEXYL>PHTHALATECHRYSENEOI-N-OCTYL PHTHALATE . . .•ENZO<B)FLUORANTHENE . . .BENZO<K>FLUORANTHENE . . .BENZO<A>PYRENEINOENOM.2. 3-CD>PYRENE . .DIBENZ(A.H)ANTHRACENE . .•ENZO<G.H, DPERYLENE . . .
UG/L1* U
UUU
5*5*1*1*1*1*1*1*5*S*1*1*1*5*1*1*1*1*1*1*2*1*1*1*1*1*1*1*1*1*1*
UUUUUUUU
UUUUUUUUUUUUUUU
U
UUUU
(!) - CANNOT BE SEPARATED FROM DIPHENYLANXNEFORM I
4184 30123
Case No: (IB*!r:.
Organics analysis Data Sheet
(Page 3)
Pesticides/PCBs
•itf'.f *<wl
ND.5*0*701
[Lo»] Hediui (Circle one)
Date Exacted/Prepared: 29-Sep-8?
Date Analy:ed: Ob-Oct-87
Conc/Dil Factor: 1
Percent M:isture;decanted) NR
6PC Cleanup Yes («]-Ko
Separatory Funnel Eitraction Yes
Continuous Liquid-Liquid Eitractior, [:] Yes
CAS [ug/L] or ug/KqNuiber
319-B4-6 Alph»-BHC 0.05 U319-85-7 BeU-BHC 0.05 U319-96-8 Delt»-BHC 0.05 U58-89-9 6a«a-BHC (Lindini) 0.05 U76-44-8 Heptichlor 0.05 U309-00-2 Aldrin 0.05 U1074-57-3 Htptichlor Epoiide . 0.05 U
959-98-8 Endosulfjn I 0.05 U
60-57-1 Ditldrin 0.1 U
72-55-9 4,4'-DDE 0.1 U
72-20-8 Endrin 0.1 U
33213-65-9 Endosulfan II 0.1 U
72-54-8 4,4'-DDB 0.1 U
1-31-07-8 Endosulfin Sulfttc 0.1 U50-29-3 4,4'-DOT 0.1 U72-43-5 Hethoiychlor 0.5 U53494-70-5 Endrin Ifetone 0.1 U57-74-9 Chlordini 0.5 U8001-35-2 Toiiphenc 1 U12674-11-2 Aroclor-1016 0.5 U11104-28-2 Aroclor-1221 0.5 U11141-16-5 Aroclor-1232 0.5 U51*69-21-9 Aroclor-1242 0.5 U12672-29-6 Aroclor-1248 0.5 U11097-69-1 Aroclor-1254 1U11096-82-5 Aroclor-1260 1 U
Vi = VoluM of extract injected (ul)Vs = Voluie of uter otricttd (•!)Ms - Htiqht of suple eitracted (9)Vt = Vcluie of total ritract (ul)
Vs = 1000 or Us = Vt 10000 Vi * 3.0
Fori I
4 1 8 4 3 0 1 2 4
Laboraiory Name ETC/Toxicon
..NOOrganics Analysis Data Sheet
(Page 4)
Tentatively Identified Compounds
Sample Number
CASNumber Compound NWTM Fraction
Ectim«t«dy*ntT»tion
ug/J or ofl/kg)
i/oAL.
I..
5.
7..
II
W..
33toai n
M65J2L5VO.
!;::= it/o
'*-
in
NFA denotes no fraction analyzedNCF denotes no compound foundUnk denotes unknownnrw denotes probable molecular weight
4 1 8 4 3 0 1 2 5
SAMPLE HUM1CRMDLGU948*!
LABORATORY NAME: ETC/TOXICON
LAB SAMPLE 10 NO: 4184-1*9SAMPLE MATRIX: WATER
DATA RELEASE AUTHORIZED tv.
ORGANICS ANALYSIS DATA SHEET<PAGE 1)
CASE NO:
•C REPORT NO:CONTRACT
41*44184
DATE SAMPLE RECEIVED:
VOLATILE COMPOUNDS
CONCENTRATION: LOUDATE EXTRACTED/PREPARED:DATE ANALYZED: 14)/«S/87COMC/OIL FACTOR: 1.PERCENT MOISTURE: (NOT DECANTED)
CAS NUHVEI
74-S7-3
74-f3-f7i-»l-47S-60-37»-*t-2
47-44-175 -18-07S-3S-47S-3S-J.!S4-4*-S
47-44-)107-44-278-1J-3
71-SS-4
S4-23-Sl«8-«S-47S-27-4
1
CHLOROMETHANE
•ROMOMETHANC
VINYL CHLORIDECHLOROETHANE
METHVLENE CHLORIDE . . . .ACETONECARION OISULFIOC
1. 1-OICHLOROETHENE . . . .
1.1-OICHLOROETHANE . . . .TRANS-1.2-OICHLOROETHENE .CHLOROFORM
1.2-DICHLOROETHANE . . . .2-tUTANONE1. 1. 1-TRICHLOROETHANE . .
CARION TETRACHLORIOE . . .VINYL ACETATE•ROMODXCHLONOMETHANE . . .
uc111414141
14
1
1
i/L• U> U> U» UI U» U
UUUUUUUUU
1 Ui U
CAS NUHtER
71-D7-S!M41-«2-47f~4»l-A
124-4S-17f-0»-§
71-43-21««41-«1-S110-7S-*
7I-2S-21M-1«-1Sfl-71-4127-11-47T-34-J
1M-M-3
1M-M-7l»»-41-4
l«*-42-S
UO/L1.2-DICHLOROPROPANE . . .
TRANS-l.l-OICHLOROPROENC .TRICHLOROCTHENEDliROMOCHLOROMETHANE . . .1.1,2-TRICHLOROETHANE . .•ENZEMCCIS-1,X-OICHLOROPROPENE .
2-CHLOROETHYLVINYLETHER .•ROMOFORH4-METHYL-2-PCNTANONI . . .2-HCXANOf«TETRACH4.0ROETHENC . . . .1,1.2.2-TETRACHLOROETHANETOLUENECHLOROIENZENCETHYLBENZENE
STYRENETOTAL XYLENES
UUUUUUUUUUUUUUUUUU
U - COMPOUND ANALYZED FOR IUT NOT DETECTED. THE REPORTEDVALUE IS THE MINIMUM ATTAINABLE DETECTION LIMIT FORTHE SAMPLE.
SEE PAGE 1A FOR COMPLETE DEFINITIONS OF THE DATA
REPORTING CUALIFIERS.FORM I
4 1 8 4 30520
Laboratory Name: ETC/Toxicon
Case No: 4184
Sample Number
Organics Analysis Data Sheet
CAS Number
67-63-0
71-36-3
78-92-2
Compound Name
Isopropyl Alcohol
N-Butyl Alcohol
sec-Butyl Alcohol
Concentrationut'L
300U
200U
200U
U TnHir^x ft^mpyii^ -^ -f j)y^ fnr t^rt ti« ArtrrtfA P>pn»t ih» minimum A^^tina limit for the tampla wtlh the U
(e.j.lOU) based on oeceisa^ conceatndon/dQntiao actioa. CTbis it not necesurily the imtraman detection limit)The footnote should read: U-Compouad was analyxed for but not detected. The number ii the minimum ttainibledetection limit for the sample.
I Indicates an estimated vatoe. Thii flat bmeddmerittenrtfimaing a concentration for tenadvery identified componndiwhere a 1:1 response is assumed or when me mass spectral data indicated the presence of a oompoond that meets me identi-fication criteria but the result fa le« than the ipecifWd^lectkwli^ 101). If limit of detection isIQpf/Land a concentration of 3ut/Liscalcul«cd.reportasU.
4 1 8 4 3 0 5 2 1
B
LABORATORY NAME:
CASE NO:
ETC/TOXICOH
418ftSAMPLE NUMBER
MDLGWC48*!
ORGANICS ANALYSIS DATA SHEET
<PAGE 2)
SEHXVOLATILE COMPOUNDS
CONCENTRATION: LOW
DATE EXTRACTED/PREPARED: *9/3*/B7DATE ANALYZED: l*/*5/87CONC/OIL FACTOR: 1.PERCENT MOISTURE: (DECANTED)
GPC CLEANUP VE5 X NO
SEPARATOftY FUNNEL EXTRACTION YES
CONTINUOUS LIQUID-LIQUID EXTRACTION YES
CAS NUMiER
1*8-95-2 PHENOL
111-44-4 tIS<2-CHLOROETHYL)ETHER .
95-57-8 2-CHLOROPHENOL
541-73-1 i,3-OXCHLOROBENZENE . . .
1*4-44-7 1,4-OXCHLOROBENZENC . . .
l**-5l-4 IENZVL ALCOHOL
95-S*-l 1,2-DXCHLOROBENZENE . . .
9S-4S-7 2-METHYLPHENOL
39438-32-9 BXS<2-CHLOROXSOPROPYL>ETHER
1*4-44-1 4-METHYLPHENOL
421-44-7 N-NITROSO-OI-N-PROPYLAHINE
47-72-1 HEXACHLOROCTHANE
98-9S-3 NITR01ENZENE
78-59-1 ISOPHORONE
88-7S-* 2-NXTROPHEMOL
1*5-47-9 2.4-OIMETHYLPHEHOL . . . .
45-85-* BENZOXC ACXO
111-91-1 IIS<2-CHLOROETHOXY>METHANE
!2*-83-2 2.4-OICHLOROPHENOL . . . .
12*-82-l 1,2,4-TRXCHLOROBENZENE . .
91-2*-3 NAPHTHALENE
1*4-47-8 4-CHLOROANILINE
•7-41-3 HEXACMLOROBUTAOXENE . . .
S9-5*-7 4-CHLORO-3-P1ETHYLPHENOL .
91-57-4 2-METHYLNAPHTHALENE . . .
77-47-4 HEXACHLOROCYCLOPENTAOIENE
88-*4-2 2. 4. 4-TRICHLOROPHENOL . .
95-95-4 2, 4.S-TRICHLOROPHENOL . .
91-58-7 2-CHLORONAPHTHALENE . .
••-74-4 2-NITROAHILXNE
131-11-3 DIMETHYL PHTHALATE . . . .
2*8-94-8 ACENAPHTHYLENE
99-*9-2 3-NXTROANXLXNE
1*
It
UG/L
1* UUU
UUUUU
1* U1* U
1* U1* U
18 U1* U
1* U
1* U5* U1* U1* U
1* U
1* U1* U18 U
1* U1* U1* U1* U5* U
1* U5* U
1* U1* U5* U
CAS NUMBER
83-32-951-28-5
132-44-9121-14-24*4-2*-284-44-27**5-72-384-73-7
534-52-184-3*-41*1-55-3118-74-187-84-585-*l-812*-12-7
84-74-2
2*4-44-*
85-48-7
91-94-1
54-55-3
117-81-7
218-*l-9
117-84-*
2*5-99-2
297-9B-9
5*-32-8193-39-553-7*-3191-24-2
ACENAPHTHENE
2,4-DINITROPHENOL . . . .
4-NXTROPHENOL
OIBENZOFURAM
2,4-DINITROTOLUENE . . . .
2.4-OXNXTROTOLUENE . . . .
OXETHYLPHTHALATE
4-CHLOROPHENYL-PHENYLETHER
FLUORENE
4-NITROANXLINC
4.4-OXNITRO-2-HETHYLPHENOL
N-NXTROSODXPHENYLAHXNE <1>
4-•ROMO PHENYL-PHENYLETHER
HEXACHLOROBENZENE . . . .
PENTACHLOROPHENOL . . . .
PHENANTHRENE
ANTHRACENE
OI-N-BUTYLPHTHALATE . . .
FLUORANTHENE
PYRENE
BUTYLBENZYLPHTHALATE . . .
3. 3'-OICHLOROBENZIOINE . .
BENZO<A)ANTHRACENE . . . .
BIS < 2-ETHYLHEXYL > PHTHALATE
CHRYSENE
DI-N-OCTYL PHTHALATE . . .
BENZO(B)FLUORANTHENE . . .
BENZO<K)FLUORANTHENE . . .
BENZO(A>PYRENE
XNOENO<1.2.3-CD>PYRENE . .
DIBENZ<A.H)ANTHRACENE . .
SENZOCG.H,I>PERYLENE . . .
1*1*5*I*
UU
UG/L
1* U5* U
%• U1* U1* U1* U1* U
uuuu
1*1*1* U5* U1* U1* U1* U1* U1* U1* U2* U1* U1* U1*1*1*1*1*1*1*1*
<1> - CANNOT BE SEPARATED FROM OXPHENYLAHINEFORM X
9 9
i::
Or;anics Analysis Data(Page 3)Pestindes/PCBs
"cncert'aticn: [In] Rediui (Circle oneiDate f.rtra:'.ed.;Fr?pared: 29-5ep-B7'ate Sra;,:ed: 07-Oct-B7Conc'Dil Factor: 1Fer:eit toistureldecanted) NR
6PC Cleanup Yes [i]-MoSecaratory Funnel Ertractio* YesContinuous Liquid-Liquid Extraction [x] Yes
CAS [ug.'L] or ug/KqNuabcr
319-84-4 Alpha-BHC 0.05 U319-B5-7 Btta-BHC 0.05 U319-B6-B BelU-BHC 0.05 U5B-B9-9 6aMi-BHC (Lindane) 0.05 U76-44-8 Heptachlor 0.05 U309-00-2 Aldrin 0.05 U1024-57-3 HepUchlor Epoxide 0.05 U959-9B-B Endosulfan I 0.05 U60-57-1 Bieldr in 0.1 U72-55-9 4,4'-DDE 0.1 U72-20-8 Endrin 0.1 U33213-65-9 Endosulfan II 0.1 U72-54-8 4,4>-ODD 0.1 U1-31-07-fl Endosulfan Sulfate 0.1 U50-29-3 4,4'-DDT 0.1 U72-43-5 Kethoxychlor 0.5 U53494-70-5 Endrin Keton* 0.1 U57-74-9 CMordane 0.5 U8001-35-2 Touphtne 1 U12674-11-2 Aroclor-1016 0.5 U11104-28-2 Arodor-1221 0.5 U
11141-16-5 Arodor-1232 0.5 U53469-21-9 Aroclor-1242 0.5 U
12672-29-6 Aroclor-1248 0.5 U11097-69-1 firoc'.or-1254 1 U11096-82-5 Aroclor-1260 1 U
Vi : Voluie of extract injected (ul)Vs * VoluH of Mter extracted (illKs - Height of saiple extracted (g)Vt * Volute of total extract (ul)
Vs = 1000 or Ms •- Vt = 10000 Vi = 3.0
fori
4 1 8 4 3 G 5 2 3
"_>f J ' -J' r ^ •
-.*> No
Organics Analysis Data Sheet(Page 4)
Tentatively Identified Compounds
CASCompound Nam* Fraction
(ug/yof ug/kg)
1.2.
J.
4.
6.
9..
110..
ai
14..
rhe..17..
i;§,::20..
!«..12..
'":£W.
29
30
NFA denotes no fraction analyzedNCF denotes no compound foundInk denotes unknownmw denotes probable molecular weight
4 1 8 4 3 0 5 2 4
LABORATORY NAME: ETC/TOXICON
LAB SAMPLE 10 NO: 4184-77
SAMPLE MATRIX: HATERDATA RELEASE AUTHORIZED §Y
ORGANICS ANALYSIS DATA SHEET(PAGE 1>
CASE NO: 4184
BC REPORT NO: 4184CONTRACT NO: O'^ *1DATE SAMPLE RECEIVED.5K*fUs
VOLATILE COMPOUNDS
CONCENTRATION: LOWDATE EXTRACTED/PREPARED.
DATE ANALYZED: i«/*9/87
OIL FACTOR: 5«. •
PERCENT MOISTURE: (NOT DECANTED>PH
CAS NUMBER
74-87-J CHLOROMETHANE74-B3-f BROMOHETHANE
7S-H-4 VINYL CHLORIDE
7S-M-J CHLOROETHANE7S-M-2 HETHYUENE CHLORIDE . . .
47-44-1 ACETONE75-1S-* CARBON DISULFIOE . . . .75-55-4 1.1-OICHLOROETHENE . . .
75-35-3 1.1-OICHLOROETHANE . . .
154-48-S TRANS-1.2-OICHLOROETHCNE47-44-3 CHLOROFORMt«7-«4-2 1.2-OICHLOROETHANE . . .
7«-»3-3 2-8UTANONE71-55-4 i,1.1-TRXCHLOROETHANE .
54-23-5 CARBON TETRACHLORIOE . .l»8-»S-4 VINVL ACETATE75-27-4 BROMOOICHLOROMETHANE . .
UG/L
SM U
U
U
SM U25 • U
SM U
25 • U
25 • U
25 • U
25« U
2S* U
25*
SM
25 •
25 •
SM
25 • U
CAS NUMBER78-87-5 1.2-DICHLOROPROPANE . . .
1M41-42-4 TRANS-1. 3-OICHLOMOPROCNE .
7»-«l-4 TRICHLOROETHENE124-48-1 OIBROMOCHLOROMETHANE . . .
79-««-5 1,1.2-TRICHLOROETHANE . .
71-43-2 BENZENE1*«41-«1-S CIS-1, 3-OICHLOROPROPENE .llt-75-i 2-CHLOROETHYLVINYLETHER .
7S-2S-2 BROMOFORH
1»8-1»-1 4-KETHYL-2-PENTANONE . . .
5*1-78-4 2-HEXANONC127-18-4 TETRACHLOROETHENC . . . .77-34-5 1.1.2.2-TETRACHLOROETHANE1*8-88-3 TOLUENE
l«8-9«-7 CHLOROBENZENEl*«-41-4 ETHYL8ENZENEl»«-«2-S STYRENE
TOTAL XYLENES
UG/L
2St> U2S*
25 •25 •
25 •
254-
25 •
25 •
SM
25*
SM
IS25 •
25*25*
25 •
UUUUUUUUUUUUJU
UUU
J - REPORTED VALUE IS LESS THAN THE DETECTION LIMIT.U - COMPOUND ANALYZED FOR BUT NOT DETECTED. THE REPORTED
.VALUE IS THE MINIMUM ATTAINABLE DETECTION LIMIT FOR
THE SAMPLE.
SEE PAGE 1A FOR COMPLETE DEFINITIONS OF THE DATA
REPORTING BUAL1FIERS.FORM I
4 1 8 4 3 0 2 6 1
Laboratory Name: ETC/Toxicon
Case No: 4184
Sample Number
Organics Analysis Data Sheet
CAS Number
67-63-0
71-36-3
78-92-2
Compound Name
Isopropyl Alcohol
N-Butyl Alcohol
sec-Butyl Alcohol
ConcentrationL.C/L
300U
200U
200U
Tnrtiratflfr compound wa$ analyzed fOf but "** 6ttKlt4L Report tbt tninimntn detection limit for die fatnplg wllb tfaC U(e, j. 10U) based on necessary concentration/dilution action. (Thia is not necessarily the instrument detection limit)The footnote chooki read: U-Compoond wta tnilyred for but not detected. The number is (be minimnm attainabledetection limit for the sample.Infirtff* an yytirmarf vahif Thlt fl«y tf nand rioter wtw-n <»«»Tma»iiig « nnnn<»nfrarinB fnr tMitativriy uJCTtifiad compnnilda
where a 1:1 response is «^"m*«< or wten the mas spectral data iiMratr* the presence of a compound that meets the ideoti-Vtr'nn trlfrii Hit rtr rrmlt h l*itt ftan thf ip^rV^ tfflpr'V^i1itT|h '* fn-xtn Aon ran (g t 1QJ). If limit of detection is10 H«/L and a concentration of 3 ug/L is calculated, report as 3J.
4 1 8 4 3 0 2 6 2
Ca^e NoSfl"ip!e
"oncentrat'On
Date Exifacte<
Date Analyze*
Conc/Dil Fact
Percent Moisi
CASNumber
108 95-2111-44-4
95-57-8
541-73-1
106-46-7
100-51-6
95-50-1
95-48-7
39638-32-9
106-44-5
621-64-7
67-72-1
9895-3
78-59-1
88-75-5
105-67-9
65-85-0
111-91-1
120-83-2
120-82-1
91-20-3
106-47-8
87-683
59-50-7
91-57-6
77-47-4
88-06-295 95-491-58 788 74-4131-11-3
208 96 899-O9 2
(Lov»Tj Medium (Circle One)
•)/Prp.par*»d
1
or-
Lire (Decant*ri)
uQ/lorug/Kg(Circfe On*
Phenol
DiS<-2-Cnforoetrty»)Ether
2-Chlofophenol1. S-Dicnlorobeniena
1 . 4-Dtcnk>robenzene
Benzyl Alcohol
1. 2-DicNorobeniene
2-M«thyfpN*nolbis(2-chlorotSooropv1)Etrwr
4-MethytphenoiN-Nitro«O-0(-n-PropY<«min«
He (jchloroetftant
Nrtrabvruene
IsopNoron*
2-Nivophenol2. 4-Oim«tt>y1pn«nQl
B«ruoic AcidSiftJ ? f*t\t (- , MI. |)L«™w fc-v 'WOcinOKyp"**' fcaiie2. 4-D«hloroph*nol
1. 2. 4-TrichJofobe'ueneNlpnt^«n«
4-Chlofojnilin*
Heuc torobutaditne
4-Chloro-3-Metr«ytph*nol
2-Mettiylnaphthatene
KecacMorocydopentadicna
2. 4. 6-Trichloropt*nol
2. 4. 5-TncMoropNenol
2-C^>lo'onaphthaiene
2-NitrMnitine
0>Ti«fhy( Phtrvilite
Acenaphthylen*
3 N.voan.l.ne
/Ou./{)&10 uIn**10klOk/nt~{hi/L/QulUlA
tfiiilOuIDuic\*.mu/Q*-
toftin\A.lOu.lOu.(dy,
/n±/flulOiAlUtf-lur*/OjA
$euMIA/On.miA
5m
Organics Analysis Data Sheet(Page 2)
Semivolatile Compounds
GPC Cleanup QYes ONo
Separatory Funnel E«traciion QYes
Continuous Liquid • Liquid Extraction QYes
CASNumtw
606-20-2
86-73-7
534.52-1
JS-01-8
3-32-9
1-28-5
00-02-7
32-649
21-14-2
-66-2005-172-3
00-07 •«
6-30-6
01-55-3
18-74-1
7-66-5
20-12-7
W-74-2
206-44X)
29-OOO15-687
11-94-1
>6-55-3
218-01-9
117-84-0
205-99-2
207-08-9
W32-8
19339 5
3703
191-24-2
Acenaphthen*
!. 4-Dirutroph«no<
4-Nitroprtenol)ibenzofuran
:. 4-Qinitroioluerx
0>«thytphth«late
4-CMoroph«nv<-ptony<«th«r
4-Nitroaninn«
og/lofog/Kg(Circto Oo«
Si*
2.£-Oin(troiolu«ne
4. 6-Oinhro-2-M*thylph«(>olN-Nrtr«odip!>er>yUmirv« (1 )
Ptntaehtorophenol
Anthracene
)i-n-Butv<ptiinalaie
Fluoranthcne
3. S'
3enzo(t)Antnracei%e
0>-n-Octy1 Phthalat*
B«nzQ(t»Ftuoranihene8enzo(li|Fluorantr>en«
8«rvro(*)Pyr«ri«
8«nzo(g. h.
lOu.
54 UI/OkHu
SonfOu
JDu
n*
7
4 1 8 4 302^85
A - a ! v s i s O a t a S h el cage :iP e s t i c i d e s / P C B s
"o-'cr'.ri'.i:-: [Lo»] KeJ:ji Circle one! 6PC Cleanup Yes [i]-Ho[it? [-.'.•;:'.;: 'c'?po"i: I'-Sero1 Separator/ Fur.nel Ertraction Yes";•.? «'i',. :E;: !'~-lct-:~ Cor.t;r.jOyS Liq-id-Liq-ii Eitractior. [x] resi:n: [•;! Fac:or: «fer:i-\ PuistLreiiiecar.tei. NR
CAS [ug/L] or ug/Kg
319-84-6 Alphi-BHC 0.25 U319-85-7 BeU-BHC 0.25 U319-86-8 Delti-BHC 0.25 U5E-B9-9 6aiw-BHC (Lindinf) 0.25 U76-44-6 Heptichlor 0.251)309-00-2 Aldrin 0.25 U1024-57-3 HeptacMor Eponde 0.25 U959-98-8 Endosulfin I . 0.25 U60-57-1 Bieidrin 0.5 U72-55-9 4,4'-DDE 0.5 U72-20-8 Endrin 0.5 U33213-65-9 Erdcsulfjn II 0.5 U72-54-8 4,4'-DDD 0.5 U1-31-07-8 Endosulfin Sulfiti 0.5 U50-29-1 4 ,4 ' -DDT 0.5 U72-43-5 Hfthoiychlor 2.5 U53494-70-5 Endrin Ketoni 0.5 U57-74-9 Chlordane 2.5 U8001-35-2 Toupheni 5U12674-11-2 Aroclor-1016 2.5 U11104-28-2 Aroclor-1221 2.5 U11141-16-5 Aroclor-1232 2.5 U53469-21-9 Aroclor-1242 2.5 U12672-29-6 ftrodor-1248 2.5 Ui:C"''-6<'-l f t r c c l o r - 1 2 5 4 5 U11^6-62-5 A r o c l o r - 1 2 6 0 5 U
Vi = Voluw of utrict injected (ul)Vs -- Voluif of vitcr t«trjcted (illMs - Kfight of satple ritrjcted (q)Vt -- Voluw of totil titract (ul)
V5 = 1000 or Ms ' Vt * 50000 Vi = 3.0
fora I
4 1 8 4 3 0 2 6 4
N.imo
No
Organics Analysis Data Sheet(Page 4)
Sample
Tentatively Identified Compounds
CASNumber Compouod Hum* Fraction
Cstirn*t*dH(-»ti<X»ug/Vg)
17
7..
10..
I**..SIH
312/can 60
|,7,
IS..
£:12TL
frUV*
II**2C..
17..
^2_
10 KMT
NFA denotes no fraction analyzedNCF denotes no compound foundUnk denotes unknov/nnrw donotec; probable molecular weight
4 1 8 4 3 0 2 6 5
LABORATORY NAME: ETC/TOXICON
LAI SAMPLE ID NO: 4184-91
SAMPLE MATRIX: MATER
DATA RELEASE AUTHORIZED BY:
oftSANicS ANALYSIS DATA SHEET(PAGE 1>
CASE MO 4184
•C REPORT NO: 4184
o -/ o
DATE SAMPLE RECEIVED: 89/29/87
VOLATILE COMPOUNDS
CONCENTRATION: LOU
DATE EXTRACTED/PREPARED:
DATE ANALYZED:OIL FACTOR: SB. •
PERCENT MOISTURE: <NOT DECANTED)
PM
CAS NUMBER
74-i7-l CHLOROMETHANt
74-iJ-» •ROMOHCTHANC
7S-B1-* VINYL CHLORIDE
7S-*»-l CHLOROETHAMC
7S-«f-2 METHYLEMC CHLORIDE . . .
47-44-1 ACETONE7S-H-* CARiON OISULFIDC . . . .
7S-3S-* 1.1-DICHLDROETHENt . . .
7S-1S-1 1.1-OICHLOROETHANC . . .
1S4-4B-S TRANS-1.2-DXCHLOROETHENC
47-44-1 CHLOROFORM
1B7-B4-2 1.2-OICHLOROETHANC . . .
78-*3-l 2-BUTANOHC
71-SS-* 1.1.1-TRICHLOROETHAME .S4-23-S CARIOM TETRACHLORIOC . .
1M-9S-4 VINYL ACETATC
75-27-4 IftOMOOICHLOROMETHAMC . .
2S*
UG/L
SM U
SM U
SM U
U
U
U
U
U
U
U
U
U
U
2S8 U
25 • U
SM U
2S8 U
2S»
21 •
CAS NUMBER
7I-C7-S 1.2-DICHLOROPROPANl . . .l**41-*2-4 TRANS-t.l-OICHLOROPROENC .
79-tl-4 TRICHLOROCTHENC
12«-4t-l OIIROMOCHLOROMETHAMC . . .
7?-M-S 1.1.2-7RICHLOROETHANE . .
71-43-2 BENZENE
1*«41-*1-S CIS-1,1-OICHLOROPROPENE .
ll»-7$-t 2-CHLOROETHYLVINYLETHER .
7S-2S-2 BROMOFDMH
1*S-1«-1 4-METHYL-2-PENTANONC . . .
SY1-7S-4 2-HCXANONE
127-1B-4 TETRACHLOROETHENC . . . .
79-34-S 1.1.2.2-TETRACHLOROETHANE
148-81-3 TOLUENE .,•"
148-t»-7^ CHLOROtENZENC
i«t-4i-*' 'ETHYLIENZENCl*«-42-S STYRENC
TOTAL XYLENE8
2S*25 •
UG/L
2S8 U2S» U
2SB U
U
U
U
U
SM U
2S8 U
SM U
SM U
2St U
SM U
348
2S« U
25* U
2S* U
21* U
U - COMPOUND ANALYZED FOR BUT NOT DETECTED. THE REPORTED
VALUE IS THE MINIMUM ATTAINABLE DETECTION LIMIT FOR
THE SAMPLE.
SEE PAGE 1A FOR COMPLETE DEFINITIONS OF THE DATA
REPORTING QUALIFIERS.
FORM I I'
Labora tory Name: ETC/Toxicon
Tase No: 4184
Sampl* Number
Organics Analysis Data Sheet
CAS Number
67-63-0
71-36-3
78-92-2
Compound Name
Isopropyl Alcohol
N-Butyl Alcohol
sec-Butyl Alcohol
Concentrationut/L
300U
200U
200U
TnHirat^t compound wts milyttd for but not df*rtpd Report (he minimum detection limit for the sample with the U(e.i. 10U) based on nectnaryccnxntratic^ctfulknactioa. (This U not necessarily the instrument detection limit)The footnote timid re«k U-Q»mpoond WM tnalyzed for but not detected. Tbe mmber is the minimum ttiuubledetection limit for the cample.Indir*t»i «n »pi-mat>rf wflnf. Thk »<f It in** «*«• «**» pfn'mariin m enncgntratioB for temarivdy identified compopndlwbert a Mrecpoiueiiusamedai•««»me mm q>ectnl dan indicated thepraeaceof • compound thai meets die identi-fkation criteria but the remit bless man the specified detection limit bat greater dan rero (04.10J). If limit of detection is10 \ig/L md a concemmion of 3 W/L it ciloilatrt. report as M.
4 1 8 4 3 0 3 0 0
LABORATORY NAME
CASE NO.ETC/TOXICON418*
SAMPLE NUMBEH
ORGANICS ANALVSIS DATA SHEET(PAGE 2)
SEMIVOLATILE COMPOUNDS
CONCENTRATION: LOWDATE EXTRACTED/PREPARED. *9/3*/87DATE ANALYZED: 19/23/07CONC/OIL FACTOR: 1.PERCENT MOISTURE (DECANTED)
GPC CLEANUP VES X NOSEPAftATOftV FUNNEL EXTRACTION YESCONTINUOUS LiaUID-LIBUIO EXTRACTION VES
CAS NUMBER UO/U1*8-95-2 PHENOL 1*111-44-4 BIS<2-CHLOROETHYL)ETHER . 1895-57-8 2-CHLOROPHENOL 1*541-73-1 1.3-OICHLOROBENZENC ... 1*1*4-44-7 1.4-OICHLOROBENZENE ... 19l**-St-4 BENZYL ALCOHOL 1995-58-1 1.2-OICHLOROBENZENE ... 1995-48-7 2-HETHYLPHENOL 1*39438-32-9 BX5<2-CHLOROISOPROPYL)ETHER 1*1*4-44-5 4-METHYLPHENOL 19421-44-7 N-NITROSO-DI-N-PROPYLAMINE 1947-72-1 HEXACHLOROETHANE 1998-95-3 NITROBENZENE 1978-59-1 X50PHOROME 1*88-75-1 2-NITROPHENOC 181*5-47-9 2.4-OIMETHYLPHENOL . . . . 1945-85-4 BENZOIC ACIO 59111-91-1 BIS(2-CHLOROETHOXY)METHANE 1912*-83-2 2.4-OICHLOROPHENOL . . . . 1912*-82-l 1.2.4-TRICHLOROIENZENC . . 1991-29-3 NAPHTHALENE 191*4-47-8 4-CHLOROANILINE 1987-48-3 HEXACHLOROBUTADIENE ... 1959-5*-7 4-CHLORO-3-METHYLPHENOL . 1991-57-4 2-METHYLNAPHTHALENE ... 1977-47-4 HEXACHLOPOCYCLOPENTAOIENE 1988-»4-2 2,4.4-TRICHLOROPHENOL . . 1*9S-95-4 2.4.5-TRICHLOROPHENOL . . 5891-58-7 2-CHLORONAPHTHALENE ... 1988-74-4 2-NITRQANILINE 59131-11-3 DIMETHYL PHTHALATE . . . . 192*8-94-8 ACENAPHTHYLENE 1*99-*9-2 3-NITROANILINE 5*
Uuuuuuuuuuuuuuuuuuuuuuuuuuuuuuuuu
CAS NUMBER83-32-951-28-51*9-92-7132-44-9121-14-24*4-2*-284-44-27*95-72-384-73-7199-19-4534-52-184-39-4191-55-3118-74-187-84-S85-91-8129-12-784-74-2294-44-9129-99-985-48-791-94-154-55-3117-81-7218-*l-9117-84-*2*5-99-22*7-*8-959- 32-8193-39-553-78-3191-24-2
ACENAPHTHENE2. 4-DINITROPHENOL . . . .4-NXTROPHENOLDIBENZOFURAN2. 4-DXNITROTOLUENE . . . .2. 4-OINITROTOLUENE . . . .OIETHYLPHTHALATE4-CHLOROPHENYL-PHENYLETHERFLUORENC4-NXTROANXLINE4. 4-OINITRO-2-HETHYLPHENOLN-NITROSODIPHENYLAHINE <1>4-BROMOPHENYL-PHENYLETHERHEXACHLOROBENZENE . . . .PENTACHLOROPKENOL . . . .PHENANTHRENEANTHRACENEOI-N-BUTYLPHTHALATE . . .FLUORANTHENEPYRENE8UTVL BENZYL PHTHALATE . . .3-3'-DICHLO»OBENZIOINE . .BENZO<A)ANTHRACENE . . . .BIS < 2-ETHYLHEXYL > PHTHALATECHRYSENEDI-N-OCTYL PHTHALATE . . .BENZO(B)FLUCRANTHENE . . .BENZO<K>FLUORANTHENE . . .BENZO<A> PYRENElNDeNO(1.2. 3-CD)PYRENE . .OIBENZ<A.H> ANTHRACENE . .
8ENZO<O.H. DPERYLENE . . .
UG/l1*585*19191*1*1*1*5959191919591*1*19191919291919191*1*1*1*1*1*19
UUU
uuuuuuuuuuuuuuuuuuuuuuuuuuuuu
<1> - CANNOT BE SEPARATED FROM DIPHENYLAHINEFORM I
4 1 8 4 3 0 3 0 1
V=E S;:
3)Pest iudes/PCBs
[Lo«jDate Ext'«tei/»'f; irei!: :9-;ep-6'
Da1.? Ara' . , :ei : C r - 3 c t - E 7
Conc/Di l f a c t o r : 1
Percent r1ois 'ure!decar, ted! Nft
6PC Cleanup Yes [i]-HoBejaratcry Funnel E»tract;on YesCc~t:".Lj:i5 Liqu;i-L!q.id E x t r a c t i o n Ji] Yes
CA3Nuiber
[ug/L] or
319-64-i Alohi-BHC 0.05 U
319-85-7 Beti-BHC 0.05 U
319-86-8 DelU-BHC 0.05 U
58-S9-9 6ana-BHC (Lindant) 0.05 U7t-«4-B Heptjchlor 0.05 U
309-00-2 Aldrin 0,05 U
1024-57-3 Heptachlor Epoiid* 0.05 U959-9B-8 Endosulfjn I . 0.05 U60-57-1 BiiUrin 0. U72-55-9 4,4'-DDE 0. U72-20-8 Endrin 0. U33213-65-9 Endosulfin II 0. U72-54-B 4,4'-DOD 0. U1-31-07-8 Endosulfin Sulfate 0. U50-29-3 4,4'-DDT 0.1 U72-43-5 Methojychlor 0.5 U53494-70-5 Endrin Kftone 0.1 U57-74-9 Chlordine 0.5 U8001-35-2 Toxaphene 1 U12674-11-2 Aroclor-1016 0.5 U11104-28-2 Aroclor-1721 0.5 U11141-16-5 Aroclor-1232 0.5 U?:469-21-9 Aroclor-1242 0.5 U12=72-29-6 Aroc'.or-1248 0.5 U;::."-t=-l »'ocls'--l?54 1 Uli:°6-3:-5 CrocIar-1260 1 U
Vi : Volaie of eitract injected l u l lVs * Volute of »ater extracted (il)(Ts - Veiqdt of sjiple extracted (q)Vt = Voluie of total eitract lull
Vs = 1000 or Us Vt = 10000 Vi * 3.0
For* 1
4 1 8 4 3 0 3 0 2
Laboraio.y Name ETC/Toxj con
Case NoSample Number
Organics Analysis Data Sheet(Page 4)
Tentatively Identified Compounds
CASNumber Compound N«m* Fr»ct*on
E«tim«t*dOC*ntntion
(yfl/yof ug/fcg)
MOP
4.
6.
9..
1O._
m9W3Ly/9/4
15.
16..
17.-
18..
19..
20..
21. -
22..
24..
25..
26..
27..
28..
30..
I/OV /CO
NFA denotes no fraction analyzedNCF denotes no compound foundUnk denotes unknownmu denotes probable molecular weight
4^84 50305
"-"6ES
LABORATORY NAME: ETC/TOXICONLAB SAMPLE 10 NO: 4184-184SAMPLE MATRIX: WATERDATA RELEASE AUTHORIZED BY:
4184
4184
ORGANICS ANALYSIS DATA SHEET<PACE 1)
CASE NO:AC REPORT NO:CONTRACT NO:DATE SAMPLE RECEIVED:
VOLATILE COMPOUNDS
89/29/87
CONCENTRATION. LOWDATE EXTRACTED/PREPARED:DATE ANALYZED: 18/83/87CONC/DIL FACTOR: 1.PERCENT MOISTURE: <NOT DECANTED)
PH
CAS NUHiER
74-87-1 CHLOROMETHANC
74-83-9 BROHOHETHANE
75-81-* VINYL CHLORIDE
75-88-3 CHLOROETHANE
75-89-2 HETHYLENE CHLORIOC . . .
47-44-1 ACETONE7S-1S-8 CARBON OISULFIOE . . . .7S-3S-4 I,l-OICHLOROETHENC . . .7S-3S-3 1.1-DICHLOROCTHANE . . .1S4-48-S TRANS-1.2-OICHLOROETHENE47-44-3 CHLOROFORM187-84-2 1,2-OICMLOROCTHAMC . . .78-93-3 2-BUTANONE71-IS-4 1.1.1-TRICHXOROETHAMC .S4-23-S CARiON TETRACHLORIOE . .188-85-4 VINYL ACETATE71-27-4 BROMOOICHLOROnETHAME . .
UG/L18 U18 U18 U18 U2 J18 U
1
UUUUUU40UU
18 Uf U
CAS NUMBER78-87-S18841-82-479-81-4124-48-179-88-S71-43-21*861-81-5118-71-87S-2S-2188-18-1591-78-*127-18-479-34-S188-88-3188-98-7188-41-4188-42-5
UO/L1.2-OXCHLOROPROPANE . . .TRANS-1. 3-OICHLOROPROENE .TRICHLOROETHENCOIIROMOCHLOROHETHANE . . .1. 1,2-TRZCHLOROETHANC . .BENZENECIS-1.3-OICHLOROPROPENE .2-CHLOROETHYLVINYLETHER .BROMOFORH4-METHYL-2-PENTANONE . . .
2-HEXANONETETRACHLOROETHENE . . . .1.1.2.2-TETRAC HLO ROETHANETOLUENECHLOROBENZENEETHYLBENZENESTYRENETOTAL XYLENES
18t18
18
S18
UUUUUUUUUUUUUJUUUU
• - COMPOUND WAS DETECTED IN THE 8C BLANK.J - REPORTED VALUE IS LESS THAN THE DETECTION LIMIT.U - COMPOUND ANALYZED FOR BUT NOT DETECTED. THE REPORTED
VALUE IS THE MINIMUM ATTAINABLE DETECTION LIMIT FORTHE SAMPLE.
SEE PAGE 1A FOR COMPLETE DEFINITIONS OF THE DATAREPORTING QUALIFIERS.
FORK I
4184 30404
Labora tory Name: ETC/Toxicon
Case No: 4184
Sample Numb«r
Organics Analysis Data Sheet
CAS Number
67-63-0
71-36-3
78-92-2
Compound Name
Isopropyl Alcohol
N-Butjl Alcohol
sec-Butyl Alcohol
ConcentrationHt/L
300U
200U
200U
U Indicates compound was analyzed for but not dftKlfiT Report the minimum detection limit for the i"np>* with the U(e.{. 10U) based on neceaary concentndoo/dOntioa actioa (This is not necessarily the instrument detection limit)The footnote thmiM read: U-Compound was analyzed for but not 4r<»ctfd. The number u the minimum attainabledetection limit fox me sample,
J TndK-^tff m »«rim«t«4 value. This flat 1s used cither when f^timtting a concentration for tentatively identified compoundswhere a 1:1 n»«pn«tf> t* *nm»^ & «&*» (hi» m*^ «p«etni A*t* imtu-^f^ (be presence of a compound that meets the identi-fication criteria but me result is lea than me sfjedfied detectkxi limit but greater flian zero (e^. 101). If limit of detection U10 \if/L and a coocentntkio of 3 tig/L U caloilarcd, report as 3J.
4 1 8 4 3 0 4 0 5
Caie No
Concentration (Low) Medium
Date Exacted 'Prepared L
Date Analyzed (C|6 / fr"?
Cone/Oil Factor
Organics Analysis Data Sh.(Page 2)
Semi volatile Compounds
(Circle One)
iPercent Moisture (Decanted).
CASNumtor
ug/lorug/Kg(CirctoOrw)
108 95-2111-44-4
95 57-8541-73-1106-46-7
100-51-695-50-195-48-7
3963832-9106-44-5621-64-7
67-72-19895-3
76-59-188-75-5105-67-9
65-85-0
111-91-1120-83-2120-82-191-20-3106-47-887-68 35950-791-57-677-47-4
88-06-29595-4
91-58-788-74-4
131-11-320896 B99-09 2
•henol
b«s(- 2 -Chloro«th vHEther2-Chloiophenol1. 3-0«chlorob«nzene
1. 4-DichtorobenteneBenzyl Alcohol1 . 2-0«chloroberuene
2-Mcthyfprwnolbis(2 -Chlofoisooropy1)£lh«r
4-Mclhy<phenotN-Nitro»0-Oi-n-Propy<«mir»e
HeuchforoethancMarobenzencIsopnoron*
2-Nnrophenol2. 4-Dim«thv10h«nolBemoic Acidbis( 2 -Chloro*thory1M«th«n«2. 4-0<hloroph«no(
V 2. 4-Tfich»<xob«'vi«r»eNdpht^t«r»€
4-ChlO'O«nilio«
He «*cM(xobut«Jt«fte
4 -Chlof o-3 Mathylphertol2-M*ttiyl naphthaleneHe K*chlorocyclooent«d«ttnt2. 4. 6-Trichlorophenol
2. 4. 5-Trtch(orOf>Neno(2 -Chlororxaphthal«ne2-Ni(ro«nilir%eDimethyl Phthatate
Acenaphttiylerx3-Nitfoarnline
IGu./flk10 uIn*.10k10k.(nt~inu.iQuIDuiIftulOu[Ou1C*.IfluIQb-
WftIHm.Wi^/Ou.ID*in±lf)H((M(Ot*-\U^/Ok
r*u(Ou
J*M
lOi*.ffilA
5 HA.
GPCC
Sep.v
Con;
CASNumber
83-32-951-28-5100-02-7132-649121-14-2
K06-20-2[84-66-27005-72-386-73-7
100-01-6534-52-186-30-6101-55-3118-74-1
B7-86-585-01-8120-12-7
184-74.2
1206-44-0|l 29 -00-0JBS-687J9 1-94-1
B6-55-31117-81-7
121 8-01 -9111 7-84 -0205-99 2
207 -06 9>0-32 8193 39 553-70 3191-24 :
A^;
-
-
*~,
£ -i
Fl.
f
4
V
t
H;
0.
,-x.
-.
"
•
-
i"
_r
•~
,
(
1:_l
Kg
(1)
Analysis Data SheetIFage I)Pesticides/PCBs
Date Ara'.y:e!J: 07-Oct-B7Conc/Dil Factor:
:-5?:-67
1HP.
6PC Cleanuc Ves [«I-NOSeparatory F-nne! Extraction VesContinuous Liquid-Liquii! Extraction [i] Yts
CAS [ug/L] or ug/KgNdiber
Il«!-B4-i ftlphi-IHC 0.05 U!:'-85-7 Beta-BHC 0.05 U319-B6-B Delta-BHC 0.05 U58-89-9 6)iia-BHC (Undine) 0.05 U76-M-B HepUchlor 0.05 U309-00-2 Aidnn 0.05 U1024-57-3 Heptachlor Epoxidf • 0.05 U959-98-8 Endosulfift I 0.05 U60-57-1 Diildrin 0.1 U72-55-9 4,4'-DDE 0.1 U72-20-8 Endrin 0.1 U33213-65-9 Endosulfin II 0.1 U72-54-6 4,4'-BDJ 0.1 U1-31-07-8 Endosulfm Sulfit* 0.1 U50-29-3 4 ,4 ' -ODT 0.1 U72-43-5 Hethoxrchlor 0.5 U53494-70-5 Endrin Keton* 0.1 U57-74-9 Chlord»n» 0.5 UB001-35-2 Touphtne 1 U12674-11-2 Arodor-1016 0.5 U11104-28-2 Aroclor-1221 0.5 U11141-16-5 Aroclor-1232 0,5 U?:»6"-21-9 Aroc lor -1242 0.5 U1:672-29-6 «roclor-1248 0.51)11097-69-1 Aroclor-1254 ID11096-32-5 Aroclor-1260 1U
Vi = Voluic of titract injected (ul)Vt = Voluie of Mtcr extracted dl)Us = Height of saiple ((traded (g)Vt ; Volute of total ex t rac t (ul)
Vs - 1COO or Us = Vt = 10000 Vi = 3.0
Fort i
4 1 3 4 3 0 4 0 7
Laboiato-y N J " • • _ .
e N o
Organics Analysis Data Sheet(Page 4)
Tentatively Identified Compounds
Sample
CASCornpourwJ NirrM Fraction
Eitirn«l«dtntionog/kfl)
1. MA
B-
1-
0-
51S611
3. • (Ur tJloWt^ Jl-O^C - 13is _s_17..
10
91
r'2C.
27.
30
NFA denotes no fraction analyzedNCF denotes no compound foundUnk denotes unknownmw denotes probable molecular weight
4 1 8 4 3 0 4 0 8
ATTACHMENT B
MASTER DISPOSAL SERVICE LANDFILL
PARTIAL ANALYTICAL DATA PACKAGE
INORGANIC COMPOUNDS AND CONVENTIONAL PARAMETERS
f o r m 1
INORGANIC ANALYSIS UAYA
ETC/Toxicon
|EHA Sample N o . _ J
I " I( /MPt-frvJQ icei (
uate OCT 3 0 1987
so.sow NO. 785
LAb SAMPLE It). NO.
Lab Keceipt Uate
QC REPORT NO.
Elements Identified and Measured
Concentration:
Matrix: Water
Low
Soil
Medium
Sludge Other
Cbncatcatkn FlagDOiJdan Msthad Cbrcentcatknr «g/kg dry weight (Circle One)
r>iii»Hnn Mtthad
1. Aluminum C9tTl
'{.. Antimony H-,0 U
3. Arsenic 0 .3/9 U
4. Barium f/fSl
S. tferylliua /.^W
b. Cadmium f8C/
7. Calcium ^7f/00
«. Chromium f7.3l
V. Cobalt *f.2U
10. Copper TS.tn
11. Iron ^1O
12. Lead /,3 U
A/
A)
— -
£
£
pFF
P
P
?>P
P
p
P
P
p
14.
15.
16.
17.
Ib.
19.
20.
21.
22.
23.
Magnesium 374>00
Manganese 9Z
hsrcury. O.7.U
Nickel f/fl
Potassium bVZO
Selenium A// tJ
Silver .- jZ.Vt/
Sodium 3SVOO
Thalliua #&/£/
Vanadium [&/1
Zinc D 21
ft
A//^
^
P
P
P
P
F
P
P
Fp
E
Precent Solids U)
Cyanide
Footnotes: For reporting results to tPA, standard result qualifiers are used. as defined on Cover Page. Additional flags or footnotes explaining
results are encouraged. Definition of such flags must be explicitand contained on Cover Page, however.
Coaoent/t: Water:ColorationArtifact(s):None
Lab Manager
4184 6C03057/M/Fl/W
Date OCT 3 0 W7
ETC/Toxicon
iMOKCAMC A.'AL'lilS UA'IA SMtt'l
CASt NO.
SOU NO. 785LAb SAMPLE II). NO.
Lab Keccipt liate 7 ' 2.1' &'/
QC REPORT NO.
tlecnents Idencified and Measured
Concent cat ion:
Matr ix : Water
Low
Soil
Medium
Sludge Other
Concentration Fl^> DLLJrim rfethodiag/kg dry weight (Circle One)
H.
U.
1. Aluminum
2. Antimony
J. Arsenic
H. bariun
5. tierylliua
b. Cadmium
7. Calcium
b. Chrooiium
V. Cobalt
10. Copper
11. Iron fao}
12. Lead
P
F
F
P
P
F
P
P
P
p
P
F
17.
Ib.
22.
2J.
Precenc Solids (1)
Cyanide
Magnesium
Manganese
f-tercury
Nickel
Potassiua
Selcniua
Silver
Sodium
Thallium
Vanadium
Zinc
P
P
P
P
F
P
P
F
P
P
Foocnoces: For report ing results to tPA, standard result q u a l i f i e r s arc usedas defined on Cover Pafce. Addit ional flags or footnotes explainingresults are encouraged. Def in i t ion of such f lags must be explicitand contained on Cover Cage, however.
Comoeots: Water :Coloration C oi.oK.Lfa Clarity
Artifact(s):None
THIS 7?fSt/iT SHetT is fo*. IRON
Lab Manager
57 /M/F1 /W
4 1 8 4 6 0 0 6 7
; a-, i
INORGANIC ANALYSIS JMVAETC/Toxicon
\ f - f f , Sample N o .
uate °CT 3 0 1987
CASE: NO.sou NO. 785
UU» SAMPLE ID. NO. - JflZ
Lab Receipt Uace
QC REPORT NO.
Elements Identified and Measured
Concent ration:
Matrix: Water
Low
Soil
Medium
Sludge Other
Qrca *J Hrinn Fl^g DQudai tfettal Oi i vt 11 «Hor> Pl^g TMVi<-lon H^irHr mg/kg dry weight (Circle One)
I. Aluminum Ll^
2. Anciotony U, f f^
3. Arsenic ftffit/
4. Barium f^S]
5. Beryllium f.CU
b. Cadmium ?.&(J
?. Calcium 26>ZOO
«. Chromium Tfc.?!
9. Cobalt <i.2(J
10. Copper ZMi>
11. Iron f^^l
12. Lead A<3 6/
/V
A/
^^
z
pFP
P
P
frP
P
P
P
P
r
1*.
16.
17.
20.
21.
22.
23.
Magnesium 23OOO
Manganese £l3]
Hercury O-2.0
Nickel f/97
Potassium T2S^6\
Selenium I.Jlt/
Silver . ^.^f
Sodium 2.OOOO
Thallium 0.4 /£/
Vanadium /~3.3~1
Zinc r/2l
fit
fit
/Q
Z,
pp
ppF
P
P
F
PP
Precenc Solid* (Z)Cyanide
Footnotes: For reporting results to tPA, standard result qualifiers arc used. as defined on Cover Page. Additional flags or footnotes explaining
results are encouraged. Definition of such flags must be explicitand contained on Cover Page, however.
Comaents: Water:ColorationArtifact(s):Nbne
Lab Manager
4184 6003157/M/Fl/W
Lr'A
Uace OCT 3 0 1987
ANALYSIS IM'IAETC/Toxicon CASK NO.
sou NO. 785LAb SAMPLE 10. NO. 4/8*+ "
Lab Receipt Uace
QC REPORT HO.
~ g7
blements Identif ied and Measured
Concent cation:
Matrix: Uacer
Cyanide
Low
Soil
Medium
SLodge Other
Pag
1 . Aluminum
2. Antimony
1). Arsenic
H. barium
5. terylliuo
6. Cadmium
7. Calcium
6. Chromium
V. Cobalt
10. Copper
11. Iron £J7ff]
12. Lead
P
FF
P
P
F
P
P
P
P
P
F
Obnoenttatiai Flag EdJuticn Vettedng/kg dry ueighc (Circle One)
U.
14.
10.
17.
Ib.
IV.
2u.
21.
22.
23.
Magnesium
Manganese
hercury
Nickel
Potassiuo
Selcniua
Silver
Sodium
Thalliua
Vanadium
Zinc
P
P
P
P
F
P
P
F
P
P
Precent Solids _(_*)_
Foocnoces: For reporting results to tPA, standard result qualifiers arc used. as defined on Cover Page. Additional flags or footnotes explainingresults are encouraged. Uefinitioa of such flags must be explicitadd contained on Cover Cage, however.
Comoents: Water: Coloration ClarityArtifact(s):None
THIS 7?gSl/tT SHetT is fo* J/?OA/
Lab Manager
57/K/Fl/ lv
4 1 8 4 6 0 0 6 S
J L H A b^-p No.
ETC/Toxicon
suu NO. 785
LAb SAMPLE ID. NO.
3Ze/
Date OCT 2 Q 1987
A.«ALY:>IS DA'M 6Ht.fl
CASE NO.
Lab Keccipt Uate
QC REPORT NO.
-f 7
-40
blements Identified and Measured
Concentration:
Matrix: Water
Cbroe
Low
Soil
Medium
Sludge Other
1.
*..
J.
6.
7.
0.
10.
11.
12.
Aluminum
Antimony
Arsenic A
barium
Beryllium
Cadmium
Calcium
Chromium
Co bale
Copper
Iron
Lead V,
T I S6\U,ff(Ji&ffUr/33j
LOU
t-.zolelZOO
SMU¥.2U
E9.Z]L3& '3 U A/
jL%
Z
pFF
P
P
P
P
P
Pp
P
F
Figg niiii-im {feted Cbnoertcatdm Flag rn'ii*-jm tfetfod«£/kg dry weight (Circle One)
U.
14.
I*.
10.
17.
Ib.
21.
22.
23.
Magnesium \~Si]
Manganese L V. Oj
hercury Q. Zl)
Nickel 13 U
Potassium J?6Y000
Selenium I.UU
Silver 2.*+U
Sodium I 95" OOO
Thallium ^.^/^
Vanadium L$«OJ
Zinc T9. 57
NV ^
^
pp
ppF
P
P
F
PP
Precenc Solids (2)
Cyanide
Footnotes: For reporting results to tPA, standard result qual i f iers arc usedas defined on Cover Pa&e. Additional flags or footnotes explainingresults are encouraged. Definition of such flags must 'be explicitand contained on Cover Page, however.
Water:ColorationArtifact(s):None
Lab Manager
4 1 8 4 6 C 0 3 85 7 / M / F l / W /
I Lr'A '. in t> ].- s > . |
Date OCT 3 0 1987
INORGANIC A-tALtsis UA'IA sutt'i
ETC/Toxicon CASK NO.
sow NO. 785
LAb SAMPLE 10. NO. 418 I' HQ_
Lab Keccipt Uace
QC REPORT NO.
tletnents Ident i f ied and Measured
Concentration:
Matrix: Water
Lou
Soil
Medium
Sludge Other
Gbncentcaticn Flag KJuticn hfethod OoncBntiatianXjg/lXor rag/leg dry weight (Circle Oa«)
Dilnrim
1 . Aluminum
2. Antimony
J. Arsenic
H. Barium
5. beryllluo
to. Cadmium
7. Calcium
(5. Chromium
9. Cobalt
10. Copper
11. Iron ££#!
12. Lead
P
F
F
P
P
F
P
P
p
P
P
r
16.
17.
16.
IV.
20.
21.
22.
Magnesium
Manganese
hercury
Nickel
Potassiuo
Selcniua
Silver
Sodium
Thallium
Vanadium
Zinc
P
P
P
P
F
P
P
F
P
P
Precenc Solids (2)
Cyanide
Footnotes: For report ing results to tPA, standard result qua l i f i e r s arc used. as defined on Cover Page. Additional flags or footnotes explaining
results are encouraged. Definit ion of such flags muse be explicitand contained on Cover Page, however.
«: Water:Coloration CoLo/tLess Clarity CLEARArtifact(s):None
THIS 'RESULT SHetT is fo* D/ssoivfP XRou OtiLY .
Lab Manager
5 7 / M / F l / W
4 1 8 4 6 0 0 7 5
^ o r r. I
INORGANIC ANALYSIS UA'IA
ETC/Toxicon
Sample No.
uate OCT 3 0 1987
CASE NO.
785sou NO.LAb SAMPLE ID. NO.
Lab Keceipt liate <?-2<?-g7
QC REPORT NO.
Elements Identified and Measured
Concentration:
Matrix: Water
Low
Soil
Median
Sludfce Other
1.'L.
3.
M .
5.
6.
7.
«.
10.
L I .
12.
Aluminum
Antimony
Arsenic t
Barium
Beryllium
Cadmium
Calcium
Chromium
Cobalt
Copper
Iron
Lead /.
r\is~]&.6U
HflI.OU
8.ZIS300O
lS
Ciulrs.n
IZZOO
tu
A/
A/
%,x
J$
pF
F
P
P/p
P
P
P
P
P
F
g / o r ing/kg dry weight (Circle One)
13.
14.
it).
L7.
Ib.
19.
21.
22.
23.
Precent Solids (I)
Cyanide
Magnesium I2.(,000
Manganese 2. 1^
ftercury O.7.0
Nickel ;3?
Potassium (o^30O
Selenium /,/ft/
Silver 2.^1)
Sodium 2Z100O
Tha 1 1 ium 0. *?/ L/
Vanadium (".231
Zinc 22
A/A/
/£?
/^
^
P
P
P
P
F
P
P
F
PE
Footnotes: For reporting results to tPA, standard result qual i f iers arc used. as defined on Cover Page. Additional f lags or footnotes explaining
results are encouraged. Definition of such flags must be explicitand contained on Cover Page, however.
Comoentc: Water : Coloration ClarityArtifact(s):None
Lab Manager
4 1 8 4 6 C 0 2 45 7 / M / F l / W
Uate OCT 3 0 1<W7
LAK
SOU NO.
ETC/Toxicon
IMORCAMO A N A L Y S I S UA'lA ilit.fl
CASt NO.
785
LAb SAMPLt ID. NO. - 95*
Lab Keccipt Uate
0^; REPORT NO.
Elements Identified and Measured
Concentration:
Matrix: Water
Cyanide
Low
Soil
Medium
Sludge Other
Mttrrf Oonoentratim Flqg DUiAian Msdrdrag/kg dry weight (Circle One)
I . Aluminum
'i. Antimony
J. Arsenic
H. barium
5. beryllium
b. Cadmium
7. Calcium
b. Chromium
*. Cobalt
10. Copper
11. Iron Ml
12. Lead
P
F
F
P
P
F
P
P
p
P
P
F
14.
13.
10.
17.
lt>.
19.
20.
21.
22.
23.
Magnesium
Manganese
Mercury
Nickel
Potassium
Selenium
Silver
Sodium
Thallium
Vanadium
Zinc
P
P
P
P
F
P
P
F
P
P
Precent Solids (2)
Footnotes: For reporting results to tPA, standard result qualif iers arc used. as defined on Cover Pa&e. Addit ional flags or footnotes explaining
results are encouraged. Def ini t ion of such f lags must be explicitand contained on Cover Cage, however.
Comoents: WaterrColoration LititTBKovJtJ Clarity CLEARArtifact(s):None _
THIS "ResuLT SHctT is fo*. "5/ssotvtD J^o/v
Lab Manager
57/M/F1/W
4 1 8 4 6 0 0 6 1
Korm 1
ANALYSIS IMVA
LAt
sou no
ETC/Toxicon
Sample No.
uace OCT 3 0 1987
CASE NO.785
LAb SAMPLE ID. NO.
Lab Receipt tiate 9
QC REPORT NO. V//V
bile men cs Identified and Measured
Concentration:
Matrix: Water
Low
Soil
HediuB
Sludge Other
uimi-fnnm
1. Aluminum frl^f]2. Antimony/^. /? L/J
J. Arsenic Oj-,1/)
*-• barium £lOT$
5. Beryllluo /.OU
6. Cadmium */.8U
7. Calciua V34>OO
8. Chroaium £".4U
9. Cobalt V.2U
10. Copper Df.8]
11. Iron T?/7
12. Lead /,$ U
rjagL
^
A/
/v
B iinm jTlNor
2x
2,
2.
"nmrq umDanttanonitg/kg dry weight (Circle One)
p" 13. Magnesium 2. f^flO
F U. Manganese fjfl
F is. Hercury O.7.0
P 16. Nickel C/7l
P 17. PotassiuQr3340l
>F"P 16. Selcniua 1 .& I/
P IV. Silver . 2MU
P 20. Sodlua /380O
p 21. Thalliua 0 ,<f/ U
p 22. Vanadlu« E9.^
P 2J. Zloc fg.O]
nagu
(J
^
iiinm
/^7
^
Ml IXl
P
P
P
P
F
P
P
F
PE
F Precent Solids (I)Cyanide
Footnotes: For reporting results Co tPA, standard result qualifiers arc used. as defined on Cover Page. Additional flags or footnotes explaining
results are encouraged. Definition of such flags must be explicitand contained on Cover Page, however.
Comoeats: Water;ColorationArtifact(s):None
Lab Manager
4 1 8 4 6 C 0 2 S5 7 / K / F l / U
\ t f A j .1 •-., • 1
Uace OCT 3 0 1987
LAK :.A:IL
sou NO.
ETC/Toxlcon
ANALYSIS UAYA SHt.fl
CASK NO.
783LAb SAMPLt 10. NO.
Lab Keccipc Date
QC REPORT NO.
Elements Identified and Measured
Concent cue ion:
Matrix: Water
Low
Soil
Medium
Sludge Other
Conoertrariai Flag Dilirim hfetfrd CbnoerTrarim Flag Dilirim MsthxiXig/L\or ng/kg dry weight (Circle One)
1 . Aluminum
2. Antimony
J. Arsenic
H. barium
5. tierylliua
b. Cadmium
7. Calcium
«. Chromium
<*. Cobalt
10. Copper
tl. Iron £?3l
12. Lead
P
F
F
P
P
F
P
P
p
P
P
F
13.
U.
I*.
16.
17.
Ib.
iy.2u.
21.
22.
2U.
Magnesium
Manganese
hercury
Nickel
Potassiua
Selcniuo
Silver
Sodium
Thallium
Vanadium
Zinc
P
P
P
P
F
P
P
F
P
P
Precent Solids (Z)
Cyanide
Foocnoces: For reporting results to tPA, standard result qualif iers arc used. as defined on Cover Page. Addit ional flags or footnotes explaining
results are encouraged. Definition of such flags must be explicitand contained on Cover Page, however.
Coauae.its: Water: Coloration Coto*lf*s ClarityArtifact(s):None
THIS SHctT iS fo* J/?o/v OtJLY
Lab Manager
57 /M/F l /W
4 1 8 * 6 0 0 6 2
tr'A jaraji !»•
Oate OCT 3 0 1987
I
LAt
SOU NO.
EIC/Toxicon
ANALYSIS U A i A illt.fl
CASE NO.
785
LAb SAMPLE 10. NO.
Lab Kecelpt liate
QC REPORT NO.
tie a>ents Identified and Measured
Concentration:
Matrix: Water
tow
Soil
Medium
Sludge Other
Cbnootzation Fl g DUi±Jm hfethod Cbncentxatim FJflg Dilution£ug/C)or mg/kg dry weight (Circle One)
i.i.3.
H.
5.
to.
7.
(5.
<*.
10.
11.
12.
Aluminum T/ £"67
Antimony /J.J9 0
Arsenic /^
harlum f/907
Beryllium 100
Cadmium 4.8 U
Calcium 380 OQ
Chromium [8. Li
Cobalt T5.27
Copper T7.V7
Iron 3O^7
Lead L3U A/
^
^
^
PFF
P
P
P
P
P
p
P
P
F
13. Magnesium yoS~OO
14. Manganese 2. 1
15. Kercury O-20
lb. Nickel fiZffJ
17. Potasstuo 03lOl
lt>. Selenluo J ,& U
IV. Silver [2.11
2o. Sodium / Z9OO
21. Thallium ^^//y
22. Vanadium T9. 77
23. Zinc f / /7
A/A/
JL*
7^
PP
PPF
P
P
F
PP
Precent Solids (t)
Cyanide
Footnotes: For reporting results to tPA, standard result qua l i f ie r* arc usedas defined on Cover Page. Additional flags or footnotes explaining
' results are encouraged. Definition of sucU flags must"be explicitand contained on Cover Cage, however.
Comoeuts: Water;Coloration ClaritvArtifact(s):None
Lab Manager
4 1 8 4 6 C 0 4 057/M/Fl/W/
Uace OCT 3 0 1987
LAt
SOU NO.
ETC/Toxicon
INOKCAMC Ai iALtSLS UA'iA iHt.E'1
CASE NO.
785
LAb SAMPLE 10. NO. - //Z
Lab Receipt Dace 9 -
QC REPORT NO.
hllements Identified and Measured
DiSS
Concentration:
Matrix: Water
Low
Soil
Medium
Sludge Other
FT^g Dilirim tfethod Cbn
1 . Aluminum
2, Antimony
J. Arsenic
<4 . barium
5. beryllium
6. Cadmium
7. Calcium
H. Chromium
V. Cobalt
10. Copper
11. Iron £$2]
12. Lead
P
F
F
P
P
F
P
P
P
P
P
F
•fixation Flgg Edluticn Ffethaing/kg dry weight (Circle One)
13.
14.
10.
17.
16.
21.
22.
21.
Magnesium
Manganese
hercury
Nickel
Potassium
Selenium
Silver
Sodium
Thallium
Vanadium
Zinc
P
P
P
P
F
P
P
F
P
P
Precent Solids (I)
Cyanide
Foocnoces: For reporting results to tPA, standard result qualifiers arc used. as defined on Cover Pa&e. Additional flags or tootnotes explaining
results are encouraged. Definition of such flags must be explicitand contained on Cover Page, however.
Comoe.\t«: Water: Coloration CoLo*.i-eis Clarity
Artif act (s): None
THIS 7?CSt/t.T SHctT iS fo* "D/sson/fP jT/?Q/v
Lab Manager
57 /M/F1 /W
4 1 8 4 6 0 0 7 7
toro 1
INORGANIC ANALYSIS DATAEDC/Toxicon
( E P A Saople No. |I " I
vJ03(oO< I
^^oate 0 0 7 3 0 1 9 8 7
NO. Ji/il.SOW NO. 785
LAb SAMPLE 10. NO.
Ub Kecelpt Date 9-,29-g?
QC REPORT NO.
Elements Identified and Measured
Coo cent radon:
Matrix: Water
Low
Soil
Medium
Sludge Other
1. Aluminum L^fl
2. Antimony V-OU
3. Arsenic O.^OU1* "
i. Barium l$3J
S. Beryllium 1.00
6. Cadmium 4»8U
7. Calcium dfftfCC
tf. Chromium •5".tfU
9. Cobalt V-.2U
10. Copper TV. 61
11. Iron //^
12. Lead /. 3 U
1
A/
-.,/\/
Mor
2Z
2
mg/kg dry weight (Circle One)
p • 13. Magnesium 2/¥OO
F • 14. Manganese ClO]
F 15. Mercury O.2U
p i6. Nickel r/<riP 17. Potassium TdZOOl
/*P lt>. Selenium / .^U
P 19. Silver J2/fU^
P 2O. Sodium* - IbffGO
p 21. Thallium O-9JU
p 22. Vanadium TV.6]
P 23. Zinc rS8l
p Preceat Solids (Z)
A/
^
10
Z
pp
ppF
P
P
F
PE
Cyanide
Footnotes: For reporting results Co tPA, standard result qualifiers are uced. as defined oo Cover Page. Additional flags or footnotes explaining
results are encouraged. Definition of such flags must be explicitand contained on Cover Page, however.
Consents: Water: Coloration ClarltvArtifact(8):Ndne
4 1 8 4 6 C 0 : 8
Dace OCT 3 0 1987
INORGANIC ANALYSIS DAI A
LAE ETC/Toxicon
NO. 785LAb SAMPLE ID. NO.
CASK NO.
Lab Receipt liate i ~ ~ -
QC R£PORT NO.
Elements Idencified and Measured
1>ISS
Concent ration:
Matrix: Water
Low
Soil
[•tedium
Sludge Other
Grcentratjm Flag rHIm-im hfedtdXig/lNor mg/kg dry weight (Circle One)
Dilitlcn Mstitxl
1. Aluminum
2. Antimony
3. Arsenic
<< . barium
3. tterylliuo
6. Cadmium
7. Calcium
8. Chromium
1. Cobalt
10. Copper
11. Iron f^5l
12. Lead
pF
F
P
P
F
P
P
P
P
P
F
13.
14.
li.
lo.
17.
20.
21.
22.
2J.
Magnesium
Manganese
tercury
Nickel
Potassiua
Selcniua
Sliver
Sodium
Thalllua
Vanadium
Zinc
P
P
P
P
F
P
P
F
P
P
Precenc Solids (Z)
Cyanide
Footnotes: For reporting results Co tPA, standard result qual i f iers arc used. as defined on Cover Pa&e. Addi t ional f lags or footnotes explaining
results are encouraged. Defini t ion of such f lags oust be explicitand contained on Cover Page, however.
Coroeoc*: Water: Coloration C»Lo*Leu. Clarity^Artifact(s):None
THIS 7?fStAT SHeiT is fo* ZRou
Lab Manager
57/M/F1/W
4 1 8 4 6 0 0 6 5
I- u r p.
( E r ' A Sample No. |
I ' I
Oace OCT 2 0 1987
LAfc r
SOU NO
I MORGAN 1C ANALYSIS UA'lA S*
ETC/Toxicon CASE NO.
785
LAb SAMPLE ID. NO.
Lab Ueceipt liace
QC REPORT NO.
Clements Identified and Measured
Concentration:
Matrix: Water
Low
Soil
Medium
Sludge Other
QmaAxaUai Flag DilUJm tfethri OmatxaUm Flag DUitlcn Mattedig/lXor ng/kg dry weight (Circle One)
£ •
2.
3.
5.
6.
7.
».
10.
L I .
12.
p_ -nAluminum L a l J
Antimony fr.ff 0
Arsenic 0 .fo U
Barium f/Ofl
tie ry Ilium /.Of
CadBium 4 8ll
Calcium 29100
Chrooium S-'fl'
Cobalt 4.20
Copper f"3.n
Iron C?tf
Lead /,J ^/
V
A/
^~^
X2,
2,
pFF
PPj*fp
P
Ppp
P
f
13.
U.
13.
16.
17.
Ib.
2u.
21.
22.
23.
Magnesium 23700
Manganese f?.fl
Mercury. O.2.O
Nickel /3U
Potassiua fZ990l
Selenium /// Z/
Silver ... 2.4f
Sodium ILOOO
Thallium 0.4 JtJ
Vanadium £6>.7l
Zinc 4.8U
A///^
jL
PP
PPFP
P
Fp
B
Precenc Solids (I)
Cyanide
Footnotes: For reporting results Co tPA, standard result qualifiers arc usedas defined on Cover Page. Additional flags or footnotes explainingresults are encouraged. Definition of such flags mist be explicitand contained on Cover Vage, however.
Contents:
Artifact(s):None
Lab Manager
4 1 8 4 6002957/M/Fl/W
uace OCT 3 0 1987INORGANIC A N A L Y S I S UAYA 6itt.fi
ETC/Toxicon CASK NO.
SOI. NO. 785
LAb SAMPLE 10. NO. - I
Lab Receipt Date
QC REPORT NO.
tlaments Ident i f ied and Measured
Concentration:
Matrix: Water
Low Medium
Soil Other
fl »•*«• raHm T>i1i<-im M^ttrj Cbmerttatiai Flqg Dili±ian bfethod«g/kg dry weight (Circle One)
1 . Aluminum
2. Antimony
3. Arsenic
H. barium
5. tterylliun
b. Cadmium
7. Calcium
ti . Chromium
V. Cobalt
10. Copper
11. Iron r/5l
12. Lead
p
F
F
P
P
F
P
P
p
P
P
F
Ib.
17.
16.
21.
Magnesium
Manganese
hercury
Nickel
PotassiuD
Seleniuo
Silver
Sodium
Thalliua
Vanadium
Zinc
P
P
P
P
F
P
P
F
P
P
Freceac Solids (2)
Cyanide
Footnotes: For reporting results to tPA, standard result qua l i f i e r s arc used. as defined on Cover Page. Additional flags or footnotes explaining
results are encouraged. Defini t ion of such flags muse be explicitand contained on Cover Cage, however.
Comoeocs: Water: Coloration C.cLoAt.eii ClarityArtif act (s): None
THIS SHctT is fo* DISSOLVCD
Lab Manager
57/M/F1/W
4 1 8 4 6 0 0 6 6
N o .
Uate OCT 3 0 19g/_
LAt ETC/Toxicon
J A.iALYilS UA'lA bhbtl
CASE NO.
NO. 785
LAb SAMPLE 10. NO.
Lab Keceipt Uace
QC REPORT NO.
Concent rat ion:
Matrix: Water
Cbn
t laments Identified and Measured
Low
Soil
Medium
Sludge Other
1. Aluminum / l<?2j
'L. Antimony fa.,01)
3. Arsenic O.^ff U
H. barium ISO]
5. beryllium ).OU
b. Cadmium ^8^
7. Calcium 35^00
b". Chromium /3
y. Cobalt V2U
10. Copper L 6.9j
11. Iron X25"
12. Lead /J(J ^
*.
A/
2_
^
^^^^^
pFF
P
P
P
P
P
pp
P
fCyanide
23.
Magnesium L*f20O]
Manganese C-S-81
Hercury 0. 2.U
Nickel f / f7
Potassium I85OO
Seleniua I ,UU
Sliver 2.*i(J
Sodium 23500
T**l.LiuaS,f/tS
Vanadium T/3l
Zinc T5-9J
A/
/I/
2
^_
P
P
P
P
F
P
P
F
PP
Precenc Solids (Z)
Footnotes: For reporting results to t'PA, standard result qua l i f i e r s arc usedas defined on Cover Page. Additional flags or footnotes explainingresults are encouraged. Definition of such flags must*be explicitand contained on Cover Page, houever.
Comae uts: Water: Coloration <Lttf(L~is ClarityArtifact(s):None
Lab Manager
4 1 8 4 6 C 0 4 157/M/Fl /W/
Lr'A b.inpl
Uace OCT 30 1967
INOKCAMC ANALYSIS UAiA
LAt
SOU NO.
ETC/lexicon CASK NO.
785LAb SAMPLE 10. NO. Lj-/8'+- 113
Lab Kecoipt Date
QC REPORT NO.
tlements Identified and Measured
Concentration:
Matr ix: Water
Low
Soil
Medium
Sludge Other
Goroertzatim Flag Dilnrim hfethod Ocncentratian Flgg QilnHmr rag /kg dry weight (Circle One)
1 . Aluminum
2. Antimony
J. Arsenic
«. barium
5. tserylliun
b. Cadmium
7. Calcium
ti. Chromium
*. Cobalt
10. Copper
H. Iron ll*i]
12. Lead
P
F
F
P
P
F
P
P
p
P
P
F
14.
13.
Ib.
17.
16.
IV.
2u.
21.
22.
Magnesium
Manganese
hercury
Nickel
Potassium
Selenium
Silver
Sodium
Thallium
Vanadium
Zinc
P
P
P
P
F
P
P
F
P
P
Freoent Solids (I)
Cyanide
Footnotes: For reporting results to KPA, standard result qualif iers arc usedas defined on Cover Pa&e. Additional flags or footnotes explainingresults are encouraged. Defini t ion of such flags must be explicitand contained on Cover fage, however.
Comoents: Water rColoration C.oi.t*.<.es± Claritv CLEARArtifact(s):None
THIS 7?fSiAT SA/wT is fo* T>/ssotvep .!/?<
iLab Manager
3A/ ^LY
P**iUN
t
1
ft}M^u\ jL-
' ^V)
57 /M/F1 /W
4 1 8 4 6 0 0 7 8
(Et'A Sample No.
LAU :.AME
SOW NO.
uate 30 1987
EIC/Toxlcon
INORGANIC ANALYSIS UA'lA SHtEl
CASE NO.
JZ85LAB SAMPLE ID. NO. - I O.3
Lab Kecelpt liate
0^: REPORT NO. <
blemencs Identified and Measured
Concent ration:
Matrix: Water
Low
Soil
Median
Sludge Other
Qxcertzadan Flag ULjdon Fbthod Oanoatratim FlfgIg/C^or ng/kg dry wight (Circle One)
1. Aluminum ["| ill
*. Antimony tl-ff U
J. Arsenic O.^ffU
H. Barium f/O3l
S. tterylllua 1. 00
b. Cadmium if-.gO
7. Calcium U2SOO
8. Chromium 5.4U
9. Cobalt +.2U
10. Copper &>.8l
11. Iron ftofl
12. Lead /, 3 U
^
ft
2.ZL
2,
ppF
P
P
/'P
P
P
P
P
F Precent Solids (I)
Cyanide
13. Magnesium 3IZOO
U. Manganese f/Oj
15. hercury O. 2 J
16. Nickel LZ£]
17. Potass luofv^/d
Ib. Selenium l.i+U
19. Silver . Z.^U
2u. Sodium /<?OOO
21. ThallluaZf ^//y
22. Vanadium 0?.?]
23. Zinc &Z
A//^ ^
^
pp
pppppppp
Footnotes: For reporting results to tPA, standard result qualifiers arc used. as defined on Cover Page. Additional flags or footnotes explaining
results are encouraged. Definition of such flags must be explicitand contained on Cover Cage, however.
WaterrColorationJuTtifact(s):Kone
Lab Manager
4184 6003257/M/Fl/W
uace OCT 3 0 1987
LAK
SOU f-O.
ETC/Toxicon
INOKCANIC A N A L Y S I S UA'iA Slttt'i
CASE NO.
785
LAb SAMPLE 10. NO. - I O3
Lab teccipt Date
QC REPORT NO.
tleoents Ident i f ied and Measured
Concentration:
Matr ix: Water
Low
Soil
Medium
Sludge Other
Cbnoentran'm Flag Dilirion tfethod Ctancenrrarim Flgg DOuticn tfethcdwg/kg dry weight (Circle One)
U.
14.
I . Aluminum
2. Antimony
J. Arsenic
A. barium
5. tterylliua
b. Cadmium
7. Calcium
ti. Chromium
9. Cobalt
10. Copper
11. Iron /"/ft! 1
12. Lead
P
F
F
P
P
F
P
P
P
P
P
F
It).
17.
16.
iy.2u.
21.
22.
Magnesium
Manganese
tercury
Nickel
Potassium
Selenium
Silver
Sodium
Thallium
Vanadium
Zinc
P
P
P
P
F
P
P
F
P
P
Precent Solids
Cyanide
Footnotes: For reporting results to tPA, s t andard result qua l i f i e r s arc used. as defined on Cover Page. A d d i t i o n a l f lags or footnotes explaining
results are encouraged. Defini t ion of such f lags must be explicitand contained on Cover Page, however.
Concents: Water :Coloration CouAUr*i Clarity r^ / f~ & &f_ *• C f t f \
Artifact(s):None
THIS -Resucr SHetT IS fo*. "D/SSOLV£D ZRON OfJLY
»-Lab Manaxe r ^dlJwu»v irfjU^^ L
5 7 / M / F 1 / W
4 1 8 4 6 0 0 6 9
li.itr.ple NO.
uate OCT 3 0 1987INORGANIC A.»AL*:>tb UA'IA
LAfc
sou
LAb SAMPLE ID. NO.
ETC/Toxicon CASE NO.
785- III
Lab Receipt Uace
QC REPORT NO.
Concentration:
Matrix: Water x
(rnpHBHtflCfl
1. Aluminum f/731
2. Antimony &.0 (J
3. Arsenic^. *f£U
•«. Barium £/&<2j
5. beryllium /.£>U
6. Cadmium </.#U
7. Calcium ?0?0O
«. Chromium f6.3"I
S». Cobalt 4.20
10. Copper f7.JZ"J
11. Iron /<?80 '
12. Lead 1,3 U
Elements Identified and Measured
Low Medium
Soil Sludge
Flag Dilution Mated Cbrcentxatian^gT^or mg/kg dry weight (Circle One)
1 p 13. Magnesium 37ZOG
b
A/
2.ZL
3s
F 14. Manganese 65
F It), tercury O-2U
P 16. Nickel r25j
P 17. Potassiua/JyjZO/
P 16. Selenium I.U-U
P IV. Silver 2.^11
P 20. Sodium 3370O
p 21. Thallium 0 .&/ (/
P 22. Vanadium D£~]
P 23. Zinc 19, 77
Other
FlflgO
y
A/
itfrj-lm
&
2__
fc£**l_nsui
ppppF
P
P
Fp
P
F Precent Solids (1)
Cyanide
Footnotes: For reporting results to tPA, standard result quali tiers arc usedas defined on Cover Page. Additional flags or footnotes explainingresults are encouraged. Uefinition of such flags must'be explicitand contained on Cover Cage, however.
Comoent*: Water; Coloration ClarityArtifact(s):None
Lab Manager
4 1 8 4 6 C 0 3 957/M/Fl/W/
Date OCT 3 0 1987
INORGANIC A ^ A L Y ^ I S UA'IA
ETTC/Toxicon CASE NO.
SOU NO. 785
LAb SAMPLE ID. NO. ~ HI
Lab Keccipt bate
QC REPORT NO.
Elements Identified and Measured
Concentration:
Matrix: Water
Low
Soil
Medium
Sludge Other
Cbnffif tf'i.ftf^on
I. Aluminum
2. Antimony
3. Arsenic
H. bariujo
S. beryllium
6. Cadmium
7. Calciun
tt. Chromium
V. Cobalt
10. Copper
11. Iron T5#]
12. Lead
P
F
F
P
P
F
P
P
P
P
P
F
Dili rim tfethodfg/L^or mg/kg dry weight (Circle One)
13.
Flag Eh"ii<-inn {fatted
li.
lb.
17.
lb.
iy.20.
21.
22.
23.
Magnesium
Manganese
hercury
Nickel
Potassium
Selcniua
Silver
Sodium
Thallium
Vanadium
Zinc
P
P
P
P
F
P
P
F
P
P
Precent Solids (Z)
Cyanide
Foocnoces: For reporting results to tPA, standard result qualifiers arc used. as defined on Cover Pa^e. Addi t iona l f lags or footnotes explaining
results are encouraged. Definition of such f lags must be explicitand contained on Cover Page, however.
Water:Coloration C.t>Lod(.es& ClarityArtifact(s):None
THIS T?£SuCT SHetT is fo* T>is<>oLveD IRON OfJLY
Lab Manager
57/M/Fi/ ; ;
4 1 8 4 6 0 0 7 6
l-ot m
| EPA Sample No.
Uate OCT 3 0 1967
ETC/Toxicon
INORGANIC ANALYSIS UA'lA SHfcE'l
CASE NO.
NO. 785
LAb SAMPLE ID. NO.
Lab Keccipc Dace
QC REPORT NO.
Klemencs Identified and Measured
Concent radon:
Matrix: Water
Low
Soil
Medium
Sludge Other
1.
3.
M .
5.
6.
7.
8.
10.
11.
12.
Aluminum
Antimony
Arsenic 6
barium
beryllium
Cadmium
Calcium
Chromium
Co bale
Copper
Iron
Lead A
nsfil^jO
i.'fffU{7s"o3
I .OU
5.3I03OOO
[<U1f/Q]C9.2]
nstt.?6V
A/
/v
2.
/*?
pFF
P
PJfp
P
P
pp
P
F
g/L^or ng/kg dry weight (Circle One)
13.
14.
I*.
16.
17.
16.
IV.
20.
21.
22.
23.
Pre cent Solids (Z)
Cyanide
Magnesium 31<*OO
Manganese 1 32O
hercury O.20
Nickel yV
Potassium V^Sfd]
Selenium /.&£/
Silver . - f6.v7
Sodium llS'OO
Thallium <9.<f/U
Vanadium C/V7
Zinc f/3]
/vA/
£
£
pp
ppF
P
P
F
PP
Footnotes: for reporting results Co tPA, standard result qua lit tecs arc used. as defined on Cover Pa&e. Addlcional flags or foocnoces explaining
results are encouraged. Definition of such flags muse be explicitand contained on Cover Page, however.
Cooaaents: Water:Coloration ClarityArtifact(s):None
Lab Manager
4 1 8 4 6 C 0 2 25 7 / M / F l / W
Uace OCT 3 0 1987
LAK :.
SOU NO.
ETC/Toxicon
INORGANIC A.tAL'li lS U.VlA bHt.t'1
CASE .NO.
785
LAb SAMPLE 10. NO. 4/8 t' 33
Lab Keccipc Uate
QC R£HORT NO.
tlements Ident i f ied and Measured
DiSS
Concentration:
Matrix: Water
Low
Soil
Medium
Sludge Other
Gonoentcatiai Flag rh"li<-im Mated CorcertzatiaiIg/L^or mg/kg dry weight (Circle One)
U.
r>ili<-inn
I . Aluminum
i. Antimony
3. Arsenic
M. barium
5. Beryllium
6. Cadmium
7. Calcium
8. Chromium
9. Cobalc
10. Copper
11. Iron /~3&7
12. Lead
P
F
F
P
P
F
P
P
P
P
P
F
lo.
17.
Ib.
IV.
i\j.
21.
22.
23.
Magnesium
Manganese
hercury
Nickel
Potassium
Selenium
Silver
Sodium
Thallium
Vanadium
Zinc
P
P
P
P
F
P
P
F
P
P
Precenc Solids (Z)
Cyanide
Footnotes: For reporting results to tPA, s tandard result qua l i f i e r s arc used. as defined on Cover Pa^e. Addi t iona l f lags or footnotes explaining
results are encouraged. Def ini t ion of such f lags must be explicitand contained on Cover Cage, however.
Comoents: .Water iColoration C_e>t-e>Kt.e&s. Clarity
Artifact(s) .-None
THIS ~R6$uCT /s foK T>/sso<-vfD J/?o/v ONLY
Lab Manager
4 1 8 4 6 0 0 5 95 7 / M / F l / W
^ o r cr. 1
j Er'A baraple No.
LAtbOV« NO.
ETC/Toxicon
Uace OCT 3 0 195?
INORGANIC ANALYSIS UA'lA SHtEl
_ CASE \o.
785
LAb SAMPLE ID. NO.
Lab Keccipt Uate
QC REPORT NO.
Elements Identified and Measured
Concentration:
Matrix: Water
Low
Soil
Medium
Sludge Other
QiuaMxaLicn Flqg niliflm Ifetfcd CbncotzatlGn FLqg Dtlut±n (fedrxijg/lNor mg/kg dry weight (Circle One)
1. Aluminum 2b(e>
i. Antimony l^.&U
J. Arsenic Gfiffl)
H. harium 2/5*
5. Berylliuo /.OO
to. Cadniua V.^U
7. Calciua 21(oOOO
(5. Chrood.ua £.4(J
9. Cobalt 4.2U
LO. Copper f/Sl
11. Iron f52~]
12. Lead j ,3 U
N
N
z.z,
10
10
pFF
P
P
AP
P
P
P
P
F
13. Magnesium iZ-Z^i
I*. Manganese [83
15. hercury O."2.(J
16. Nickel I3U
17. Potassium 7&800
Ito. Selenium /, ^£/
IV. Silver . fV.Ol
20. Sodium 5/2.OO
21. Thalliua^,^/^/
22. Vanadium 0^1
23. Zinc i:%i)
V
A/
/L>
2_
pp
ppFppF
PE
Precenc Solids (Z)
Cyanide
Footnotes: For reporting results to tPA, standard result qualif iers arc used. as defined on Cover Page. Additional flags or footnotes explaining
results are encouraged. Definition of such flags must be explicitand contained on Cover Cage, houever.
Comnents: Water:Coloration ClarityArtifact(s):None
Lab Manager
4 1 5 4 6 C 0 2 35 7 / M / F l / W
ETC/Toxicon
SOU NO. 785
LAb SAMPLK ID. NO.
Date OCT 3 0 1987
A:<ALt:>lS IM'lA
CASK NO.
Lab Receipt Date
QC REPORT NO.
tletaencs Identified and Measured
Concentration:
Matrix: Water
Low
Soil
[-tedium
Sludge Other
Ccrcenrrarton Flag Dilirim rfethod Flag T>i"li*-ifT|
I. Aluminum
'i. Antimony
J. Arsenic
•i. barium
5. tferylliua
b. Cadmium
7. Calcium
b. Chromium
9. Cobalc
10. Copper
11. Iron ££&!
12. Lead
P
F
F
P
P
F
P
P
p
P
P
F
mg/kg dry weight (Circle One)
13.
U.
17.
Ib.
21.
22.
23.
Magnesium
Manganese
hercury
Nickel
Potassium
Selenium
Silver
Sodium
Thallium
Vanadium
Zinc
P
P
P
P
F
P
P
F
P
P
Precent Solids (Z)
Cyanide
Footnotes: For reporting results to tPA, s tandard result qua l i f i e r s arc used. as def ined on Cover Page. Addit ional flags or footnotes explaining
results are encouraged. Def in i t ion of such flags must be explicitand contained on Cover Page, however.
Coroent*: Water: Coloration Clarity
Artifact(s):None
THIS 7?fSuiT SHttT is fo* OrtLY
Lab Manager
5 7 / M / F l / W
6 G Q 6 0
I
Date OCT 3 0 1987
LMOI&AMC ANALYSIS UAVA
LA£ T.AME
SOW NO.
EIC/Toxicon CASE NO.
785
LAB SAMPLE 10. HO.
Lab Receipt Gate
QC REPORT NO.
Eleaents Identified and Measured
CooGeneration:
Matrix: Water
Low
Soil
Kedluai
Sludge Other
Hag QmatmUon PIqg DQut±n Matted•g/kf dry weight (Circle One)
1. Aluminum 2^3
•/. Antlaony U.ffU
3. Arsenic 030U
4. barlua / /9O
S. eerylllua 1.00
6. Cadvlua 9.1
7. Calclua ^0,OOO
<J. Chroodua /4
9. Cobalt pTSl
10. Copper r/2l
11. Iron ILSOO12. Lead AJ ^/
AJ
.-
A/
X,
/^
•
pppppF
U.
IS.
16.
17.
16.
20.
21.
22.
23.
Magneslua l57,OOO
Manganese 82.
Mercury O.2U
Nickel SS
Potasslua 838O
Selenlua l>l±U
Sliver 2.HU -.
Sodlua ' '•'.& tyj D00
Thalllua S.f/t/
Vanadlua £.3 Ij
Zloc D 3]
A/
A/
10
JL
pp
pppppppE
Freceot Solids (Z)
Cyanide
Footnotes: For reporting results to tPA, standard result qualifiers are used. as defined oo Cover Pa^e. Additional flags or footnotes explaining
results arc encouraged. Definition of such flags aust be explicitand contained on Cover Page, however.
UateriColoratlonArtif act(s):None
4 1 8 4 6 0 0 3 S
uace OCT 3 0 1987
INORGANIC A. iALts lS UA'lA SllLt'1
LAK
SOU NO.
ETC/Toxlcon CASE NO. V/gV
785
LAb SAMPLE II). NO.
Lab Keccipc liace / "V?9" ff 7
QC REPORT NO.
Elements Identif ied and Measured
1HSS
Concentration:
Matrix: Water
Low
Soil
Medium
Sludge Other
Cbnoentratiai Flgg piliirim hfediod Cbraentxatiaijg/lNor tug/kg dry ueight (Circle One)
rKli<-inn ^fetJtxi
1 . Aluminum
'i. Antimony
J. Arsenic
H. Barium
5. beryllium
t>. Cadmium
7. Calcium
tt. Chromium
<y. Cobalt
10. Copper
11. Iron /?9
12. Lead
P
F
F
P
P
F
P
P
P
P
P
F
u.[4.
1>.
10.
17.
15.
iy.20.
21.
22.
Magnesium
Manganese
Hercury
Nickel
Potassium
Selenium
Silver
Sodium
Thallium
Vanadium
Zinc
P
P
P
P
F
P
P
F
P
P
Precenc Solids (2)
Cyanide
Footnotes: For reporting results to tPA, standard result qualifiers arc used. as def ined on Cover Page. Addi t iona l flags or footnotes explaining
results are encouraged. Defini t ion of such flags must be explicitand contained on Cover Page, however.
Comoeuc*: Water:Coloratlon ClarityArtifact(s):None
THIS SHftT is fo* ~t>moLyet>
Lab Manager
57/M/F1/W
4 1 8 4 6 0 0 7 2
l-orr I
ANALYSIS UA'lA
LAt
SOU NO.
ETC/Toxicon CASt NO.
Sample No.
wo yjo/ I
OCT 3 Q mr
785 Ub Receipt Uate 9-29-87
LAb SAMPLE 10. NO. QC REPORT NO. y/gy
Elements Identified and Measured
Matrix:
Cyanide
Footnotes:
ration: Low
Water x
ainum fi I3l
Lmony lk,$(J
snic CfyfO*)
Lum T& 8l
fllium ADD
ilum 4.8U
:ium £S\QO
>mium 5.4U
ilc ^.2iJ>er rs.n* f(.8li / ,3cV
Medium
Soil Sludge
Flqg DLIudcn!
A/
N
^>L
2.
fEPcn UTcerctaticnmg/kg dry weight (Circle One)
p 13. Magnesium 2_(*70C
F 14. Manganese [~7. 1
F IS. hercury O.ZU
P Ib. Nickel l3\J
P 17. Potassium .58/0
y^ Ib. Selenium .j.llU
P IV. Silver Z.4U
P 20. Sodium 'HZO
p 21. Thallium <$> ,*? I U
p 22. Vanadium f8.<TI
P 23. Zinc £&.£]
Other
Flag T>n»*-fan
VV
/£?
^
mA**4hnsD]
pp
ppF
P
P
Fp
E
F Precent Solids (Z)
For report ing results to tPA, s tandard result qual i f iers arc usedas defined on Cover Page. Additional f lags or footnotes explainingresults are encouraged. Ueflnltloa of such f lags must be explicitand contained on Cover Page, houever.
Comoents: Water: Coloration ClarityArtifact(s):None
Lab Manager
4 1 8 4 6 C 0 1 95 7 / M / F l / W
Uace OCT 3 0 19°7
LAtsou NO.
ETC/Toxicon
A N A L Y S I S UA'lA SHtE'l
CASt NO. V/gV785
LAb SAMPLE ID. NO. " 90
Lab Keccipt Uace
QC REPORT NO.
Elements Identified and Measured
Con ce n C era c ion:
Matrix: Wacer
Low
Soil
tedium
Sludge Other
Gcnoantraticn Flag DOyCkn rfetiiod
1 . Aluminum
i. Antimony
J. Arsenic
•*. barium
3. Beryllium
6. Cadmium
7. Calcium
tt. Chromium
9. Cobalc
10. Copper
11. Iron Z /3
12. Lead
P
F
F
P
P
F
P
P
P
P
P
F
Xfg/lNor mg/kg dry weight (Circle One)
13.
14.
16.
17.
Ib.
iy.2U.
21.
22.
23.
Precenc Solids (Z>
Cyanide
Magnesium
Manganese
hercury
Nickel
Potassium
Selenium
Silver
Sodium
Thallium
Vanadium
Zinc
P
P
P
P
F
P
P
F
P
P
Footnotes: For repor t ing results to tPA, standard result qua l i f i e r s arc used. as defined on Cover Page. Addit ional flags or footnotes explaining
results are encouraged. Definition of such flags must be explicitai\d contained on Cover Page, hoover.
Comae MM: Water: Coloration Claritv CLEARArtifact (s):None
THIS SHctT is foX. ~D/sso<-v«? IRON
Lab Manager
4 1 8 4 6 0 0 5 65 7 / M / r l / W
l -o rm I
INORGANIC ANALYSIS UA'lA
Sample Ho. \"
Oace OCT 3 0 198/I ^
LAt
SOU NO.
ETC/Toxicon CASE NO.
785LAb SAMPLK ID. NO. - 89
Lab Keccipt liate q-
<}C REPORT NO. f 184
Elements Identified and Measured
Concent radon:
Matrix:
on : Low
iter X
<<£» zm
Soil
Uutim Mated/L\or rag/kg
P
Medium
Sludge Other
CbncsTtCBtdon Floe Qdry weight (Circle One)
13. Magnesium L^/J
Ilirlcn Mated
P1. Aluminum 22H
'£.. Antimony ff*.d I?
3. Arsenic 0.^6 U
H. Barium 6>49
5. Beryllium f.OU
o. Cadmium ^.8U
7. Calcium 2i?OOO
«. Chromium £7
V. Cobalt ^,2U
10. Copper f /Vl
U. Iron L.(*S~]
12. Lead /.3 ^
N
N
2,2.
10
to
pFF
P
P
t?FpPpppF
13. Magnesium L7/J
14. Manganese tS'tJ
IS. hercury O.2U16. Nickel /3U
17. Potassiua LjIfOOO
Ib. Selenium \M U
IV. Sliver -T(o.f[
l\j. Sodium 2O5000
21. Thallium ff.^jf/U
22. Vanadium ("/ f 7
23. Zinc T/¥7
A/
^
/o;&
^
pp
ppF
P
P
F
P£
Preoent Solids (I)
Cyanide
Footnotes: For reporting results to tPA, standard result qua lit lees arc used. as defined on Cover Pa e. Additional flags or Footnotes explainingresults are encouraged. Definition of such flags must be explicitand contained on Cover Cage, however.
Comaene$: Water:Coloration Clarity
Artifact(s):None
Lab Manager
4 1 6 4 6 C 0 1 8
f o r m I
\ E f f , Sample No. |
I
Date OCT 3 n 10Q7
INORGANIC ANALYSIS UA'iA
ETC/Toxicon CASK .so.
NO. 785
LAb SAMPLE ID. NO.
Lab Keceipt liate *f->
QC REPORT NO.
Elements Identified and Measured
ISS
Concentration:
Matrix: Water
Low
Soil
Medium
Sludge Other
n i*>ni 1'nrim
1. Aluminum
2. Antimony
J. Arsenic
H. Barium
5. berylliua
6. Cadniua
7. Calciua
b. Chromium
V. Cobalt
10. Copper
11. Iron Z"3/l
12. Lead
P
F
F
P
P
F
P
P
P
P
P
r
U.
14.
13.
16.
17.
Ib.
19.
20.
21.
22.
23.
\JS UnXaLlili
ight (Circle One)
Kagnesiua
Manganese
hercury
Nickel
Potassiuo
Seleniua
Silver
Sodiua
Thallluo
Vanadiua
Zinc
tia^ui iim-im ctau.ua
P
P
P
P
F
P
P
F
P
P
Preoenc Solids (Z)
Cyanide
Footnotes: For reporting results Co tPA, standard result qualif iers arc used. as defined on Cover Page. Additional flags or footnotes explaining
results are encouraged. Definition of such flags muse be explicitand contained on Cover Cage, however.
Comneots: Water .'Coloration ClarityArtifact (s): None
THIS "ReSuLT SHctT i$ fe* Dm PL VCD OtiLY
Lab Manager
4 1 8 4 6 C 0 5 55 7 / M / F l / W
[Et'A Sanple No. |
I - I
\ JofSc i I
Oate OCT 30 1987
LAK NAME _
SOW NO.
LAb SAMPLE ID. NO.
INORGANIC ANALYSIS UAIAETC/Toxicon CASE NO.
785- IPS
Lab Kecelpt Bate
QC REPORT NO.
Concent ration:
Matrix: Water
Elements Identified and Measured
Low Medium _
SludgeSoil Other
n i » i-g •Tar-inn
1. Alumloum flLfD~l
2. Antimony & .0 (J
3. Arsenic 0,50U
H. barium .S^T]
5. Beryllium /. OU
6. Cadmium *+.%[)
7. Calcium 84IOO
«. Chromium £5.41
V. Cobalt V.2L/
10. Copper [7s"7
11. Iron C8£]
12. Lead /r5 ^/
tUKU
(uj
A/
•
/J
n nw-im ]
7t)or
.&
2,
TcUCu *'"*** *fi! it ii«g/k.g dry weight (Circle One)
p 13. Magnesium 20LOO
F 14. Manganese /^¥
F IS. hercury O ^jj
P 16. Nickel /3L>
P 17. Potassium FS^S"]
P 16. Seleniua 1 >H-U
P IV. Silver F3. 5l
P 2O. Sodium /^29VOT
p 21. Thallium 0,9/ L/
p 22. Vanadium £?. 77
P 23. Zinc 2V
F Preceat Solid* (Z)
nqgL
^
^
ina-im
^
^
rauuu
P
P
P
Cyanide
Footnotes: For reporting results Co tPA, standard result qualifiers arc ueedas defined on Cover Pa^e. Additional fla^s or footnotes explainingresults are encouraged. Definition of such flags must* be explicitand contained on Cover Cage, however.
Comnents: Jfater: Coloration <n*itArtif act (s): None
Lab Manager
4 1 8 4 6003657/M/n/W/
j K i' A 1.. i m; i 11 •
Dace OC7 3 0 1987
INORGANIC A N A L Y S I S UA'IA
ETC/Toxlcon CASt .\o.
NO. 785
LAb SAMPLE 10. NO. - /g 3
Lab Receipt liate ?- Z1-97
QC REPORT NO.
bleoencs Ident if ied and Measured
Concenccacion:
Matrix: Wacer
Low
Soil
Medium
Sludge Other
Cbrcantzatian Flgg pOm-im ffethd Gcrcentxatian Flfg TMIirimr rag/kg dry weight (Circle One)
1 . Aluminum
2. Antimony
3. Arsenic
H. barium
5. tterylliua
b. Cadmium
7. Calcium
b. Chromium
^. .Cobalt
10. Copper
1 1. Iron tZ*ll
12. Lead
•
P
FF
P
P
F
P
P
p
P
P
F
U.
15.
10.
17.
16.
iy.2u.
21.
22.
23.
Magnesium
Manganese
hercury
Nickel
Pocassiua
Selcniua
Silver
Sodium
Thallium
Vanadium
Zinc
P
P
P
P
F
P
P
F
P
P
Precenc Solids (Z)
Cyanide
Footnotes: For report ing results to tPA, s tandard result qua l i f i e r s arc used. as defined on Cover Page. Addi t ional f lags or tootnotes explaining
results are encouraged. Definition of such flags must be explicitand contained on Cover Page, however.
Comoeots: Water: Coloration &>u*L&s Clarity
Artifact(s):None
THIS SHftT fo* J/?OA/
Lab Manager
f o r m I
J E P A No.
OCT 3 0 1387
INORGANIC ANALYSES IM'IAETC/Toxicon CASE NO.
sou NO. 785
LAb SAMPLE ID. NO.
Ub Keccipc Uate
QC REPORT NO.
Elements Identified and Measured
Con cent radon:
Matrix: Water
Low
Soil
Medium
Sludge Other
Cbroertxatlon FUg DLTuelcn rfathadjg/L\or mg/kg dry weight (Circle One)
1.'t.
3.
5.
b.
7.
a.
10.
u.12.
Aluminum (t>5Z
An t imony JJ*. $ 0
Arsenic Cbffr
harlum CY5]
Beryllium I.QU
Cadmium f.&O
Calcium Q^OOO
Chromium ,5".mJ
Cobalt 1.2U
Copper fiSl
Iron LSQ
Le«d /..^ 6/
A/
A/
^
^
-^L
PFF
PP
^pP
Pp
p
PF
H.
14.
1*.
Ib.
17.
16.
21.
22.
23.
Preoent Solids (Z)
Cyanide
Magnesium LV^f
Manganese [*/ , V~I
hercury- O.2U
Nickel /3 U
Potassium 2HZOO
Seleniua . I'MtJ
Silver - - 2 A U
Sodium U I^QO
Thallium 0 rf/ U
Vanadium F/2^1
Zinc 4. \ U
A/
A/^
2.
P
P
P
P
F
P
P
F
PE
Footnotes: For reporting results to tPA, standard result qua l i f i e r s arc used. as defined on Cover Page. Additional f lags or footnotes explaining
results are encouraged. Definition of sued flags must be explicitand contained on Cover Page, however.
Comoeot*: Water: Coloration Clarity
Artif act (s): None
A.Lab Manager
^4 1 8 4 60021
5 7 / M / F l / W
K l ' A j.i rr. p 1 1-
Uacc OCT 3 0 1987
ANALYSIS UA'lA
ETC/Toxicon CASK NO.
NO. 783LAb SAMPLE ID. NO. - 92.
Lab Keccipt liate
QC REPORT NO.
b'letnencs Identified and Measured
DlSS
Concentration:
Matrix: Water
Low
Soil
Medium
Sludge Other
n n
1. Aluminum
2. Antimony
3. Arsenic
H. barium
5. tterylliua
b. Cadmium
7. Calcium
b. Chromium
9. Cobalt
10. Copper
II. Iron Z"/Sl
12. Lead
p
F
F
P
P
F
P
P
p
P
P
f
^fc^^r^^ CbnDentcatacn Flag DUiticn bfethcdg/L^or mg/kg dry weight (Circle One)
13.
16.
17.
20.
21.
22.
23.
Magnesium
Manganese
hercury
Nickel
Potassium
Selenium
Silver
Sodium
Thallium
Vanadium
Zinc
P
P
P
P
F
P
P
F
P
P
Precent Solids (I)
Cyanide
Footnotes: For reporting results to tPA, s tandard result q u a l i f i e r s arc used. as defined on Cover Page. Additional flags or footnotes explaining
results are encouraged. Definition of such flags must be explicitand contained on Cover Hage, houever.
Water: Coloration ClarityArtifact(s):Nbne
T/y/S 7?gSt/tT SHctT is fo*
Lab Manager
4 1 8 4 6 0 0 5 85 7 / M / F l / W
i -orm 1
INORGANICLAt :.AME
SOW NO.
ETC/Toxicon
785LAb SAMPLE 10. NO. - < \ \
UAYA
(EPA Sample No.
Uate OCT 3 0 1987
CASK NO.
Lab Kecclpc Uate 9- 29-87
QC REPORT NO.
Elements Identified and Measured
Concencration:
Matrix: Water
Low
Soil
Medium
Sludge Other
Cbnoentcatlcn Flgg DUition tettad GbnomtraCLon Flag Dilutim Mattedjg/L^or mg/kg dry weight (Circle One)
13.
14.
15.
16.
17.
Ib.
19.
20.
21.
22.
23.
I.
'i.
3.
•i.
5.
6.
7.
tt.
9.
10.
U.
12.
Aluminum
Antioiony
Arsenic
barium
Beryllium
Cadmium
Calcium
Chromium
Cobalt
Copper
Iron
Lead
DillV-.ou
0.9ouC7<fl
l.ouf«u
5V900
S^U
^.iU2AU
C3fl
/ .3U
/V
A/
zz
/c
PFF
P
P
ftP
P
P
P
P
F
Magnesium [|O7j
Manganese £3.\]
hercury O.ZU
Nickel 13 U
Potass lua 6>33O^
Selenium / . V U
Silver .. - 2.</U
Sodium Z t f lOO
Thallium 0.9/ U
Vanadium CV.7U
Zinc 0?}
A/
Z
2
P
P
P
P
F
P
P
F
PP
Precent Solids
Cyanide
Footnotes: For reporting results to tPA, standard result qual i f iers arc used. as defined on Cover Page. Additional flags or footnotes explaining
results are encouraged. Definition of such flags must be explicitand contained on Cover Page, however.
Comoenta: Water: Coloration Clarity
Artifact(s):None
Lab Maoa^er
4 1 8 4 6 C 0 2 05 7 / M / F l / W
! L t 'A L_ 1-1,- i.
INORGANIC
ETC/lexicon
SOU NO. 785
LAb SAMPLE 10. NO. */AS"f -
Uace OCT 3 0
U.VIA
CASK NO.
Lab Keccipc Uace
QC REPORT NO.
tleraents Identif ied and Measured
THSS
Concentration:
Matrix: Water
Low
Soil
Medium
Sludge Ocher
Ctaroenfntfjm Fkg Di.1i.fim tfediod Cbrcentiaricn Flag Dilirim tfethadrag/kg dry weight (Circle One)
U.1 . Aluminum
'(.. Antimony
J. Arsenic
•*. barium
5. tserylliuo
b. Cadmium
7. Calcium
8. Chrootium
9. Cobalc
10. Copper
11. Iron f?./l
12. Lead
P
F
F
P
P
F
P
P
P
P
P
F
Ib.
17.
Ib.
IV.
2o.
21.
22.
23.
Magnesium
Manganese
hercury
Nickel
Potassiuo
Selcniuo
Silver
Sodium
Thalliua
Vanadium
Zinc
P
P
P
P
F
P
P
F
P
P
Precenc Solids (I)
Cyanide
Footnotes: For report ing results Co tPA, s tandard result q u a l i f i e r s arc used. as def ined on Cover Page. Addit ional f lags or tootnotes explaining
results are encouraged. Definition of such flags must be explicitand contained on Cover Cage, however.
Comoencs: Water: Coloration ClarityArcifact(s):Norte
THIS ~R£$uCT SHctT iS foi? ZRon OfJLY
Lab
4 1 8 4 6 0 0 5 7T 7 / M / F 1 / W
INORGANIC ANALYSIS UAVALAt
SOVt NO.
ETC/Toxicon
L > j r r ; > L e N o -
uate OCT 3 Q 1987
CASE NO.
785
LAb SAMPLE IU. NO.
Lab Kcccipt liace 9-23-f 1
QC REPORT NO.
Elements Identified and Measured
Concentration:
Matrix: Water
Low
Soil
Medium
Sludge Other
Fl g Dilution rfethod Ctnoertxatiai Dlluticn tferiulig/r)or a^/kg dry weight (Circle One)
1.t.
3.
H .
5.
6.
7.
45.
10.
11.
12.
Aluminum
Antimony fa
Arsenic &
barium j
teryllium
Cadmium
[/SOI1.0LJ30U~JSO]
1.00480
Calcium IOIOOO
Chromium
Cobalt
Copper
Iron
Lead y
fall¥.2054
2£3,3 U
A/
»
AV
^^
/^
pFF
P
P
P
P
P
p
P
P
F
15.
17.
£o.
1«».
20.
21.
22.
23.
Magnesium
Manganese
hercury
Nickel
Potassium
Selenium
Silver
Sodium
Thallium i
Vanadium
Zinc
H-OOOO
/OS"
G.-LUr*3i
f/goo]l.bV[2.11bISO?.<//{/
C/31(*(*
fj
VZL
^
pp
ppF
P
P
F
PP
Precent Solids (1)
Cyanide
footnotes: For reporting results to tlPA, standard result qualifiers arc usedas defined on Cover Page. Additional f lags or footnotes explainingresults are encouraged. Definit ion of such flags must 'be explicitand contained on Cover fage, however.
Comoe.it*: Water:Coloration PjJtrdLt+' ClarityArtifact(s):None
.UAAlMx:^vLab Manager w
4 1 8 4 6 C 0 5 75 7 / M / F l / W /
LAKSOU NO.
EIC/Toxicon
785LAb SAMPLE 10. NO. <//o"f -
Uatc OCT 3 0 1937
A;.ALYiLb UAlA
CASt NO. V/gV
Lab Receipt Date
QC REPORT NO.
Elements Ident i f ied and Measured
Concencracion:
Matr ix: Water
Cyanide
Low
Soil
(tedium
Sludge Other
I . Aluminum
2. Antimony
J. Arsenic
A. Barium
5. tterylliun
6. Cadmium
7. Calcium
b. Chromium
9. Cobalt
10. Copper
11. Iron ft/]
12. Lead
P
F
F
P
P
F
P
P
P
P
P
r
Flag DUutJan rfetfaxi Cbnoatxataan Flag DUutim Mattedig/L^or ng/dg dry weight (Circle One)
U.
10.
17.
Ib.
IV.
2o.
21.
22.
23.
Magnesium
Manganese
ftercury
Nickel
Potassiun
Selcniua
Silver
Sodium
Thallium
Vanadium
Zinc
P
P
P
P
F
P
P
F
P
P
Precent Solids (Z)
Footnotes: For reporting results to tPA, s t andard result qua l i f i e r s arc used. as def ined on Cover Pa^e. Addi t iona l f lags or tootnotes explaining
rftsuics are encouraged. Def ini t ion of such f lags must be explicitand contained on Cover Cage, however.
Comneots: Water :Coloration CbiJXU&> ClarityArtifact(s):None
THIS 7?fSutT SHctT IS fo^ J.RON
Lab Manager
4 1 8 4 6 G 0 7 4
Ko r m 1
INORGANIC A*ALY:>IS UAYA
ETC/Toxlcon
j E t - A Sample No. _ j
Oace OCT 3 0 1987
CASt NO.
SOU NO. 785
LAb SAMPLE II). NO. ~ <??
Ub Kecelpt Late
QC REPORT NO.
9-29-87
Elements Identified and Measured
Concent ration:
Matrix: Water
Low
Soil
Medium
Sludge Other
Flat DLTiJtLan terird OimlmLkn Flag DOitim Mathodr rag/kg dry weight (Circle One)
1. Aluminum 35?
't. Antimony &,0 U
3. Arsenic C& .(*)
A. barium j}83
5. tSerylliua / ,OU
6. Cadmium \S
7. Calcium ZS10OO
«. Chromium j20
9. Cobalt C/G
10. Copper [fl]
11. Iron >2tlOO
12. Lead /,3U
A/
AJ
2,2.
to
10
pFF
P
P
/*P
P
p
P
P
F
U. Magnesium I70OOO
U. Manganese //V-O
li. hercury ^).2U
16. Nickel /02.
17. Potassium <oS(*00
16. Selenium / . Jf. /S
IV. Silver . fV./7
2O. Sodium 3Q3OOO
21. Thallium 47 ^/^/
22. Vanadium f^^J
23. Zinc 121
fll
/V
/o
1
/O
&
P
P
P
P
F
P
P
F
PE
Precent Solids (I)
Cyanide
Footnotes: For reporting results to t'PA, standard result qual i f iers arc used. as defined on Cover Page. Additional flags or footnotes explaining
resales are encouraged. Definition of such flags Bust be explicitand contained on Cover Page, however.
Conoents: Water: Coloration
Artifact(s):NoneClarity
Lab Manager
4 1 8 4 6 0 0 2 65 7 / M ' F i / w
oate OCT 3 0 1987
INORGANIC A..ALt^li UA'IA
LAL
sou
ETC/Toxicon CASE NO.
785
LAb SAMPLE 10. NO. - 97
Lab Keccipt Uate
QC REPORT NO.
Elements Idencified and Measured
DiSS
Concentrat ion:
Matrix: Wacer
Cyanide
Low
Soil
Medium
Sludge Other
1 . Aluminum
'i. Antimony
3. Arsenic
•i. barium
5. tierylliua
to. Cadmium
7. Calcium
y. Chromium
9. Cobalt
10. Copper
11. Iron fV^] 1
12. Lead
P
FF
P
P
F
P
P
p
P
P
F
<Viym< mi-innng/kg dry weight (Circle One)
13.
14.
Pilit-inn
16.
17.
Ib.
22.
23.
Magnesium
Manganese
hercury
Nickel
Pocassiuo
Selcniua
Silver
Sodium
Thalliuo
Vanadium
Zinc
P
P
P
P
F
P
P
F
P
P
Precent Solids (Z)
Footnotes: For reporting results to tPA, s tandard result qual i f iers arc used. as def ined on Cover Pa^e. A d d i t i o n a l flags or footnotes explaining
results are encouraged. Def in i t ion of such flags must be explicitacid contained on Cover Page, however.
Comoeots: _Water:Coloration ClarityArt.lfact(s):None
THIS "Re^uCT SHetT is fo* DISSOLVED
Lab Manager
5 7 / M . F 1 / W
4 1 8 4 6 0 0 6 ^
f o r m I
Sample No. j"
Uate OCT 3 0 1987
fc :.A,'tt ETC/Toxlcon
sou NO. 785
; ANALYSIS UA'lA ihttl
CASt NO.
LAb SAMPLE ID. NO.
Ub Receipt Uate <j-29-$7
QC REPORT NO.
Elements Identified and Measured
Concent ration:
Matrix: Water
Low
Soil
Medium
Sludge Other
CbnDsntratian Flag
Cyanide
hfetftxi Cbncertxatixn Flqg Dthttcn tfethodQg/kg dry weight (Circle One)
1. Aluminum 3OO
L. Antinony U.0 U
J. Arsenic 0 30 U
i. Kariua F/53^
5. berylllua LOU
t>. Cadnlum 9.7
7. Calcium 25"IOOO
«. Chrooiua /S
V. Cobalt [9.3]
10. Copper f/21
11. Iron f IOOO
12. Lead j .3 U
t\
ti
?,2
/O
/^
p
FF
P
P
/'P
P
p
P
P
p
13.
14.
13.
16.
17.
16.
20.
21.
22.
Magnesium lb%OOO
Manganese / /3O
hercury 0. 2.0
Nickel }O3>
Potassiua (olf SOO
Seleniua 1 . k. U
Silver fS.Vl
Sodium 30V-OOO
Thalliua <?.*7/{/
Vanadium T.2?3
Zinc (e>$2-
A/
A/
10
1010ZL
pp
PpF
P
P
Fp
P
Precent Solids
Footnotes: For reporting results to tPA, standard result qua 11 tiers arc used. «* defined on Cover Page. Additional flags or footnotes explainingresults are encouraged. Definition of sued flags must be explicitand contained on Cover Cage, however.
Comoents: Water; Coloration ClarityArtifact(s):N6ne
Lab Manager
4 1 8 4 6 0 0 2 757/y. /Fl/W
OCT 3 0 1987'
IMOKCANIC AI 'ALtSLS UA'tA
ETC/lexicon CASK .NO.
sou NO. 785
LAb SAMPLK II). NO. 4/8*+-
Lab Keccipt Uace
QC REPORT NO,
blements Ident i f ied and Measured
Concentration:
Matrix: Wacer
Low
x Soil
i it i >4frifn F13R T i li jm M*f j \y \
[•tedium
Sludge
/Vu-L L LltTUTCfint
Other
mg/kg dry weight (Circle One)
1 . Aluminum
2. Antimony
J. Arsenic
«. barium
5. tferylliuo
6. Cadmium
7. Calcium
tt. Chromium
*. Cobalt
10. Copper
IL. Iron fV97
12. Lead
P
F
F
P
P
F
P
P
P
P
P
F
13. Magnesium
14. Manganese
li. hercury
16. Nickel
17. Potassium
16. Selenium
lu. Silver
2o. Sodium
21. Thallium
22. Vanadium
23. Zinc
P
P
P
P
F
P
P
F
P
P
Precenc Solids (I)
Cyanide
Footnotes: For repor t ing results Co tPA, s t andard result q u a l i f i e r s arc used. as defined on Cover Pa&e. Additional flags or footnotes explaining
results are encouraged. Definit ion of such f lags must be explicitacid contained on Cover fage, however.
Comoencs: Water: Color at ion ClarityArtifact(s):None
THis ~R£Sut.~T SHetT is fo* ~Dis.Soi.vfD ZRon
Lab Manager
5 7 / M / F 1 / W
4 1 9 4 6 0 C 6 4
ETC/Toxicon
INOHCAMC A^ALYalS UA'iA SHfcEl
CASE NO.
baople No. |
I " II/*\ D L Q. UJ Q gC 01 I
Uate OC1" 3 0 1987
NO. 785
LAb SAMPLE 10. NO.
Lab Kecclpt Uate
QC REPORT NO.
Elements Identified and Measured
Concent radon:
Matrix: Water
Low
Soil
Medium
Sludge Other
QiuatfHtlm Flag T>t1i rim tfethri Cbrcertmrlm Flag Ttilirinn MattedKg/kg dry weight (Circle One)
13.
14.
1 . Aluminum /"/ 75 1
'£. Antimony lL,0 (}
3. Arsenic £)30U
H. Barium d>£^
S. Beryllium / .OL>
fe. Cadmium 7.1
7. Calcium /33OOO
B. Chromium T^.^
i>. Cobalt V.ZU
10. Copper £7.Q]
11. Iron 72700
12. Lead / *3 V
A/
A/
r1^*
2,
10
pFF
P
P
^PP
P
pp
P
F
16.
17.
Ib.
IV.
20.
21.
22.
Hagneslua KfpOOO
Manganese 2%
hercury G.ZO
Nickel ¥2.
Potassluo 622^7
Selenlua /.>>^/
Sllv«r 24U
Sodium IV2.OOO
Thalllua j.tf/L'
Vanadium f/fl
Zinc ¥0
A/
A/
/0
/<P
.
P
P
P
P
F
P
P
F
PE
Precenc Solid* (2)
Cyanide
Footnotes: For reporting results to EPA, standard result qualifiers arc used. as defined on Cover Page. Additional flags or tootnotes explaining
results are encouraged. Definition of such flags must be explicitand contained on Cover Page, however.
Co Water rColorationArtifact(s):None
4 1 8 4 6 C 0 3 357/M/Fl/W
j LI' A. '_.inp If
OCT 3 0 1987
INORGANIC A N A L Y S I S UA'IA
LAKSOU NO.
ETC/Toxicon CASt \o.
785
LAb SAMPLE ID. NO.
Lab Keccipc Date ?'
QC REPORT HO. V/gV
Elements Identif ied and Measured
Concent rat ion:
Mat r ix : Water
Low
Soil
Medium
Sludge Other
CorcenrrTirim Flag DOurjcn ttedxri Cbnoertratam Flag Diliricn hfetfadjgTlNor «g/kg dry weight (Circle One)
1. Aluminum
L. Antimony
J. Arsenic
•i. barium
5. Berylliua
6. Cadmium
7. Calcium
b. Chromium
9. Cobalt
10. Copper
11. Iron //5
12. Lead
P
FF
P
P
F
P
P
P
P
P
F
U.
17.
16.
iy.20.
21.
22.
23.
Magnesium
Manganese
hercury
Nickel
Pocassiuo
Selcniua
Silver
Sodium
Thalliua
Vanadium
Zinc
P
P
P
P
F
P
P
F
PP
Precent Solids (Z)
Cyanide
Footnotes: For repor t ing results to tPA, s tandard result qua l i f ie rs arc usedas def ined on Cover Pa^e. Addi t ional f lags or footnotes explainingresults are encouraged. Definition of such f lags muse be explicitand contained on Cover Page, however.
Comoents: Water : Coloration Cet.o4.LeiS Clarity CLEAR __Artifact(s):None _ ___ _
THIS 7?fStAT SHctT iS fo* "D/sSQivfP OfJLY
Lab Manager
57/M/Fl /v :
4 1 P /I 6 7 C 7
CONVENTIONALS CHEMICAL PARAMETER ANALYTICAL DATA.
PTC/TOXICON IDENTIFICATIONCUF:Jsrr IDEKHFICATIONSAMPLE MATRIXDATE SAMPLED
PARAMETER UNITS
4184/84MDLSW00803
09/21/87
4184/89MDLGW04401Wxer09/27/87
4184/90MDLCW0430IWtier09/27/87
4184/91MDLGW0470IWater09/27/87
4184/92MDLGW0460IVJmer09/27/87
4184/93MDLGW0400IWater09/26/87
*.**-*- ^0&amAW5i--^i ,-^-vi. r ^u - jAlluUiruty. Toul mg/LChemic*! O>ygen Demand (COD) mgfLCyanide, ToUl mg/L
NA<5.0<02
1600<5.0<.02
270<5.0<.02
400(9<.02
30049<.02
47054<.02
I ludnen. Total fflg/LResidue, FUienMe (TDS) mg/LResidue, Total Suspended (TSS) mg/L
25038038
3102,0005,300
2703903.000
1506005,100
25037013,000
44068011,000
NA denote* Not Analyzed.
oo
-OCDCDO
CONVENTIONAL^ CHEMICAL PARAMETER ANALYTICAL DATA.
CTC/TOXICON IDENTIFICATIONCUIT-NT IDENTIFICATIONSAMPLE MATRIXDATE SAMPLED
4184/94MDLGW04101Water09/26/87
4184/95MDLGW03301Water09/26/87
4184/96MDLGW03401Water09/26/87
4184/97MDLGW04901Water
4184/98MDLGW04902Water09/27/87
4184/99MDLGW03601Water09/26/87
t» *> 8 ~fOPARAMETER UNITS
Alkalimry. Toul mg/LChemical Oxygen Dcmmd (COD) mg/LCyanide, Total mg/L
640180<02
1600160<.02
300<5.0<.02
2,000310<.02
2,100370<.02
1,300<5.0<.02
R, Toul mg/LRendue, Filterable (TDS) mg/LResidue, Total Suspended (TSS) mg/L
7106507.100
9201,800950
2203802,900
1.3002,400150
1,3002,400140
2101,300860
NA denotes Not Analyzed.
^
CD
CD
CDCD
CONVENTIONALS CHEMICAL PARAMETER ANALYTICAL DATA.
fTCYTOXICON IDENTIFICATIONCLIENT IDENTIFICATIONSAMPLE MATRIXDATE SAMPLED
4184/100MDLGW03602Water09/26/J7
4184/101MDLGWD3001Water09/25/S7
4184/102MDLCW03101Water09/25/17
4184/103MDLGW03801Water090647
4184/104MDLGW0500IWater09/27/87
4184/105MDLGWB00001WllCT09/75/87
PARAMETER UNITS
Alkalinity, TotalChemical Oxygen Demand (COD)Cyanide, Total
mg/Lmg/Lmg/L
290<50<.02
43028<.02
190<5.0<.02
190<50<.02
82066«.02
.44<50<.02
I ludnen, Toul mg/LResidue, Rllerable (TDS) mg/LResidue, Todl Suspended (TSS) mg/L
1702807,800
350550340
17027049
2906701.100
8601,400NA
<.200170<4.0
NA denotes Not Analyzed
-T>.._A
OO
CONVENTIONALS CHEMICAL PARAMETER ANALYTICAL DATA.
ETC/TO X1CON IDENTIFICATIONCLIFJMT IDENTIFICATIONSAMPLE MATRIXDATCSAMJUD
4184/106MDLGW0420IWater09/26/87
4184/108MDLGWW501Water0*27/87
4184/109MDLGW04801Water09/27/87
4184/110MDLGW03201W*er09/26/17
4184/111MDLGW03901Waier09/76/87
4184/112MDLGW03501Water09/26/87
PARAMETER UNITS
Alkalinity. ToutChemical Oxygen Demand (COD)Cyanide. Total
mg/Lmg/Lmg/L
1.400180•c.02
42021<.02
37021<.02
100<5.0<.02
42026<.02
33047<.02
Hardnen. TouU mg/LResidue. Filterable (TDS) mg/LRetidue. Tocal Suapended (TSS) mg/L
1.2002.100NA
36092026.000
4701.60014,000
2001.200310
40058074
3401.20063.000
NA denote* Not Analyzed
00
CONVENT1ONALS CHEMICAL PARAMETER ANALYTICAL DATA.
CTC/TOXICON IDENTIFICATIONCLIENT IDENTIFICATIONSAMPLE MATRIXDATE SAMPLED
4184/113MDLGW03701Water09/26/87
EPAQCStandardIdentification
EPAQCStandardTtue Value
mg/L
EPAQCPereenlRecovery
PARAMETER UNITS CONCENTRATION
Alkalinity. ToUl mg/LChemical Oxygen Denund (COD) mg/LCyuude, Total mg/L
2.200<5.0<.02
WP3I4-2WP12M-2WP586
17.5145.300
9792
100
llardneu. Total mg/LResidue, filterable (TDS) mg/LResidue, Total Suipended (TSS) mg/L
1.2001.40020.000
WPJM-2WP1IS5-3WP1185-3
20.7140307
949388
NA denotes Not Analysed
-fc*
CO
oCD