food - feed waters - soils sunscreen...

20
Food - Feed Waters - Soils Sunscreen products PHYSICS CHEMISTRY MICROBIOLOGY SENSORY ● GRAINS ● FEED ● FOOD ● DRINKS ● ● WATERS ● SOILS ● AIR COSMETICS ● BIPEA - ISO/IEC 17043 - ISO 9001 PROFICIENCY TESTING PROGRAMS REFERENCE MATERIALS

Upload: voque

Post on 04-May-2018

221 views

Category:

Documents


2 download

TRANSCRIPT

Page 1: Food - Feed Waters - Soils Sunscreen productsjornades.uab.cat/workshopmrama/sites/jornades.uab.cat.workshopmr... · Food - Feed Waters - Soils Sunscreen products ... Over 40 years’

Food - Feed Waters - Soils

Sunscreen products

PHYSICS ● CHEMISTRY ● MICROBIOLOGY ● SENSORY

● GRAINS ● FEED ● FOOD ● DRINKS ●

● WATERS ● SOILS ● AIR ●

● COSMETICS ●

BIPEA - ISO/IEC 17043 - ISO 9001

PROFICIENCY TESTING PROGRAMS REFERENCE MATERIALS

Page 2: Food - Feed Waters - Soils Sunscreen productsjornades.uab.cat/workshopmrama/sites/jornades.uab.cat.workshopmr... · Food - Feed Waters - Soils Sunscreen products ... Over 40 years’

International proficiency testing programs ~ 2 ~

Page 3: Food - Feed Waters - Soils Sunscreen productsjornades.uab.cat/workshopmrama/sites/jornades.uab.cat.workshopmr... · Food - Feed Waters - Soils Sunscreen products ... Over 40 years’

International proficiency testing programs ~ 3 ~

CONTENT

About BIPEA (proficiency testing provider) p. 4-5

Proficiency testing programs p. 6-18

- PT Grains: physico-chemical analysis p. 6

- PT GMOs - DNA testing in food p. 6

- PT Milling: physico-chemical analysis p. 7

- PT Feed: physico-chemical analysis and contaminants p. 8

- PT Food: physico-chemical and tasting analysis p. 9

- PT Food: contaminants p. 10

- PT Food: microbiological analysis p. 11

- PT Drinks: physico-chemical analysis p. 12

- PT Drinks: contaminants p. 13

- PT Waters: physico-chemical analysis p. 14

- PT Waters: contaminants p. 15-16

- PT Waters: tasting analysis p. 17

- PT Waters: microbiological analysis p. 17

- PT Soils p. 18

- PT Air p. 18

- PT Cosmetic p. 19

Page 4: Food - Feed Waters - Soils Sunscreen productsjornades.uab.cat/workshopmrama/sites/jornades.uab.cat.workshopmr... · Food - Feed Waters - Soils Sunscreen products ... Over 40 years’

International proficiency testing programs ~ 4 ~

ABOUT BIPEA

(Proficiency testing provider)

Created in 1970, BIPEA is a European independent organisation certified ISO 9001 and accredited

ISO/IEC 17043.

BIPEA organises proficiency-testing programs in a wide variety of sectors such as grains, food, beverages,

feed, water, contaminants, soils, cosmetics, etc.

Present in more than 110 countries and with over 40 years of experience, BIPEA members are laboratories

concerned by control and quality (+2500 laboratories worldwide).

BIPEA services

Regular proficiency testing programs (PT)

Reference Materials (ERM)

Customised PT programs for a group of laboratories

Accuracy Monitoring charts

Technical control

Training session

Why choose BIPEA?

A technical expertise officially recognised (ISO 9001 certified by LRQA, ISO 17043 accredited by COFRAC)

Over 40 years’ experience and a worldwide presence, A multi-sector activity in constant evolution, A wide range of matrices and criteria, PT programs defined by committees and technical groups composed of experts, Reports made according to ISO 13528 standard, and results validated by technical experts, Confidentiality of results.

Annual programs

In order to evaluate the analysis performance of your laboratory on a long-term basis, BIPEA offers regular programs of interlaboratory comparisons in the form of annual series. Each annual series begins in September and finishes in June of the following year. Each series is composed of various rounds. Depending on the programs, there can be one sample to analyse or more, per round. Laboratories participating in a proficiency-testing program will receive all designated samples for that program. They can choose to analyse all criteria or only those that are of interest for them.

Page 5: Food - Feed Waters - Soils Sunscreen productsjornades.uab.cat/workshopmrama/sites/jornades.uab.cat.workshopmr... · Food - Feed Waters - Soils Sunscreen products ... Over 40 years’

International proficiency testing programs ~ 5 ~

BENEFITS FOR LABORATORIES

BIPEA participating laboratories play a crucial role!

In order to meet its member needs, BIPEA sets up regular meetings for each proficiency testing program. These committees are represented by an elected person who is also a participating member of the program. All participating laboratories are invited to join these meetings where laboratories and BIPEA staff discuss possible improvements for the PT programs: nature of the samples, shipment frequency, calculation of the assigned value, etc. These committees are also meant to promote a friendly atmosphere allowing formal and informal discussions among members of our community. These meetings are thus a major forum for exchanging technical and scientific information. The members can easily suggest improvements for the PT Program. Once they have expressed their wishes, we study the feasibility of the project, set up the final series, and fix the testing schedule.

Benefits of our proficiency testing programs

Interlaboratory comparisons meet the requirements of laboratories’ quality standards and are a strategic part of their quality system. Thus a large number of laboratories taking part in our programs join us within the framework of their accreditation/certification by official bodies. BIPEA proficiency-testing programs are more than basic tests. In fact, the main goal of our proficiency-testing programs is to prove the laboratory’s technical skills on a worldwide basis. Laboratories do not often have the opportunity and time to compare their results with others. Interlaboratory comparisons are considered fundamental: a laboratory needs to compare its testing results with the real value of a specific material, to check its accuracy. Moreover, a systematic bias or drift of test results can only be highlighted through long-term observation. In the case of unsatisfactory results, laboratories can use their results from our proficiency-testing programs as a tool for improvement. These enable a laboratory to determine the reasons for its deviation. Whether this is a one time or systematic problem of method, drift, or bias, it can be identified by an appropriate participation in our proficiency-testing programs. Thus, participating in interlaboratory comparisons set up by an external organisation such as BIPEA clearly allows confirmation of the analytical performance of a laboratory. To sum it up, BIPEA interlaboratory comparisons can help laboratories to identify sources of analytical error, taking corrective actions and improving the analytical performance on a short, medium and long term basis. Our tests can also be used for training, in order to check employees’ technical skills. Finally, BIPEA proficiency-testing programs are a key factor in laboratory quality systems and can reassure stakeholders on the good quality service of a laboratory.

Page 6: Food - Feed Waters - Soils Sunscreen productsjornades.uab.cat/workshopmrama/sites/jornades.uab.cat.workshopmr... · Food - Feed Waters - Soils Sunscreen products ... Over 40 years’

International proficiency testing programs ~ 6 ~

PT Grains: physico-chemical analysis accredited*: scope 1-1495 www.cofrac.fr

PT GMOs - DNA in food

Proficiency Testing Matrices Parameters Weight Round /

year Sample /

round

40a - GMOs Corn, Soya Detection and quantification ELISA and PCR method

250 g 3 2

40b - DNA Finished products (biscuits, chips) + Mix sample for detection

PCR method: Quantification of DNA for finished products Detection of DNA for grains cross contamination

250 g to 500 g 3 2

Proficiency Testing Matrices Parameters Accreditation ISO

17043 Weight

Round / year

Sample / round

01 - Common wheat Common wheat

Analysis on grains, milling test, analysis on flour, Alveograph, Farinograph, Mixolab

accredited* 1700 g 10 1

05 - Common wheat: varietal identification

Common wheat

Identification of varieties

1000 g 6 1

06 - Durum wheat Durum wheat

Physico-chemical analysis, sieve control, impurities determination

1200 g 10 1 or 2

08 - Impurities determination Grains Impurities determination, sieve control

100 g to 500 g

10 2 or 4

09 - Moisture determination Grains, Flour

Moisture content accredited* 250 g to 500 g

10 4

10 - Oilseeds Grains Impurities, fatty acid composition accredited* 500 g to 1200 g

10 2 or 3

11 - Brewing barley: Physico-chemical analysis

Barley Physico-chemical analysis, sieve control, germination test, IR analysis

100 g to 900 g

10 2 or 3

12 - Food pulses Grains Analysis according to the Addendum n°VII

500 g to 1250 g

10 1

23 - Brewing barley: specific and varietal purity

Barley Specific and varietal purity: Visual analysis, PCR analysis

200 g 10 1

69 - Wheat: French bread making test

Common wheat

Milling test, flour analysis, bread making test parameters, sensory analysis

2000 g 3 1

Page 7: Food - Feed Waters - Soils Sunscreen productsjornades.uab.cat/workshopmrama/sites/jornades.uab.cat.workshopmr... · Food - Feed Waters - Soils Sunscreen products ... Over 40 years’

International proficiency testing programs ~ 7 ~

PT Milling: physico-chemical analysis accredited*: scope 1-1495 www.cofrac.fr

Proficiency Testing Matrices Parameters Accreditation

ISO 17043 Weight

Round / year

Sample / round

02 - Flour: physico-chemical analysis and alveograph

Flours Physico-chemical analysis Alveograph

accredited* 750 g 10 1

03 - Flour: French bread making test Flours Physico-chemical analysis Flour analysis, French bread making test criteria, sensory analysis

1050 g 5 2

07 - Semolina Semolina Physico-chemical analysis

400 g 10 1

16 - Filth test Flours, Pasta, Semolina

Rodents, insects, acarinas, fragments…

300 g to 600 g

5 1 to 2

25 - Flour: Farinograph and Mixolab Flours Physico-chemical analysis Farinograph / Mixolab

accredited* 1250 g 10 1

41 - Flour: Rheofermentometer Flours Rheology accredited* 11g and 1000 g

10 2

47 - Flour: French Tradition bread Flours Physico-chemical analysis Flour analysis, French bread making test criteria, sensory analysis

1050 g 10 2

72 - Flour: Mixolab standard protocol Flours Standard protocol parameters accredited* 250 g 10 1

Page 8: Food - Feed Waters - Soils Sunscreen productsjornades.uab.cat/workshopmrama/sites/jornades.uab.cat.workshopmr... · Food - Feed Waters - Soils Sunscreen products ... Over 40 years’

International proficiency testing programs ~ 8 ~

PT Feed: physico-chemical analysis and contaminants accredited*: scope 1-1495 www.cofrac.fr

Proficiency Testing Matrices Parameters Accreditation

ISO 17043 Weight

Round / year

Sample / round

13 - Feed Feed (raw materials and finished products)

Physico-chemical analysis Nutritional value, minerals, amino acid, vitamins, pigments, microscopic analysis, fatty acid profile, drug residues, …

accredited* 350 g to 750 g

10 2 to 3

14 - Forages Forages

Physico-chemical analysis Parietal components, minerals, digestibility forecast, cellulose digestibility, nitrogeneous value, energetic value forecast

300 g 10 1

22 - Silages Silages Physico-chemical analysis Parietal components, alcohols, volatil fatty acids, digestibility, other parameters…

1500 g 4 1

26a - Amino acids Feed (raw materials and Finished products)

Amino acids by hydrolysis method, free amino acids, protein content

accredited* 300 g 5 1 to 2

32c - Trace elements Feed Trace elements accredited* 150 g to 200 g

4 1

42 - Premix Premix Physico-chemical analysis, minerals, vitamins, metals... accredited* 350 g 10 1 to 2

67 - Petfood (10 rounds) Feed - Dog and Cat (raw materials and Finished products)

Physico-chemical analysis Amino acids, antioxidants, biogenic amines, mycotoxins, vitamins, minerals, contaminants, fatty acids, trace elements, collagen…

accredited*

100 g to 400g

30 ml to 250 ml

10 2 to 3

67a - Petfood (5 rounds) accredited* 30 g to 2000 g

5 2 to 3

Page 9: Food - Feed Waters - Soils Sunscreen productsjornades.uab.cat/workshopmrama/sites/jornades.uab.cat.workshopmr... · Food - Feed Waters - Soils Sunscreen products ... Over 40 years’

International proficiency testing programs ~ 9 ~

PT Food: physico-chemical analysis accredited*: scope 1-1495 www.cofrac.fr

Proficiency Testing Matrices Parameters Accreditation

ISO 17043 Weight

Round / year

Sample / round

20 - Dietary products Food Physico-chemical analysis caloric value, minerals, vitamins, fatty acids

accredited* 70 g to 300 g

10 1 to 2

21 - Fats and oils Fats, oils Physico-chemical analysis Fatty acids, trans fatty acids, sterols, triglycerides…

accredited* 250 ml 10 1

21a - Olive oil: Physico-chemical analysis

Olive oil

Physico-chemical analysis Fatty acids, trans fatty acids, sterols, triglycerides…

accredited* 250 ml 3 1

21b - Olive oil: Tasting analysis Sensory analysis accredited* 500 ml 3 1

26b - Amino acids for food Various food Amino acids by hydrolysis method, protein content

accredited* 300 g 5 1

46 - Honey

Honey

Physico-chemical analysis, microscopic analysis, identification, sensory analysis

accredited* 300 g 6 1

46a - Adulterated honey 13C (‰) whole honey, 13C (‰) protein extract, C4 sugars (%) Interpretation and conclusion

200 g 1 1

62 - Flavourings and fragrances

Flavourings, Essential oils, Fragrances,

Physico-chemical analysis: quality control

30 ml to 100 g

5 1

62d - Flavourings and fragrances: GC analysis

GC analysis

5 ml 2 1

62e - Flavourings and fragrances: LC analysis

LC analysis

10 ml 2 1

62f - Flavourings and fragrances: Chirality

Chirality

5 ml 1 1

75 - Dairy food Dairy food Physico-chemical analysis: caloric value, minerals, vitamins, fatty acids

accredited* 300 g 1 1 to 2

Page 10: Food - Feed Waters - Soils Sunscreen productsjornades.uab.cat/workshopmrama/sites/jornades.uab.cat.workshopmr... · Food - Feed Waters - Soils Sunscreen products ... Over 40 years’

International proficiency testing programs ~ 10 ~

PT Food: contaminants accredited*: scope 1-1495 www.cofrac.fr

Proficiency Testing Matrices Parameters Accreditation

ISO 17043 Weight

Round / year

Sample / round

28 - Patulin determination Compote, Juice, Cider, Apple Patulin accredited* 200 g 3 1

19 - Pesticides Fruits, Cereals, Vegetables, Fats, Oils, Honey, Dairy, Plants, Egg

Pesticides accredited* 100 ml / 250 g 4 to 6 1

66 - Multi-residue screening of pesticides

Fruits, Cereals, Honey, Vegetables, Essential oils

Pesticides accredited* 30 ml

110 g to 250 g 1 1

31a - Mycotoxins: Dried fruits and spices

Dried fruits, spices and other food matrix

Aflatoxins, ochratoxin A accredited* 200 g to 250 g 5 1

31b - Mycotoxins: Cereals Cereals Aflatoxins, ochratoxin A, deoxynivalenol, fumonisins, nivalenol, zearalenone…

accredited* 200 g to 250 g 5 1

31c - Mycotoxins: Baby food Baby food Aflatoxins, deoxynivalenol, fumonisins, nivalenol, zearalenone…

accredited* 200 g to 250 g 2 1

31d - Mycotoxins: Milk Milk M1 aflatoxin accredited* 200 g to 250 g 1 1

32 - Trace elements Plants, Seafood, Feed, Food, Dairy food, Plants

Trace elements accredited* 150 g to 200 g 4 1

44a - PCB / DIOXINS Food Indicator PCBs, Dioxin-like PCBs

accredited* 100 ml / 250 g 5 2

44b - PAH Food PAH accredited* 100 ml / 250 g 5 2

74 - Melamine Milk Melamine, cyanuric acid

150 g 2 1

76 - Contaminants in dairy food Dairy food Pesticides, trace elements, mycotoxins, PCB / PAH, Melamine

100 g to 250 g 5 1 to 2

77 - Allergens Flour, Dietary food, Industrial water, Fish, Dried fruits, Chocolate, Meat

Gluten, egg, milk, histamine, sulfites, nuts, soya

80 g to 250 g 2 3

Page 11: Food - Feed Waters - Soils Sunscreen productsjornades.uab.cat/workshopmrama/sites/jornades.uab.cat.workshopmr... · Food - Feed Waters - Soils Sunscreen products ... Over 40 years’

International proficiency testing programs ~ 11 ~

PT Food: microbiological analysis accredited*: scope 1-1495 www.cofrac.fr

Proficiency Testing Matrices Parameters Accreditation

ISO 17043 Weight

Round / year

Sample / round

51a - Food microbiology: E.coli O157 Meat E.coli (presence / absence)

accredited* 25 g 3 3

51b - Food microbiology: Multiple parameters enumeration

Meat

Multiple parameters enumeration: Bacillus cereus, Clostridium perfringens, Coliforms at 30°C, Enterobacteria, Escherichia coli, Listeria monocytogenes, Total plate count 30°C, Staphylococcus aureus, Total coliforms, Thermotolerant coliforms

accredited* 25 g 3 1

51c - Food microbiology: Salmonella Meat Salmonella spp (presence / absence)

accredited* 25 g 3 3

51d - Food microbiology: Listeria Meat Listeria monocytogenes (presence / absence)

accredited* 25 g 3 3

51e - Food microbiology: Yeasts / Moulds Meat Yeasts and moulds (enumeration)

accredited* 25 g 2 1

51f - Juice microbiology: Yeasts / Moulds Fruit juices Yeasts and moulds (enumeration)

accredited* 25 g 2 1

51h - Food microbiology: Listeria Sea products Listeria spp Listeria monocytogenes

(enumeration) accredited* 25 g 3 1

56 - Flour microbiology: Multiple parameters enumeration

Flours

Multiple parameters enumeration : Coagulasepositive Staphylococci, Escherichia coli, yeasts, moulds, Sulfite-reducing anaerobic bacteria at 46°C, Salmonella, total germs, total coliforms

250 g 4 1

79 - Wines: Microbiology Wines Brettanomyces, lactic bacteria accredited* 200 ml 3 1

83 – Virus detection in food Fruits, Water GI Norovirus, GII Norovirus, Hepatite A virus

25g 2 4

Page 12: Food - Feed Waters - Soils Sunscreen productsjornades.uab.cat/workshopmrama/sites/jornades.uab.cat.workshopmr... · Food - Feed Waters - Soils Sunscreen products ... Over 40 years’

International proficiency testing programs ~ 12 ~

PT Drinks: physico-chemical analysis accredited*: scope 1-1495 www.cofrac.fr

Proficiency Testing Matrices Parameters Accreditation

ISO 17043 Weight

Round / year

Sample / round

17 - Wines Different type of wines (sparkling, aromatized, liquor, sweet), wine flavored drink

Physico-chemical analysis (sugars, gas), inorganic compounds (anions, cations, other), volatils compounds (alcohols, esters, organic acids, other), preservatives

accredited* 60 ml to 1000 ml

10 1 to 2

17a - Grape must Grape juice, Rectified must

Physico-chemical analysis (sugars), inorganic compounds (cations, other), volatils compounds (alcohols, organic acids, other), preservatives

accredited* 250 ml to 1000 ml

2 2

18 - Spirits Liquors, Spirits, alcohols

Physico-chemical analysis (sugars), inorganic compounds (cations, other), volatils compounds (alcohols, esters, organic acids, other), flavourings

accredited* 750 ml to 1000 ml

10 1

18a - Distillate Distillate Physico-chemical analysis, volatil compounds (alcohols, esters, organic acids, other)

accredited* 500 ml 1 1

27 - Fruit juices and other soft drinks

Juice, Nectar, Sodas, Smoothie, energy drinks

Physico-chemical analysis, sugars, acids, organic and inorganic compounds, sugars substitute, anions, cations

accredited* 250 ml to 1000 ml

10 1 to 2

36a - Aromatized ciders Aromatized ciders Physico-chemical analysis, sugars, organic acids, alcohols, other organic compounds, cations

accredited* 1500 ml to

2000 ml 4 2

36b - French ciders, perry and pommeau

French ciders, Perry / Pommeaux

accredited* 1500 ml to

2000 ml 6 2

39 - Fortified wines Port wines, fortified wines Physico-chemical analysis, acids, sugars, inorganic and volatils compounds…

accredited* 750 ml 6 1

58 - Alcohols Crude alcohol, Neutral alcohol Physico-chemical analysis, higher alcohols, inorganic compounds, denaturants, tasting analysis

accredited* 100 ml to 1000 ml

10 3

58a - Dehydrated alcohols

Dehydrated alcohol Physico-chemical analysis, higher alcohols, inorganic compounds

accredited* 250 ml to 1000 ml

7 1

73 - Vinegar Vinegar Physico-chemical analysis, alcohols, acids, anions, cations

accredited* 750 ml to 1000 ml

3 1

Page 13: Food - Feed Waters - Soils Sunscreen productsjornades.uab.cat/workshopmrama/sites/jornades.uab.cat.workshopmr... · Food - Feed Waters - Soils Sunscreen products ... Over 40 years’

International proficiency testing programs ~ 13 ~

PT Drinks: contaminants accredited*: scope 1-1495 www.cofrac.fr

Proficiency Testing Matrices Parameters Accreditation ISO

17043 Weight

Round / year

Sample / round

19f - Pesticides: wines Wines Pesticides accredited* 250 ml 4 1

55 - Contaminants in wines Wines Ochratoxine A, phthalates, amines, acids, haloanisoles, halophenols, other organic compounds

accredited* 500 ml 5 1

65 - Compounds extracted from wood – Spirits

Spirits Aromatic compounds accredited* 150 ml 3 1

70 - Haloanisoles and halophenols in oak wood

Oak wood Haloanisoles, halophenols accredited* 100 g to 500 g

4 1

71 - Allergens in wines Wines Casein, lyzozyme, ovalbumin accredited* 250 ml 3 3

80 - Contaminants in spirits Spirits Phthalates, other contaminants accredited* 150 ml 3 1

81 - Compounds extracted from wood - Wines

Wines Aromatic compounds

150 ml 2 1

Page 14: Food - Feed Waters - Soils Sunscreen productsjornades.uab.cat/workshopmrama/sites/jornades.uab.cat.workshopmr... · Food - Feed Waters - Soils Sunscreen products ... Over 40 years’

International proficiency testing programs ~ 14 ~

PT Waters: Physico-chemical analysis accredited*: scope 1-1495 www.cofrac.fr

Proficiency Testing Matrices Parameters Accreditation

ISO 17043 Weight

Round / year

Sample / round

34 - Fresh waters - Physico-chemical analysis

Drinking water, surface water, groundwater

Physico-chemical analysis Minerals and trace compounds

accredited* 125 ml to 3000 ml

6 4 to 10

34a - Bathing waters - Physico-chemical analysis

Bathing water (swimming-pool)

Physico-chemical analysis Chloride, turbidity, isocyanuric acid, oxydabilité with KMn04 in acid solution, oxydability in alkalin solution, total organic carbon

accredited* 1000 ml 3 2

34b - Fresh waters - Basic physico-chemical analysis

Drinking water, surface water, groundwater

Physico-chemical analysis accredited* 125 ml to 3000 ml

4 2

34c - Fresh waters - Chlorophyll A, Pheopigment index

Drinking water, surface water, groundwater

Chlorophyll A, pheopigment index accredited* 1000 ml 3 1

37a - Bathing waters - THM Bathing water (swimming-pool)

THM accredited* 40 ml 3 2

48a - Waters - AOX Drinking water, waste water AOX accredited* 500 ml 6 1

48b - Waters - Hydrocarbons Drinking water, waste water Hydrocarbons (C10 - C40) accredited* 1000 ml 6 1

48c - Waters - Volatil Hydrocarbons

Drinking water, waste water Volatil hydrocarbons (C5 - C11) accredited* 40 ml 3 1

52 - Waste waters - Physico-chemical analysis

Waste water (inlet and outlet) and industrial waste water

Physico-chemical analysis Mineral and trace compounds

accredited* 250 ml to 1500 ml

6 4 to 10

52b - Waste waters: basic physico-chemical analysis

Waste water (inlet and outlet) and industrial waste water

Physico-chemical analysis Natural structure

accredited* 250 ml to 1500 ml

3 2

57 - Waters - Field analysis by samplers

Drinking water, surface water, groundwater, waste water, industrial waste water

Field analysis Conductivity at 25°C, chlorine (free, total, active), dissolved oxygen, Redox potential, pH, salinity, stabilizing agent: isocyanuric acid, turbidity

accredited* 10 ml to 1000 ml

3 5

57a - Waters - Field analysis: Organoleptic quality

Drinking water Qualitative analysis of odour, flavour, colour

accredited* 1000 ml 3 4

Page 15: Food - Feed Waters - Soils Sunscreen productsjornades.uab.cat/workshopmrama/sites/jornades.uab.cat.workshopmr... · Food - Feed Waters - Soils Sunscreen products ... Over 40 years’

International proficiency testing programs ~ 15 ~

PT Fresh Waters: Contaminants accredited*: scope 1-1495 www.cofrac.fr

Proficiency Testing Matrices Parameters Accreditation

ISO 17043 Weight

Round / year

Sample / round

37 - Fresh waters - Micropollutants Drinking water, surface water, groundwater

Pesticides, PCB, PAH, ureas, triazines, BTEX, volatils, other parameters

accredited* 1 ml to 1000 ml 6 2 to 4

37b - Fresh waters - PBDE

Surface water

PBDE accredited* 1 ml to 1000 ml 2 1 to 2

37c - Fresh waters - Alkylphenols & Bisphenol A

Alkylphenols & bisphenol A accredited* 1 ml to 1000 ml 2 1 to 2

37d - Fresh waters - Organotins Organotins accredited* 1 ml to 1000 ml 2 1 to 2

37e - Fresh waters - Chloroanilines Chloroanilines accredited* 1 ml to 1000 ml 2 1 to 2

37f - Fresh waters - Chloroacetic acid Chloroacetic acid accredited* 1 ml to 1000 ml 2 1 to 2

37g - Fresh waters - Epichlorhydrin Epichlorhydrin accredited* 1 ml to 1000 ml 2 1 to 2

37h - Fresh waters - Polychlorinated alkanes Polychlorinated alkanes accredited* 1 ml to 1000 ml 2 1 to 2

37i - Fresh waters - Acrylamide Acrylamide accredited* 1 ml to 1000 ml 2 1 to 2

37j - Fresh waters - Nitroaromatics Nitroaromatics accredited* 1 ml to 1000 ml 2 1 to 2

37k - Fresh waters - Chlorophenols Chlorophenols accredited* 1 ml to 1000 ml 2 1 to 2

37l - Fresh waters - Perfluorinated compounds

Perfluorinated compounds accredited* 1 ml to 1000 ml 2 1 to 2

37m - Fresh waters - Multi-pesticides (Environmental technical approval)

Pesticides accredited* 1000 ml 3 1

37n - Fresh waters - Parabens Parabens accredited* 1000 ml 2 1

37o - Fresh waters - ESA and OXA Metabolites

Ethane sulfonic acid and oxanilic acid metabolites

accredited* 1000 ml 2 1

59 - Waters - Multiresidues search of organic substances

Drinking water, surface water, groundwater

Pesticides accredited* 250 ml to 1000 ml

3 1 to 2

Page 16: Food - Feed Waters - Soils Sunscreen productsjornades.uab.cat/workshopmrama/sites/jornades.uab.cat.workshopmr... · Food - Feed Waters - Soils Sunscreen products ... Over 40 years’

International proficiency testing programs ~ 16 ~

PT Waste Waters: Contaminants accredited*: scope 1-1495 www.cofrac.fr

Proficiency Testing Matrices Parameters Accreditation

ISO 17043 Weight

Round / year

Sample / round

53 - Waste water - Micropollutants

Waste water (inlet and outlet) and industrial waste water

Pesticides, PCB, PAH, ureas, triazines, BTEX, volatils, other parameters

accredited* 1 ml to 1000 ml 6 1 to 3

53b - Industrial waste water - PBDE

Industrial waste water

PBDE accredited* 1 ml to 1000 ml 2 1 to 2

53c - Industrial waste water - Alkylphenols & Bisphenol A

Alkylphenols & Bisphenol A accredited* 1 ml to 1000 ml 2 1 to 2

53d - Industrial waste water - Organotins

Organotins accredited* 1 ml to 1000 ml 2 1 to 2

53e - Industrial waste water - Chloroanilines

Chloroanilines accredited* 1 ml to 1000 ml 2 1 to 2

53f - Industrial waste water - Chloroacetic acid

Chloroacetic acid accredited* 1 ml to 1000 ml 2 1 to 2

53g - Industrial waste water - Epichlorhydrin

Epichlorhydrin accredited* 1 ml to 1000 ml 2 1 to 2

53h - Industrial waste water - Polychlorinated alkanes

Polychlorinated alkanes accredited* 1 ml to 1000 ml 2 1 to 2

53j -Industrial waste water - Nitroaromatics

Nitroaromatics accredited* 1 ml to 1000 ml 2 1 to 2

53k - Industrial waste water - Chlorophenols

Chlorophenols accredited* 1 ml to 1000 ml 2 1 to 2

53l - Industrial waste water - Perfluorinated compounds

Perfluorinated compounds accredited* 1 ml to 1000 ml 2 1 to 2

PT Waters: Tasting analysis

Proficiency Testing Matrices Parameters

Weight Round /

year Sample /

round

78 - Sensory analysis on drinking Water: ODOUR and FLAVOUR

Drinking water Odour, Flavour NF EN 1622 standard

1000 ml 1 2

Page 17: Food - Feed Waters - Soils Sunscreen productsjornades.uab.cat/workshopmrama/sites/jornades.uab.cat.workshopmr... · Food - Feed Waters - Soils Sunscreen products ... Over 40 years’

International proficiency testing programs ~ 17 ~

PT Waters: Microbiological analysis accredited*: scope 1-1495 www.cofrac.fr

Proficiency Testing Matrices Parameters Accreditation

ISO 17043 Weight

Round / year

Sample / round

35 - Waters - Microbiological analysis except Legionella

Drinking water, well water, drilling water, bathing water

Multiple parameters by filtration method and NPP method: Total coliforms, E.coli, Enterococci, Pseudomonas aeruginosa, Staphylococci, Culturable micro-organisms (22°C and 36°C) Sulfite Reducing Anaerobic Spores (Clostridium)

accredited* 50 ml to 500 ml

6 3 to 4

50 - Waters - Microbiological analysis Legionella

Hot water for sanitary use

Legionella, Legionella pneumophila accredited* 1000 ml 3 2

50a - Cooling tower waters - Microbiological analysis Legionella

Synthetic cooling tower water

Legionella, Legionella pneumophila accredited* 1000 ml 3 2

54 - Waters - Microbiological analysis Salmonella

Drinking water, well water, drilling water, bathing water

Salmonella spp (presence / absence)

accredited* 250 ml 3 3

86a - Waters for medical use: waters under bacteriological control

Non-pyrogenic water Enumeration of revivifiable aerobic bacteria at 22°C & 36°C, and Pseudomonas aeruginosa

220 ml 1 2

86b - Waters for medical use: Microbiology of dialysis waters (hemodiafiltration)

Ultrapure water (dialysate)

Enumeration of viable germs at 22°C in 7 days on R2A and Pseudomonas aeruginosa

120 ml 1 2

86c - Waters for medical use: Microbiology of endoscope rinse waters

Endoscope rinse water (Pharmacopee Neutralizer Diluent)

Revivifiable aerobic flora at 22°C for 5 days 120 ml 1 2

PT Waters: Hydrobiology

Proficiency Testing Matrices Parameters Accreditation

ISO 17043 Weight

Round / year

Sample / round

82 - IBGN (Standardized Global Biological Index)

Fresh water macroinvertebrates in solution

Faunistic list and index calculations NF T90-350 standard (March 2004) and XP T90-388 standard (June 2010)

250 ml 1 1

Page 18: Food - Feed Waters - Soils Sunscreen productsjornades.uab.cat/workshopmrama/sites/jornades.uab.cat.workshopmr... · Food - Feed Waters - Soils Sunscreen products ... Over 40 years’

International proficiency testing programs ~ 18 ~

PT Soils accredited*: scope 1-1495 www.cofrac.fr

Proficiency Testing Matrices Parameters Accreditation

ISO 17043 Weight

Round / year

Sample / round

15 - Soils Soils Physical and chemical analysis, metals, particule size

accredited* 750 g 10 1

15a - Fresh soils Soils

Water content, nitrogen mineralization potential, carbon mineralization potential, microbial biomass, organic matter fractionation, soil aggregate stability

500 g 2 1

24 - Mineral fertilizers Mineral fertilizers

Physical and chemical analysis, particule size, metals

400 g 7 1

38a - Sludges, sediments, soils Physico chemistry

Sludges, Sediments, soils

Physical analysis, metals accredited* 150 g 6 1

38b - Sludges, sediments, soils Micropollutants

Sludges, Sediments, soils

PCB, PAH, pesticides… accredited* 125 g to

150 g 6 1

45 - Organic fertilizers Organic fertilizers

Physico-chemical analysis, organic matter stability, inert analysis, metals

5 to 7 litres

5 1

45a – Compost Household waste compost

Mercury, PCB, PAH 150 g 1 1

PT Air

Proficiency Testing Details of the program Round /

year

Stack emission analyses Mercury, Gaseous hydrochloric acid, Gaseous hydrofluoric acid, Gaseous metals and particles, PAH, Gaseous sulphur dioxide, Gaseous ammonia

1

Stack emission sampling Evaluation of the total dust concentration measurement method : Mass concentration of dust (3 or 4 days on-site at Verneuil-en-Halatte (FRANCE)

1

Workplace air analyses Metals, Mercury, Inorganic acids, BTEX, Aldehydes 1

Indoor air analyses Benzene, Formaldehyde 1

Page 19: Food - Feed Waters - Soils Sunscreen productsjornades.uab.cat/workshopmrama/sites/jornades.uab.cat.workshopmr... · Food - Feed Waters - Soils Sunscreen products ... Over 40 years’

International proficiency testing programs ~ 19 ~

PT Cosmetic products

Proficiency Testing Matrices Parameters Weight Round /

year Sample /

round

60 - Sunscreen products: SPF in vivo Sunscreen products

Static in vivo SPF, water resistance… 30 ml 2 2

63 - Sunscreen products: UVA in vivo Sunscreen products

in vivo UVA PF 30 ml 1 2

64 - Sunscreen products: UVA in vitro Sunscreen products

in vitro UVA PF 30 ml 2 3

85 - Microbiology in cosmetic products Dermatologic cream

enumeration of yeast, mold and mesophilic aerobic bacteria

20 g 1 1

Page 20: Food - Feed Waters - Soils Sunscreen productsjornades.uab.cat/workshopmrama/sites/jornades.uab.cat.workshopmr... · Food - Feed Waters - Soils Sunscreen products ... Over 40 years’

International proficiency testing programs ~ 20 ~

CONTACT

BIPEA CAP 18 - 189 rue d’Aubervilliers

75018 PARIS - France

Tel : +33.1.40.05.26.30 / Fax :+33.1.42.09.26.85 www.bipea.org / [email protected]