fhoh:: marian murphy, tat region ii :i: ,^| ,m subject ... · cuetoiner nuimbei:;: t134ii...
TRANSCRIPT
$ Underwood €!:,.» UdLnm,, MJr OH3075
TECHNICAL ASSISTANCE: TEAP4 FOR EMERGENCY RESPONSE REMOVAL AND PREVENTIONEPA CONTRACT 68-AVO-00.36
J'amie Fenske, O.SC, 1SPA, Reqion :i:;]::i: TDD # 91 1 ]. -- 2 6Western Response flection PCS #2035
THRU':: Hike ZloRlei:,, TM'L, Region HI \
FHOH:: Marian Murphy, TAT Region II :i: , | ,M
SUBJECT: Big John (1iEi S.EI m pi e:=s A:n.:i].y1:.:i.cal Review
DAM; January 10, 1992
This riEsport. covers the review of the ana'Lyticai d'at-Ei package forI'ive (Si) drum samples and oine (1) ssiolid ss^mpLe collected .Eit: the E3dgJohn ' s S it a O'ti December 1.0 , 19 91 , The samples were received atPrinceton Testing on December 12,, UJiJl. Three drums were .zrnaLyzedi:or volatile organics (VGA) and i:lashpolnt,, One drum was analyzedfor FClEJi-!,, and one .drum was analyzed for suiri.tes., The solid samplewa :=; ci.m EI !L y ;;; e c:t (: o t: a. £= l:> E;; £3; t: c:> E= ,
AKrAlLYTICAL METHODOUXS-Y
The VOA samples were analysed in accordance with EPA Kethod 8:340,The FOB sample was analyzed In accordance with EPA Method BOH 0 „The flashpoint sajDoiples were analysed in accordance with 35! FA Met.hod:L.G;»O , The sulf ite a.nalys ].;£> was performed in accordance 'with KF'AMethod 377., 1., The solid was analysed for ass.bestos by PLM[«
Signed chain-of -custody records were received ,
The GC/MS tune data for t:h.& VOAs and the int:er:nalstandard , data were acceptable,, The initial andcontinuing oalibratio'ti, data had some compounds out oJ: QCcriteria,, however, onLy 2-butanone was qualifiedapproximate,, for sample DO1 . The matrix spike/matrixspike duplicate recover ie:=; , surrogate spike recoveriesand relative: perceril:. difference (K?D) values wereacceptable: for the nosst part,, The method blank contained:methylene chloride and acetone. Samples DG3L,, DO 5 and D06ss.hould be considered not detected for methyle:ne chloride fand si:i]iiple DO 6 should be conss iciered not detected foracetone.
Roy l:. Wesl:oni,F Ifiu:.MAJOR PROGRAMS DIVISIONIn A!J««i:i.,attioi:n vdlh FoisltBr IVlnEnehiJr E[ivii''E'ipoas<, lnt:.,r Resouircis1 A|]'|iliu||ai||p:Eiatjji|i|.jiC!,.. &: Miillho'itM,. P.C,R.I:;,, SiirdeiM A:s»iKiiil<>!!, and GRII lEiirviironrnunlal! S^irviicesv Inc. ' '•• ™ » '«J U O (!. J
Bio; John's Samples Analytical ReviewJanuary 10, 1&&2Page 2
• The PCB calibration data was acceptable. The methodb Ian3: w<a -t 1:r EJ EJ o 1: contamlnation., The sur r o<:|at ei :spi-L.Iwssrecovery for sample DO4 WEIS lower than the QC limits, butno PCBiEi were found, therefore no data was quEilified, A&:M.O' iP'C'KiH. were found, no second column confIrmatlons werepeiMI'oncLtrid.
COUfCLUSI-OH
Accept the data as presented except for inethylene chloride, acetoneand 2••'but<-inone. The methylene chloride should be considered notdetected for sainples DO!,, DO5 and DO6 clue to blank contamination.,The aceitone should be ccnE5>idered not detected l:oi: saunple D06 due toblank contamination. The ;>--'butanone should be consideredapproximate for sample D01 due to calibration, outliers.. It i-sho'Li.ldbe noted that any volatile analysis marked '"E1" should be consideredapproxlm-sitiE! IE;ince it Is an estimated concentration.,
flRI00630
aas iMl C
I'M-' 'F
J»"l -jii: .»> •
iii ]!.!! "'
O ji
<•<"
'v
aEI:O(.3LIJ
no
E»UL.c>
u
bK:IJLI
;<:g> ;E:
i.. •••• , «•V.J •»-
ci! l"~i *5;
ciIE:
ijli
9 '.!
4 '"•:
fl '
SSH
-all'-.
iri]::a;jji]:
SN«S
x NNV NX,s NXN
N,
-
\
U
i.»LI
ac: (. '
N\s
-, S-1*s.
O ]J-
;ij
.......•> iE!
:ii:i.
<;«:••»
(
c::
|s
*s\
'«»X
x<'01.-. ||:
I1
?it
I
t *
K•1t:c:.ji
ih-«tIh-
13't'ti'i)
•dwcoLLI:E
lUUi
ii!
'S
1
\,( 1
*
— 1J....... jj
I I
>\ !'*
•-J.Ii!: <!
C
!s'k,l\;
>• '
I Is,
>i !s;\ i
<•
•I
'<(
|.
P*!:;f-
•iIs
"**
\
•i
•1
A ......) '
\
5 vi 'I" ):r-
;
J
;lj .
<'
i
•|i X,\
;if-p •-
>
s;N|
>('
<«=I,o
::><;
sv
i;
M
\ f
isn(S.
1
,;;;
it1
-j
a
fX
V.
V
I,;:i
'*
's
1
I
V
-
X.
'si'
r
.
|!
n
X
.:
'><;.
^ki
r '
!:
-1ji
Cstj.
)
0
1JE1
'>1C
• I
<:
C:
,-J"
'!<t
: -.j
•j
0
'N
O0-
iP-ll1
«
c
e.z:•1S.I
n
i
I1.JE
..k
'*..'.I1:
• •
'0
-
r.
1:'
'i!i!
| •'
i::
if
atj::
C ;- .1
'«!ia:
•i
jh!;>
"iiiIE13:
i'Ma
It<E!
£ \u.K >
i|-:|
r s,
•
3;-s»•v>v
Jii
iii:•ii
>'iil<iiice:
.1
IB;illO
•1c:
.j:':5i
'(Uu:
1
>\ !•'
MB.^IIS
II, EEI;;............• k*Bl
if
I
.E:H: ,
'HI.*:
ice: . ..
IE'i-(BflC3
Oiii
'iii
Ii ili }illi:::4->
:r
iat:
LL!
LL
j>i:ViiSoCka'e:
'IEiia13
C'(Ii
i:O
»
ni! p'ti Un. ife::.!. .!':
W<=;ston TAT!:» Und.erwoocSi Court
Delrem, New Jersey 09Attn,:; Marian Murphy
JOB $ 9:i.08360-001/2GN
Mornbor: 'Arn<:r;;,3ri Cruncil of Indisnonc'^nt Laboratories.
Weston TAT January :» , 1!i 5 Underwood Court Joib #:: 91C(3:n| Delran,, Hew Jersey 01=1075! „. Attn;: .Karian Murphy
TABLE: OF CONTENTS
PAGE
SMPLE ANALYSIS: REQUEST FOPM (SAR)
CHAIN OF CUSTODY
FLASHPOINT .Sc SULFlTIi; RESULTS
PCB KEISIJLTS
VO L A T 3C 11, El ORGAN I C F !ES S '01,7 S
ASBESTOS RESULTS
Muirber: Air.^ricairi Council of
iiiiimiiimiiiim
•u Page l of 1 <:oi»-c
ji p "i? i:o;j act No„ :; 9 X083 6 0 •» C) C) JLG'KWH
Weston TAT3 iL];ndi»rwoocl Court Date Received:; 12/1 :t / E) 1D =: ]. r a n, N e v J e r ES ey 0 S 0 7 3 .ft n a 1 y s i s D u & ;: 12 / 2 Si / 91
Attienti.on: Marlaa Murphy Number Oi: Samples :; (5Phone;" (EJ09) 4(51-4003 " Number 01: Containers;; (5
Cuetoiner Nuimbei:;: T134ii Report::;:; Standard Report FormatCredit By:: Heather MendelApproved By:: Susan Sharpies
001 - Sample D01 •••————» FlashpoointPur<;ieable Volatile Organicsa; By Method 8240 Page 1Purqeable Volatile Orga.nicssi By Method 13:240 Page 2
002 - Sample D03 »————-• Suli:ite (As S(003 - Sample 004 •••»———— PoLychlorinati004 - Sample DO.Si
005 -• SampLe, D(3(5
)3) In Solid Phasesd iEMphenyls In Oil
Volatile organic® By GCMS - Method (Volatile Orqanice By GCMS - Method (
Volatile Orqanicjsi By GCMS - MethodVolatile Organics By GCMS - Method
24 Page 1i24 Page 2
i24 Page 1Page 2
006 - Sample A07 ••-••••••••— Asbestos In Bulk/Non-Aqueous Sample By PLM
Motes:
1. Samples or.i.ginated from Weston,, Wheeling, VJV .;!fiO(>:3..2, Kxtra copy o.i: report to; Roy K*. Weston^, ][nc..
141 HacldLeiEi lUin Rd,. ,, Wheeling WFV 2600:3.,Attn: Pat Bisshop
:s., Samples ca.mH; in after U;;00 a./nu 12/L1/9:L,,4.. Per Client "s instructions to H MenzeL,, l:or Sample D04(, run only the
oiL portion l:'or FOB,, Flashpoint to All Service'.S3» Plea,,se sue. attached, list for Detect i on limit,(3... NOTE THAT FOR RESULTS EJCCEEDIHG THE PRESCRIBED TUmMWTOD TIME (IM
CALENDAR DAYS), A REDUCTION IN THE TOTAL CHARGE WILL BE THREE1 PERCENT\FOR THE FIRST DAY, TWO PERCENT FOR THE SECOND DAY, AND AN ADDITIONALONE PERCENT FOR EACH ADDITIONAL DAY,.
;Joto -I'yp©: Standard/PLM
""""l:i:iI:S;l al'ii"/i- " "Reoejwed By lab;: __ ___ • Printed By:; Chris JamiesonQ« A» PP:roved: ————————^ ,| ri | Q.|j3|jJ ,37: i%................................................. IHi MI"
Misnnb'frir: AmfTicari Council of IndEiip^incUiru. Leibc)r;ji:orii»i,t Ini:'
-- .;: •;•
;i: - " •::' •
x't $''' "•:: -: •
:\
,}P(
•;s-..s~-
itjLLt••i ~i
O ,:;-f :~
C|
cr"'iM"'"k. ,
| ——— <onD<;„>
Oz;!•••
MM!
T!>=[• ,,;
"' '•!(
"s!
;l' ->"j l!:C. CJ
..c
!•I ...*• ;.;
-; u «•
;-,* '"" II1
r£ '"' 1L
o: o u•;.' :j'u «'s. "C/3
a>
CL
i
o:«:UJ..jCl
cc:
cc;uj!:: D-.K ::;,, •=(
O
UI"t; ..4 'j; (— -t< yjto u.
1. r
•t•;;. =3
jfijiii;!j'ltlHj
i[l3i|||EI|Ulllmll
-r»•r.;J«--.
L
c
•--kJ
"
V:;•*:;
a'..
LLJ."to
]-• :j $<j .«:. «;.i 1 ? i«' <:) :i: c(....y.JsL.S:™
...."3 i:°: 1-3 ;!:t»; :;;». „</> .c:iii «j»! !2r"3. 'tf•'• 5f' ' s:i ;
u:UJ
1......
-
:z:...LU..1-IOu
o,K
UI
i-.....UI
u
!1
:
1i
—————————— f —————— ———
?-
.;.SSX '''I
ssNVvJ's^-l
*"T-
'5-'"-$''\]*'O1>.,*'
(--L.
V£7..........
<1c:
D3
i3:
°
11;
*"•cr:h-;
3:
-v
v "?;».'
;>:. , i"'!!i f1'** !i*
uj1:1
X
!
1
'x•A
'XSii
>5rs, J_ p.* **s-."i^ v. "t"1"
',7..........
..........
""'•
Y-11 ss(i
'-•-J
.s i
\\l
x:>*'••
']\;
'X\k C' "l lk " '
J' "J:*>;'f-s;:..
\::;-...........
X;.---s.
v,!?..........
ss ...,
.-;N
*"•*•.
- ';;•;^
\sSs-
•*-->' "**-,
,s.
. S;
,-J'
'0•»
, ."""•v
•s' ' 1s ''s<!>?;. v
Xj,
.... —— .
VJ
N.
„,
.............-..•...
NsS
: ^ :
i
i
UJ
1
1
v.33e'JJ
q*;a:UI
01'J
a m •«-r »•- :sui <C ii! ;;; H «:
...........i........
!R G D
i:^~Bii
j
1h:>.iJj-
!•-(C
1-•a;
C)
..)•a:
«; '$o o
"J*f[ :S-
ii«:1
C o !ctUI»-•..i
iji !i!i: '.: -=. ;;icc; <c .. ,-,o » & ::!:! § 3 S
h-
c:
;j'ii3:
...|ii-
||
i
i»'•;
jr<j,'*• ECi» :::) :K -j '
I' -5Cr ? SIj^Ju < S
II) <( 1" <c•a: LUI <i: i\..t i« <k. .:
;.
1
Ji.
O
! j !1
; I > l[
;I i
:;r
.fi"*
i A[ -" s
"'*"»
i-\
\.' sNN
\\ s\" !;.
\/'\-I*» 1 '
~'*"" (*'*'' '*•$ ,
N«^i r- t .' \ [••
13 ^'/---" "i"s"'"' ,
£
;; '.J "
;; ':-' ^ p•1' .-- >:: 0
,; l'_ >•
\ f*'1 \
UJ•" vo
»""•>.
':;;;.
*s.JIN"'[*»:>Ss
<-"•.-1•v\J
1s. •x i
'X*
I(*s.Sj
L
j:ci
"! ..j:
III »'a «,111 |!j
ui i!ui •;
11!
' in l!S s:
Ci c::?• 1!.ji J;EC iii
,v•j"s*x1""'V'^'Jsv
i"r»is\KN3S
j !;s.""- S
- ")r
x1 -^/k - ,.
•..:-st
,_'''-....,IV.1
'"?
\l>
If*;s'N*ss
:-i;'-,
.1
('* j (
,, ,
ss,_
;A
s"••»
i.'*'
"
f
J
I
....
.?*•s**--liV'1
':;?;•»-..'k'L
\v!is Hi
s\"'•ijiS'llN\*
V»
>I
'<:'-.-
*s.
\\\
<:-<
/'N^ S*"s.
\Sj,""'X
*v
>Si
' n
^
S\ *
i[-\ IVv~;jf . j1\ »„> '>S0
r; i""\•
S
,
/'\
*;*s3
'ss.
•\ ,.i A. r. •1 'J \i U' L'.. .....U
P.O. Ho*. VIC&3490 U.S. Rnun 1
FAX [609) 4S2.(
WestonTAT '" Report Dale: 01/02/925 Underwood Court Job Number: 91083(10-001GMWHDelran, New.Jers.ev OS075 Date Received: 12/L3/91Attention: Marian Murphy••i;;::::':?::':1:?: ::^ •' •:':-'-:.::- • .-;••.."•:••::•;;;:-•• , • •<% ;.:.-•;.. •"• • ;= -.;!;- -: :• _,f~: :;.>.;•-_; •:;•;•:•.•.•-::-•;;: •;:- ;•;• ..- •••', ;•.-'•;:/:;-'-'':•;:•; ;.;:; ••;•;: Wf- - : " :>::,'-:. :;;:;- :;:i:: i:;::-:i.:;;.:}:.:;:::: ;.••••.•.•. •i:::"... -i::. •• - ••' "IX .;«:.. -: ;;.::U.ii-i.K1!:. .ii!;-:: :.:::; ::/::l.:.:.:; ^:1•l;;::::S:;;;:v.::.;::,:ii.!.
.J? ; 5,:iip-i.h? .OC1/ Sctrr^.h? 003 Sampls DO5
i: in <:lr, mg/k,gw .37K £•'? , SOO
,. 7%
.Z", L) . : Sample 006
Flashpoint: i.n degrejssj i:ahr«nhi:!:Lt: 13T ].-'::• C
Hot.
(2
For inquirujis CEill u:s at (609]' 413:2!-HCISO and ask for our Customer Seivicr: Anmrkari CoLincilicI1 Inclo^oniJisint Uahoratorimi. Inc.. l" '() (J (J -
P.O. Box '3.1083490 U.S. Route "I
, N| C;3,:I4:K3K)8(609MS2-9050
FAX (609) 452-0 K7
Western TAT '" Report Date: 01/07/9;!3 Underwood Court Job Number: 910S,:!60-001G:V[V/HDe.lra.ri, New Jersey OS075 Date. Received: 12/13/91.Attention: Marian'Murphy
II ri OilU rills.: rnci/I<C|
T. . D . : Swpl.a DQk Blank 12/23/9.1
1221. . <5 <5
.1232 . ' . _ " . <5 . . \ <3
1:262 _ '' " : ". . ' . <3 _ " " <:3ArocLor I'2h& ' ' '"" <3 <3
.125 ' <3 <3
U.60 <-> <3Arocl-cr L01.6 . "" ' '<3 <3
RECOVERY DATA
•fe_Alcl]:J.ri (Suirr."} . . _ (.55 --lASft) . '. . " .; '^i7^ " ' 1.55%
, SupervisorGhrom8.tog.raphy laboratory
Low . TEscoveiry due t:o exten:3iv« j3LilJ:'u]:i.<:acid . cleanup; . ' .[.-..• ','. ;..'•.'..:'.'..
For inquiries call! us ai: (6:i9) 4f52-9050 l|i"i;|i|3l|1|:|f|:|Iji'^ S«ivic:«
r: American Council ol IndigipEimlonl Lgilhor.sttorios, Inc. h» () (J. (\ ^ ,1
L, : '-'<. r, ,:L i" :. . c: : L ! t .:.' •-'
r •=»••;: ! -:1 ":C r: " ''. *L -" : •' "O "VJ: '
P i"' i n c e t. o n T e s t. :i n g .. a & c- r a t & r y A n a 1 v s i s R e o o r t: .
;-: •:•; ':; .:..-. ?:: ::•: sr; :=• ,•• • .1 .....
: 3.MC H;:";,;-.
In factor : 25-7' C
' J ,J . •' j (;[',. L;:^: 1 i , 1L5Z ;.;.;"; '!»,:.;>.,:; ! *; I . • '. '."'. " .'•. . ' : * ;'•;•„
K ]},$j!) ; i';-! •"'.'. '*".L* -« ': *ii'" '?^ ;*;.]"? •:' •::,»'•: •'•.'!'i"" :!;''. il.!M :>!!v!': -;.^;: -!..''i::i -I..''-':-' ':!'v:';; -:•! ::.;i: *:; ::: ;..!!)•• I !!:
..».: - .!!' :.;.!:: !..! :i :]"-•. . . ; '. .1:. :.: . i1.:.:/" -!:v
'V
ARI00638- 00005
::;:'K:::::^••-•r*'!;;';::":'-'':';-'''v. •••• :-'1'-':L-''S'y..;:::'••-'" . • o ''•:.:.'•:•;:r '*"•'•;:";: •- V. '•/-..-•?'-/:"- ••••;• '>-'.'" !: ":•"•:'>* ..;i; "•'- • """T ":<"r;v-: •".-• -';-'r; -^ %•':;.iilta:.::/. :^ •....:. .1. „,.... ...>......,: •'.ii.-.-j.::-.:. ., ,!",.. ::....,:..:- _,,;.<..'.... ;.„;.-. .,. .. .. .,.„_....,.. ...,.., ;"„ e, '\s
Is 'X, ..„ !
"" , ..„! i.:s.:>CC— — I ;
'7*'"V" :'": ..... ""3"
ISO
ICO
2-— i'
;>...:::•'....
ii
IIi!,1,l!:j
•t\*.r. fi:ie : O.CO nin i;ij Iju • : JLVij j;.r !.:« >•:-;;; L : -ljii.0':•iJC:^- ;:2-::tor: 0 - - =:;:!; OffMt: -l^i n- • Plot :al«: :!!3!)-i[i
... ... ,„ ...... ,-. --.......:... ' . - , : i . i :
; : •.
.;;:i » -:.; ;i. .::• a. v_or;o o<r ? b ;::» -r:' -r ::r '-.:>-: oD o
10 LS :::oi • i"t"i e [ - -"i : '"\ J
HRIQ0639
•:',:: f •: S.-J 3 •' ':• ''' ••:•:' '=; 1.0 r• : :'• . i -". ". »•'.'.'. .:!• -"'£. 'i.~: • 1 IL / I'5-'- •' ° i 1 :- : •-•':.•S .li "1 G j. =:: N 3;: • := : r..: • •*: 0 " X':; & C i •:: C ':Dc.t.,=i F :>:«s : •:;: \ 2/oc(. .::!.=.t..=i::;\r::.;?-4::
•=5'":L: ?= PC;=J " :. ; .:= : i~" :: \ £ *7 -*0\ O-—Vi.!:" '. 1 I.<: -i J; n.sr :-,:rr=;r--:: • : v^-i"^.^ Z-iOC i:-..-.c:k ':;.^i;i" 1 ;=: •-!-•::•:" i". " J. . 0 :00
P i" i n c s t c n T s s 2 i n g L a =• c i' a L o r y A n a 1 y s i 5 R 3 o o r t
••in-
I &.M1 S-=%
& L.*T| i.KN L.SI7? ^(J&Sj-ZJi) •ICJtSL.:- v: —-•
J 7JQ"! V3%: \ 11
18 ?.21* - J..9Q*- l.r??? ?[UI3M.7i! ZQ^^l.^ <\ - . ..1::1%"H 9.*U 4.M6J 4.U64 4?3S7vf.'}0"B4]:L]:''\'-"-—— l.l*iZ2c2Q 9.S<& AtOR!*! • 2.1*9] j.1591 33ZtiZOS.53541?*S.l-.i:"3.1:[l ^C - •/:"!!.
?I %Q.Li] L%5ZL LI!?! i25?:73.S? L.124:^7——— '. .1::'-: *
25 !3.:35 i!!.4'li il.*3L] 1;""1;%(?2 I..'"*! v* ....... -.!/7:2i !?. ?"? "EFT? y'.} E?0! ?.;&]& ^.lt!t 3^j;S.t%(l2 1. ;!.•: *"< C.:1L^ D:% '.::;!?:
?E 11J&? jS.&Iio 2!.&3#2 2J'i.-^Q.?E !./*: ' : —•-- i.i^E19 L"1.!T6 *-EHLC?^HE. kl?33 M033 I4? 1J1.'J l?&m.-* E* -;.??'4 I9C - i.iZO'a:
4\ U 11.W4 • 2.156? Z.15H U!i^36.U2?28?3.44?#"—-'"'' 3? ' 11.806 .'EMO 1 Q.?%0& • 'O.nW 1355@1.»' IOU@?,!.7 ',7 i)J2;8 Q3C" 31 11.9H A*CI!i.C';G:NE 5.M55 5.Q9U. . 3^ 12.018 4JZ6& <.1?(,5
6 i?.4i5lo:ELORIK .' '4JW. <"%+.2%WH' 12.7*7 "Q&E"" ' 11.3JS% • L.3553
{^•.M"13.@]*.-EHOAI% - - 11.M75V' n.im .')2&2D6?,0'!'t66334.9nV-CJ31J.D:c "^ . -"-•" -sr u.??i Excoi -i.6?*5 '. -s:*
ARI00640 " 0000?
.[:.;'i; liMJ?!!!! M;:- 'i.' S 'i.v:H 3^hi;!i!i.i:" ;••::=.;. •'' ''i! |-..L:,if. ;••; - ;.$:;':'
,.i ".;*.:;• :>iJC;':!i:r: T.f.i'1' :';.^-7" lU!:!:::!.(0 :i. ••;.•:: !i\< v).):'!: :••.;*:> ;j.:;: ^i : ,n:.i I;;.:M:J 3'': ;.;: •;.;:i-: v/ -;}.-i;i- H:
:.i.j.]?; ^...io^ ?;si>:?!.•::; ^'iiii'i.^ vv -----
(l.lHii 0.1I-I2 liJiiiil.i1 i'::.::;.:;: :'' - ——
o.:;:^- :i,!'-;:i • I,::;.:",:- [::':••.••: \\- :.' : ;:-;:•!.;.-:'; *.;:;: ::-:~:c..'] :'\i-\.:\ ••, - - - - - -
i:.::,: • i;/':':i (>.:';:,7 J.r?M: ,I': i'*!: .::! l: ------•j.-T1? ;.::.:':(;,::: -'' i-!.1!: S1- -----
. % i'f'"i ..'. M'lj 1 . „ i •:: ' •>,:"'•• ••',:.i,!;! i • : ;;. J J •-;.... , J ..• • <* i. . ••
~:.'.'.'.;,: "i... js. ".;..:,.: ::..'..;.-i.051: ;,i;;;i:: ::i'M :"'.::• lirii:.:-: :::
v,:ir j r." ."--:LCO :7 :: : \ '! .=: -y C,: l^rrir:
•f i: [•• ''•;•: : M:i!- i r: :;•;:*.-M : ;:1:::;: :.::•>:,•:• t \\\* : •;.;••: ir.:;:>: = f «;;••: t1
-' ' !
:''
:,-.:;;..' (..J
..J ! I!!- -J i III
...j i I!!ii!' !
-J 1! ii
- i ! ! : l
-1! «i2-;:00——i :• ilj
.-'-'.—-• ! !!i
I ;
i=-o^i !!i!'
""i !-]! if lilSii'i1^ f!" i-wjiiii.!^"'. | ,., ..... . . ..
I • oo u 'i5? ;s w IjJii;;;:? ;•? ;2;?:>i £jj (jJ LJJ | _ ;:• {]_ v.-C_j» ..-•(;;) (;;i ;:jj ("j f—. t..' L!J
I <;' 1-1) C*l III '* 131 CJI^'Ei illHj.J t"; Li..1 LiJ !!*: 'III C"i|...... ... .....T... .....r™--r----r:..-:::T™::.r-:.~I, ' ' ' ' I ' ' ' I ' l ' ' ! ' ' ' ' I ' ' ' ' i0 S 1,0 . 15 . 20 25
..'",' ... Retention Time [rn'inj... .„
OU009
•'•'::'- t:..'i.;:.--T: V^ .• sicr - S . 1 i:-:-..: :• •
::.=.:•;;:• : /: N.:-, -:: : 1 ;: II :. OO'.'i-! •' LT'.;. • :.-•, " j. ! •:• : •:: : \ " "'00'. ••;:.:i *.. .-" '• 1 i. .. i. •" .1 •"• . rv:-.<.-j •": .s-...:::•!.::• • .: A'i»:: i: : .:: •'•::••:•. : -•"' -:.::• •• ;;::.--•' •»:: • : - -r.'.= :.':...M,ri^-, : v^P. ]:--^ ,"- >J i^a.::« • : -:-. L : 0- 0
Pr i nC'»s t ::n Tes t: i. no L/bora c.o:-v Ana Xy=;:. := Fs.?=:oor t
.!.:•:! fi.'-::-'!.)
; ! *( * ;i 'M'*i .1 -.'i.i.'i :" v'. . >: :, -•i.; ',:::;.......... i,- • • .:£ . J . i . i _ M.,;y'.- J,;:;j:: ^.. 1 .-•>.:. .•••"..;': .!! ,..: •.•.,':,'
l:.!lj!.-i :.-.'.•;:'J'.• •'}'.''.'.' ;'•. "-U ilrJ:!,1,; !i' -••-••-••• '; .'..• jC.v;'.'. *,:•:', ;. ,;.'.Jr.'.-'J vj L; :; . 'l 1 ! (I'!1?, i i. -;:!; -•••---•
j.isoac
AR1Q06U3 - OUO-.
-1500-
.-* i i;sooo— • !?
HI!
u.. 2000—i i:r.n -1 i I,71 Mil
.,"". —i i :-*-- "i l i1500—iJi
-in
. .-. , .| i : •• • •! , .4..
I <
•;..-• < ... j ":i:::i < ::;::.:• - c: o L.JI:::: o -.x. o in oou'i O'~"'ir: m oo */"':••:'*> -- CM K>cMi-'l --r --- c: m .or i'C r--' 1 -(-. -' ,'.— .C'l-l .'fl ••'• - ". ,•." 1.- ••" -," -,—^ - -*.. <t.l J..-J.. .A, .•„ „ ., - .J , ,. .._. . . , ,1.-
' ' ' " '""' '' '"''' '' 1
i i • i0 5: ' .. 10
- Kete nt icin I i r"r"ir:: | r"n i r\ \
' r :L n c >=> t: o r. T •:• -•:. i ;-,.-:: L. .=i o 6 " & t;:; •- y --;~ a 1 v •=: : =; : .-= ::• c: r -
;.,;•'. ; •„ .
, „ . ., .
.%:%•
::.;!'•!
;: :"' ':''!':'' ;! """""
.: -; •: , i : •>
.. ••• >."-.; .. •' ,
i '"'III:'.---
'. '.''.' I '.'.. '•'•''' ' ',
. .'•: •:.:. '.•'-',:..-. '•:\ '\:'''.:: y,'• •:••.'.'• \- ::.
'•,:'•'• ' '• ':'.':' : i ::
•; i: :• • ; .-',"• ' '• :: •
::•':'!; :-; 1 • : - ' ) ' , - : : ''.!'-:,"-•!'.'" -.::':; !; :::
V .=•.-:. an i:-:c:? Csa:::! 1 lary Co 1 j rrr.-. C: : : IMi; - o C 3 :;0'-' X C , ;:.;i::rirr'
ARI006H5 f
<is-:!!i» I: ill . ;>i.;g. 1 ;f I ..
;:;n >•?- 'i.'1
i: ,,. " "|
RR1006U6D i) n
Sof tx.?.re /srsi rn: J. i -'ZA23.'o .;.;;•::: A .i:;:;; . '• : '": o;:S-amc le N.T.rr;« : I 01. •:.• .:' C C;.••.:=, '...
i:a Jr i 'le : -•:;: '."cov .-o. :,.v,:'\ 1.1 •::].•:;;:::..- .-.-> :•.?. is: i:./:: i /'-';.-eoijE-r.c-TS. " :=:«.: :•: -::": oo-, o.- ~ -s ::• -, ;L :.::: -:, :•.. _::«;: : , :: t~ : :::: •:•••..:.-.
f:' r i n c: e t: o n T «•«. t. i n <u .. ,=i b c^ r- a t: o r v
t ' I ','. . ;.'!;• .1 -. !\ 1 "1 i;. 1.' .• : .1 •.'•> :•. .:: -• •.:J .1 if?;! .'in: * ,1- i/t{ ^ .:.-•. •* - j . s t : ; •••. L-v j'.iT i- t! i ?•:;•:: >'< v- i'ii „•.'';-i *. , .:.-:., i.'.'.'wi!
.1 l; \.:'i fl :"':' >"i 'Vii'i'l3 !i.;f;:f :„;«•:;• '•.Oi'ij'.
!.->;;i !;.-:-i:(;3
:!.!jfi.i: ; ,:•;.;[;; ii'r'-I'ilJ ji! :-M:.i- ,L!/ '•'•
ii.JSK! l(::;'':i. : :::::.:.•: :il ---• l.ISC;:;.-
A .r- i .=t n o •-; C) C) C.«: ::• :L 1 1 a.;" v C: ,::• : L. -n r- Gi C. : D ir: - :i:: := .: ."' ;'-i
"': : rtr:- ' ... • • . .,ij lr.v.jSJ-t.V:,....,...- .. , ,_.. ; . ... • •„• :
!'li>)S-!?."••"% • -"••'-" ' ''.-''•' - ; • • • ' ' . •' '
0001
J":
tfi
P-=:«.':.i ::.:: •:!':• ; -: "' •• •:.' -. •• :: -:o :- :->-p r.:.;i-
ii: ijii:: :: .CLi. ;;::!K :;:!:::.: *: ^ ;i!;^i I :f 1;.:.-;:!,; : ;;: \ *' \\.C",\r.i\ "•.."-.••• '.i:.'i : ::./ii ::. " : l i '
.-.i!! ''!; s...! Ii ill . l|
11; l:r:i n
j =-
3000 — i :— . :
~"j |
'"! !•-i c: .-\.-\ . ii. „' •„"..'• —— -i !
"" i :— ' :
1i-=: "
i
ill :'
i;l ::
...: ;t :
H ii 1:;000— -•: !; :
l :i i
""" ji •
. „..., '-I- i •
i !:!
!
I !
! J I i i :, r:irr......j .; II
•:: -T MM!-'-'V- "i : i | :
' '| il l lil;. :;V;C :...
O" . ic!?!!1-!- ! 1:.---v-':
"~f "'""' r
< .... xo < :j::o< o L.JO o L.I >.o '."i oo-j'i . oom in oo m m o-r- Cs| rOCNH-rl r'0 l°.'•/*.* h j. >.'-. il.; '-«.* »'.,< X( l \/ i >' *'•
I I I I . [ ! ! ! ! | ! 1 ! ! ] ! I ! ! j ! ! ! . , ..-.p.- ... . ..--:S - .. -, .. 10 . ]..3.. :- - 20 .,. ... . -25
";'"'l.;.'-V"" :*• • •-•-' -;-'-•. ;;Rete.ntion Ti rhe :" { rnin J-- ::- - .-»•". • • • .,-• • • • •• . •«. oao
r«i IL
•:'OT :>j,:i - i- • •?.;
::;. =. rn •::• 1 ~ ;v;. ;-. •!- af i- - :r - ' ..-
-•.'I . :. :-
) - i n r:; v t,- n •]• ,=> .=: t: i n r-, L. =1 b o r- =1t o r ••/ A n .=• 1. ,' :=> i. :=i P ==:: c: i
i
,t;
J.:;,i-i'
-.-.,.:;j:;;s'i-
i*.ii.!C2!::•:i:'N7ti'3
;•?;:a
"•ilir ::*r• ,,;
1, iff*&.*:.:Uiiir.:*t•> , 1 •!( i
T H:
'!..S;ii: , :! . :
i!ir-ii. ;ij-•>.•;;;:-'.':;•<
,}'!!'! '3l1' *":I'LiiJ.LH"
JiMSi"ID.SSi]i).?:i; C£:?: :!«i!J.i«iU.iJJ-i!.i.i;:iii.^;' ? 1 '• ».
1 ! . i •:. ':::.'sj ::•::: :••:!;:n.J:-J
M.:N'J
,,;a:f,: :,-,,.-,,, ,,
'•'.:: * V:V 3 l . t r ! ! : rr
i i;!!» o': : iiiiiii:r T'!';,: :i :;;"• '.: mf i"-j.i:i?-> -s.v;™ i;'i^,:i;.2'»::? ;;- ;::•:•:/ ?M:iii: jiJ.L:':: •;.:•::::• n;:-ji,:!.£.:.:;> :.: r ;i:i;!;.:o
?..<:;:• 0.30C;:- ;•:•!:!:,".:
:•;;:; ••;;!: .:;:3;;';;?.:•-'! ).-j:S35 ;-:»"?U!.34L,?;::.i J.J-^CC- :?;S: ::,-:;:.;«iO . =•.;•:;;« ;i:-:';v!*.r;-:.;!;••.• •;.]•)[•:; ;•;:<:•;,;;i'i-i-" i'ijir" wj!^'-1;i, 20U ':. j'Jj i ;:!0i:'i' .; i^ , S i i £ ; 0.3:!-j;: ii:^::.:;1,3::-:: j.IOO;; !'J-::i.s:.:J5.;*;:=: ?.iv.=; 'i-*.!':.;-:.»::i. !.]::•::! ::t:'iM:.:'J;,&;i?;s :.:-.; j=:- ai';:1;-.].;"li : JCM l ; i i ' : ; . ' i" ii;':; " "•"•;" r*.:;.ii '':j. MS • ;, j.'iC" ^ :'"' ; '•?.::;•.[ M":. ^-j ij " =K'T'i i v"'; ::::M '-r!.::.-£• :.;::3:i -ty?::3,:!:.:(!S; v.3!:3!! iv:^i;,U
;•;-.•; != :.:;:::--
:-:- :•;':: .........
J ': it J : :: - - - - - - -j-Vl! •• " ..-..-..-..;:; -,1 : i '• ............
.irV.t],,v: ;; ...........
J •: :i .: i i: - - - - - - -
•::-N.:i ,-i. --"-:*.:] - i . j . 1 1; ..........
1 . ' ! :! ', ' t '.', ..........; . L . . • . .' •r '.;:,.". • -f '.'. ........ H ..
;;;,;:: .;, :.-, ..........
•ilj.;:..;; i\' ------
i:.:!.1:;-;: i:' ";')]:': '::<:' :;::;:j.ii.:!..;i :v •-•--•i!.::'::'.i'i •'= -----l(-',\ :':.';: :'• ••---•- -i-:1.1:!1. v* i'' "L .: ~;: ".'.'•• I ;'.'•> •.:.::,;;,_';- ,;; ...........
• i.L";!?3'.i:! -ii ••- — ••-•J.I-?::.:: ::! ••----: . ; •:. •.; :, ...........
" : . ;; ; - • : ...........-;;./;, -,-, -.;;;:• •-,; . . '-'i.ji[f'i! :; ..!..!.!!..
;ii:»].:-; i: j.:;;- ":^ .:;.-?;•j!0;?:.:0 i: -----
::-:;: •:,:::;
, -..>ii
l!;?xls: •;::•;'..: j[j-tji'li[.:•:• Xiii.! V,1;':;
• -.-,--: ::
;.;?:=•:!.=•>; :;•-•-:• :i,
I.X4J:-:.;.;;o(!2:.;.;i-;i'.r:.1 .:!••••: ::
:.;-:!j;:5-:i.;;-:--1'::.;,;:,;•.,.:
I-,.-: .-1 !!
L,:-;3-::-::.;,:(:::;::.1. I-VJi!:;: V"\';.:.
• • • y i . ,.
• -. ,,:.
: ' " i'T. :•
:.•}:[;••::•;. •!(•::';.= :i
3-1-00 Caoi. 1 lary Col urnn GC : i:Jl:!-603 ,::oi X 0 . Ir-In ;j.si:: I:or : 250 ""C" -
OOQIG
Pest it '. dr::..' PC-::; Cnr ;:>mat:Kj ra.Ti
" s fi: •?• '"" ;v;« i of isii].!:.::;!-.?.* fista : n.-n/'ii :':;><
- Mart. Tiii'i : C.CU 13.1 E-.I:' Iii* : :i!.0< ][•• L:« Pcir; : -i.](l.ili! 1.7 !';:;i i' M : -0(1.';£kale i:i::br: t ;'!:•; 0!;:':;: -K!) tV i'i:)t 3<:ai«: Si^ii li
3000—I•"!
250O--. .-•""i
2000--]-1
. "1
1500-----i
x <=.,"„-, -...i !soo..-p
• *" '
oi5H^?J?|U.A .SJK -J- T"i|V^ >!i l. \ !i'!il(l| SJi IC?"ir i . "T
-,.. J1' ' ' ^.jL..Ai:-.;.A:..fV!i iUj'.y.vwirPi-MifvH'- -'V\ i . II' « • : I I ' ' • . - '
."' :...j ! '" UJ ' I C",' "["i"l «"" """ • "•••'" '";
•.;"! •:";<";•-" :':-oi,!'i in
IL ::»
0001
':• o f " « 3 r = -' t: i" s i' o n : .7 . 1 -. 11A 2 3 :-
Samola ^ .ina : 1 -:- 3 5-1-CUG/ L,
ns c r:.<:T!S'i u : V' F. E AN :"-T 00 *< /= c \.' ' :..?. 1 : 0 / .7' i I1 ::•<•;: "-f.'. -;:• r : --• '.Samol «=. A 'O-j "it ; .. . OOOO Oi .. ..=: :.::••" - r. j; r•:,•" .:
iP r :L n c e t o n T e s 1: i n o L a b o - a t: o f v A i - a i y s i s R s o o r t \
^sait -«: Ms: CM:'-.'!'.' (^-:
. ,,.2 t.^W MIS.JRS)
i 3 Jii
j .. ;
'. •:.;
3 '.:„.
if;'1'?j} iL'.s::hi- l].i!3"!i 1!.::1S17 11. 733li! Li1.-?:*
?(! :j. ii] ii t t i; I'J'vr .-..; ;jvli -ii ,, l C> ;,;.;-j i C :!<.>
-it i . i'i:*. J-r. :., J
!U:M] :,:;;; ;y-,:s:i ,V0 [«; ::,D,1rfr:
, ,.,, , ...,. ...... ... .... ... :V ."i : v. .JC'i?'. ,;* .. .O" . '.-5 i.; f -••,(): J:.
i f ;^ > : f i; c •,'':;.:•);;••."-:;•:; i : j: ..•; i — •; ' r .. ''':;;;; ii.S,....1 i . J i l . i'J7 ':•:...,-• ;i ;,rlj, .-.;» . ..- ;.;.•••! "..,• '. ..•'j".f.1
J,.)!fJ,. Ij.l/vl.'. ., . .-:•.«. :.:i,.'.;. - u.
;.ijii'.: D.iJCiJS i:;!:V;j.:': ;:1'^'.-1 ^' ••------
v.'"1?;1 vi.iijo' *;j::-!'S.-;i> .; >{«*•.:.; /: ••-••-••-•-;.-::c- •!. -.!.;•. 0 ::•:•':.;,:•; .;i.t..:.j , • :: •:>:• - - - - - - -
... :.. v.vv... i.j... .:...'.., ..... -i.it.. » ...
•i /;•- <•. '('.(iji i';: •;'; ::' i:.:ji i: -i; ........... . .., j .. (j, ...............•.;•• .. j.jji :-...•;:••: • •. , • -, . J, •• ',, -••-••-••-
;;;;!; j;!;;; ;;;;;;;;:; •;:;;;:;;; ;';::::.:::: ':i"Wl;;:;; ;-|2 ::;i;:::;-;;; :E:;-:;; ;;;;;;;;;M f\i\.'. j ){\i)( '-vi'i'-'i !-* '1<:l(*" «' £'•' -.--••--
t , i!;i;; .i..;t'>: : i :!i ,. '. . i \- '. . T • '/ . '.• 1 ' '.. "• . , ' „ . ' • .'"• :;.•'•••» •»(•"! ii .1 vi" i'. •";')• •: — •: .'J •;::...........i , : -,;:,. 1 . . J '„• J ;:;..„•,.. . i .,.'.. i . .
!:'?! =::.:
• '.'•':•*.:.W..K<:C,
:-::!|«- "7.1". .'
• -rii^l; •••'••--'- •••'••* - • - - • -
:. .; -
• i .'..-. " . ,
:..0w ;•••••.
• • .r ,• • .
^.".Varian 3400 Cao.i. 1 lary Column GO : C3-t.OG 30M >: 0 . 5J-mm % . D . Oetec Lor,?' "In.iector: 250 C ' .
':,.";> - . • "•••-- ... ...'-."•' - -- :.. • • -i r'-:;. -.-;- . -. -'•s rv'--.1-1...-';''." - T - • ' • • • •, -V1'".;..-'-, .'^ • ., - , . . - . - .'• •••''-. i1 '"Tr " •' •'•!••'' ' '
0001
P;::st. i ci el-.:: / "';.::: Cl'i:"on!:ri :.;:*a r .=1:11
y,i^= : i;!*:* :icw:;;L :-!ii);i! t: ;:t n^ [ ofrileilMEi : 3.:\:!i \(!!l.!;:\:[!:;!0!.i.r3'» • O^ii: l!./n;)]. 3 : 1 1 'SUrt iii* : 3.,01) ni.i lird TJ.IJ. : ilJ.C'i ii..i lc^?;)iii!. : -KIO..OO i'1 Hi;jh Point : j/i!;:i!i!> ':;;:i::r: C Plo; (Ift'if!;:: -1^ n» PlM Sells:. Ii-Iij i1/
V 3COO---1 i i--! ! I
i...'.' J •
LSOO—i |,.., ,," " i l l
"!! / ^\ :,-- ...u: '• \*"M' i : %i ;-:f'::
"Ti I ! US . x '•"** i,) l | I :-. "'7 HfcSiiir::!. \*. "Vf" !i ii I...fjl " \i._x \,, -T jl ! ilMl|i||l!i ,!lv'> ,J!fUA. r 'L . ........„.,--.-
o-| -, ^ • '•" -\^ ''"
-c ... :::i::: < ":.:".r-: o LLJ:::IO ,_••: : :•;•;• >r o>"i ."• LO o O
u:-:-- co ,---:::;::: x :cr "•• » r •• : ;
. . , . (
:; • 1.0
k't 0001
Software v^rs ion : 5 . 1 ."2A21."Da La: 1:. '"::. ' =•! 9: 5^s o .n o ]. a '• j - s= : •; H L :: -. u -- N =: .. = o u > z, :..
,E: c Li a r* c F i ". :: : Z? : \ 2 ''''.".' C \ 0 A " 2 \ i .L 2 1 •'-- \ . = : 7 * r i '2 : '.'." C h 3 >'. r- s Lns t. rum = "• r : V A"! 1 AN 3—00 v ack ••' v ; .:• : : •'- ' 2 2 .'• s :' 2 C " : - •
oo>rno].'3 MrTD'jr" : 1.. OCCO :-;.:..,•;:..;•- F- :'::::• r :. ...
P r i r. c e t; o n T a s 1:1 n g L a b o r a t o r y A n a 1 y s i s R s o o r t ,
:| hVj -H
:: (!.!.i;i
3 Uid
* j J;.E rr** ;•;!]);•
£ ? c 'i
S 5.13?
n ?/i3 :jii-.; ^-src1) IQ.L??It, [0.:::IT I :\ i\-:ti , Lil. .'j ::
:? iij:5
31 !.Z,.Dil?24 32,t:!5 C:"3 H!:?"?!:.1-1. .25 11. sisM i::.jo :•;•; •:-i.v:
73 i ;;!•>:!
;IIC/L; :,?,.: •>*::] ,>,y] !H CCC-M-^ ^-:= .= -•:•:•
.,.;..: ; . . J ..- •; .. i .; . : :,'•.....-..:-,.. • .,.•..-•.:
(! "<;'' ". 'iTi'if -li^i] :i! '//'•" "" -T .•-••-..-. ' : ';•':.':.'!:.•
9'1 " .: '- .'' .'' V' - '••!,"• i ' J i • '' "• " 'i • ' '•• ........... •* ' i" '' • .
r.?.:.i'-^ •.:'.*!.••.!.' j' i"ii:: . '.•'; ',- 'i -: ' . . : ';*. -••--•-• ...'•.'..':
i.' . ;. J ,.- S J . ,' • j v : (.-.•: u ,'.., ! ..*..;•.: - - - - . . I.1 J .: . *:
•'. " c" T .-. -i.-.-.i1; - •:•. :<;t 7 ,; .":.; ;•,:;....-., '. ••; i". \ •
'.',;>' :.'.'t'. •; -i • '.' -..'. 1 , J ..•-„;.:.:..-... j . .- , i .- V
i TI.J: i -;f,i;t I.T::.; ::, v::: :•; :;: .......... • .•.-.-.-;
.»,... A ,--,,. .,--,., .......... - ...-.,.•...L;,}.. v.;,,. ..;..>.,-. .-. ...... .. ; .,
,.' . .1 i ' J '- . '.- L' '.' , . ,; J •/ .: T .... j - ..O .1 . . • . - . . ... •„• - ..
,1 .K:" -. .•,."•.: :n:" .: •:,-- " . ;;: .......... -.•*' .w.i.1; jj. -..-(-.-.••. ' fl j: .... ....Jr ..,*.,. . . j,. - .. .
i. . - i ,H -,r . -,r MJ 1 " ; .( 11 P . ! J 1 : • . ! j, . ;. . f " ...'.-•-.
r.!L?i :.a:«: n^.-o .: ;.<,:.•: :. ' ::- •:•:•>;•»- :.-••:•.
j.-'i.'i i . ^ i ' ; 1 : / i '.-*;.!, i: .:. !:.->i ;..;:• .. . : :^"; '';L-:r' " ; , , : ; i - - l
3- 00 Caoi.]. lary Column QC :• 08-603 30h1 X C .. S-Smm i; ,. D . De !: =: c:': o r : :!:OOCr:'' 250 C
000 2 G
^ ..ai
/ PCjij " hr -xnat.og ram '-. v " ' , . - ''..:••• \,':-:'- •
!:-;i;!,: VIM : OI'.OMW IVJM. . - ;4i:!ls r:: N . - P-KI-J i :•? i .!:><>!<:!(:! : i^;'7(l3\!ai,!;Ui:!i;>:<. rsii Jiit'r :' lim/?:: r;S(»iiUrl: TiiS1 : 'J.OH ;ifi ii:;! 'riii2 :• liO.C!) ii.i Lor t'oi il. ; -l^.CO iiV S=!i:;i F^inl, :. .W-:.!:) V
4000
.-.!
—!
(•" ——!
«." ""'1L.L "'I
1500
L 000-
•::,;'i("l .-..
n
'l .!3 i .!| n.
ii.1<1ir
1 -X iif-|-•-; ^;'-: ;rS-|l-d.l
:;l -::?j- Ii;!i:::l::
iiijji -i >i.,'«.V *—, :-.,,..
ioC' i.
r - , 4 • 1 i . •- - -1 I . , i . I ' ' ' I , . *' "f V'"'
.X:i t < :i[i cjx o uj,:::r o ix c: LI"! Y ">r » '.i'l ooio i,:": -:~ o -.o 1/1"S •'-- "M r-Vi!-: -t;- T-- O !.:". -::i"^ (XJ '*-*—
"-> i. .. i. • ., .. "r" ,.... .., fi""..v.. : ,. ]'~\ '":' * «::: i' •! i. i!-.-'( i i i i i i';::' • > i i t I •>
* • 0 0 0 2 !.
P,- i n c s t •:: n T e s t i n q .. n !::• o r s !: ::• r y A " a 1 y z ;.
r [z:.\. :I-H; /::;•.] ['.':•/< ;L;'-:-:.:!. V" ':" XE:m
': :;.;;, -.t -.." ! •• '"/.; .:!*.!•.."• '' - ":• ' -..-••---.
T .,;'" • •:;•' f "V.' .; '>.''. i.\.'--:- ''- ''•••• "• '•"• ••'.• "•"•• '•."' '•>'.-
•- :.-•:; -:.;::" -:.:,:• j-;;::!..:-. ;,;:::;.:: : -----: ?..:••: - - . r i r - - . i i : : - i^'::^-.:: /ii:::/:; ii -----^ .:;i :•:•:;' ;:v.:;; -;uc;* -;.::;-: -:.:;: .:: i.-::;....:1 :; -:.:::':; :-;::
" :":": :'';:": .::::::::'..'! .T:!'!'" :'.... ..... ..,.., . . : . . . . . - . . , . . . •
Is) .::.* I . : ; - ; - ';.*•-*: U:"1:-.:: :;::.;,i:.:. !-i -•---
ri :. .:!•» :...:?;: ;,:-:;: ::::•:..:. :'; :'•::-..:•:: •: ---••... | - . • . _._. .. r . ,. :i ,.,...._ , ,. . : •. • .- • ; .; : '; : ;• : • . ; : : : • : ;• • : ' ' - - ; -
.-•...: I,...!-..:....:..' .,...-'. : . - . " ;'...•... '-.........•• . . . . . . . . i. '
i! \\.r:i i.rvii o:i:: £;;;.;•*.:: *!:::;.•: .; ---•is !i..in ;.;i;i: ?.::•:•; ;i;:=;'i.:: J::»:.E.:: ;; -----ii ii.,t'.i :'!•.-(-• .. . .v:i.: r.-j ;;.-::- -::':1. : .^ ••;i,: j::-. :: ' > -..:..-,- .^ :••
3. J Jl.li'ii irC'fii.1"'" !1'" : " • • ' 1:> '''••'(• '".•:,::' ": :'T.'-". :: " . :: ' :> ', \ : :
1:3 I?-'1'1: * .: :: : ;^.i: :<; I;:S i: i."; -•'!::.::: : •• ••- •• •• -
•'•i ;" ! •• : : • ; ; • ; : • : : •>•:•• ". •„•':::.• :,i ; • . •. ...; • ;;..-;. ....... .....;•„ .;„•.••„• .••..>.••.•;•.'-•'
'.[ :'. :•:: •;'?• '•: • • ' ' :::T: ' : V- ' "' " "•:'- • i . • . . . ' • - ; 1;;;:" V - • *•• ....... ........ ..,.„.......:....,-•• ...... .....
, • ... . .. .4 . . . . . • . • . ' < ~ : , . • - - . - • > • ' •
? iiiil;;-! Ji;-; JS ;;S:" ;;;»;•» •-;:"• ;S
..... ... ,e; . .. .
. ; : r
1 ':"-
- .: . • • . •. .....
. ....
' . " . .1' .'•
.... ....
;.•::.?:•
.. ........
:•.::••'••::
... : -
J.M'j1:1!. - .. i. -
:.••»?-:=:. . •• i . ; . -
' '.:;r:i: • :
;
'so n.m -fisfini iiiijf i.;^- i.nn IMSSD..^ :'icst;!.2s vy o.;i5::9 -SCBP:JI 'K.:.S] IMir/" 5?,.3iiJ? li-t?!s;.;.!!!i. ;!.i:Ji!t VV ----- -
{!.?!':fl 'H !•:: . - 0002'
'•" L-j - r. GC :: '".-& - i. '70 1. JI-O!11" '-' C , -^x-;-:- I. . •'.'• . O.E; :: ::;.c ':.c ;" : :"-C:i.
" ""
-•-..j3300-"- -i
ill;3CCC---v!:
-•^' - - i ! pLJH.. .. i-itr-rir
ii •• "
i i ii hii i ij i< t=
. .I.LJ LL] LLJ [].-. ;-; . C3- *-O;.-JOC:i C.j. Oh- <-J ... ., LU-I I ! L..I "j. L,J I i i: ;z ;::: ;;;• ;;?: LJ t::v. -•• . C.;•or cc] t::> :i: •<=: : ' " '
s'; . •. " •-•;••'.-io
"Sarno La '-.A,i\ •: •• L 260 tC J \G. LCaba ?il<3 : d:\270C\ . r.a5\ ICZ-JOC :• . " r.:-j I' •*::£ : -1Sea%iencs " :. 'I a : D ; \ :i:7CO \ i'--;TA •: , l •;:::.; J :. . 7,4- % -.. - :: 1 e . -Tn:str'jr,2'"!% • v-i" r.^N 5-CO :<aci«. •• \ i 1 : - ••' •• Oc-r - :.'..•am:::;, e --•\\\o-j\-<\ : J. . OOOO " :. .: •. 7. :; •:••• •• v::-
P r i. n :: e C. o n T EJ s 1: :L r•. c L. a b c r- a t: a r y A n a 1 y s :i s R e 1:3 c::-':. •>
;..V = . J :
I '„;,.", ... '...,• ' ., ' . . , '. ' , • ' ' 1 ' -.,,.....,.\ '\i\\\' ":• : ' J - i . i, •.':•,. '-•' ":•:.. :- :: • ; -. • . •. 1, .-v;i! -
: :.::« i.;;r- ::.:- i:-;. :;.:::,:..:;: » --»t ij. . i'l . ' ': ' •.•"!.' * .•;. '.•'•.:..:. ....•:....
i •> t. . . '; ;•<";' .. i ; .') ' :: :, 3 :;.• ,v •-• '-t '. t'.\ "i .........•j.;-. *!..,-...!' ..:'.-,: •.:........' i;i!....
J, 1 ? 'i I * : - - 5 •:;;,; : ;. ? ;'i * " -. • : 1 " 'I •. " '1 • •.--•.----.
I; H.CK- Iii?' 'G '.OK 'if' i "'.isi-!* "'.i: '- iii /-.j';:. Jv ^li;:;],ii :i. :,'V'.. £ "j; ii.iit!: •s-csncs.o i. ::.:;u- :.;:i :r- i!,:': '.ri'u,.!: :-' i.::;: ; c'• i:..':o;; Eic-o i ' -.'iii: *.-;';: :";V;M;.:-; ';!•;•';:.::: -ii -x;:- :• ;.-, ! '} ' '. "\ *i"[ •. '" ".'•'' 7 r- j. \ '-. '•.'• ' f, .:- • > ' 1 •. ,' ."-••-••-
; i> .;:; Ei'Mj-v'!* j jr" : -:i- ;<:?i;r ^ : 'j- ::' ;v -ii r>\*. " "u !.;..::•! gfii \a\v^ i .:r VijSJ-s.--! K; .;,::: ;•- •:.•;:•:: ;sj
Li: L5.3?i 'EH^iili. ^i.jiij «.;^i ^^55I.:3 iV^ :'< :.i::> Ui!:i l:i.:.3!1 (}.:;=•:. ". 'f: i!!? '1::.:'- ;i;!.::i.'i: -!i --•-•M !:S..ii? VO3 ; L:. •:.:::: a.iiii; i-vi':1:!.:-.-!1; 'I. ::•:•::: =.":•:); ;:ii:
:! 5'!-;n qiUi -: !'!'!:' -;'-j r; i-«';ir .'il;-1;1!1 > ";!"f:!: ;;;i' [j;i:i """" "" w\* "n!: ^ ii: 1":/!-;1 -""-"'11 M-.;:i: E«owi?^t t.£?r t.sr 1:5 :.':* i;-:i:-!/- v; :.«:: c--35 U.:i3'' E:BT - is3/lii: -5.:;-!- :::l;' .i :J:i: v* .v i 0:'!
•!3 it. Ill 'uil'ii. "11'iilji "rlj isll;;?"' i'r::'/ - -— -:j ts.n? • 20.0115 ::.o ! ::.:OKt:.::' :,;':, •.•; --...-" i. i :, 1 " ii i . i / i . . t i t ' '.' : >i : . ' " •• . ; ; ; * •" . ; ; > ...........i „• L.!. J • . !i. ;,•*':* ,:. „•!;• . ..-,:• .... •-•; '.;-.;..,' • "
" s i L v ; i -i :r : . •"•::;, •;::' •'•',:;• • • ; . , '.,........,
..... ....... ...
...... .....
: ,;..:.:-i-, , . ..
. . , .. ..• .r -;;i;
:.::;••::;.';h::, .•: :,•::..:: • :. :• : ::
- :.^:ii:• .•[•':-.:
".::".-. .„:'-:••:
• .::'.'•". .'••••• '•••':
:...,.:.-
.: • r:
; i '. ' '. : ii
; • - , . .
, ......
•; -;v .»:•<•;; :; -n ::-,::• :: .M „..,..,.„ • :.-.,:.....!.; -j v, i .t ,.. i ; .*•.".-!...;*' ...••••
J; i:UiU [ilJC iJIi. 'i:1 MMI?? ilfiHilJii.CHJ 4..i!.'»i: til «.:»?!() !iBC i !.!•;;
35 n.m jii.iiis'i :!f,.si!i'! i:i' .t!!;.iji \..n VE. —- '..-i::;i:if ii3,.*!i3 i.ura !..n"3 MIDJ-I.:!: i;;i!M.-;i :!S' -—••- i..i:'?:-!;
i:!.i!Vi< ;33Ml:,3;i 70Ml!;i.;,i •: •--- _ i..i::Ja.iiiH ];!OM*.::» r»ii;'.;r? EII ----- ' i.:1 :.':'
11,11100658 K, 0002;
A Fl I C I] 6 '5':002"!
—— 1
>,'--"""•
". •\l.'.' '""i,' .
.'•\s.;;
'.J..
i"-'"i'D
ui..
... i— , ! !.....; ; i
?;:::-00----|ii.1 <
-..! !|-.; ! ).....ill
.3000-™--!!_ ; i •
t i1 — '. : :
"-' i 1
-M!•250C--~!i|
...J!:... !
-ii!"••"! ' i,
" OOC1— - • i ! :— -- i i i... .-..- i i ;t
1 I • t!"- ! i'"", ! ;
L:::00™--i- ;•-''! !•™i s i i;;; i r i ;
1000- ji .;•™: ! 1•—i • , :i •...... ^ .
::,-- .- I ! -IJl—— ^|i(
"S :;:
•:'<! '\:n\
I ' •• •- III II ' !'. ! (> jl [..I i h! • 1 . ' 1 'I"',•i i! - {!; •; j 1-- Ji !: Ii !:•( -, •;• . ; .- • t l • :
X :
::E: ;i: :;: ,::: ;:;; j.:: .;E::C: .:::Q; o n::,.[], ..i., ,..., Q_ .r. Q « •
•< i o :: < x <' • i 1 ; ! ' ! ! , , i i 1 : !
\"\ 'S'1;:: r;; L i O Pi I r C\"\ ';:: |[
ftRlOOSBOtA.-n 002 7
Pi-incctcn, MJ :)8.5-3-.3108.' I ' "
.... .... ..,'.! :>.-. .it-'
V/estonTAT " Report Date;: 01/06/925 Underwood Court. • Job Number: 9108360-OOIGMV/HDelran, New Jersev ()S()73 Date Received; 1.2/13/91Attention; Marian Mu.rphy
Volatile Olrj:i£inlc:s. By MethodE'F - ICO. ,000 Dry Wet.
I.D. : Sample DO I.
Vinyl. Chlori^ <2,740Chl.oi: i
Acroleiin. ' • - : . . - . - <1JJ,700<:L,JJ7C
Carbon 13 i.uul i::L cle <:L(3;pO' ' '
(Total.) '<]. ,37(3'[' i: i cli ].c i: c- J: 1 u c« irorn e: than ES <: ]. , 3 7 (3Chlorofcmi •... - - ' ' <1,37C3
t:hans < 1,370Carbon To t;rach:i.or:u3i- <].,37'0•M.nyl rt.c<3t;at:e . <]. ,37'C)1,1,2, 2-Tei:rach:Lorc>et:hatie <]. , 3703. ,;i-Di.c:hlo]:opropanEi - • . ..••-:; . = .- •.<]. ,370Iransi-l.Ji-Di.chloropropen^ <]. , 370'r:d.«:.hlc)roei:h«:ne •" : .: ". : . . <::!., 370[):ibrc)inochloroniet:hane <1. , 370
' . • - . • - ' : - ' • • < 1 ,370<:1,370
' " ' ". . . . . .2 -ChLoroE! thy ]L vinyl & ther <l ,,370Bromoforni . . "...:'. . ." •• •-.•:'- . • " :• <1,,370
To tTO LUNIKS . ].!=.[) 60(3 E; ;<;. "X,<1, 370
<1,3-70Total Xylones; EH ,6001., 3--Dloh].orobi;;nz(2'ne <1 , 370
"r 00028Mombor: An-^'i^irH^obrol (:l rll!M:iHr1 |iji;ydE)t)IWrios.'ro.
P.O. Sax 11083490 U.S.
. NJ C&S
::-7[:i FAX (609] 452-C ^
Western TAT Report Date: 01/06/925 Underwood Court Job Number: 9108360-001GMWHDelran, New Jersey 08075 Date Received: 12/13/91AttenMon: Marian Murphy
: F]liLircji:!Eil;il« Volatile Cr^Hnlcs, By M'E»1:lriO'cl B240 P'agtt 2UnliLscat'a/ktji DF =, 100,000 Dry
P«=tr.3r.TiE!i:.£!r5 Sample I..O. : S.simp.Zf! DO'1.
I , 4 - 13 i.oh:LorobEin;:en,E! <1 , 370
RECOVERY DATA
:U ( Suirr . ) 76Tolue-ne-d.8"- fSurir'.-) .- .: ".Bll-lK) . 9 Si
flRI00662 .. ?qu lj> u '•• "o:f IridHp'Und'ianriit L.afc>c)ri3ii;ori«s. Inc.,
P.O. Box "11(333490 U.S. Route 1
F'rir^on, Nf OS^H M 081609} 4S:2-S'i:i50
FAX [609] 4;;;>-0347
WestonTAT Report Date: 01/06/925 Underwood Court Job Number: 9108360-001GMWHDelran, New Jersey 03075 Date Received: 12/13/91Attention: Marian Murphy
:: Volatile Orcianics 1=1 v GCIVIS - Method W2AUnits: ug/™l DF=10,COO 3* -10,000
F,sir.:Lrn«.:'ej:-s? tor .! e: ,r.D.. S<5.,7ip.U! jM.fi 5«3-mp.[,e DC'6" JJLsrnk J '/-?£
(Total) <50 - <;:i(3Tr i.chl or o f luor ome t:han£i < 3 0 < ::i 0Chlorofcrrr, . <!:>0
Cl-ilo : ob 'E!ii;s; (j n«. <: f j 0 < S ()70:iO
. . . ., 3 - Di.ch].ci:obi=in.:Kene <1.GO •<: 1.00
ARI00663M«mbi=ir ArriHric^in Conrril of IrdEicxindori't I ;ihni'?rfririHi[ Inc.
C hi o i: OWES thane < 10 0 1 2 J <L C)ftromome t;han.'Ei' <].OC) ' <LOO <\ 0Vinyl Chloride; <].CC) <].00 • <10ChloroeCihane '•' . •'• <].00 <].00 <10M:(=!t:hvl.«no Chloride EU3J 3ZJ 2. (ijAci;ojLi=!:Ln " . ' - ' • " . • • : • • • <500 • <fiOC) • <SCiAc6»-t:on« , 30 330 4 , .4 JAcryLonitrllo . : <!iOO C500Carbon Dli3ull:idi=: C.3C
,<!: 0
Carbon. X^urachloi: I.de <!iO .<:>C) <3Vinyl Aci=!i:at:.:s <!: 0 <!i 0 <fiKi:oia.odi.chlo]:o[Fiei::han.e •••••-•'•...". • . . • • <'50 : • :•• . <!JO <.=>1 „ 1 „ 2 „ :;:-Te C:]:,£L<:hloroecha.Tie <!50 <:50 <:.:,- ' ' .
<!50 <!5C) <::•. .. . . .. <SO • ' '• 170 " <!:•
•plbro:Dioc:hloi:ome thane <!)0 <!iO <!:1,1 .a-TrlcihloiroHtrhanei . ,. <!iO ' <!>0 <a
21.0 <!5
Methyl- S!'vE'(rcitanoiru> <:>0 <5iO <!)700 E; <'i
;'-:"""<-7:-C{--, .. 1-wi,- - - Prin:ei:on,. ss j 0£I:)-13'-:MOH
V/estonTAT " Report Dale: 01/06/925 Underwood Court Job Number: 9108360-00:1 GMV/HDdran, New Jersey OSG7!> Date Received: 12/13/91Attention: Marian Muiphy
Analy is'lsr VoiaUlH Organic® IBy GCiVIS •» Method 624 PEKJEI 2'5,'tmple I.D.. ; S,a/7ipl(J 130') iS-strn^.h: D06 Blank .12/20/91
<100 <:U)0, . <100 . : <:U)0
RJSCOVERY DATA-' ".-.-• - - - , QC LXMIIS , : • • "•• . . •:Lt2-E):Lch]Loi:oe.chairus-dA (Sun:.) 7o-lU 1.18.** 11.4 , S7:Coluene-di3; :. i •( Suor. ,:>--:" .:- '-' '• ::-V ' •• 88-1.10 • = 105. " " ' ' 105 " • ' • 103^-ISro]iio:flu(3roben:2:(;ne (Suirr,) . 8(3-ll:> . . 98 . . N'R . 103
H, - K;E!1: i.ttiatEsd value; above; 1 InEiai: rangesN"t;>. Ho 'r«:ic;cvon:y <t\a.l:& du.e t:o matri.x l
» Chjluileli, Oi: 01:: L:LwJ.ti
F:dr inquiriiesi call u=; at ((309) 4.&M:KIE>0 and as;k for our Cuakii '• •«•- - -- nomMombeir; Ameirbsin O:niric;i!l ciil IricJopond'isint L«t3oratort«s. Inc. ' '•' •
LABORATORY CHRONICLEORGANIC ANALYSIS
Company: .__J;i_:: !_:;,;:b:ii:L_...IVL:L:..___.__. ._______..____.___. Job •-': £i..:;.j;L£<:;~c;~-.~.
D a 1:, e R *=: c e i. v e d & E e f. r i & e r a t. e d: .„„.„„../.:<L l;L.2i, ' :L:..—..—...,——.......-.„.....-„.—....
Em&cmiM JIUi 'IlUAIIQU AiimilSIS IHI'lBJlLIIQhl
Base-Heutra 1 Extraotables Ease; - bi eut ;ral Ext; ractab lea
.
.aid. lilxtractab les Ac id Ext ractables
...... .__./__„/._.. ......... ...._/.__./.__
Pest i.c ids s/ PCSs Pe;=jt; ic id® ES-/ PCBs
only PCBs only
R e r b i c 3. d <:: ;=3 If i K: i:-1:»i c i d e s
Pesst icicles (EPTOX) . Pesticidesi C EPTOX)........ „_./_../__ ......... ..__/__/.._..
01; h & r : .___.__„ V o 1 a t; ;L 1 e s - 60.1. / 6 0 21
o La tils £2! -- 624/8240
Othe
Dept, Mcina.^er 'Rev i^»w and. Approval;: ..........>,//:"//'' ,-• / /• ,£• /'«!C Supervisor Revievj' and Approva 1: ....j:'s:?:;;<Jic:-i::i,.../'.iM;'J!!L
IV If? I U ^' "^
\
H j n >;
1. 5. 0
i!|R10066>S
SI 40. /. 6 3. 0 9. 0 93 7 i:i !:>. 0. 1 ----- 2. O 1,74 O I PA
3153&. 76. 3 SO. 0 ----- 9'Li 7*j. 3 PAlS;Si£i. &. 4 5. O 9. 0 J.74 7, l PA,
17& Stiao. 74.8 93.0 101.0 17 •'» 93. 1 PA177 1,374. 4. V !:>, 0 9. O 1.76 4. ;=» PA
f1! "1U O
S'B? 3. 02K Ki '~\
J" 4-> 41°- 103 0, 474;:3? !->• 16 141:?6. 104 <;>,. 0744? 16, 10 4344. 10!!) O 4,<34-? !<->• 0^3 2i344. | 13 O 124" ' "' °- 06 1.7.. l;>7 0 <=>0« ' • 1 . 4 / 4 I, 4 , 1 1 9 !;» M4'3'* 0. »-9 33, 120 <V 3349 ' 3- *0 1017. 128 0 1 1•'° ' 17. S3 5032. 133 0. 6O-r' ». 92 3L&72. 134 2 «iO3';"' 0. 09 24. 135 0.' 13:3" ' O. 07 21. 1L4'L 0 P"!J5" -L- 58 447. M3 o" 1656'1 1. 99;'"?'? 4. 39
I:"1-;^n- K-:t?:i , . , , . ,
3'. £ [;i ;? l •/9. 30
1OO. OO7. S30.. 05-
41 ;/ '?- ;-:- 626. 99 0, 2:3
•'&1. 15-5 0. 05 r=>;-3®. 173 o. 05 r>
, t.f. i!S3- 17^1 7&. 30 2!3:(c»,5 1. ;;.=,' 449. 175 5 4t 1'V' s"? 0.93 263. 176 74.B3 2ll;io:'-3JL ? =J. ^'fe 1.062. 177 4 RV 1Trj(-3;"? 3-^2 966. 207 0'3:-, '^44'«? 2,70 763.6E5? 0, 07 21.67? . 0 44 125.63? B, 37 2304.'»!? 0. SO 2434."?0 1 24 3:50.":r]- 0, 64 1.E3-:?:.
:;/'=- 1 19 3.3.3.N-3 6 74 1.90,::.74 12. 64 336^3.7-> '-3. 03 121 n76 3. 73" I . 36/' ;:i 0 ':»-J;79 .t. ,:030 0. 19R I 'I 'H 1 K '-).'-\*•• L -L . v.l-1- • .."L. • )
52 0.61 172!C'. 78 ::;;i 9.5. 13 1462.:=•- 39 1304.
492.
RR
»-(JE: <SluhuIELc::ic»::
'LiJi .
co
. <:n»"(
C3i c::r-I- ILIJI LJJ'K3! «cji ;?: ...<::> ic»i •<][: c.:> ::j •; ••- ILL a. w ' •••u'3 i::;:: 1:0 LO ''..: .r'...;:: »• cj LO :.ui LI""
R! 00 Ei 68
..(.-r
I1.'
11r
Uj 1•Ll"' i'•L" >! ,'
/
f::! ,-.-, f•
£ ^. /•CM I:LJ /01, :::i /
§ .. !:ii ''\:a
IN a< t:;:'|-tt SI £' " !ii:: 5:| ,r.l<N ;;*; ir.IN I:LJ ::<:: co •»IN o: i:ji «--i coI:Q ...j: h: rt;>I.L. <]: c:i .-I <;i: .1:0 o u.i (.:• ,., . ]i-» !!!]• H-' -\' :::> Vo: -a: r- t:;j Vi::j >:.j LI:: CM \LUI u:> m_ 'i
LU c::i '\ \•ii: '£::! * " |::; ,['•• I';•; iLi!i c? r.i!ii -s' \i:u, :as: :;:: \i"o :"j "i \l$ S ?;! \
UJ "" \
<i: t::~i cnj -:c' -'::' i•0;.: «/ i.j. id., --r- !t;!i:N;: !- !;n| ..:; (|;i|| <;ri -j=5 ;;5 f,'!"' U'J C.31
O N UJ '! ... I<::> ...j i>T uj I
:E: — • i/j <:j o::
"""T" "T fu:iij'j
-
...
-
,:. u:j R*N (!, Uj
..
-
...
„
-
Ir
i
l'ff
ii1/iJ
r/if
f .i
/
1
j
\
\\
\\
\1
\"1 ——— T——— 1»--
U't1 T' -f
-
.
-
•
I.C.• Ij'J.CN'
-*"
..
-
...
.
Ill
2 *?; f-* o:>
r:r;
»
R i <
iii
i'ii
iiii(i
i'i
iiir1f
tI
,;'
f
1
ii
\\\\
\\
\
ir-ri
30669
:
!
1
-
..
.p<Npi|• i^; vF: $ !u.i tj tj...
.
...
,.
f
ii/i,'ti
/'/
1 :1,11
I1','lr
i,'f
1
f
t
!
\1!
\
''l,
\
\\.\\\\
I
'v'l'i.
ll1
1
: ' •-/ ':> r -
-
i1"!.., '.j.!1 *•
•:-.i '.;.
jr
]•/•in c-
.. !)"J »IN (.t
.i.
i-;i ,..,.., U': •
0 ! ',„
.,
ri i".
,::. :•;:••::•"•!; C =3 ': .3 . !:>i::3l=i ": 2 3 3 3 3 s e rn/'i. 93.-! -,:?• ;••:•:: co H- fr ;::3 0.3 ii CALTAB u 3 RJ:C: 211200._........ :: [N;,; A r,:, '.List: C C Ac c: i; No. : 8477
"\
E o ;-) ,'- b 'j T1 -J .-i n .: -,'.' C r i. \: z r i &;:i.-';: 
:;I/0::-''-;"" ^:^.CO + 6123 C^i' V i! : ? "''% "——-- -- s-3 NABS --,:•:.- ;.;:;:;:;: :- "TU;::,; W:-< ~ ' *2liSO°-
... .••• -> • f» .. ..•-.:> => L.I
5'
6 I "6S':
."
74
,HC.. A:::::> P,^Crv-::o COLL M;;." :-; T'-fCO .•-,;:•'.:
'•O => L.I
0. 00
:J'? J :/' RA J'1 :<in. i'':- •/ L:,V
•• •• ill •-!.• i - I i r i .[" i .:•;-, » ;
l':<'i :i -.i ^ 01 "'. t .;? :•:
1"1 4, 06 1=592. 93' 6. 23 S46fl. 9
O. 76 :.o,n c:
•i»;:)<:. ..,a...!E34'!...,-v.jiS.aa. • n.::?J., 64."''-- 33)38.^. 03 -.: -.15130;i."38 •;,;:: '::-;933,
'-''-' ' .. .1.. <-3 C3I • • J-l < .-' 'I 'I -]F J-. ,-i...
•y 0- V5 374.3. 134 '131.;!,S. '>9 ' -•• 1.1.74.,S. S9 :; ' 897,
B 0. 30 1 ]L7.9 1. 05 413.S 0. 1,9 748 °- 72 aaa.
-,.«,«, • "• -•• . •• •--• !:>0/- • 'L29 o RO -n-T••6b' - -.-7.71 .;.: :; 30124. 130 C 39 fin'
9-« "" 3696. 131 o!75 29^
4364.'*? 37.. 56 147:36.
r' '*-' ^'i»i». 91 J or; AI-;r;;4 l^^ l?a l!7a 70V.
S. 9':? | 17.:;B, 4,:: 3304
;::;.:, ;:;•• '::'"; iLJt'- v:) 1.00. oo :w--nnj:' v- ^ 362 4. 7^ 7 -H -.n:^4':v> 19. 17 7530, 97 oi ^r^45<> is-sa Aoaa. 98 o ;; ! 1 7'?:/ -• °-^- 174. .101, o, ;;•*' A - 9 3 -•' 764. -103 04? J-i'
-: ">. •- IS ?« = :- 'M2 IS: !S2 S: 4
in *-K:» ., .. ... ... • B-v- ' *f •0. 15. 60.
0,. 41 160.,1- '51. 593,0. 50 - 19
•••-' 0, 65: ' O. S4'
,
70 ' 3. 59 1410.
H -ran ?- 14i ° 5: 203.;; r : ..:b-:0- i« o,,92 3A,33 0. 99 370
o, s:0,, 920, 93
1.47 o. 43
79 :L- 76 692. i72 0 IA - " ;-
:!? S'?t 2IB- 173 0^4 174',4 fn !!!;;!°' "4 67.00 2707: ::-"i ' - ! I' 175 4.93 1734.
'L- B/ •''•'«- 176 &&. is, ;:»«i9*,TJ'^ 655' 177 ^ *7 1754'°- /::) 295. ;?05 1, (|T «-,»/
36 1-26 493. SOT . ': ;; ;"57 6-87 2696. 220 ' « ^
.I— ...I
j!. — • ,f • I If- LiJi[JJ ''"'
IN i.n "J
»• Li. IX ;.,-"li.-j a:,'L-'1' L.»*I L? "j:>- •:;> ...i«' '< u"? '. «:::!UJ '"* 'N'
•:t: -«i -:;c' •::• i:.j =«:;::. •::• 1/1 >..> t—
h-
-1:
o u I)- 3
CJ UJLO 'j'r
IN :«:=»: 1:0 ::t:
UJ Ml)t— •::•ui i::j .
h"' i;:i rr'LJJ """
,r,
0 0 0 4
.".i^'rou'L/^avr^S-lS-vf
Cofnp 0 u 11 ;|
c o i o c; H;L '13 R ci'iET H A * i :E -& *CO! 5 IirUlHCMIELTHANE:C020 VINY1;.. CHLORIC!- *CO:-!;:! CHLGFK3IE: THANEC03O MiEITHYL-KNIE- CHUJF? :t t: ::.[;251 ACROLIN:CO 3 [5 ACIE1TCINEE. .CSS. 3: ACRYLONJCTRILECO-K) CARftGN iKSULF:iD£ . -•00451 IL » J.-DlCKL.ti'FlCSIriTHKINiE: «•0050 li; l-DlCHLGFlOlEETHANi:; H«-c o 5 5 TH AN i-s - i , 2 -D i c HLOR CHKTI-IEE: MCOOO TFUCHLClFlDf-LUaROMErrHAC060 CHLGROFGRri '-w '_ -•C065 i . s:-- 1) I:CHLOFU:IETHANI=: ,C110 S-B'UTANCINE: " -r •. C 1 J, S 1 * 1 1 1 -TR I CHLOH GETH ANIEE:C 120 CARBON! '1 |:L 1 KACHL'Dfl I DIE: - :CJL25 VINYL" ACIE:.TATi=: '.:<-', ."-."
"•!U3Q BRQhO DKOHLORCIhiEiTHANEE; -"•i 1 40 1 > 2-0:t OHLOROPRGP'AME-: - - •'•,C14.5 TRANiEi-1, 3 I) ICMLDRQP 'RGF1 EE0150 TrtlCHLGFUDEETHENIE' - -01 55 DXBRGMaCHLiDROMEITHAMIE:C160 1, 1L» 2-TRICH!LGRaiE;THANE: •Ci,65 B.E=:NI2IE:NE: ' '"VV '" ;. ' ' ..:' " "C1.43 Cl^-l. 3-D;[CHl.,GRi:3PRGPE:NIE:C175 'isL-CRUaRClEITHY'L VINYL' E-THC J.IEJO I'lRtllMEJPOTM «•«•C220 M:llR:ACHLORQg;THiE::iNiEc:2io H-HIEIIOVNCJNI::C 2'0 5 4 -Mi=:T H Nf1!. 2 -l:i £NT A T^l C:iM!E:;c ;;.::.;; i , i ., 2, S-TIE-TRACHLEIIFI OETHAcs::-:) TOLUI=;ME=: .»«.: 3;j!: CHLGROlJEiMXiSiN!:; *•<•CS-)S0 E-THYL BE:MZ:=:h!=: *C245 EE.TYRI=:ME=:•:;.-: 50 M-XVLENIEIC:i::!:K:l l»-3-DI'::HLt]Ri:]'[J;::NZi=:N!::r| "' '•; j' '[ , *l ••;[) I, *l:l'iL.,CIl F? []'IllE.i^J !'!="hil:li" "• f. 'Si -\ "i „ |'\ 1 .•" i.ii r-p n r? 'j i" \ i •• i"> <\~*.. i'. .' .t ,L i si I./ J. *.if ! U.I.I r< LJ hi ". i J i. Illi »LL
r i" =-r\ n.:'ip X *•'!' l"i*<i"
10
C.0.0.0.I..0.0.0..1,0.,IL,O.1.1.0.0.0.0.o.,0,.o.;0,,'[],0,o."0.0.0.0.0.o.0,0,1,,0.0.0.0.0,0.o.0.
-'NO
764607rl.;?6
03 6-£57177550612614331,974221:*66!=iE376C-35541L4 3! 61795433216953!:) 247821:3 1862fa •'=> 51 4 6343!:> 8 21201 92;:i7012694744 1!=3445065064=776 1 5974
F'
O.0.0,0,1 ,0,o.0.1.6.1.1 .1.1.0,0,0,,0..0.O1.0.0.0.0.o.0.0.0.0.0.00-0100000o01
'
r*
IE;; 7!: 7 329 £00327 11 iEJ 5660631fc 1 2: 9iE3( 25;to4<:071:39C 57
44019256 1345•E32I3417S03:io3t 73USEJ0993906211672IEJ84931.74e?9lE)450E:,7i=354360559 :i720:»63
Ii:50
0.0,0,0.0.0.0.0.1 .o.1.I.1.,1,.0,,a..0.0.0.,0.0.o!0.0.0.0,0.0,,0,(3.0.0.0.1.0.0.0.00.0(3c:
cNO
94741=14620276921274133635B9375957318328071EH2964OM'591'521:32:58584315379E-I4365453021397798164379623124231.4221 7 495E3:4448645005204556!=M.990
10
O.0.0.o.0.0.0,0.,1.,o.IL.1.1.1.0.0.0.0.0,0,.0,,'o,,0,0,o.0.0.0.0.0.o.0.0.1,0.0.(30c-000
r":)NO•3 1 ;:»233!: 4 =522 173-n26";IS?6647177O1:>421702IEJ670!:)•9540535564 EJ61945873718444225523189051:34411334065961 IL 4254474ISO944•3-43IEJ674995S7522f;-J2974
F-
O.0,0.o.0 ,0,C3.0.I.0.1.1.0.1.I.0.0,0,0..0.0.0.0.0.0.0.0.0.0.0.0.0,.0..1..0.,n.
0.0.0.0.0.1 .
•,;v:;
.LSI;ifOi!• : ::: II.7 I 032413 !31=32;:)7:>6771;)7,20321.B6993'i:05E3OS-EJ575517264 ,6063591=36042':>S-fc'33209 ]L 2E::c:;3193* 1 !:•6;I:EJI 302514671, ;:iO91:! 94? 41=391540!; 5 55 1 56 9 isC- 2 -t
l'\ ••
O ,0.0.c.0.0.o.0.1.o.1.J1,],„0.0,0-.o.
. , o.o.0.0.0.0.o.0.0,o.0.,0..0.o.0.IL.0.0.0.0.0.o.0.1.
8944 6 '•52927O'£]: ::: 12. '.' 31 52666722<:»TO517134«! 1 374093i=30 5 156341:312:1L757-fi.•350E-105 •4- :L i-,5293O589O8051. 57383,£> 1 01 :3 12434451. 5 79 hi:4 4 i:.E?69!:- 1 754313 1 6673005
>.;••>
6.54.24.1 1.17.12.17.14.6,
1.1.1:0,,:i 2...is:7,9.17.
. 'irtrft'"•-- 4.
5.1=1.4.6.E>,2,.1=3.
2:3 .•h.3.
1 5.14.11.1.2.1.2.4.7.9.63
£
ti7'-[3 -I:L 1(L, C
61Br;1: :i>2;1 i9-i:. .
0!9;41/I52-21V7I$I6729417e:
:Lc:ti
Ci;
(I"/
.: "• :: ••: ''i.',n.i r t .[ •:!;? n t; i F' i,: r:7 i ;. i :: r =2; L L-J n E3 :i i;'i> ,U>
MAX F:
CO 10<: o i :5cor:;)CO 2 3CO. 30C 3 5 1CO 3 3C252CO 40CO 4 3CO 30CO 3 3£000C060C065C 1 1 0C 1 1 5C120C125C 1 30C 1 <l 0C 1 4 5C 1 5 0-c :i s sC160C" HL 'i ciC143C173C180C2£0: 2 1. oc:=?o:3c: .J:'>;;1C230I"- "r:i*=(
C;MOC£43C2::0C«:':3c 2 :> 4C 2 !: 5csso
:L^:/;a:/r J. T J . H - - 12; 0>PU' F:L':?* CCC (•* > ••-•- 2:i ;:L- F:"L:F? SPCC ( «"i > ~5 o. 300
Co rip i: u n cl
DROMQhi-THAN'::VINYL CHLGFn;i)IE: «•CHLOROE:THA,\£NIE-THYLENE:: CHLGRIDEE:ACROL1NACIEITGNEE:ACRVLCIW:ETFM:LI=;CAR l:i GM DniULFIDE:
I,. l-DICHLOFIOEITHEiNiS *1 . l-'DICHL.ORGEn'HANiEi «T R A N £:! - 1L t 2 - D I C H L, G ,F! C3 !:• TH £ N
TFn;CHLORGFLUOROHIE:THACHL..O'F?C!=:C]R!M «•1. 2:--DICHLGRGEE;THAN!E:2-.[3!LJ'TANGMi::
IL, IL. 1.-TRICHL.DROI:iTHAMEE:CARBC3N it:. IF^ACHLORIDH:VINYL ACIE:TATEB Ft C] M 0 D .!, C H L.. [] R C] M IEITH A M £ ^1, 2-DlCHLGFU]PRi:)l:tAME=:TRANS-lj 3 DrCHLORGF^JDF'ETRICHLGRGEE:THI:;NI=:D]:BRGHGCHL.(]Ri:JhU=;THAME1,. 1, B»-TFrtCHU:)ROE:THAiNI:i]-I!E:NZIE:NEE:a™CHLCiFlC]IE-THVL VINYL E-THI:IRGMGF-[]:RH HHI-'T £ T F51 ? t: ri'L C3 l-f OIE'T hi E: N1 ==2-Ht:'X ;N'C3NI=:•!• - M EE; T' hi y L ;=; -p EE: f si T' N I:JN i=:1, 1, 2, 2--TETRACHLGRG!::THATGUUEiN!:: *r 'r,'.\ i[".iC>r]'r}|:::"N7f-'K[C'1 iHhE!'THVL"iSi!=:N:2:E=:r^' *s TYI=M=:NIE;
i 1 "*- ?i T I.. Ir Ml"] '"1 •"" I'l [ (* MIL "j 1=' I'l i"( FN '? ' E" N! E"'
1, 4™j:HCHLC3:M:)i:HE:N:!'EE:NE::1 . 2-DTCHL :3RD1:IE::M;!.E:;ME
a^P XY !..£:: ME:
:•: c:
h:'«Rh
0,0,0.0..0,0.'o.o.1.0.1.1.1.1.0.0.0.c.0.0,0,,0,,0.0,0.0.0.0.0.o.0.0.0.1.0.C'000.0,01
0
i\r\( i )
4 a 4529270f:K:l 1273'152'6667 2' ,26C32-5!. 7134.2 1 ;374093803136348 12 i 73763508054 1 6529305B90BO 51573sa6 IL 01 3 1•2434 4 =j1 579614468693 1 7348316673005
RF
0.0.0.0,0,0.0.0.1.0.:L.:L .0.i..0.0,0.0.0,o.0.0.0.0.0.0.0.0.0.0.0.0.01.0.0.0.0.0.0.o0
CO)
7464 '!==:562:3S5-670,2691367066206324640539 1 4725900049504417293573335E331374533320901=3•331li:33402'>641 1 I224464i 5696 1430852'501I :• 0 E3'47:3630974
'>.
3.6.
20.24.1.
10.6.5.t;
13'.7
2'4.0.4,.;:j.10.13.34.0.4.3,10.0.4.--,:i''
:L:?.3,7
I 3 .74,00.3-1.3.7.763
D
•i ;:• : •:1 1 04 9 aG 0 :jT74ISOC30S?9068244333. 4 ,:>696902O£=I51 9 li-ft 3 &2 B :?'755!:•:]. 0334l=?d2 3 5691=769003193540li)564867 1 175117703600466=3CJ' 2 :?1 0 '1:? 7 o3 :s i:)447032
|!iR 100675
i.::i o.. 1/1 •«• •• a. i.i'i "•-<<M -:i:—« o ...J
• 0V-r-< u;ii 1:0
HJ.
343
7S910111213:L415;L &l?li=3]. '=?•SO;=M.2:2!:i:;s
2:3;=!6272 ?:i«:=?30;:-.' :;, S
20.J1 v"'
3ii3 7333'-?40414;;:'43
• ::>•3-647
C I 0 1,c :t i oCISCCE:115CSG5CSIOCO'10COILScos-ocoa-sC0:30<::;:> 31C03.SCS5S!COK)C045CO 50C055CO 00C060CO 65C IL 1 0C 1L 1 S»ClLSOCIS1 5cnoC14OC 1 4 S3C 1 SOC 1 3 SC 1 60CL63C 143C173•C 1 80C2.2QC 2 1 0C.2'0502:25C2:30C 2. 3 5CS40C:2 ^
«»C;-I!:J'S5
Br'LJNGC^ILORCM^THANiE: *nt rNT. S'l'D. * >*
1. r :2:--D:[ChiLQRai:THAN;=:-D4 - E... STD, ««T3L.U!E-:MEE:--D3 ^»S. EITD. **
CHLaFlOMEiTHANEE. **BRGNGMETF-IAN!::VINYL CHLORrOE «•CHLGnGIE-TMANi::METHYLE-MEE: CHLGR;:DEE:ACRGL1NACETONE:ACKYLONITiRILECARBON DESULFIEJE:
ILi 1-D;[CHLG':F?GE=:TH1E:NIEE »i, I-D:[CHLGRDEE:THAN!E; -»»T R A M SI - 1 ,. 2 - D I C: H LO P! 0 1» T H !=• IN 11
CH-LGRDF^CIRM *1.» 2:-D:ECHLGROEE:THANE:S-vB'UTAMONE:
l.r 1» I'-TRICHLUFiGEiTHANE;CAR MINI TEETRACMLOFUDEVENYL ,^CEE:TAT=;!. RONG 13 1 C HLORGMiEEiTHANtE:
TRANS--1, 3: DI IIULGROF^ilCPEME-T.:i! I CHLOROEn'HENE:C i !EtRGl1-1i:JC!-;.L..aRGMiE:TH^M'E=:1, .1 . ;iJ-Ti'-M;(;hLGRCi=:TH ME:::EI=::M:;E:NEc i s - 1 . 3 - :/ 1: •:: r i L.. t:i R o p n 1:3 p IE; :• t »:2 -C HLOftOiEITHYL V I NYL ETrlE-iFl:IJRQMGFGRll HJ-*TIE: T F? AC HL'jRC cE:THEE:MiE:S-vHEiXAMONiE;$ - i"! .:: T' HI V L. 2 ™ P ,::! f-,1 T /=. ,M G 1^ IE:1. 1...2, 2:-TETRACHL.GROi::'THANE: *^TOLUHE.NEE: ^CHLGl:M]r3:::M:::E:NI::. ^-«-ETHYL. BEE:N:Z:E:NI=: *STYRI=;N:;;:
M-XYLE-NEE.i , ::J-D;[(:HLGRGE?.EEN;!EE:NE if| D 1
'L n r '"HI HPi'l r> ::hr» c: k irr ''''1. , ;=!-0 rCHLOROBE-iN^E^NF-'
•}•.-!-.m i :; t;'? ;l b y PTL An a 1 'j =• t;: C? C
ArlQUf-lT-AfiiSA * R!i:i- Ar.r-.iT/< Ri»l" .i»HE:A * RE3? F='ACT>>:.s ii p . f«i c:.. f r om L i b r a r ij; l~n 1; r ij
"• OvJ04-\
:3.--" * r l L i=:: S V G l:- •=> C ,=. ].
I TT <: t' r ij ir. [> n t I <:! *= PI 't i f: J E- T* : F:' I NN•:«,: ibr,«tic:-n Dot* : 1 .=]-•:. :E;--91-
..ands-rd F: i 1 e-: SVC3 j. 2=1:.,-a 't # : 0 !. /' C' c.! ,' 9 2 "' :L rr, f E : 11. C' 3: O C)J-;A;: Fi::>:3 F-"G?=; CCC (. * :• ^ 2!5 :".N;N R:: F:IGR spec (?-^'! - o. o:;"
0015
::o;?ocasiC03:?csss
, CO 40, C04S', coso• CO'55:.. CO 00, CC'60; C065
C 1 1 O. C 1 1 5
|. C120'* 125|, 130!• C140j" CI 45'• C150'" :::L 55
'' ::i60- 'l f.. «:
• :i43: C1.7S: ClfcJO\ csso.: caio• caos0:2:25i" fj "] o0 = 35CI =• : 0C £ 'i :.-C 2. 1:: 0c «: :: 3c ;:;::• -aC i:'. '.•".?
•:':=: oo
VINYL CHi-OF? IDt=: •*(•CHLORGIEET'HAMsE:Ni=:THYL'E:.ME=: CHLOR1EHACRGLIMAC£7[:iM£i^CiFlYLGMITRlLECAFUM3M DllEiULFIDEE:
IL, l-DiCHLGRCiE=:THENE •«1. :L-DICHLi:]ROE::THANE: '* aTRANE>™1. ;2--G:ECHLDRGeTHE=:M
TR]:CKLCFU:irl..UGRGiriE:THACHLORGFGrW •«•
1, ,- cJ'-Dl 'i* HHJKUi:: 1 HA ME:.^-BUTAMGNE
1 , Ir 1L--TFJ:[CHLORi:]!E:.THf:iNE:CAR 13 DM TETRACHLG.F! IDEVI:N:YL ACETATE;DRGriG 0:1 CHLGROME::THANIE;Hi 21-DICHLGRGPFU:iF3lAN!=;TR ANS- 1 , :3 U I C HLORGI=>R GF3 ETFnCHLGRGETHENEDIlIlRaNGCHLGF'.CJhETHAME::1, 1, a-TR;[CHLORO!=;TH:AMEBE-NZE-NS.C 1 13-1 r 3-D I CHLGRGP FIQPENE-:a-CHLGF? GETHYL V 1 MYL E: THI:BFlOM[:iF='t:iRM •»•«•T:E;.TF?:ACHLGRGI::THEE:ME2--HEE:XAMaNI=:fl -METHYL a-PcMTAWONE:1* 1, 2, a-THTr?ACHLQRG!=;,T"HATGLUiiiN!:! «•cHLORGBiEiiM:: EE:NI=: *•*ETHYL :[J:EE.N2.E::Ni:: -^
v STYRIE:;N::::!'!->; YLEI'NE:
1, S-DICHLGROIi'-MIIEil-.iE-i. , fl--oicHLQFGni=:M;:ENi::
;L ' ei! — i.' I uHL'-ji-i .- LJ CL.IM.I ij.J'JbG P X'i'LEi ;•:!
0,0.0.l"p
0.0.0.0.1 ,o,1 .1.IL.1.0.0.0.0.0.00.0.0:.0.o.0.0.0.0,0,00.0.1.G.0.00.0.o\
£="7-446452927088 12731 Si a66*37:2.2:692!S- 1 71342 1 ::i740938051!:>6G41131S 1 '757-fo35GE=I05fl. 1 652930589013 0'51S73 1;3 £36 IL O131a: 4 3!fl4515796 14-:-6(:!;-,?Sr 1 7!:J4iESS 1 667.3C 0 ':
1.0.0.0,0.0.0.0.1.0,1.1.0.1.0.o.0.0.0.0.0.00.0.0.1I
• 0.0.0.0.0.0.011
0./I,
0G.0.0G
o <; <j r
J .' M'
EEiOO2341 6 167 i,926777sai/'1 fl 59615436710474 1 i3482204763707i=35:3:£3Ofl 5 2:302005785090304"''591:)099a 1 946 '=3 '•"'2 fl 7o;:::yfl fl 3£:' :•: fl-•I S: <:•47243152S960
j. i;.
SE;
'•;'
14,':>C1
11,. i a .0.0.
20.1 1.28.8.
27,,27,
11 7 .3.2.':;! .14.0.12.
ti. .42,2 I,
1.124.9 .t;
7.
f,o .6.
13.16.2. : ,
.':
' i 1
1 i-> ::po;=:i706•"» *' c;/ "t w
S S 92. :r c:' '*''3; 1 3927y530866laa7 a?176:I3 '13 S(., L <:, i»''''457EIS462187797S4S94406391=31=317 1 :3SC52:fl67' !:. t*1 '*'''035££!:«''99)1 -"'3':'•;..'?•-70.;; •• ;. -3
'..'*. '"? "!,
0004G
i.u !:s:'
j/5
CO
U-;,
'
£jg-0-gyg •-•-•-••--•----• --••--•- --
• 0 \) 0 4
(|V'
0 .;!!:;•: EEiVCJ ].;:;«. T!01 /:: 21/92 1 1: 09: 00
, ,..*.' GLASS i=»ACKED CGLOMM/t'lETHGD 6:2-t•: ,j riTru 1 a . SML '[ n •=. tr urn tf n <; : f=" I. NN !•;:? :. ;; :• : '£''..!) ffi i :: t; e? ci t) j : l:> T L. A n £i 1y ;; *;: C C: .•:,::•:: ': N -:\ •
r'< ij .=;!]• , f 3 c . f T" :; m L i t) r -3 r ij lEIri t; Tk L|
t\l 13 IN;) rn «>1 C 1C 0 1 BRGMGCHLCF? GMETHANE «•« !C NT. STD -w «a C 1 10 1* 4-D];:F:L.UGRD3EN;:ENE «••?>• INT. 'ESTD. «-^:3 CISO CHLGRG[3EM:!;EHIE:-D5 M»;[ MT. STD, *nefl CSl'S) 1, 2-DICHLGRG!E:TIH;AMEE:-D4 *«Ei. STO. *•*5 CSOS5 TGLUI=;NEE:-D8 -(ntS. EElTD. «•*
7 CO 10 CHLGI:U:ihETHAiN,»: **8 COIL 5 BRGHGhETHAWEE: ' . j:9 CO SO VINYL CHLGfrEOE *
1C) 0025 CHLGROETHAME 311 0030 METHYLEIMEE: CHLCJRIDSE.12 C251 ACRCILriNI1.3 C031S AOETGNE^4 caisa. ACRYLGM:ETRI:LIE;1 5 C 0 4 G' C A R 3 0 M D1S U L IF: I D Ei16 C04 5 1, 1 •»:[>:[ CHLGRGETHEiNE w-1"1' CO 50 1, 1.-IHCHLGRGETHANE *w
CO55 TRAINIB-I, a,-D]ECHLGRGIE:TH1E;iNE. 1.9 0000 TRlCHLOiFU:iF='LUQRGMIE;THAME=:
ao 006O CKlLCIRCJFOlRri «• a 1 0 065 1» 2-D rOHLGRGETHANE
aa: Cl 10 2-1-IUTANGME23 C i 1 ':J 1, 1 r 1 -TR !E CHLORG^TH AM.E=:2:4 C ISO C ARDGINI TETRACHLO^ IDEE;SS CiaS- VINYL ACETATE26 C130 BROMQ D1CHLGROHETHANE27 ClflG 1, a-EXECHLGRGPFS.GP'ANE »28 C145 TRAINlEEi-l,. 3 D IC HLORGRRGRENE29 C JL 50 TR 10 HLGRGETIHEEiNE30 C 1 55 D I'H F?,GHaCHLCiFU:tt'lETHANI=:3 1 C 1 60 1, 1, 2-TR •[ CHLGHOETHANE32 C 16:> '[jEMZEiNE::• s c 14 :;j c :t s •-1 - 31 - G i c H L G n c; F R :: p E:: N E::-\ C175 2--CHLG;rH:iK;THYL W :: N,V L EiTHEH
;:;•::; ca:::o TE:TRA\:HLar;CE:T!-:EE.r-,iEE:3':' CaiO' S-HE/AM^Ni-;;:• -;f i c; a 0' :;• •*> - M E T n Y !.. ;=» -• i=J '=: M T A M a .M JE: ..'I:? C225 1 • 1, 2, «:-Ti:;Ti:<ACHLC!ri:GIE:THAI''JiFE •«•>
4:: CS-TO E-THYL ]J!=:N::=:N::: -''] C243 STYr-IENEI-i C25O M™X'r'LE-N:i:
-?::• C 2:5:3 • - I .. :3-iy[ChLC=ia3EE1M;:E:.r-iE:-?• -; . c ;=:':? 4 i, 4 -1:1 E c M i.. o :=; a [3 EE r i;: E:: r-: EE:
"" - -"- ««" ' .L.T-W )•; EM- Kri F Me
i , f 9 :::';;" £: 26 r -• °':'0 *;=- J- •• 4 :.V 1 ;:; .:«, 2 •_ --„-,.-, A'•' J' 1? "''" :=--: : =-:> 3 1 . 000 A
"';' i;;;7 J- '• — 'I 1 1 , :•::& A;:j cj •" ''•. •-. '-T — — —L''"''T <="": '=:-": 0 0. "'-S3 A
!;' 95 1C95 27: £4 3 i. i67 A;; i;;';' ?7 1 : 11 1 0, 139 At:l v4 ''r:?' •!• ' :->^? 1 0, 234 AL: 6;- 30]- a "32 : 0. ;30o M,
-•':> <=•* 142 3: 33 :. Q 4;:*, AI1 49 217 5:26 i o. 644 A^ 56 251 6: 17 1 0. 715 Ajj ''3 250 fo: :15 i o 74p A14 53 275 6:53 1, , ;, B16 A;;> 7* 277 ±: 56 1 ,>. B22 A•16 96 ::24 i3 ; 07 I o. 96 1 A|7 « -70 9; ;is i 3>> O=?E3 A•l'=* M fl02 10:04 J 3 19"! A19 KU E=?4 7:22! 1 0. 87.?' A-° 33 4:LE:I 10:;28 1 ] ;?40 A"::L 6a 452 1 i: 1'9 1 1,,, :34i: AE-:CS: 4:-! 477' 1 !•: iSi 2 0. 6:37 A•::;;: 97 4*3 12-28 2 o. 665 A':-4 :L:l/ SIS IS" 49 3- 0. 684 A:~'5 43 S37 :L3 26 2 0, 717 A;:;!:; 8:t 536 13 25 a 0. 716 Aa-f '--' ft 9! Ifl 4R •:' n -rcio,. Jl T 1 *-' <=- U. / WY (^'"'=' ''"' 6(>S 15 04 S o R04 A29 '" ^24 15 37 2 0. E:i33 A:-f° J-29 &44 16 07 2 0, E5&0 A!:;!, 97 *52 16 1,9 2 0.870 A ]*:i<:! /a •->•'» E3 I- 6 13 2 0 B65 A ];:f!;[ 75" ^2 is 04 2 o,. so 4 A ]";4 &:J 700 17 ::31 ;:. Q 9;3S, A }:=i:=l :l73 751 10: 41:3 2 1 003 A ]^ 166 345 21: 09 3 0, 901 A 1•3:; " B62 21: 35 3 0. 919 A i33 43 796 19: 53 3 0. 849 A I:;;! S3 840 2:1:02 3 0.896 A I:;';3 9:t 901 23:33 3 0.961 A (7l JL:L£I! VJ"3 23: 36 3 i. 005 A E:::;. ^ L0i'^ ":2* 3 i.oea A E"fj 1C-'- H47 ;28: fl3 3 [. ;:.p3 A t'?4 l0^ H55 28:55 3 1. 231 A I••>!:> 14 fo :i2s?4 32- :"'"! -J i- ':;on .. T'"' " • r- »-' -l JL . *.ii.iU (-^ L-<-». i-^A 1:3:24 ::j:j: o==i 3 3 otp M >^•7 14' -3fl2 33: 35 3 ] ,]""( M )- ... , , j- • • •- .t 1 1 r"'- lX'° 3--:;7 29: .^3 3 1. 2-fcS- A 1C
>Ul AT-?l3(Hght ) ^.r-nc-ynt: y - ,•C'Q 22':>:335. so. 000 hjr: V' »«;DB 599206 5^.000 NO ' -SB [? !:. 1 1 1 A 1 =: -i '• '- - M .-,- l ! j ° J • .-"J . t-'^iu N^ \ j:; «,Sa 141310. :=:: 5-1 1 N0 {' BIJ 561"M 1 .=. -. — -» M..v : ' "*• •• i - - -'• " --- M'.-; 1 {-39J:i3 372368. !:::>. ;;S ;p N.;-: -L |:j(,Ml P:-:1;.'5.?? c ^ ".- -- nr- - -=-"-«€../. , . . i=_ j. -r r,|(j. , .-,
:M. ] Oc:, •[ v •[ !=•••» .=-.-)-> . ,,.'L 'L- - J -- "?" '*k ; 98XA 12^Sfc4. 5.7 901 I',.': -• "t^1 1-' -» -1 r- r. .. ' ' *" l=- • '• '~r:':' '-3:j--E3'- so. ?oi N3 j Ra::! J^«7- ^-54 NG iie?•;' :>,=;/,=;!. .<;;;,. ::-oa NC; , 49
[JI- 3i073. ..:;:;:. 73S N-3 I •= RDB 151170, 47. 740 NG l' 77:"" '13-01.9. 50. i:iB NG I ' FJ'JB!J 175096. ,j,o. 7;iS NG ..,' .:,;.iiEJ :3<1.273&. ,5,5. OEi5 MO p 41BD 2579! 6. 51.925 NO {' 90BO S: 161566. 109. 5E'9 MG 4 o«iBI! 347998. 59. 696 NO ?' piP° 151009. 55.395 MG ,?' o^1:1 U 27610. 63. QOO MS p -riBB 24567B. 74. -01. IMG '?' 77vii soa.sa.:>. /6. i.so NO p R-tB" 13M53. 75. 1125 NG P 79JJ' 1 285142. 55. 116 NG p'o*"i:i 231113. 56. 151 NG p' OSCi!J 470243. 5&.905 NG p' ioQD 237220. 54. 594 NG ?' op
270578. 53.S71 NG f 9AJD 130713. 53. S67 NIG 1: 9R;!fl foOSOSS. «,;:)., 014 MG ]' QA1B 470242. 56. 905 NG ?' io10 53B92. 53. 719 NG S" <?*>11:1 iE:::L(:,!:i4. I;,;;.. oa:3 N,{J ] yp11:1 305593. 51. 808 NG l" 9P111 &02'&9. I;,;::. 573 N,3 , 94111 11.1875. ;j3. ;:;51 NG ,, j .:,:" 2:3'=n.'93. :;:;,. 3 ,3 N:-: .:;' ,'.:111 636909. 52. 285 NG l" 9^J!t 51097:3. 51. ;-;;, ;,,G ^ ^~jJ1 225937. 51. 113 NG 1. S9J!:! «:=!6i:30. !?2. CSV Kfl l .:>-]JB 247937, so. iCO NG 1 ' 87!" 240953. -4.336 NG aioi;;; «.'-:oo48. 54. c=: NG 2.00jX ;::696 8. .::=> :::;:3 r,iQ ,_ 69••Ei 'I'j'OcSa. ;=• ; c-ri :ji:: ,, ' o-->
RRI0068
3 AWater Volat:i 1 K. Kea.trix Spike/Matrix Spike Duplicate Recovery
Lab Name: 3:!:c:j5:r3CLeL!=i.S=LKL..[i!<iL-i'tJJ: :L..-!=L=5.fe Contract: .....JJL3[!!sELt....!!!A'3™.............».........
Lab Code: ......Fn:......_...... Case No,,;: 910j:L=ULQ.... '3 A S3' No,.:: .„„.„.„„„„....„ SDG No.::
Matrix Spi.>:e - EPA Sample No,. : ...............Ji.;!jL(3L::.iL....[.KiiJ;L.i.iOO.).......................................
S49i=;2 S 4 96:3,
1 COMPOUND
1 , 1-DichloroetheneTriehloroetb.eaeBen:>;eneTolueneChlorobe:fi ;:ehe
SPIKEADDED(ug/L)
50SO50=i 0 150
S. AMPLECONCENTRATION
(ug/L.)
NDND
.. ___£_____I 3 „ 3
ND
MSCONCENTRATION
(ug/L)
3 0 „ 1(51f Ui;>4 . 648 .7
MS3
REC #
<=;n*:i. 2 2 *u1 0 297
ocLIMITS
REC
•61™ L4!i7 1 - L 2 1 »76- 12''76- 1.2.17 S - }. 3 1 )
COWPOUWD
1 1 1-DichloroetheneTrichloroetheneBenzene .TolueneChLorobiaihzistne
•i5PTK:Er""ADDED(ug/L)
5050505-(>50
MsDGOW'ClSWTRA'nrOM
(ug/LJ
30-., (36 ]. , 4
_£_______5 4 ,. 34 B , B
MSD
:R,E,C f
61123*UIbi98
..............................
%RPD #
21U11
QC L:RPD
1.414:].].133i3
:MITSREC
(51-:. 4 571-:. so7 6-:. 2 7"76-:.2:>7 5™:. 30
# Column to be used to i: lag recovery <:i:ncl RPD v&]Lues with an asteri.s)
-*1 Values outside of: QC limits
KPD: ..........[L............. «u't: oi: ...............A............ outside limitsSpike Recovery:, ...........JL.......... ou€ o i' ...........JL............. outside 1 imits
COMMENTS:: .....J=!...:::L.. icJJ:i;ij;L.J::(:L.j;i|j:r3:!;L=Lj:j3Lj;:i:L.....jiLj:L.Jii&EEl£L£L£i!i&:£:<i........»........j]Lc!:L::j]L<i>ns>!:[j=!J[]jELi:Li£..j:i<3L]t:]
VOA-1
1/87 Rev
lembitr: Anneirican Council of llntlwpcnclcrii LaJiximoriev, Inic..
•>;-:•.!;. . C;..A:::5 F C:•,:::;• COLU:--H M'^vTHL j ,£>.:;-!•/:[. C J. O/1 £::/=? 3.V :»r-;T-.u Ui : S5is1!... " nn i; r LMV='r.: : FINN3:.i!3,ni t Led :i :j : PTL An £J 3. y =, t; • CC ,-»•:•: t;.
Ai-?OUMT-=ARI=;A -» f::£:!F:' Ai^i^JT/ Cri'^r ARiEiA •> KEiSP FACT tf:: o :s n . f =i •::. -f! v a 11: 1. i. ':> r- ,;i'- g E: 11!; r 'j
• t M;3. ' , ' . • • - ' ; L
. .:., ,. : -i
.;3:H-j IS:'Y/"V *' .;3. .»,: /'v . .;-S.'/.... . , 7•••/ii'1' '. - ->/••:>>•:•.• 'L 1=)
-- ?)&?-• i ?jV-/v:' * JO'-•' •'i ny'i. \3',' ,•# i -i-' ./ ,::,'3 I :L"'
f '::':;.r '':,.'; !•&/J0jf|i ' 17
!'*.&'&''- "i • 1 9/"•>v: ->i so',;V' j'| ,9 1
il;[/'!i•:;.; ::;;!-.,;. . • •, «:/
;• "*
..:'.''^ 'Nj^
• . : •• '3
134
•IJ C)
13 T
, . ::;!Io4;-'4;:.
-•"*.. "; <•»-':•''.• /•• :! ;(,],
: •' " ' ;; 47
N =ltl»:'
c; i: o iC I, 1 0C I SOCBi::>C30!:>d B :l 0CO 10CO i:5CO 20co;=2SiCO 30C2S1v ' ? J '"'casaC040CO4!:iCO!:iO
COCOC060C06IJC 1 1 0C 1 1 5<:i2:c3cia-sc:j.:ioCJ.40:: j. 4 >•;; i :?oC135C 1 60C! 1 -::i ':ici4::iC 17;:
C220(I 2 1 0ca-asc:=z:3oC=!40C.=!4!=>C«!! 0
C;>!;»4C: »l\ !;: !:>
1 •: Fi: CI t- 1 ill C !n L. C3 R C) M E=: T' h1 A h J E -s- -=- 1 N T . £ T D . * <•i , 4-D i FLUOH on E:N :i=;Ni:: *«• :E N r ., STD.
CHLOrMliJENlENEi-nri ^-^IMT. STE3. -B-I, 2-D]:c:HLORQ:;'THANi;:-D4 HHfES. STD. <HTOL.ui:ENi=:-]:K=t «•«••£; . STD. «•«•C ML C] H} CJHETH A N'E; ^- ~iEJ i"! C3 T1 II) M I:! T f 'I i N' ,••VINYL CHLElirllDI:: »•CHLORGETHANIE:METHYLEiNE: CHLORIDE:'ACRCILIMt\\ ' E" Ft I t^lc"ACRYLDMI:TRI:LE:CARHDN! DISULPine
ii :L™I):[C:HLOR(:K::TKE:NI=- *li l-DLCHLORCIEiTHAN!:: **
T,FM;CHLClFU:iF:L,lJ!:3RG|-!ETnAM=;:CHl..ai=lC31"i:Hi!M •»It a--:C)lCHLClFU]l::THANE:
1, 1, l-TRICHLGRaEThlAME::CAR3QN TEi-rJlACHLORIC'E-:VINYL iSiCFEiTAT!::CIROWO DICHLaROMEtT-r-'^NIE:1, S-DECh-'l.ORaPROF^MNE; «•TRAMS- 1> 13 OICHLO^GPROPEN!::
DM^JOMHCHLDRQM^THAN!::U ,U £- T!:> j:CHLOFi[j!E;THAN!:;I3EE:M;:.E:NiE:CIEJ-IL. ::j-i:n<:HL..cRGpRat:it::M£=:2- CHUSRQETHYL V 1NYL E-:THEE.r?
TETRACHLORCc THEME,=2-HIE: XAMGr.!E-:
4"'NE;!|H l,;!:;'::!>£:i'|Tf'r:ICl[;15.TOLUE:NE=: *ETHYL GENZiEIWE:: *JEITYFUE'ME-
t'l-X Yt.EiNE:
l.l4-0?iHLcSaSEN?ENEE III B I 0 (1 - ; -D.ECHL.CRO!Jf::;'i;!E::ME;: 0 0 0 5
"•o m .' :.;i ' .4 9::: :L IL 4;n 1 1 7•!• 6 ::•
; ;:> VB6 <?;:»
: 7 NOTi:3 NOT
. . ! 9 NOT;. • ( '10 NOT
•;r:: "•'[ ;L«! MOT"-V-:!t;."i 13 43;:';,V--.. f 1.4 NOTi57 : J L'3 NOT;/,."• ;•':.'- -. 3.6 NOT'•.U1;,:-/'/ ' 3.7 NOTS&f.. ! jiB NOT.'13':-.: :-, 19 NOT•j"K?v so N.ar£''•'%' 1 . «I:L IMDTt. ' r. ££ NOT1 >'.:"i-::' «t::i NOTF;".r II1 24 NOT;'.,,.-' '• S:> 43S ! .;: 26 NOT•.':?••;-- V! 27 NOT^•'••' ^ 23 NOT-V . ;;• 2-9 9'5•.v-\'r 30 NOT.,;'-';.:-?• 31 INIOT•]•;•" '[ ::ts WOT. :-:« <• 33 NOT:''v!:>;-r 34 NOTv, ::i'S NOT
•-. -.:J 06 NOT' " j? NOT
:33 4:33.;=' NOT4-;N 9].4 L MOT
. - • - •=•«! 10S-13 MOT44 NOT4=j NOT46 NOT47 NOT
: ' 43 NOT
Svi^n T i m :i K-:i; l:'.h! T *•':«; ':ri Ar •? ;) •'. M-:i r. 'C '»::r:tv •=:: :=v-:> L :L. ooo A 133 L ;::;:•.•: "7"7 ••••':• I"-.' 4:? B! 1 . 00') A 13:3 l=!n 7. ::..:]::.,.9;:r*f ;::3: :^o ::i i. ooo . A 1313 £5 10.4*.447 1 1 : 1 1 1 1. '32 ; A El 8::J9C6.874 ;=!2. ;•:"! 3 o. 7;; 3 A 1:1; 2 7 '391::-.!1096 ;=!7; 2 6 0 1, 167 A 01- 0;J9;:i9.
RMJNC3FDU [••:•[>FGUMI)FOUMC'
«!17 ir. .[]6 1. 0. 64 A 13 £3 4179,FOUND
;25I. 6: 17 1. 0. 7 4 Si A Efl 1454.FOUNDFC3UNDFOUND
F' DUMB-FOUNDFOUNDFOUNDFOUNDFOUNDFOUND .
£506 1.3: S3 2 0. 71fr A BEI 79.RIiUiNiDFOUNDFOUND
630 JL5: 46 3. 0. IEJ41 A IlEi 1L073.FOUNDFOUNDFOUNDFOUNDFOUNDFOUNDRMJ'WDFCiUr.i:E3
SEHO 20: 1.6 3 0. 1EJ63 A BB 90':'.FOUMD
901 2.2: 33 3 0. 960 A E3 [J 1490,FQUMD1.01.6 «:::•: 26 3 1. 0':32 A 13 13 4!.9
FOUNDF:OUNDF[].'UNI)FOUNI3FOur-:[)FGUP'.IO
* - '• <., : :• 7. T o 1;;:-;;. co:.' r.:r 16. •:/•:0. c: o :: N:? 16. 37::>o cco r-,:1:- i .E>. 37•;::s. S.-M r-i^ 14. ;-:6':>i . 4:=;::: M-3' 1. :>. B1?M i:.,r: 2 NG 16 91
=1. SSa NO V 0. E34
,/4. 3 7 9 NC! ' 1. 43
-
0.p2';r!N-3 0. 02:<'
.-'"*O X;8 NG 0, 1,8'''
*-•"(!x;=:-;'4 NG 0. «!6'' ,'''""
'/.'<!: !::;:; MG 0 08t,sf'''
Q'''j,94 NO 0. 06
11
::-.' ••. i"iL-::- --ri'..^: :i;:o
.":..• ••::•: S<:A:I -v 'V T'S r:-:'r:-i;:: :_:::•.•..••-;•• •., LI"T~:i"i;;•
• [:•
: L
1 T
.:.
i•..[I*ftI
!' ";A I ,
r.s.'<3•E;T•.-
i ' ;•-!:•:A"L£TCI..f::F; 3. c
T OCA•£]•;: AN
H3EN'fV.fHT.M
7F?!•;:
i: c fs •:: :• :sE:!i:/::i
THi-JESHOLD
'5I1?2S
i-I101
1600630
TIC l i
TOA i B LLIN A :-i:=: L
Li !]::•SSI^•/CM;LS
i TARGET COMPOUND AMALYE:i]ES:ti'i.J TAR:G:E-TS IS TOTAL.:{; (GUAM LIST:- PEAKS PE=:AW,£=.
10 :3 13
. . ,. FILTER PRClCE-'SSING:.••.;'•!:•/
T[]TAL <: 1E3.T :>.LA!3T C MIN C S-CAN > MAX M TOTAL TOTALPEIftXS SCAN SCAN .F? 1C HT TOL PEi,AW3 F:E:JE™CT3; TICSi
& 0 " 0 0 i3 0 6 0
NO UNKNOWN PEAKS TO 13 EE! I DE-NT IF I ED,-
.. -.oil oilin o'ia: »-->h- ...I
o"i1 IIin^-<::>
\CIj•i.r--,1:1! L'*"1
p' ...N
UJ '-ill. CH'.'"I '\i*j'i1/1 'N
'L..'l
l^-*r
'*""
to
i--:
§i I)(„>
:j:: iii):i-i i--!.U C>LJJ :r:
0..tiii''ii' ij*t
uj I".i>• in
I.LJ «....J IJ"!I
&= '»3
.•-•.i—'iii.....;*;;'..iCIl
" i.!".!r ;i •— iIj.l
";-, .-.,lij'«.''i ,i ~"
Ji- •;:
LJ.i
LJJ
HRlti3D687
L
IXI
IN IN
...j ,..jIII] CLJ
L0
.Is- 1"J . !j"co in;- ui '.:i •"." ::L: u'l I.LJT-J I— •;!]; iIJJ i.•'-" UJ ,..J
i.Ll
..p.....n.....—r—-—[...... ~T-.
*1™.I10688 S* QUO 5 5
A •* R'-i" ,-;,v'MT,f: 'Ei c: , 1: :"0i;i L i. b r ;n-ij. !:•;'".' U
1 C I 0 3. U R C^GCHLORCTETHAI'^:; ** ! NT. STD *•*I-! C i 1. 0 1 > -'t-D ]. i"LLGn aSEl-J £:=; ME •*-* I NT.. S TI), * -3 ct:;v) C!-nj:)KO!3i::N !:iMc:-D-3 -UNT, STD •»*4 CSl'S 1, 2-D]:CHLOR'[:iETHANE--ri4 **S. STD •» *;=• CSO:? TOLUENE -DS1 ^ S. STD. «•>6 CS10 4-l:!ROMai::LUC.rU:»BE:N;:E.VL:: >^-S. STD. #•»7 CO 10 C:HL..CJRGis1ETH.AME •« -:(EEI CO 1.5 DFUDHGilETHANEE:9 CO 120 VINYL CHLORIDE »
10 CO:2:Si CHL.Qi=!GErH,AME1 I C030 METHYLENIE: CHLORIDEIS CS51 ACROLIN13 CO:3!:i ACETONE14 c;:!::>«» ACRYLONITRILE£5- C040 CARBON DISULF"! DE16 C 04!3 1.. 1 -D ICHLGROETHENE »17 COSO Li1-DICHLGROETHANE **I B C 0513 TR AMS- 1 ,, S-D E C HL.ORGE THEMEi 9 C 000 TR I CHLGROF"L.UORGrH:ETHAME2.0. C060 CH"L.GRQFGRM ^>
•P2S: G L 10 2-!:iUTANGNE23 CllliJ 1., 1. l-TRICHLDRCETHAME24 C 120 CARBON TETRACHLOR IDE-:SS- CI 35 VINYL ACETATE26 C 130 ;EJm:ii"tO D]:CHLOROt'll::THANES 7 C 1 4 0 ]., 2\ - D IC H L 0 R 0 F3' F^! CI P A N is-: *2.B C I 4S TR ANS™ 1. r 13 D I CHLCROP RCPEpJi:;2=? C1SO TR ICHLGFJOETHENE;-:C C 1 S3 C ::i:r:C:iGCHLO!:UJ«'!ETHAi .'E:?: i c i -:iO i.. L ,' :;i-TF!::.^HLCRCCTHAME
': :\ C [ 7 i) :I -;: HLGr; OiEiTi-i:'; L, V IhJYL. E-:TJ-»t:l.!:!': ;:• C I ::JO EJ:; CMOF.:; 1 -4-->
:• v ;:«! i •:; 2--r-\:::<ANONE:3':- c«M:::> i - i - :=!, 2-TEr,:?--.CHLC^OETHANE -i- >40 CS30 TCUUENE •»
4:; :::j;:4o ETHVL BEN;:ENE •*44 ;:«::;:o M--XYLENE*S: CS53 1 - III-DICHLCRaiill-NZ-Er-iE:
1 o ~ ::, "I.IS; 1 1,1 3 4 3 Xi. .S4I. !. = ::» 29 41
II*moo 6
so 4-NOT FCLMD
1 0. ::4I A BB 4747. .1 . 15; :? r, 'V
.1 0, 763 A B3 7797. .1 ::;. 4:>;3 N3, iT NOT ,--,,„ ......
l':» NOT FCjUNO.. 16 MOT FGUMD'-'17 NOT FOUND13 MOT FGUMD19 NOT FGUMO2:0 NOT FGUMD2.[ NOT FGUMD£«! NOT FGUMD£3 97 498 12:28 2 0. 66:> A M 449,, O. 09V MQ O. 0:324 NOT FGUMDSS NOT FGUMD;;i6 NOT FGUMD£7 NOT FGUMD23 NOT FGUMD29 9 Si 631 L5-:4E=i 2 G. 842 A .BB 2137. 0, 50=? Nft 0. L <<>30 NOT FOUND31 NGT FOUND3;i! 70 6':»2 ].fe:l:? 2 0.870 A D [J 3S!:>='. 0 Z^3 MO 0.0933 NOT FGUMD34 NOT' F:'OUND31? NOT F:'GU!kJD13 •:> I -fi 6 3 4 (\ 2 1: 0 El 13 0. B 9 9 A [3 [3 S 2 & ].. 0 . 3 7 g M Q 0. 1,2.37 NOT F:'OUND::;:3 NOT F'GUN:;::r-? NOT F:'GUhJD40 -' 1 901 «!2: 33 0' 0. 9::0 A • B I; 'iJ2:j':v 0 -^O MO 0. I :3
1, 0•::•:: A E;j 2S3::. C 5:. '; MGi, :•];::•: A ;];]; 4077. ::• 4.-? •- MO o. i!=ii ::::•: A s;? S9:s. " ;::;•. r-i-t o. 1,9L. :::=:: A E;3. 230!;.. 0, 4 = =• M' f ' 0. 1.31,, 41=;: A VV :M:=' 0 C™.:. Mf: 0. 021 , 4:3::- A 13'3 1 :>.:•::.. 0 ^CO' N- f 0. 091 , :2!: :•! A I];!]; 4;JO'7. i: -i:: •=• MO 0. 1 4
i.j •:»?
:>:: tin ; J::: u.i-ir: : :<::" ..j L.I -r-•:::• on >:c: r--.0.. -:f
If"' t"i "-t— i CI' L-'i •-
•a: i-< -o:i— ...J :::?•:K 01 ••:»• ui?1111 il.) OJ. - ( .1.0 -1-
*
S;t .::/;• u..:•".' ".-• <<'i iij•:::> u. o «.:« ,,-—-
co
LJJ...I
tillLJ^:<IL:CIl
UJmi'113...J
:•: in: c.i™' h— -J>..:' u.i iJii, :•:: i/i
<i '* J.
tilt 1— «..> lit. O
u.i ii LJ.I. -:ic:
CJll
r-i
r-
j-
I"1*!
.,
' E
CO -<J-
CM
:>::i/> EJ:i r>iOJ: in N.
Itt '"" " UJIN ...J L.O"M o: a:•II) '1.3 UII
UJ...Ju!dijc=;ci-L..a;l/i
r-. a: ajo-'j. in. <:::• '--• ...................:«: III 1— If..
'113 I.LJ ...1
U'l O -II) '.-
LJ o .....I '.J ill! -:j: i."Ji»-•• i::: i— >:nLJ.. i>- :in <i: .... p u.i '.iii c: '>J
mi; ,— 'i.j tit: •::<
S z!
-
::rf
i'.i\'.t.
ir
•¥...
F.>'
- UJ
•IL
...
-
.
....
Ll'l
i- l.j.,
-. -'I''.l"l
i !-"Ji— ULJ
-• !1!,. Cj
J- r.vr.ri,.T..r,.1.
•z r' f.
i/'<
K- i
LJ!' CJI1 •ib'i Li"<
U'l
.X L'IJ
V'J !:j::LLJ LiJ
...
..
.....
^ f]
ilt:1'"•J ......„..„.„...
' UJ C>. ... J •'.• LJL. •'—
till O J
CIj ^_4
'.n •:!'
-
RIO|69S
ii
C"'
•
•
... K
•
- S
-
•
'!!»
••
•
-
L ~
'v 13 f
•
-
-
•-
-
. ...
r-rp -r-rp-T-r-q'.::> <.~.y•II' OIliLi*' ''.'it
1, •'-*01) D B >
" .1 ::• _
•• • •", ::••": ; ;L.. 'JF- 4000: -•' -JIVL ;; :•• ;•> s :•• .< - « r r • , " i N
; •: : 10 i . -- -u F'.j.j'irio::-::;-;':;:::';-;: --••:- ;;:-;r. ^..:. C r=:0 '"H!.-.;; 0'?:'.M":.t::N?:l-D:; >-.>^tST. :: "!" '.'. . *-*••* C:;::.;;. i : -'--D I C HI ..IIRO .'"1- AN.:~ -C-l **=. STD.:: '.SO-? TGL.'.lEN -::?a ^^G. STi: -'-*•- •:.;•> i 0 '^-LiP ' .M.OPLOOF? Ol"i!::N'£::::Nt:: •••---:!. -=;T I .
•> c ;;•".::• viLs'-sYi, OHLOt::i.:::-:i,;,-•• •-.: '.::;:«: CHL.CRCKT'-A:^ •:
,:. . co 3;: :•:;=: T ;»YU;:!V=: Cr-:...-.:;;' L '-:' •": Ii!:? I. AC;:::C'L..""«
o4 C1L?!> S-GHLGROi-ITHYL V:MV:-S CISC BRGNOFGRM. ^^«36 CSSO Ti-iTI-lAGH37 csio S-HE:::<AMC:!ME=:
' 0 ij 0 6
I i M,* r. >.r '•' r K . ;'i =; " '; Ar ;;- :. i H :; '" :: '; -••: .; . •• :: '\"~ - •;":-':- 2. :. .000 A :?;.:i :Li3C:=:3. ::,'.':•:.: ING .! . i:3:=:
.!. J. 4 7 :J :. 1 B'. 1 .' V -" ::' ;:;;
••»::> . "M:; :. :L
X"V./ rr .-. .i; • - -• •- .-. '. _^-i
^- i.ooo ;-. G^. 26S980 ::::.:.:;:; KG i.e;23 i. coo A B3 :r?7B:i;7. i:::. c::o N-:? i.£2
j. ..:'....'.: r-: .: ,;•
'." v .2 7- ••- j V
00063
:z::'•:::C.Ji UIO'i
;» • - -,--4 <#«"» '| , &U;:i. . ' JE; i:» >-Si' - '-ar ' - •.
I'"' .i[ >;•: -=J!!)[' c:i S '1 ., '• 'i^1 . • -& . -?•-' '' "'/; [ . " . ' :,..'
i:V.':r.."'->J .«t't
%'•
."•)en(!:•i" i\.<:;»11.)•\.1.0mio:i:Ik-iui'il,Iin...i*::•<..!
CI)IJLI
r"3K3'ii«-*!
..<KI,-t-i .i:?:.™!
CJ>•<i":;3iii..<>...iUJ(jii<c...1
..-a: Is-1:1. -T
-i Oon .,. .,N UJ i. -.<".:> ...i u't LUI<:"* U. lilt I..31
„.„,;:;:::»;»:::::—-—-———••••—i«! '——..—... ......... .,„,..._..„..„
'C3S CS?O ».'C33' 1/3
irs., • <:;» <::>... <:;> .'.»:o <::»c*»
-ru-j
l 100&96
*sW
LU "•I.'1! C.)
to
f q
LJ's.
in '.5'-p ...jC3
CI3'*' !;Li
"SJ -Xa.p.,.>-.:-i c:> i u-ii:i « . r;;i i/|I.I „., ,;-,-, _]jj 01- c.;iLJ •"'L. O'l MI '•ji '^s LU «c:» ..ji i.oI ft (''••! [X iII3i.-t -. :-i ::i• :i: CM <j; c:j:•:: '- 1.0 nj
(..iii
r 'iLJJ
•!fjT3"'
IX
III.'Ii"*i.ji—
UJ
IUJ
HRlOO69
fLL
;
r--.ur-
k! j: .1: S! ;;':\ <fj-i •&-V ' LO x.,-' CSD' "-; .CM '-•< u.i
CM -J. l'"l••> '-•> oc: <:c,*. (Iii C.J Oil
1 3p ";f : 1 :'?'•* •»<:
j<
1 • si:;•* ' U'l I-- 01:> • '"! Li4 !j"!
i ]» T:J ix IK c?'i -«B i;:> .0 <:n~; TE> "' i "i \i\r; fa. cj (T.( rk>
' , ' L=i: '--1 L|"''
-j O liii -it: v:1u.. >>- iiii <:E: ;-... . u.i cs »ii» »::i
iiii j": cj iiti •»-•..
•fiT' i r"'","T-;
! r'-
tCtr
-53
:.. ;;;: :
; 5...- |N!
I.LJ- <:o„ IL"'
.
"
.
;_
.
- K:. '=•{"- !-?!• '.-'I
3— -11
> ;i3|
U— LJJ
ir
L.
r---T---r— -r
• ' i -'
i
;..:
:l
.. lit: '•'-.!•;;•
-.."' r'i
.. 1/3 U:>
.... ,_fj
• ri'I mi" ;\, LU• u.i :"S:ij*i "ii— i^ci LJ]..
...
:.
»:-;r cc>
i. £i. §'•_ uii
I.. -' ";•• U.. '--'
• t"» —1- Ili. f"\
- ijii •:; i
.,.. i,/! - 1
..
i-j. prrrn. .,.,,. n
>:': ' O" .
- ['•:!
..... r..
:. ie
.— • ilo
••
•' 10— u:i
.:" ra
'...
• Ln... ,-r
|-
•••
;:C L;7
" •;?i-
p.T_,n,..i ., — ,•'•' '::• •?
•- -'-i'
•
••
"
.-
••
.r, .1...— *.
. , | r-vr-ri
''i' r.
-
A ,R 1C 06 98
u'j
"'S UL.L.I — J-.:..:..:..,
[
•-r i
£=;
,-* i it—ii
ir') *r
D: !il!
•!; ir;j •--! I.LJ(M ...1 i/iS3 ii
.J-i
£.;!a:<ii:LA
ui
"r illi..J
\?l UJ Cfl(3:: LlJ Jf.«::> <t: ..ji01 13.. :>- >::*r-i :•:: u: i:i« "• ——————
:»: CI> h— C'l
•;:> " :•: 1/1o;i ::[• cp r;;. ™'.-''' ?-•' '•-? 'v
UJ 0 «....i c.; j:ii ^ic: .--iLI., in- ;jii <:c. ;;.
*:c: o: o "ic -."J•L'13' 1— '..1 LI; — •
::;! -;
r '-r
L.l-L.J..L.L.i.J..t.L.
J" "*
,'.!" u..
;.,r
•
... rj;
ILl.1
"•
..
-
....
:. ^.,
u.•. • 3
i.Il
' uli
i-ii
"_• ''„•
"•t
L.,i,i.J-;. -I.J...I.L.
i jr>r- —.......,.
.1 ... r1 '--1 ^
iiir ••"•in;
• cri iiii•'4- in
V"!.. i i cut
, :. J
[ IJ;' <l
'M t3":i LJJ
,.,
"-r,.
-- (N
" i/i
"" IJJ c?'. ;-> n .LJ., — •
- -•: ':-..'' •-• '-
>-- i, •>(
...
.
j p-..,...r.j.. r..-rr
HE: -IE:
u., i— ::i.UJ -II.-::c: 'i,.3 I:L.
: <M N-I u.i u<••• 0>i ..Ji 1,/f '•- i.niL ci! ui u*ii
Ijj...IIJL.HI)
I.C)rj-
UI'
l-i 9
'10'.'• JI.'-J
O'l
a;:n•CN.ibi.o
,I.ji—«
<i:
10
...j'-J
*- ,1,-. .-,-. (.f1
fj*iO"lC '*!=W.
r-fjCT'iT'j"
'.''l
a]..jI.L.
<::
'LOir--<lit' 1 LJ•o: :;;:Cl. I.LJ... ...
';-' ••?
CI)!L" '!!>:n> ("i'™' *' -iCL. '..'•ii> ••'"'"ie fi™ ::;!UJ 'II-'.i1 n»,
O'lCO:tl:
*'!'/;;i0"lU'l
r^-C!K'
11/',«
..,;" 11'-31 "',j'-J l"'.c-/- ..i--- tJt:: :"i;
I --t'• J
5J:'"iJ'•inrj.
c-i till\ LJJ
IVfli I'D07.01 , Q0069
T
*;»
L: .
'- 'Li
m >
•=! '
••:'in "
\ ,i "' .::.•>! M-I I.LJ
(N ...1 1. 1 ..——..........-—————-. <ic: -i:...» ...' LL)
i/i.:! ' UIU ;::!
LL.;'! '-) Ji ii -01
«•• i. . — —',*•
.: .
Si :;:: ui in.l ill) fM ••<•j i/i :;:: Q| L0' lit! IICI :»:1 S! !x ...i c::> ::::' aw. ii:5 : :: >TI" ri;-' !! I-"-! '/'
'''. o:t ::: « :> r-.'if n> • r •:: -i./t ci" i--4a. ^ j LI it'j Ci .,; '..| "
"-'-' '" : il !-•• o iLL. Y— ::> -:: ^LJ.I . 13 ill •; i-;i: c.:i ; i. o iI-: i3-; i: :IE xmi i~--: ;j lit! -'
r
\i ......... .... —-—• • — •
-L
E-tL
'i'1
!vj
, t.
•
:...
..; -
:I.^-
: ::f".
..
••
F '^rP i.« it" ....k ;::
!" UJr- ,„,
U UJf
i
'•
'':; *':
:
i:r\i -
CJ1
LJ.. "-..
Ill
'T' r1
:.... ;;-- .X L"-'I ui :1i!- : j: :;::• HLJ LJ
::'.' '.'_
- in.
\ I~~:'
• u.i «i::i...i ...
' (III — r- u;= 1?"'
: i-- <-"i
Lp....................
r -. -r-
.-:;.
.-
-
••
-:!-. :
;
;•
- ;*-- iT
\
1
.'
-
- u:!
,"-- Li ",'
-. ?
--
,...';]; ';"•
•
....
•;;
::
-"
•
•
r::;•:-'.
Q \ao7-02
"
.
CI'•:•••} LL:".'
i.':.1
1
:ti:1.0in rs;r
;»• *cr /"J.... lll! ,:>.OM c" IjJ(M -J l/i—i oi -.IE:rll' C.li Oil
1 [/i
;' • LiJi• —1
Li.113.
t -LI;',;- oi!:>:
' I--:. i.O
i .
:; LA "-' - •"",1 t-t. I.LJ —l:'; Ui ci: ::;: =ft;-•[ in <:c I.LJ •— — — :— - ci. ...j <::»
' cj 'V ':.r(«:• .. i:: ",/i -[ o:i ill 'i:> r*. ~
LU o ... ..."..j 'i. iiii <~: »<
• '.31 '';i U"! '"" !r;j .—,.....::
illJ l:-: dJi lit: -t
i" ....
\
•I ns •".
."•J
- 3;0
.... S
hj
• 1:,-"---
-- 1-;|' 5«!r i '"i.L '.:"..
I...Jilj; I! .........
i.'u
i"i"
r..,-,..... ..........
L' " L M
r
- ;g;. '•'>
!:•' - -
1O'l Li'O
;\' uj.LfJ O;
•Lii uj
-.
•-
•
:. 2c">i
' 0-1" C-i
II'1'
LU i;:li -— ' ."
'.K••X '-
"'r
r-... ...,.,..,.....
• jj
-
" ""j
-
"•$•
...
" -T!.... ij'j
'•
-•
"
'— 1—— v—i
•
•
— IO
rr ,....-,.., ....'..I '•• ~-
'
••":
-.
•{r— :
.:
.:::•'-,
.,,.T...r...-
i." '.'.
II1-110° 3
r-..r ••-.
:;;: N.•ID I.LI 0:1i.o ;:: —t1-4 .LJ --1
IPs., III! ..J =»:
••" i\t <*'• <••'lw 'Ci> ci. osion " ci> 1/1«:»cmo'i:::: r::> i---M- iii' u'.i •::.ij'i 'II' O'.la. <.:> I/.-in "J" •»-»;. I.LJ o -I-
S ...J '..' O -3LL. i— :ii'i
i I.LJ '->i 'Oi '.:i CL.i ii— LI; :E:I! 01 s3I 'ID; i:ij i— f..)
O*r'jH "
lit:<::>I.LJi.o-'31
I in: rL- .- L...c ay M!
. U'l
—' ;*3.O'l LI'J'
L.j.:.j..i.L.J.-:-j-i-JL.i.L,J..i.L.j..:.i-i.J
01)072
v] ->: 1 iI;Lj:w'L. Or «:OGX •' -rr':._ !~ r =i : r L ,vi •=• r. ;c:. !::i!N?'ii ' •: ••' c! '.' .! ' '••• ":',B'"£•*'•'• •'••!' £ 1 '•* :: '' '. CO
!i 1 0 1' 4 —D I ::":..;jC r- Gi::£Ni";:!N!:L* ->--:IN7, o'TD. ---•-•
9 C020 VINYL. ' G HLGH LSiEI "10 C0«!& CHLGR•:]:•='7HAN;:-
jL-S1 csg'i ACRI:S!..]:N3.:3 w02!5' ACI::TGNi:I
7 co:?o 1... JL-;:':-cHL.!:3ROE7;-iAr--Ei: -j-'-, i:; C 0 S !3 T R /i M E=! -»1 - S •» D 3! C - •' L., 0 r; Q E T »• E! N;:!. -v coco i:=? :• CHLOROI" L..L::: an-rrHAMJi:;-o coco CHL.C3KO?:•(:;?:in *
iiEiiiiEiiiiii!;!Eiii(|E;(jijiji;i(jiiiE!iiiii!!i;r,.Eia..M.; >:i»:..---. <i<..«.i< >.. i iH <>il - ^ ^
i.:: C,', 30 E3 FGi'iO D ICHiLDRlCMEiTHAWIE-
':?::! C i 43 C IS--'.. 3-D] CHLOifJnp.^DPEiME::34 C ITS! 2-CH.L.O'F? QE::THYL V ]• !NIVL. EiTHEE3:i- C180 2;tRGis10l::CF?n '-*r<fS i. C S S! G T £ 7 R A C K;.. 0 R 0 £ 7 H i=: N IE-37 C210 ;:t-Hl=:XANOME::•J: .=3' t: 2QS< 4 -ME T H V L. £ - P EN 7 A N G N !=•:':'.: -: c. . •: :L, i,. 2, :;•-Tcrr^ACHLGriGi-:THANE:
000'
3 '.f B: :•:.-? J :. - ooo A si:-;74:r :ti:!: 45 :-2 1. 000 A BB 3;:'9:=i£4.93B 23:29 :3 :L.OOO A Bl-1 353-2':>,,444 ;l 1 : 07 i 1.31ft A 13:3 lG2!:>p!3
0. 952 A. 33 39 724, ~>£ i.::-L; !V3i. 1&& f\ 13 E3 . 2 7 •:;•:• 3 L. &9 I.:'- MO
"Crr POUND,
r.|QT FOUND /-
-:-,' i ,-. .-J ,. .» ' / U. oc;
JG V 2, :33
i>*)ikiiiii. i«M b£U ««ia u:h3-t --:---.e.<*;.ii |iiiiiiiii(i!«ii.ig «i!i4'id-
:;0 MGT FGUNi:;2) MOT i~GUN.il•;:" :-:07 i"!:JL':J'[:
24 NG r KJUMD
:i'b WOT POUND"7 MOT POUNDOii NOT POUND
:••;: NOT rDUMOs, ,I:-:: IBS, B4<:» ; 2 j. : 1 -. 3 0, 902 " ,-i E3 E3:-.; •:••;;"•"•' POUND
t'> «?y P? ,D ":_ ';| "' ' "' ''"' _;"; . / p43 NO7 i=;i::oi:-.iE:!
; 3531.540,.
--::: \;::rr POUND•I-/ MOT POUND^•• ==::J :<:?: 40 3 •.. 2. 3 A ii!? '2'2773 3 0. OOi, C::::
•• Jli'f
I.LJ'
"">01)
cri ---Ioil -v
t-U,-J
u.iS:LJll
L.Oi UJ «•••"•-':;:: »M•L'I:: LJJ :«:
'--' '«:! " '!'.'':.."' in;
.LU O ill) '!!'::: o LI. t:-i
\ zr £ .-.f >::•i*.i
LJJ IE:"
I.L)
:«: O I.LJ I.T1.
'::• ill)
' ' .0 G u:':....! vii^ • ••..J t..' till '.". >r-1
LJJ ^ii' tiij 'iii•'t: '..i1 LJ., <'-jr-- L'J';: :;i: :i-: y,,
iiiinii
-' '"i 131'•-it::;::C3Ii LJ.I
U')
UJI.'"I
...(III
•:::' ix. LJJen :•! III.;;s- '•::!' ...i
>— r.i: :::: :i: x•x <:: o. '-IL- OMiiij I1-- 'i.;1 ij.. '--'
i */i
.t.L.Il
-" LJJcri LI'i
\\ IK 11 u 'l-'l! J '- 0 0 0 7 3M, II
:\
ti'i,-, (*-J<::» *::>—i O't
Cr C.J'
inLU1-t I--4r I.L.mi
-I
I.LJ
i
»IJ
!l
•i'i's.*
r-k
ii.i
]fit':LJ:IiC" 1
•IJf1 ci;'.-> oc:iCSD' »..••- ' Ii.
CN "
ai 'S:ioi p
ui i::i...J iLJi.L. I—- - '-^i-: I;L:
•M-
L.l;;;;Kl:;::LlJcm...iini—LU:'-23=%!n.
!J|?:::;c:>:;i:
;2;<!!>,— i:[[:
v1cnU'l
Hr
•(IC''"::::•'ji'iiij:ii*
>Jl-
•o: c-jiiii I— (..» iii; '-*
..I.,...!.....!.!..
-"' fjll
L l L.J> .. LJJ'*"" f 'i
uj1 "ic:".o u:<3: .in;lIO LU
00079
1 i1 jj'l<• i
\ f,.,: ,.,V
•
i
*' ' !H ' i-:• 1
lit:
! ' ..-4
•ti! (:r'o (N
'•• --i cri . <>: ' =et; -;f" r\r: L/li.;, JK: MI •"-•' ;"; -'< LJJ
- o: 'i;c.-•- JJ t J .Mi
'•; UJ
L;:I|
f' <-i'' LJ""I
vt
.'• ,r
I '•? !;i: i:<-"1'. i"< uj •'-< ' ::,1 IJ"> lit: ...J :«B' '10 'i-1. ' -"
""• !=ts :;<I 'N;«: ii^i (IL. .;n<— i -• '> -ri'<'•! (II) l/l<::t :.i: «.::i LO^ '?»• ::i« ir> -:o; LI i '..' '.'-_( "•
J. i^=: — T '•'-'
t UJ ''«i ,;j- ; i
1 LJ., h- :::i --IE: :'-,' ""LJ.I Llj L", '11'
<:c: S. >!-' ;ic: ('•'»iiij h— i^jt L'J:: —i
k-
-r-rC'l.".
L ' ' ' 1 L J J" 1
•: 'J< ..::
Iv
*" O'l
•-" p „;- rij ,
ii*:- '-»,'
,.-!'
:li5:
...
"
:: -:.....•-- co-'." -'-I •;
: = ---
' '>Ji" :;S-[. '.nii •> »r -'ii,•• -• t. ..t ' ,.\' -l:1 ' '"'1" i'i"i .-:
L i i::J:.. 5f;_
,— i'":'c--:i
! 1 1 L ' ' 1 ' 1 J
fr
':-,
•:o
;....
i"ji
•p-HI
1.0'•"'
"' r" J i::a;\. ujLJ.I :ii
- L!'! 22d:i D
-
;•;.....
!. o*'• ;;;!"" :'}•' :: 'C i •-••O'.i" 'CMn— 'i"\"•*\r .., .:•... ']!.. Lt-l ':-:'i !![]' --i' O --i• LL. .:n
iiij cj
' i-'" -: jir '''''"":
1 L ' ' 1 1 L ' '
-
r;--. • '
... g0
"" -I
iii'i»!
-,
— i,:rj
•
- ("i
7" '•;!"
!"'
- c::.--- 'HJ
"...
• .:a— i.Lj•
— iJ ')
"... ('r'....
[
t—'"'.!"'•*
•*«•
1 1
:
-•.
-;
...
:
; •
•
..::
:".,
i
. [ . ,
ARI 007 I 2
LJ..—.
COJiJIB
1.0in CM:;;;; .J
". LA'CM >••>'CM ...1•"' <IIL£=? '--•iyii •
:; LJ' ...1
U.'"t (II)i ( t'•:, -ai
:. ]--'.
• *',"'i
1 §v i I***• i«i•* *^f" (!E?\n oi
"•« llL.• "-* :«i"i;HI i")
C.31*;-.J -
j. c?-i i'i'.'"i ill1
LIJ. :I,..ji c.:'I---II.I.. h™
Li.l-ic: f..:tL... (]J,''
a: -x
i
r j':"!' '!J;:'...
L.Ji... ra: L
LI
.... 1C"l
1
,:k;T"I.LJI.l"l•OIi:ci
i] j1LJ -*'y 'SSB;i.i]...J' C l">-• C'l''•«•• l'1'l"i" --r'i".: './ic::> '.:« ' -:::,- :ir ji i_;,
•--•
ciii •::: -<:;:: »™ TIin* *'« '••.<iii tiii 'iij(J.. O'-J,... ...r .^••ii» vs. c-j. — "<..) iitL •— •
oi-.—iV 'I'
•__»..-.;!_•;
..
1
-
- i_i>CI!'
...... •«-«,
:MJ;S.
"" Ll.lU'l• 'III
.. -:l
-
-
--
"
...
...irl.--«
..... *"*ills
" irsii™*i ......" 'ir'ii
-r1.»'ii
" '? .„.:::-i- .u.'i:!!•• •:«!
u :-i1" s!
'['3 3:: .:::..., '"' • ""•::-
, [jJ
K*0')-
i"...1'.....Ilit:" '•*•
L..,
''"I1
r-'i'-"' t-ii0"i IO.... •--<
L-l ,
AS iiijN. UJ
' 1 LJ ?'-'"> -i-•01 :iii;
. i;'»Ji..
...
> ...
1
..
. 1-0inM. '*"*''
•SIR1r — -1 'L'l'"r'ri
CMCM,..ii'"i"~".r'""1
" rjS ..::- ~.'.i ".- t.L. — «
• III) --tl"t' '"'1 •
" -Ji \.llij 'II?;;;; r>i•'"3" *
... 1— .--JI1 '-0""1
n a o
T;!J i ~. ! GO-.-'L Oi ."..COX / ::•;*!•.. I :'i =; f;';"- LJ r-;-: r,-: ; :- IN• - • •• • • . •' .i.
Cjv-r-LrSr -- -; - ^ ^
oo :: 1. --•;;:.;4 C !.?.=>30 C1.SO:•:& C220
k ' • 00032
1. 811 - S11. 81
49 327 S: 2::> 1 1. 000 A 33 1 1 353.114 7-i:; 13: 4fi 2 1. OOO A 33 361'='66. 50. OCG N117 92- 2.3:30 3 1. 000 A 33 23 = 593.
11: 11 1 1. 326 A 33 1C" 2 3. ;:OV- r-.:-.? 2. 07;:::,!: :•:! 2 ., 0. 449 A 33 3Z3%1 5 .. '2 .•--• :.rNO \ .. 91
-- '•4
NOT KCUNO•'.'-'•• 2:=i" 5 1 IS 1 1. 663 A
NOT FO'JNi:NOT FOUND
NOT
:-.:-• i'-ii.j ,' ,- -JL':\ L,':.';.- NOT FO-jrJr: •:.:; IN J]' V '" G' J '• •; C
:-.
-'
;
'."•'
.\
/';-.
NOT FDUND
NOT FOUNDNOT P'CrUr.'!::-7;.% (:;''V v
;•;:•: ;::;:;;;:;•:,
: -'-- ".: -
.-...., -.- ...."\" ::'L:;r:YrlOT rC'V'Vi'1O6 : o : vMOT r'OUl'VNOT "0'JN3 .
!">:• -IJS
! 6 : i 5
% '; ' -~'o
,.,.
.23: = 1
'" --
• . • =; '-< "" ""; / ,' '• ;ip *? ', '"•'"; ". '-l' *•::•. i .3 ;-.: ..•. "!':. :i; ••-: &x i ../ - -'••
0 0 0 8 3
'II;-rj-
till <„>
<N
I.LJIJ'liN<1I •<]-I-LJ O;)
O'l —«NOil -
en •C". «;»•
\ Ll.l - ...1:1:- ...i ".'~i uj•r-.i 'X :rii L.II>\.'j *-. :-i in: r":>-~< "'-I II .... --C,ili: —•" '.''i n..." LJ..
r-..
ui-
in•:i- -in:«: '«]•
L,'"ta:LJll
LUI..JI
u"!
c::i
•M•:><
LL:;;: a•ID it' -« .iit: I-• 3: >::'•< 1 i. :iiy'3' v.: ciar^t 'CI]t'C.Ji 111:31 . c.
£rli C" tcri :5 : (•";f' I" i ••i>'i (i ' •:cj . >;.• i. i • 'ij.i v: i ....i *..>V*""' !:." H1 ';vi: -x -I
; ijo3Bt:
.; 'Lf'i< «:•i envf1 ll'l
1 ('I 1t1 1
T ...
j <;" ': i-i i> ijij •> "ii '
L.J..J.-J,...,:.i..L..
MJ CIH:?s. LJ.I
LlJ
. till (JLI
RIO07 I 7
— •-»•,f *
1
U"> :l:~>
\
LJ''"' l
ii1.. ,o> -f l
:»:
fs. U-'— r ,;;iCM cn:«: %r- I\J
10EJ;: :si:Cfr • "CM P---I ' LJCM ..jl t'l'•"< (j.! <]I"o i...* ti:i.!>'.0
LU...J1—4LL.tillot:ii:i:-!<l:>—i./i
U.ItiiiP— iEJ,:
3' _j• :z: c.;iCD' <rt'iun, uj (s»Li; i'.]i :»:•^a- o: ...jiCN ft. >-. LOJ:N :EE: :IE: c::« ..,............—.—..
•«: c:3 i— • cri>:.) LU -;r-ij"> :E:: u*ii:;* di»ii^i :::: «::> CM•«i- :ii' «•••> ci'i.'i <ii> >::>OL, *..f v"t
t'j •::! ... -.....i <..( iiii .=:3: •«.p-i :::: j— i:nLJ,., >"' III' -JI S.LJJ Mil nil i::i<rs: L:I I"L. c-j- cj;: :•:: ::-.: s.<:[: -ic; >:::• -:i: i>jLIJ >— r..J IJL:_ "••'
,.,. _ . ....... . ....
i-.". .".,
'.!.'..... ..
'"
ii
•...•"•i
- ,.-••r
»'... iiJ
:ii:UJi_ i 'I•; j.illj
-
-
•
-
..
.....
- I'Mi.'N!;s«.
. lJ"3 . .. ,i;_3i ... .—
. rri
. "-i"(.0
" -:i:.. ,...•'i:'• fi— J«i.lr :=
• iii:LJJ
:- "rr'i -,"• TT-VI—
. -J
tLL
LO ""r-/•-.. ..-...— -J
"... iCL; --••t-•' !c:i
" i""i Oil*,r LF"I,.,,
f..O....
• -i '-'....I.LJ •:]•ij i :ti•' |" ".''*tl.J LLJ
-•
-•
...
"""...
"L,
""" |S..
OJ1;«= "1lit;'11.. r,j
. (>4•».<" !:P' «/i
•i • 'ii1'"" LJ '11
...1 ..••-' '," (IJ-. —
• L::! •::•LJ>:. •?'!-- <i[: '\Liii >:">::: CM-:: -s. :-• CML iii '--i
-
r-if !„,.. ....,-... ,-.,..,.„..
.= ' i ^ "-,
-:;,
-
..._.'.", 1
"
I'll... r--«
.
r;>— LtJ.
••
..
11
— S
-..--
"I"1... '(j-.
-•
'.1.I'
-.•
:Li' ':"'.-,, ^ .... .....
..
.
-
•
.
•...
-•
...
.....
......
...
ii
r
::.•.;-;.
...........
i
1 I • ''.[
i " • :.
RIO07 11:1
iri
LL.VIIl
1.J<J1
C.JU'l
ii (3.. o
I.LJ O "i....J LJ, d-1'--•< :;:; i—Li. IP- III' <ICi.u1 ':"' en•or .i1 L'i.,
f*
-
,....,_.„.........„...
l" •> —
'' ! ' .'.L;'' >
(•
•;-
. r"'!'\::::
, LJ.!
LJli
.
•
.........................
..
- :pti
".. W• 0S)
"' v-'''1
" i:i-:" •-:]!
illj
'.' -IIJLlJ•"is
!""" :!;-- Ciji
;• J .-.
•:::•
c'iLI:- ir»
.. rvi o•s LLJHI! '..>
;"""W^• iicj u]
..
--
-
. r-i
:. !j:i!. ''- ilij;- 1:0. LU >::!'...i -..
>-.i CM- Li.. '-'
" S!?l< it: 'sciii i;::>"""" *-'• :>i/i ...»
•:: • .: :•
i:-'
-
•'
.,
• in... vj-
•
-
-
h.'
t,-l
"
-—• i::i..... ,-.-,
--
"• -i
'[ 007^
,. CS| OII-, .1-1I:
UJ!...J'
LiJt i l:i:::E: IL- •
'II? LU!LO C3'
L..J.J..L_J.J..I..1..JJ.
'"•'* 'J"-1
in in
' nj ru ni3rv "r' - ;- !--- .::. L.... '[
"< I L.ll.: ' 13 :qBt: ..........is. .«: . j
!:;i '!i: • .;: r 1/3
UJ
OS"
UJ
f- i.LJ
.0
I.L3'Li>
0720
i-. '
[::: LK '[
\c!:"c :
••-.-ICO ["-
oi' LI':>'•;h CII'iji' en:"tt': %t" 1 '1 J
1,0CD ...(M '"• I.LJCM ...1 LO— • "III '31£:• (..» a:
.Ijt—»
•a:III3!
IL.I:
i"ii> -inp«l 1 t'lct; LJ :«=•
'«• a! uj u:>LI> :SII ISJ i;S3':jl: i") "il 'C*"iii..j LU. -a-U'i ftj' '.ri(•:> iii)Cri mi U"i' C •.!i., ,;:;, ,.„r.L. r..:i O'i" • :!•£! *••'
I.LJ O' •"...J i'.J. illll :IC '-I
u! i--y.ii:i <t \li.ij »:::i en c:<j j ':-3 'tis: ... V1'•o: 'oi: c:- "it -:'MClj !!•— 'LJ t'ji; -- «
[ • r • • .'.r* * ••i/' • -ir- •' ;
; !'
;:!>
— l"l '1
,:»:
" ''I'•'*-
. I.f1.,[:s.:..
LJ.I•,/tIII
• fi.)
;- ••
" °"!LJ'I'in•"I?en'.l'l ....„ .
1 j.3ir • ;3I
i.ij•• illj.
LlJ!'. _.'''.".
•r::!UJ
rr-r--r-f-r-T--!-r"j- •" i'11 I;''i i ; —•.«
'f
!'-*3L'.1
— L.J
[]]; ,." j..!
'Hi
i?:i• co nci(--- lj'>
i.O•».'
...|''LJ |""
S. I.LJ"" :::: oI.LJ ::]i, «.«LO iii;aj LJJ
'
-
. U3'«=•
lit:1— cp•• >csi. ••"
CIIik 113-ini,
•" '.ii>..Ii ".r--. 0-1
. LJ.. —— •
• (II) ——ttJ'.. l""l• -.r: smi i::»iii: •• i[:!: ,'
• U'l -M
•[ I T . 1 T , \ 1
C ' '•- '
•:: ' •:' •!;: !
" ;i:;
-- '.;".i
„,.,_ •;;'"" ,"«
" w
...
i1:)— tlL)•
.
•!••:'-• .
.
.
"'•-'-'•'"
•
-
J" ...r.t.v.,....r.ri:;« '.:;•
t-'j •::" .;;'••r' I>.H
":....I.......
i "....
:
-...•
..••
•
i
fTT'l'.I.
.;.:'
..
..
. i i . , . i''.:' >'" ''i
111 R I 0 D 71 \ o o 0 8 9
i - L J
LJJ
un
11.1
llLJl
• 'it':C31iLOi|— 41
CO <3i•M- ft.«io :K::«= 'II?
il.l|j"j«:sj iiii'i1"! :in'•.J' '""1L'"l ill)
i» y:.i !niLL! i—
I.LJ
i--: !:i:
LJJin;L...Ll.lc:3'o:C"1'..iC.)•'311 1:i «UJI-i*^jC-JI..)
Q
:ri-iii)tX
C''I""•'F'':!:B"iri''Jj*!'in,,-..L.Oi
C'CI
j
-•i: *:-•31 •iiij (:I.*
\ L/' .1 —k L.j..'..j.....L.j.-t.j.j.. 1. :,:..L.j.j..i,...i.i., LJ.,-,
CI '"N
I.LJ'.n
1/3
-'f
r>j tin'S LJ.I
i/i
..J ..»•--' O Iu... —»Llll —'LJ-. '.n
00722
CO' 'Of. '>-'—' a., x: in
UJ O •»...i c.;> ciir -x—- ••:;:: i—LJ.. r- ill' :::LJ.I CI' illj
Li"'
LL)'
LJJ...i
——' LJ.JO'l L;'i
l-kl I"]S, I.LJ
LLJ <r.LO :E:aj i'u.
o
" LU CIJ..J ...i-^ i:-jLL. •'--;1.
-:r al ';T;,
Of '1
P R I INI C E T 0 N T E S T I N G L A B 0 R A T 0 R Y
Westcn TAT -'ob Mumber: 9-.Oe.36G"002GMWHJi Und£;rvv'occl Co jrt[lalran, New JE!r:;.:>yOe07i)
I3L.L.K ASBEST
SAMP LIE:IDIEIMTIFICATICN :
ANALYTICALMETHOD::
GROSS SAMPLE-APPEARANCE::
SAMPLE TRE-ATMENT:ASBESTOS RISERS
P RE SEE. NT'? ;:ASBESTOSCO NCIHsIT RATION ;:
AMOSITECHRYSomjEI ROC IDOL 3: TEE;OTHERTOTAL
OTHER RCESROIJSM:ATIE:RIAL:
"JEIROU;. GLASSCELLULOSE:OT-IEIFI
NoMiFiiaiROUsMAT:::E:I:AL PRESENT:
ANALYST:
:>3 ANALYSIS R!i;:)ORT - METHOD: E
001A07
Polarized Light:Microscopy IV :i thDispersion S'ta i n.i ng
HomogeneousFibrousGray
.Homogenized
Yes
45%0%0%0%
45%
S'i 1 i catesBindersOthers
Sus&n Sharpies
PA-6CQ/M4-82-020
I
ARI0072UQ 0 0 9 :