experimental considerations in the measurement of thermal relaxation and recovery of strained seals...

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Experimental Considerations in the Measurement of Thermal Relaxation and Recovery of Strained Seals Kurt Miller Axel Products, Inc. www.axelproducts.com

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Page 1: Experimental Considerations in the Measurement of Thermal Relaxation and Recovery of Strained Seals Kurt Miller Axel Products, Inc

Experimental Considerations in the Measurement of Thermal Relaxation and Recovery of Strained Seals

Kurt Miller

Axel Products, Inc.

www.axelproducts.com

Page 2: Experimental Considerations in the Measurement of Thermal Relaxation and Recovery of Strained Seals Kurt Miller Axel Products, Inc

Available at: www.axelproducts.com.

Page 3: Experimental Considerations in the Measurement of Thermal Relaxation and Recovery of Strained Seals Kurt Miller Axel Products, Inc

Overview

• Elastomer Seals• Stress, Strain and Temperature• A Particular Experiment

Page 4: Experimental Considerations in the Measurement of Thermal Relaxation and Recovery of Strained Seals Kurt Miller Axel Products, Inc

Elastomer Seals

• Normally Compressed• Fill a Space• Provide a Reaction

Force• Survive Temperature

Changes• Survive Chemical

Attack

Page 5: Experimental Considerations in the Measurement of Thermal Relaxation and Recovery of Strained Seals Kurt Miller Axel Products, Inc

Stress, Strain and Temperature

• Mental Experiment• Actual Experiment

Page 6: Experimental Considerations in the Measurement of Thermal Relaxation and Recovery of Strained Seals Kurt Miller Axel Products, Inc

Stress, Strain and Temperature

Page 7: Experimental Considerations in the Measurement of Thermal Relaxation and Recovery of Strained Seals Kurt Miller Axel Products, Inc

Stress, Strain and Temperature

• Short Term Stress Relaxation

• Some Softening

Page 8: Experimental Considerations in the Measurement of Thermal Relaxation and Recovery of Strained Seals Kurt Miller Axel Products, Inc

Stress, Strain and Temperature

Page 9: Experimental Considerations in the Measurement of Thermal Relaxation and Recovery of Strained Seals Kurt Miller Axel Products, Inc

Stress, Strain and Temperature

• Thermal Expansion • Elastomer > Steel

• Thermal Softening• Thermal Degradation• Additional Crosslinking

Page 10: Experimental Considerations in the Measurement of Thermal Relaxation and Recovery of Strained Seals Kurt Miller Axel Products, Inc

Stress, Strain and Temperature• Thermal Expansion vs Thermal Softening

Page 11: Experimental Considerations in the Measurement of Thermal Relaxation and Recovery of Strained Seals Kurt Miller Axel Products, Inc

Stress, Strain and Temperature

• NOT Long Term Stress Relaxation

Page 12: Experimental Considerations in the Measurement of Thermal Relaxation and Recovery of Strained Seals Kurt Miller Axel Products, Inc

Stress, Strain and Temperature

Page 13: Experimental Considerations in the Measurement of Thermal Relaxation and Recovery of Strained Seals Kurt Miller Axel Products, Inc

Stress, Strain and Temperature

• Thermal Contraction• Reduced Reaction Force

Page 14: Experimental Considerations in the Measurement of Thermal Relaxation and Recovery of Strained Seals Kurt Miller Axel Products, Inc

Stress, Strain and Temperature

Page 15: Experimental Considerations in the Measurement of Thermal Relaxation and Recovery of Strained Seals Kurt Miller Axel Products, Inc

Stress, Strain and Temperature• Additional Thermal Contraction• Reduced or Possible Loss of Reaction Force• The Seal May go into Tension!

Page 16: Experimental Considerations in the Measurement of Thermal Relaxation and Recovery of Strained Seals Kurt Miller Axel Products, Inc

A Particular Experiment

Page 17: Experimental Considerations in the Measurement of Thermal Relaxation and Recovery of Strained Seals Kurt Miller Axel Products, Inc

A Particular Experiment

Page 18: Experimental Considerations in the Measurement of Thermal Relaxation and Recovery of Strained Seals Kurt Miller Axel Products, Inc

A Particular Experiment

• Example Data, Constrained Seal

Page 19: Experimental Considerations in the Measurement of Thermal Relaxation and Recovery of Strained Seals Kurt Miller Axel Products, Inc

A Particular Experiment

• Example Data, Constrained Seal

Page 20: Experimental Considerations in the Measurement of Thermal Relaxation and Recovery of Strained Seals Kurt Miller Axel Products, Inc

A Particular Experiment

• This does not replace aging experiments.

Page 21: Experimental Considerations in the Measurement of Thermal Relaxation and Recovery of Strained Seals Kurt Miller Axel Products, Inc

A Particular Experiment

• This does not replace aging experiments.

Page 22: Experimental Considerations in the Measurement of Thermal Relaxation and Recovery of Strained Seals Kurt Miller Axel Products, Inc

A Particular Experiment

• This does not replace:– Thermal Expansion by TMA– Compression Set

Page 23: Experimental Considerations in the Measurement of Thermal Relaxation and Recovery of Strained Seals Kurt Miller Axel Products, Inc

Overview• Bad Things Happen When Hot,

Become Evident When Cold• Experimental data is Helpful