Temperatur pH

0 10 65.7 7.9 21 9 25.61 20 67.6 9.47 22 10 13.22 30 68.1 9.82 40 10 7.83 40 68.4 12.84 60 10 8.64 50 68.4 14.82 85 8 4.65 60 68.4 14.82 90 8 4.56 70 68.4 14.82 90 8 9.77 80 68.4 14.82 90 8 8.68 90 68.4 14.82 90 8 8.59 100 68.4 14.82 90 8 8.410 110 68.4 14.82 90 8 8.511 120 68.4 14.82 90 8 8.412 130 68.4 14.82 90 8 8.4

T(C) T(K) 1/T Ca 1/Ca-1/Cao 1/Ca

0 21 294 0.003401 5.55 4.73018018018018 0.180180180180181 22 295 0.00339 3.0875 4.87388663967611 0.3238866396761132 40 313 0.003195 1.6375 5.16068702290076 0.6106870229007633 60 333 0.003003 1.875 5.08333333333333 0.5333333333333334 85 358 0.002793 0.9125 5.6458904109589 1.09589041095895 90 363 0.002755 0.8625 5.70942028985507 1.159420289855076 90 363 0.002755 2.125 5.02058823529412 0.470588235294118

No sampel

Waktu (10

menit)

Piknometer + resin

Waktu viskositas(s)

Volume Titrasi 1(ml)

No sampel

0 20 40 60 80100

120140

1.361.38

1.41.421.441.461.48

1.51.521.54

Grafik hubungan antara densitas resin terhadap waktu

Hubungan antara densitas resin terhadap waktu

Waktu(menit)

Dens

itas r

esin

(gr/

ml)

0 20 40 60 80 100 120 1400123456789

10

Grafik hubungan kadar bebas formalin terhadap waktu

Grafik hubungan kadar bebas formalin terhadap waktu

Waktu(menit)

Kada

r for

mal

in b

ebas

0 20 40 60 80 100 120 1400

10

20

30

40

50

60

70

80

Grafik hubungan kadar resin terhadap waktu

Grafik hubungan kadar resin terhadap waktu

Waktu(menit)Ka

dar r

esin

7 90 363 0.002755 1.8875 5.07980132450331 0.5298013245033118 90 363 0.002755 1.8625 5.08691275167785 0.5369127516778529 90 363 0.002755 1.8 5.10555555555556 0.55555555555555610 90 363 0.002755 1.8375 5.09421768707483 0.5442176870748311 90 363 0.002755 1.825 5.09794520547945 0.54794520547945212 90 363 0.002755 1.825 5.09794520547945 0.547945205479452

0 20 40 60 80 100 120 1400

0.20.40.60.8

11.21.41.61.8

2

Grafik Hubungan Ln Ca0/Ca Terhadap Waktu

Grafik Hubungan Ln Ca0/Ca Terhadap Waktu

Waktu(menit)

LnCa

0/Ca

0 20 40 60 80 100 120 1400

0.2

0.4

0.6

0.8

1

1.2

1.4

Grafik Hubungan 1/Ca Terhadap Waktu

Grafik Hubungan 1/Ca Terhadap Waktu

Waktu(menit)

1/Ca

B1(gram) B3(gram) B4(gram) Pikno kosong (gr) Pikno+air (gr)

21 - - - - 28.2 54.513.7 11.1 11.7 3.7 3.8 28.2 54.57.5 11.8 11.4 5.5 5.3 28.2 54.58.6 7.9 6.6 5.1 4.8 28.2 54.54.9 11.3 11.2 4.95 4.83 28.2 54.54.6 10.9 10.9 7.3 1.7 28.2 54.59.5 11.3 11.2 4.9 5 28.2 54.58.7 11.2 10.7 5.2 4.9 28.2 54.58.6 10.6 10.6 4.9 4.9 28.2 54.58.2 10.9 10.6 5.1 5 28.2 54.58.4 10.9 11.3 4.9 5.3 28.2 54.58.4 10.8 10.3 5.24 4.91 28.2 54.58.4 8.6 7 4.7 4.7 28.2 54.5

Berat cawan ksong1 49.62 29.83 27.6

0.000874 4 365 29.36 26.67 30.88 28.99 27.610 32.911 32.9

LnCao/Ca2 LnCao/Ca t sampel K1 Ln K1 K2 Ln K2

0.05563827376863 2.22045E-16 10 2.22045E-17 -38.346238482 0.473018018018 -0.74862179820.1797817819937 0.586436226 20 0.029321811 -3.5294236273 0.2436943319838 -1.4118405768

0.63914146830915 1.220627239 30 0.040687575 -3.2018325245 0.1720229007634 -1.76012766710.48748029945126 1.085189268 40 0.027129732 -3.6071250415 0.1270833333333 -2.06291223972.05822982504286 1.805365121 50 0.036107302 -3.3212601508 0.1129178082192 -2.18109508582.30378213351258 1.861718058 60 0.031028634 -3.4728448138 0.0951570048309 -2.35222706910.37952618469389 0.960026125 70 0.013714659 -4.289290023 0.0717226890756 -2.6349481369

Volume Titrasi 2(ml)

B2(gram)

0 20 40 60 80 100 120 1400123456789

10

Grafik hubungan kadar bebas formalin terhadap waktu

Grafik hubungan kadar bebas formalin terhadap waktu

Waktu(menit)

Kada

r for

mal

in b

ebas

0 20 40 60 80 100 120 1400

10

20

30

40

50

60

70

80

Grafik hubungan kadar resin terhadap waktu

Grafik hubungan kadar resin terhadap waktu

Waktu(menit)

Kada

r res

in

0 20 40 60 80 100 120 1400

0.00050.001

0.00150.002

0.00250.003

0.00350.004

0.0045

Grafik hubungan viskositas terhadap waktu

Grafik hubungan viskosi-tas terhadap waktu

Waktu(menit)

Visk

osita

s res

in (g

r.cm

.s)

0.48104498652048 1.078544726 80 0.013481809 -4.3064139785 0.0634975165563 -2.75675448320.49404561675841 1.091878256 90 0.012131981 -4.411910286 0.0565212527964 -2.87313855590.52894997770319 1.126011263 100 0.011260113 -4.4864886538 0.0510555555556 -2.9748409145

0.5075804867256 1.105391976 110 0.010049018 -4.6002803646 0.0463110698825 -3.07237425610.51455745626071 1.112217941 120 0.009268483 -4.6811355763 0.0424828767123 -3.15865418510.51455745626071 1.112217941 130 0.008555523 -4.761178284 0.0392149631191 -3.2386968928

0 20 40 60 80 100 120 1400

0.2

0.4

0.6

0.8

1

1.2

1.4

Grafik Hubungan 1/Ca Terhadap Waktu

Grafik Hubungan 1/Ca Terhadap Waktu

Waktu(menit)

1/Ca

0.0026 0.0028 0.003 0.0032 0.0034 0.0036

-3.5

-3

-2.5

-2

-1.5

-1

-0.5

0

f(x) = 2700.30735923794 x − 10.2582505232528R² = 0.829476002974903

Grafik Hubungan 1/T Terhadap Ln K2

Grafik Hubungan 1/T Terhadap Ln K2Linear (Grafik Hubungan 1/T Terhadap Ln K2)

Massa air (gr) Vol pikno (ml) viskos resin NSp G1

26.3 0.997 26.3791374122 1.421577947 0.0021126528 1.417222866 -

26.3 0.997 26.3791374122 1.493604563 0.0026608229 2.044419785 29.32

26.3 0.997 26.3791374122 1.512558935 0.0027941785 2.197000604 31.67

26.3 0.997 26.3791374122 1.523931559 0.0036809578 3.211622252 29.76

26.3 0.997 26.3791374122 1.523931559 0.0042485822 3.86107802 26.38

26.3 0.997 26.3791374122 1.523931559 0.0042485822 3.86107802 27.1

26.3 0.997 26.3791374122 1.523931559 0.0042485822 3.86107802 26.66

26.3 0.997 26.3791374122 1.523931559 0.0042485822 3.86107802 27.5

26.3 0.997 26.3791374122 1.523931559 0.0042485822 3.86107802 32.86

26.3 0.997 26.3791374122 1.523931559 0.0042485822 3.86107802 29.9

26.3 0.997 26.3791374122 1.523931559 0.0042485822 3.86107802 17.42

26.3 0.997 26.3791374122 1.523931559 0.0042485822 3.86107802 17.32

26.3 0.997 26.3791374122 1.523931559 0.0042485822 3.86107802 17.4

rair rresin

0 20 40 60 80 100 120 1400

0.00050.001

0.00150.002

0.00250.003

0.00350.004

0.0045

Grafik hubungan viskositas terhadap waktu

Grafik hubungan viskosi-tas terhadap waktu

Waktu(menit)

Visk

osita

s res

in (g

r.cm

.s)

0.4 0.5 0.6 0.7 0.8 0.9 1 1.1 1.20

1

2

3

4

5

6

7

f(x) = − 2.83046411526436 x + 6.91792492381064R² = 0.361220229245905

Grafik hubungan Nsp/Cr terhadap Cr

Grafik hubungan Nsp/Cr terhadap CrLinear (Grafik hubungan Nsp/Cr terhadap Cr)

Cr

Nsp

/Cr

0.0026 0.0028 0.003 0.0032 0.0034 0.0036

-3.5

-3

-2.5

-2

-1.5

-1

-0.5

0

f(x) = 2700.30735923794 x − 10.2582505232528R² = 0.829476002974903

Grafik Hubungan 1/T Terhadap Ln K2

Grafik Hubungan 1/T Terhadap Ln K2Linear (Grafik Hubungan 1/T Terhadap Ln K2)

G4 itun Cr Nsp/Cr dv %CH2O/100 ml %CH2O/ml

- - - - 23.3 16.66665 0.166666532.36 30.4 0.454056 4.5025740077 13.45 9.2717625 0.09271762535.36 36.9 0.558134 3.9363300407 7.65 4.9174125 0.04917412533.55 37.9 0.57757 5.5605760584 8.6 5.630625 0.0563062530.22 38.4 0.58519 6.5979936032 4.75 2.7402375 0.02740237531.38 42.8 0.652243 5.9196951954 4.55 2.5900875 0.02590087531.08 44.2 0.673578 5.7321935376 9.6 6.381375 0.0638137532.86 53.6 0.816827 4.7269207904 8.65 5.6681625 0.05668162538.49 56.3 0.857973 4.5002300953 8.55 5.5930875 0.05593087535.89 59.9 0.912835 4.2297655153 8.3 5.4054 0.05405423.69 62.7 0.955505 4.0408764651 8.45 5.5180125 0.05518012523.78 64.6 0.98446 3.9220271573 8.4 5.480475 0.0548047524.65 72.5 1.10485 3.4946614395 8.4 5.480475 0.05480475

0.4 0.5 0.6 0.7 0.8 0.9 1 1.1 1.20

1

2

3

4

5

6

7

f(x) = − 2.83046411526436 x + 6.91792492381064R² = 0.361220229245905

Grafik hubungan Nsp/Cr terhadap Cr

Grafik hubungan Nsp/Cr terhadap CrLinear (Grafik hubungan Nsp/Cr terhadap Cr)

Cr

Nsp

/Cr

CH2O/l

166.666592.71762549.174125

56.3062527.40237525.900875

63.8137556.68162555.930875

54.05455.180125

54.8047554.80475

C.1 C.2

Kadar resin

0 10 1.42157795 0.002112653 - 01 20 1.49360456 0.002660823 30.4 12 30 1.51255894 0.002794179 36.9 23 40 1.52393156 0.003680958 37.9 34 50 1.52393156 0.004248582 38.4 45 60 1.52393156 0.004248582 42.8 56 70 1.52393156 0.004248582 44.2 67 80 1.52393156 0.004248582 53.6 78 90 1.52393156 0.004248582 56.3 89 100 1.52393156 0.004248582 59.9 910 110 1.52393156 0.004248582 62.7 1011 120 1.52393156 0.004248582 64.6 1112 130 1.52393156 0.004248582 72.5 12

C.4

Ca LnCao/Ca K1

0 10 5.55 2.22E-16 2.22E-17 01 20 3.0875 0.58643623 0.02932181 12 30 1.6375 1.22062724 0.04068757 23 40 1.875 1.08518927 0.02712973 34 50 0.9125 1.80536512 0.0361073 45 60 0.8625 1.86171806 0.03102863 56 70 2.125 0.96002613 0.01371466 67 80 1.8875 1.07854473 0.01348181 78 90 1.8625 1.09187826 0.01213198 89 100 1.8 1.12601126 0.01126011 910 110 1.8375 1.10539198 0.01004902 1011 120 1.825 1.11221794 0.00926848 1112 130 1.825 1.11221794 0.00855552 12

No sampel

Waktu (10

menit)rresin h resin (gr/cm.s) No

sampel

No sampel

Waktu (10

menit)

No sampel

c.3

Volume titrasi rata-rata NSp Cr Nsp/Cr

23.3 16.66665 0.166665 0 1.417223 - -13.45 9.2717625 0.092717625 1 2.04442 0.454056 4.5025747.65 4.9174125 0.049174125 2 2.197001 0.558134 3.936338.6 5.630625 0.05630625 3 3.211622 0.57757 5.560576

4.75 2.7402375 0.027402375 4 3.861078 0.58519 6.5979944.55 2.5900875 0.025900875 5 3.861078 0.652243 5.9196959.6 6.381375 0.06381375 6 3.861078 0.673578 5.732194

8.65 5.6681625 0.056681625 7 3.861078 0.816827 4.7269218.55 5.5930875 0.055930875 8 3.861078 0.857973 4.500238.3 5.4054 0.054054 9 3.861078 0.912835 4.229766

8.45 5.5180125 0.055180125 10 3.861078 0.955505 4.0408768.4 5.480475 0.05480475 11 3.861078 0.98446 3.9220278.4 5.480475 0.05480475 12 3.861078 1.10485 3.494661

Ca 1/Ca-1/Cao K2 T(K) 1/T

10 5.55 4.73018018 0.473018018 0 294 0.00340120 3.0875 4.87388664 0.243694332 1 295 0.0033930 1.6375 5.160687023 0.172022901 2 313 0.00319540 1.875 5.083333333 0.127083333 3 333 0.00300350 0.9125 5.645890411 0.112917808 4 358 0.00279360 0.8625 5.70942029 0.095157005 5 363 0.00275570 2.125 5.020588235 0.071722689 6 363 0.00275580 1.8875 5.079801325 0.063497517 7 363 0.00275590 1.8625 5.086912752 0.056521253 8 363 0.002755

100 1.8 5.105555556 0.051055556 9 363 0.002755110 1.8375 5.094217687 0.04631107 10 363 0.002755120 1.825 5.097945205 0.042482877 11 363 0.002755130 1.825 5.097945205 0.039214963 12 363 0.002755

CH2O/100 ml CH2O/ml No sampel

Waktu (10 menit)

No sampel

K1 Ln K1 K2 Ln K2

2.22E-17 -38.3462385 0.473018018 -0.7486217980.029322 -3.52942363 0.243694332 -1.4118405770.040688 -3.20183253 0.172022901 -1.760127666

0.02713 -3.60712504 0.127083333 -2.0629122420.036107 -3.32126015 0.112917808 -2.1810950880.031029 -3.47284481 0.095157005 -2.3522270670.013715 -4.28929002 0.071722689 -2.6349481380.013482 -4.30641398 0.063497517 -2.7567544760.012132 -4.41191029 0.056521253 -2.873138552

0.01126 -4.48648865 0.051055556 -2.9748409060.010049 -4.60028037 0.04631107 -3.0723742540.009268 -4.68113558 0.042482877 -3.1586541780.008556 -4.76117828 0.039214963 -3.238696896