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11
ERT 208 REACTION ENGINEERING MISMISURAYA MEOR AHMAD School of bioprocess engineering Unimap September 2011

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Page 1: ERT 208 REACTION ENGINEERING - UniMAP Portalportal.unimap.edu.my/portal/page/portal30/Lecturer Notes... · ERT 208 REACTION ENGINEERING ... of CSTR Lab 2: Effect of flow rate

ERT 208 REACTION ENGINEERING

MISMISURAYA MEOR AHMAD School of bioprocess engineering

Unimap September 2011

Page 2: ERT 208 REACTION ENGINEERING - UniMAP Portalportal.unimap.edu.my/portal/page/portal30/Lecturer Notes... · ERT 208 REACTION ENGINEERING ... of CSTR Lab 2: Effect of flow rate

CO1: Ability to solve the rate of reaction and their kinetics CO2: Ability to apply the laws and principles of reactions in order to analyze reactions in chemical and biochemical reactors CO3: Ability to calculate conversion and sizing for reactors and to explain steady-state isothermal reactor CO4: Ability to analyze the catalysis and catalytic reaction mechanisms.

Course outcomes

Page 3: ERT 208 REACTION ENGINEERING - UniMAP Portalportal.unimap.edu.my/portal/page/portal30/Lecturer Notes... · ERT 208 REACTION ENGINEERING ... of CSTR Lab 2: Effect of flow rate

Teaching plan

Study Week

Course Content Delivery Mode Assessment

1 MOLE BALANCE Rate of reaction, general balance equation, and general mole balance to the three most common types of industrial reactors; mole balances in

terms of conversion. (CO1) (3 hours)

Lecture, Prob. Solving.

2-3 CONVERSION AND REACTOR SIZING Equations to size CSTRs and PFRs; CSTRs and PFRs; and overall conversions

for reactors arranged in series; design equations for CSTRs and PFRs. (CO3) (6 hours)

Lecture, Prob. Solving.

Lab 1: Effect of stirring, flow rate and temperature on conversion in series of CSTR Lab 2: Effect of flow rate and temperature on conversion in tubular reactor

Laboratory experiment

Laboratory report, test

4-5 RATE LAW AND STOICHIOMETRY Rate law in terms of concentration and the Arrhenius temperature dependence; stoichiometric table to write the concentration in terms of

conversion; reaction system. (CO1) (6 hours)

Lecture, Prob. Solving.

Lab 3: Effect of temperature on the reaction in CSTR Lab 4 : Determination of activation energy and Arrhenius constant in a batch reactor

Laboratory experiment

Laboratory report, test

Lecturer: miss mismisuraya bt meor ahmad

Page 4: ERT 208 REACTION ENGINEERING - UniMAP Portalportal.unimap.edu.my/portal/page/portal30/Lecturer Notes... · ERT 208 REACTION ENGINEERING ... of CSTR Lab 2: Effect of flow rate

Teaching plan Lecturer: dr. MOHD IRFAN HATIM BIN MOHAMED DZAHIR

6-7 COLLECTION AND ANALYSIS OF RATE DATA Rate law and rate law parameters using graphical and numerical techniques; method required in using non-linear regression and

reactor selection. (CO2) (6 hours)

Lecture, Prob. Solving.

Lab 5: Determination of reaction rate constant and reaction order in batch reactor

Laboratory experiment

Laboratory report, test

9-10 MULTIPLE REACTIONS Different types of multiple reactions (series, series-parallel and Parallel reaction); the reaction system that maximizes the selectivity; yield and selectivity for multiple reactions. Algorithm for solving Reaction Engineering problems with multiple

reactions; Residence Time Distribution (RTD). (CO2) (6 hours)

Lecture, Prob. Solving.

Lab 6: Effect of residence time in CSTR

Laboratory experiment

Laboratory report, test

11 BIOREACTIONS IN BIOREACTORS

Pseudo-steady-state hypothesis (PSSH) in gas-phase reactions; rate laws; reaction mechanism, chain reaction and reaction pathways utilizing biomolecular reaction (yeast fermentation i.e Saccharomyces

cerevisiae) (CO2) (3 hours)

Lecture, Prob. Solving.

Page 5: ERT 208 REACTION ENGINEERING - UniMAP Portalportal.unimap.edu.my/portal/page/portal30/Lecturer Notes... · ERT 208 REACTION ENGINEERING ... of CSTR Lab 2: Effect of flow rate

Teaching plan Lecturer: MR. Zulfakar mokhtar

12-13 ISOTHERMAL REACTOR DESIGN Pressure drop and effect of system variables such as particle size on the conversion; optimized conversion when the catalyst particle

size is varied. (CO3) (6 hours)

Lecture, Prob. Solving.

14-15 CATALYSIS AND CATALYTIC REACTION MECHANISM Steps in a heterogeneous reaction (adsorption, surface reaction, and desorption) and rate-limiting step; different types of surface reaction (single site, dual site, and Eley-Rideal); rate law for

Langmuir-Hinshelwood kinetics. (CO4) (6 hours)

Lecture, Prob. Solving.

Lab 7: Catalytic reaction in packed bed reactor Laboratory experiment

Laboratory report, test

Page 6: ERT 208 REACTION ENGINEERING - UniMAP Portalportal.unimap.edu.my/portal/page/portal30/Lecturer Notes... · ERT 208 REACTION ENGINEERING ... of CSTR Lab 2: Effect of flow rate

1)Lectures: 42 hours (60 %)

2)Labs: 21 hours (30%)

3)Tutorials: 7 hours (10%)

LEARNING APPROACH

Page 7: ERT 208 REACTION ENGINEERING - UniMAP Portalportal.unimap.edu.my/portal/page/portal30/Lecturer Notes... · ERT 208 REACTION ENGINEERING ... of CSTR Lab 2: Effect of flow rate

1)Examination (70 %)

Mid Term: 20 %

Final Exam: 50 %

2) Course work (30 %)

Assignments/ Quizzes: 10 %

Laboratory: 20 %

Evaluation contribution

Page 8: ERT 208 REACTION ENGINEERING - UniMAP Portalportal.unimap.edu.my/portal/page/portal30/Lecturer Notes... · ERT 208 REACTION ENGINEERING ... of CSTR Lab 2: Effect of flow rate

text book

RM 78 Main Office, School Of Bioprocess

Page 9: ERT 208 REACTION ENGINEERING - UniMAP Portalportal.unimap.edu.my/portal/page/portal30/Lecturer Notes... · ERT 208 REACTION ENGINEERING ... of CSTR Lab 2: Effect of flow rate

LAB BRIEFING

• Lab briefing by Mr. Mahfuz Affif Mohd Ruslan

15 September 2011

2.00 pm

LAB (MRD)

Compulsory, attendance will be taken

Page 10: ERT 208 REACTION ENGINEERING - UniMAP Portalportal.unimap.edu.my/portal/page/portal30/Lecturer Notes... · ERT 208 REACTION ENGINEERING ... of CSTR Lab 2: Effect of flow rate

Type of Reactor

Characteristics

Kinds of Phases Present

Use

Advantanges

Disadvantanges

Batch

CSTR

PFR

PBR

ASSIGNMENT

Comparison of Reactor Types:

Page 11: ERT 208 REACTION ENGINEERING - UniMAP Portalportal.unimap.edu.my/portal/page/portal30/Lecturer Notes... · ERT 208 REACTION ENGINEERING ... of CSTR Lab 2: Effect of flow rate

Q &A

THANK YOU