epa project no.: ard008052508 contractor work order ...sampling qa/qc plan popile inc. site...

SAMPLING QA/QC PLANPopile Inc. Site

ElDorado, Union County, Arkansas

Prepared byEcology and Environment, Inc.Technical Assistance Teaa - Region 6

EPA Project No . : ARD008052508Contractor Work Order.: T06-8909-07EPA Contract No . : 68-01-7368

APPROVALS

Ecology and Environment, Inc. EPA

Robert Sullivan Date Pat H a m m a c k D a t eProject Manager On-Scene Coordinator

1.0 BACKGROOMD

The Popile Inc. •ite sampling activity is being conductedby the EPA Region 6 Emergency Response Branch (ERB)to determine imminent threats to public health andthe environment posed by visual offsite migration ofcontaminants into Bayou de Loutre.

The following information is known about the site:

The Popile site, a former wood treatment facility,occupies approximately 41 acres and is located onSouthfield Road, approximately 2000 feet south of theintersection of Southfield Road and U.S. 82, ElDorado, Union County, Arkansas. While the propertyhas been split and sold to two parties, Popite and ElArk, the property is considered one site in thisplan. The property includes the building used forwood treatment, closed waste water impoundments, a"salt flat" north of the closed impoundments, a"spray area" for water from the closed impoundments,and the storage area for the treated wood.

The types of wood treating material suspected to behandled by the facility were:

PentachiorophenolCreosote

These compounds are on the Hazardous Substance List.

The volume of contaminants is unknown. Wood treatmentat the site began in 1947 and ceased in 1982.

The scope of possibly contaminated media to beaddressed are surface soils, subsurface soils,sediments, surface water, and groundwater.

The basis of this information is taken from anEcology and Environment, Inc. FIT report dated03 October 1988 and an Arkansas Department ofPollution Control and Ecology (ADPC&E) report from a23 March 1989 site evaluation.

2.0 OBJECTIVES

The objective of this project is to determine:

The presence, extent, magnitude, impact and offsitemigration of contamination.

For the purpose of:

Site characterization, risk assessment and evaluation

•3 - ^of rexaval alteznafciye*. •

The data will be evaluated against: -

Federal(EPA)/State(ADPC&E) action levels.

3.0 QUALITY ASSURANCE OBJECTIVES

Site acreening methodologies including a field •urvey andestablishment of an accurate base map, soil gas sampling,air aonitoring, electroaagnetic conductivity (EM), andground penetrating radar (GPR) will be utilized to aapanomalous areas. This will help in qualifying locationsduring enactment of the sample plan. y^

K^000

All sampling and shipping procedures will be conducted inaccordance with EPA Directive 9240.0-1, User's Guide tothe Contract Laboratory Program (CLP).,

PARAMETERS DATA QA OBJECTIVE

Field Survey Base map, sample locations, QA-1geohydrologic contours•

Air Monitoring Hnu PI-101 for real-time QA-1monitoring, Photovac 10S70for sample analysis.

Soil Gas Sampling Tenax Tube/Tedlar Bag samples QA-1collected by SKC air pump.

Geophysical Survey Geonics EM-31 and GSSI GPR QA-1for subsurface investigation.

CLP Sampling Soil/sediment/water for HSL 9240.0-1Organics, HSL Metals andTotal Dioxin/Furan.

Methods to be employed for both analysis and confirmationare outlined in 9240.0-1. Laboratory scheduling isprovided by the CLP Sample Management Office (SMO). Datavalidation is provided by the EPA Houston Laboratory.

4.0 APPROACH AND SAMPLING METHODOLOGIES

4.1 Geophysical.

4.la Media.Soil/water/contaminant interfaces. Subsurfacematerial.

3 )4.1b Sampling Equipment.

Magnetic/Cable Locator. Detects a metallicobject or an induced field.

Geonics EM-31. Measures the electricalconductivity of subsurface material.

GSSI GPR. Profiles response of radar wavereflections in subsurface material.

4.Ic Sampling Equipment Decontamination.Cable Locator and EM-31 is non-contact method.GPR antenna is sled-mounted. Sled will beplaced on dedicated visqueen liners. Moist wipefor dust.

4.Id Sampling design.Equipment operated in a continuous datacollection mode upon a gridded site area forpoint referencing. Grid established by fieldsurvey. Equipment will be calibrated andoperated consistent with manufacturerspecifications.

4.le Standard Operating Procedures.E&E SOP - Surface Geophysical Techniques.E&E SOP - Conducting Electromagnetic

Conductivity Surveys.EPA-ERT SOP 2159 - General Surface Geophysics.

4.2 Soil Gas.

4.2a Media.Relative soil hydrocarbon vapor concentration.

4.2b Sampling Equipment.Slambar/Tile Probe/Copper Pipe/Tygon Tubing.Tenax Tubes/Tedlar Bags.SKC Air Pump/Dessicator.Hnu PI-101.Photovac 10S70.

4.2c Sampling Equipment Decontamination.Slambar/Tile Probe - physical removal, Alconoxdetergent wash, potable water rinse. Tenaxtubes/tedlar bags • dedicated to each sample.Analytical equipment - purge after each samplewith ambient air.

4.2d Sampling Design.Tile probes to be driven into the ground 3 to 5foot depth at gridded sample locations. Copperpipe/tygon tubing placed in hole initiated bytile probe. Real-time air monitoring with HnuPI-101 for volatile organics. Collect selected

•^) :)!tmsac tube/tedlar bag samples using 8KC airpump/dessicator and analyze with Photovac 10S70for total volatile organics.

4.2e Standard OperatingE&E SOP - Soil GasEPA-ERT SOP 2149 -EPA-ERT SOP 2050 -EPA-ERT SOP 2052 -

4.3 CLP Sampling.

Procedures.Saapling.Soil Gas Sampling.Tedlar Bag Sampling.Tenax Tube Sampling.

4.3a

4.3bMatrix/MediaSurface waterGroundwaterSedimentSurface soilSubsurface soil

Media.Surface water.Groundwater.Sediment.Surface soil.Subsurface soil.Sampling equipment.

EquipmentSample bottleWell bailerSample bottleEckman dredgeSample bottleTrowelSample bottleSlambarSleeveSample bottle

FabricationGlass/plasticTeflonGlass/plasticStainless steelGlassStainless steelGlassStainless steelAcetateGlass

DedicatedYesNoYesNoYesYesYesNoYesYes

4.3C

4.3d

4.3e

Sampling Equipment Decontamination.Nondedicated equipment - physical removal,Alconox detergent wash, potable water rinse,distilled/deionized water rinse. Acetonesolvent rinse. Sample bottles moist wipe.

Sampling Design.Collect 20 grab surface soils for totaldioxin/furan, HSL organics and HSL metalsanalysis. Survey base map and collect 50 grabor composite surface or subsurface soils forHSL organics and HSL metals analysis. Collect10 surface water or groundwater samples for HSLorganics and HSL metals analysis. Samplecollection, manifesting, packaging and shippingprotocols will follow 9240.0-1.

Standard Operating Procedures.E&E SOP - Groundwater Sampling.EPA-ERT SOP 2007 - Groundwater Well Sampling.EPA-ERT SOP 2012 - Soil Sampling.

^ ^EPA-ERT SOP 2013 - Surface Water Sampling.EPA-ERT SOP 2016 - Sediment Sampling.EPA-ERT SOP 2151 - Water Level Measurement.

4.4 Sample Documentation.

All sample documents must be completed legibly inink. Any corrections or revisions must be made bylining through the incorrect entry and by initialingthe error.

4.4a Field Logbook.The Field Logbook is essentially a descriptivenotebook detailing site activities andobservations so that an accurate account of

^•: • ^4.4o Ch»in*-of-Custody Record.

A Chain-of-Custody record must be maintainedfrom the time the sample is taken until itsfinal disposition. Every transfer of custodymust be noted and signed for and a copy of thisrecord kept by each individual who has signed.When samples (or groups of samples) are notunder direct control of the individualresponsible for them, they must be stored in alocked container sealed with a Chain-of-Custodyseal.

The Chain-of-Custody record should include (atminimum) the following:

1. Sample identification number.2. Sample information.3. Sample location.4. Sample date.5. Name(s) and signature(s) of sampler(s).6. Signature (s) of any individual (s) with

control over samples.7. Airbill and shipping paper numbers.

4.4d Chain-of-Custody Seals.

Chain-of-Custody Seals demonstrate that asample container has not been tampered with oropened.

The individual in possession of the sample(s)must sign and date the seal, affixing it insuch a manner that the container cannot beopened without breaking the seal.

4.4e Traffic Forms.

CLP Routine Analytical Service (RAS) requiressubmission of Organic and Inorganic TrafficForms. Special Analytical Service (SAS)requires submission of Packing Lists. Samplesfor dioxin analysis require submission ofDioxin Shipment Record. All requisite formswill be completed per 9240.0-1.

4.4f Corrective Action.

Corrective actions are those taken in responseto nonconformance reports, audited findings, orsurveillance findings. The quality assurancerepresentative is responsible for reviewing'audit reports and nonconformance reports todetermine the significant or repetitiousconditions adverse to quality, or failure to

) ^implement or adhere to required qualityassurance practices. When such problems aredefined, the responsible manager mustinvestigate the causes of the probleas anddefine and implement the necessary actions tocorrect the problems. Documentation thatsupports major corrective actions must bemaintained in the project files.

5.0 PROJECT ORGANIZATION AND RESPOSIBILITIES.

The EPA On-Scene Coordinator, Pat Hanmack, is responsiblefor the coordination of resources to develop andimplement the Sampling QA/QC Plan and will providedirection to Ecology and Environment, Inc. concerningproject objectives, sampling needs, and schedule.

The Ecology and Environment, Inc. Project Manager, BobSullivan, is the primary point of contact with the EPA On-Scene Coordinator. The project manager is responsible forthe development and completion of the Sampling QA/QC Plan,project team organization, and supervision of all projecttasks, including reporting and deliverables. In addition,he is responsible for ensuring field adherence to theSampling QA/QC Plan and recording any deviations. Theproject manager is also the primary contact with theRegion Sample Coordinator (RSC), Myra Perez in Region 6,for questions concerning sampling efforts.

The Ecology and Environment, Inc. Project Director, BobMarguccio, is responsible for auditing and guiding theproject team, reviewing the final deliverables andproposing corrective action, if necessary, fornonconformity to the Sampling QA/QC Plan.

The Ecology and Environment, Inc. Site Safety Officer,Bill demons, is responsible for adherence to all companyand established field health and safety protocols.

The following field personnel will work on this project:

Bob Sullivan (PM) - Supervisory.Bob Marguccio (PD) - Geohydrologic.

Tom Yank - Sampler.Keith Demerit! - Sampler.

6.0 QUALITY ASSURANCE REQUIREMENTS.

6.1 QA-1.

3J) )

6 .la Instrument calibration and/or perfoxxance cheekof the given t—t methods will be documented byfield data sheets or logbook.

6.1b Detection limit will be determined, unlessinappropriate•

6.ic Samples will be documented by field logbook.

6.2 9240.0-1.

6.2a User's Guide to the Contract LaboratoryProgram (CLP).

6.2b Document discrepencies with RSC and SMO.

7.0 DELIVERABLES.

The Ecology and Environment, Inc., Project Manager, BobSullivan, will maintain contact with the EPA On-SceneCoordinator, Pat Hamaack, to keep him informed about thetechnical and financial progress of this project. Thiscommunication will commence with the issuance of the workassignment. Activities under this project will bereported in status reports, analytical reports, and afinal report. Activities will also be summarized inappropriate format for inclusion in monthly and annualreports.

8.0 DATA VALIDATION.

8.1 QA-1.Data will be evaluated for calibration and detectionlimits at a minimum.

8.2 Contract Laboratory Program (CLP).EPA Houston Laboratory will QA/QC all datadeliverables from submitting laboratories as per9240.0-1.

REGION VI PLRMNEO SAMPLING WTIVITY - CUP WWLVSCS

Ca^li's /̂̂ >p^MW2SIT • .._..........___.._ •SI TE_/?J3/^^;S^_...___ LOCRT \W_£^_JD^^f_^_/f^_ SftS •.CASE •

^SftMPl-ING ORef»IIZ«TION^5^_/̂ 4.» î̂ _:̂ £7^ CONTRCT PERSON^^_^1 '̂?Z^^^^ T6L •^^f5^3270,

SUBCONTRf̂ TOR^^^^ '̂̂ ^ -̂̂ CONTRCT PERSON/̂ ê Lî ^ a,- TEL ll.̂ .̂ -.Ẑ .-:.̂ .̂/.̂

SAMPLING DRTE^^ff^^^!py SHIPPIN8 t)RTE_J!?//A/^l___ flLTCRNRTE SWMP/'SHIPPIMB n«TE___

TWC OF INVESTIGATION ^^•f

U.S.KNVIltONHUITAL PROTKOTZON A6KNCYCt.9 ••»?!• H«n«gi—flt Offia«201 Kcdi—n flt. Alexandria, V 22134Phon«( 703/957-2490Tol DJL«n« Cutl*r

; SAS Kurbar It (

SPECIAL ANALYTICAL SERVICESCliant Raqirttt

A. KPA Ragion/CUant; fisfllfiQ Yl

B. R»CC R«pra««ntativt M^ra ^ ESCtS ^ BÂ y«CEft& r-

C. T»l»phon» • t i.Wi iS2l212S ^00

D* 0«t« of Uttquftati 0@

B. 3if N«B«: Popil« Inc. • 11 Dorado, Ar. ^

?!•••• provida b«low dwoription of your r«qvftfc for 8p«ol«l Analytical S«rvic<und«r th« Contract Laboratory Program. :n ordar to Moat •ffleiently obtain la-boratory capability for your raqua»t, plaaaa addraaa the following conftidaraticIf epplioabla. Inoorpl«t« or •rronaou* -nforxiation May raault in a delay in Uprocaaainf of your raquaat. ?!•••• continua raapon«« on additional ahaafca, orattach auppl«»«nfry information aa naadad.

1. Ganaral daacription of analytical aarvica raquaatad:f

TCL organica, aatala and pelyc^lonv>A^^ ô^^•+ purAn^ en^ê-S . A/o C^.

2. Definition and numbar of work unita involvd (apacify whathar whola •aaplaaor fraetionay whathar oraanica or inoraaniea; whathar aquaoua or •oil andaadfanft and whathar low, radium or high eonoantration.

•AS - 10 low cone. watara for TCL organica and wtala* No CN.

70 •adiun aoila

Tol D^——kOu^l—^ ) )POBti iXiBlr.- THtt-» ii .. •. ...P«f 2

6. Mu»bar of day analyaia •nd data raquirad aftar laboratory racaipt of ••«•plaai

. „ , ap+o.+w^ly-oi'ifc 6^) ^Ay5" W6)C'.wM^*F

..) )Tor Dtiufr-OuUT^Poplla Xno«?••• •

12* D«to r«qulr«irnt«

P«r«irfr

HAS S«»pl««

•At S««pl««

13. QC ftftquir«»«nt«

Audlta yquifd

D«t«Gtton li»it

Aa per ZPB ProtocolA* p«r ZFB Protoeol

Froquonoy of •udlf

A* par IFB Protocol0^

A« p«f ZFB Protoeo^r000

Li.»if ( K or concent)0©

A« pT XFB Protoeol

14. Action r«quir«d if linita •r« •xe*^l«d

Contact Dl«n* Cutl*r fro» SMO i«««di«t«ly. 9HO will contact th« DPQ •ndr*qu««t Inatruotl.ona.

?!•••• return thi« r«qir«t to th« 9a»pl« Management Off left aa •con •• po««ibl«to •xp«dit« proe«i»»ing of your r«qu««t for ftp«ci«l •nclytieal ••rvlo«»* Shouldyou h«v any qu««tion« or nwd •ny •••i«t«nc«, ?!•••• cont«et your R«9ion«lK«prft«ftntativ •t tha S«Rpl* Man«g«««nt Of flea.

ATT«eiMUT A

•••• NOTKt ZF 2,»,7»e- TCOD It DKTKCTKO AT 0.» PP» OR ORKATXR ON THI Dfc-S•quired if control liaita ara axeaadad.

A xothod blank •uat ba praparad by tha laboratory for ovary 20 aaaplaa of aaatriK, or whonovor aarplaa ara extracted, whiehovar ia treater. The concen-tration of any analyte in the »athed blank ahould be laaa than tha dataetionlimit* liatad above. If an analyta ia detected in the •ethod blank, allaaeooiatad aaaploa containing laaa than fiva tiftaa tha blank eoneantration ofthe analyte ara to be fla««ed with a • on the data raport auaRary. MS/USDanalyaia ia to be eonduoted en one aaaple per 20 for a aiven •atrix. Spikato obtain a final axtraet oonoantration of SOO n»/l for tha tetra thru haptaiaeaara and 2000 n«/l for the oota iaonara* Raooveriea ahould be 40 • 120 ft.No aotien ia to be taken if KS/M8D raaoveriea are out of control li»ita.

a.-,, • ^

^MiMlMlll • 8 -

•̂pT«il«A and HMlyr Pr««—l ff Oily ••11/MlMftt tawl— (fto«ftl«>.•

••114 iMtflai V«« !F« (M«M. toltf Ol««««lo«i f to«l«w«t»« ludgw MMI••11«, irino Mhto«ftw«l nitrlo acid itf reflux 4liw~— MeM««*y «• rtlowiany •lly MtTlcl. Analyc tflQ«««««— ky XF9 Pr«i—l«. Thi« r •wll«- in

oo•tel* ftp •12 fetal* w MtMl in «h« ire. PT ^ .^ w CPfl H ĥod 24C.I,(toroury in ••tfliMHrt, mi fWthwta f«p Chwmfal mMlylB •f (MT 14 Uu«««,ftar«h, fl. 0

fî•) ftrrly«l«^ c-ulti • f«XXi» XF» (AM) PfwfcMl o

b) 0«i«eirn llNltfl • foll«w If (KM) Pr«««o«l

«) OC (Uqulrffntt - f«ll«u IF! (MM) Protowl

4) Aetfn r«oulr«d If ItMlif •r« •«CM«M - fftllcM IFB Protocol,am«M< MO ft dir—tfA.

•) Itold rife • f*ll«w IF«

U.S. ENVKONMENXAL PROTECTION AGENCYCLP Sample Management OfficeP.O. Box 818 - Alexandria, Virginia 22313Phone: 703/557-2*90 - FTS/557-2490

SPECIAL ANALYTICAL SERVICEPACKING LIST

SA5 Number^^- rCOPIED FROMPOOR QUALITY

r\Sampling Office:

^.^"SI ^1\ • / < i i7. f €>?- . .

8. J 08 ' , • . i ,9. t 0^7 i i » < i « i i

io. I (o i , ' • i f / »11. ? 1 1 , , ' < ... - ,12. i ( ;L13. 13 ' . ' • ' • ' <14. 1 M , . , • • / ,15. \ ,is. ! / y19. \ t^20< i 20 , .. . . . .

Sampling Date(s):

/•-̂ 'a-.Date Shipped:

l o U & f ' . ^

Site Name/Code:p^,,,e- //WP^ry^l,^-^

Ship To:^>\5-^^A^£;4 /^H^/y'-A^I

^

U^ EhnfIROfrttWifl̂ PW^CTIO^ AGENCYCLP Sample Manag—ogm Office- " - " • • 'P.O. Box 818 - Alexandria, Virginia 22313Phone: 703/557-2490 - FTS/557-2490

'syssssss-€~ow- F

SPECIAL ANALYTICAL SERVICEPACKING LIST

Sampling Office:f?b6(->^ fo .PAK.AI.

Sampling Contact:(^3(1

USEPA Contract LabtxattxyProy.il)Sampte- Ulsuy^tiwK-filisus^^-.. ..PO. Box 818 Alexandra, Virginia 22313FTS 8-557-2490 703/557.2490 ^LP DIOXIN SHIPMENT RECORD

WHITE—SMO Copy YELLOW—Region Copy PINK—Lab Copy for Return to SMO GOLI>-Lab Copy

MgN^̂ ^

^^®E3^ î̂ rfy \̂

ENVIRONMENTAL PROTECTION AGENCYOffice of Enforcement

CHAIN OF CUSTODY RECORD

REGION 6First International BIdg., 1201 Elm St.

_____Dallas, Texas 75270____PROJ. NO.

•TtP-f<PROJECT NAME

fop(L^SAMPLERS: (SifMUM)

STA. NO. DATE TIME STATION LOCATION

NO.

OF

CON-TAINERS

REMARKS

/(. ; • . 1030

^ '/ ' /oJ^

>« -« < i /oVo

,

ENVIRONMENTAL PROTECTION AGENCY, ,Office of Enforcement


REGIONSFirst International BIdg., 1201 Elm St.

Dallas. Texas 75270PROJ.NO.

TF^-KPROJECT NAME

fOfttESAMPLERS: (SUMtunt


NO.

OF

CON-TAINERS

REMARKS

" " s» ̂ y17 f- o^J-?g^

—r-

^ te-fi ») /O^P

^-^ 1Rifttquiched by: (Sigmtur,) Date/Time

iT)i^|^|oypf)Received by: (Sigmwrfl Relinquished by: ISigmturfl Date/Time Received by'

SUP

NW»l

SHE NAME: «-> . . .'.».'- .•»•; ;•; ..•-:•" .'ro^\cd

1.F '°

l̂ cm flp CT

^-

i

srrcspRJ.io: -R>f̂ P^

^1

-

.&

' z

i •) ->

. ^

6RAS -

ANALTOlO

1î

TYPeOPAAlVlWtd^dN^ ,..,...SUPERFUN&-PA Sl ESI R1FS RO RA

NPLD OWJ OTMEB__MOfctStipgaaiMP- • annnnAM

SmPTO:———— — ————•""i '

l̂-f 2»(^ê^^ôl 7r^s?r.-€.B^f^s^C>r\w.^ lJ\ -70(Z6»ATTM-/^T''-i^y '^>/^9-£r>

^ __ _ a^^îit

; TYPE OF ACTIVITY (CIRCLE ONE) . . . , fl̂ SHIP TO. , - - 7 - - 7 - ® - --. '-. SAMPLE OE^eQQt̂ ®; SUPERFUND-PA SIESI RtFS RD RA/tR ^..t^ SiL».+L A$(£».r^ ?£££K*ftR /fK-^Suai f* n&u nruBB • V ^ pi»^i» •^v*"'T'̂ ^fc-»c*«i t^ft •i«oufwnu& —AIBM \p. pet-';...:..-- • ^NCUJ OUM O T H E R . — . S s a ' . p _ . ^ GROUND WATER T'OlCTsas^ ,

NON^PERFUND—______._PROGRAM (pBt^l [T^S ^r;fc..0(c*

TYPE OF ACTIVITY (OBOE ONE) . fl)SUPERFUND-PA 8l ESt RIPS RD RA(ER

MPLD 09M 07MEB2=^MniiUtiippaFUMn' .••i/yi^

CLPSAMPLENUMBER

(FROM LABELS)

-Fk ^45-^-7Ce^••:--•• --- r

—s^-i, \\

-

. 1 ®e


PROJECT NAMEPROJ. NO.

m'/< fO^ll-S'.EPS: (SifMtUH)

"KA-AJ^V y \ )

STA. HO. DATE TIME


NO.

OF

CON-TAINERS

REGION 6Pint International Btdg.. 1201 Elm St.

_____Dallas. Texas 75270

REMARKS

STATION LOCATION

SL 0 I

3St Cf^ ?/

JZ.St (3^ J -£2-Sl 0^

St ^Q 3SL \\SL \Z. -Sl

//30 SL 1 3 ± -H.^-^6^^.A I

SL ^-Date/Time

iReceived by: ISifmiurfl Relinquished by: (SigmtunI Date/Time Received by: ISigmitirf)

Date/Time Received by: ISigmninI Relinquished by: ISignatur»l Date / Time Received by: (Sigmiur»l

Rellnauiihed by: (Signituiv) Date/Time Received for Laboratory by:(Sigfuturvl

Date /Time Remarks

Diltributidn: Origind Accompani— Shipment; Copy to Coordinator Field File*




Dallas, Texas 75270PROJECT NAME

pofii^e

8TA.NO. DATE TIME

^r"^"^~x^s^ ̂. it • . . - - \C Ol I -̂

STATION LOCATION

NO.

OF

CON-TAINERS

REMARKS

6-^6?.^yQ •r

f̂i \/ m

• » ' • » : -

EN«lJ»6iNMENTAl. PROTECTION AGENCY-4^g Office of Enforcement

NO. PROJECT NAME

tRS: tSiyutur*)

STA. NO. DATE TIME


NO.

OF

CON-TAINERS

REGION 6Firrt International BIdg.. 1201 Elm St.____ Dallas, Texas 75270

REMARKS

"I A 6 ^ '•.STATION LOCATION

3

-K-

-a-

5Z. .?^

-LL AJL•

ENVIRONMENTAL PROTECTION AGENCY^»^ Office of Enforonnent


Dallas, Texas 75270

ENVIRONMENTAL PROTECTION AGENCYOff ice of Enforcement



_____Dallas, Texas 75270PROJECT NAMEPROJ. NO.

rf^ eofi^SAMPLERS: (SiSMtunI - i i

U^y?^^,^J^^ Tifl̂ ^suJ^


NO.

OF

CON-TAINERS

REMARKS

^ i

IENTAL PROTECTION AGENCYfe OffiOl of Enforcement


'mi

^yn^M. î f^YX) ̂ ̂STATION LOCATION

REGION 6First International Bidg., 1201 Elm St.

Dallas, Texas 75270

NO.

OF

CON-TAINERS

- '•- \ \\ \

\ "REMARKS .\

, \ - -V'

-̂ €>(, W-l .^-^^1-7 ^ -^H q -7- — — * • • ' ' ' f V ~ g'f -'-' '—/ • • ^ 'f-"i-^ ' '

^^^^-^37.^[^-g^^

5^ '70 (- - ^-b -{7,2 > /„ . .-) b^i ^ S I ^ .v fe. Q 6 ̂ J |

XPIED FROMQUALITY

)RiGINAL

\ \\ '

Oaf/Tim*

loi^l-QoOODate /Time Received by: (Sigmturff

Received by: iSiiMtuni Relinquished by: ISigmturf)

Relinquished by: tSisnanirif

Date / Time Received t>y: fSivmpunIll\^

Date/Time Received by.;/s

EPA Form 2075-7 (•-•7)

WHITE — SMO COPY PINK - CLIENT COPY WHITE — LAB COPY FOR RETURN TO SMO YELLOW — LAB COPY

SUPCRRJWD—PA 1 ESTRIPS RO RA/• NPLO'OliM' OTHER__2

NON^UPERPUNO-..—._____PROQfU

SITE NAME: ^..•..-,^^J-.^.-...,-;.FO^I ^€ ' ' : " ' " "•• ' -________^/^

CnY. STATE; . ••-.' .̂-̂ . SITE SPILL 10:^7 T^^J^ ̂ f^pwyt^t

TY-PeOF ACTIVITY (aRCtEO^)———SUPERFUND-.PA 81 ESI RIFS RD

NPLO O&M OTHER.NON-8UPEBFUND—— PBC

SITE NAME: , ^ iroff/e. - ^

CITY. STATE: ' .^/ ̂ .̂ ^>. •/

REGION NO: SAMPLING COMPANY(p ^4^ -rvr-

SAMPLER: (NAME)^L ;•

.̂ ys.'iis-"-' •V •: ' • ' : .'"'JOtiarl̂ r^Ca'TS^Q^--"-.. '•.:».siWU.'spmfy>SvierJ^ii^.-iSr-fwrnw .-

i.'. . • •J'MX WT-t • •




Dallas, Texas 75270PROJ. NO.

TIA^

PROJECT NAME

?C^ ^<SAMPLERS: ISHnuunI

STA.NO. DATE TIME STATION LOCATION

NO.

OF

CON-TAINERS

REMARKS

SL -i{ M.gL •)^ 3^,^L^9 1 • I .• • * . T *

TYPE OP ACTIVITY (CIRCLE ONE)SUPERPUND-PA 81 ESI RIFS RO RA,

NPLO O&M OTHER__NON.SUPERFUND—________PROGRAM

SITE NAME:

SHIP TO:

BEGIN: / ^ " j ?^ END: fafl^l'!-^

DATE SHIPPgP- /̂ /̂ /ĵ AHRIgH-Tc^^

AIRBILL WQ^QS531Q1

RASANALYSIS

HIGHONLY(SAS)

SPECIALHANDLING

SHIP MEDIUM AND HIGH CONCENTRA .-.OriSAMPLES IN PAINT CANS

eSTATION

LOCATION

//

£PA Form 2075-6 (8-87)WHITE — SMO COPY PtNK — CLIENT COPY WHITE — LAB COPY FOR RETURN TO SMO YELLOW — LAB COPY

'I^FPa CONTRSFT I f tBDRATDRY PPOG

,'i l,3,i'-» *\1

SITE NAME:

CITY, STATE: r SITE SPILL ID:C^-r^ff /4< ^cn^i5ny

^/Y^tf-f^ (̂ >

;PA Form 2075-B

PA Form 207S-9 («-e7)\WHITE— SMO COPY PINK — CUENT COPY WHITE — LAB COPY FOR RETURN TO We; YELLOW — LAB COPY



REGION 6First International BIdg.. 1201 Elm St.

_____Dallas. Texas 75270PROJ. NO.

TFA-»<PROJECT NAME

rWlBSAMPLERS: (SifMtufI

&{/ Q^yyt^MSTA.NO. DATE TIME STATION LOCATION

NO.

OF

CON-TAINERS

REMARKS

Of SV- 01

Ot

Yb-o fe34 \ \

ivoo

U»0

\0 ĴZL^g" St I 0

-&t-WP^ ?L l \ t> -0^341^

II

?< -S -̂i-̂ ^L | ?

IS | v | uso

lol'kf^ I ̂ 00• f l̂B*A /TiBWk^Date/Time Received by: ISigmwnl Relinquished by: (Siginwr») Date / Time Received by: (Siymunf

Relinquished by: (Siyutun) Date /Time Received for Laboratory by:ISignsturu)

Date /Time Remarks

Oittribution: Origin*! AccompAnc* Shipment; Copy to Coordinator Field Files

fl^f ^fl

^^^-J^/•y © o y / 5



REGION 6Firrt International Btdg., 1201 Elm St.

Dallas, Texas 75270PROJECT NAMEPROJ. NO.

tt^ ftopiL^y 5 ^ ^ - 4 -^ îz^asas- uTIME STATION LOCATION«TA. M>. DATE

iS; ••

K $L \b




____ Dallas, Texas 75270PROJECT NAMEPROJ. NO.

|7^̂ rSAMPLERS: ISiyrtyrtI < , r

we^fi C&nn^- ,< k̂(L \)^^k.DATE STATION LOCATION TIMESTA.NO.

Si 2^

NO.

OF

CON-TAINERS

REMARKS

3J-/ -32=

03? !000

Relinquished by: ISigmturvl Date/Time Received by: ISigiuwrfl Relinquished by: (Signaturel Date / Time Received by: tSiyrmura)

/%/^7 I g^Oished by: (SifMtiinl Date/Time Received by: {Siyuwivl Relinquished by: ISignstursi Date /Time Received by: ISigMtun)

Relinquished by: (Sigmtun) Date/Time Received for Laboratory by:(Sigmturfl

Date /Time

Distribution: Originil Accompanit Shipment; Copy to Coordinator Field Files

RemarksM ' l f




Dallas. Texas 75270PROJ. NO.

7^^SAMPLERS: ISHMMf)

to^^ ^^^v^L^jLDATE STATION LOCATION TIMESTA.NO.

NO.

OF

CON-TAINERS

REMARKS

L

//oo /

Relinquished by: (SigmtuM)

^ pi^lelinquishedBy: fSifmwru)

Date/Time Received by: (Sigmturfl Relinquished by: (Signawrfl Date/Time Received by: ISigniturt)

Date/Time Received by: ISigmtunt Relinquished by: (Signature/ Date/Time Received by: ISigmnirfl

Relinquished by: fsismninl Date /Time Received for Laboratory by:fSiyntun)

Date /Time Remarks

Dittribution: Origin*) Accompani— Shipmfnt; Copy to Coordinator Frtd File*




_____Dallas, Texas 75270_____PROJ. NO.

/^^SAMPLERS: ISHMtun)

STA. NO. DATE TIME

NO.

OF

CON-TAINERS

STATION LOCATION

REMARKS




Dallas, Texas 75270PROJ. NO. PROJECT NAME

SAMPLERS: (SUMWMl

^STA. NO. DATE TIME STATION LOCATION

NO.

OF

CON-TAINERS

REMARKS

3^ -n -^Jy^ff^ —~———

^7 W^ ̂

~ _'• f'-t ̂ f f^'v — _=—a70 Wt ,!- Relinquished by: (Signaturs) Date/Time Received by: rSwiur̂

Relinquished by: (Sigfutun) Date/Time Received by: fs^rtur*^ Relinquished by: ISignatursi Date /Time Received by: (Signaturs/

Rel̂ iquished by: (Siyntun) Date/Time Received for Laboratory by:ISianMunI

Date /Time Remarks

Distribution: Original AccompTliM Shipment; Copy to Coordinator Frid File*

PAForm2075-B(a-a7)WHITE — SMO COPY PINK — CLIENT COPY WHITE — LAB COPY FOR RETURN TO SMO YELLOW - LAB COPY



REGION 6First International BIdg.. 1201 Elm St.

_____Dallas, Texas 75270PROJ. NO.

-m' ̂PROJECT NAME

SAMPLERS: fSiyuwnl


NO.

OF

CON-TAINERS

REMARKS

< ̂ /^/: -7^ ^

gL It^-^^y^ 4r. -z.

'̂ /

77 I0 ̂ ̂ W 5L 77 6-Q/^^l: '. / l. •• '•/ -' 4 . ^ -•?6 -^^g-^^" '

,/

R«UfK|ybhed by: (SigMtunI Oaf/Time

/£"/^|^ ^^

Received by: ISurutunt Relinquished by: (Sigmtun) Date / Time Received by: (Sigiwti/nl

Relinquished by: (Sigmtun) Date /Time Received by: lSiy»tur»l Relinquished by: ISignaturfl Date /Time Received by: ISigmunI

Relinquished by: ISigiunin) Date / Time Received for Laboratory by:(Sigmtun)

Date /Time Remarks

Diltribution: Original Accompwiii Shipment; Copy to Coordirrtor Field File*

,...--»• -,"T - ' >1A. Cost Canter:

TS1306

1B. Account No.:TAR0220SAA

TAT ZONE II CONTRACTCONTRACT NO. 68-01-7368

TECHNICAL DIRECTION DOCUMENT (TDD)ECOLOGY AND ENVIRONMENT. INC.

2. No.;T T06-8S09-07

FAmendment

3A. PriorityDHighD MediumD Low

3B. Key EPA Contact:

Name: Haramack

Phone: g55-227C

4A. Estimate ofTo^Hours:

Total Costs:$102,000

4C. Non-dedicatedApproved:

^Rio

5A. EPA Site Name:

Popile, Inc.SB. SSID No.:

N/A

5C. City /County /State:

El Dorado, Union, ARof Funds: Q Other

•CERCLA311UST

7. CERCLIS ID:

ARD0080525088. Completion Date:

5/25/90

8A. Reference Info:'w D Attachedlo D Pick-up

9. Type of Activity:CWA-311 CERCLA AS SPECIFIED ABOVE

SPCCOn-Scene MonitoringSpill Clean-up Funded

sSite AssessmentRemoval FundedRemoval PRP (AO/CO)On-Site Monitoring

Special ProjectAnalytical ProjectPreparednessUSTFEMA

Quality AssuranceTrainingProgram ManagementTechnical AssistanceInformation Management

10. General Task Description:Conduct site assessment at PopilefacillLy in El Durauu, AR. 1 1 . Desired Reportfwn:

^Formal ReportLetter ReportFormal BriefingOther (Specify)

12. Specific Elements:TDD amended to extend completion date.

Original Specific Elements:13. Interim Deadlines:Aaaiat OGC in iaitial viaifc to aifee.

2) Complete standard site assessment.Photodocument site.

Cunduut PRP yudruh.5) Prepare sampling plan, QAPP, and site safety

plan for posslBle sampling.- m

oo00000

6 ) Amended element: Complete field surveying, soil gas suryeynyarogeo logic assessment, ana (-^^ sampling.

Page i of 11TDDI; mfi-ftOOq-Q?

Photographer / WitnessSullivan/HainnackDate / Tiae / Direction9-21-89/1215/NCo—enta: p^ny operations area.

Photographer / WitnessSullivan/HaninackDate / Ti«e / Direction

000884

ofTDD|: T06-8909-07

Photographer / Nitnessîî Yan/Tfatmia îf

Date / Tl»a / DirectionQ-71-ftQ/l 91^/1?

Co—ents: —plant ^aparationa/praeemrav^ggql

Photographer / Nitnesa.̂ il 1 i ua>./n>,nmfl^

Date / Tine / Direction9-21-89/1215/SECQ—entBt Plant operations/flog line

assembly.

000885

"" " . - . « , • . , „ » • * . , , " ' . ' • . - ' • • • "L • ^«, •̂«t, • . . '»î . •'

of 11TDD

Page of _JJ_TDDf; T06-8909-07

Photographer / NitnessSullivan/H«««̂ lrDate / Tine / Direction9-21-flQ/19T;^JU

Co—ents:* Drainage pathway.

Photographer / WitnessSullivan/Hamnack_______Date / TiBC / Direction9-21-89/1215/SCOMentflt Plant operations hank ofdrainage pathway._____________

000888

ofTDDji TOfi-fiqnq-n?

Photographer / WitnessSullivan/HammackDate / Time / Direction9-21-89/1215/SEComments: Drainage pathway.

Photographer / WitnessVoidDate / Tine / Direction

Comments:

000889

of llTDDl; T06-8909-07

Photographer / WitnessSullivan/Tfammfl̂ lf

Date / TIRO / Direction9-21-89/1215/SECo—ents: Drainage area.

Photographer / WitnessSullAvan/Hamnack_______Date / Tl>e / Direction

9-21-89/1215/SCo—entS: Drainage arpfl.

000891

of 11TDD

of 11TDDt; T06-8909-07

Photographer / NitnessSlllli'VflTi/Hi'fflmnrk——————Date / Time / Direction9-21-89/1215/S_________Co—enta: Confluence.

Photographer / WitnessSullivan/Hanmack_______Date / Tim / Direction9-21-89/1215/Do«n_________CO——Cntfi» Sheen on haynn af ^nnflî r̂ o

000893

Photographer / HitnesarcuLd—————————————————Date / Tile / Direction

000894

Page of 16TDDt; T06-8909-07

Photographer / WitnessSullivan/ErfaniDate / Tine / Direction

.N,: •iSr• ^pl'

"''N

^h

1 ti ::

^tt" . t•* f\ ^

i;:?r^1|i' • • " ,^

:.~••' ' ' • .-w'^.'^- ' . ' ' . . '" •

•''"'• ";•., ".••:-'

^. ; 1; '.:

^M&fe-l.' —; .:

f /- lO-Ti- /̂l̂ /N"

^ COBBentS: planf, ppor-al-i/wia/Drainage/

i J; ; Closed impoundments. ; : . :. • : ^ l, i^| is; :'; • . • • i . ' ' . . . . ' '"^. '̂..,. . . .1 ...: • .' • . - : ; '•• ^ :.^'.^:;••

' ^ ' . • . ' : ' • ; ' • ; • ,'" i,' ?• ;• ^'s',.^.

• : ' . • • • • ; : ' : . . . ' . , '^s' ;:^•

fc.,..tf^>^.-,i,v,,4-.Nl.,^tfe^^,^^ •..,.———— ^' • • • ' . .; ,::̂ :;:]M:;:it—————————.^.i—————:. •' ?J^ • ; - . - • ----^--—^.;.^.!-,^--.-^^-^aikliait^^

^ - .' '.. . ' • • • ; 1

; •;

• .

.

: .

^•iM^

Page _^__ of ^TDDt t T06-8909-07

Photographer / WitnessSullivan/ErfaniDate / TiBe / Direction

10-15-89/1600/WCo—enta: Plant operations/drying track.

Sample 01.

Photographer / WitnesaSullivan/ErfaniDate / Tim / Direction

l(M5-89/16nn/WCO——CntS ; Plant: npP.raHnna/pt-aea.̂ o

VM^I. sampio n? m rv,

000896

Page _3__ of 16TDD|; TO6-8909-07

Photographer / WitnessSullivan/ErfaniDate / Ti«e / Direction10-15-89/1600/NCO——entS: Plani- np»fafinnQ/.».1x^

assembly. Sample 05.

Photographer / WitnessSullivan/ErfaniDate / TiBe / Direction10-15-89/1600/WCo—ents s Plant operations /floy ),\^Qassembly. Sample 06.

000897

Page of 16TDD|; T06-8909-07

Photographer / WitnessSullivan/ErfaniDate / Tine / Direction10-15-89/1600/NECo—enta: Plant operations/upright tank.

Sample 07. 10.

Photographer / WitnessSullivan/Erfani_________Date / TiBe / Direction

10-15-fiQ/ifinn/sRCo—enta; plant- nppr-a«-î a/o.^fa^

unpnimflinpnt-—Sanpla 08, 09, 13.

000898

of 16TDD|; T06-8909-07

Photographer / WitnessSullivan/Erfani_________Date / Tiae / Directionin-is-ftQ/ifinn/R_______Co—enta: plant operationa/sucfacaiiqpoundnent. Saq)le 11, 13.______

Photographer / WitnessSullivan/ErfaniDate / Tim / Direction10-15-89/1600/E________Co—entfl; Plant operations/sump. Sample15.

000899

of 16TDD|; T06-8909-07

Photographer / NitnesaSullivan/Hannack_______Date / Tim / Directionin-Ti-ftq/lffyVSK________________

CO——entS; Plant- »pQ^ ,̂»^ 0,̂ 1 ^ ]/,

Photographer / HitneasSill 1

of 16TDDJ t T06-8909-07

Photographer / NitnesaSullivan/Erf ani

Date / Tiae /10-15-89/1600/SW

Direction

Co—enta: Drainage pathway/plantoperations bank. Sample 17.

Photographer / WitnessSullivan/Erfani

Date / Ti»e /10-15-89/1600/SW

Direction

. Co—ents: Drainage pathway.

000901

of 16TDD|; T06-8909-07

Photographer / WitnessSullivan/Erf ani

Date / Tiae / Direction10-15-89/1600/NWCo—enta: Drainaaa pathway,

Photographer / NitneaaSiini'van/ffirfanADate / TiBe / Direction

10-15-89/1600/SECo—entfl; Drainage pathway.

000902

Page _J__ of 16TDDf j T06-8909-07

Photographer / WitnessSullivan/ErfanA_________Date / TiMe / Directionin-i^ftQ/i^nn/M^_______Co—enta: Grid line.____

Photographer / WitnessSullivan/Erfani________Date / Time / Direction10-15-89/1600/NW________Co—ents: Grid line.

000903

of 16TDD|; 106-8909-07

Photographer / WitnessSullivan/ErfaniDate / Tiae / Direction

10-15-89/lffln/NWCo—ents: Grid Imp.


Date / Tiae / Direction10-15-89/1600/NWCo—ents: Grid line.

000904

of 16TDD| t T06-8909-07

Photographer / WitnessSulllvan/Erfani________Date / Ti«e / DirectionlQ-T?-fl9/16nn/NE________Co—ents:

Photographer / WitnesaSullivan/ErfaniDate / TiBe / Direction

10-15-89/1600/NW________Co—entSi Confluence.

000905

of 16TDDj; T06-8909-07

Photographer / WitnessSulllvan/ErfanADate / Tiae / Direction10-15-89/1 fflO/nngnco—ents: nr̂ Tv.g» »^»

Photographer / HitneasSullivan/ErfaniDate / TiBe / Direction

10-15-89/1600/Down_______Co—ents t Drainage area.

000906

of 16TDDj; T06-8909-07

Photographer / WitnessSullivan/ErfaniDate / Time / Direction10-15-89/1600/DownCo—enta: Drainage area.

Photographer / WitnessSullivan/ErfaniDate / Tixe / Direction

10-15-89/1600/ECo—entS; Area north nf pina^

^"iPfflinfliipnrH

000907

of 16TDDj;. T06-8909-07


Date / Tiae / Directionlo-Ti-ftq/î nn/M

Co—ents; Arfta north of G.R.I,&P.railroai.

Photographer / WitnessSullivan/ErfaniDate / Tim / Direction10-15-89/1600/NWCo—ent8: Confluence.

000908

of i6TDDj t T06-8909-07

Photographer / NitnesaSullivan/Erfani________Date / Tine / Directionin-n-flq/î /pMmCo—enta: Point discharge into Bayou deLoutre.

Photographer / HitneaaSullivan/ErfaniDate / TiBa / Direction

10-15-89/1600/NCO——entfi: Bavou dawnstrAam.

000909

Of 16TDDj: TQ6-8QQQ-n7


Date / TiBe / Direction10-14-89/0900/NW________

Co—enta: TAT member bailing well ^.Sample 73.

Photographer / WitnessSullivan/ErfaniDate / Tiae / Direction10-15-89/16QO/.̂ JCo—ents l Veil tf3.

000910

MEMORANDUM TO PTUi

EPA ID NUMBER: /̂ P 0^ ^ O^^O^

SITE NAME: ^Q^/ /^ . ^T^c .

FILE REOPENED TO CONDUCT EXPANDED SITE INSPECTION ON2/15/91.

^^ ̂ ^X 3/2 3 h INAME DATE

ATTACHMENT A: ANALYSIS FOR POLYCHLORINATED DIOXINS AND FURANSATTACHMENT B: PREPARATION AND ANALYSIS PROTOCAL FOR OILY SOIL / SEDIMENT SAMPLES METALS

epa project no.: ard008052508 contractor work order ...sampling qa/qc plan popile inc. site...

Documents