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  • ENTERED - Welcome to NewMexico.gov Refinery - Gallup...2012/05/17  · SampType: MSD TestCode: EPA Method 300.0: Anions Bromide 1.6 0.10 2.500 0 65.3 76 114 3.44 20 S Sulfate 38 0.50
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From: To: Cc: Subject: Date: Attachments: Dear Kristen, Larsen. Thurman VanHorn. Kristen. NMENV ENTERED Chavez. Carl J. EMNRD; Cobrajn. Dave. NMENV MPPE INmAL TEST RESULTS (5/8, 5/10, 5/11, 5/12, 5/13, 5/14) Thursday, May 17, 2012 11:46:38 AM Rot 1205459 vl.pdf Rot 1205563 vl.pdf Rpt 1205562 vl.pdf Rpt 1205591 vl.pdf Rpt 1205595 vl.pdf Rpt 1205592 vl.pdf The MPPE began sending effluent wastewater to STP-1 at or about 1500 hrs on May 8, 2012. In accordance with Comment 17 a, Western will be initially required to collect daily effluent samples to submit to Hall Environmental Laboratories. The laboratory results and flow measurements will be submitted via e-mail to both NMED and OCD as prescribed in accordance with Comment 17 f. Effluent sample collection for MPPE wastewater going to STP-1 began on the evening of May 8. The initial results of the analysis were recently received for May 8, 10, 11, 12, 13, and 14. The May 9 sample results will not be used because it was learned that the sample bottle was previously used and contained a hydrochloric acid preservative. Western plans to collect one additional day of samples in order to meet the 15 day sampling requirement. Regards, Beck Larsen

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  • From: To: Cc: Subject: Date: Attachments:

    Dear Kristen,

    Larsen. Thurman VanHorn. Kristen. NMENV

    Jc~ ENTERED

    Chavez. Carl J. EMNRD; ~; Cobrajn. Dave. NMENV MPPE INmAL TEST RESULTS (5/8, 5/10, 5/11, 5/12, 5/13, 5/14) Thursday, May 17, 2012 11:46:38 AM Rot 1205459 vl.pdf Rot 1205563 vl.pdf Rpt 1205562 vl.pdf Rpt 1205591 vl.pdf Rpt 1205595 vl.pdf Rpt 1205592 vl.pdf

    The MPPE began sending effluent wastewater to STP-1 at or about 1500 hrs on May 8, 2012. In

    accordance with Comment 17 a, Western will be initially required to collect daily effluent samples to

    submit to Hall Environmental Laboratories. The laboratory results and flow measurements will be

    submitted via e-mail to both NMED and OCD as prescribed in accordance with Comment 17 f.

    Effluent sample collection for MPPE wastewater going to STP-1 began on the evening of May 8. The

    initial results of the analysis were recently received for May 8, 10, 11, 12, 13, and 14. The May 9

    sample results will not be used because it was learned that the sample bottle was previously used

    and contained a hydrochloric acid preservative. Western plans to collect one additional day of

    samples in order to meet the 15 day sampling requirement.

    Regards,

    Beck Larsen

  • May 17, 2012

    Western Refining Southwest, GallupThurman B. Larsen

    Dear Thurman B. Larsen:

    RE: MPPE-1 OrderNo.: 1205459

    FAX (505) 722-0210TEL: (505) 722-3833

    Rt. 3 Box 7Gallup, NM 87301

    Hall Environmental Analysis Laboratory4901 Hawkins NE

    Albuquerque, NM 87109

    Website: www.hallenvironmental.comTEL: 505-345-3975 FAX: 505-345-4107

    Hall Environmental Analysis Laboratory received 1 sample(s) on 5/10/2012 for the analyses presented in the following report.

    Andy Freeman

    These were analyzed according to EPA procedures or equivalent. To access our accredited tests please go to www.hallenvironmental.com or the state specific web sites. See the sample checklist and/or the Chain of Custody for information regarding the sample receipt temperature and preservation. Data qualifiers or a narrative will be provided if the sample analysis or analytical quality control parameters require a flag. All samples are reported as received unless otherwise indicated.

    Please don't hesitate to contact HEAL for any additional information or clarifications.

    Sincerely,

    Laboratory Manager4901 Hawkins NEAlbuquerque, NM 87109

    http://www.hallenvironmental.comhttp://www.hallenvironmental.com

  • Project: MPPE-1Client Sample ID: MPPE-1

    Collection Date: 5/8/2012 5:00:00 PMMatrix: AQUEOUS

    CLIENT: Western Refining Southwest, Gallup

    Lab ID: 1205459-001

    Date Reported: 5/17/2012

    Analytical ReportLab Order 1205459

    Analyses Result Qual Units Date AnalyzedDFRL

    Hall Environmental Analysis Laboratory, Inc.

    Received Date: 5/10/2012 8:00:00 AM

    EPA METHOD 8015B: DIESEL RANGE Analyst: JMPDiesel Range Organics (DRO) 5/10/2012 4:22:31 PM1.0 mg/L 110Motor Oil Range Organics (MRO) 5/10/2012 4:22:31 PM5.0 mg/L 116 Surr: DNOP 5/10/2012 4:22:31 PM61.3-164 %REC 1120

    EPA METHOD 8015B: GASOLINE RANGE Analyst: NSBGasoline Range Organics (GRO) 5/10/2012 11:43:43 AM0.25 mg/L 50.42 Surr: BFB 5/10/2012 11:43:43 AM69.3-120 %REC 5102

    EPA METHOD 8021B: VOLATILES Analyst: NSBMethyl tert-butyl ether (MTBE) 5/10/2012 11:43:43 AM12 µg/L 5NDBenzene 5/10/2012 11:43:43 AM5.0 µg/L 5NDToluene 5/10/2012 11:43:43 AM5.0 µg/L 5NDEthylbenzene 5/10/2012 11:43:43 AM5.0 µg/L 5NDXylenes, Total 5/10/2012 11:43:43 AM10 µg/L 5ND Surr: 4-Bromofluorobenzene 5/10/2012 11:43:43 AM55-140 %REC 592.5

    EPA METHOD 300.0: ANIONS Analyst: BRMFluoride * 5/11/2012 11:41:36 AM2.0 mg/L 2060Chloride 5/10/2012 10:40:46 PM25 mg/L 50430Nitrogen, Nitrite (As N) 5/10/2012 1:09:46 PM0.10 mg/L 1NDBromide 5/10/2012 1:09:46 PM0.10 mg/L 10.48Nitrogen, Nitrate (As N) 5/10/2012 1:09:46 PM0.10 mg/L 10.49Phosphorus, Orthophosphate (As P) 5/10/2012 1:09:46 PM0.50 mg/L 10.71Sulfate 5/10/2012 1:22:11 PM10 mg/L 20800

    EPA METHOD 200.7: METALS Analyst: ELSCalcium 5/14/2012 8:20:36 AM1.0 mg/L 187Magnesium 5/14/2012 8:20:36 AM1.0 mg/L 121Potassium 5/14/2012 8:20:36 AM1.0 mg/L 162Sodium 5/14/2012 8:28:31 AM5.0 mg/L 5500

    EPA 120.1: SPECIFIC CONDUCTANCE Analyst: DBDConductivity 5/10/2012 1:02:28 PM0.010 µmhos/cm 14,200

    SM4500-H+B: PH Analyst: DBDpH H 5/10/2012 1:02:28 PM1.68 pH units 18.42

    Qualifiers:

    Page 1 of 9

    */X Value exceeds Maximum Contaminant Level. B Analyte detected in the associated Method BlankE Value above quantitation range H Holding times for preparation or analysis exceededJ Analyte detected below quantitation limits ND Not Detected at the Reporting LimitR RPD outside accepted recovery limits RL Reporting Detection LimitS Spike Recovery outside accepted recovery limits

  • Project: MPPE-1Client: Western Refining Southwest, Gallup

    17-May-12

    QC SUMMARY REPORT 1205459WO#:Hall Environmental Analysis Laboratory, Inc.

    Sample ID MB-1899

    Batch ID: 1899

    Analysis Date: 5/14/2012Prep Date: 5/11/2012

    Analyte Result SPK value SPK Ref Val %REC %RPDLowLimit HighLimit RPDLimit Qual

    Units: mg/L

    PQL

    Client ID: PBW RunNo: 2742

    SeqNo: 76144

    MBLKSampType: TestCode: EPA Method 200.7: Metals

    Calcium 1.0NDMagnesium 1.0NDPotassium 1.0NDSodium 1.0ND

    Sample ID LCS-1899

    Batch ID: 1899

    Analysis Date: 5/14/2012Prep Date: 5/11/2012

    Analyte Result SPK value SPK Ref Val %REC %RPDLowLimit HighLimit RPDLimit Qual

    Units: mg/L

    PQL

    Client ID: LCSW RunNo: 2742

    SeqNo: 76145

    LCSSampType: TestCode: EPA Method 200.7: Metals

    Calcium 50.00 100 85 1151.0 050Magnesium 50.00 99.5 85 1151.0 050Potassium 50.00 95.4 85 1151.0 048Sodium 50.00 97.4 85 1151.0 049

    Qualifiers:

    Page 2 of 9

    */X Value exceeds Maximum Contaminant Level. B Analyte detected in the associated Method BlankE Value above quantitation range H Holding times for preparation or analysis exceededJ Analyte detected below quantitation limits ND Not Detected at the Reporting LimitR RPD outside accepted recovery limits RL Reporting Detection Limit

  • Project: MPPE-1Client: Western Refining Southwest, Gallup

    17-May-12

    QC SUMMARY REPORT 1205459WO#:Hall Environmental Analysis Laboratory, Inc.

    Sample ID MB

    Batch ID: R2702

    Analysis Date: 5/10/2012Prep Date:

    Analyte Result SPK value SPK Ref Val %REC %RPDLowLimit HighLimit RPDLimit Qual

    Units: mg/L

    PQL

    Client ID: PBW RunNo: 2702

    SeqNo: 75161

    MBLKSampType: TestCode: EPA Method 300.0: Anions

    Chloride 0.50NDNitrogen, Nitrite (As N) 0.10NDBromide 0.10NDNitrogen, Nitrate (As N) 0.10NDPhosphorus, Orthophosphate (As P 0.50NDSulfate 0.50ND

    Sample ID LCS

    Batch ID: R2702

    Analysis Date: 5/10/2012Prep Date:

    Analyte Result SPK value SPK Ref Val %REC %RPDLowLimit HighLimit RPDLimit Qual

    Units: mg/L

    PQL

    Client ID: LCSW RunNo: 2702

    SeqNo: 75162

    LCSSampType: TestCode: EPA Method 300.0: Anions

    Chloride 5.000 94.1 90 1100.50 04.7Nitrogen, Nitrite (As N) 1.000 94.1 90 1100.10 00.94Bromide 2.500 95.9 90 1100.10 02.4Nitrogen, Nitrate (As N) 2.500 98.0 90 1100.10 02.5Phosphorus, Orthophosphate (As P 5.000 98.5 90 1100.50 04.9Sulfate 10.00 94.7 90 1100.50 09.5

    Sample ID 1205476-001BMS

    Batch ID: R2702

    Analysis Date: 5/10/2012Prep Date:

    Analyte Result SPK value SPK Ref Val %REC %RPDLowLimit HighLimit RPDLimit Qual

    Units: mg/L

    PQL

    Client ID: BatchQC RunNo: 2702

    SeqNo: 75166

    MSSampType: TestCode: EPA Method 300.0: Anions

    Bromide 2.500 63.1 76 114 S0.10 01.6Sulfate 10.00 101 80.5 1190.50 27.2237

    Sample ID 1205476-001BMSD

    Batch ID: R2702

    Analysis Date: 5/10/2012Prep Date:

    Analyte Result SPK value SPK Ref Val %REC %RPDLowLimit HighLimit RPDLimit Qual

    Units: mg/L

    PQL

    Client ID: BatchQC RunNo: 2702

    SeqNo: 75167

    MSDSampType: TestCode: EPA Method 300.0: Anions

    Bromide 2.500 65.3 76 114 20 S0.10 0 3.441.6Sulfate 10.00 103 80.5 119 200.50 27.22 0.61638

    Sample ID MB

    Batch ID: R2739

    Analysis Date: 5/11/2012Prep Date:

    Analyte Result SPK value SPK Ref Val %REC %RPDLowLimit HighLimit RPDLimit Qual

    Units: mg/L

    PQL

    Client ID: PBW RunNo: 2739

    SeqNo: 76007

    MBLKSampType: TestCode: EPA Method 300.0: Anions

    Fluoride 0.10ND

    Qualifiers:

    Page 3 of 9

    */X Value exceeds Maximum Contaminant Level. B Analyte detected in the associated Method BlankE Value above quantitation range H Holding times for preparation or analysis exceededJ Analyte detected below quantitation limits ND Not Detected at the Reporting LimitR RPD outside accepted recovery limits RL Reporting Detection Limit

  • Project: MPPE-1Client: Western Refining Southwest, Gallup

    17-May-12

    QC SUMMARY REPORT 1205459WO#:Hall Environmental Analysis Laboratory, Inc.

    Sample ID LCS

    Batch ID: R2739

    Analysis Date: 5/11/2012Prep Date:

    Analyte Result SPK value SPK Ref Val %REC %RPDLowLimit HighLimit RPDLimit Qual

    Units: mg/L

    PQL

    Client ID: LCSW RunNo: 2739

    SeqNo: 76008

    LCSSampType: TestCode: EPA Method 300.0: Anions

    Fluoride 0.5000 97.8 90 1100.10 00.49

    Sample ID 1205508-001BMS

    Batch ID: R2739

    Analysis Date: 5/11/2012Prep Date:

    Analyte Result SPK value SPK Ref Val %REC %RPDLowLimit HighLimit RPDLimit Qual

    Units: mg/L

    PQL

    Client ID: BatchQC RunNo: 2739

    SeqNo: 76012

    MSSampType: TestCode: EPA Method 300.0: Anions

    Fluoride 0.5000 105 72.9 1130.10 00.52

    Sample ID 1205508-001BMSD

    Batch ID: R2739

    Analysis Date: 5/11/2012Prep Date:

    Analyte Result SPK value SPK Ref Val %REC %RPDLowLimit HighLimit RPDLimit Qual

    Units: mg/L

    PQL

    Client ID: BatchQC RunNo: 2739

    SeqNo: 76013

    MSDSampType: TestCode: EPA Method 300.0: Anions

    Fluoride 0.5000 102 72.9 113 200.10 0 2.820.51

    Sample ID MB

    Batch ID: R2739

    Analysis Date: 5/11/2012Prep Date:

    Analyte Result SPK value SPK Ref Val %REC %RPDLowLimit HighLimit RPDLimit Qual

    Units: mg/L

    PQL

    Client ID: PBW RunNo: 2739

    SeqNo: 76061

    MBLKSampType: TestCode: EPA Method 300.0: Anions

    Fluoride 0.10ND

    Sample ID LCS

    Batch ID: R2739

    Analysis Date: 5/11/2012Prep Date:

    Analyte Result SPK value SPK Ref Val %REC %RPDLowLimit HighLimit RPDLimit Qual

    Units: mg/L

    PQL

    Client ID: LCSW RunNo: 2739

    SeqNo: 76062

    LCSSampType: TestCode: EPA Method 300.0: Anions

    Fluoride 0.5000 104 90 1100.10 00.52

    Sample ID 1205524-001AMS

    Batch ID: R2739

    Analysis Date: 5/11/2012Prep Date:

    Analyte Result SPK value SPK Ref Val %REC %RPDLowLimit HighLimit RPDLimit Qual

    Units: mg/L

    PQL

    Client ID: BatchQC RunNo: 2739

    SeqNo: 76068

    MSSampType: TestCode: EPA Method 300.0: Anions

    Fluoride 0.5000 95.0 72.9 1130.10 0.53671.0

    Sample ID 1205524-001AMSD

    Batch ID: R2739

    Analysis Date: 5/12/2012Prep Date:

    Analyte Result SPK value SPK Ref Val %REC %RPDLowLimit HighLimit RPDLimit Qual

    Units: mg/L

    PQL

    Client ID: BatchQC RunNo: 2739

    SeqNo: 76069

    MSDSampType: TestCode: EPA Method 300.0: Anions

    Fluoride 0.5000 94.4 72.9 113 200.10 0.5367 0.3011.0

    Qualifiers:

    Page 4 of 9

    */X Value exceeds Maximum Contaminant Level. B Analyte detected in the associated Method BlankE Value above quantitation range H Holding times for preparation or analysis exceededJ Analyte detected below quantitation limits ND Not Detected at the Reporting LimitR RPD outside accepted recovery limits RL Reporting Detection Limit

  • Project: MPPE-1Client: Western Refining Southwest, Gallup

    17-May-12

    QC SUMMARY REPORT 1205459WO#:Hall Environmental Analysis Laboratory, Inc.

    Sample ID MB-1882

    Batch ID: 1882

    Analysis Date: 5/10/2012Prep Date: 5/10/2012

    Analyte Result SPK value SPK Ref Val %REC %RPDLowLimit HighLimit RPDLimit Qual

    Units: mg/L

    PQL

    Client ID: PBW RunNo: 2674

    SeqNo: 75054

    MBLKSampType: TestCode: EPA Method 8015B: Diesel Range

    Diesel Range Organics (DRO) 1.0NDMotor Oil Range Organics (MRO) 5.0ND Surr: DNOP 1.000 116 61.3 1641.2

    Sample ID LCS-1882

    Batch ID: 1882

    Analysis Date: 5/10/2012Prep Date: 5/10/2012

    Analyte Result SPK value SPK Ref Val %REC %RPDLowLimit HighLimit RPDLimit Qual

    Units: mg/L

    PQL

    Client ID: LCSW RunNo: 2674

    SeqNo: 75055

    LCSSampType: TestCode: EPA Method 8015B: Diesel Range

    Diesel Range Organics (DRO) 5.000 93.5 74 1571.0 04.7 Surr: DNOP 0.5000 108 61.3 1640.54

    Sample ID LCSD-1882

    Batch ID: 1882

    Analysis Date: 5/10/2012Prep Date: 5/10/2012

    Analyte Result SPK value SPK Ref Val %REC %RPDLowLimit HighLimit RPDLimit Qual

    Units: mg/L

    PQL

    Client ID: LCSS02 RunNo: 2674

    SeqNo: 75056

    LCSDSampType: TestCode: EPA Method 8015B: Diesel Range

    Diesel Range Organics (DRO) 5.000 96.9 74 157 231.0 0 3.584.8 Surr: DNOP 0.5000 113 61.3 164 000.57

    Qualifiers:

    Page 5 of 9

    */X Value exceeds Maximum Contaminant Level. B Analyte detected in the associated Method BlankE Value above quantitation range H Holding times for preparation or analysis exceededJ Analyte detected below quantitation limits ND Not Detected at the Reporting LimitR RPD outside accepted recovery limits RL Reporting Detection Limit

  • Project: MPPE-1Client: Western Refining Southwest, Gallup

    17-May-12

    QC SUMMARY REPORT 1205459WO#:Hall Environmental Analysis Laboratory, Inc.

    Sample ID 5ML RB

    Batch ID: R2706

    Analysis Date: 5/10/2012Prep Date:

    Analyte Result SPK value SPK Ref Val %REC %RPDLowLimit HighLimit RPDLimit Qual

    Units: mg/L

    PQL

    Client ID: PBW RunNo: 2706

    SeqNo: 75305

    MBLKSampType: TestCode: EPA Method 8015B: Gasoline Range

    Gasoline Range Organics (GRO) 0.050ND Surr: BFB 20.00 103 69.3 12021

    Sample ID 2.5UG GRO LCS

    Batch ID: R2706

    Analysis Date: 5/10/2012Prep Date:

    Analyte Result SPK value SPK Ref Val %REC %RPDLowLimit HighLimit RPDLimit Qual

    Units: mg/L

    PQL

    Client ID: LCSW RunNo: 2706

    SeqNo: 75306

    LCSSampType: TestCode: EPA Method 8015B: Gasoline Range

    Gasoline Range Organics (GRO) 0.5000 95.2 101 123 S0.050 00.48 Surr: BFB 20.00 110 69.3 12022

    Sample ID 1205459-001AMS

    Batch ID: R2706

    Analysis Date: 5/10/2012Prep Date:

    Analyte Result SPK value SPK Ref Val %REC %RPDLowLimit HighLimit RPDLimit Qual

    Units: mg/L

    PQL

    Client ID: MPPE-1 RunNo: 2706

    SeqNo: 75308

    MSSampType: TestCode: EPA Method 8015B: Gasoline Range

    Gasoline Range Organics (GRO) 2.500 103 75.4 1210.25 0.42003.0 Surr: BFB 100.0 112 69.3 120110

    Sample ID 1205459-001AMSD

    Batch ID: R2706

    Analysis Date: 5/10/2012Prep Date:

    Analyte Result SPK value SPK Ref Val %REC %RPDLowLimit HighLimit RPDLimit Qual

    Units: mg/L

    PQL

    Client ID: MPPE-1 RunNo: 2706

    SeqNo: 75309

    MSDSampType: TestCode: EPA Method 8015B: Gasoline Range

    Gasoline Range Organics (GRO) 2.500 92.0 75.4 121 10.50.25 0.4200 9.522.7 Surr: BFB 100.0 111 69.3 120 00110

    Qualifiers:

    Page 6 of 9

    */X Value exceeds Maximum Contaminant Level. B Analyte detected in the associated Method BlankE Value above quantitation range H Holding times for preparation or analysis exceededJ Analyte detected below quantitation limits ND Not Detected at the Reporting LimitR RPD outside accepted recovery limits RL Reporting Detection Limit

  • Project: MPPE-1Client: Western Refining Southwest, Gallup

    17-May-12

    QC SUMMARY REPORT 1205459WO#:Hall Environmental Analysis Laboratory, Inc.

    Sample ID 5ML RB

    Batch ID: R2706

    Analysis Date: 5/10/2012Prep Date:

    Analyte Result SPK value SPK Ref Val %REC %RPDLowLimit HighLimit RPDLimit Qual

    Units: µg/L

    PQL

    Client ID: PBW RunNo: 2706

    SeqNo: 75366

    MBLKSampType: TestCode: EPA Method 8021B: Volatiles

    Methyl tert-butyl ether (MTBE) 2.5NDBenzene 1.0NDToluene 1.0NDEthylbenzene 1.0NDXylenes, Total 2.0ND Surr: 4-Bromofluorobenzene 20.00 91.9 55 14018

    Sample ID 100NG BTEX LCS

    Batch ID: R2706

    Analysis Date: 5/10/2012Prep Date:

    Analyte Result SPK value SPK Ref Val %REC %RPDLowLimit HighLimit RPDLimit Qual

    Units: µg/L

    PQL

    Client ID: LCSW RunNo: 2706

    SeqNo: 75367

    LCSSampType: TestCode: EPA Method 8021B: Volatiles

    Methyl tert-butyl ether (MTBE) 20.00 94.3 50.5 1582.5 019Benzene 20.00 93.5 80 1201.0 019Toluene 20.00 96.2 80 1201.0 019Ethylbenzene 20.00 93.1 80 1201.0 019Xylenes, Total 60.00 92.3 80 1202.0 055 Surr: 4-Bromofluorobenzene 20.00 96.3 55 14019

    Sample ID 1205459-001AMS

    Batch ID: R2706

    Analysis Date: 5/10/2012Prep Date:

    Analyte Result SPK value SPK Ref Val %REC %RPDLowLimit HighLimit RPDLimit Qual

    Units: µg/L

    PQL

    Client ID: MPPE-1 RunNo: 2706

    SeqNo: 75369

    MSSampType: TestCode: EPA Method 8021B: Volatiles

    Methyl tert-butyl ether (MTBE) 100.0 102 58 13912 1.445100Benzene 100.0 95.9 70.1 1185.0 096Toluene 100.0 99.5 72.3 1175.0 0100Ethylbenzene 100.0 91.9 73.5 1175.0 0.597092Xylenes, Total 300.0 93.5 73.1 11910 3.165280 Surr: 4-Bromofluorobenzene 100.0 95.6 55 14096

    Sample ID 1205459-001AMSD

    Batch ID: R2706

    Analysis Date: 5/10/2012Prep Date:

    Analyte Result SPK value SPK Ref Val %REC %RPDLowLimit HighLimit RPDLimit Qual

    Units: µg/L

    PQL

    Client ID: MPPE-1 RunNo: 2706

    SeqNo: 75370

    MSDSampType: TestCode: EPA Method 8021B: Volatiles

    Methyl tert-butyl ether (MTBE) 100.0 99.3 58 139 15.212 1.445 2.35100Benzene 100.0 86.0 70.1 118 16.45.0 0 10.886Toluene 100.0 88.9 72.3 117 13.95.0 0 11.389Ethylbenzene 100.0 83.7 73.5 117 13.55.0 0.5970 9.2284Xylenes, Total 300.0 82.8 73.1 119 12.910 3.165 12.0250 Surr: 4-Bromofluorobenzene 100.0 97.1 55 140 0097

    Qualifiers:

    Page 7 of 9

    */X Value exceeds Maximum Contaminant Level. B Analyte detected in the associated Method BlankE Value above quantitation range H Holding times for preparation or analysis exceededJ Analyte detected below quantitation limits ND Not Detected at the Reporting LimitR RPD outside accepted recovery limits RL Reporting Detection Limit

  • Project: MPPE-1Client: Western Refining Southwest, Gallup

    17-May-12

    QC SUMMARY REPORT 1205459WO#:Hall Environmental Analysis Laboratory, Inc.

    Sample ID 1205459-001BDUP

    Batch ID: R2699

    Analysis Date: 5/10/2012Prep Date:

    Analyte Result SPK value SPK Ref Val %REC %RPDLowLimit HighLimit RPDLimit Qual

    Units: µmhos/cm

    PQL

    Client ID: MPPE-1 RunNo: 2699

    SeqNo: 75151

    DUPSampType: TestCode: EPA 120.1: Specific Conductance

    Conductivity 200.010 0.3084,200

    Qualifiers:

    Page 8 of 9

    */X Value exceeds Maximum Contaminant Level. B Analyte detected in the associated Method BlankE Value above quantitation range H Holding times for preparation or analysis exceededJ Analyte detected below quantitation limits ND Not Detected at the Reporting LimitR RPD outside accepted recovery limits RL Reporting Detection Limit

  • Project: MPPE-1Client: Western Refining Southwest, Gallup

    17-May-12

    QC SUMMARY REPORT 1205459WO#:Hall Environmental Analysis Laboratory, Inc.

    Sample ID 1205459-001BDUP

    Batch ID: R2699

    Analysis Date: 5/10/2012Prep Date:

    Analyte Result SPK value SPK Ref Val %REC %RPDLowLimit HighLimit RPDLimit Qual

    Units: pH units

    PQL

    Client ID: MPPE-1 RunNo: 2699

    SeqNo: 75108

    DUPSampType: TestCode: SM4500-H+B: pH

    pH H1.688.44

    Qualifiers:

    Page 9 of 9

    */X Value exceeds Maximum Contaminant Level. B Analyte detected in the associated Method BlankE Value above quantitation range H Holding times for preparation or analysis exceededJ Analyte detected below quantitation limits ND Not Detected at the Reporting LimitR RPD outside accepted recovery limits RL Reporting Detection Limit

  • May 17, 2012

    Western Refining Southwest, GallupBeck Larsen

    Dear Beck Larsen:

    RE: MPPE-4 OrderNo.: 1205562

    FAX (505) 722-0210TEL: (505) 722-0258

    Rt. 3 Box 7Gallup, NM 87301

    Hall Environmental Analysis Laboratory4901 Hawkins NE

    Albuquerque, NM 87109

    Website: www.hallenvironmental.comTEL: 505-345-3975 FAX: 505-345-4107

    Hall Environmental Analysis Laboratory received 1 sample(s) on 5/12/2012 for the analyses presented in the following report.

    Andy Freeman

    These were analyzed according to EPA procedures or equivalent. To access our accredited tests please go to www.hallenvironmental.com or the state specific web sites. See the sample checklist and/or the Chain of Custody for information regarding the sample receipt temperature and preservation. Data qualifiers or a narrative will be provided if the sample analysis or analytical quality control parameters require a flag. All samples are reported as received unless otherwise indicated.

    Please don't hesitate to contact HEAL for any additional information or clarifications.

    Sincerely,

    Laboratory Manager4901 Hawkins NEAlbuquerque, NM 87109

    http://www.hallenvironmental.comhttp://www.hallenvironmental.com

  • Project: MPPE-4Client Sample ID: MPPE-4

    Collection Date: 5/11/2012 3:55:00 PMMatrix: AQUEOUS

    CLIENT: Western Refining Southwest, Gallup

    Lab ID: 1205562-001

    Date Reported: 5/17/2012

    Analytical ReportLab Order 1205562

    Analyses Result Qual Units Date AnalyzedDFRL

    Hall Environmental Analysis Laboratory, Inc.

    Received Date: 5/12/2012 11:30:00 AM

    EPA METHOD 8015B: DIESEL RANGE Analyst: JMPDiesel Range Organics (DRO) 5/15/2012 9:44:42 AM1.0 mg/L 17.1 Surr: DNOP 5/15/2012 9:44:42 AM61.3-164 %REC 1125

    EPA METHOD 8021B: VOLATILES Analyst: NSBMethyl tert-butyl ether (MTBE) 5/15/2012 12:35:23 AM12 µg/L 5NDBenzene 5/15/2012 1:42:28 PM5.0 µg/L 5NDToluene 5/15/2012 1:42:28 PM5.0 µg/L 5NDEthylbenzene 5/15/2012 1:42:28 PM5.0 µg/L 5NDXylenes, Total 5/15/2012 1:42:28 PM10 µg/L 5ND1,2,4-Trimethylbenzene 5/15/2012 1:42:28 PM5.0 µg/L 5ND1,3,5-Trimethylbenzene 5/15/2012 1:42:28 PM5.0 µg/L 5ND Surr: 4-Bromofluorobenzene 5/15/2012 1:42:28 PM55-140 %REC 597.3

    EPA METHOD 300.0: ANIONS Analyst: SRMFluoride * 5/15/2012 2:19:31 PM5.0 mg/L 5080Chloride 5/16/2012 12:02:52 AM50 mg/L 100960Phosphorus, Orthophosphate (As P) H 5/14/2012 3:11:55 PM2.5 mg/L 5NDSulfate 5/15/2012 2:19:31 PM25 mg/L 50870Nitrate+Nitrite as N 5/14/2012 5:37:53 PM1.0 mg/L 5ND

    EPA METHOD 200.7: METALS Analyst: ELSCalcium 5/16/2012 6:48:55 AM1.0 mg/L 190Magnesium 5/16/2012 6:48:55 AM1.0 mg/L 128Potassium 5/16/2012 6:48:55 AM1.0 mg/L 169Sodium 5/16/2012 7:29:16 AM10 mg/L 10890

    EPA 120.1: SPECIFIC CONDUCTANCE Analyst: DBDConductivity 5/14/2012 9:25:14 PM0.010 µmhos/cm 15,900

    SM4500-H+B: PH Analyst: DBDpH H 5/14/2012 9:25:14 PM1.68 pH units 18.40

    Qualifiers:

    Page 1 of 9

    */X Value exceeds Maximum Contaminant Level. B Analyte detected in the associated Method BlankE Value above quantitation range H Holding times for preparation or analysis exceededJ Analyte detected below quantitation limits ND Not Detected at the Reporting LimitR RPD outside accepted recovery limits RL Reporting Detection LimitS Spike Recovery outside accepted recovery limits

  • Project: MPPE-4Client: Western Refining Southwest, Gallup

    17-May-12

    QC SUMMARY REPORT 1205562WO#:Hall Environmental Analysis Laboratory, Inc.

    Sample ID MB-1934

    Batch ID: 1934

    Analysis Date: 5/16/2012Prep Date: 5/15/2012

    Analyte Result SPK value SPK Ref Val %REC %RPDLowLimit HighLimit RPDLimit Qual

    Units: mg/L

    PQL

    Client ID: PBW RunNo: 2797

    SeqNo: 77728

    MBLKSampType: TestCode: EPA Method 200.7: Metals

    Calcium 1.0NDMagnesium 1.0NDPotassium 1.0NDSodium 1.0ND

    Sample ID LCS-1934

    Batch ID: 1934

    Analysis Date: 5/16/2012Prep Date: 5/15/2012

    Analyte Result SPK value SPK Ref Val %REC %RPDLowLimit HighLimit RPDLimit Qual

    Units: mg/L

    PQL

    Client ID: LCSW RunNo: 2797

    SeqNo: 77729

    LCSSampType: TestCode: EPA Method 200.7: Metals

    Calcium 50.00 102 85 1151.0 051Magnesium 50.00 101 85 1151.0 050Potassium 50.00 98.1 85 1151.0 049Sodium 50.00 99.5 85 1151.0 050

    Sample ID 1205563-001DMS

    Batch ID: 1934

    Analysis Date: 5/16/2012Prep Date: 5/15/2012

    Analyte Result SPK value SPK Ref Val %REC %RPDLowLimit HighLimit RPDLimit Qual

    Units: mg/L

    PQL

    Client ID: BatchQC RunNo: 2797

    SeqNo: 77734

    MSSampType: TestCode: EPA Method 200.7: Metals

    Calcium 50.00 82.9 70 1305.0 336.8380Magnesium 50.00 96.7 70 1305.0 77.99130Potassium 50.00 94.6 70 1305.0 51.0098

    Sample ID 1205563-001DMSD

    Batch ID: 1934

    Analysis Date: 5/16/2012Prep Date: 5/15/2012

    Analyte Result SPK value SPK Ref Val %REC %RPDLowLimit HighLimit RPDLimit Qual

    Units: mg/L

    PQL

    Client ID: BatchQC RunNo: 2797

    SeqNo: 77735

    MSDSampType: TestCode: EPA Method 200.7: Metals

    Calcium 50.00 85.6 70 130 205.0 336.8 0.354380Magnesium 50.00 96.4 70 130 205.0 77.99 0.154130Potassium 50.00 93.8 70 130 205.0 51.00 0.43398

    Qualifiers:

    Page 2 of 9

    */X Value exceeds Maximum Contaminant Level. B Analyte detected in the associated Method BlankE Value above quantitation range H Holding times for preparation or analysis exceededJ Analyte detected below quantitation limits ND Not Detected at the Reporting LimitR RPD outside accepted recovery limits RL Reporting Detection Limit

  • Project: MPPE-4Client: Western Refining Southwest, Gallup

    17-May-12

    QC SUMMARY REPORT 1205562WO#:Hall Environmental Analysis Laboratory, Inc.

    Sample ID MB

    Batch ID: R2765

    Analysis Date: 5/14/2012Prep Date:

    Analyte Result SPK value SPK Ref Val %REC %RPDLowLimit HighLimit RPDLimit Qual

    Units: mg/L

    PQL

    Client ID: PBW RunNo: 2765

    SeqNo: 76616

    MBLKSampType: TestCode: EPA Method 300.0: Anions

    Phosphorus, Orthophosphate (As P 0.50NDNitrate+Nitrite as N 0.20ND

    Sample ID LCS

    Batch ID: R2765

    Analysis Date: 5/14/2012Prep Date:

    Analyte Result SPK value SPK Ref Val %REC %RPDLowLimit HighLimit RPDLimit Qual

    Units: mg/L

    PQL

    Client ID: LCSW RunNo: 2765

    SeqNo: 76617

    LCSSampType: TestCode: EPA Method 300.0: Anions

    Phosphorus, Orthophosphate (As P 5.000 97.0 90 1100.50 04.9Nitrate+Nitrite as N 3.500 95.7 90 1100.20 03.3

    Sample ID 1205583-003AMS

    Batch ID: R2765

    Analysis Date: 5/14/2012Prep Date:

    Analyte Result SPK value SPK Ref Val %REC %RPDLowLimit HighLimit RPDLimit Qual

    Units: mg/L

    PQL

    Client ID: BatchQC RunNo: 2765

    SeqNo: 76623

    MSSampType: TestCode: EPA Method 300.0: Anions

    Nitrate+Nitrite as N 3.500 102 83.9 1120.20 03.6

    Sample ID 1205583-003AMSD

    Batch ID: R2765

    Analysis Date: 5/14/2012Prep Date:

    Analyte Result SPK value SPK Ref Val %REC %RPDLowLimit HighLimit RPDLimit Qual

    Units: mg/L

    PQL

    Client ID: BatchQC RunNo: 2765

    SeqNo: 76624

    MSDSampType: TestCode: EPA Method 300.0: Anions

    Nitrate+Nitrite as N 3.500 90.6 83.9 112 200.20 0 11.43.2

    Sample ID MB

    Batch ID: R2795

    Analysis Date: 5/15/2012Prep Date:

    Analyte Result SPK value SPK Ref Val %REC %RPDLowLimit HighLimit RPDLimit Qual

    Units: mg/L

    PQL

    Client ID: PBW RunNo: 2795

    SeqNo: 77644

    MBLKSampType: TestCode: EPA Method 300.0: Anions

    Fluoride 0.10NDChloride 0.50NDSulfate 0.50ND

    Sample ID LCS

    Batch ID: R2795

    Analysis Date: 5/15/2012Prep Date:

    Analyte Result SPK value SPK Ref Val %REC %RPDLowLimit HighLimit RPDLimit Qual

    Units: mg/L

    PQL

    Client ID: LCSW RunNo: 2795

    SeqNo: 77645

    LCSSampType: TestCode: EPA Method 300.0: Anions

    Fluoride 0.5000 96.4 90 1100.10 00.48Chloride 5.000 98.5 90 1100.50 04.9Sulfate 10.00 99.1 90 1100.50 09.9

    Qualifiers:

    Page 3 of 9

    */X Value exceeds Maximum Contaminant Level. B Analyte detected in the associated Method BlankE Value above quantitation range H Holding times for preparation or analysis exceededJ Analyte detected below quantitation limits ND Not Detected at the Reporting LimitR RPD outside accepted recovery limits RL Reporting Detection Limit

  • Project: MPPE-4Client: Western Refining Southwest, Gallup

    17-May-12

    QC SUMMARY REPORT 1205562WO#:Hall Environmental Analysis Laboratory, Inc.

    Sample ID 1205624-002AMS

    Batch ID: R2795

    Analysis Date: 5/15/2012Prep Date:

    Analyte Result SPK value SPK Ref Val %REC %RPDLowLimit HighLimit RPDLimit Qual

    Units: mg/L

    PQL

    Client ID: BatchQC RunNo: 2795

    SeqNo: 77649

    MSSampType: TestCode: EPA Method 300.0: Anions

    Fluoride 0.5000 85.4 72.9 1130.10 1.7192.1Sulfate 10.00 105 80.5 1190.50 37.4048

    Sample ID 1205624-002AMSD

    Batch ID: R2795

    Analysis Date: 5/15/2012Prep Date:

    Analyte Result SPK value SPK Ref Val %REC %RPDLowLimit HighLimit RPDLimit Qual

    Units: mg/L

    PQL

    Client ID: BatchQC RunNo: 2795

    SeqNo: 77650

    MSDSampType: TestCode: EPA Method 300.0: Anions

    Fluoride 0.5000 84.7 72.9 113 200.10 1.719 0.1652.1Sulfate 10.00 102 80.5 119 200.50 37.40 0.53448

    Sample ID 1205631-001AMS

    Batch ID: R2795

    Analysis Date: 5/15/2012Prep Date:

    Analyte Result SPK value SPK Ref Val %REC %RPDLowLimit HighLimit RPDLimit Qual

    Units: mg/L

    PQL

    Client ID: BatchQC RunNo: 2795

    SeqNo: 77681

    MSSampType: TestCode: EPA Method 300.0: Anions

    Fluoride 0.5000 85.3 72.9 1130.10 1.5622.0Sulfate 10.00 103 80.5 1190.50 30.1640

    Sample ID 1205631-001AMSD

    Batch ID: R2795

    Analysis Date: 5/15/2012Prep Date:

    Analyte Result SPK value SPK Ref Val %REC %RPDLowLimit HighLimit RPDLimit Qual

    Units: mg/L

    PQL

    Client ID: BatchQC RunNo: 2795

    SeqNo: 77682

    MSDSampType: TestCode: EPA Method 300.0: Anions

    Fluoride 0.5000 87.6 72.9 113 200.10 1.562 0.5762.0Sulfate 10.00 103 80.5 119 200.50 30.16 0.16240

    Qualifiers:

    Page 4 of 9

    */X Value exceeds Maximum Contaminant Level. B Analyte detected in the associated Method BlankE Value above quantitation range H Holding times for preparation or analysis exceededJ Analyte detected below quantitation limits ND Not Detected at the Reporting LimitR RPD outside accepted recovery limits RL Reporting Detection Limit

  • Project: MPPE-4Client: Western Refining Southwest, Gallup

    17-May-12

    QC SUMMARY REPORT 1205562WO#:Hall Environmental Analysis Laboratory, Inc.

    Sample ID MB-1936

    Batch ID: 1936

    Analysis Date: 5/15/2012Prep Date: 5/15/2012

    Analyte Result SPK value SPK Ref Val %REC %RPDLowLimit HighLimit RPDLimit Qual

    Units: mg/L

    PQL

    Client ID: PBW RunNo: 2758

    SeqNo: 76513

    MBLKSampType: TestCode: EPA Method 8015B: Diesel Range

    Diesel Range Organics (DRO) 1.0ND Surr: DNOP 1.000 116 61.3 1641.2

    Sample ID LCS-1936

    Batch ID: 1936

    Analysis Date: 5/15/2012Prep Date: 5/15/2012

    Analyte Result SPK value SPK Ref Val %REC %RPDLowLimit HighLimit RPDLimit Qual

    Units: mg/L

    PQL

    Client ID: LCSW RunNo: 2758

    SeqNo: 76834

    LCSSampType: TestCode: EPA Method 8015B: Diesel Range

    Diesel Range Organics (DRO) 5.000 96.5 74 1571.0 04.8 Surr: DNOP 0.5000 97.7 61.3 1640.49

    Sample ID LCSD-1936

    Batch ID: 1936

    Analysis Date: 5/15/2012Prep Date: 5/15/2012

    Analyte Result SPK value SPK Ref Val %REC %RPDLowLimit HighLimit RPDLimit Qual

    Units: mg/L

    PQL

    Client ID: LCSS02 RunNo: 2758

    SeqNo: 76835

    LCSDSampType: TestCode: EPA Method 8015B: Diesel Range

    Diesel Range Organics (DRO) 5.000 88.7 74 157 231.0 0 8.414.4 Surr: DNOP 0.5000 103 61.3 164 000.52

    Qualifiers:

    Page 5 of 9

    */X Value exceeds Maximum Contaminant Level. B Analyte detected in the associated Method BlankE Value above quantitation range H Holding times for preparation or analysis exceededJ Analyte detected below quantitation limits ND Not Detected at the Reporting LimitR RPD outside accepted recovery limits RL Reporting Detection Limit

  • Project: MPPE-4Client: Western Refining Southwest, Gallup

    17-May-12

    QC SUMMARY REPORT 1205562WO#:Hall Environmental Analysis Laboratory, Inc.

    Sample ID 5ML-RB

    Batch ID: R2774

    Analysis Date: 5/14/2012Prep Date:

    Analyte Result SPK value SPK Ref Val %REC %RPDLowLimit HighLimit RPDLimit Qual

    Units: µg/L

    PQL

    Client ID: PBW RunNo: 2774

    SeqNo: 77103

    MBLKSampType: TestCode: EPA Method 8021B: Volatiles

    Methyl tert-butyl ether (MTBE) 2.5ND Surr: 4-Bromofluorobenzene 20.00 90.0 55 14018

    Sample ID 100NG BTEX LCS

    Batch ID: R2774

    Analysis Date: 5/14/2012Prep Date:

    Analyte Result SPK value SPK Ref Val %REC %RPDLowLimit HighLimit RPDLimit Qual

    Units: µg/L

    PQL

    Client ID: LCSW RunNo: 2774

    SeqNo: 77104

    LCSSampType: TestCode: EPA Method 8021B: Volatiles

    Methyl tert-butyl ether (MTBE) 20.00 98.2 50.5 1582.5 020 Surr: 4-Bromofluorobenzene 20.00 92.3 55 14018

    Sample ID 1205559-001A MS

    Batch ID: R2774

    Analysis Date: 5/14/2012Prep Date:

    Analyte Result SPK value SPK Ref Val %REC %RPDLowLimit HighLimit RPDLimit Qual

    Units: µg/L

    PQL

    Client ID: BatchQC RunNo: 2774

    SeqNo: 77112

    MSSampType: TestCode: EPA Method 8021B: Volatiles

    Methyl tert-butyl ether (MTBE) 20.00 97.9 58 1392.5 0.176020 Surr: 4-Bromofluorobenzene 20.00 108 55 14022

    Sample ID 1205559-001A MSD

    Batch ID: R2774

    Analysis Date: 5/14/2012Prep Date:

    Analyte Result SPK value SPK Ref Val %REC %RPDLowLimit HighLimit RPDLimit Qual

    Units: µg/L

    PQL

    Client ID: BatchQC RunNo: 2774

    SeqNo: 77113

    MSDSampType: TestCode: EPA Method 8021B: Volatiles

    Methyl tert-butyl ether (MTBE) 20.00 97.3 58 139 15.22.5 0.1760 0.65020 Surr: 4-Bromofluorobenzene 20.00 100 55 140 0020

    Sample ID 5ML RB

    Batch ID: R2805

    Analysis Date: 5/15/2012Prep Date:

    Analyte Result SPK value SPK Ref Val %REC %RPDLowLimit HighLimit RPDLimit Qual

    Units: µg/L

    PQL

    Client ID: PBW RunNo: 2805

    SeqNo: 77914

    MBLKSampType: TestCode: EPA Method 8021B: Volatiles

    Benzene 1.0NDToluene 1.0NDEthylbenzene 1.0NDXylenes, Total 2.0ND1,2,4-Trimethylbenzene 1.0ND1,3,5-Trimethylbenzene 1.0ND Surr: 4-Bromofluorobenzene 20.00 93.2 55 14019

    Qualifiers:

    Page 6 of 9

    */X Value exceeds Maximum Contaminant Level. B Analyte detected in the associated Method BlankE Value above quantitation range H Holding times for preparation or analysis exceededJ Analyte detected below quantitation limits ND Not Detected at the Reporting LimitR RPD outside accepted recovery limits RL Reporting Detection Limit

  • Project: MPPE-4Client: Western Refining Southwest, Gallup

    17-May-12

    QC SUMMARY REPORT 1205562WO#:Hall Environmental Analysis Laboratory, Inc.

    Sample ID 100NG BTEX LCS

    Batch ID: R2805

    Analysis Date: 5/15/2012Prep Date:

    Analyte Result SPK value SPK Ref Val %REC %RPDLowLimit HighLimit RPDLimit Qual

    Units: µg/L

    PQL

    Client ID: LCSW RunNo: 2805

    SeqNo: 77915

    LCSSampType: TestCode: EPA Method 8021B: Volatiles

    Benzene 20.00 101 80 1201.0 020Toluene 20.00 104 80 1201.0 021Ethylbenzene 20.00 102 80 1201.0 020Xylenes, Total 60.00 103 80 1202.0 0621,2,4-Trimethylbenzene 20.00 93.6 80 1201.0 0191,3,5-Trimethylbenzene 20.00 98.6 80 1201.0 020 Surr: 4-Bromofluorobenzene 20.00 104 55 14021

    Qualifiers:

    Page 7 of 9

    */X Value exceeds Maximum Contaminant Level. B Analyte detected in the associated Method BlankE Value above quantitation range H Holding times for preparation or analysis exceededJ Analyte detected below quantitation limits ND Not Detected at the Reporting LimitR RPD outside accepted recovery limits RL Reporting Detection Limit

  • Project: MPPE-4Client: Western Refining Southwest, Gallup

    17-May-12

    QC SUMMARY REPORT 1205562WO#:Hall Environmental Analysis Laboratory, Inc.

    Sample ID 1205508-001B

    Batch ID: R2760

    Analysis Date: 5/14/2012Prep Date:

    Analyte Result SPK value SPK Ref Val %REC %RPDLowLimit HighLimit RPDLimit Qual

    Units: µmhos/cm

    PQL

    Client ID: BatchQC RunNo: 2760

    SeqNo: 76802

    DUPSampType: TestCode: EPA 120.1: Specific Conductance

    Conductivity 200.010 0.1471,400

    Sample ID 1205514-001B

    Batch ID: R2760

    Analysis Date: 5/14/2012Prep Date:

    Analyte Result SPK value SPK Ref Val %REC %RPDLowLimit HighLimit RPDLimit Qual

    Units: µmhos/cm

    PQL

    Client ID: BatchQC RunNo: 2760

    SeqNo: 76818

    DUPSampType: TestCode: EPA 120.1: Specific Conductance

    Conductivity 200.010 1.485,700

    Qualifiers:

    Page 8 of 9

    */X Value exceeds Maximum Contaminant Level. B Analyte detected in the associated Method BlankE Value above quantitation range H Holding times for preparation or analysis exceededJ Analyte detected below quantitation limits ND Not Detected at the Reporting LimitR RPD outside accepted recovery limits RL Reporting Detection Limit

  • Project: MPPE-4Client: Western Refining Southwest, Gallup

    17-May-12

    QC SUMMARY REPORT 1205562WO#:Hall Environmental Analysis Laboratory, Inc.

    Sample ID 1205508-001B

    Batch ID: R2760

    Analysis Date: 5/14/2012Prep Date:

    Analyte Result SPK value SPK Ref Val %REC %RPDLowLimit HighLimit RPDLimit Qual

    Units: pH units

    PQL

    Client ID: BatchQC RunNo: 2760

    SeqNo: 76756

    DUPSampType: TestCode: SM4500-H+B: pH

    pH H1.68 0.1437.02

    Sample ID 1205514-001B

    Batch ID: R2760

    Analysis Date: 5/14/2012Prep Date:

    Analyte Result SPK value SPK Ref Val %REC %RPDLowLimit HighLimit RPDLimit Qual

    Units: pH units

    PQL

    Client ID: BatchQC RunNo: 2760

    SeqNo: 76767

    DUPSampType: TestCode: SM4500-H+B: pH

    pH H1.68 0.6517.66

    Qualifiers:

    Page 9 of 9

    */X Value exceeds Maximum Contaminant Level. B Analyte detected in the associated Method BlankE Value above quantitation range H Holding times for preparation or analysis exceededJ Analyte detected below quantitation limits ND Not Detected at the Reporting LimitR RPD outside accepted recovery limits RL Reporting Detection Limit

  • May 17, 2012

    Western Refining Southwest, GallupBeck Larsen

    Dear Beck Larsen:

    RE: MPPE-3 OrderNo.: 1205563

    FAX (505) 722-0210TEL: (505) 722-0258

    Rt. 3 Box 7Gallup, NM 87301

    Hall Environmental Analysis Laboratory4901 Hawkins NE

    Albuquerque, NM 87109

    Website: www.hallenvironmental.comTEL: 505-345-3975 FAX: 505-345-4107

    Hall Environmental Analysis Laboratory received 1 sample(s) on 5/12/2012 for the analyses presented in the following report.

    Andy Freeman

    These were analyzed according to EPA procedures or equivalent. To access our accredited tests please go to www.hallenvironmental.com or the state specific web sites. See the sample checklist and/or the Chain of Custody for information regarding the sample receipt temperature and preservation. Data qualifiers or a narrative will be provided if the sample analysis or analytical quality control parameters require a flag. All samples are reported as received unless otherwise indicated.

    Please don't hesitate to contact HEAL for any additional information or clarifications.

    Sincerely,

    Laboratory Manager4901 Hawkins NEAlbuquerque, NM 87109

    http://www.hallenvironmental.comhttp://www.hallenvironmental.com

  • Project: MPPE-3Client Sample ID: MPPE-3

    Collection Date: 5/10/2012 8:00:00 PMMatrix: AQUEOUS

    CLIENT: Western Refining Southwest, Gallup

    Lab ID: 1205563-001

    Date Reported: 5/17/2012

    Analytical ReportLab Order 1205563

    Analyses Result Qual Units Date AnalyzedDFRL

    Hall Environmental Analysis Laboratory, Inc.

    Received Date: 5/12/2012 11:30:00 AM

    EPA METHOD 8015B: DIESEL RANGE Analyst: JMPDiesel Range Organics (DRO) 5/15/2012 10:06:08 AM1.0 mg/L 17.1 Surr: DNOP 5/15/2012 10:06:08 AM61.3-164 %REC 1127

    EPA METHOD 8021B: VOLATILES Analyst: NSBMethyl tert-butyl ether (MTBE) 5/15/2012 1:06:11 AM12 µg/L 5NDBenzene 5/15/2012 1:06:11 AM5.0 µg/L 5NDToluene 5/15/2012 2:13:02 PM5.0 µg/L 511Ethylbenzene 5/15/2012 1:06:11 AM5.0 µg/L 5NDXylenes, Total 5/15/2012 1:06:11 AM10 µg/L 5ND1,2,4-Trimethylbenzene 5/15/2012 1:06:11 AM5.0 µg/L 5ND1,3,5-Trimethylbenzene 5/15/2012 1:06:11 AM5.0 µg/L 5ND Surr: 4-Bromofluorobenzene 5/15/2012 1:06:11 AM55-140 %REC 5100

    EPA METHOD 300.0: ANIONS Analyst: SRMFluoride * 5/15/2012 2:56:45 PM2.0 mg/L 2025Chloride 5/15/2012 3:21:35 PM250 mg/L 5003,700Phosphorus, Orthophosphate (As P) H 5/14/2012 3:34:22 PM2.5 mg/L 5NDSulfate 5/15/2012 3:09:10 PM25 mg/L 501,100Nitrate+Nitrite as N 5/14/2012 5:49:07 PM1.0 mg/L 5ND

    EPA METHOD 200.7: METALS Analyst: ELSCalcium 5/16/2012 6:37:16 AM5.0 mg/L 5340Magnesium 5/16/2012 6:37:16 AM5.0 mg/L 578Potassium 5/16/2012 6:37:16 AM5.0 mg/L 551Sodium 5/16/2012 7:26:01 AM20 mg/L 201,700

    EPA 120.1: SPECIFIC CONDUCTANCE Analyst: DBDConductivity 5/15/2012 11:30:13 AM0.050 µmhos/cm 514,000

    SM4500-H+B: PH Analyst: DBDpH H 5/14/2012 9:29:21 PM1.68 pH units 18.46

    Qualifiers:

    Page 1 of 9

    */X Value exceeds Maximum Contaminant Level. B Analyte detected in the associated Method BlankE Value above quantitation range H Holding times for preparation or analysis exceededJ Analyte detected below quantitation limits ND Not Detected at the Reporting LimitR RPD outside accepted recovery limits RL Reporting Detection LimitS Spike Recovery outside accepted recovery limits

  • Project: MPPE-3Client: Western Refining Southwest, Gallup

    17-May-12

    QC SUMMARY REPORT 1205563WO#:Hall Environmental Analysis Laboratory, Inc.

    Sample ID MB-1934

    Batch ID: 1934

    Analysis Date: 5/16/2012Prep Date: 5/15/2012

    Analyte Result SPK value SPK Ref Val %REC %RPDLowLimit HighLimit RPDLimit Qual

    Units: mg/L

    PQL

    Client ID: PBW RunNo: 2797

    SeqNo: 77728

    MBLKSampType: TestCode: EPA Method 200.7: Metals

    Calcium 1.0NDMagnesium 1.0NDPotassium 1.0NDSodium 1.0ND

    Sample ID LCS-1934

    Batch ID: 1934

    Analysis Date: 5/16/2012Prep Date: 5/15/2012

    Analyte Result SPK value SPK Ref Val %REC %RPDLowLimit HighLimit RPDLimit Qual

    Units: mg/L

    PQL

    Client ID: LCSW RunNo: 2797

    SeqNo: 77729

    LCSSampType: TestCode: EPA Method 200.7: Metals

    Calcium 50.00 102 85 1151.0 051Magnesium 50.00 101 85 1151.0 050Potassium 50.00 98.1 85 1151.0 049Sodium 50.00 99.5 85 1151.0 050

    Sample ID 1205563-001DMS

    Batch ID: 1934

    Analysis Date: 5/16/2012Prep Date: 5/15/2012

    Analyte Result SPK value SPK Ref Val %REC %RPDLowLimit HighLimit RPDLimit Qual

    Units: mg/L

    PQL

    Client ID: MPPE-3 RunNo: 2797

    SeqNo: 77734

    MSSampType: TestCode: EPA Method 200.7: Metals

    Calcium 50.00 82.9 70 1305.0 336.8380Magnesium 50.00 96.7 70 1305.0 77.99130Potassium 50.00 94.6 70 1305.0 51.0098

    Sample ID 1205563-001DMSD

    Batch ID: 1934

    Analysis Date: 5/16/2012Prep Date: 5/15/2012

    Analyte Result SPK value SPK Ref Val %REC %RPDLowLimit HighLimit RPDLimit Qual

    Units: mg/L

    PQL

    Client ID: MPPE-3 RunNo: 2797

    SeqNo: 77735

    MSDSampType: TestCode: EPA Method 200.7: Metals

    Calcium 50.00 85.6 70 130 205.0 336.8 0.354380Magnesium 50.00 96.4 70 130 205.0 77.99 0.154130Potassium 50.00 93.8 70 130 205.0 51.00 0.43398

    Qualifiers:

    Page 2 of 9

    */X Value exceeds Maximum Contaminant Level. B Analyte detected in the associated Method BlankE Value above quantitation range H Holding times for preparation or analysis exceededJ Analyte detected below quantitation limits ND Not Detected at the Reporting LimitR RPD outside accepted recovery limits RL Reporting Detection Limit

  • Project: MPPE-3Client: Western Refining Southwest, Gallup

    17-May-12

    QC SUMMARY REPORT 1205563WO#:Hall Environmental Analysis Laboratory, Inc.

    Sample ID MB

    Batch ID: R2765

    Analysis Date: 5/14/2012Prep Date:

    Analyte Result SPK value SPK Ref Val %REC %RPDLowLimit HighLimit RPDLimit Qual

    Units: mg/L

    PQL

    Client ID: PBW RunNo: 2765

    SeqNo: 76616

    MBLKSampType: TestCode: EPA Method 300.0: Anions

    Phosphorus, Orthophosphate (As P 0.50NDNitrate+Nitrite as N 0.20ND

    Sample ID LCS

    Batch ID: R2765

    Analysis Date: 5/14/2012Prep Date:

    Analyte Result SPK value SPK Ref Val %REC %RPDLowLimit HighLimit RPDLimit Qual

    Units: mg/L

    PQL

    Client ID: LCSW RunNo: 2765

    SeqNo: 76617

    LCSSampType: TestCode: EPA Method 300.0: Anions

    Phosphorus, Orthophosphate (As P 5.000 97.0 90 1100.50 04.9Nitrate+Nitrite as N 3.500 95.7 90 1100.20 03.3

    Sample ID 1205583-003AMS

    Batch ID: R2765

    Analysis Date: 5/14/2012Prep Date:

    Analyte Result SPK value SPK Ref Val %REC %RPDLowLimit HighLimit RPDLimit Qual

    Units: mg/L

    PQL

    Client ID: BatchQC RunNo: 2765

    SeqNo: 76623

    MSSampType: TestCode: EPA Method 300.0: Anions

    Nitrate+Nitrite as N 3.500 102 83.9 1120.20 03.6

    Sample ID 1205583-003AMSD

    Batch ID: R2765

    Analysis Date: 5/14/2012Prep Date:

    Analyte Result SPK value SPK Ref Val %REC %RPDLowLimit HighLimit RPDLimit Qual

    Units: mg/L

    PQL

    Client ID: BatchQC RunNo: 2765

    SeqNo: 76624

    MSDSampType: TestCode: EPA Method 300.0: Anions

    Nitrate+Nitrite as N 3.500 90.6 83.9 112 200.20 0 11.43.2

    Sample ID MB

    Batch ID: R2795

    Analysis Date: 5/15/2012Prep Date:

    Analyte Result SPK value SPK Ref Val %REC %RPDLowLimit HighLimit RPDLimit Qual

    Units: mg/L

    PQL

    Client ID: PBW RunNo: 2795

    SeqNo: 77644

    MBLKSampType: TestCode: EPA Method 300.0: Anions

    Fluoride 0.10NDChloride 0.50NDSulfate 0.50ND

    Sample ID LCS

    Batch ID: R2795

    Analysis Date: 5/15/2012Prep Date:

    Analyte Result SPK value SPK Ref Val %REC %RPDLowLimit HighLimit RPDLimit Qual

    Units: mg/L

    PQL

    Client ID: LCSW RunNo: 2795

    SeqNo: 77645

    LCSSampType: TestCode: EPA Method 300.0: Anions

    Fluoride 0.5000 96.4 90 1100.10 00.48Chloride 5.000 98.5 90 1100.50 04.9Sulfate 10.00 99.1 90 1100.50 09.9

    Qualifiers:

    Page 3 of 9

    */X Value exceeds Maximum Contaminant Level. B Analyte detected in the associated Method BlankE Value above quantitation range H Holding times for preparation or analysis exceededJ Analyte detected below quantitation limits ND Not Detected at the Reporting LimitR RPD outside accepted recovery limits RL Reporting Detection Limit

  • Project: MPPE-3Client: Western Refining Southwest, Gallup

    17-May-12

    QC SUMMARY REPORT 1205563WO#:Hall Environmental Analysis Laboratory, Inc.

    Sample ID 1205624-002AMS

    Batch ID: R2795

    Analysis Date: 5/15/2012Prep Date:

    Analyte Result SPK value SPK Ref Val %REC %RPDLowLimit HighLimit RPDLimit Qual

    Units: mg/L

    PQL

    Client ID: BatchQC RunNo: 2795

    SeqNo: 77649

    MSSampType: TestCode: EPA Method 300.0: Anions

    Fluoride 0.5000 85.4 72.9 1130.10 1.7192.1Sulfate 10.00 105 80.5 1190.50 37.4048

    Sample ID 1205624-002AMSD

    Batch ID: R2795

    Analysis Date: 5/15/2012Prep Date:

    Analyte Result SPK value SPK Ref Val %REC %RPDLowLimit HighLimit RPDLimit Qual

    Units: mg/L

    PQL

    Client ID: BatchQC RunNo: 2795

    SeqNo: 77650

    MSDSampType: TestCode: EPA Method 300.0: Anions

    Fluoride 0.5000 84.7 72.9 113 200.10 1.719 0.1652.1Sulfate 10.00 102 80.5 119 200.50 37.40 0.53448

    Sample ID 1205631-001AMS

    Batch ID: R2795

    Analysis Date: 5/15/2012Prep Date:

    Analyte Result SPK value SPK Ref Val %REC %RPDLowLimit HighLimit RPDLimit Qual

    Units: mg/L

    PQL

    Client ID: BatchQC RunNo: 2795

    SeqNo: 77681

    MSSampType: TestCode: EPA Method 300.0: Anions

    Fluoride 0.5000 85.3 72.9 1130.10 1.5622.0Sulfate 10.00 103 80.5 1190.50 30.1640

    Sample ID 1205631-001AMSD

    Batch ID: R2795

    Analysis Date: 5/15/2012Prep Date:

    Analyte Result SPK value SPK Ref Val %REC %RPDLowLimit HighLimit RPDLimit Qual

    Units: mg/L

    PQL

    Client ID: BatchQC RunNo: 2795

    SeqNo: 77682

    MSDSampType: TestCode: EPA Method 300.0: Anions

    Fluoride 0.5000 87.6 72.9 113 200.10 1.562 0.5762.0Sulfate 10.00 103 80.5 119 200.50 30.16 0.16240

    Qualifiers:

    Page 4 of 9

    */X Value exceeds Maximum Contaminant Level. B Analyte detected in the associated Method BlankE Value above quantitation range H Holding times for preparation or analysis exceededJ Analyte detected below quantitation limits ND Not Detected at the Reporting LimitR RPD outside accepted recovery limits RL Reporting Detection Limit

  • Project: MPPE-3Client: Western Refining Southwest, Gallup

    17-May-12

    QC SUMMARY REPORT 1205563WO#:Hall Environmental Analysis Laboratory, Inc.

    Sample ID MB-1936

    Batch ID: 1936

    Analysis Date: 5/15/2012Prep Date: 5/15/2012

    Analyte Result SPK value SPK Ref Val %REC %RPDLowLimit HighLimit RPDLimit Qual

    Units: mg/L

    PQL

    Client ID: PBW RunNo: 2758

    SeqNo: 76513

    MBLKSampType: TestCode: EPA Method 8015B: Diesel Range

    Diesel Range Organics (DRO) 1.0ND Surr: DNOP 1.000 116 61.3 1641.2

    Sample ID LCS-1936

    Batch ID: 1936

    Analysis Date: 5/15/2012Prep Date: 5/15/2012

    Analyte Result SPK value SPK Ref Val %REC %RPDLowLimit HighLimit RPDLimit Qual

    Units: mg/L

    PQL

    Client ID: LCSW RunNo: 2758

    SeqNo: 76834

    LCSSampType: TestCode: EPA Method 8015B: Diesel Range

    Diesel Range Organics (DRO) 5.000 96.5 74 1571.0 04.8 Surr: DNOP 0.5000 97.7 61.3 1640.49

    Sample ID LCSD-1936

    Batch ID: 1936

    Analysis Date: 5/15/2012Prep Date: 5/15/2012

    Analyte Result SPK value SPK Ref Val %REC %RPDLowLimit HighLimit RPDLimit Qual

    Units: mg/L

    PQL

    Client ID: LCSS02 RunNo: 2758

    SeqNo: 76835

    LCSDSampType: TestCode: EPA Method 8015B: Diesel Range

    Diesel Range Organics (DRO) 5.000 88.7 74 157 231.0 0 8.414.4 Surr: DNOP 0.5000 103 61.3 164 000.52

    Qualifiers:

    Page 5 of 9

    */X Value exceeds Maximum Contaminant Level. B Analyte detected in the associated Method BlankE Value above quantitation range H Holding times for preparation or analysis exceededJ Analyte detected below quantitation limits ND Not Detected at the Reporting LimitR RPD outside accepted recovery limits RL Reporting Detection Limit

  • Project: MPPE-3Client: Western Refining Southwest, Gallup

    17-May-12

    QC SUMMARY REPORT 1205563WO#:Hall Environmental Analysis Laboratory, Inc.

    Sample ID 5ML-RB

    Batch ID: R2774

    Analysis Date: 5/14/2012Prep Date:

    Analyte Result SPK value SPK Ref Val %REC %RPDLowLimit HighLimit RPDLimit Qual

    Units: µg/L

    PQL

    Client ID: PBW RunNo: 2774

    SeqNo: 77103

    MBLKSampType: TestCode: EPA Method 8021B: Volatiles

    Methyl tert-butyl ether (MTBE) 2.5NDBenzene 1.0NDEthylbenzene 1.0NDXylenes, Total 2.0ND1,2,4-Trimethylbenzene 1.0ND1,3,5-Trimethylbenzene 1.0ND Surr: 4-Bromofluorobenzene 20.00 90.0 55 14018

    Sample ID 100NG BTEX LCS

    Batch ID: R2774

    Analysis Date: 5/14/2012Prep Date:

    Analyte Result SPK value SPK Ref Val %REC %RPDLowLimit HighLimit RPDLimit Qual

    Units: µg/L

    PQL

    Client ID: LCSW RunNo: 2774

    SeqNo: 77104

    LCSSampType: TestCode: EPA Method 8021B: Volatiles

    Methyl tert-butyl ether (MTBE) 20.00 98.2 50.5 1582.5 020Benzene 20.00 101 80 1201.0 020Ethylbenzene 20.00 100 80 1201.0 020Xylenes, Total 60.00 102 80 1202.0 0611,2,4-Trimethylbenzene 20.00 89.3 80 1201.0 0181,3,5-Trimethylbenzene 20.00 96.1 80 1201.0 019 Surr: 4-Bromofluorobenzene 20.00 92.3 55 14018

    Sample ID 1205559-001A MS

    Batch ID: R2774

    Analysis Date: 5/14/2012Prep Date:

    Analyte Result SPK value SPK Ref Val %REC %RPDLowLimit HighLimit RPDLimit Qual

    Units: µg/L

    PQL

    Client ID: BatchQC RunNo: 2774

    SeqNo: 77112

    MSSampType: TestCode: EPA Method 8021B: Volatiles

    Methyl tert-butyl ether (MTBE) 20.00 97.9 58 1392.5 0.176020Benzene 20.00 105 70.1 1181.0 021Ethylbenzene 20.00 104 73.5 1171.0 021Xylenes, Total 60.00 105 73.1 1192.0 0631,2,4-Trimethylbenzene 20.00 96.7 65.8 1211.0 0.4080201,3,5-Trimethylbenzene 20.00 104 71.1 1181.0 021 Surr: 4-Bromofluorobenzene 20.00 108 55 14022

    Sample ID 1205559-001A MSD

    Batch ID: R2774

    Analysis Date: 5/14/2012Prep Date:

    Analyte Result SPK value SPK Ref Val %REC %RPDLowLimit HighLimit RPDLimit Qual

    Units: µg/L

    PQL

    Client ID: BatchQC RunNo: 2774

    SeqNo: 77113

    MSDSampType: TestCode: EPA Method 8021B: Volatiles

    Methyl tert-butyl ether (MTBE) 20.00 97.3 58 139 15.22.5 0.1760 0.65020Benzene 20.00 101 70.1 118 16.41.0 0 4.4520Ethylbenzene 20.00 98.6 73.5 117 13.51.0 0 5.4420

    Qualifiers:

    Page 6 of 9

    */X Value exceeds Maximum Contaminant Level. B Analyte detected in the associated Method BlankE Value above quantitation range H Holding times for preparation or analysis exceededJ Analyte detected below quantitation limits ND Not Detected at the Reporting LimitR RPD outside accepted recovery limits RL Reporting Detection Limit

  • Project: MPPE-3Client: Western Refining Southwest, Gallup

    17-May-12

    QC SUMMARY REPORT 1205563WO#:Hall Environmental Analysis Laboratory, Inc.

    Sample ID 1205559-001A MSD

    Batch ID: R2774

    Analysis Date: 5/14/2012Prep Date:

    Analyte Result SPK value SPK Ref Val %REC %RPDLowLimit HighLimit RPDLimit Qual

    Units: µg/L

    PQL

    Client ID: BatchQC RunNo: 2774

    SeqNo: 77113

    MSDSampType: TestCode: EPA Method 8021B: Volatiles

    Xylenes, Total 60.00 99.9 73.1 119 12.92.0 0 5.23601,2,4-Trimethylbenzene 20.00 92.4 65.8 121 13.51.0 0.4080 4.42191,3,5-Trimethylbenzene 20.00 99.2 71.1 118 13.71.0 0 4.2620 Surr: 4-Bromofluorobenzene 20.00 100 55 140 0020

    Sample ID 5ML RB

    Batch ID: R2805

    Analysis Date: 5/15/2012Prep Date:

    Analyte Result SPK value SPK Ref Val %REC %RPDLowLimit HighLimit RPDLimit Qual

    Units: µg/L

    PQL

    Client ID: PBW RunNo: 2805

    SeqNo: 77914

    MBLKSampType: TestCode: EPA Method 8021B: Volatiles

    Toluene 1.0ND Surr: 4-Bromofluorobenzene 20.00 93.2 55 14019

    Sample ID 100NG BTEX LCS

    Batch ID: R2805

    Analysis Date: 5/15/2012Prep Date:

    Analyte Result SPK value SPK Ref Val %REC %RPDLowLimit HighLimit RPDLimit Qual

    Units: µg/L

    PQL

    Client ID: LCSW RunNo: 2805

    SeqNo: 77915

    LCSSampType: TestCode: EPA Method 8021B: Volatiles

    Toluene 20.00 104 80 1201.0 021 Surr: 4-Bromofluorobenzene 20.00 104 55 14021

    Qualifiers:

    Page 7 of 9

    */X Value exceeds Maximum Contaminant Level. B Analyte detected in the associated Method BlankE Value above quantitation range H Holding times for preparation or analysis exceededJ Analyte detected below quantitation limits ND Not Detected at the Reporting LimitR RPD outside accepted recovery limits RL Reporting Detection Limit

  • Project: MPPE-3Client: Western Refining Southwest, Gallup

    17-May-12

    QC SUMMARY REPORT 1205563WO#:Hall Environmental Analysis Laboratory, Inc.

    Sample ID 1205591-001C

    Batch ID: R2782

    Analysis Date: 5/15/2012Prep Date:

    Analyte Result SPK value SPK Ref Val %REC %RPDLowLimit HighLimit RPDLimit Qual

    Units: µmhos/cm

    PQL

    Client ID: BatchQC RunNo: 2782

    SeqNo: 77366

    DUPSampType: TestCode: EPA 120.1: Specific Conductance

    Conductivity 200.010 0.8804,900

    Qualifiers:

    Page 8 of 9

    */X Value exceeds Maximum Contaminant Level. B Analyte detected in the associated Method BlankE Value above quantitation range H Holding times for preparation or analysis exceededJ Analyte detected below quantitation limits ND Not Detected at the Reporting LimitR RPD outside accepted recovery limits RL Reporting Detection Limit

  • Project: MPPE-3Client: Western Refining Southwest, Gallup

    17-May-12

    QC SUMMARY REPORT 1205563WO#:Hall Environmental Analysis Laboratory, Inc.

    Sample ID 1205508-001B

    Batch ID: R2760

    Analysis Date: 5/14/2012Prep Date:

    Analyte Result SPK value SPK Ref Val %REC %RPDLowLimit HighLimit RPDLimit Qual

    Units: pH units

    PQL

    Client ID: BatchQC RunNo: 2760

    SeqNo: 76756

    DUPSampType: TestCode: SM4500-H+B: pH

    pH H1.68 0.1437.02

    Sample ID 1205514-001B

    Batch ID: R2760

    Analysis Date: 5/14/2012Prep Date:

    Analyte Result SPK value SPK Ref Val %REC %RPDLowLimit HighLimit RPDLimit Qual

    Units: pH units

    PQL

    Client ID: BatchQC RunNo: 2760

    SeqNo: 76767

    DUPSampType: TestCode: SM4500-H+B: pH

    pH H1.68 0.6517.66

    Qualifiers:

    Page 9 of 9

    */X Value exceeds Maximum Contaminant Level. B Analyte detected in the associated Method BlankE Value above quantitation range H Holding times for preparation or analysis exceededJ Analyte detected below quantitation limits ND Not Detected at the Reporting LimitR RPD outside accepted recovery limits RL Reporting Detection Limit

  • May 17, 2012

    Western Refining Southwest, GallupBeck Larsen

    Dear Beck Larsen:

    RE: MPPE-5 OrderNo.: 1205591

    FAX (505) 722-0210TEL: (505) 722-0258

    Rt. 3 Box 7Gallup, NM 87301

    Hall Environmental Analysis Laboratory4901 Hawkins NE

    Albuquerque, NM 87109

    Website: www.hallenvironmental.comTEL: 505-345-3975 FAX: 505-345-4107

    Hall Environmental Analysis Laboratory received 1 sample(s) on 5/14/2012 for the analyses presented in the following report.

    Andy Freeman

    These were analyzed according to EPA procedures or equivalent. To access our accredited tests please go to www.hallenvironmental.com or the state specific web sites. See the sample checklist and/or the Chain of Custody for information regarding the sample receipt temperature and preservation. Data qualifiers or a narrative will be provided if the sample analysis or analytical quality control parameters require a flag. All samples are reported as received unless otherwise indicated.

    Please don't hesitate to contact HEAL for any additional information or clarifications.

    Sincerely,

    Laboratory Manager4901 Hawkins NEAlbuquerque, NM 87109

    http://www.hallenvironmental.comhttp://www.hallenvironmental.com

  • Project: MPPE-5Client Sample ID: MPPE-5

    Collection Date: 5/12/2012 8:00:00 AMMatrix: AQUEOUS

    CLIENT: Western Refining Southwest, Gallup

    Lab ID: 1205591-001

    Date Reported: 5/17/2012

    Analytical ReportLab Order 1205591

    Analyses Result Qual Units Date AnalyzedDFRL

    Hall Environmental Analysis Laboratory, Inc.

    Received Date: 5/14/2012 1:39:00 PM

    EPA METHOD 8015B: DIESEL RANGE Analyst: JMPDiesel Range Organics (DRO) 5/15/2012 10:27:49 AM1.0 mg/L 18.2Motor Oil Range Organics (MRO) 5/15/2012 10:27:49 AM5.0 mg/L 1ND Surr: DNOP 5/15/2012 10:27:49 AM61.3-164 %REC 1125

    EPA METHOD 8015B: GASOLINE RANGE Analyst: NSBGasoline Range Organics (GRO) 5/14/2012 5:55:43 PM0.25 mg/L 50.97 Surr: BFB 5/14/2012 5:55:43 PM69.3-120 %REC 594.7

    EPA METHOD 8021B: VOLATILES Analyst: NSBMethyl tert-butyl ether (MTBE) 5/14/2012 5:55:43 PM12 µg/L 5NDBenzene 5/14/2012 5:55:43 PM5.0 µg/L 5NDToluene 5/14/2012 5:55:43 PM5.0 µg/L 515Ethylbenzene 5/14/2012 5:55:43 PM5.0 µg/L 5NDXylenes, Total 5/14/2012 5:55:43 PM10 µg/L 5ND1,2,4-Trimethylbenzene 5/14/2012 5:55:43 PM5.0 µg/L 5ND1,3,5-Trimethylbenzene 5/14/2012 5:55:43 PM5.0 µg/L 5ND Surr: 4-Bromofluorobenzene 5/14/2012 5:55:43 PM55-140 %REC 597.3

    EPA METHOD 300.0: ANIONS Analyst: SRMFluoride * 5/15/2012 7:54:37 PM10 mg/L 10015Chloride 5/14/2012 8:28:11 PM25 mg/L 50480Phosphorus, Orthophosphate (As P) H 5/14/2012 4:57:07 PM2.5 mg/L 5NDSulfate 5/14/2012 5:09:32 PM10 mg/L 20790Nitrate+Nitrite as N 5/15/2012 1:17:29 PM1.0 mg/L 5ND

    EPA METHOD 200.7: METALS Analyst: ELSCalcium 5/16/2012 7:04:39 AM1.0 mg/L 182Magnesium 5/16/2012 7:04:39 AM1.0 mg/L 122Potassium 5/16/2012 7:04:39 AM1.0 mg/L 150Sodium 5/16/2012 7:32:33 AM10 mg/L 10580

    EPA 120.1: SPECIFIC CONDUCTANCE Analyst: DBDConductivity 5/15/2012 11:34:20 AM0.010 µmhos/cm 14,900

    SM4500-H+B: PH Analyst: DBDpH H 5/15/2012 11:34:20 AM1.68 pH units 18.01

    Qualifiers:

    Page 1 of 1

    */X Value exceeds Maximum Contaminant Level. B Analyte detected in the associated Method BlankE Value above quantitation range H Holding times for preparation or analysis exceededJ Analyte detected below quantitation limits ND Not Detected at the Reporting LimitR RPD outside accepted recovery limits RL Reporting Detection LimitS Spike Recovery outside accepted recovery limits

  • Project: MPPE-5Client: Western Refining Southwest, Gallup

    17-May-12

    QC SUMMARY REPORT 1205591WO#:Hall Environmental Analysis Laboratory, Inc.

    Sample ID MB-1934

    Batch ID: 1934

    Analysis Date: 5/16/2012Prep Date: 5/15/2012

    Analyte Result SPK value SPK Ref Val %REC %RPDLowLimit HighLimit RPDLimit Qual

    Units: mg/L

    PQL

    Client ID: PBW RunNo: 2797

    SeqNo: 77728

    MBLKSampType: TestCode: EPA Method 200.7: Metals

    Calcium 1.0NDMagnesium 1.0NDPotassium 1.0NDSodium 1.0ND

    Sample ID LCS-1934

    Batch ID: 1934

    Analysis Date: 5/16/2012Prep Date: 5/15/2012

    Analyte Result SPK value SPK Ref Val %REC %RPDLowLimit HighLimit RPDLimit Qual

    Units: mg/L

    PQL

    Client ID: LCSW RunNo: 2797

    SeqNo: 77729

    LCSSampType: TestCode: EPA Method 200.7: Metals

    Calcium 50.00 102 85 1151.0 051Magnesium 50.00 101 85 1151.0 050Potassium 50.00 98.1 85 1151.0 049Sodium 50.00 99.5 85 1151.0 050

    Sample ID 1205563-001DMS

    Batch ID: 1934

    Analysis Date: 5/16/2012Prep Date: 5/15/2012

    Analyte Result SPK value SPK Ref Val %REC %RPDLowLimit HighLimit RPDLimit Qual

    Units: mg/L

    PQL

    Client ID: BatchQC RunNo: 2797

    SeqNo: 77734

    MSSampType: TestCode: EPA Method 200.7: Metals

    Calcium 50.00 82.9 70 1305.0 336.8380Magnesium 50.00 96.7 70 1305.0 77.99130Potassium 50.00 94.6 70 1305.0 51.0098

    Sample ID 1205563-001DMSD

    Batch ID: 1934

    Analysis Date: 5/16/2012Prep Date: 5/15/2012

    Analyte Result SPK value SPK Ref Val %REC %RPDLowLimit HighLimit RPDLimit Qual

    Units: mg/L

    PQL

    Client ID: BatchQC RunNo: 2797

    SeqNo: 77735

    MSDSampType: TestCode: EPA Method 200.7: Metals

    Calcium 50.00 85.6 70 130 205.0 336.8 0.354380Magnesium 50.00 96.4 70 130 205.0 77.99 0.154130Potassium 50.00 93.8 70 130 205.0 51.00 0.43398

    Qualifiers:

    Page 2 of 1

    */X Value exceeds Maximum Contaminant Level. B Analyte detected in the associated Method BlankE Value above quantitation range H Holding times for preparation or analysis exceededJ Analyte detected below quantitation limits ND Not Detected at the Reporting LimitR RPD outside accepted recovery limits RL Reporting Detection Limit

  • Project: MPPE-5Client: Western Refining Southwest, Gallup

    17-May-12

    QC SUMMARY REPORT 1205591WO#:Hall Environmental Analysis Laboratory, Inc.

    Sample ID MB

    Batch ID: R2759

    Analysis Date: 5/14/2012Prep Date:

    Analyte Result SPK value SPK Ref Val %REC %RPDLowLimit HighLimit RPDLimit Qual

    Units: mg/L

    PQL

    Client ID: PBW RunNo: 2759

    SeqNo: 76514

    MBLKSampType: TestCode: EPA Method 300.0: Anions

    Chloride 0.50NDPhosphorus, Orthophosphate (As P 0.50NDSulfate 0.50ND

    Sample ID LCS

    Batch ID: R2759

    Analysis Date: 5/14/2012Prep Date:

    Analyte Result SPK value SPK Ref Val %REC %RPDLowLimit HighLimit RPDLimit Qual

    Units: mg/L

    PQL

    Client ID: LCSW RunNo: 2759

    SeqNo: 76515

    LCSSampType: TestCode: EPA Method 300.0: Anions

    Chloride 5.000 95.5 90 1100.50 04.8Phosphorus, Orthophosphate (As P 5.000 101 90 1100.50 05.0Sulfate 10.00 96.5 90 1100.50 09.6

    Sample ID 1205594-001BMS

    Batch ID: R2759

    Analysis Date: 5/14/2012Prep Date:

    Analyte Result SPK value SPK Ref Val %REC %RPDLowLimit HighLimit RPDLimit Qual

    Units: mg/L

    PQL

    Client ID: BatchQC RunNo: 2759

    SeqNo: 76517

    MSSampType: TestCode: EPA Method 300.0: Anions

    Phosphorus, Orthophosphate (As P 5.000 99.0 79.3 1080.50 04.9

    Sample ID 1205594-001BMSD

    Batch ID: R2759

    Analysis Date: 5/14/2012Prep Date:

    Analyte Result SPK value SPK Ref Val %REC %RPDLowLimit HighLimit RPDLimit Qual

    Units: mg/L

    PQL

    Client ID: BatchQC RunNo: 2759

    SeqNo: 76518

    MSDSampType: TestCode: EPA Method 300.0: Anions

    Phosphorus, Orthophosphate (As P 5.000 101 79.3 108 200.50 0 1.715.0

    Sample ID MB

    Batch ID: R2795

    Analysis Date: 5/15/2012Prep Date:

    Analyte Result SPK value SPK Ref Val %REC %RPDLowLimit HighLimit RPDLimit Qual

    Units: mg/L

    PQL

    Client ID: PBW RunNo: 2795

    SeqNo: 77644

    MBLKSampType: TestCode: EPA Method 300.0: Anions

    Fluoride 0.10NDNitrate+Nitrite as N 0.20ND

    Sample ID LCS

    Batch ID: R2795

    Analysis Date: 5/15/2012Prep Date:

    Analyte Result SPK value SPK Ref Val %REC %RPDLowLimit HighLimit RPDLimit Qual

    Units: mg/L

    PQL

    Client ID: LCSW RunNo: 2795

    SeqNo: 77645

    LCSSampType: TestCode: EPA Method 300.0: Anions

    Fluoride 0.5000 96.4 90 1100.10 00.48Nitrate+Nitrite as N 3.500 100 90 1100.20 03.5

    Qualifiers:

    Page 3 of 1

    */X Value exceeds Maximum Contaminant Level. B Analyte detected in the associated Method BlankE Value above quantitation range H Holding times for preparation or analysis exceededJ Analyte detected below quantitation limits ND Not Detected at the Reporting LimitR RPD outside accepted recovery limits RL Reporting Detection Limit

  • Project: MPPE-5Client: Western Refining Southwest, Gallup

    17-May-12

    QC SUMMARY REPORT 1205591WO#:Hall Environmental Analysis Laboratory, Inc.

    Sample ID 1205624-002AMS

    Batch ID: R2795

    Analysis Date: 5/15/2012Prep Date:

    Analyte Result SPK value SPK Ref Val %REC %RPDLowLimit HighLimit RPDLimit Qual

    Units: mg/L

    PQL

    Client ID: BatchQC RunNo: 2795

    SeqNo: 77649

    MSSampType: TestCode: EPA Method 300.0: Anions

    Fluoride 0.5000 85.4 72.9 1130.10 1.7192.1Nitrate+Nitrite as N 3.500 98.9 83.9 1120.20 0.54934.0

    Sample ID 1205624-002AMSD

    Batch ID: R2795

    Analysis Date: 5/15/2012Prep Date:

    Analyte Result SPK value SPK Ref Val %REC %RPDLowLimit HighLimit RPDLimit Qual

    Units: mg/L

    PQL

    Client ID: BatchQC RunNo: 2795

    SeqNo: 77650

    MSDSampType: TestCode: EPA Method 300.0: Anions

    Fluoride 0.5000 84.7 72.9 113 200.10 1.719 0.1652.1Nitrate+Nitrite as N 3.500 96.2 83.9 112 200.20 0.5493 2.403.9

    Sample ID 1205631-001AMS

    Batch ID: R2795

    Analysis Date: 5/15/2012Prep Date:

    Analyte Result SPK value SPK Ref Val %REC %RPDLowLimit HighLimit RPDLimit Qual

    Units: mg/L

    PQL

    Client ID: BatchQC RunNo: 2795

    SeqNo: 77681

    MSSampType: TestCode: EPA Method 300.0: Anions

    Fluoride 0.5000 85.3 72.9 1130.10 1.5622.0Nitrate+Nitrite as N 3.500 98.5 83.9 1120.20 2.4075.9

    Sample ID 1205631-001AMSD

    Batch ID: R2795

    Analysis Date: 5/15/2012Prep Date:

    Analyte Result SPK value SPK Ref Val %REC %RPDLowLimit HighLimit RPDLimit Qual

    Units: mg/L

    PQL

    Client ID: BatchQC RunNo: 2795

    SeqNo: 77682

    MSDSampType: TestCode: EPA Method 300.0: Anions

    Fluoride 0.5000 87.6 72.9 113 200.10 1.562 0.5762.0Nitrate+Nitrite as N 3.500 98.8 83.9 112 200.20 2.407 0.1975.9

    Qualifiers:

    Page 4 of 1

    */X Value exceeds Maximum Contaminant Level. B Analyte detected in the associated Method BlankE Value above quantitation range H Holding times for preparation or analysis exceededJ Analyte detected below quantitation limits ND Not Detected at the Reporting LimitR RPD outside accepted recovery limits RL Reporting Detection Limit

  • Project: MPPE-5Client: Western Refining Southwest, Gallup

    17-May-12

    QC SUMMARY REPORT 1205591WO#:Hall Environmental Analysis Laboratory, Inc.

    Sample ID MB-1936

    Batch ID: 1936

    Analysis Date: 5/15/2012Prep Date: 5/15/2012

    Analyte Result SPK value SPK Ref Val %REC %RPDLowLimit HighLimit RPDLimit Qual

    Units: mg/L

    PQL

    Client ID: PBW RunNo: 2758

    SeqNo: 76513

    MBLKSampType: TestCode: EPA Method 8015B: Diesel Range

    Diesel Range Organics (DRO) 1.0NDMotor Oil Range Organics (MRO) 5.0ND Surr: DNOP 1.000 116 61.3 1641.2

    Sample ID LCS-1936

    Batch ID: 1936

    Analysis Date: 5/15/2012Prep Date: 5/15/2012

    Analyte Result SPK value SPK Ref Val %REC %RPDLowLimit HighLimit RPDLimit Qual

    Units: mg/L

    PQL

    Client ID: LCSW RunNo: 2758

    SeqNo: 76834

    LCSSampType: TestCode: EPA Method 8015B: Diesel Range

    Diesel Range Organics (DRO) 5.000 96.5 74 1571.0 04.8 Surr: DNOP 0.5000 97.7 61.3 1640.49

    Sample ID LCSD-1936

    Batch ID: 1936

    Analysis Date: 5/15/2012Prep Date: 5/15/2012

    Analyte Result SPK value SPK Ref Val %REC %RPDLowLimit HighLimit RPDLimit Qual

    Units: mg/L

    PQL

    Client ID: LCSS02 RunNo: 2758

    SeqNo: 76835

    LCSDSampType: TestCode: EPA Method 8015B: Diesel Range

    Diesel Range Organics (DRO) 5.000 88.7 74 157 231.0 0 8.414.4 Surr: DNOP 0.5000 103 61.3 164 000.52

    Qualifiers:

    Page 5 of 1

    */X Value exceeds Maximum Contaminant Level. B Analyte detected in the associated Method BlankE Value above quantitation range H Holding times for preparation or analysis exceededJ Analyte detected below quantitation limits ND Not Detected at the Reporting LimitR RPD outside accepted recovery limits RL Reporting Detection Limit

  • Project: MPPE-5Client: Western Refining Southwest, Gallup

    17-May-12

    QC SUMMARY REPORT 1205591WO#:Hall Environmental Analysis Laboratory, Inc.

    Sample ID 5ML-RB

    Batch ID: R2774

    Analysis Date: 5/14/2012Prep Date:

    Analyte Result SPK value SPK Ref Val %REC %RPDLowLimit HighLimit RPDLimit Qual

    Units: mg/L

    PQL

    Client ID: PBW RunNo: 2774

    SeqNo: 77075

    MBLKSampType: TestCode: EPA Method 8015B: Gasoline Range

    Gasoline Range Organics (GRO) 0.050ND Surr: BFB 20.00 86.7 69.3 12017

    Sample ID 2.5UG GRO LCS

    Batch ID: R2774

    Analysis Date: 5/14/2012Prep Date:

    Analyte Result SPK value SPK Ref Val %REC %RPDLowLimit HighLimit RPDLimit Qual

    Units: mg/L

    PQL

    Client ID: LCSW RunNo: 2774

    SeqNo: 77076

    LCSSampType: TestCode: EPA Method 8015B: Gasoline Range

    Gasoline Range Organics (GRO) 0.5000 112 101 1230.050 00.56 Surr: BFB 20.00 97.6 69.3 12020

    Sample ID 1205591-001A MS

    Batch ID: R2774

    Analysis Date: 5/14/2012Prep Date:

    Analyte Result SPK value SPK Ref Val %REC %RPDLowLimit HighLimit RPDLimit Qual

    Units: mg/L

    PQL

    Client ID: MPPE-5 RunNo: 2774

    SeqNo: 77091

    MSSampType: TestCode: EPA Method 8015B: Gasoline Range

    Gasoline Range Organics (GRO) 2.500 116 75.4 1210.25 0.97403.9 Surr: BFB 100.0 98.5 69.3 12098

    Sample ID 1205591-001A MSD

    Batch ID: R2774

    Analysis Date: 5/14/2012Prep Date:

    Analyte Result SPK value SPK Ref Val %REC %RPDLowLimit HighLimit RPDLimit Qual

    Units: mg/L

    PQL

    Client ID: MPPE-5 RunNo: 2774

    SeqNo: 77092

    MSDSampType: TestCode: EPA Method 8015B: Gasoline Range

    Gasoline Range Organics (GRO) 2.500 102 75.4 121 10.50.25 0.9740 9.083.5 Surr: BFB 100.0 104 69.3 120 00100

    Qualifiers:

    Page 6 of 1

    */X Value exceeds Maximum Contaminant Level. B Analyte detected in the associated Method BlankE Value above quantitation range H Holding times for preparation or analysis exceededJ Analyte detected below quantitation limits ND Not Detected at the Reporting LimitR RPD outside accepted recovery limits RL Reporting Detection Limit

  • Project: MPPE-5Client: Western Refining Southwest, Gallup

    17-May-12

    QC SUMMARY REPORT 1205591WO#:Hall Environmental Analysis Laboratory, Inc.

    Sample ID 5ML-RB

    Batch ID: R2774

    Analysis Date: 5/14/2012Prep Date:

    Analyte Result SPK value SPK Ref Val %REC %RPDLowLimit HighLimit RPDLimit Qual

    Units: µg/L

    PQL

    Client ID: PBW RunNo: 2774

    SeqNo: 77103

    MBLKSampType: TestCode: EPA Method 8021B: Volatiles

    Methyl tert-butyl ether (MTBE) 2.5NDBenzene 1.0NDToluene 1.0NDEthylbenzene 1.0NDXylenes, Total 2.0ND1,2,4-Trimethylbenzene 1.0ND1,3,5-Trimethylbenzene 1.0ND Surr: 4-Bromofluorobenzene 20.00 90.0 55 14018

    Sample ID 100NG BTEX LCS

    Batch ID: R2774

    Analysis Date: 5/14/2012Prep Date:

    Analyte Result SPK value SPK Ref Val %REC %RPDLowLimit HighLimit RPDLimit Qual

    Units: µg/L

    PQL

    Client ID: LCSW RunNo: 2774

    SeqNo: 77104

    LCSSampType: TestCode: EPA Method 8021B: Volatiles

    Methyl tert-butyl ether (MTBE) 20.00 98.2 50.5 1582.5 020Benzene 20.00 101 80 1201.0 020Toluene 20.00 103 80 1201.0 021Ethylbenzene 20.00 100 80 1201.0 020Xylenes, Total 60.00 102 80 1202.0 0611,2,4-Trimethylbenzene 20.00 89.3 80 1201.0 0181,3,5-Trimethylbenzene 20.00 96.1 80 1201.0 019 Surr: 4-Bromofluorobenzene 20.00 92.3 55 14018

    Sample ID 1205559-001A MS

    Batch ID: R2774

    Analysis Date: 5/14/2012Prep Date:

    Analyte Result SPK value SPK Ref Val %REC %RPDLowLimit HighLimit RPDLimit Qual

    Units: µg/L

    PQL

    Client ID: BatchQC RunNo: 2774

    SeqNo: 77112

    MSSampType: TestCode: EPA Method 8021B: Volatiles

    Methyl tert-butyl ether (MTBE) 20.00 97.9 58 1392.5 0.176020Benzene 20.00 105 70.1 1181.0 021Toluene 20.00 105 72.3 1171.0 0.386021Ethylbenzene 20.00 104 73.5 1171.0 021Xylenes, Total 60.00 105 73.1 1192.0 0631,2,4-Trimethylbenzene 20.00 96.7 65.8 1211.0 0.4080201,3,5-Trimethylbenzene 20.00 104 71.1 1181.0 021 Surr: 4-Bromofluorobenzene 20.00 108 55 14022

    Sample ID 1205559-001A MSD

    Batch ID: R2774

    Analysis Date: 5/14/2012Prep Date:

    Analyte Result SPK value SPK Ref Val %REC %RPDLowLimit HighLimit RPDLimit Qual

    Units: µg/L

    PQL

    Client ID: BatchQC RunNo: 2774

    SeqNo: 77113

    MSDSampType: TestCode: EPA Method 8021B: Volatiles

    Qualifiers:

    Page 7 of 1

    */X Value exceeds Maximum Contaminant Level. B Analyte detected in the associated Method BlankE Value above quantitation range H Holding times for preparation or analysis exceededJ Analyte detected below quantitation limits ND Not Detected at the Reporting LimitR RPD outside accepted recovery limits RL Reporting Detection Limit

  • Project: MPPE-5Client: Western Refining Southwest, Gallup

    17-May-12

    QC SUMMARY REPORT 1205591WO#:Hall Environmental Analysis Laboratory, Inc.

    Sample ID 1205559-001A MSD

    Batch ID: R2774

    Analysis Date: 5/14/2012Prep Date:

    Analyte Result SPK value SPK Ref Val %REC %RPDLowLimit HighLimit RPDLimit Qual

    Units: µg/L

    PQL

    Client ID: BatchQC RunNo: 2774

    SeqNo: 77113

    MSDSampType: TestCode: EPA Method 8021B: Volatiles

    Methyl tert-butyl ether (MTBE) 20.00 97.3 58 139 15.22.5 0.1760 0.65020Benzene 20.00 101 70.1 118 16.41.0 0 4.4520Toluene 20.00 99.1 72.3 117 13.91.0 0.3860 5.8520Ethylbenzene 20.00 98.6 73.5 117 13.51.0 0 5.4420Xylenes, Total 60.00 99.9 73.1 119 12.92.0 0 5.23601,2,4-Trimethylbenzene 20.00 92.4 65.8 121 13.51.0 0.4080 4.42191,3,5-Trimethylbenzene 20.00 99.2 71.1 118 13.71.0 0 4.2620 Surr: 4-Bromofluorobenzene 20.00 100 55 140 0020

    Qualifiers:

    Page 8 of 1

    */X Value exceeds Maximum Contaminant Level. B Analyte detected in the associated Method BlankE Value above quantitation range H Holding times for preparation or analysis exceededJ Analyte detected below quantitation limits ND Not Detected at the Reporting LimitR RPD outside accepted recovery limits RL Reporting Detection Limit

  • Project: MPPE-5Client: Western Refining Southwest, Gallup

    17-May-12

    QC SUMMARY REPORT 1205591WO#:Hall Environmental Analysis Laboratory, Inc.

    Sample ID 1205591-001C

    Batch ID: R2782

    Analysis Date: 5/15/2012Prep Date:

    Analyte Result SPK value SPK Ref Val %REC %RPDLowLimit HighLimit RPDLimit Qual

    Units: µmhos/cm

    PQL

    Client ID: MPPE-5 RunNo: 2782

    SeqNo: 77366

    DUPSampType: TestCode: EPA 120.1: Specific Conductance

    Conductivity 200.010 0.8804,900

    Qualifiers:

    Page 9 of 1

    */X Value exceeds Maximum Contaminant Level. B Analyte detected in the associated Method BlankE Value above quantitation range H Holding times for preparation or analysis exceededJ Analyte detected below quantitation limits ND Not Detected at the Reporting LimitR RPD outside accepted recovery limits RL Reporting Detection Limit

  • Project: MPPE-5Client: Western Refining Southwest, Gallup

    17-May-12

    QC SUMMARY REPORT 1205591WO#:Hall Environmental Analysis Laboratory, Inc.

    Sample ID 1205591-001C

    Batch ID: R2782

    Analysis Date: 5/15/2012Prep Date:

    Analyte Result SPK value SPK Ref Val %REC %RPDLowLimit HighLimit RPDLimit Qual

    Units: pH units

    PQL

    Client ID: MPPE-5 RunNo: 2782

    SeqNo: 77348

    DUPSampType: TestCode: SM4500-H+B: pH

    pH H1.68 0.2498.03

    Qualifiers:

    Page 10 of 1

    */X Value exceeds Maximum Contaminant Level. B Analyte detected in the associated Method BlankE Value above quantitation range H Holding times for preparation or analysis exceededJ Analyte detected below quantitation limits ND Not Detected at the Reporting LimitR RPD outside accepted recovery limits RL Reporting Detection Limit

  • May 17, 2012

    Western Refining Southwest, GallupBeck Larsen

    Dear Beck Larsen:

    RE: MPPE-7 OrderNo.: 1205592

    FAX (505) 722-0210TEL: (505) 722-0258

    Rt. 3 Box 7Gallup, NM 87301

    Hall Environmental Analysis Laboratory4901 Hawkins NE

    Albuquerque, NM 87109

    Website: www.hallenvironmental.comTEL: 505-345-3975 FAX: 505-345-4107

    Hall Environmental Analysis Laboratory received 1 sample(s) on 5/14/2012 for the analyses presented in the following report.

    Andy Freeman

    These were analyzed according to EPA procedures or equivalent. To access our accredited tests please go to www.hallenvironmental.com or the state specific web sites. See the sample checklist and/or the Chain of Custody for information regarding the sample receipt temperature and preservation. Data qualifiers or a narrative will be provided if the sample analysis or analytical quality control parameters require a flag. All samples are reported as received unless otherwise indicated.

    Please don't hesitate to contact HEAL for any additional information or clarifications.

    Sincerely,

    Laboratory Manager4901 Hawkins NEAlbuquerque, NM 87109

    http://www.hallenvironmental.comhttp://www.hallenvironmental.com

  • Project: MPPE-7Client Sample ID: MPPE-7

    Collection Date: 5/14/2012 8:00:00 AMMatrix: AQUEOUS

    CLIENT: Western Refining Southwest, Gallup

    Lab ID: 1205592-001

    Date Reported: 5/17/2012

    Analytical ReportLab Order 1205592

    Analyses Result Qual Units Date AnalyzedDFRL

    Hall Environmental Analysis Laboratory, Inc.

    Received Date: 5/14/2012 1:39:00 PM

    EPA METHOD 8015B: DIESEL RANGE Analyst: JMPDiesel Range Organics (DRO) 5/15/2012 10:49:17 AM1.0 mg/L 19.9Motor Oil Range Organics (MRO) 5/15/2012 10:49:17 AM5.0 mg/L 1ND Surr: DNOP 5/15/2012 10:49:17 AM61.3-164 %REC 1125

    EPA METHOD 8015B: GASOLINE RANGE Analyst: NSBGasoline Range Organics (GRO) 5/15/2012 1:36:57 AM0.25 mg/L 50.97 Surr: BFB 5/15/2012 1:36:57 AM69.3-120 %REC 5104

    EPA METHOD 8021B: VOLATILES Analyst: NSBMethyl tert-butyl ether (MTBE) 5/15/2012 1:36:57 AM12 µg/L 5NDBenzene 5/15/2012 1:36:57 AM5.0 µg/L 5NDToluene 5/15/2012 1:36:57 AM5.0 µg/L 5NDEthylbenzene 5/15/2012 1:36:57 AM5.0 µg/L 5NDXylenes, Total 5/15/2012 1:36:57 AM10 µg/L 5ND1,2,4-Trimethylbenzene 5/15/2012 1:36:57 AM5.0 µg/L 5ND1,3,5-Trimethylbenzene 5/15/2012 1:36:57 AM5.0 µg/L 5ND Surr: 4-Bromofluorobenzene 5/15/2012 1:36:57 AM55-140 %REC 5103

    EPA METHOD 300.0: ANIONS Analyst: SRMFluoride * 5/15/2012 12:52:40 PM5.0 mg/L 50120Chloride 5/14/2012 8:15:46 PM25 mg/L 50460Phosphorus, Orthophosphate (As P) 5/14/2012 5:46:47 PM2.5 mg/L 5NDSulfate 5/14/2012 5:59:12 PM10 mg/L 20530Nitrate+Nitrite as N 5/15/2012 1:29:53 PM1.0 mg/L 5ND

    EPA METHOD 200.7: METALS Analyst: ELSCalcium 5/16/2012 7:11:13 AM1.0 mg/L 157Magnesium 5/16/2012 7:11:13 AM1.0 mg/L 117Potassium 5/16/2012 7:11:13 AM1.0 mg/L 190Sodium 5/16/2012 7:35:40 AM10 mg/L 10730

    EPA 120.1: SPECIFIC CONDUCTANCE Analyst: DBDConductivity 5/15/2012 11:42:39 AM0.010 µmhos/cm 14,900

    SM4500-H+B: PH Analyst: DBDpH *H 5/15/2012 11:42:39 AM1.68 pH units 19.09

    Qualifiers:

    Page 1 of 10

    */X Value exceeds Maximum Contaminant Level. B Analyte detected in the associated Method BlankE Value above quantitation range H Holding times for preparation or analysis exceededJ Analyte detected below quantitation limits ND Not Detected at the Reporting LimitR RPD outside accepted recovery limits RL Reporting Detection LimitS Spike Recovery outside accepted recovery limits

  • Project: MPPE-7Client: Western Refining Southwest, Gallup

    17-May-12

    QC SUMMARY REPORT 1205592WO#:Hall Environmental Analysis Laboratory, Inc.

    Sample ID MB-1934

    Batch ID: 1934

    Analysis Date: 5/16/2012Prep Date: 5/15/2012

    Analyte Result SPK value SPK Ref Val %REC %RPDLowLimit HighLimit RPDLimit Qual

    Units: mg/L

    PQL

    Client ID: PBW RunNo: 2797

    SeqNo: 77728

    MBLKSampType: TestCode: EPA Method 200.7: Metals

    Calcium 1.0NDMagnesium 1.0NDPotassium 1.0NDSodium 1.0ND

    Sample ID LCS-1934

    Batch ID: 1934

    Analysis Date: 5/16/2012Prep Date: 5/15/2012

    Analyte Result SPK value SPK Ref Val %REC %RPDLowLimit HighLimit RPDLimit Qual

    Units: mg/L

    PQL

    Client ID: LCSW RunNo: 2797

    SeqNo: 77729

    LCSSampType: TestCode: EPA Method 200.7: Metals

    Calcium 50.00 102 85 1151.0 051Magnesium 50.00 101 85 1151.0 050Potassium 50.00 98.1 85 1151.0 049Sodium 50.00 99.5 85 1151.0 050

    Sample ID 1205563-001DMS

    Batch ID: 1934

    Analysis Date: 5/16/2012Prep Date: 5/15/2012

    Analyte Result SPK value SPK Ref Val %REC %RPDLowLimit HighLimit RPDLimit Qual

    Units: mg/L

    PQL

    Client ID: BatchQC RunNo: 2797

    SeqNo: 77734

    MSSampType: TestCode: EPA Method 200.7: Metals

    Calcium 50.00 82.9 70 1305.0 336.8380Magnesium 50.00 96.7 70 1305.0 77.99130Potassium 50.00 94.6 70 1305.0 51.0098

    Sample ID 1205563-001DMSD

    Batch ID: 1934

    Analysis Date: 5/16/2012Prep Date: 5/15/2012

    Analyte Result SPK value SPK Ref Val %REC %RPDLowLimit HighLimit RPDLimit Qual

    Units: mg/L

    PQL

    Client ID: BatchQC RunNo: 2797

    SeqNo: 77735

    MSDSampType: TestCode: EPA Method 200.7: Metals

    Calcium 50.00 85.6 70 130 205.0 336.8 0.354380Magnesium 50.00 96.4 70 130 205.0 77.99 0.154130Potassium 50.00 93.8 70 130 205.0 51.00 0.43398

    Qualifiers:

    Page 2 of 10

    */X Value exceeds Maximum Contaminant Level. B Analyte detected in the associated Method BlankE Value above quantitation range H Holding times for preparation or analysis exceededJ Analyte detected below quantitation limits ND Not Detected at the Reporting LimitR RPD outside accepted recovery limits RL Reporting Detection Limit

  • Project: MPPE-7Client: Western Refining Southwest, Gallup

    17-May-12

    QC SUMMARY REPORT 1205592WO#:Hall Environmental Analysis Laboratory, Inc.

    Sample ID MB

    Batch ID: R2759

    Analysis Date: 5/14/2012Prep Date:

    Analyte Result SPK value SPK Ref Val %REC %RPDLowLimit HighLimit RPDLimit Qual

    Units: mg/L

    PQL

    Client ID: PBW RunNo: 2759

    SeqNo: 76514

    MBLKSampType: TestCode: EPA Method 300.0: Anions

    Chloride 0.50NDPhosphorus, Orthophosphate (As P 0.50NDSulfate 0.50ND

    Sample ID LCS

    Batch ID: R2759

    Analysis Date: 5/14/2012Prep Date:

    Analyte Result SPK value SPK Ref Val %REC %RPDLowLimit HighLimit RPDLimit Qual

    Units: mg/L

    PQL

    Client ID: LCSW RunNo: 2759

    SeqNo: 76515

    LCSSampType: TestCode: EPA Method 300.0: Anions

    Chloride 5.000 95.5 90 1100.50 04.8Phosphorus, Orthophosphate (As P 5.000 101 90 1100.50 05.0Sulfate 10.00 96.5 90 1100.50 09.6

    Sample ID 1205594-001BMS

    Batch ID: R2759

    Analysis Date: 5/14/2012Prep Date:

    Analyte Result SPK value SPK Ref Val %REC %RPDLowLimit HighLimit RPDLimit Qual

    Units: mg/L

    PQL

    Client ID: BatchQC RunNo: 2759

    SeqNo: 76517

    MSSampType: TestCode: EPA Method 300.0: Anions

    Phosphorus, Orthophosphate (As P 5.000 99.0 79.3 1080.50 04.9

    Sample ID 1205594-001BMSD

    Batch ID: R2759

    Analysis Date: 5/14/2012Prep Date:

    Analyte Result SPK value SPK Ref Val %REC %RPDLowLimit HighLimit RPDLimit Qual

    Units: mg/L

    PQL

    Client ID: BatchQC RunNo: 2759

    SeqNo: 76518

    MSDSampType: TestCode: EPA Method 300.0: Anions

    Phosphorus, Orthophosphate (As P 5.000 101 79.3 108 200.50 0 1.715.0

    Sample ID MB

    Batch ID: R2795

    Analysis Date: 5/15/2012Prep Date:

    Analyte Result SPK value SPK Ref Val %REC %RPDLowLimit HighLimit RPDLimit Qual

    Units: mg/L

    PQL

    Client ID: PBW RunNo: 2795

    SeqNo: 77644

    MBLKSampType: TestCode: EPA Method 300.0: Anions

    Fluoride 0.10NDNitrate+Nitrite as N 0.20ND

    Sample ID LCS

    Batch ID: R2795

    Analysis Date: 5/15/2012Prep Date:

    Analyte Result SPK value SPK Ref Val %REC %RPDLowLimit HighLimit RPDLimit Qual

    Units: mg/L

    PQL

    Client ID: LCSW RunNo: 2795

    SeqNo: 77645

    LCSSampType: TestCode: EPA Method 300.0: Anions

    Fluoride 0.5000 96.4 90 1100.10 00.48Nitrate+Nitrite as N 3.500 100 90 1100.20 03.5

    Qualifiers:

    Page 3 of 10

    */X Value exceeds Maximum Contaminant Level. B Analyte detected in the associated Method BlankE Value above quantitation range H Holding times for preparation or analysis exceededJ Analyte detected below quantitation limits ND Not Detected at the Reporting LimitR RPD outside accepted recovery limits RL Reporting Detection Limit

  • Project: MPPE-7Client: Western Refining Southwest, Gallup

    17-May-12

    QC SUMMARY REPORT 1205592WO#:Hall Environmental Analysis Laboratory, Inc.

    Sample ID 1205624-002AMS

    Batch ID: R2795

    Analysis Date: 5/15/2012Prep Date:

    Analyte Result SPK value SPK Ref Val %REC %RPDLowLimit HighLimit RPDLimit Qual

    Units: mg/L

    PQL

    Client ID: BatchQC RunNo: 2795

    SeqNo: 77649

    MSSampType: TestCode: EPA Method 300.0: Anions

    Fluoride 0.5000 85.4 72.9 1130.10 1.7192.1Nitrate+Nitrite as N 3.500 98.9 83.9 1120.20 0.54934.0

    Sample ID 1205624-002AMSD

    Batch ID: R2795

    Analysis Date: 5/15/2012Prep Date:

    Analyte Result SPK value SPK Ref


Technical Report for - Microsoft · 2020. 4. 10. · Chloride 8.6 0.50 mg/l EPA 300.0 Fluoride 1.7 0.10 mg/l EPA 300.0 Sulfate 149 5.0 mg/l EPA 300.0 D42816-1B ARAPAHOE Calcium 5.9

Attachment A2 - Welcome to NewMexico.gov Isolation Pilot...  · Web view2020. 8. 24. · operations of the hoist system (such as overtravel, overspeed, power loss, circuitry failure,

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