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International Journal of Mechanical And Production Engineering, ISSN: 2320-2092, Volume- 2, Issue- 6, June-2014 Effect of Microwave Drilling on Micro Hardness Over Perspex Surface 78 EFFECT OF MICROWAVE DRILLING ON MICRO HARDNESS OVER PERSPEX SURFACE 1 NITIN KUMAR LAUTRE, 2 APURBBA KUMAR SHARMA, 3 PRADEEP KUMAR 1,2,3 Department of Mechanical and Industrial Engineering, Indian Institute of Technology Roorkee, Roorkee, India E-mail: [email protected], [email protected], [email protected] Abstract- The work tries to investigate the surface characteristic of microwave drilled surface. The influence of heat concentrated by a concentrator over the perspex (PMMA) specimen is studied. Perspex is widely used as a substitute of conventional glass applications. Vicker hardness (Hv) is analyzed for blind and through hole. The three different surface affected by heating are identified as pile up, heat affected and normal zone. Different hardness values are experienced in different zones. A COMSOL software analysis is also used to show the formation of heat zones over the specimen surfaces. The experimental observations are similar with the simulated trials. The Hv values at heat affected zone were found different for through and blind hole. The result helps to control the microwave power for less variation of Hv during the process. Keywords- Microwave Drilling, Perspex, Vickers Hardness, Concentrator. I. INTRODUCTION Nonconventional machining has wide choices of processes to drill holes. In addition to these process researchers are investigating the use of microwave energy to drill holes in characteristically different materials [1 - 4]. The research in drilling through microwave effectively started in 2000. The possible reason to research is to find the applicability of microwave as an alternate to laser machining. Nowadays laser beam drilling is widely used for automobile fuel injectors, spinning nozzles [5]. The process lack in simplicity and initial cost involvement, among the various other available nonconventional processes. The material perspex find vide application and one of the alternative of glass specimen. It is less fragile, less water sorptive, less soluble, less toxic and wear resistant. The characteristic of perspex are necessarily appreciated in the field of dentistry since 1930. The mechanical property of perspex is widely changed with the application of heat. The heat application in microwave is through hot plasma formed at tip of copper bit. At moderate temperature copper forms a porous oxide in presence of oxygen of the order of 0.1 microns. The increase in temperature or processing time may affect the conductivity and burning of copper. In microwave drilling the copper tool starts from the to surface of perspex, feed the tool through it. The tool feed through the hole is through liquid formed by hot plasma. The plasma is created through electrical discharges and the applications are very common in nonoscience field. At elevated temperature of excited plasma the formation of porous oxide is more in order of 2.5 micron in 150 min. In microwave drilling this may results in nailing of concentrator to work specimen. The microwave power has to be balance to overcome the oxide layer, at the same time prevent copper concentrator from burning. As alternative argon gas is used as primary plasma gas, through a torch jet. At 2.45 GHz, 200 W the inserted copper cannula is used to gain temperature that can melt copper. The simulation studies of electric fields are performed on Ansoft HFSS software and verified through experiments. The ejection of hot plasma by localized microwave impingement on copper tip also spreads copper particle on the perspex specimen. The nanoparticles so scattered during the process get deposited in heat affected zone (HAZ). These effects are not been extended exhaustively in the process of machining the product. The phenomenon of microwave drilling is well understood offsite through various simulations. An axisymmetric finite element method based thermal model is developed to determine hot profile and extent of HAZ during laser drilling of aluminium sheet. The model is tried for the heat input in deep hole drilling. The work on simulation on microwave assisted drilling of hole is found least explored. The numerical studies are verified with Vicker harness number (VHN). The test is commonly used to check the strength of acrylic denture resins with and without reinforcements. Most of the use of Vicker hardness test is for the comparison of different perspex products. A finite-difference time domain method is used to simulate the thin wire in air. The method discretizes the differential Maxwell’ equation to find electric and magnetic field effects. These effects are not been extended exhaustively in the process of machining the product. The present study focuses on the performance of the microwave drilling process on the surface characteristic of perspex specimen. The modification

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International Journal of Mechanical And Production Engineering, ISSN: 2320-2092, Volume- 2, Issue- 6, June-2014

Effect of Microwave Drilling on Micro Hardness Over Perspex Surface

78

EFFECT OF MICROWAVE DRILLING ON MICRO HARDNESS OVER PERSPEX SURFACE

1NITIN KUMAR LAUTRE, 2APURBBA KUMAR SHARMA, 3PRADEEP KUMAR

1,2,3Department of Mechanical and Industrial Engineering, Indian Institute of Technology Roorkee, Roorkee, India

E-mail: [email protected], [email protected], [email protected]

Abstract- The work tries to investigate the surface characteristic of microwave drilled surface. The influence of heat concentrated by a concentrator over the perspex (PMMA) specimen is studied. Perspex is widely used as a substitute of conventional glass applications. Vicker hardness (Hv) is analyzed for blind and through hole. The three different surface affected by heating are identified as pile up, heat affected and normal zone. Different hardness values are experienced in different zones. A COMSOL software analysis is also used to show the formation of heat zones over the specimen surfaces. The experimental observations are similar with the simulated trials. The Hv values at heat affected zone were found different for through and blind hole. The result helps to control the microwave power for less variation of Hv during the process. Keywords- Microwave Drilling, Perspex, Vickers Hardness, Concentrator. I. INTRODUCTION Nonconventional machining has wide choices of processes to drill holes. In addition to these process researchers are investigating the use of microwave energy to drill holes in characteristically different materials [1 - 4]. The research in drilling through microwave effectively started in 2000. The possible reason to research is to find the applicability of microwave as an alternate to laser machining. Nowadays laser beam drilling is widely used for automobile fuel injectors, spinning nozzles [5]. The process lack in simplicity and initial cost involvement, among the various other available nonconventional processes. The material perspex find vide application and one of the alternative of glass specimen. It is less fragile, less water sorptive, less soluble, less toxic and wear resistant. The characteristic of perspex are necessarily appreciated in the field of dentistry since 1930. The mechanical property of perspex is widely changed with the application of heat. The heat application in microwave is through hot plasma formed at tip of copper bit. At moderate temperature copper forms a porous oxide in presence of oxygen of the order of 0.1 microns. The increase in temperature or processing time may affect the conductivity and burning of copper. In microwave drilling the copper tool starts from the to surface of perspex, feed the tool through it. The tool feed through the hole is through liquid formed by hot plasma. The plasma is created through electrical discharges and the applications are very common in nonoscience field. At elevated temperature of excited plasma the formation of porous oxide is more in order of 2.5 micron in 150 min. In microwave drilling this may results in nailing of concentrator to work specimen. The microwave power has to be

balance to overcome the oxide layer, at the same time prevent copper concentrator from burning. As alternative argon gas is used as primary plasma gas, through a torch jet. At 2.45 GHz, 200 W the inserted copper cannula is used to gain temperature that can melt copper. The simulation studies of electric fields are performed on Ansoft HFSS software and verified through experiments. The ejection of hot plasma by localized microwave impingement on copper tip also spreads copper particle on the perspex specimen. The nanoparticles so scattered during the process get deposited in heat affected zone (HAZ). These effects are not been extended exhaustively in the process of machining the product. The phenomenon of microwave drilling is well understood offsite through various simulations. An axisymmetric finite element method based thermal model is developed to determine hot profile and extent of HAZ during laser drilling of aluminium sheet. The model is tried for the heat input in deep hole drilling. The work on simulation on microwave assisted drilling of hole is found least explored. The numerical studies are verified with Vicker harness number (VHN). The test is commonly used to check the strength of acrylic denture resins with and without reinforcements. Most of the use of Vicker hardness test is for the comparison of different perspex products. A finite-difference time domain method is used to simulate the thin wire in air. The method discretizes the differential Maxwell’ equation to find electric and magnetic field effects. These effects are not been extended exhaustively in the process of machining the product. The present study focuses on the performance of the microwave drilling process on the surface characteristic of perspex specimen. The modification

International Journal of Mechanical And Production Engineering, ISSN: 2320-2092, Volume- 2, Issue- 6, June-2014

Effect of Microwave Drilling on Micro Hardness Over Perspex Surface

79

of near by surface of the hole generated are studied for Vickers hardness test. The interaction of copper bit at different power levels is investigated. A closed microwave safe applicator is used to study the performance of drilling process for two different hole depths. An attempt is also made to understand the effect of hardness in HAZ and other zone. II. PLAN OF EXPERIMENTATION The proposed setup used for microwave experimentation for drilling hole is shown in Fig. 1. The setup has different component as applicator, magnetron, supporting work platform and the drilling zone. Earlier researchers have attempted the process in combination of both wave guide and coax. [1], [3], [4]. At high temperature the dielectric burning of coax and complex wave guide creates reservation in simple application of the process. The cavity consists of a microwave safe Faradays cage of size, x = 440, y = 420, z = 210 mm (L X B X H). It consists of the front opening of metallic glass panes to place the specimen inside. A standing wave at 2.45 GHz, 90 W to 900 W is created by magnetron. The stirring and specimen rotation in the cavity is completely eliminated to properly concentrate microwaves at the tip of copper bit. The drill tool used is of size � 0.8 mm X 25 mm with a conical tip at one end as shown in Fig 2. In drilling zone, the jig is used to hold and position bit over the specimen as shown in Fig. 3. The jig provides the self weight to control the bit feed during the process. The material removal rate (MRR) during microwave drilling depends on the gravity feed of bit which affects the HAZ formation around the hole. The jig is covered by a supportive microwave transparent teflon disk over the specimen.

Fig. 1. Microwave drilling setup

The work material used in trials is perspex (PMMA)

of 13 mm thickness. It is one of the alternatives to glass and has a melting point of about 160 OC. The hot plasma generated at copper tip act as a source for microwave absorption during drilling of perspex specimen. As per the viscoelastic behavior of perspex, the Vickers hardness test is considered to be suitable among the others. The Vicker hardness number (VHN) is expressed in the form Hvtest load. The test is performed with standard Vickers indenter fitted on THSV – 800M – A (Model: VH-1 MD) measuring machine. The diamond pyramidal shape indenter has a standard opposite face angle of 136O. The machine is also equipped with “Image-300” software to perform automatic measurement and calculations. The setup also has the facility of moving specimen to a least count of 0.01 mm. The different test available are 1 kgf (9.8 N), 500 gf, 300 gf, 200 gf, 100 gf, 50gf (Hv0.05) , 25 gf, 10 gf (0.098 N). The instrument has the facility of applying the test load automatically for the duration of 30 s, as per ISO 6507-3: 2005. The force is applied in three distinct steps of loading, dwell (10 s) and unloading. The dwell time is considered to be sufficient for perspex to undergo the viscoelastic recovery. The observations are recorded through software at 400 X magnifications and manually at 100 X. The Hv number is estimated within the tolerance band to 2 % during repetitive readings. III. COMSOL MULTIPHYSICS SIMULATION The COMSOL Multiphysics 4.4.0.195 is used as simulating software for the effect of plasma heat on HAZ. The hot plasma formation over the perspex specimen at the start of drilling is shown in Fig. 4. The fine meshed formed during simulation is also shown in Fig. 5. The total number of vertex element, the edge element and the boundary elements were 37, 2770 and 58723 respectively. It accounted for the total number of elements to be 259224. The RAM of processor of 8 GB had the free meshing time been 122.79 s with a minimum element quality of 0.1693. The process before meshing involves defining parameters, geometry, material and physics of microwave heating (mh). The study is chosen for a frequency transient study. The shape order for mesh elements near coordinates are considered as linear. The high order shape functions are avoided due to the highly deformed mesh.

The mesh deformation is significant due to the size

Applicator

Magnetron

Work support

Drilling zone

International Journal of Mechanical And Production Engineering, ISSN: 2320-2092, Volume- 2, Issue- 6, June-2014

Effect of Microwave Drilling on Micro Hardness Over Perspex Surface

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variation from the bit to specimen to the applicator. The variation in solving the finite element (FE) equations for coordinates inside the cavity is shown in Fig. 6. It is observed that the mesh size variations are high along the breadth (B) of the cavity. The variation is also present along the height (H) but along the length (L) is observed to be constant. In simulation, the work piece and the bit material are assumed to be homogenous and isotropic. The workpiece material is transparent and does not interact with microwave by its own. The copper bit is reflective material and concentrate bit at the tip due to skin depth. The time-stepping is completed by time-dependent solver in average time of 143 s ( 2 minutes, 23 seconds). The solver adopts backward differentiation formulas (BDF) and converges the solution in 9th time step as shown in Fig. 7.

0

0.02

0.04

0.06

0.08

0.1

0.12

0 10 20 30 40 50

Number to trials

Coo

rdin

ate

posi

tion

in c

avity

(m)

L B H

Fig. 6. Variation of shape order at mesh

Fig. 7. Solution convergence time step for BDF

IV. VICKERS HARDNESS POST MICROWAVE DRILLING The indentation process of measuring hardness is found quantitative over the other wear assisted process. It is considered to be relatively simple and cheap to provide useful information under wide application of load on the specimen. The hardness value is tested to check the polymer degradation under the influence of heat. The hardness was measured randomly on three distinct surface viz. (a) pileup, (b) HAZ and at (c) normal surface as shown in Fig. 8. The pileup surface has the solidified perspex residue deposited on the circumferential surface. The surface consists of solidified mixture of porous and - metal particle embedded particles, as shown in Fig. 9. The

melted perspex moves up to float on surface by capillary action. It is expected to have large variation of hardness in the pile up residue surface. The next zone away from the hole is the surface of HAZ. As per the circular cross section of copper tool the HAZ zone ends with circular boundary. The glazing in HAZ zone is easily observed under light reflection manually. V. RESULTS AND DISCUSSION The study shows the effective interaction of copper drill bit over perspex specimen directly and indirectly. One of the samples is shown in Fig. 10 with a through hole drilled of average diameter of 1.4 mm at 90 W and in a short time of 10 s. It also shows minimum pile up of perspex residue. The circumference appears to be a joining of two semi-circles on micro scale. The deposits of tool wear are also seen on the surface of HAZ near the drilled hole. The pile up surface on the through hole and blind hole is shown in Fig. 11. It is evident in through hole to have less porous surface as in through hole the feed of bit is uninterrupted. The entire microwave energy is focused at hot plasma, which melts the perspex till it comes out from the other end. In blind hole the hot plasma conduct heat back to drill bit length. The heat conduction also attracts microwaves to lesser skin depth. As on the surface the charge breaks down occurs, it causes spatter and wear of surface particles. The heat experience by top surface is more in blind hole drilling causes oxidation in pileup region, causing more porosity.

Fig. 9. Boundary of pileup and HAZ on perspex surface

International Journal of Mechanical And Production Engineering, ISSN: 2320-2092, Volume- 2, Issue- 6, June-2014

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Fig. 10. Through hole drilled on perspex at 90 W, 10 s

The cut section of drilled blind hole is shown in Fig. 12. The hole exactly replicates the tool shape with smooth and uniform surface texture. The average dimensions of the blind hole observed are a = Φ1.4, b = Φ1.2, c = 5.3, d = 8.4, e = Φ4.6, f = Φ1.6, g = 13 mm. The results from COMSOL simulation shows the zone of heating on perspex at the start of the time interval is shown in Fig. 13. The zone is found to be elliptical in nature due to the wave nature to the microwaves. The simulation results are similar to the drilled hole of Fig. 10.

Fig. 12. Cut section of blind hole

The resistive losses of 1.0357 X 10-3 W/m3 is observed at the start of simulation. There is not much variation in the resistive losses even after t = 55 s (1.0352 X 10-3 W/m3) as shown in Fig. 14. The heat losses are not much in the microwave due to the dielectric properties of the materials at high frequency.

Fig. 13. Heating effect on perspex surface

The microwave on and off time are variable as per the power requirement. At 900 W, the microwaves are focusing all the time on bit. On reducing the power the microwave on time and off time are controlled in the step of 20%, 25%, 50 %, 75% for 90 W, 180 W, 360W, 600 W respectively. The various time steps output of heat generated at drill tip and its effect on perspex is analysed. The heat transferred to perspex is increased exponentially in seconds. The growth of HAZ is also increased accordingly in perspex. The propagation of hot spot energy appears to be constant after 5s. The limiting boundary of HAZ till t = 10 s found to be moderate. The hole drilling in 10 s thus does not allow forming a large HAZ in the perspex. The switching off of microwave power after t = 10 s, accelerates the HAZ expansion. The temperature gradient within different zone of HAZ is linearly affected.

The bit is removed over a specially designed jig, immediately after drilling the hole. The specimen is allowed to cool and then the hardness is measured. A seventeen pickup points for indentation are picked randomly to cover all variations as shown in Fig. 15. The surfaces variations as observed in Fig. 11 are different for different drill depths. For through hole the indent points are selected as an incremental distance from hole. The blind holes variations are considered with incremental and decremented distance selection for indentation within 2% of error.

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Fig. 15. Indentations pick up points from the drilled hole

It is observed that the tip of bit while performing the drilling also spreads nanoparticles near drilled surface. The spread of particle affects the surface hardness HAZ. The hardness variation for a two sample drilled at same setup condition is shown in Fig. 16. The measurement at pile up surface appears to be erratic due to surface unevenness. The blind hole Hv values are less due to high porosity of pile up material. In HAZ the variations in Hv value is more and of higher order as compared to through holes. This may be due to the surface spatter along the drill length. In case of both type of hole the hardness Hv0.05 is slowly dampens to the average value of 41. It implies that the microstructural HAZ is much bigger than the HAZ observed in light reflection physically. The lower value of Hv in HAZ of through holes may result untimely cracks and surface damages than the blind holes.

Fig. 16. Variations of hardness on perspex

CONCLUSION A microwave drilling process for through and blind hole is performed on perspex. Microwave exposure of less than a minute was observed to sufficient to drill a through hole in the perspex of 13 mm thickness. The importance of control of HAZ around the surface to control the hardness and defects formation is vital. The HAZ formation was in the order of 1.6 to 4.6 mm (perspex) for a drill concentrator of � 0.8 mm. The surface Hv value of blind hole was more as compared to the through hole in HAZ. It is observed due to the hot plasma intensity reduction inside hole and spatter

of copper particles over the surface. COMSOL Multiphysics software helps to predict the effect of hot plasma heat over the work specimen. A combination of software and experimental observation found to be complimenting each other. The values are in agreement with conventional microwave theories for different thermal conditions of perspex specimen. The study at elevated temperature in microwave applicator has shown the feasibility of drilling hole and the sensitivity of HAZ and Hv on the surface modification characteristics. These characteristic are also helpful to study the creep and fatigue characteristic of specimen in microwave drilling. The study helps to focus on simple and useful process in the domain of costly and complex nontraditional methods.

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