draft hazardous waste permit to u of m - fay thompson center … · 2018. 12. 19. · draft...

DRAFT

Hazardous Waste Storage Facility Permit EPA ID# MN0000981415

Facility name: U of M - Fay Thompson Center for Environmental Management 501 23rd Avenue SE Minneapolis, MN 55455 Hennepin County

Issuance date: [month day, year]

Modification date:

Expiration date: [five years from issuance date (month day, year)]

In accordance with the provisions of Minn. Stat. chs. 115 and 116, Minn. R. 7001.0010 to 7001.0730, and Minn. R. 7045.0020 to 7045.1400, a Hazardous Waste Storage Facility Permit (Permit) is hereby issued to the Permittee listed on the following page for a facility located at 501 23rd Avenue SE in Minneapolis, Hennepin County, Minnesota (the Facility).

This Resource Conservation and Recovery Act (RCRA) Permit has been prepared based on the information provided by the Permittee’s most recent Permit Application (Part A and Part B) including revisions received through October 31, 2018. The Permit Application is referenced throughout this Permit and as such, is an integral and enforceable part of this Permit. This Permit shall become effective on the date of issuance by the Minnesota Pollution Control Agency (MPCA) Commissioner or MPCA personnel who have been delegated explicit authority by the Commissioner. The original Permit was on August 2, 1993. It was reissued April 7, 1999, September 21, 2005, and September 27, 2012. The existing permit was modified and reissued to the Facility on September 9, 2016. The Permittee must at all times conduct their hazardous waste management activities in accordance with the terms and conditions of this Permit and any other requirements imposed by law or Minnesota Rules.

This permit is effective on the issuance date identified above and supersedes the previous permit. This Permit is effective until five years from date of issuance or until terminated, revoked, or modified by the MPCA, whichever comes first, and it expires at midnight on the expiration date identified above.

This document has been electronically signed. for the Minnesota Pollution Control Agency Steven Giddings, Manager Solid Waste Section Resource Management and Assistance Division

Signature: Type e-Signature

Table of Contents

Page 1. List of Permittees ........................................................................................................................................................... 3 2. Facility description ......................................................................................................................................................... 3 3. Facility layout ................................................................................................................................................................. 4 4. Summary of subject items.............................................................................................................................................. 5 5. Limits and other requirements ...................................................................................................................................... 6 6. Submittal/action requirements.................................................................................................................................... 27 7. Appendix ...................................................................................................................................................................... 28

Permit Issued: [month day, year] Permit Expires: [month day, year]

EPA ID# MN0000981415 of 50

1. List of Permittees

Permittee – owner and operator: University of Minnesota 501 23rd Avenue SE Minneapolis, Minnesota 55455

University of Minnesota is the owner and operator; and hence referred as the Permittee hereafter.

2. Facility description

The U of M - Fay Thompson Center for Environmental Management (Facility) is located at 501 23rd Avenue SE in Minneapolis, Hennepin County, Minnesota. The Facility is at latitude 44.96963824, longitude -93.23986902, Township 029, Range 23, and Section 30. A map of the site boundary can be found in Figure A-1 of the Permit Application. The legal description of the site can be found in Section B of the Permit Application.

Hazardous wastes are received at the Facility from many waste-generating activities throughout the University of Minnesota system. For example: research and teaching laboratories, printing and photography operations, vehicle maintenance, medical and veterinary activities, agricultural activities, and from non-university generators through the Chemical Safety Day Program and other programs. The majority of the wastes received by the Facility are generated by the Minneapolis and St. Paul campuses. The Facility has been designed to manage and store wastes having a wide variety of physical and chemical properties, including corrosive, ignitable, reactive and toxic wastes. The specific waste codes that the University of Minnesota is authorized to store at the Facility can be found in Appendix of the Permit.

Hazardous wastes are segregated into 15 storage rooms within the Facility based on specific characteristics of the waste. The loading dock and staging area are also approved storage areas. Total container storage capacity is 128,100 gallons, and three 2,500-gallon indoor tanks provide a total tank storage capacity of 7,500 gallons. The Facility has approximately 20,000 square feet of hazardous waste management and storage area.

Hazardous waste is generated off site; hence the Facility is considered an off-site Facility. This Permit authorizes and requires the Permittee to conduct the following hazardous waste management activities:

Operating status

Operate an Indoor storage container area(s). Operate an Indoor storage tank(s).


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3. Facility layout

Specific operating, emergency, record keeping, reporting, and general conditions apply to the permitted regulated units. However, for the purposes of corrective action, the Facility includes all property owned or used by the Permittee. Hazardous waste storage locations are shaded blue.


EPA ID# MN0000981415 of 50

4. Summary of subject items

Component ID Description Process Status

STRU1 Container Storage Area 106

Indoor storage container

Operating



Operating



Operating



Operating



Operating



Operating

STRU7 Container Storage Area 116A


Operating



Operating



Operating



Operating



Operating



Operating



Operating



Operating



Operating

STRU17 Container Storage Area 117A - Tank 1

Indoor storage tank

Operating


Indoor storage tank

Operating


Indoor storage tank

Operating

STRU20 Container Storage Area 115B


Operating

STRU21 Container Storage Area 116B


Operating


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5. Limits and other requirements

Specific hazardous wastes authorized to be managed

The Permittee is hereby authorized to manage the hazardous wastes listed in the Appendix of this Permit.

Storage of hazardous waste in containers

The Permittee is authorized to store the following types and quantities of hazardous wastes in containers as specified in the following table:


EPA ID# MN0000981415 of 50

Location Maximum storage capacity (gallons)

Waste Code

DOT approved container

Secondary containment capacity (gallons)

Container Storage Area 106

10450

Listed in the Appendix of this permit

Boxes, Bulk Drums, Labpacks, Pails, Gas Cylinders, Aerosol Cans, Bags, Cans, Plastic Jugs, Freezer Boxes, Commercial Containers

2583


900


Bottles (Glass & Plastic), Boxes, Bulk Drums, Labpacks, Pails, Cans, Bags, Carboys, Plastic & Glass Jugs, Commercial Containers, Containment Trays

1138


1200



1814

Container Storage Area 111 Reactive Chemical Process Area

900



941

Container Storage Area 115, and 115A

3925



10657

Container Storage Area 115B

825


Aerosols and compressed gases. Bottles (Glass & Plastic), Boxes, Bulk Drums, Labpacks, Pails, Cans, Bags, Carboys, Plastic & Glass Jugs, Commercial Containers, Containment Trays

3149

Container Storage Area 116 Flammable Liquid Labpack Preparation Area

1200 Listed in the Appendix of this permit

Bottles (Glass & Plastic), Boxes, Bulk Drums, Labpacks,

1441


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Pails, Cans, Bags,

Carboys, Plastic & Glass Jugs, Commercial Containers.

Container Storage Area 116A 3840 Listed in the Appendix of this permit

Bottles (glass and plastic), Bulk Drums, Labpacks, Pails. Bulk containers of flammable liquids & organic acids must be kept separated as specified in Section D of the Permit Application and as required in 5.1.53 of this Permit.

2858 (Free Liquids)

Container Storage Area 116B 10320 Listed in the Appendix of this permit

Bulk Drums, Labpacks, Pails. Bulk containers of flammable liquids, inorganic & organic acids must be kept separated as specified in Section D of the Permit Application.

9040

Container Storage Area 117 Drum Storage


Bulk Drums, Bottles (glass & plastic), Boxes, Labpacks, Pails, Cans, Bags, Carboys, Commercial Containers

2265

Container Storage Area 117A (including Tanks)


Drums 8392


600


Gas Cylinders, Aerosol Cans, Pressurized Containers, Boxes, Drums, Labpacks, Pails, Commercial Containers, Containment Trays

1616

Container Storage Area 120 10450 Listed in the Appendix of this permit

Boxes, Bulk Drums, Labpacks, Pails, Gas Cylinders, Aerosol Cans, Bags, Cans, Plastic Jugs, Freezer Boxes, Commercial Containers

14084


Bottles (Glass & Plastic), Boxes, Bulk Drums, Labpacks, Pails, Cans, Bags, Carboys, Plastic & Glass Jugs, Commercial Containers

15173


EPA ID# MN0000981415 of 50

Location

Maximum storage capacity (gallons)

Waste code




Bottles (Glass & Plastic), Boxes, Bulk Drums, Labpacks, Pails, Cans, Bags, Carboys, Plastic & Glass Jugs, Freezer Boxes, Commercial Containers

1320


1800



2517

Container Storage Area 124A

49440


Bulk Drums, Labpacks, Pails, Boxes, Bottles (glass and plastic)

14776

Storage of hazardous waste in tanks

The Permittee is authorized to store the following types and quantities of hazardous wastes in tanks as specified in the following table:

Location

Maximum storage capacity (gallons)

Waste code



Container Storage Area 117A - Tank 1

2500


NA

8392 Container Storage Area 117A - Tank 2

2500


NA

8392 Container Storage Area 117A - Tank 3

2500


NA

8392


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Total Facility Serial

Number Permit Condition

5.1.1 The Permittee shall at all times properly operate and maintain the storage Facility, including all hazardous waste management units and all appurtenances related to the storage of hazardous wastes. Proper operation and maintenance includes effective performance, adequate funding, adequate operator staffing and training, and adequate laboratory and process controls. The Permittee shall install and maintain appropriate back-up and auxiliary facilities as needed to remain in compliance with the terms and conditions of this Permit. [Minn. R. 7045]

5.1.2 The Permittee shall prevent the discharge of hazardous waste from the Facility to the surface waters or groundwaters of the State. The Permittee shall prevent hazardous waste from entering drains, sewer inlets, storm sewers, sanitary sewers, doorways, vents, tunnels, pipes, windows, and other areas with permeable floors. [Minn. R. 7045]

5.1.3 The Permittee shall operate and maintain the Facility to minimize the possibility of fire, explosion, or other event that might allow hazardous wastes to escape into the air, land, or water. [Minn. R. 7045.0462, subp. 2]

5.1.4 The Permittee must ensure that the type and condition of containers used to store hazardous waste will be selected and maintained in accordance with Minn. R. 7045.0526 and the operations manual set forth in the Permit Application. [Minn. R. 7045.0526]

5.1.5 The containers must be of sturdy leak-proof construction, adequate wall thickness, adequate weld, hinge, and seam strength. Further, the containers (except glass containers) must be of sufficient strength to withstand side and bottom shock, when filled, without impairment of the ability of the container to fully contain the hazardous waste. [Minn. R. 7045.0526, subp. 2(A)]

5.1.6 The containers must have lids, caps, hinges, or other closure devices of sufficient strength and construction so that when closed they will withstand dropping, overturning, or other shock without impairment of the container's ability to fully contain the hazardous waste. [Minn. R. 7045.0526, subp. 2(B)]

5.1.7 The containers (except glass containers) must be made of or lined with materials which will not react with, and are otherwise compatible with, the hazardous waste to be stored and other substances that the container may foreseeably contact, so that the ability of the container to contain the waste is not impaired. [Minn. R. 7045.0526, subp. 3]

5.1.8 If a container holding hazardous waste does not meet the requirements of Minn. R. 7045.0526, subp. 2.A and B., or if it begins to leak, the Permittee shall transfer the hazardous waste in the defective container to a container that does meet the requirements of Minn. R. 7045.0526. [Minn. R. 7045.0526, subp. 2]

5.1.9 A container, or the outer packaging for multiple containers, holding hazardous waste must be labeled with an accumulation start date, the words "Hazardous Waste," and a content description.

[Minn. R. 7045.0526, subp. 4a]

5.1.10 Containers must be kept closed during storage, except when it is necessary to add or remove waste. For labpack drums, this requirement may be met by placing covers on the labpack drums when waste is not being added or removed, and by fully closing the labpack drums at the end of the day or at the end of packing operations, whichever comes first. For labpack boxes, this requirement may be met by assuring that the inner containers of the labpack boxes are always closed and that covers are in place when waste is not being added or removed and tightly in place at the end of the day. [Minn. R. 7045.0526, subp. 4]

5.1.11 A container holding hazardous waste must not be opened, handled, or stored in a manner which may rupture the container or cause it to leak. [Minn. R. 7045.0526, subp. 4]

5.1.12 Drums and commercial containers holding hazardous waste that are stored in one of the long-term storage areas must be marked with the Permittee's container identification number in such a way that the number is visible when the drum is viewed by a person standing on the floor. [Minn. R. 7045]

5.1.13 The Permittee shall maintain the container storage area secondary containment system to ensure that the system is capable of collecting and holding spills, leaks, and precipitation. [Minn. R. 7045.0526, subp. 6(A)]

5.1.14 The maintenance of the secondary containment system must ensure that the compatible base underlying the containers is free of cracks or gaps and is sufficiently impervious so as to contain leaks and spills until the collected material is detected and removed. [Minn. R. 7045.0526, subp. 6(A)(1)]

5.1.15 The maintenance of the secondary containment system must ensure that the compatible base is sloped to drain and remove liquid resulting from leaks, spills, and accumulated precipitation. [Minn. R. 7045.0526, subp. 6(A)(2)]

5.1.16 The maintenance of the secondary containment system must ensure that the secondary containment system has sufficient capacity to contain at least ten percent of the volume of all containers or the volume of the largest container, whichever is greater. [Minn. R. 7045.0526, subp. 6(A)(3)]

5.1.17 The interface between the dike or sidewall and the underlying base of the container storage area secondary containment system is sealed to contain leaks, spills, and accumulated liquids. [Minn. R. 7045.0526, subp. 6(A)(1)]


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5.1.18 The Permittee shall operate the tank system (tank(s), ancillary equipment, and secondary containment

system) in accordance with Minn. R. 7045.0528 and this part of this Permit. [Minn. R. 7045.0528]

5.1.19 The Permittee's tank secondary containment system consists of concrete floors and curbs with chemically resistant coatings. This secondary containment system must be operated to prevent the migration of hazardous waste or constituents or accumulated liquid to the soil, groundwater, or surface water, as well as to detect and collect releases and accumulated liquid until the collected material is removed. [Minn. R. 7045.0528, subp. 4(A and B)]

5.1.20 The secondary containment system must be constructed of or lined with materials that are maintained to be compatible with the hazardous waste placed in the tanks and must have sufficient strength and thickness to prevent failure owing to pressure gradients, including static head and external hydrological forces, physical contact with the waste to which it is exposed, climatic conditions, and the stress of daily operation, including stresses from nearby vehicular traffic. [Minn. R. 7045.0528, subp. 4(C)(1)]

5.1.21 The secondary containment system must be placed on a foundation or base capable of providing support to the secondary containment system, resistant to pressure gradients above and below the system, and capable of preventing failure due to settlement, compression, or uplift.

[Minn. R. 7045.0528, subp. 4(C)(2)]

5.1.22 The secondary containment system must be provided with a leak detection system that is designed and operated to detect the failure of either the primary or secondary containment structure or the release of any hazardous waste or accumulated liquid in the secondary containment system WITHIN 24 HOURS. [Minn. R. 7045.0528, subp. 4(C)(3)]

5.1.23 The secondary containment system must be sloped or otherwise designed or operated to drain and remove liquids resulting from leaks, spills, and precipitation. [Minn. R. 7045.0528, subp. 4(C)(4)]

5.1.24 In addition to the requirements of 7045.0528, subp. 4.A. to 4.C. the Permittee shall maintain the concrete floors and curbs with chemically resistant coatings secondary containment system in accordance with Minn. R. 7045.0528, subp. 4, item [E, F, G]. [Minn. R. 7045.0528, subp. 4(E - G)]

5.1.25 The Permittee shall maintain secondary containment for tank ancillary equipment in accordance with Minn. R. 7045.0528, subp. 4, item H. [Minn. R. 7045.0528, subp. 4(H)]

5.1.26 Valves, pipes, fittings, and other closure devices and appurtenances must be of sufficient strength to withstand shock and internal pressure without impairment of the ability of the tank to fully contain the waste. Gasketed closures must be fitted with gaskets comprised of materials that are sufficient to prevent leakage and that will not be deteriorated by the contents. Written tank system assessments required by Minn. R. 7045.0528, subps. 2 and 3 must be maintained at the Facility. [Minn. R. 7045.0528, subp. 2 and 3]

5.1.27 The Permittee shall use check valves and dry disconnect couplings for spill prevention controls. The Permittee shall use high level alarms and automatic feed cutoffs as overfill prevention devices. These controls and devices shall be properly operated and maintained to prevent failure of the tank system. [Minn. R. 7045.0528, subp. 6]

5.1.28 In the event the Permittee shall be required by the MPCA to conduct monitoring, the following requirements shall be complied with: 1. Samples and measurements taken for the purpose of monitoring shall be representative of the monitored activity. 2. The method used to obtain a representative sample of the waste to be analyzed must be the appropriate method set forth in Title 40 of the Code of Federal Regulations, Part 261, Appendix I. Laboratory methods must be those specified in the latest edition of EPA publication Test Methods for Evaluating Solid Waste: Physical/Chemical Methods SW-846, or an equivalent method approved by the MPCA. [Minn. R. 7045.0484]

5.1.29 The Permittee shall notify, and document in writing, each generator from whom it receives wastes that the Permittee has received this Permit from the MPCA. [Minn. R. 7045.0452, subp. 3(C)]

5.1.30 In the event the Permittee receives a shipment of hazardous wastes that the Permittee is not authorized to receive and store at the Facility, the Permittee shall IMMEDIATELY notify the MPCA and wait for further instructions before accepting the waste. [Minn. R. 7045.0452, subp. 3(B)]

5.1.31 In the event the Permittee manages hazardous waste that is used as fuel or used to produce fuel, the Permittee must comply with Minn. R. 7045.0692. [Minn. R. 7045.0692]

5.1.32 In accordance with the Waste Analysis Plan set forth in the Permit Application, and the requirements of Minn. R. 7045.0458, the Permittee shall obtain a detailed chemical and physical analysis of a representative sample of each waste that the Permittee intends to manage at the Facility. The Permittee shall keep this analysis at the Facility and shall provide a copy to the MPCA upon request.

[Minn. R. 7045.0458, subp. 1(A)]

5.1.33 The waste analysis may include data developed under parts 7045.0102 to 7045.0155 and existing published or documented data on the hazardous waste or on hazardous waste generated from similar processes, including data obtained from the generator. [Minn. R. 7045.0458, subp. 1(B)]

5.1.34 The waste analysis must be repeated, to ensure that it is accurate and up-to-date, at anytime that the Permittee has reason to believe that the process or operation generating the waste has changed.


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[Minn. R. 7045.0458, subp. 1(C)(1)]

5.1.35 The waste analysis must be repeated, to ensure that it is accurate and up-to-date, at anytime that the Permittee has reason to believe a hazardous waste that has been received does not match the waste specified on the accompanying manifest. [Minn. R. 7045.0458, subp. 1(C)(2)]

5.1.36 The waste analysis must be repeated, to ensure that it is accurate and up-to-date, at anytime that the waste analysis plan set forth in Section C of the Permit Application requires a particular shipment of hazardous waste to be analyzed. [Minn. R. 7045.0458, subp. 1(C)]

5.1.37 The Permittee shall not allow any employee to work at the Facility in a job related to hazardous waste management until that employee has received all training required by Minn. R. 7045.0454 and the Personnel Training Plan set forth in the Permit Application. [Minn. R. 7045.0454]

5.1.38 The Permittee shall comply with the manifest requirements in Minn. R. 7045.0474. [Minn. R. 7045.0474]

5.1.39 If the Permittee discovers a major discrepancy in a manifest, the Permittee shall attempt to reconcile the discrepancy. If the Permittee is unable to reconcile the discrepancy with the generator and transporter WITHIN TEN (10) DAYS, the Permittee shall IMMEDIATELY submit to the MPCA a letter describing the discrepancy, attempts made to reconcile it, and a copy of the manifest or shipping paper. The type of discrepancy must be noted on the manifest. [Minn. R. 7045.0476, subp. 3(A)]

5.1.40 If the Permittee discovers a minor discrepancy in a manifest, the Permittee shall attempt to reconcile the discrepancy with the generator and transporter. If the discrepancy cannot be reconciled, the Permittee shall note the type of discrepancy and its resolution on the manifest. [Minn. R. 7045.0476, subp. 3(B)]

5.1.41 The definitions of "major discrepancy" and "minor discrepancy" can be found in Minn. R. 7045.0476, subp. 2. [Minn. R. 7045.0476, subp. 2]

5.1.42 The Permittee shall take precautions to prevent accidental ignition or reaction of ignitable or reactive waste. This waste must be separated and protected from sources of ignition or reaction, including, but not limited to open flames, smoking, cutting and welding, hot surfaces, frictional heat, static sparks, electrical sparks, mechanical sparks, spontaneous ignition, and radiant heat. When ignitable or reactive waste is being handled, the Permittee shall confine smoking and open flame to specially designated locations. "No Smoking" signs must be conspicuously placed wherever there is a hazard from ignitable or reactive waste. [Minn. R. 7045.0456, subp. 1]

5.1.43 The Permittee shall take precautions to prevent reactions which generate extreme heat, pressure, fire, explosions, or violent reactions unless the Permittee is Permitted to handle these types of reactions. [Minn. R. 7045.0456, subp. 2(A)]

5.1.44 The Permittee shall take precautions to prevent reactions which produce uncontrolled toxic mists, fumes, dusts, or gases in sufficient quantities to threaten human health or the environment.

[Minn. R. 7045.0456, subp. 2(B)]

5.1.45 The Permittee shall take precautions to prevent reactions which produce uncontrolled flammable fumes or gases in sufficient quantities to pose a risk of fire or explosions. [Minn. R. 7045.0456, subp. 2(C)]

5.1.46 The Permittee shall take precautions to prevent reactions which damage the structural integrity of the device or facility. [Minn. R. 7045.0456, subp. 2(D)]

5.1.47 The Permittee shall take precautions to prevent reactions which through other means threaten human health or the environment. [Minn. R. 7045.0456, subp. 2(E)]

5.1.48 Containers holding ignitable or reactive wastes and materials must be located at least 15 meters (50 feet) from the Facility's property line as delineated on the map Appendix I, hereof. [Minn. R. 7045.0526, subp. 7]

5.1.49 Ignitable and reactive wastes placed in tanks must be stored in such a way that they are protected from any materials or conditions which may cause the waste to ignite or react. [Minn. R. 7045.0528, subp. 10(B)]

5.1.50 Protective distances for tanks must be followed as specified in the Minnesota State Fire Code, chapter 7510. [Minn. R. 7045.0528, subp. 10]

5.1.51 Incompatible wastes or wastes which are incompatible with other material must not be placed in the same container, unless compliance with Minn. R. 7045.0456, subp. 2, is achieved. [Minn. R. 7045.0526, subp. 8]

5.1.52 Hazardous waste must not be placed in an unwashed container that previously held an incompatible waste or material. As required by Minn. R. 7045.0458, subp. 2, the waste analysis plan must include analyses to comply with these special requirements. Minn. R. 7045.0456, subp. 3, requires waste analyses, trial tests, and documentation to ensure compliance with Minn. R. 7045.0456, subp. 2. All results obtained from testing must be maintained in the Facility operating record. [Minn. R. 7045.0526, subp. 8]

5.1.53 A storage container holding a hazardous waste that is incompatible with any waste or other materials stored nearby in other containers, waste piles, open tanks, or surface impoundments, must be separated from other such waste or material by means of a dike, berm, wall, or other protective device. [Minn. R. 7045.0526, subp. 8]


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5.1.54 Incompatible wastes and/or incompatible wastes and materials must not be placed in the same tank,

unless compliance with Minn. R. 7045.0456, subpart 2 is maintained. [Minn. R. 7045.0528, subp. 11]

5.1.55 The Permittee shall conduct inspections at the Facility and for all hazardous waste management units as required under the inspection plan set forth in Section E of the Permit Application, Minn. R. 7045.0452, subp. 5, 7045.0526, subp. 5, and 7045.0528, subp. 7 shall be followed. [Minn. R. 7045.0452]

5.1.56 The Permittee shall maintain a 24-hour surveillance system which continuously monitors and controls entry onto the active portion of the Facility, or an artificial or natural barrier which completely surrounds the active portion of the Facility and a means to control entry at all times through gates or other entrances to the active portion of the Facility. The fence shall be locked at times when the Facility is unattended and access to the Facility shall be provided only to persons who are authorized by the Permittee to enter the Facility. The Permittee shall post a sign legible from a distance of 25 feet with the legend, "Danger - Unauthorized Personnel Keep Out," at each entrance to the Facility as defined in Minn. R. 7045.0020, subp. 3. [Minn. R. 7045.0452, subp. 4]

5.1.57 The Permittee shall provide adequate lighting for the Facility to ensure safety and proper operation. [Minn. R. 7045.0452]

5.1.58 In regards to Liability Coverage, Pursuant to Minn. R. 7045.0498. supb. 1, the Permittee, as an entity of the State of Minnesota, is exempt from the requirements of Minn. R. 7045.0498 to 7045.0524. [Minn. R. 7045.0504]

5.1.59 In regards to financial assurance for closure, Pursuant to Minn. R. 7045.0498. supb. 1, the Permittee, as an entity of the State of Minnesota, is exempt from the requirements of Minn. R. 7045.0498 to 7045.0524. [Minn. R. 7045.0518]

5.1.60 The Permittee shall place all hazardous waste received from off-site generators into the storage unit within 24 hours after receipt of the waste. [Minn. R. 7045]

5.1.61 Hazardous waste treatment shall be conducted at the Facility only as part of training activities for students, faculty, or staff. Treatment conducted as part of training activities, as described in Section D-6 of the Permit Application, is considered to be training rather than hazardous waste treatment, and does not require a Part B hazardous waste facility permit. Hazardous waste that is to be used as part of the training activities shall be stored in accordance with the requirements of the Permit until it is treated. Any hazardous waste generated as part of the treatment shall be stored in accordance with the requirements of this Permit. [Minn. R. 7045]

5.1.62 a. The Permittee shall have a contingency plan for the facility. The contingency plan must be designed to minimize hazards to human health or the environment from fires, explosions, or any unplanned sudden or nonsudden release of hazardous waste or hazardous waste constituents to air, land, or water.

b. The contingency plan must contain all applicable items listed in Minn. R. 7045.0466, subp. 4.

c. The Permittee must ensure that the provisions of the contingency plan, set forth in the Permit Application, are carried out IMMEDIATELY whenever there is a release, fire, or explosion of hazardous waste or hazardous constituents which could threaten human health or the environment.

[Minn. R. 7045.0466, subp. 3 and 4]

5.1.63 The Permittee shall amend the contingency plan whenever this Permit is revised. [Minn. R. 7045.0466, subp. 6(A)]

5.1.64 The Permittee shall amend the contingency plan whenever said plan fails in an emergency. [Minn. R. 7045.0466, subp. 6(B)]

5.1.65 The Permittee shall amend the contingency plan whenever the Facility changes in its design, construction, operation, maintenance, or other circumstance in a way that increases the potential for fires, explosions, or the release of hazardous waste or hazardous constituents, or changes the response necessary in an emergency. [Minn. R. 7045.0466, subp. 6(C)]

5.1.66 The Permittee shall amend the contingency plan whenever the designated emergency coordinator changes. [Minn. R. 7045.0466, subp. 6(D)]

5.1.67 The Permittee shall amend the contingency plan whenever the list of emergency equipment changes. [Minn. R. 7045.0466, subp. 6(E)]

5.1.68 The Permittee shall maintain a copy of its contingency plan at the Facility at all times. [Minn. R. 7045.0466, subp. 5(A)]

5.1.69 The Permittee shall submit a copy of its Contingency Plan to all local police departments, fire departments, hospitals, and all local and state emergency response teams that may be called upon to respond in an emergency situation at the Facility. [Minn. R. 7045.0466, subp. 5(B)]

5.1.70 At a minimum, the Permittee shall maintain emergency equipment required by the contingency plan. [Minn. R. 7045.0462]

5.1.71 The Permittee shall test and maintain all Facility communications or alarm systems, fire protection equipment, and spill control equipment to ensure proper operation in time of emergency. The


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maintenance and inspection of emergency equipment shall be conducted in accordance with the

Inspection Plan set forth in the Permit Application. [Minn. R. 7045.0462, subp. 4]

5.1.72 The Permittee shall ensure that whenever hazardous waste is being poured, mixed, spread, or otherwise handled, all personnel involved in the operation shall have immediate access to an internal alarm or emergency communication device, either directly or through visual and/or voice contact with another employee. [Minn. R. 7045.0462, subp. 5]

5.1.73 The Permittee shall maintain at least three (3) feet of aisle space in all hazardous waste storage areas to allow the unobstructed movement in an emergency of personnel, fire protection equipment, spill control equipment, and decontamination equipment. [Minn. R. 7045.0462, subp. 6]

5.1.74 The Permittee shall at all times have at least one (1) employee either on the Facility premises or on call with the responsibility for coordinating all emergency response measures. The following person[s] qualifies as the emergency coordinator and each assumes all emergency procedure responsibilities described in Minn. R. 7045.0468 and this Permit. Adam Krajicek – 765-404-9626 (cell) Calvin Cole - 612-490-3687 (cell) Brett Alstad - 612-730-1277 (cell) [Minn. R. 7045.0468, subp. 1]

5.1.75 The Permittee may change the names of employees who qualify as emergency coordinator by contacting the MPCA and identifying the new emergency coordinator[s]. [Minn. R. 7045.0468, subp. 1]

5.1.76 If there should be a leak of hazardous waste from the "tank system" (which is defined to include the tank, secondary containment system, and all ancillary equipment such as pumps, valves, monitoring equipment etc.), the Permittee shall IMMEDIATELY stop the flow of hazardous waste into the tank system and inspect the tank system to determine the cause of the leak. [Minn. R. 7045.0528, subp. 8(A)]

5.1.77 If there should be a leak of hazardous waste from the "tank system" (which is defined to include the tank, secondary containment system, and all ancillary equipment such as pumps, valves, monitoring equipment etc.), the Permittee shall WITHIN 24 HOURS after detection of the leak, or at the earliest practicable time, whichever is sooner, remove as much of the waste as is necessary to prevent further release of hazardous waste to the environment (i.e., escaping the secondary containment system) and repair the tank system. [Minn. R. 7045.0528, subp. 8(B)(1)]

5.1.78 If there should be a leak of hazardous waste from the "tank system" (which is defined to include the tank, secondary containment system, and all ancillary equipment such as pumps, valves, monitoring equipment etc.), the Permittee shall IMMEDIATELY conduct a visual inspection of all property affected by the release. Based upon the inspection findings, the Permittee shall prevent further migration of the release to surrounding soils and surface waters. All contaminated media, structures, and equipment shall be properly managed at the direction of the MPCA. [Minn. R. 7045.0528, subp. 8(C)]

5.1.79 If there should be a leak of hazardous waste from the "tank system" (which is defined to include the tank, secondary containment system, and all ancillary equipment such as pumps, valves, monitoring equipment etc.), the Permittee shall notify the MPCA IMMEDIATELY after a release of hazardous waste to the environment if it is determined, based on the criteria in Minn. R. 7045.0528 and this Permit, that such notification is required. [Minn. R. 7045.0528, subp. 8(D)]

5.1.80 If there should be a leak of hazardous waste from the "tank system" (which is defined to include the tank, secondary containment system, and all ancillary equipment such as pumps, valves, monitoring equipment etc.), the Permittee shall evaluate the release and submit a written report to the MPCA WITHIN 15 DAYS after detection of a release requiring implementation of the contingency plan. This report must contain the following information and may be combined with the Post Emergency Report required by Minn. R. 7045.0470, subp. 3. 1) The likely route of migration of the release. 2) The characteristics of the surrounding soil, including soil composition, geology, hydrogeology, and climate. 3) The results of any monitoring or sampling conducted in connection with the release, if available. If sampling or monitoring is not available WITHIN 15 DAYS after detection of the release, the data must be submitted to the MPCA as soon as they become available. 4) The proximity to downgradient drinking water, surface water, and populated areas. 5) A description of response actions taken or planned. [Minn. R. 7045.0528, subp. 8(D)(2)]

5.1.81 If a leak from a tank should cause an emergency situation requiring implementation of the contingency plan, the Permittee shall follow the procedures specified in the "Emergency Procedures" section of this permit in addition to items 1 to 5 listed above. [Minn. R. 7045.0528, subp. 8]

5.1.82 The Permittee shall repair the tank secondary containment system in accordance with Minn. R. 7045.0528, subp. 8, items E and F. [Minn. R. 7045.0528, subp. 8(E and F)]

5.1.83 Upon evaluation of the 15 day written report required above, the Commissioner may require the Permittee to sample appropriate media (soil, surface water, groundwater, air) as necessary to determine


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the extent of contamination. Further, upon review of the sampling analysis, the Commissioner may

require the Permittee to submit a remediation plan for approval and to remediate the contaminated media affected by the release. Upon remediation, a final report summarizing remedial efforts taken shall be submitted to the Commissioner. [Minn. R. 7045.0528, subp. 8]

5.1.84 If there should be a leak of hazardous waste from a storage container, the Permittee shall IMMEDIATELY inspect the containers to determine which container or containers are leaking. Having identified the leaking container or containers, the Permittee shall contain the spill as soon as possible. Any leaking container and adjacent or affected area shall be inspected by the Permittee to determine the reason for the leak. The contents of the container shall be overpacked into another container and be managed in accordance with Minn. R. 7045.0526, subp. 6, item C. [Minn. R. 7045.0526]

5.1.85 If there should be a leak of hazardous waste from a storage container, spilled or leaked waste or inadvertent run-on must be removed from the secondary containment system in a timely manner. If the collected material (including spill containment equipment and debris/residue) is a hazardous waste, the Permittee must manage the material in accordance with Minn. R. 7045.0526, subp. 6.C. If the collected material is discharged through a point source to waters, Minn. R. 7045.0526, subp. 6.C., must be followed. [Minn. R. 7045.0526, subp. 6(C)]

5.1.86 If there should be a leak of hazardous waste from a storage container, the Permittee shall notify the MPCA IMMEDIATELY after any leak or spill of hazardous waste to the environment if it is determined, based on the criteria in 5.1.105, of this Permit, that such notification is required. [Minn. R. 7045.0526, subp. 6(C)]

5.1.87 If there should be a leak of hazardous waste from a storage container, the Post Emergency Reporting requirements of Minn. R. 7045.0466, subp. 3 should be consulted to determine if a written report is required. [Minn. R. 7045.0526, subp. 6(C)]

5.1.88 If there should be a leak of hazardous waste from a storage container, the MPCA may require the Permittee to sample appropriate media (soil, surface water, groundwater, air) as necessary to determine the extent of contamination. Further, upon review of the sampling analysis, the MPCA may require the Permittee to remediate the contaminated media affected by the release. Upon remediation, a final report summarizing remedial efforts taken shall be submitted for approval to the MPCA. [Minn. R. 7045.0526, subp. 6(C)]

5.1.89 If there should be a leak or spill of hazardous waste to the environment (escaping the secondary containment system) from any source at the Facility other than the tanks or containers in Permitted regulated units covered above, the Permittee shall comply with the following requirements: 1) The Permittee shall stop the leak or spill and clean up any released hazardous waste as soon as possible; 2) The Permittee must IMMEDIATELY conduct a visual inspection of the area around the leak or spill and prevent further migration of the leaked or spilled hazardous waste to soils and surface waters; 3) The Permittee shall notify the MPCA IMMEDIATELY after any leak or spill of hazardous waste to the environment if it is determined, based on the notification criteria in this Permit, that such notification is required; 4) In addition to the requirements in items 1-3 above, the Permittee shall follow the procedures specified in the Emergency Procedures requirements in this permit if the leak should require implementation of the contingency plan. [Minn. R. 7045.0466]

5.1.90 Minn. Stat. 115.061 and 116.061 require notification to the MPCA regarding discharges to water and air, respectively, for any materials, including hazardous waste. Minn. R. 7045.0468, subp. 5, item B, and subp. 6 also provide requirements for reporting to the Agency discharges of hazardous waste. Compliance under the notification requirements below satisfies the Agency notification requirements regarding releases of hazardous waste at permitted hazardous waste facilities for both the rules and statutes cited above.

All notifications required by items 3 and 5 below must be made to the Minnesota Duty Officer at one of the appropriate numbers provided below. Notification to the Minnesota Duty Officer satisfies the requirement for notifying the agency.

TWIN CITIES METRO AREA (AND OUTSIDE MINNESOTA): 651- 649-5451

GREATER MINNESOTA: 1-800-422-0798. [Minn. R. 7045.0468, subp. 5&6]

5.1.91 1) Except as provided in paragraph 2 below, it is the duty of every person to notify the Agency of the discharge, accidental or otherwise, of any substance or material under its control which, if not recovered, may cause pollution of waters of the State, and the responsible person shall recover as rapidly and thoroughly as possible such substance or material and take immediately such other action as may be reasonably possible to minimize or abate pollution of waters of the State caused thereby.

2) Notification is not required under paragraph 1 above for a discharge of five gallons or less of petroleum,


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as defined in section 115C.02, subd. 10. This paragraph does not affect the other requirements of

paragraph 1 above. [Minn. R. 7045]

5.1.92 The following actions constitute compliance with the Agency reporting requirements of Minn. Stat. § 115.061 and with Minn. R. 7045.0468, subp. 5, item B, and subp. 6 regarding discharges of hazardous waste, other than releases to air, at permitted hazardous waste facilities. The Minnesota Duty Officer must be notified immediately of any of the following discharges: 1) A fire, explosion, or discharge that could threaten human health or the environment outside the Facility; 2) A discharge to the secondary containment of a permitted unit that is NOT completely contained in the secondary containment and/or is NOT recovered in a timely manner; 3) All discharges to areas outside of the containment systems described in item 2 above, that could cause pollution of soil, surface water, or groundwater. [Minn. R. 7045.0468, subp. 5&6]

5.1.93 In accordance with Minn. Stat. 116.061, Subd. 1; a person who controls the source of an emission must notify the Agency immediately of excessive or abnormal unpermitted emissions that:

1) may cause air pollution endangering human health; 2) may cause air pollution damaging property; or 3) cause obnoxious odors constituting a public nuisance. If a person who controls the source of an emission has knowledge of an event that has occurred and that will subsequently cause an emission described in items 1, 2, or 3 above, the person must notify the Agency when the event occurs. [Minn. R. 7045.061, subd. 1]

5.1.94 In accordance with Minn. Stat. 116.061, Subd. 2; a person who is required to notify the Agency under Minn. Stat. 116.061, Subd. 1 must take immediate and reasonable steps to minimize the emissions or abate the air pollution and obnoxious odors caused by the emissions. [Minn. R. 7045.061, subd. 2]

5.1.95 In accordance with Minn. Stat. 116.061, Subd. 3; the following are exempt from the requirements of Minn. Stat. 116.061, Subd. 1 and 2: 1) emissions resulting from the activities of public fire services or law enforcement services; 2) emissions from motor vehicles, as defined in section Minn. Stat. 169.01, Subd. 3; 3) emissions from an agricultural operation deemed not a nuisance under section Minn. Stat. 561.19, subdivision Subd. 2; or 4) emissions from Agency regulated sources that are routine or authorized by the Agency. [Minn. R. 7045.061, subd. 3]

5.1.96 In accordance with Minn. Stat. 116.061, Subd. 4; a person who notifies the Agency of emissions under Minn. Stat. 116.061, Subd. 1 and who complies with Minn. Stat. 116.061, Subd. 2 shall not be subject to criminal prosecution under Minn. Stat. 115.071, subdivision 2. [Minn. R. 7045.061, subd. 4]

5.1.97 In accordance with Minn. Stat. 116.061, Subd. 5; any notice submitted under Minn. Stat. 116.061, Subd. 1 is not admissible in any proceeding as an admission of causation. [Minn. R. 7045.061, subd. 5]

5.1.98 Compliance with the statutory notification requirements above in 5.1.107 - 5.1.111, and the requirement in 5.1.105, constitutes compliance with the agency reporting requirements of Minn. R. 7045.0468, subp. 5. item B, and subp. 6 regarding discharges of hazardous waste to the air at permitted hazardous waste facilities. Notification must be provided for a fire, explosion, or discharge that could threaten human health or the environment outside the facility. [Minn. R. 7045.0468]

5.1.99 Note: For reporting requirements regarding discovery of "noncompliance" with a condition of this Permit which could endanger human health or the environment, please refer to 5.1.126 - 5.1.142, of this Permit. [Minn. R. 7045]

5.1.100 Whenever the contingency plan is implemented; the emergency coordinator shall IMMEDIATELY activate internal Facility alarms or communication systems. [Minn. R. 7045.0468, subp. 2]

5.1.101 Whenever the contingency plan is implemented; the emergency coordinator shall IMMEDIATELY identify the character, exact source, amount, and areal extent of any released material. [Minn. R. 7045.0468, subp. 3]

5.1.102 Whenever the contingency plan is implemented; the emergency coordinator shall IMMEDIATELY assess possible hazards to human health or the environment, considering both direct and indirect effects of the release, fire, explosion; effects from any toxic, irritating, or asphyxiating gases that are generated; and effects of any hazardous surface water run-off from water or chemical agents used to control fire and explosions. [Minn. R. 7045.0468, subp. 4]

5.1.103 Whenever the contingency plan is implemented; the emergency coordinator shall IMMEDIATELY carry out the appropriate provisions of the contingency plan set forth in the Permit Application. [Minn. R. 7045.0468, subp. 1]

5.1.104 If the emergency coordinator determines that the hazardous waste or hazardous constituent release, fire, or explosion could threaten human health or the environment, outside the Facility; or evacuation of local areas may be advisable; or a released hazardous waste or hazardous constituent may cause pollution of the air, land resources, or waters of the State, then the emergency coordinator shall IMMEDIATELY notify:


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1) Appropriate State and local authorities, 2) The governmental official designated as the on-scene

coordinator for that geographical area, or the National Response Center at (800) 424-8802. The information below shall be given to each of the above authorities at the time of the notification: 1) Name and telephone number of reporter, 2) Name and address of Facility, 3) Date, time, and type of incident, 4) Name and quantity of material involved, 5) Extent of damages or injuries, if any, and 6) The possible hazards to human health and/or the environment. [Minn. R. 7045.0468, subp. 5]

5.1.105 During an event that requires implementation of the contingency plan, the emergency coordinator shall ensure that releases, fires, and explosions do not occur, recur, or spread to other hazardous waste at the Facility. [Minn. R. 7045.0468, subp. 7]

5.1.106 If the Facility stops operations, the emergency coordinator shall monitor for leaks, pressure build-up, gas generation, or ruptures in valves, pipes, or other equipment, wherever this is appropriate. [Minn. R. 7045.0468, subp. 8]

5.1.107 IMMEDIATELY after an event that requires implementation of the contingency plan, the Permittee shall provide for treating, storing, or disposing of recovered waste, contaminated soil, groundwater, and any other contaminated material resulting from the emergency incident at the Facility, in a manner required by applicable laws and rules. [Minn. R. 7045.0470, subp. 1]

5.1.108 The Permittee shall not recommence operations after an emergency until the EPA, MPCA, and local police and fire departments have been notified and the Facility is in compliance with Minn. R. 7045.0470, subp. 2. [Minn. R. 7045.0470, subp. 2]

5.1.109 WITHIN 15 DAYS after an event that requires implementation of the contingency plan as required by Minn. R. 7045.0466, subp. 3, the Permittee shall submit a written report to the Agency describing the incident, containing information as required by Minn. R. 7045.0470, subp. 3. [Minn. R. 7045.0470, subp. 3]

5.1.110 The Permittee shall note in the operating record the time, date, and details of any incident that requires implementation of the contingency plan. [Minn. R. 7045.0470, subp. 3]

5.1.111 The Permittee shall maintain at the Facility at all times a copy of the most recent MPCA-approved version of a waste analysis plan as set forth in the Permit Application, and that meets the requirements of Minn. R. 7045.0458. [Minn. R. 7045.0458, subp. 2]

5.1.112 The Permittee shall maintain at the Facility at all times a copy of the most recent MPCA-approved version of a personnel training plan as set forth in the Permit Application, and that meets the requirements of Minn. R. 7045.0454. [Minn. R. 7045.0454]

5.1.113 The Permittee shall maintain at the Facility at all times a copy of the most recent MPCA-approved version of a contingency plan as set forth in the Permit Application, and that meets the requirements of Minn. R. 7045.0466. [Minn. R. 7045.0466]

5.1.114 The Permittee shall maintain at the Facility at all times a copy of the most recent MPCA-approved version of a closure plan as set forth in the Permit Application, and that meets the requirements of Minn. R. 7045.0486. [Minn. R. 7045.0486]

5.1.115 The Permittee shall maintain at the Facility at all times a copy of the most recent MPCA-approved version of an inspection plan as set forth in the Permit Application, and that meets the requirements of

Minn. R. 7045.0452, subp. 5. [Minn. R. 7045.0452, subp. 5]

5.1.116 The Permittee shall keep a written operating record at the Facility that contains the information in Minn. R. 7045.0478, including the following information: 1) The names of each hazardous waste generator and its EPA identification number; 2) The arrival date of incoming hazardous waste, and the shipment date of outgoing hazardous waste, corresponding with the transporter's name and identification number; 3) A description and statement of the quantity of each hazardous waste received, or shipped, and the method and date when stored. 4) The location of each hazardous waste shipment or container within the Facility and the total quantity of hazardous waste at each location. This information must be cross-referenced to the manifest accompanying the waste; 5) The records and results of each waste analysis performed; 6) The records and results of each inspection performed; 7) The results of any monitoring performed at the Facility; 8) Summary reports and details of all incidents which required implementation of the Contingency Plan; 9) All annual reporting requirements specified in this Permit; 10) All Land Disposal Restricted waste notifications required by Minn. R. 7045.1390, which incorporates by reference 40 CFR § 268.7, with the exceptions to incorporation listed in Minn. R. 7045.1390; and 11) A copy of the notices provided by the Permittee to each of the generators from whom the Permittee is obtaining hazardous wastes for storage at the Facility. [Minn. R. 7045.0478]

5.1.117 The Permittee shall maintain at the Facility at all times a copy of the job title for each position at the Facility related to hazardous waste management and the name of the employee filling each job. [Minn. R. 7045.0454, subp. 6]


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5.1.118 The Permittee shall maintain at the Facility at all times a copy of a written job description of each position

at the Facility related to hazardous waste management. This description may be consistent in its degree of detail with descriptions for other similar positions in the same company location or bargaining unit, but must include at least the requisite skill, education, or other qualifications and duties of employees assigned to each such position. [Minn. R. 7045.0454, subp. 6]

5.1.119 The Permittee shall maintain at the Facility at all times a copy of a written description of the type and amount of both introductory and continuing training in accordance with the Personnel Training Plan set forth in the Permit Application, that will be given to each person filling a hazardous waste position related to hazardous waste management. [Minn. R. 7045.0454, subp. 6]

5.1.120 The Permittee shall maintain at the Facility at all times a copy of records that document the training provided to each employee filling a position related to hazardous waste management.

[Minn. R. 7045.0454, subp. 7]

5.1.121 The Permittee shall record all inspections in an inspection log. These records must include the date and time of the inspection, the name of the inspector, a notation of the observations made, and the date and nature of any repairs or other remedial actions. [Minn. R. 7045.0478, subp. 3(G)]

5.1.122 The Permittee shall retain records of all monitoring information, including all calibration and maintenance records and all original strip chart recordings for continuous monitoring instrumentation, copies of all reports and records required by this Permit, and records of all data used to complete the Application for this Permit. [Minn. R. 7045.0150, subp. 2]

5.1.123 Records of monitoring information shall specify: 1) The date(s), exact place, and time(s) of sampling or measurements; 2) The individual(s) who performed the sampling or measurements; 3) The date(s) analyses were performed; 4) The individual(s) who performed the analyses; 5) The analytical techniques for methods used; and 6) The results of such analyses. [Minn. R. 7045.0150, subp. 2(B and C)]

5.1.124 The Permittee shall maintain all records for at least three (3) years after generation of the record unless the record is required by Minn. R. 7045.0478, subp. 3 or Minn. R. 7001.0720, subp. 2, item B to be kept for a longer period of time. Records required to be kept until closure of the Facility are listed in Minn. R. 7045.0478, subp. 3 and Minn. R. 7001.0720, subp. 2. These retention periods are automatically extended during the course of and at least for the duration of an unresolved enforcement action regarding the Permittee and shall also be extended upon request of the Agency. These records shall be made available to the Agency upon Request. [Minn. R. 7045.0478, subp. 3]

5.1.125 As used herein, the term "noncompliance" refers to any failure, intentional or unintentional, avoidable or unavoidable, to satisfy any requirement of this Permit. [Minn. R. 7045]

5.1.126 1) If the Permittee discovers that noncompliance with a condition of the Permit has occurred, which could endanger human health, public drinking water supplies, or the environment, the Permittee shall, WITHIN 24 HOURS after the discovery of the noncompliance, orally notify the Commissioner. WITHIN FIVE (5) DAYS of the discovery of the noncompliance, the Permittee shall submit to the Commissioner a written description of the noncompliance; the cause of the noncompliance; the exact dates of the period of noncompliance; and, if the noncompliance has not been corrected, the anticipated time it is expected to continue and steps taken or planned to reduce, eliminate, and prevent recurrence of the noncompliance. 2) For noncompliance occurrences not required to be reported above, the Permittee shall submit a written report to the Commissioner WITHIN 30 DAYS after the noncompliance is discovered. [Minn. R. 7045.0150, subp. 3(K)]

5.1.127 The Permittee shall give advance written notice to the Commissioner as soon as possible of any planned physical alteration of or addition to the Permitted Facility and of any activity that may result in noncompliance with its Permit or with any requirement of state or federal law. This notice does not relieve the Permittee of: 1) The requirement to obtain a modification of this Permit, or 2) Any liability for noncompliance with this Permit or the law. [Minn. R. 7001.0150, subp. 3(M)]

5.1.128 The Permittee shall certify each year at the time of submission of its annual report that a program is in place to reduce the volume and toxicity of waste and pollution to the maximum degree economically practicable, and that the method used to manage waste and pollution minimizes present and future threats to human health and the environment to the extent practicable as required by Minn.

R. 7045.0478, subp. 3.K. The program shall consist of a plan which includes these elements: 1) A policy statement articulating upper management support for eliminating or reducing the generation of waste and pollution at the facility; 2) A description of the current processes generating or releasing waste and pollution that specifically describes the types, sources, and quantities of waste and pollution currently being generated;


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3) A description of the current and past practices used to eliminate or reduce the generation of waste and

pollution and an evaluation of the effectiveness of these practices; 4) An assessment of technically and economically practicable options available to eliminate or reduce the generation of waste and pollution; 5) A statement of waste and pollution reduction objectives based on the assessment in item 4 above, and a schedule for achieving those objectives; 6) An explanation of the rationale for each waste and pollution reduction objective; and 7) A listing of options that were considered not to be economically and technically practicable. [Minn. R. 7045.0478, subp. 3(K)]

5.1.129 The Permittee shall pay the required annual facility fee as specified in Minn. R. 7046.0020. [Minn. R. 7045.0020]

5.1.130 All reports or other information required to be submitted to the Agency in accordance with the terms and conditions of this Permit shall carry the certification required by Minn. R. 7001.0070 and 7001.0540. [Minn. R. 7045.0540]

5.1.131 All written reports required to be submitted by the Permittee shall be sent to: Minnesota Pollution Control Agency Supervisor, Land Permits Unit Resource Management and Assistance Division 520 Lafayette Road North St. Paul, Minnesota 55155-4194. [Minn. R. 7045.0482]

5.1.132 If the Permittee decides to close all or a portion of the RCRA Facility, the Permittee shall close in accordance with the MPCA-approved closure plan in effect at the time. The present MPCA-approved closure plan is set forth in the Permit Application. The MPCA may require additional closure work plans to be developed if necessary to reflect Facility specific closure or partial closure activities to be conducted. [Minn. R. 7045.0486, subp. 3]

5.1.133 After receiving the final volume of hazardous waste at the Facility, the Permittee shall remove all hazardous wastes in accordance with the closure plan schedule in effect at the time, which shall not exceed 180 days unless approved by the Commissioner. The present closure schedule is detailed in the closure plan set forth in the Permit Application. [Minn. R. 7045.0488, subp. 1]

5.1.134 In July, 1998, TechLaw Inc., as contractor to EPA, conducted a Preliminary Assessment/Visual Site Inspection, a form of RCRA Facility Assessment, for the Facility. A total of six (6) Solid Waste Management Units (SWMUs) were identified. No Areas of Concern (AOCs) were identified. The SWMUs identified at the Facility were: 1. Operational area 2. Tertiary containment area 3. Waste container roll-off 4. Loading dock area and sump

5. Tank area spill containment trench 6. Solvent transfer area and sump. [Minn. R. 7045.0488, subp. 3]

5.1.135 The Permittee maintains that currently, there are no known releases of hazardous waste or constituents requiring corrective action from any solid or hazardous waste management units (as defined in Minn. R. 7045.0020, subp. 36a.) at the Facility. If any information becomes available concerning releases from solid or hazardous waste management units, the Commissioner will commence an action to modify this Permit to require the Permittee to undertake appropriate corrective action in accordance with Minn. R. 7045.0485. [Minn. R. 7045.0485]

5.1.136 Issuance of this Permit by the MPCA does not release the Permittee from any liability, penalty, or duty imposed by Minnesota or federal statutes, rules or local ordinances, except the obligation to obtain this Permit. [Minn. R. 7001.0150, subp. 3(A)]

5.1.137 Issuance of this Permit by the MPCA does not release the Permittee from or affect any liability which the Permittee may incur as a result of the operation of the Permitted Facility. [Minn. R. 7001.0150, subp. 3]

5.1.138 This Permit does not prevent the future adoption by the MPCA of pollution control rules, standards, or orders more stringent than those now in existence and does not prevent or affect the enforcement of these rules, standards, or any orders against the Permittee. [Minn. R. 7001.0150, subp. 3(B)]

5.1.139 This Permit does not convey a property right or an exclusive privilege. [Minn. R. 7001.0150, subp. 3(C)]

5.1.140 This Permit does not obligate the MPCA or the Commissioner to enforce laws, rules, or plans. [Minn. R. 7001.0150, subp. 3(D)]

5.1.141 This Permit authorizes the Permittee to perform the activities described in this Permit under the conditions of this Permit. In issuing this Permit, the State and Commissioner assume no responsibility for injury to persons or damage to property or the environment caused by the activities of the Permittee including those activities authorized, directed, or undertaken under this Permit. To the extent the State and Commissioner may be liable for the activities of State employees, that liability is explicitly limited to


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that provided in the Tort Claims Act, Minn. Stat. § 3.736. [Minn. R. 7001.0150, subp. 3(O)]

5.1.142 Compliance with the terms of this Permit does not constitute a defense to any action brought under Section 7003 of the Resource Conservation and Recovery Act, Section 106(a) of the Comprehensive Environmental Response, Compensation, and Liability Act of 1980 (42 U.S.C. 9601 et seq., commonly known as CERCLA), the Minnesota Environmental Response and Liability Act of 1983 (Minn. Stat. ch. 115B), Minn. Stat. chs. 116, 400, 473, or any other Minnesota or Federal statutes, rules or regulations, or local ordinances. [Minn. R. 7001.0150]

5.1.143 This Permit establishes minimum standards for the operation of the permitted Facility. Nothing in this Permit precludes the Permittee from taking additional steps to protect the public health or welfare or the environment so long as these additional steps are not inconsistent with the terms and conditions of this Permit. The Permittee is solely responsible for ensuring that the Permitted Facility adequately safeguards public health and welfare and the environment. [Minn. R. 7001.0150]

5.1.144 The Permittee shall perform the actions and conduct the activity authorized by this Permit in accordance with the plans and specifications approved by the MPCA and in compliance with the conditions of this Permit and applicable local, state, and federal hazardous waste laws, rules, ordinances, and regulations. [Minn. R. 7001.0150, subp. 3(E)]

5.1.145 In accordance with Minn. R. 7045.0478, subp. 3.K., the Permittee shall certify at least annually that it has a program in place to reduce the volume and toxicity of the waste and pollution to the maximum degree economically practicable, and that the method used to manage the waste and pollution minimizes present and future threats to human health and the environment to the extent practicable. [Minn. R. 7045.0478, subp. 3(K)]

5.1.146 The Permittee shall not knowingly make a false or misleading statement, representation, or certification in a record, report, plan or other document submitted to the MPCA or to the Commissioner. The Permittee shall IMMEDIATELY upon discovery report to the Commissioner an error or omission in any such record, report, plan, or other document. [Minn. R. 7001.0150, subp. 3(G)]

5.1.147 The Permittee shall, when requested by the Commissioner, submit within a reasonable time the information and reports that are relevant to the control of pollution, regarding the construction or operation of the Facility covered by this Permit, or regarding the conduct and the activity covered by this Permit, in accordance with Minn. Stat. §§ 115.04 and 116.07, subd. 9. [Minn. R. 7001.0150, subp. 3(H)]

5.1.148 When authorized by Minn. Stat. §§ 115.04, 115B.17, subd. 4, or 116.091, and upon presentation of proper credentials, the MPCA, or an authorized employee or agent of the MPCA, shall be allowed by the Permittee to examine and copy books, papers, records, or memoranda pertaining to the construction, modification, or operation of the Facility covered by this Permit or pertaining to the activity covered by this Permit. [Minn. R. 7001.0150, subp. 3(I)]

5.1.149 If the Permittee discovers, through any means, including notification by the MPCA, that noncompliance with a condition of the Permit has occurred, the Permittee shall promptly take all reasonable steps to minimize the adverse impacts on human health, public drinking water supplies, or the environment resulting from the noncompliance. [Minn. R. 7001.0150, subp. 3(J)]

5.1.150 Pursuant to Minn. R. 7045.0498. supb. 1, the Permittee, as an entity of the State of Minnesota, is exempt from the financial assurance and liability requirements of Minn. R. 7045.0498 to 7045.0524.

[Minn. R. 7045.0522, subp. 2]

5.1.151 This Permit may be modified, revoked and reissued, or revoked without reissuance for cause, as specified in Minn. R. 7001.0170 to 7001.0190 and Minn. R. 7001.0730. The filing of a request for a Permit Modification, Revocation and Reissuance, or Revocation without Reissuance, or the notification of planned changes or anticipated noncompliance on the part of the Permittee does not stay or affect the applicability or enforceability of a Permit condition. Requests for modification of plans or specifications integral to this Permit must be approved by the Commissioner prior to implementing the requested change. [Minn. R. 7001.0170]

5.1.152 If the Permittee wishes to continue an activity allowed by this Permit after the expiration date of this Permit, the Permittee shall submit a complete Application for reissuance of the Permit at least 180 calendar days before this Permit expires, unless written permission for a later date has been granted by the Commissioner. [Minn. R. 7001.0040, subp. 3]

5.1.153 This Permit will remain in effect beyond the Permit's expiration date if the Permittee has submitted a timely and complete Application for reissuance of the Permit provided that the Commissioner determines, based on available information, that all of the following are true: 1) The Permittee is in compliance with the terms and conditions of the expired Permit; 2) The Permittee continues at all times to work diligently and in good faith to meet the requirements and satisfy the concerns of the Commissioner with respect to the Permit Application; and 3) The Commissioner, through no fault of the Permittee, has not taken final action on the Application before the expiration date of this Permit. [Minn. R. 7001.0160]


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5.1.154 This Permit is not transferable to any person without the express written approval of the MPCA, and then

only after compliance with the requirements of Minn. R. 7001.0190 and 7045.0452, subp. 3. item D. A party to whom this Permit has been transferred shall comply with the terms and conditions of this Permit. [Minn. R. 7001.0190]

5.1.155 The provisions of this Permit are severable, and if any provision of this Permit, or the application of any provision of this Permit to any circumstance is held invalid, the application of such provision to other circumstances and the remainder of this Permit shall not be affected thereby. [Minn. R. 7001.0190]

5.1.156 The Permittee need not comply with the conditions of this Permit to the extent and for the duration that the noncompliance is authorized in an emergency Permit in accordance with Minn. R. 7001.0690. [Minn. R. 7001.0690]

5.1.157 The Permittee may allow an authorized representative to sign reports submitted in accordance with the requirements of this Permit in accordance with the conditions of Minn. R. 7001.0720, subp. 2, item F. [Minn. R. 7001.0720, subp. 2(F)]

5.1.158 The review of each submittal, document, report, or schedule (collectively referred to hereafter as "submittal") which is required to be submitted to the Commissioner for review and approval shall be as follows: 1) The Commissioner shall review each submittal made by the Permittee as required by this Permit. In the event the submittal is approved, it shall become an integral and enforceable part of this Permit. If the submittal is disapproved in whole or part, the Commissioner shall notify the Permittee in writing and shall explain the amendments or revisions that are necessary to bring the submittal into compliance with this Permit. 2) Within 30 calendar days of receipt of any notice of disapproval or modification, or on the first working day thereafter (if said 30th day fell on a Sunday or Holiday) the Permittee shall: a. Submit revisions to correct inadequacies that led to disapproval, or, b. State in writing the reasons why the submittal, as originally submitted, should be approved. The Permittee may have longer than 30 days to respond if the longer time period is specified in the Commissioner's review letter referenced in paragraph 1 above. 3) If, within 30 calendar days from the date of the Permittee submission under paragraph 2, above, the parties have not reconciled all issues with respect to the submittal, the Commissioner shall inform the Permittee of the second disapproval of the submittal and whether in the Commissioner's view, the Permittee may be in violation of the Permit. In such event, the matter may be referred for enforcement action. 4) The Commissioner and the Permittee shall provide the opportunity to consult with each other during the review of submittals or modifications. [Minn. R. 7001.0090]

5.1.159 All time extensions must be requested by the Permittee in writing. The requests shall specify the reasons why the extension is needed. Extensions shall only be granted for such a period of time as the Commissioner determines is reasonable under the circumstances. A requested extension shall not be effective until approved by the Commissioner. The burden shall be on the Permittee to demonstrate to the satisfaction of the Commissioner that the request for the extension has been submitted in a timely fashion and that good cause exists for granting the extension and that the extension shall have no adverse effect upon human health or the environment. Extension of compliance schedule dates provided in this Permit may be granted if requests are submitted in a timely fashion and good cause exists for granting the extension, and if the extension would have no adverse effect upon human health or the environment. [Minn. R. 7001.0090]

5.1.160 The Permittee shall comply with all applicable land disposal restrictions in Minn. R. 7045.1390, which incorporates by reference 40 CFR pt. 268, with the exceptions to incorporation listed in Minn. R. 7045.1390 and 7045.0090. All of the land disposal requirements of Minn. R. 7045.1390 are subject to the exceptions to incorporation listed in Minn. R. 7045.1390 and Minn. R. 7045.0090. [Minn. R. 7045.1390]

5.1.161 A mixture of any restricted waste with any nonrestricted waste is a restricted waste under 40 CFR § 268.1. [Minn. R. 7045.1390]

5.1.162 The Permittee shall not in any way dilute a restricted waste or the residual from treatment of a restricted waste as a substitute for adequate treatment to achieve compliance with the treatment standards in 40 CFR pt. 268, subp. D, to circumvent the effective date of a prohibition in 40 CFR pt. 268, subp. C, to otherwise avoid compliance with a prohibition in 40 CFR pt. 268, subp. C, or to circumvent a land disposal prohibition imposed by Section 3004 of RCRA. [Minn. R. 7045.1390]

5.1.163 The Permittee shall prepare and maintain a current list of the hazardous waste codes for all wastes handled at the Facility that are identified or listed in 40 CFR § 268.20-.39 . The list shall include all wastes and waste codes handled at the Facility, and any associated treatment standards, and shall be updated through the inclusion of new treatment standards, as promulgated or amended. This list shall be provided to the MPCA representative, or its designees, upon request. [Minn. R. 7045.1390]

5.1.164 The Permittee shall test, in accordance with 40 CFR § 268.7, any waste generated at the Facility, or use knowledge of the waste, to determine if the waste is restricted from land disposal. [Minn. R. 7045.1390]


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5.1.165 For restricted wastes with treatment standards expressed as concentrations in the waste extract, as

specified in 40 CFR § 268.40, the Permittee shall test the treatment residues, or an extract of such residues developed using the test methods described in 40 CFR § 268.40(b) (Method 1311, Toxicity Characteristic Leaching Procedure or TCLP) to assure that the treatment residues or extract meet the applicable treatment standards of 40 CFR § 268.40. Such testing shall be performed pursuant to the requirements of Minn. R. 7045.0458. [Minn. R. 7045.1390]

5.1.166 A restricted waste for which a treatment technology is specified in 40 CFR § 268.42 may be land disposed after it is adequately treated using that specified technology or an equivalent treatment method approved by the EPA under the procedures set forth in 40 CFR § 268.42. [Minn. R. 7045.1390]

5.1.167 For restricted wastes with treatment standards expressed as concentrations in the waste, as specified in 40 CFR § 268.40, the Permittee shall test the treatment residues (not an extract of such residues) to assure that the treatment residues meet the applicable treatment standards of 40 CFR § 268.40. Such testing shall be performed as required by 40 CFR § 268.40. [Minn. R. 7045.1390]

5.1.168 The Permittee shall comply with all the applicable prohibitions on storage of restricted wastes specified in 40 CFR § 268.50. [Minn. R. 7045.1390]

5.1.169 The Permittee may store restricted wastes in tanks and containers solely for the purpose of the accumulation of such quantities of hazardous wastes as necessary to facilitate proper recovery, treatment, or disposal provided that: 1) Each container is clearly marked to identify its contents and the date each period of accumulation begins; 2) Each tank is clearly marked with a description of its contents, the quantity of each hazardous waste received, and the date each period of accumulation begins, or such information for each tank is recorded and maintained in the operating record at the Facility. [Minn. R. 7045.1390]

5.1.170 The Permittee may store restricted wastes for up to one (1) year unless the MPCA can demonstrate that such storage was not solely for the purpose of accumulating such quantities of hazardous waste as are necessary to facilitate proper recovery, treatment or disposal. [Minn. R. 7045.1390]

5.1.171 The Permittee may store restricted wastes beyond one (1) year provided that the Permittee proves that such storage was solely for the purpose of accumulating such quantities of hazardous waste as are necessary to facilitate proper recovery, treatment or disposal. [Minn. R. 7045.1390]

5.1.172 The Permittee shall not store any liquid hazardous waste containing polychlorinated biphenyls (PCBs) at concentrations greater than or equal to 50 ppm unless the waste is stored in a storage facility that is a commercial storer of PCB waste as defined in 40 CFR § 761.3. This waste must be removed from storage and treated or disposed within one (1) year of the date when such wastes are first put into storage. The requirement above, which allows storage for over one (1) year with specified demonstration, does not apply to PCB wastes. [Minn. R. 7045.1390]

5.1.173 The Permittee must not dilute metal-bearing wastes (listed in Appendix XI of 40 CFR Part 268), if the diluted waste will be used as fuel in any RCRA permitted facility, unless you have demonstrated that the diluted waste complies with one or more of the criteria specified in 40 CFR § 268.3(c). [40 CFR 268.1390]

5.1.174 The Permittee shall comply with all applicable requirements of Minn. R. 7045.0549, regarding air emissions from process vents. [Minn. R. 7045.0549]

5.1.175 The Permittee shall mark each piece of equipment to which 40 CFR pt. 264, subp. BB applies in such a manner that it can be distinguished readily from other piece of equipment. [Minn. R. 7045.0551]

5.1.176 The Permittee shall determine each hazardous waste stream for which: (1) the hazardous waste is "in light liquid service" as defined in 40 CFR § 264.1031 and (2) the hazardous waste has an organic concentration of at least 10 percent by weight. The Permittee shall manage all "in light liquid service" and that compliance with pumps in light liquid service under 40 CFR § 264.1052 as required. [Minn. R. 7045.0551]

5.1.177 The Permittee shall comply with all applicable requirements of 40 CFR § 264.1050 through § 264.1065, regarding air emission standards for equipment leaks. [Minn. R. 7045.0551]

5.1.178 Each sampling connection system, except in-situ sampling systems and sampling systems without purges, shall be equipped with a closed-purge, closed-loop, or closed-vent system which meets one of the following requirements: 1) Return the purged process fluid directly to the process line; 2) Collect and recycle the purged process fluid; or 3) Be designed and operated to capture and transport all the purged process fluid to a waste management unit that complies with applicable sections of 40 CFR § 264.1084 through § 264.1086 or a control device that complies with 40 CFR § 264.1060, Standards for Closed-Vent Systems and Control Devices. [Minn. R. 7045.0551]

5.1.179 Each open-ended valve or line must be equipped with a:

1) cap; 2) blind flange; 3) plug; or


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4) second valve, which seals the open-end at all times except during operations requiring hazardous waste

stream flow through the open-end valve or line. [Minn. R. 7045.0551]

5.1.180 When a double block and bleed system is used, the bleed valve or line may remain open during operations that require venting the line between the block valves but shall seal the open-end at all other times. The unit shall be conducted in accordance with equipment leaks hereinafter specified. [Minn. R. 7045.0551]

5.1.182 Conduct monthly monitoring to detect leaks as required by 40 CFR § 264.1063(b) and as described in the Section D-18 of Part B Application. [Minn. R. 7045.0551]

5.1.183 Perform visual inspection each calendar week for indications of liquids dripping from the pump seal. [Minn. R. 7045.0551]

5.1.184 Pumps and valves in heavy liquid service, pressure relief devices in light liquid or heavy liquid service, and flange and other connectors shall be monitored within five (5) days by the method specified in 40 CFR § 264.1063(b) if evidence of a potential leak is found by visual, audible, olfactory, or any other detection method. [Minn. R. 7045.0551]

5.1.185 A leak is detected if an instrument reading is measured at or greater than 10,000 ppm. [Minn. R. 7045.0551]

5.1.186 1) When a leak is detected, the Permittee shall repair the leak as soon as practicable, but no later than 15 calendar days after it is detected, except as provided in 40 CFR § 264.1059. The first attempt at repair shall be made no later than 5 calendar days after each leak is detected. 2) First attempts at repair at repair include, but are not limited to, the best practices described in 40 CFR § 264.1057(e). [Minn. R. 7045.0551]

5.1.187 Delay of repair of equipment for which leaks have been detected will be allowed if: 1) The repair is technically infeasible without a hazardous waste management unit shutdown; or 2) The equipment that is isolated from the hazardous waste management unit and does not continue to contain or contact hazardous waste with organic concentration at least 10 % by weights. [Minn. R. 7045.0551]

5.1.188 Delay of repair for pumps will be allowed if: 1) Emissions of purged material resulting from immediate repair are greater than the emissions likely to result from delay of repair; and 2) When repair procedures are effected, the purged material is collected and destroyed or recovered in a control devices complying with 40 CFR § 264.1060. [Minn. R. 7045.0551]

5.1.189 Delay of repair for pumps will be allowed if: 1) repair requires the use of a dual mechanical seal system that includes a barrier fluid system; and 2) repair is completed as soon as practicable, but not later than six (6) months after the leak was detected. [Minn. R. 7045.0551]

5.1.190 Delay of repair beyond a hazardous waste management unit shutdown will be allowed for a valve if it meets the provisions of 40 CFR § 264.1059(e). [Minn. R. 7045.0551]

5.1.191 The leak test methods and procedures shall be as specified in 40 CFR § 264.1063. [Minn. R. 7045.0551]

5.1.192 When each leak is detected as specified in 40 CFR §§ 264.1052, 264.1053, 264.1057 or 264.1058, the Permittee shall comply with the following requirements: 1) A weatherproof and readily visible identification, marked with the equipment identification number, the date evidence of potential leak was found in accordance with 40 CFR § 264.1058(a), and the date the leak was detected, shall be attached to the leaking equipment. 2) The identification on equipment as herein specified, except valves, may be removed after it has been repaired; 3) The identification on valve may be removed after it has been monitored for two (2) successive months as specified in 40 CFR § 264.1057(c) and no leak has been detected during those two (2) months.

[Minn. R. 7045.0551]

5.1.193 The Permittee shall record the following information in the facility operating record: 1) Equipment identification number and hazardous waste management unit identification; 2) Approximate locations within the facility; 3) Type of equipment (e.g., a pump or pipeline valve); 4) Percent-by-weight total organics in the hazardous waste stream at the equipment; 5) Hazardous waste state at the equipment (e.g., liquid); and 6) Method of compliance with the standard. [Minn. R. 7045.0551]

5.1.194 The Permittee shall record the following information in an inspection log which shall be kept in the facility operating record when each leak is detected as specified in 40 CFR §§ 264.1053, 264.1057 and 264.1058: 1) The instrument and operator identification numbers and the equipment identification number; 2) The date evidence of a potential leak was found in accordance with 40 CFR § 264.1058(a); 3) The date the leak was detected and the dates of each attempt to repair the leak;


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4) Repair methods applied in each attempt to repair the leak;

5) "Above 10,000" if the maximum instrument reading measured by the methods specified in 40 CFR § 264.1063(b) after each repair attempt is equal to or greater than 10,000 ppm; 6) "Repair delayed" and the reason for the delay if a leak is not repaired within 15 calendar days after discovery of the leak;

7) Documentation supporting the delay of repair of a valve in compliance with 40 CFR § 264.1059(c); 8) The signature of the owner or operator (or designate) whose decision it was that repair could not be effected without a hazardous waste management unit shutdown;

9) The expected date of successful repair of the leak if a leak is not repaired within 15 calendar days; and 10) The date of successful repair of the leak. [Minn. R. 7045.0551]

5.1.197 The Permittee shall notify the MPCA of any waste management units which become subject to the requirements of Minn. R. 7045.0551, within 30 day of startup of the regulated activity. [Minn. R. 7045.0551]

5.1.198 The Permittee must comply with all applicable requirements of Minn. R. 7045.0540, which incorporates by reference 40 CFR § 264.1080 through 40 CFR § 264.1090, with the exceptions to incorporation listed in Minn. R. 7045.0540, subp. 2 and Minn. R. 7045.0090 regarding air emission standards for containers and tanks handling hazardous waste. All containers not exempt from 40 CFR pt. 264, subp. CC must be managed using Level 1 control or Level 2 control as appropriate. The Permittee must not manage hazardous waste in tanks which require Level 2 control. The Permittee must not conduct any waste stabilization process, as defined in 40 CFR § 265.1081, in containers and tanks. [Minn. R. 7045.0528, subp. 12]

5.1.199 In accordance with the procedures specified in 40 CFR § 264.1083, the Permittee must determine the average volatile organic (VO) concentration of: 1) generated hazardous waste at the point of origination, and 2) treated hazardous waste. The Permittee must determine the maximum organic vapor pressure of a hazardous waste. [40 CFR 264.1083]

5.1.200 The Permittee must manage hazardous waste with a VO concentration of 500 parts per million and greater by weight (ppmw) in containers with Container Level 1 standards as stipulated under 40 CFR § 264.1086(c). The hazardous waste stored in Level 1 containers must meet the following requirements.

a. Unless all containers are treated as Level 2 containers, they must be stored in a separate area or clearly marked to avoid potential mix up with the Level 2 containers.

b. Containers with a design capacity equal to or greater than 0.46 meter cube (m3) (122 gallons) shall not be used in light material service as defined in 40 CFR § 265.1081.

c. A Level 1 container must: 1) Meet the applicable U.S. Department of Transportation (DOT) regulations as specified in 40 CFR § 264.1086(f), 2) Be equipped with a cover and closure devices with an acceptable tightness and construction materials in accordance with 40 CFR § 264.1086(c)(1)(ii), or 3) Be an open-top container with organic vapor suppressing barrier to prevent hazardous waste from being exposed to the atmosphere as specified in 40 CFR § 264.1086(c)(1)(iii).

Containers, which meet the requirements of Condition D.2.c.2) or 3), must be equipped with covers and enclosures suitable for the physical and chemical characteristics of hazardous waste in containers, maintaining container integrity throughout the life of the container, and the environments under which the containers are placed in the storage facility. Any chemical used for vapor suppression must not generate heat and/or fume and must be compatible with the hazardous waste in the container. Vapor suppression chemicals must act as an acceptable and stable barrier to the hazardous waste, thus preventing releases of VO concentration into the environment. The barrier shall not chemically react to the hazardous waste. [40 CFR § 264.1086(c)(2)]

d. All covers and closure devices must be in closed position whenever hazardous waste is in a container. Opening of a closure device or cover is allowed if it meets the purpose and operates as defined in 40 CFR § 264.1086(c)(3)(i) through (v).

e. The Permittee must inspect the containers and their covers and closure devices in accordance with 40 CFR § 264.1086(c)(4). 40 CFR 264]

5.1.201 Containers with a design capacity greater than 0.46 m3 and in light material service must be managed and meet the requirements of Container Level 2 standards per 40 CFR § 264.1086(d). a. Emission control. Containers must meet one of the following: 1) The applicable U.S. Department of Transportation regulations and 40 CFR § 264.1086(f) for the purpose


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of compliance,

2) Operate with no detectable organic emissions as defined in 40 CFR § 265.1081 and determined in accordance with 40 CFR § 264.1086(g), or 3) Be vapor tight within the preceding 12 months by using 40 CFR Part 60, Appendix A, Method 27. [40 CFR § 264.1086(d)(1)] b. Transfer of hazardous waste in or out of a container must be conducted using an engineered method generally accepted and practiced by the industry, or its equivalent method to minimize the release of organics into the atmosphere. [40 CFR § 264.1086(d)(2)] c. All covers and closure devices must be in closed position whenever hazardous waste is in a container. Opening of a closure device or cover is allowed if it meets the purpose and operates as defined in 40 CFR § 264.1086(d)(3)(i) through (v). d. The Permittee must inspect the containers and their covers and closure devices in accordance with 40 CFR § 264.1086(d)(4). [Minn. R. 7045.0526, subp. 10]

5.1.202 Each tank storing hazardous waste with a VO concentration equal or greater than 500 ppmw must comply with the following: The design capacity of each tank must be less than 75 m3 and the maximum vapor pressure, as determined by 40 CFR § 264.1083(c)(2), must be less than 76.6 kilopascal (kPa).

The hazardous waste in the tank shall not be heated to a temperature that is greater than the temperature at which the maximum vapor pressure of 76.6 kPa is determined.

The hazardous waste in the tank shall not be treated by any waste stabilization process as defined in 40 CFR § 265.1081.

The Permittee must comply with Level 1 control requirements in accordance with 40 CFR § 264.1084. Each tank must be a fixed roof design complying with the following specifications:

The fixed roof tank shall be of butt and/or lap welded construction throughout and shall, upon initial installation, be hydraulically and/or air tested to the maximum working pressure without leaks according to standards set forth by the American Petroleum Institute (API), American Standard for Testing Materials (ASTM) standards, or other appropriate standard engineering codes and standards.

The tank closure devices must be designed and constructed to form a continuous barrier over the entire surface area of the hazardous waste in the tank. Gaskets used for closure devices or piping systems shall be of suitable materials compatible with the hazardous wastes and shall be in accordance with good engineering practices.

Each opening in the fixed roof and any manifold system associated with the fixed roof shall be either:

1) Equipped with a closure device designed to operate such that when the closure device is secured in the closed position there are no visible cracks, holes, gaps, or other open spaces in the closure device or between the perimeter of the opening and the closure device, or

2) Connected by a closed-vent system that is vented to a control device. [40 CFR § 264.1084(c)(2)(iii)]

The control device shall remove or destroy organics in the vent stream, and shall be operating whenever hazardous waste is managed in the tank, except during periods when it is necessary to provide access to the tank for performing routine inspections, maintenance, or other activities needed for normal operations, and for removal of accumulated sludge or other residues from the bottom of the tank.

Whenever a hazardous waste is in the tank, all openings (e.g., manholes, instruments connections, pipe nozzles) must be securely closed to prevent releases of vapors into the atmosphere, except for routine inspections, and maintenance. (40 CFR § 264.1084(c)(3))

The Permittee must inspect the tanks, at least once per year, or retest the tanks to ascertain that the air emissions from the tank systems comply with the design and with the requirements stipulated in 40 CFR § 1084(c)(4).

You must process a Class 1 permit modification and obtain an approval from the Director, if the Permittee plans to operate or to modify the tank systems for complying with Level 2 control. [Minn. R. 7045.0528, subp. 12]


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5.1.203 Each tank requiring Level 2 control shall be covered by a fixed roof and vented directly through a

closed vent system to a control device in accordance with the requirements stipulated under 40 CFR § 264.1084(g)(1)(i) through § 264.1084(g)(1)(iv). Whenever a hazardous waste is in the tank, the fixed roof shall be installed with each closure device secured in the closed position and the vapor headspace underneath the fixed roof vented to the control device except under those conditions specified in 40 CFR § 264.1084(g)(2)(i) and (ii). The Permittee must inspect and monitor the air emission control equipment in accordance with the requirements stipulated under 40 CFR § 264.1084(g)(3). The closed vent system and control device shall be designed and operated in accordance with the requirements of 40 CFR § 264.1087. [40 CFR 264]

5.1.204 Closed-vent systems and control devices shall comply with the provisions of 40 CFR §§ 264.1033, 264.1060 and 264.1087. Each tank shall be equipped with inert gas blanketing, a spring-loaded pressure-relief valve closure device, a closed-vent system, and a control device. The inert gas blanketing must be supplied from a centrally located nitrogen supply system with a complete piping and instrumentation system to each tank. The closed-vent and control device shall meet the requirements of 40 CFR § 264.1087 and shall include: Vent Piping & Carbon System The vent control device shall reduce the total organic content of the inlet vapor stream vented to the control device by at least 95 percent by weight in accordance with 40 CFR § 264.1087(c)(1)(i). The closed-vent system and the control device shall comply with the following requirements:

The Carbon Adsorption System shall have a minimum removal efficiency of 95 percent in accordance with 40 CFR §264.1033(h).

The Carbon Adsorption System shall be inspected and monitored in accordance with 40 CFR § 264.1088 by detector types (e.g., flame ionization, photoionization, infrared absorption) that meet the requirements specified in 40 CFR pt. 60, Appendix A, Method 21, or an alternative analytical method per 40 CFR § 264.1033(i).

If breakthrough is greater than 5 percent of organic concentration of the input concentration, the filter will be replaced or removed completely. The filter will be replaced once every five year, if no breakthrough is detected, or removed completely.

After the Carbon Adsorption System beds are spent, the spent carbon must be treated/disposed of in a RCRA permitted TSD facility. All spent carbon removed from the control devices shall be handled as a hazardous waste.

The closed vent system shall not include any bypass devices that could be used to divert the gas or vapor stream to the atmosphere before entering the control device.

Periods of planned routine maintenance of the control device, during which the control device does not meet the control efficiency required under Condition D.6.f.3) shall not exceed 240 hours per year.

Malfunctions of the control device must be corrected as soon as practicable after their occurrence to minimize emissions of air pollutants. (40 CFR § 264.1087(c)(2)(v))

Compliance with IV.D.6. shall be demonstrated by recording the information specified in 40 CFR § 1089(e)(1)(v), Recordkeeping Requirements. [40 CFR 264]

5.1.205 Under this permit, the Permittee must demonstrate by direct measurement or approved method that for each container and tank the Permittee claims to be exempt under Subpart CC, the average VO concentration for hazardous waste, determined in accordance with 40 CFR §§ 264.1083(a) and 265.1084(a)(2) and (3), is less than 500 ppmw. [Minn. R. 7045.0540]

5.1.206 For each container and tank, the Permittee must review and update this determination in accordance with 40 CFR § 264.1082(c)(1) at least once every 12 months following the date of the initial determination. For each container or tank, the Permittee must prepare and maintain the records described in 40 CFR

§ 264.1089(f). These records must be maintained as part of the operating record. [Minn. R. 7045.0540]


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6. Submittal/action requirements

Total Facility Serial

Number Permit Condition

6.1.1 The Permittee shall submit an annual report: Due annually, by the 1st of March of each year, for the previous calendar year. The annual report must include the information required by Minn. R. 7045.0482, subp. 2. [Minn. R. 7045.0482, subp. 1]

6.1.2 The Permittee shall notify the agency of full or partial closure: Due 45 calendar days before Closure Date prior to the expected date of commencement of full or partial closure of the Facility. The written notice shall include: 1) The anticipated last day of operation; 2) The existing inventory count and inventory reduction schedule; and 3) A discussion of how conditions of this Permit and state and federal law will be met. [Minn. R. 7045.0486, subp. 5]

6.1.3 The Permittee shall submit certification: Due 60 calendar days after Closure is Completed Date submit to the Commissioner a certification signed by the Permittee and by an independent registered professional engineer that the Facility has been closed in accordance with the MPCA approved closure plan and any additional closure work plans if developed. The certification shall contain language as stated in Minn. R. 7001.0070 and 7001.0540. [Minn. R. 7045.0488, subp. 4]

6.1.4 The Permittee shall notify the agency of bankruptcy: Due 10 calendar days after Commencement of Bankruptcy Proceedings Date by certified mail of the commencement of a voluntary or involuntary proceeding under United States Code, Title 11, Bankruptcy, naming the Permittee as debtor.

[Minn. R. 7045.0522, 1]

6.1.5 The Permittee shall submit an application for permit reissuance: Due 180 calendar days before Permit Expiration Date. [Minn. R. 7001.0040, 3]


EPA ID# MN0000981415 of 50

7. Appendix

Approved Hazardous Waste Codes


EPA ID# MN0000981415 of 50

Waste Code

CAS Number Chemical Name

D004 7440-38-2 Arsenic

D005 7440-39-3 Barium

D018 71-43-2 Benzene

D006 7440-43-9 Cadmium

D019 56-23-5 Carbon tetrachloride

D020 57-74-9 Chlordane

D021 108-90-7 Chlorobenzene

D022 67-66-3 Chloroform

D007 7440-47-3 Chromium

D023 95-48-7 o-Cresol

D024 108-39-4 m-Cresol

D025 106-44-5 p-Cresol

D026 - Cresol

D016 94-75-7 2,4-D

D027 106-46-7 1,4-Dichlorobenzene

D028 107-06-2 1,2-Dichloroethane

D029 75-35-4 1,1-Dichloroethylene

D030 121-14-2 2,4-Dinitrotoluene

D012 72-20-8 Endrin

D031 76-44-8 Heptachlor (and its epoxide)

D032 118-74-1 Hexachlorobenzene

D033 87-68-3 Hexachlorobutadiene

D034 67-72-1 Hexachloroethane

D008 7439-92-1 Lead

D013 58-89-9 Lindane

D009 7439-97-6 Mercury

D014 72-43-5 Methoxychlor

D035 78-93-3 Methyl ethyl ketone

D036 98-95-3 Nitrobenzene

D037 87-86-5 Pentrachlorophenol

D038 110-86-1 Pyridine

D010 7782-49-2 Selenium

D011 7440-22-4 Silver

D039 127-18-4 Tetrachloroethylene

D015 8001-35-2 Toxaphene

D040 79-01-6 Trichloroethylene

D041 95-95-4 2,4,5-Trichlorophenol

D042 88-06-2 2,4,6-Trichlorophenol

D017 93-72-1 2,4,5-TP (Silvex)

D043 75-01-4 Vinyl chloride

D001 - Ignitability

D002 - Corrosivity


EPA ID# MN0000981415 of 50

D003 - Reactivity

MN01 - Minnesota Lethality

MN02 - Lab Pack Waste

MN03 - Polychlorinated Biphenyl Waste

MN04 - Used Oil not Managed for Recycling

F001

-

The following spent halogenated solvents used in degreasing: Tetrachloroethylene, trichlorethylene, methylene chloride, 1,1,1- trichloroethane, carbon tetrachloride and chlorinated fluorocarbons; all spent solvent mixtures/blends used in degreasing containing, before use, a total of ten percent or more (by volume) of one or more of the above halogenated solvents or those solvents listed in F002, F004, and F005; and still bottoms from the recovery of these spent solvents and spent solvent mixtures.

F002

-

The following spent halogenated solvents: Tetrachloroethylene, methylene chloride, trichloroethylene, 1,1,1-trichloroethane, chlorobenzene, 1,1,2- trichloro- 1,2,2-trifluoroethane, ortho-dichlorobenzene, trichlorofluoromethane, and 1,1,2- trichloroethane; all spent solvent mixtures/blends containing, before use, a total of ten percent or more (by volume) of one or more of the above halogenated solvents or those solvents listed in F001, F004, and F005; and still bottoms from the recovery of these spent solvents and spent solvent mixtures.

F003

-

The following spent non-halogenated solvents: Xylene, acetone, ethyl acetate, ethyl benzene, ethyl ether, methyl isobutyl ketone, n-butyl alcohol, cyclohexanone, and methanol; all spent solvent mixtures/blends containing, before use, only the above spent non-halogenated solvents; and all spent solvent mixtures/blends containing, before use, one or more of the above non- halogenated solvents, and a total of ten percent or more (by volume) of one or more of those solvents listed in F001, F002, F004, and F005; and still bottoms from the recovery of these spent solvents and spent mixtures.

F004

-

The following spent non-halogenated solvents: cresols, cresylic acid, and nitrobenzene; all spent solvent mixtures/blends containing, before use, a total of ten percent or more (by volume) of one or more of the above non- halogenated solvents or those solvents listed in F001, F002, and F005; and still bottoms from the recovery of these spent solvents and spent solvent mixtures.

F005

-

The following spent non-halogenated solvents: toluene, methyl ethyl ketone, carbon disulfide, isobutanol, pyridine, benzene, 2-ethoxyethanol, and 2- nitropropane; all spent solvent mixtures/blends containing, before use, a total of ten percent or more (by volume) of one or more of the above non- halogenated solvents or those solvents listed in F001, F002 or F004; and still bottoms from the recovery of these spent solvents and spent solvent mixtures.


EPA ID# MN0000981415 of 50

F020

-

Wastes (except wastewater and spent carbon from hydrogen chloride purification) from the production or manufacturing use (as a reactant, chemical intermediate, or component in a formulating process) or tri- or tetrachlorophenol or of intermediates used to produce their pesticide derivatives. (This listing does not include wastes from the production of hexachlorophene from highly purified 2,4,5-trichlorophenol.)

F021

-

Wastes (except wastewater and spent carbon from hydrogen chloride purification) from the production or manufacturing use (as a reactant, chemical intermediate, or component in a formulating process) of pentachlorophenol, or of intermediates used to produce derivatives.

F024

-

Process wastes including, but not limited to, distillation residues, heavy ends, tars, and reactor clean-out wastes, from the production of certain chlorinated aliphatic hydrocarbons by free radical catalyzed processes. These chlorinated aliphatic hydrocarbons are those having carbon chain lengths ranging from one to and including five, with varying amounts and positions of chlorine substitution. (This listing does not include wastewaters, wastewater treatment sludges, spent catalysts, and waste listed in Sections 261.31 or 261.32)

F025

-

Condensed light ends, spent filters and filter aids, and spent desiccant wastes from the production of certain chlorinated aliphatic hydrocarbons, by free radical catalyzed processes. These chlorinated aliphatic hydrocarbons are those having carbon chain lengths ranging from one, to and including five, with varying amounts and positions of chlorine substitution.

F027 58-90-2 2,3,4,6-Tetrachlorophenol

F027 93-76-5 2,4,5-T

F027 95-95-4 2,4,5-Trichlorophenol

F027 88-06-2 2,4,6-Trichlorophenol

F027 93-76-5 Acetic acid, (2,4,5-trichlorophenoxy)-

F027

-

Discarded unused formulations containing tri-, tetra-, or pentachlorophenol or discarded unused formulations containing compounds derived from these chlorophenols. (This listing does not include formulations containing hexachlorophene synthesized from prepurified 2,4,5-trichlorophenol as the sole component.)

F027 87-86-5 Pentachlorophenol

F027 58-90-2 Phenol, 2,3,4,6-tetrachloro-

F027 95-95-4 Phenol, 2,4,5-trichloro-

F027 88-06-2 Phenol, 2,4,6-trichloro-

F027 87-86-5 Phenol, pentachloro-

F027 93-72-1 Propanoic acid, 2-(2,4,5-trichlorophenoxy)-

F027 93-72-1 Silvex (2,4,5-TP)


EPA ID# MN0000981415 of 50

F032

-

Wastewaters, process residuals, preservative drippage, and spent formulations from wood preserving processes generated at plants that currently use, or have previously used, chlorophenolic formulations [except potentially cross- contaminated wastes that have had the F032 waste code deleted in accordance with Section 261.35 (i.e., the newly promulgated equipment cleaning or replacement standards), and where the generator does not resume or initiate use of chlorophenolic formulations]. This listing does not include K001 bottom sediment sludge from the treatment of wastewater from wood preserving processes that use creosote and/or pentachlorophenol.

F034

-

Wastewaters, process residuals, preservative drippage, and spent formulations from wood preserving processes generated at plants that use creosote formulations. This listing does not include K001 bottom sediment sludge from the treatment of wastewater from wood preserving processes that use creosote and/or pentachlorophenol.

F035

-

Wastewaters, process residuals, preservative drippage, and spent formulations from wood preserving processes generated at plants that use inorganic preservatives containing arsenic or chromium. This listing does not include K001 bottom sediment sludge from the treatment of wastewater from wood preserving processes that use creosote and/or pentachlorophenol.

P001

81-81-2

2H-1-Benzopyran-2-one, 4-hydroxy-3-(3-oxo-1-phenylbutyl)-, & salts, when present at concentrations greater than 0.3%

P001

81-81-2

Warfarin, & salts, when present at concentrations greater than 0.3%

P002 591-08-2 1-Acetyl-2-thiourea

P002 591-08-2 Acetamide, N-(aminothioxomethyl)-

P003 107-02-8 2-Propenal

P003 107-02-8 Acrolein

P004

309-00-2

1,4,5,8-Dimethanonaphthalene, 1,2,3,4,10,10-hexachloro-1,4,4a,5,8,8a,- hexahydro-,(1alpha,4alpha,4abeta,5alpha,8alpha,8abeta)-

P004 309-00-2 Aldrin

P005 107-18-6 2-Propen-1-ol

P005 107-18-6 Allyl alcohol

P006 20859-73-8 Aluminum phosphide (R,T)

P007 2763-96-4 3(2H)-Isoxazolone, 5-(aminomethyl)-

P007 2763-96-4 5-(Aminomethyl)-3-isoxazolol

P008 504-24-5 4-Aminopyridine

P008 504-24-5 4-Pyridinamine

P009 131-74-8 Ammonium picrate (R)

P009 131-74-8 Phenol, 2,4,6-trinitro-, ammonium salt

P010 7778-39-4 Arsenic acid H3AsO4

P011 1303-28-2 Arsenic oxide As2O5

P011 1303-28-2 Arsenic pentoxide

P012 1327-53-3 Arsenic oxide As2O3

P012 1327-53-3 Arsenic trioxide


EPA ID# MN0000981415 of 50

P013 542-62-1 Barium cyanide

P014 108-98-5 Benzenethiol

P014 108-98-5 Thiophenol

P015 7440-41-7 Beryllium powder

P016 542-88-1 Dichloromethyl ether

P016 542-88-1 Methane, oxybis[chloro-

P017 598-31-2 2-Propanone, 1-bromo-

P017 598-31-2 Bromoacetone

P018 357-57-3 Brucine

P018 357-57-3 Strychnidin-10-one, 2,3-dimethoxy-

P020 88-85-7 Dinoseb

P020 88-85-7 Phenol, 2-(1-methylpropyl)-4,6-dinitro-

P021 592-01-8 Calcium cyanide

P021 592-01-8 Calcium cyanide Ca(CN)2

P022 75-15-0 Carbon disulfide

P023 107-20-0 Acetaldehyde, chloro-

P023 107-20-0 Chloroacetaldehyde

P024 106-47-8 Benzenamine, 4-chloro-

P024 106-47-8 p-Chloroaniline

P026 5344-82-1 1-(o-Chlorophenyl)thiourea

P026 5344-82-1 Thiourea, (2-chlorophenyl)-

P027 542-76-7 3-Chloropropionitrile

P027 542-76-7 Propanenitrile, 3-chloro-

P028 100-44-7 Benzene, (chloromethyl)-

P028 100-44-7 Benzyl chloride

P029 544-92-3 Copper cyanide

P029 544-92-3 Copper cyanide Cu(CN)

P030 - Cyanides (soluble cyanide salts), not otherwise specified

P031 460-19-5 Cyanogen

P031 460-19-5 Ethanedinitrile

P033 506-77-4 Cyanogen chloride

P033 506-77-4 Cyanogen chloride (CN)Cl

P034 131-89-5 2-Cyclohexyl-4,6-dinitrophenol

P034 131-89-5 Phenol, 2-cyclohexyl-4,6-dinitro-

P036 696-28-6 Arsonous dichloride, phenyl-

P036 696-28-6 Dichlorophenylarsine

P037

60-57-1

2,7:3,6-Dimethanonaphth[2,3-b]oxirene, 3,4,5,6,9,9- hexachloro1a,2,2a,3,6,6a,7,7aoctahydro(1aalpha,2beta,2aalpha,3beta,6beta,6a alpha,7beta, 7aalpha)-

P037 60-57-1 Dieldrin

P038 692-42-2 Arsine, diethyl-

P038 692-42-2 Diethylarsine


EPA ID# MN0000981415 of 50

P039 298-04-4 Disulfoton

P039 298-04-4 Phosphorodithioic acid, O,O-diethyl S-[2-(ethylthio)ethyl] ester

P040 297-97-2 O,O-Diethyl O-pyrazinyl phosphorothioate

P040 297-97-2 Phosphorothioic acid, O,O-diethyl O-pyrazinyl ester

P041 311-45-5 Diethyl-p-nitrophenyl phosphate

P041 311-45-5 Phosphoric acid, diethyl 4-nitrophenyl ester

P042 51-43-4 1,2-Benzenediol, 4-[1-hydroxy-2-(methylamino)ethyl]-, (R)-

P042 51-43-4 Epinephrine

P043 55-91-4 Diisopropylfluorophosphate (DFP)

P043 55-91-4 Phosphorofluoridic acid, bis(1-methylethyl) ester

P044 60-51-5 Dimethoate

P044 60-51-5 Phosphorodithioic acid, O,O-dimethyl S-[2-(methylamino)-2-oxoethyl] ester

P045 39196-18-4 2-Butanone, 3,3-dimethyl-1-(methylthio)-,O-[methylamino)carbonyl] oxime

P045 39196-18-4 Thiofanox

P046 122-09-8 alpha,alpha-Dimethylphenethylamine

P046 122-09-8 Benzeneethanamine, alpha,alpha-dimethyl-

P047 534-52-1 4,6-Dinitro-o-cresol, & salts

P047 534-52-1 Phenol, 2-methyl-4,6-dinitro-, & salts

P048 51-28-5 2,4-Dinitrophenol

P048 51-28-5 Phenol, 2,4-dinitro-

P049 541-53-7 Dithiobiuret

P049 541-53-7 Thioimidodicarbonic diamide [(H2N)C(S)]2NH

P050 115-29-7 6,9-Methano-2,4,3-benzodioxathiepin,6,7,8,9,10,10-hexachloro-1,5,5a,6,9,9a- hexahydro-,3-oxide

P050 115-29-7 Endosulfan

P051

72-20-8

2,7:3,6-Dimethanonaphth [2,3-b]oxirene, 3,4,5,6,9,9-hexachloro- 1a,2,2a,3,6,6a,7,7a- octahydro(1aalpha,2beta,2abeta,3alpha,6alpha,6abeta,7beta, 7aalpha)-, & metabolites

P051 72-20-8 Endrin

P051 72-20-8 Endrin, & metabolites

P054 151-56-4 Aziridine

P054 151-56-4 Ethyleneimine

P056 7782-41-4 Fluorine

P057 640-19-7 Acetamide, 2-fluoro-

P057 640-19-7 Fluoroacetamide

P058 62-74-8 Acetic acid, fluoro-, sodium salt

P058 62-74-8 Fluoroacetic acid, sodium salt

P059 76-44-8 4,7-Methano-1H-indene, 1,4,5,6,7,8,8-heptachloro-3a,4,7,7a-tetrahydro-


EPA ID# MN0000981415 of 50

P059 76-44-8 Heptachlor

P060

465-73-6

1,4,5,8-Dimethanonaphthalene, 1,2,3,4,10,10-hexachloro-1,4,4a,5,8,8a- hexahydro-(1alpha,4alpha,4abeta,5beta,8beta,8abeta)-

P060 465-73-6 Isodrin

P062 757-58-4 Hexaethyl tetraphosphate

P062 757-58-4 Tetraphosphoric acid, hexaethyl ester

P063 74-90-8 Hydrocyanic acid

P063 74-90-8 Hydrogen cyanide

P064 624-83-9 Methane, isocyanato-

P064 624-83-9 Methyl isocyanate

P065 628-86-4 Fulminic acid, mercury(2+) salt (R,T)

P065 628-86-4 Mercury fulminate (R,T)

P066 16752-77-5 Ethanimidothioic acid, N-[[(methylamino)carbonyl]oxy]-,methyl ester

P066 16752-77-5 Methomyl

P067 75-55-8 1,2-Propylenimine

P067 75-55-8 Aziridine, 2-methyl-

P068 60-34-4 Hydrazine, methyl-

P068 60-34-4 Methyl hydrazine

P069 75-86-5 2-Methyllactonitrile

P069 75-86-5 Propanenitrile, 2-hydroxy-2-methyl-

P070 116-06-3 Aldicarb

P070 116-06-3 Propanal, 2-methyl-2-(methylthio)-, O-[(methylamino)carbonyl]oxime

P071 298-00-0 Methyl parathion

P071 298-00-0 Phosphorothioic acid, O,O,-dimethyl O-(4-nitrophenyl) ester

P072 86-88-4 alpha-Naphthylthiourea

P072 86-88-4 Thiourea, 1-naphthalenyl-

P073 13463-39-3 Nickel carbonyl

P073 13463-39-3 Nickel carbonyl Ni(CO)4, (T-4)-

P074 557-19-7 Nickel cyanide

P074 557-19-7 Nickel cynaide Ni(CN)2

P075 54-11-5 Nicotine, & salts

P075 54-11-5 Pyridine, 3-(1-methyl-2-pyrrolidinyl)-, (S)-, & salts

P076 10102-43-9 Nitric oxide

P076 10102-43-9 Nitrogen oxide NO

P077 100-01-6 Benzenamine, 4-nitro-

P077 100-01-6 p-Nitroaniline

P078 10102-44-0 Nitrogen dioxide

P078 10102-44-0 Nitrogen oxide NO2

P081 55-63-0 1,2,3-Propanetriol, trinitrate (R)


EPA ID# MN0000981415 of 50

P081 55-63-0 Nitroglycerine (R)

P082 62-75-9 Methanamine, N-methyl-N-nitroso-

P082 62-75-9 N-Nitrosodimethylamine

P084 4549-40-0 N-Nitrosomethylvinylamine

P084 4549-40-0 Vinylamine, N-methyl-N-nitroso-

P085 152-16-9 Diphosphoramide, octamethyl-

P085 152-16-9 Octamethylpyrophosphoramide

P087 20816-12-0 Osmium oxide OsO4, (T-4)-

P087 20816-12-0 Osmium tetroxide

P088 145-73-3 7-Oxabicyclo[2.2.1]heptane-2,3-dicarboxylic acid

P088 145-73-3 Endothall

P089 56-38-2 Parathion

P089 56-38-2 Phosphorothioic acid, O,O-diethyl O-(4-nitrophenyl) ester

P092 62-38-4 Mercury, (acetato-O)phenyl-

P092 62-38-4 Phenylmercury acetate

P093 103-85-5 Phenylthiourea

P093 103-85-5 Thiourea, phenyl-

P094 298-02-2 Phorate

P094 298-02-2 Phosphorodithioic acid, O,O-diethyl S-[(ethylthio)methyl] ester

P095 75-44-5 Carbonic dichloride

P095 75-44-5 Phosgene

P096 7803-51-2 Hydrogen phosphide

P096 7803-51-2 Phosphine

P097 52-85-7 Famphur

P097 52-85-7 Phosphorothioic acid, O-[4-[(dimethylamino)sulfonyl]phenyl] O,O-dimethyl ester

P098 151-50-8 Potassium cyanide

P098 151-50-8 Potassium cyanide K(CN)

P099 506-61-6 Argentate(1-), bis(cyano-C)-, potassium

P099 506-61-6 Potassium silver cyanide

P101 107-12-0 Ethyl cyanide

P101 107-12-0 Propanenitrile

P102 107-19-7 2-Propyn-1-ol

P102 107-19-7 Propargyl alcohol

P103 630-10-4 Selenourea

P104 506-64-9 Silver cyanide

P104 506-64-9 Silver cyanide Ag(CN)

P105 26628-22-8 Sodium azide

P106 143-33-9 Sodium cyanide

P106 143-33-9 Sodium cyanide Na(CN)

P108 57-24-9 Strychnidin-10-one, & salts


EPA ID# MN0000981415 of 50

P108 57-24-9 Strychnine, & salts

P109 3689-24-5 Tetraethyldithiopyrophosphate

P109 3689-24-5 Thiodiphosphoric acid, tetraethyl ester

P110 78-00-2 Plumbane, tetraethyl-

P110 78-00-2 Tetraethyl lead

P111 107-49-3 Diphosphoric acid, tetraethyl ester

P111 107-49-3 Tetraethyl pyrophosphate

P112 509-14-8 Methane, tetranitro- (R)

P112 509-14-8 Tetranitromethane (R)

P113 1314-32-5 Thallic oxide

P113 1314-32-5 Thallium oxide Tl2O3

P114 12039-52-0 Selenious acid, dithallium(1+) salt

P114 12039-52-0 Thallium(I) selenite

P115 7446-18-6 Sulfuric acid, dithallium(1+) salt

P115 7446-18-6 Thallium(I) sulfate

P116 79-19-6 Hydrazinecarbothioamide

P116 79-19-6 Thiosemicarbazide

P118 75-70-7 Methanethiol, trichloro-

P118 75-70-7 Trichloromethanethiol

P119 7803-55-6 Ammonium vanadate

P119 7803-55-6 Vanadic acid, ammonium salt

P120 1314-62-1 Vanadium oxide V2O5

P120 1314-62-1 Vanadium pentoxide

P121 557-21-1 Zinc cyanide

P121 557-21-1 Zinc cyanide Zn(CN)2

P122 1314-84-7 Zinc phosphide Zn3P2, when present at concentrations greater than 10% (R,T)

P123 8001-35-2 Toxaphene

P127 1563-66-2 7-Benzofuranol, 2,3-dihydro-2,2-dimethyl-, methylcarbamate

P127 1563-66-2 Carbofuran

P128 315-18-4 henol, 4-(dimethylamino)-3,5-dimethyl-, methylcarbamate (ester)

P128 315-8-4 Mexacarbate

P185 26419-73-8 1,3-Dithiolane-2-carboxaldehyde, 2,4-dimethyl-, O-[(methylamino)- carbonyl]oxime

P185 26419-73-8 Tirpate

P188

57-64-7

Benzoic acid, 2-hydroxy-, compd. with(3aS-cis)-1,2,3,3a,8,8a-hexahydro-1,3a,8- trimethylpyrrolo[2,3-b]indol-5-yl methylcarbamate ester (1:1)

P188 57-64-7 Physostigmine salicylate

P189 55285-14-8 Carbamic acid, [(dibutylamino)-thio]methyl-, 2,3-dihydro-2,2-dimethyl- 7- benzofuranyl ester

P189 55285-14-8 Carbosulfan


EPA ID# MN0000981415 of 50

P190 1129-41-5 Carbamic acid, methyl-, 3-methylphenyl ester

P190 1129-41-5 Metolcarb

P191 644-64-4 Carbamic acid, dimethyl-, 1-[(dimethyl-amino)carbonyl]- 5-methyl-1H- pyrazol- 3- yl ester

P191 644-64-4 Dimetilan

P192 119-38-0 Carbamic acid, dimethyl-, 3-methyl-1-(1-methylethyl)-1H- pyrazol-5-yl ester

P192 119-38-0 Isolan

P194 23135-22-0 Ethanimidothioc acid, 2-(dimethylamino)-N-[[(methylamino)carbonyl]oxy]-2- oxo-, methyl ester

P194 23135-22-0 Oxamyl

P196 15339-36-3 Manganese dimethyldithiocarbamate

P196 15339-36-3 Manganese, bis(dimethylcarbamodithioato-S,S')-

P197 17702-57-7 Formparanate

P197 17702-57-7 Methanimidamide, N,N-dimethyl-N'-[2-methyl-4- [[(methylamino)carbonyl]oxy]phenyl]-

P198 23422-53-9 Formetanate hydrochloride

P198

23422-53-9

Methanimidamide, N,N-dimethyl-N'-[3-[[(methylamino)-carbonyl]oxy]phenyl]-, monohydrochloride

P199 2032-65-7 Methiocarb

P199 2032-65-7 Phenol, (3,5-dimethyl-4-(methylthio)-, methylcarbamate

P201 2631-37-0 Phenol, 3-methyl-5-(1-methylethyl)-, methyl carbamate

P201 2631-37-0 Promecarb

P202 64-00-6 3-Isopropylphenyl N-methylcarbamate

P202 64-00-6 m-Cumenyl methylcarbamate

P202 64-00-6 Phenol, 3-(1-methylethyl)-, methyl carbamate

P203 1646-88-4 Aldicarb sulfone

P203 1646-88-4 Propanal, 2-methyl-2-(methyl-sulfonyl)-, O-[(methylamino)carbonyl] oxime

P204 57-47-6 Physostigmine

P204 57-47-6 Pyrrolo[2,3-b]indol-5-ol, 1,2,3,3a,8,8a-hexahydro-1,3a,8-trimethyl-, methylcarbamate (ester), (3aS-cis)-

P205 137-30-4 Zinc, bis(dimethylcarbamodithioato-S,S')-,

P205 137-30-4 Ziram

U001 75-07-0 Acetaldehyde (I)

U001 75-07-0 Ethanal (I)

U002 67-64-1 2-Propanone (I)

U002 67-64-1 Acetone (I)

U003 75-05-8 Acetonitrile (I,T)

U004 98-86-2 Acetophenone

U004 98-86-2 Ethanone, 1-phenyl-


EPA ID# MN0000981415 of 50

U005 53-96-3 2-Acetylaminofluorene

U005 53-96-3 Acetamide, N-9H-fluoren-2-yl-

U006 75-36-5 Acetyl chloride (C,R,T)

U007 79-06-1 2-Propenamide

U007 79-06-1 Acrylamide

U008 79-10-7 2-Propenoic acid (I)

U008 79-10-7 Acrylic acid (I)

U009 107-13-1 2-Propenenitrile

U009 107-13-1 Acrylonitrile

U010

50-07-7 Azirino[2,3:3,4]pyrrolo[1,2-a]indole-4,7-dione, 6-amino-8- [[(aminocarbonyl)oxy]methyl]-1,1a,2,8,8a,8b-hexahydro-8a-methoxy-5-methyl- , [1aS-(1aalpha,8beta,8aalpha,8balpha)]-

U010 50-07-7 Mitomycin C

U011 61-82-5 1H-1,2,4-Triazol-3-amine

U011 61-82-5 Amitrole

U012 62-53-3 Aniline (I,T)

U012 62-53-3 Benzenamine (I,T)

U014 492-80-8 Auramine

U014 492-80-8 Benzenamine, 4,4-carbonimidoylbis[N,N-dimethyl-

U015 115-02-6 Azaserine

U015 115-02-6 L-Serine, diazoacetate (ester)

U016 225-51-4 Benz[c]acridine

U017 98-87-3 Benzal chloride

U017 98-87-3 Benzene, (dichloromethyl)-

U018 56-55-3 Benz[a]anthracene

U019 71-43-2 Benzene (I,T)

U020 98-09-9 Benzenesulfonic acid chloride (C,R)

U020 98-09-9 Benzenesulfonyl chloride (C,R)

U021 92-87-5 [1,1-Biphenyl]-4,4-diamine

U021 92-87-5 Benzidine

U022 50-32-8 Benzo[a]pyrene

U023 98-07-7 Benzene, (trichloromethyl)-

U023 98-07-7 Benzotrichloride (C,R,T)

U024 111-91-1 Dichloromethoxy ethane

U024 111-91-1 Ethane, 1,1'-[methylenebis(oxy)]bis[2-chloro-

U025 111-44-4 Dichloroethyl ether

U025 111-44-4 Ethane, 1,1'-oxybis[2-chloro-

U026 494-03-1 Chlornaphazin

U026 494-03-1 Naphthalenamine, N,N'-bis(2- chloroethyl)-

U027 108-60-1 Dichloroisopropyl ether

U027 108-60-1 Propane, 2,2'-oxybis[2-chloro-

U028 117-81-7 1,2-Benzenedicarboxylic acid, bis(2-ethylhexyl) ester


EPA ID# MN0000981415 of 50

U028 117-81-7 Diethylhexyl phthalate

U029 74-83-9 Methane, bromo-

U029 74-83-9 Methyl bromide

U030 101-55-3 4-Bromophenyl phenyl ether

U030 101-55-3 Benzene, 1-bromo-4-phenoxy-

U031 71-36-3 1-Butanol (I)

U031 71-36-3 n-Butyl alcohol (I)

U032 13765-19-0 Calcium chromate

U032 13765-19-0 Chromic acid H2CrO4, calcium salt

U033 353-50-4 Carbon oxyfluoride (R,T)

U033 353-50-4 Carbonic difluoride

U034 75-87-6 Acetaldehyde, trichloro-

U034 75-87-6 Chloral

U035 305-03-3 Benzenebutanoic acid, 4-[bis(2-chloroethyl)amino]-

U035 305-03-3 Chlorambucil

U036 57-74-9 4,7-Methano-1H-indene, 1,2,4,5,6,7,8,8- octachloro-2,3,3a,4,7,7a-hexahydro-

U036 57-74-9 Chlordane, alpha & gamma isomers

U037 108-90-7 Benzene, chloro-

U037 108-90-7 Chlorobenzene

U038 510-15-6 Benzeneacetic acid, 4-chloro-alpha-(4-chlorophenyl)-alpha-hydroxy-, ethyl ester

U038 510-15-6 Chlorobenzilate

U039 59-50-7 p-Chloro-m-cresol

U039 59-50-7 Phenol, 4-chloro-3-methyl-

U041 106-89-8 Epichlorohydrin

U041 106-89-8 Oxirane, (chloromethyl)-

U042 110-75-8 2-Chloroethyl vinyl ether

U042 110-75-8 Ethene, (2-chloroethoxy)-

U043 75-01-4 Ethene, chloro-

U043 75-01-4 Vinyl chloride

U044 67-66-3 Chloroform

U044 67-66-3 Methane, trichloro-

U045 74-87-3 Methane, chloro- (I, T)

U045 74-87-3 Methyl chloride (I,T)

U046 107-30-2 Chloromethyl methyl ether

U046 107-30-2 Methane, chloromethoxy-

U047 91-58-7 beta-Chloronaphthalene

U047 91-58-7 Naphthalene, 2-chloro-

U048 95-57-8 o-Chlorophenol

U048 95-57-8 Phenol, 2-chloro-

U049 3165-93-3 4-Chloro-o-toluidine, hydrochloride

U049 3165-93-3 Benzenamine, 4-chloro-2-methyl-,hydrochloride


EPA ID# MN0000981415 of 50

U050 218-01-9 Chrysene

U051 - Creosote

U052 1319-77-3 Cresol (Cresylic acid)

U052 1319-77-3 Phenol, methyl-

U053 4170-30-3 2-Butenal

U053 4170-30-3 Crotonaldehyde

U055 98-82-8 Benzene, (1-mehylethyl)- (I)

U055 98-82-8 Cumene (I)

U056 110-82-7 Benzene, hexahydro- (I)

U056 110-82-7 Cyclohexane (I)

U057 108-94-1 Cyclohexanone (I)

U058 50-18-0 2H-1,3,2-Oxazaphosphorin-2-amine, N,N-bis(2-chloroethyl)tetrahydro-, 2- oxide

U058 50-18-0 Cyclophosphamide

U059

20830-81-3

5,12-Naphthacenedione, 8-acetyl-10-[(3- amino-2,3,6-trideoxy)-alpha-L-lyxo- hexopyranosyl)oxy]-7,8,9,10- tetrahydro-6,8,11-trihydroxy-1- methoxy-, (8S- cis)-

U059 20830-81-3 Daunomycin

U060 72-54-8 Benzene, 1,1-(2,2-dichloroethylidene)bis[4-chloro-

U060 72-54-8 DDD

U061 50-29-3 Benzene, 1,1-(2,2,2- trichloroethylidene)bis[4-chloro-

U061 50-29-3 DDT

U062 2303-16-4 Carbamothioic acid, bis(1-methylethyl)- , S-(2,3-dichloro-2-propenyl) ester

U062 2303-16-4 Diallate

U063 53-70-3 Dibenz[a,h]anthracene

U064 189-55-9 Benzo[rst]pentaphene

U064 189-55-9 Dibenzo[a,i]pyrene

U066 96-12-8 1,2-Dibromo-3-chloropropane

U066 96-12-8 Propane, 1,2-dibromo-3-chloro-

U067 106-93-4 Ethane, 1,2-dibromo-

U067 106-93-4 Ethylene dibromide

U068 74-95-3 Methane, dibromo-

U068 74-95-3 Methylene bromide

U069 84-74-2 1,2-Benzenedicarboxylic acid, dibutyl ester

U069 84-74-2 Dibutyl phthalate

U070 95-50-1 Benzene, 1,2-dichloro-

U070 95-50-1 o-Dichlorobenzene


U071 541-73-1 m-Dichlorobenzene


U072 106-46-7 p-Dichlorobenzene

U073 91-94-1 [1,1'-Biphenyl]-4,4'-diamine, 3,3'- dichloro-


EPA ID# MN0000981415 of 50

U073 91-94-1 3,3'-Dichlorobenzidine

U074 764-41-0 1,4-Dichloro-2-butene

U074 764-41-0 2-Butene, 1,4-dichloro- (I,T)

U075 75-71-8 Dichlorodifluoromethane

U075 75-71-8 Methane, dichlorodifluoro-

U076 75-34-3 Ethane, 1,1-dichloro-

U076 75-34-3 Ethylidene dichloride

U077 107-06-2 Ethane, 1,2-dichloro-

U077 107-06-2 Ethylene dichloride

U078 75-35-4 1,1-Dichloroethylene

U078 75-35-4 Ethene, 1,1-dichloro-

U079 156-60-5 1,2-Dichloroethylene

U079 156-60-5 Ethene, 1,2-dichloro-, (E)-

U080 75-09-2 Methane, dichloro-

U080 75-09-2 Methylene chloride

U081 120-83-2 2,4-Dichlorophenol

U081 120-83-2 Phenol, 2,4-dichloro-

U082 87-65-0 2,6-Dichlorophenol

U082 87-65-0 Phenol, 2,6-dichloro-

U083 78-87-5 Propane, 1,2-dichloro-

U083 78-87-5 Propylene dichloride

U084 542-75-6 1,3-Dichloropropene

U084 542-75-6 1-Propene, 1,3-dichloro-

U085 1464-53-5 1,2:3,4-Diepoxybutane

U085 1464-53-5 2,2-Bioxirane

U086 1615-80-1 Hydrazine, 1,2-diethyl-

U086 1615-80-1 N,N'-Diethylhydrazine

U087 3288-58-2 O,O-Diethyl S-methyl dithiophosphate

U087 3288-58-2 Phosphorodithioic acid, O,O-diethyl S-methyl ester

U088 84-66-2 1,2-Benzenedicarboxylic acid, diethyl ester

U088 84-66-2 Diethyl phthalate

U089 56-53-1 Diethylstilbesterol

U089 56-53-1 Phenol, 4,4'-(1,2-diethyl-1,2- ethenediyl)bis-, (E)-

U090 94-58-6 1,3-Benzodioxole, 5-propyl-

U090 94-58-6 Dihydrosafrole

U091 119-90-4 [1,1'-Biphenyl]-4,4'-diamine, 3,3'- dimethoxy-

U091 119-90-4 3,3'-Dimethoxybenzidine

U092 124-40-3 Dimethylamine (I)

U092 124-40-3 Methanamine, N-methyl- (I)

U093 60-11-7 Benzenamine, N,N-dimethyl-4-(phenylazo)-

U093 60-11-7 p-Dimethylaminoazobenzene

U094 57-97-6 7,12-Dimethylbenz[a]anthracene

U094 57-97-6 Benz[a]anthracene, 7,12-dimethyl-


EPA ID# MN0000981415 of 50

U095 119-93-7 [1,1'-Biphenyl]-4,4'-diamine, 3,3'-dimethyl-

U095 119-93-7 3,3'-Dimethylbenzidine

U096 80-15-9 alpha,alpha-Dimethylbenzylhydroperoxide

U096 80-15-9 Hydroperoxide, 1-methyl-1-phenylethyl-

U097 79-44-7 Carbamic chloride, dimethyl-

U097 79-44-7 Dimethylcarbamoyl chloride

U098 57-14-7 1,1-Dimethylhydrazine

U098 57-14-7 Hydrazine, 1,1-dimethyl-

U099 540-73-8 1,2-Dimethylhydrazine

U099 540-73-8 Hydrazine, 1,2-dimethyl-

U101 105-67-9 2,4-Dimethylphenol

U101 105-67-9 Phenol, 2,4-dimethyl-

U102 131-11-3 1,2-Benzenedicarboxylic acid, dimethyl ester

U102 131-11-3 Dimethyl phthalate

U103 77-78-1 Dimethyl sulfate

U103 77-78-1 Sulfuric acid, dimethyl ester

U105 121-14-2 2,4-Dinitrotoluene

U105 121-14-2 Benzene, 1-methyl-2,4-dinitro-

U106 606-20-2 2,6-Dinitrotoluene

U106 606-20-2 Benzene, 2-methyl-1,3-dinitro-

U107 117-84-0 1,2-Benzenedicarboxylic acid, dioctyl ester

U107 117-84-0 Di-n-octyl phthalate

U108 123-91-1 1,4-Diethyleneoxide

U108 123-91-1 1,4-Dioxane

U109 122-66-7 1,2-Diphenylhydrazine

U109 122-66-7 Hydrazine, 1,2-diphenyl-

U110 142-84-7 1-Propanamine, N-propyl- (I)

U110 142-84-7 Dipropylamine (I)

U111 621-64-7 1-Propanamine, N-nitroso-N-propyl-

U111 621-64-7 Di-n-propylnitrosamine

U112 141-78-6 Acetic acid ethyl ester (I)

U112 141-78-6 Ethyl acetate (I)

U113 140-88-5 2-Propenoic acid, ethyl ester (I)

U113 140-88-5 Ethyl acrylate (I)

U114 111-54-6 Carbamodithioic acid, 1,2- ethanediylbis-, salts & esters

U114 111-54-6 Ethylenebisdithiocarbamic acid, salts & esters

U115 75-21-8 Ethylene oxide (I,T)

U115 75-21-8 Oxirane (I,T)

U116 96-45-7 2-Imidazolidinethione

U116 96-45-7 Ethylenethiourea

U117 60-29-7 Ethane, 1,1'-oxybis-(I)

U117 60-29-7 Ethyl ether (I)

U118 97-63-2 2-Propenoic acid, 2-methyl-, ethyl ester


EPA ID# MN0000981415 of 50

U118 97-63-2 Ethyl methacrylate

U119 62-50-0 Ethyl methanesulfonate

U119 62-50-0 Methanesulfonic acid, ethyl ester

U120 206-44-0 Fluoranthene

U121 75-69-4 Methane, trichlorofluoro-

U121 75-69-4 Trichloromonofluoromethane

U122 50-00-0 Formaldehyde

U123 64-18-6 Formic acid (C,T)

U124 110-00-9 Furan (I)

U124 110-00-9 Furfuran (I)

U125 98-01-1 2-Furancarboxaldehyde (I)

U125 98-01-1 Furfural (I)

U126 765-34-4 Glycidylaldehyde

U126 765-34-4 Oxiranecarboxyaldehyde

U127 118-74-1 Benzene, hexachloro-

U127 118-74-1 Hexachlorobenzene

U128 87-68-3 1,3-Butadiene, 1,1,2,3,4,4-hexachloro-

U128 87-68-3 Hexachlorobutadiene

U129 58-89-9 Cyclohexane, 1,2,3,4,5,6-hexachloro-, (1alpha,2alpha,3beta,4alpha,5alpha,6beta)-

U129 58-89-9 Lindane

U130 77-47-4 1,3-Cyclopentadiene, 1,2,3,4,5,5-hexachloro-

U130 77-47-4 Hexachlorocyclopentadiene

U131 67-72-1 Ethane, hexachloro-

U131 67-72-1 Hexachloroethane

U132 70-30-4 Hexachlorophene

U132 70-30-4 Phenol, 2,2'-methylenebis[3,4,6-trichloro-

U133 302-01-2 Hydrazine (R,T)

U134 7664-39-3 Hydrofluoric acid (C,T)

U134 7664-39-3 Hydrogen fluoride (C,T)

U135 7783-06-4 Hydrogen sulfide

U136 75-60-5 Arsinic acid, dimethyl-

U136 75-60-5 Cacodylic acid

U137 193-39-5 Indeno[1,2,3-cd]pyrene

U138 74-88-4 Methane, iodo-

U138 74-88-4 Methyl iodide

U140 78-83-1 1-Propanol, 2-methyl- (I,T)

U140 78-83-1 Isobutyl alcohol (I,T)

U141 120-58-1 1,3-Benzodioxole, 5-(1-propenyl)-

U141 120-58-1 Isosafrole

U142 143-50-0 1,3,4-Metheno-2H-cyclobuta[cd]pentalen- 2-one, 1,1a,3,3a,4,5,5,5a,5b,6- decachlorooctahydro-

U142 143-50-0 Kepone


EPA ID# MN0000981415 of 50

U143

303-34-4

2-Butenoic acid, 2-methyl-, 7-[[2,3- dihydroxy- 2-(1-methoxyethyl)-3-methyl-1- oxobutoxy]methyl]- 2,3,5,7a-tetrahydro-1H-pyrrolizin-1- yl ester, [1S- [1alpha(Z),7(2S*,3R*),7aalpha]]-

U143 303-34-4 Lasiocarpine

U144 301-04-2 Acetic acid, lead(2+) salt

U144 301-04-2 Lead acetate

U145 7446-27-7 Lead phosphate

U145 7446-27-7 Phosphoric acid, lead(2+) salt (2:3)

U146 1335-32-6 Lead subacetate

U146 1335-32-6 Lead, bis(acetato-O)tetrahydroxytri-

U147 108-31-6 2,5-Furandione

U147 108-31-6 Maleic anhydride

U148 123-33-1 3,6-Pyridazinedione, 1,2-dihydro-

U148 123-33-1 Maleic hydrazide

U149 109-77-3 Malononitrile

U149 109-77-3 Propanedinitrile

U150 148-82-3 L-Phenylalanine, 4-[bis(2- chloroethyl)amino]-

U150 148-82-3 Melphalan

U151 7439-97-6 Mercury

U152 126-98-7 2-Propenenitrile, 2-methyl- (I,T)

U152 126-98-7 Methacrylonitrile (I, T)

U153 74-93-1 Methanethiol (I, T)

U153 74-93-1 Thiomethanol (I,T)

U154 67-56-1 Methanol (I)

U154 67-56-1 Methyl alcohol (I)

U155 91-80-5 1,2-Ethanediamine, N,N-dimethyl-N'-2- pyridinyl-N'-(2-thienylmethyl)-

U155 91-80-5 Methapyrilene

U156 79-22-1 Carbonochloridic acid, methyl ester

U156 79-22-1 Methyl chlorocarbonate (I,T)

U157 56-49-5 3-Methylcholanthrene

U157 56-49-5 Benz[j]aceanthrylene, 1,2-dihydro-3-methyl-

U158 101-14-4 4,4'-Methylenebis(2-chloroaniline)

U158 101-14-4 Benzenamine, 4,4-methylenebis[2-chloro-

U159 78-93-3 2-Butanone (I,T)

U159 78-93-3 Methyl ethyl ketone (MEK) (I,T)

U160 1338-23-4 2-Butanone, peroxide (R,T)

U160 1338-23-4 Methyl ethyl ketone peroxide (R,T)

U161 108-10-1 4-Methyl-2-pentanone (I)

U161 108-10-1 Methyl isobutyl ketone (I)

U161 108-10-1 Pentanol, 4-methyl-

U162 80-62-6 2-Propenoic acid, 2-methyl-, methyl ester


EPA ID# MN0000981415 of 50

U162 80-62-6 Methyl methacrylate (I,T)

U163 70-25-7 Guanidine, N-methyl-N'-nitro-N-nitroso-

U163 70-25-7 MNNG

U164 56-04-2 4(1H)-Pyrimidinone, 2,3-dihydro-6- methyl-2-thioxo-

U164 56-04-2 Methylthiouracil

U165 91-20-3 Naphthalene

U166 130-15-4 1,4-Naphthalenedione

U166 130-15-4 1,4-Naphthoquinone

U167 134-32-7 1-Naphthalenamine

U167 134-32-7 alpha-Naphthylamine

U168 91-59-8 2-Naphthalenamine

U168 91-59-8 beta-Naphthylamine

U169 98-95-3 Benzene, nitro-

U169 98-95-3 Nitrobenzene (I,T)

U170 100-02-7 Phenol, 4-nitro-

U170 100-02-7 p-Nitrophenol

U171 79-46-9 2-Nitropropane (I,T)

U171 79-46-9 Propane, 2-nitro- (I,T)

U172 924-16-3 1-Butanamine, N-butyl-N-nitroso-

U172 924-16-3 N-Nitrosodi-n-butylamine

U173 1116-54-7 Ethanol, 2,2'-(nitrosoimino)bis-

U173 1116-54-7 N-Nitrosodiethanolamine

U174 55-18-5 Ethanamine, N-ethyl-N-nitroso-

U174 55-18-5 N-Nitrosodiethylamine

U176 759-73-9 N-Nitroso-N-ethylurea

U176 759-73-9 Urea, N-ethyl-N-nitroso-

U177 684-93-5 N-Nitroso-N-methylurea

U177 684-93-5 Urea, N-methyl-N-nitroso-

U178 615-53-2 Carbamic acid, methylnitroso-, ethyl ester

U178 615-53-2 N-Nitroso-N-methylurethane

U179 100-75-4 N-Nitrosopiperidine

U179 100-75-4 Piperidine, 1-nitroso-

U180 930-55-2 N-Nitrosopyrrolidine

U180 930-55-2 Pyrrolidine, 1-nitroso-

U181 99-55-8 5-Nitro-o-toluidine

U181 99-55-8 Benzenamine, 2-methyl-5-nitro-

U182 123-63-7 1,3,5-Trioxane, 2,4,6-trimethyl-

U182 123-63-7 Paraldehyde

U183 608-93-5 Benzene, pentachloro-

U183 608-93-5 Pentachlorobenzene

U184 76-01-7 Ethane, pentachloro-

U184 76-01-7 Pentachloroethane

U185 82-68-8 Benzene, pentachloronitro-


EPA ID# MN0000981415 of 50

U185 82-68-8 Pentachloronitrobenzene (PCNB)

U186 504-60-9 1,3-Pentadiene (I)

U186 504-60-9 1-Methylbutadiene (I)

U187 62-44-2 Acetamide, N-(4-ethoxyphenyl)-

U187 62-44-2 Phenacetin

U188 108-95-2 Phenol

U189 1314-80-3 Phosphorus sulfide (R)

U189 1314-80-3 Sulfur phosphide (R)

U190 85-44-9 1,3-Isobenzofurandione

U190 85-44-9 Phthalic anhydride

U191 109-06-8 2-Picoline

U191 109-06-8 Pyridine, 2-methyl-

U192 23950-58-5 Benzamide, 3,5-dichloro-N-(1,1-dimethyl-2-propynyl)-

U192 23950-58-5 Pronamide

U193 1120-71-4 1,2-Oxathiolane, 2,2-dioxide

U193 1120-71-4 1,3-Propane sultone

U194 107-10-8 1-Propanamine (I,T)

U194 107-10-8 n-Propylamine (I,T)

U196 110-86-1 Pyridine

U197 106-51-4 2,5-Cyclohexadiene-1,4-dione

U197 106-51-4 p-Benzoquinone

U200 50-55-5 Reserpine

U200

50-55-5

Yohimban-16-carboxylic acid, 11,17- dimethoxy-18-[(3,4,5- trimethoxybenzoyl)oxy]-, methyl ester, (3beta,16beta,17alpha,18beta,20alpha)-

U201 108-46-3 1,3-Benzenediol

U201 108-46-3 Resorcinol

U202 81-07-2 1,2-Benzisothiazol-3(2H)-one, 1,1- dioxide, & salts

U202 81-07-2 Saccharin, & salts

U203 94-59-7 1,3-Benzodioxole, 5-(2-propenyl)-

U203 94-59-7 Safrole

U204 7783-00-8 Selenious acid

U204 7783-00-8 Selenium dioxide

U205 7488-56-4 Selenium sulfide

U205 7488-56-4 Selenium sulfide SeS2 (R,T)

U206 18883-66-4 D-Glucose, 2-deoxy-2-[[(methylnitrosoamino)-carbonyl]amino]-

U206 18883-66-4 Glucopyranose, 2-deoxy-2-(3-methyl-3-nitrosoureido)-, D-

U206 18883-66-4 Streptozotocin

U207 95-94-3 1,2,4,5-Tetrachlorobenzene

U207 95-94-3 Benzene, 1,2,4,5-tetrachloro-

U208 630-20-6 1,1,1,2-Tetrachloroethane


EPA ID# MN0000981415 of 50

U208 630-20-6 Ethane, 1,1,1,2-tetrachloro-

U209 79-34-5 1,1,2,2-Tetrachloroethane

U209 79-34-5 Ethane, 1,1,2,2-tetrachloro-

U210 127-18-4 Ethene, tetrachloro-

U210 127-18-4 Tetrachloroethylene

U211 56-23-5 Carbon tetrachloride

U211 56-23-5 Methane, tetrachloro-

U213 109-99-9 Furan, tetrahydro-(I)

U213 109-99-9 Tetrahydrofuran (I)

U214 563-68-8 Acetic acid, thallium(1+) salt

U214 563-68-8 Thallium(I) acetate

U215 6533-73-9 Carbonic acid, dithallium(1+) salt

U215 6533-73-9 Thallium(I) carbonate

U216 7791-12-0 Thallium chloride Tlcl

U216 7791-12-0 Thallium(I) chloride

U217 10102-45-1 Nitric acid, thallium(1+) salt

U217 10102-45-1 Thallium(I) nitrate

U218 62-55-5 Ethanethioamide

U218 62-55-5 Thioacetamide

U219 62-56-6 Thiourea

U220 108-88-3 Benzene, methyl-

U220 108-88-3 Toluene

U221 25376-45-8 Benzenediamine, ar-methyl-

U221 25376-45-8 Toluenediamine

U222 636-21-5 Benzenamine, 2-methyl-, hydrochloride

U222 636-21-5 o-Toluidine hydrochloride

U223 26471-62-5 Benzene, 1,3-diisocyanatomethyl- (R,T)

U223 26471-62-5 Toluene diisocyanate (R,T)

U225 75-25-2 Bromoform

U225 75-25-2 Methane, tribromo-

U226 71-55-6 Ethane, 1,1,1-trichloro-

U226 71-55-6 Methyl chloroform

U227 79-00-5 1,1,2-Trichloroethane

U227 79-00-5 Ethane, 1,1,2-trichloro-

U228 79-01-6 Ethene, trichloro-

U228 79-01-6 Trichloroethylene

U234 99-35-4 1,3,5-Trinitrobenzene (R,T)

U234 99-35-4 Benzene, 1,3,5-trinitro-

U235 126-72-7 1-Propanol, 2,3-dibromo-, phosphate (3:1)

U235 126-72-7 Tris(2,3-dibromopropyl) phosphate

U236

72-57-1

2,7-Naphthalenedisulfonic acid, 3,3'- [(3,3'- dimethyl[1,1'-biphenyl]-4,4'- diyl)bis(azo)bis[5-amino-4-hydroxy]-, tetrasodium salt


EPA ID# MN0000981415 of 50

U236 72-57-1 Trypan blue

U237 66-75-1 2,4-(1H,3H)-Pyrimidinedione, 5-[bis(2-chloroethyl)amino]-

U237 66-75-1 Uracil mustard

U238 51-79-6 Carbamic acid, ethyl ester

U238 51-79-6 Ethyl carbamate (urethane)

U239 1330-20-7 Benzene, dimethyl- (I,T)

U239 1330-20-7 Xylene (I)

U240 94-75-7 2,4-D, salts & esters

U240 94-75-7 Acetic acid, (2,4-dichlorophenoxy)-, salts & esters

U243 1888-71-7 1-Propene, 1,1,2,3,3,3-hexachloro-

U243 1888-71-7 Hexachloropropene

U244 137-26-8 Thioperoxydicarbonic diamide[(H2N)C(S)]2S2, tetramethyl-

U244 137-26-8 Thiram

U246 506-68-3 Cyanogen bromide (CN)Br

U247 72-43-5 Benzene, 1,1-(2,2,2- trichloroethylidene)bis[4- methoxy-

U247 72-43-5 Methoxychlor

U248 81-81-2 2H-1-Benzopyran-2-one, 4-hydroxy-3-(3- oxo-1-phenyl-butyl)-, & salts, when present at concentrations of 0.3% or less

U248 81-81-2 Warfarin, & salts, when present at concentrations of 0.3% or less

U249 1314-84-7 Zinc phosphide Zn3P2, when present at concentrations of 10% or less

U271 17804-35-2 Benomyl

U271 17804-35-2 Carbamic acid, [1- [(butylamino)carbonyl]-1H- benzimidazol-2-yl]-, methyl ester

U278 22781-23-3 1,3-Benzodioxol-4-ol, 2,2-dimethyl-, methyl carbamate

U278 22781-23-3 Bendiocarb

U279 63-25-2 1-Naphthalenol, methylcarbamate

U279 63-25-2 Carbaryl

U280 101-27-9 Barban

U280 101-27-9 Carbamic acid, (3-chlorophenyl)-, 4- chloro-2-butynyl ester

U328 95-53-4 Benzenamine, 2-methyl-

U328 95-53-4 o-Toluidine

U353 106-49-0 Benzenamine, 4-methyl-

U353 106-49-0 p-Toluidine

U359 110-80-5 Ethanol, 2-ethoxy-

U359 110-80-5 Ethylene glycol monoethyl ether

U364 22961-82-6 1,3-Benzodioxol-4-ol, 2,2-dimethyl-,

U364 22961-82-6 Bendiocarb phenol

U367 1563-38-8 7-Benzofuranol, 2,3-dihydro-2,2- dimethyl-

U367 1563-38-8 Carbofuran phenol

U372 10605-21-7 Carbamic acid, 1H-benzimidazol-2-yl, methyl ester


EPA ID# MN0000981415 of 50

U372 10605-21-7 Carbendazim

U373 122-42-9 Carbamic acid, phenyl-, 1-methylethyl ester

U373 122-42-9 Propham

U387 52888-80-9 Carbamothioic acid, dipropyl-, S- (phenylmethyl) ester

U387 52888-80-9 Prosulfocarb

U389 2303-17-5 Carbamothioic acid, bis(1-methylethyl)- , S-(2,3,3-trichloro-2-propenyl) ester

U389 2303-17-5 Triallate

U394 30558-43-1 A2213

U394 30558-43-1 Ethanimidothioic acid, 2- (dimethylamino)-N-hydroxy-2-oxo-, methyl ester

U395 5952-26-1 Diethylene glycol, dicarbamate

U395 5952-26-1 Ethanol, 2,2'-oxybis-, dicarbamate

U404 121-44-8 Ethanamine, N,N-diethyl-

U404 121-44-8 Triethylamine

U409 23564-05-8 Carbamic acid, [1,2-phenylenebis (iminocarbonothioyl)]bis-, dimethyl ester

U409 23564-05-8 Thiophanate-methyl

U410

59669-26-0

Ethanimidothioic acid, N,N'- [thiobis[(methylimino)carbonyloxy]]bi s-, dimethyl ester

U410 59669-26-0 Thiodicarb

U411 114-26-1 Phenol, 2-(1-methylethoxy)-, methylcarbamate

U411 114-26-1 Propoxur

MN03 - Polychlorinated Biphenyls

draft hazardous waste permit to u of m - fay thompson center … · 2018. 12. 19. · draft...

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