4015 13th Avenue W, Seattle, WA 98119 ▪ Billing: PO Box 31936, Seattle, WA 98103
Office (206) 691 0476 ▪ Fax (206) 675 0650 www.kane-environmental.com
Underground Storage Tank Removal and Remedial Excavation Report
902 North Broadway Everett, Washington 98201
Prepared For:
Mr. Stanley Sidell NAP Management, Inc. G.P.
December 4, 2018
Project Number: 57302-2.2 Prepared By: Kane Environmental, Inc. 4015 13th Avenue West Seattle, WA 98119 ________________________ _________________________ Nathan Evenson John Kane, LHG Project Geologist, President, Principal UST Site Assessor #ICC00245994
TABLE OF CONTENTS
EXECUTIVE SUMMARY ............................................................................................................................... I
1.0 INTRODUCTION AND SITE BACKGROUND .................................................................................. 1
1.1 Property Location and Ownership .................................................................................................. 1
1.2 Property History .............................................................................................................................. 1
1.3 UST System Data ........................................................................................................................... 1
1.4 Surrounding Property Characteristics ............................................................................................. 2
1.5 Scope of Work ................................................................................................................................ 2
2.0 SUBSURFACE CONDITIONS ........................................................................................................... 4
2.1 Geologic Setting ............................................................................................................................. 4
2.2 Hydrogeologic Setting .................................................................................................................... 4
3.0 METHODOLOGY ............................................................................................................................... 5
3.1 Soil Sample Collection Methods ..................................................................................................... 5
3.2 Analytical Methods.......................................................................................................................... 5
3.2.1 Laboratory QA/QC Procedures ................................................................................................... 6
4.0 UNDERGROUND STORAGE TANK REMOVAL, REMEDIAL EXCAVATION, AND SOIL
SAMPLING ................................................................................................................................................... 7
4.1 UST System Inspection .................................................................................................................. 7
4.2 Fuel Dispenser, Product Line, and UST Removal .......................................................................... 7
4.2.1 Fuel Dispenser and Product Line Removal – November 8, 2017 .............................................. 7
4.2.2 UST Removal – November 9, 2017 ............................................................................................ 8
4.3 Remedial Soil “Hotspot” Excavation – November 13, 2017 ........................................................... 9
5.0 ANALYTICAL RESULTS ................................................................................................................ 11
5.1 Soil Results ................................................................................................................................... 11
6.0 FINDINGS AND CONCLUSIONS .................................................................................................... 13
7.0 LIMITATIONS .................................................................................................................................. 14
8.0 REFERENCES ................................................................................................................................. 15
Underground Storage Tank Removal and Remedial Excavation Report 902 North Broadway, Everett, Washington Project #57302-2.2
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FIGURES
Figure 1 – Vicinity Map
Figure 2 – Site Plan
Figure 3 – Site Plan Detail with Soil Sample Locations
TABLES
Table 1 – Summary of Petroleum Hydrocarbons and VOCs in Soil
ATTACHMENTS
Attachment A – Laboratory Analytical Reports
Attachment B – Field Photographs
Attachment C – Ecology UST Site Assessment Checklist
Attachment D – UST Rinse and Inerting Certifications
Attachment E – Soil Disposal Documentation
Underground Storage Tank Removal and Remedial Excavation Report 902 North Broadway, Everett, Washington Project #57302-2.2 Page i
EXECUTIVE SUMMARY
Kane Environmental, Inc. (Kane Environmental) has completed an underground storage tank (UST)
removal scope of work at the property located at 902 North Broadway in Everett, Washington (Snohomish
County Assessor’s tax parcel 29051700201100) (“the Property”). The Property owner, N A Properties Inc,
retained Kane Environmental to complete a number of tasks related remediation of petroleum
contamination in soil and groundwater on the Property, one of which involved the UST removal described
in this report. This report updates and finalizes a draft version of this report which was submitted to N A
Properties Inc, dated February 19, 2018.
Kane Environmental provided oversight for the site assessment, decommissioning, and removal of three
12,000-gallon fiberglass USTs, two fuel dispensers, subsurface fiberglass product lines, and other features
related to a former gasoline service station located on the Property. To prevent the possible failure of a
sidewall of the UST excavation and resulting public safety hazards and damage to public utilities, the
northernmost four to five feet of each UST was left in place. UST inspection and site cleanup staff at the
Washington State Department of Ecology (Ecology) and the City of Everett have been informed and have
acknowledged these circumstances.
Field observations and analytical results obtained from soil samples collected during removal of these USTs
and associated features indicate that a release of gasoline has occurred from this UST system. The release
or releases appear to have occurred at one or more joints in the fiberglass product lines. This finding is
supported by the elevated concentrations of benzene and gasoline reported in soil samples collected from
beneath product line joints, and the presence of field indicators of contamination associated with these
joints.
Along with the removal of USTs and associated features, approximately 56.65 tons of gasoline-
contaminated soil including the most contaminated soils encountered during UST removal activities have
been removed from the Property as part of a remedial soil hotspot excavation. Soil containing
concentrations of gasoline, benzene, and naphthalene at concentrations exceeding Model Toxics Control
Act (MTCA) Method A Soil Cleanup Levels were left in-place in the sidewalls of the UST and soil hotspot
excavations. This residual contamination is being addressed by a soil vapor extraction remediation system
that was subsequently installed and has been operating on the Property since March 2018.
The release identified as originating from the fuel transfer piping removed in November 2017, does not
account for the entirety of the gasoline contaminated soil and groundwater identified at deeper depths and
at other locations of the Property. Forensic analysis of lead speciation and gasoline additives in petroleum
contaminated soil and groundwater on the Property, reported by Apex Forensics (2018), concluded that
some of the gasoline released at the Property was manufactured prior to 1986, which was before installation
of the recent gas station infrastructure.
Underground Storage Tank Removal and Remedial Excavation Report 902 North Broadway, Everett, Washington Project #57302-2.2 Page 1
1.0 INTRODUCTION AND SITE BACKGROUND
Kane Environmental has conducted sampling and oversight tasks related to the removal of three USTs,
fuel dispenser pumps, and subsurface product lines from a property located at 902 North Broadway in
Everett, Washington (Snohomish County Assessor’s tax parcel 29051700201100) (“the Property”). A
topographic map showing the Property vicinity is included in Figure 1. A Site Plan is displayed in Figure 2.
1.1 Property Location and Ownership
The Property is composed of one tax parcel, which is bounded to the north by Tower Street and to the west
by North Broadway. The Property owner is “N A Properties Inc”, according to Snohomish County Assessor
records.
1.2 Property History
According to a description of the Property facilities and history in the Kane Environmental Revised Remedial
Investigation and Feasibility Study Report (Kane Environmental, 2016), the Property has been occupied by
a service station since approximately 1960. No development of the Property prior to 1960 was described.
Previous environmental investigations of the Property, as summarized by Kane Environmental (2016),
indicate that soil on the Property contains gasoline; benzene, toluene, ethylbenzene, and xylenes (BTEX);
and methyl-t-butyl ether (MTBE) at concentrations exceeding MTCA Method A Soil Cleanup Levels. These
previous investigations also indicated that groundwater on the Property contained gasoline, benzene,
ethylbenzene, xylenes, naphthalene, MTBE, 1,2-dichloroethane (EDC), and 1,2-dibromomethane (EDB) at
concentrations exceeding MTCA Method A Groundwater Cleanup Levels (Kane Environmental, 2016). The
Property is listed in the Ecology Voluntary Cleanup Program (VCP) database (VCP No. NW3032), the
Ecology UST database (UST Site ID No. 97367), and the Ecology Leaking UST (LUST) database.
The USTs, pumps, and product lines that were removed as part of the scope of work described in this report
were the second generation of service station infrastructure at the Property, installed in 1987 (Kane
Environmental, 2016). While no regulatory documentation regarding the USTs present on the Property prior
to 1987 was available, a detailed analysis of historical aerial photography concluded that the first generation
USTs may have been located in the vicinity of the second generation pump islands, with the first generation
pump islands likely located to the south and southeast of the original USTs.
1.3 UST System Data
The locations of the second-generation gas station features on the Property addressed in this report are
shown in Figure 2. According to the most recent tank tightness testing report available for the USTs
removed as described in this report, the USTs were 8,000-gallon double-walled fiberglass USTs equipped
with fiberglass product piping (Kane Environmental, 2016). This information is consistent with that listed in
Underground Storage Tank Removal and Remedial Excavation Report 902 North Broadway, Everett, Washington Project #57302-2.2 Page 2
the Ecology UST database for the site, except that the three USTs are listed as 10,000 gallons in size in
Ecology records. According to Kane Environmental (2016) and Ecology UST records, these USTs were
used to store gasoline. No records documenting storage of diesel fuel on the Property were available.
Observations regarding the USTs, fuel dispensers, and product lines gathered during field activities
conducted as part of this scope of work are described in Section 4 below.
1.4 Surrounding Property Characteristics
The Property is adjoined to the north by Tower Street, with a paved parking lot and government office
building located beyond. The Property is adjoined to the east by North Broadway, with a Washington State
University academic and administrative building located beyond. To the south, the Property is adjoined by
a paved parking lot and a Providence Healthcare building. The Property is adjoined to the west by a paved
parking lot, with the Everett Community College fitness center located beyond.
The south adjoining property is the location of the “Time Station 168” site, which is listed on Ecology’s VCP,
UST, and LUST databases. This site was occupied as a service station between the 1960s and 1989.
Petroleum contamination was discovered in soil and groundwater at this site in 1992. Remediation of site
soil and groundwater to MTCA Method A Soil and Groundwater cleanup levels was completed in 2011, and
the site was granted No Further Action (NFA) Status (Kane Environmental, 2016). Based on its NFA status,
this site is not considered to have a potential to impact soil and groundwater on the Property.
No other listed regulated sites were identified on adjoining properties by a review of the Ecology Facility/Site
Database Site Map.
1.5 Scope of Work
In a Proposal issued on August 21, 2017, and approved by Mr. Stanley Sidell of NAP Management Inc.,
G.P., on September 6, 2017, Kane Environmental was retained to perform supplemental site
characterization tasks, complete remedial actions (including design, installation, and operation of a soil
vapor extraction system), and perform ongoing maintenance and monitoring of the SVE system and
groundwater on the Property. One of the primary remedial actions (approved as Task 2 of this proposal)
was the decommissioning of the gasoline service station infrastructure, including removal of the USTs, fuel
dispensers, and product piping. This Task included the following activities:
Utility Locating: The Property was to be marked for a public one-call locate, and a private locate
was to be conducted to identify on-Property subsurface utilities not identified by the public locate
Permitting: A SEPA checklist and Land Use Application, along with other City of Everett permits,
were required for completion of the UST removal.
Underground Storage Tank Removal and Remedial Excavation Report 902 North Broadway, Everett, Washington Project #57302-2.2 Page 3
Demolition and Removal of Service Station Infrastructure: A UST decommissioning
subcontractor, Spooner Contracting, LLC (Spooner Contracting) was to be retained to remove the
fuel dispenser canopy, fuel dispenser pumps, product lines, and USTs.
Excavation: A limited excavation of contaminated soil (referred to as a “soil hotspot excavation”)
was to be completed from the areas below the USTs, fuel dispensers, and/or product lines. This
excavation was to be backfilled with imported clean fill or stockpiled site soils that had been
sampled and demonstrated to be appropriate for reuse by laboratory analysis.
Soil Sampling and Analytical: Soil samples were to be collected from the bottoms and sidewalls
of the UST and hotspot excavations. These samples were to be submitted to a laboratory for
analysis of constituents required by Ecology guidelines (Ecology, 1991).
Reporting: A brief report was to be prepared summarizing the activities completed at the Property.
This report was to be submitted to the Client.
This report documents the activities undertaken by Kane Environmental and subcontractor staff to complete
the Task 2 scope of work.
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2.0 SUBSURFACE CONDITIONS
2.1 Geologic Setting
The U.S. Geological Survey (USGS) Marysville, WA 7.5-Minute Quadrangle Topographic Map (Figure 1),
indicates that the ground surface of the Property is generally level. The elevation of the Property is
approximately 80 feet above mean sea level. Shallow soils encountered during subsurface investigations
on the Property consists of variable fill soils to a depth of approximately five feet, bgs, with localized deeper
fill soils surrounding the UST excavation. Shallow native soil underlying the fill were primarily comprised of
glacial soils composed of a mixture of soft to stiff silt and clay. Dense grading to very dense fine to medium
sands were encountered at approximately 25 to 65 feet below ground surface (bgs). These soils are
interpreted as advance outwash glacial deposits (Kane Environmental, 2016).
During the removal of fuel dispensers and product lines at the site, soils underlying these features were
observed to consist of medium to coarse sand soils of relatively low density, which were interpreted as fill
soils. The USTs were bedded in gravel fill soils.
2.2 Hydrogeologic Setting
Perched groundwater in native glacial soils was not encountered during the subsurface investigations
described by Kane Environmental (2016). Perched groundwater was previously identified in shallow
groundwater monitoring wells and soil borings in the immediate vicinity of the USTs and fuel dispensers.
These accumulations of groundwater are interpreted to be present only in fill soils surrounding service
station infrastructure (Kane Environmental, 2016). Regional groundwater is present at the Property at
depths of approximately 60 feet bgs. The regional groundwater flow direction at the Property is northerly to
northeasterly (Kane Environmental, 2016).
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3.0 METHODOLOGY
Methodology described in this section of the report is applicable to field observations and procedures
described in Sections 4 and 5 below.
3.1 Soil Sample Collection Methods
Where accessible, soil samples were collected by hand, or using a decontaminated stainless-steel sampling
trowel. Where access was not safely or practically available to collect a soil sample by hand, soil samples
were collected with assistance of an excavator operated by Spooner Contracting staff. The excavator
bucket was used to remove an area of undisturbed soil from a location identified by Kane Environmental.
Once removed from the excavation, Kane Environmental collected a soil sample from soil in the excavator
bucket that was located at least several inches from the metal surface of the bucket. Field samples were
screened for volatile organic compound contents using a photo-ionization detector (PID).
The locations of grab samples documented in this report were determined within a coordinate system with
an origin located near the southwest corner of the concrete-paved area in which the fuel dispensers were
installed. A “site north” direction was established for this system as being parallel to the east and west
margins of this concrete area, which was also parallel to the east and west margins of the concrete hold-
down slab overlying the USTs. Sample nomenclature for all samples documented in this report (with the
exception of stockpile samples) is as follows: “NxEy:zft, where “x” is the distance north of the origin in feet,
“y” is the distance east of the origin in feet, and “z” is the depth below the pavement surface in feet prior to
commencement of UST removal activities.
Sampled soils were placed into pre-cleaned, laboratory prepared containers, including 4-ounce glass jars
and 40-milliliter glass vials containing methanol preservative. Following sample collection, sample
containers were immediately placed into an ice-filled cooler and subsequently delivered to the analytical
laboratory under standard chain-of-custody procedures.
3.2 Analytical Methods
All samples collected during this scope of work were submitted to Fremont Analytical, a Washington
Department of Ecology-accredited analytical laboratory. Based on the contaminants of concern previously
identified in soil at the Property (see Section 1.2 above) and the analytical requirements described in Table
6-1 of the Ecology Guidance for Site Checks and Site Assessments for Underground Storage Tanks
(Ecology, 1991), all soil samples collected at the Property during UST removal and hotspot excavation
activities were analyzed for the following constituents:
Total Petroleum Hydrocarbons as Gasoline-Range Organics (GRO) by Washington Method
NWTPH-Gx, and,
Benzene, Toluene, Ethylbenzene, and Xylenes (BTEX) by EPA Method 8260.
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Selected soil samples, particularly those in sampling locations specified by the Ecology (1991) UST Site
Assessment guidance and the stockpile samples, were also analyzed for the following constituents:
MTBE, EDB, EDC, and Naphthalene by EPA Method 8260; and,
TPH as Diesel- (DRO) and Heavy Oil-range Organics (ORO) by Washington Method NWTPH-
Dx/Dx Extended.
All analyses were performed in accordance with Fremont’s in-house Quality Assurance/Quality Control
Plans. Sample analyses were performed in compliance with EPA analytical methods and Ecology
guidelines. Samples were analyzed within specified holding times. All detection limits were within method
requirements and no factors appeared to adversely affect data quality.
3.2.1 Laboratory QA/QC Procedures
Internal test methods run by the laboratory to ensure data accuracy and reproducibility include method
blanks, laboratory control standards, sample duplicates, matrix spikes, and matrix spike duplicates.
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4.0 UNDERGROUND STORAGE TANK REMOVAL, REMEDIAL EXCAVATION, AND SOIL
SAMPLING
All field observation and soil sampling activities were conducted by Kane Environmental UST Site Assessor
Nathan Evenson. Figure 3 shows the locations of removed features, the extents of the UST and Soil Hotspot
excavations, and the locations of soil samples. All laboratory analytical reports are included as Attachment
A. Photographs of the USTs and other Property features prior to and during removal are included as
Attachment B. An Ecology Site Check/Site Assessment Checklist for Underground Storage Tanks, required
for all UST Site Assessments, is included as Attachment C.
4.1 UST System Inspection
Prior to the commencement of UST removal activities, Kane Environmental inspected features of the USTs
and fuel dispensers accessible from the paved Property surface.
Kane Environmental opened each of the three USTs to determine their dimensions and contents, if any.
Each UST was approximately 8 feet in diameter. A few inches of liquid were present in the bottom of each
UST; these liquids appeared to consist of residual petroleum and water.
Each UST was equipped with a square vault near its south end, which housed the pump turbine. These
vaults were covered with metal lids and were enclosed with metal walls from the concrete slab surface to
approximately 0.75 feet bgs, and with plywood walls from 0.75 feet bgs to 1.75 feet bgs. Below
approximately 1.5 feet below the top of the vault, dirt was present. No secondary containment was noted
below the turbines or product lines in these vaults.
Each of the two fuel dispensers appeared in average condition. The base of each dispenser was open to
the underlying soil; no secondary containment sumps were observed. No obvious indications of
contamination were observed in the surficial soil visible beneath these dispensers.
4.2 Fuel Dispenser, Product Line, and UST Removal
Prior to commencement of the removal of USTs, fuel dispensers, and product lines, Marine Vacuum
Service, Inc. triple-rinsed the USTs and removed the rinse water for off-Property disposal. On the date of
UST removal, a marine chemist from Sound Testing, Inc. certified the USTs as safe for hot work and
mechanical demolition. Certifications of these activities are included in Attachment D.
4.2.1 Fuel Dispenser and Product Line Removal – November 8, 2017
On November 8, 2017, Kane Environmental was on the Property to oversee the removal of fuel dispensers
and product lines. Under Kane Environmental oversight, Spooner Contracting exposed the product lines
from the locations where they entered the subsurface to its point of entry into the UST area. Product lines
were observed to be single-wall fiberglass piping. No holes, cracks, or other defects were observed in the
Underground Storage Tank Removal and Remedial Excavation Report 902 North Broadway, Everett, Washington Project #57302-2.2 Page 8
product lines. At all observed joints, product lines appeared to have been joined using epoxy; however,
many of the inspected joints could be pulled apart manually.
Product lines were bedded in loose, medium to coarse sandy soils. These fill soils exuded a petroleum odor
in the areas below the dispenser islands and the joints located east of dispenser island (see Figure 3 for
sample locations; a description of the location of each sample is included in Table 1). Soil samples were
collected from 1 to 2 feet below each of these dispenser islands and joint locations. Product lines were
removed from the subsurface for off-Property disposal.
4.2.2 UST Removal – November 9, 2017
On November 8, 2017, Kane Environmental was on the Property to oversee the removal of the USTs.
Under Kane Environmental oversight, Spooner Contracting removed soils overlying the USTs and
stockpiled them on plastic sheeting. Kane Environmental estimated that less than 100 cubic yards of soil
were present in this stockpile. These soils did not display a petroleum odor or PID readings; therefore, Kane
Environmental collected three samples from this stockpile for laboratory analysis to characterize these
samples for possible re-use.
Following exposure of the tops and sides of the USTs, Kane Environmental measured them to be
approximately 34 feet long. Based on these dimensions and the 8-foot diameter measured previously, the
USTs were determined to be approximately 12,000 gallons in volume. During removal of the USTs, they
were discovered to be single-wall tanks, rather than the double-wall construction indicated in records
discussed in Section 1.3. Each UST was observed to be in good condition prior removal, with no obvious
cracks, holes, or other damage. The USTs were bedded in pea gravel fill. No accumulation of groundwater
was observed in the UST excavation during or following the removal of USTs.
Decommissioning and removal of USTs was conducted by Bill Spooner of Spooner Contracting, an
individual certified in Washington State for UST decommissioning. During removal of the first UST, its extent
was found to be farther north than previously known. Caving of the excavation sidewalls during UST
removal indicated that the soils surrounding the excavation were prone to failure. Based on these
observations, it appeared to Kane Environmental and Spooner Contracting staff that the removal of the
entirety of each UST would result in the collapse of soils in the sidewall north of the UST area. This north
sidewall failure would threaten the sidewalk and public utility corridors (which included a City of Everett
water main) located on the south side of Tower Street, north and adjacent to the Property. Kane
Environmental and Spooner Contracting staff decided to leave the northernmost 4 to 5 feet of each UST
in-place, in order to support the soils along the northern edge of the excavation while the remaining portions
of the USTs were removed. Mr. Will Bergquist, the Ecology UST Inspector who was present at the Property
during this part of the decommissioning, verbally indicated that it was permissible to leave the UST
fragments in-place to protect public safety and infrastructure. Kane Environmental and Spooner Contracting
Underground Storage Tank Removal and Remedial Excavation Report 902 North Broadway, Everett, Washington Project #57302-2.2 Page 9
proceeded to remove all but the northernmost portions of the USTs, which were left in place as described.
Remaining product lines within the UST excavation, and vent lines and the aboveground vent line frame
located northeast of the UST excavation were also removed. Removed portions of the USTs, product lines,
and vent lines were disposed of off-site.
Following completion of UST removal activities, Kane Environmental solicited and received
acknowledgement for leaving the UST fragments in place from Mr. Bergquist, Mr. Michael Warfel, the
Ecology VCP Site Manager for the Property, and Mr. Steve Goforth, an Assistant Fire Marshal with the
Everett Fire Department.
The bottoms of the USTs were located at a depth of approximately 11 feet bgs. Kane Environmental
collected soil samples from below the southern portion of each UST. Samples were also collected from the
soils below each of the UST fragments left in-place. Kane Environmental collected a sample from each of
the sidewalls of the UST excavation, with exception of the northern sidewall, which was inaccessible due
to the presence of the UST fragments left in-place. Sample locations are shown in Figure 3, and the location
of each sample is described in Table 1.
Overall, no indicators of significant petroleum contamination were present in most of the UST excavation,
with exception of the southwestern portion of the excavation, where the product lines exited the UST area.
The strongest evidence of petroleum contamination was observed in soils beneath product line joints
located in the southwest corner of the UST area. These soils displayed petroleum staining, strong petroleum
odor, and elevated PID readings. A soil sample was collected from beneath these piping joints. These soils
were subsequently excavated during the remedial soil excavation described below. Following removal of
the USTs, no further excavation of soils from other portions of the UST excavation was conducted.
4.3 Remedial Soil “Hotspot” Excavation – November 13, 2017
Following removal of the USTs, fuel dispensers, and product lines, a limited remedial excavation of soils
displaying the strongest field indicators of petroleum contamination was conducted. Kane Environmental
directed Spooner Contracting staff to excavate soils from the area beneath the northern portion of the
removed product lines leading from the dispenser islands to the UST excavation. The boundaries of this
soil hotspot excavation are shown in Figure 3. The bottom of the excavation was approximately 7 to 8 feet
bgs. During this excavation, the locations of several previously collected soil samples were removed; see
Figure 3 for details. Excavated soils consisted primarily of medium to coarse sand fill soils. A total of 56.65
tons of petroleum-contaminated soil were removed from the hotspot excavation. These soils were
transported by Hayter Trucking to an off-Property Cadman soil disposal facility in Everett, Washington.
Documentation of soil disposal is included as Attachment E. No accumulation of groundwater was observed
in this excavation.
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Following completion of the remedial soil hotspot excavation, Kane Environmental collected samples from
the bottom and sidewalls of the excavation to document contaminant concentrations in soils left in-place.
These samples are identified in Table 1, and their locations are shown in Figure 3. The excavated areas
on the Property were subsequently backfilled with imported clean gravel borrow fill and stockpiled soils,
and compacted. As discussed below, laboratory analysis characterized stockpiled soils as Category 2 soils,
which are suitable for reuse on commercial and industrial sites as backfill above the water table (Ecology,
2016).
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5.0 ANALYTICAL RESULTS
Results of laboratory analyses of soil samples and MTCA Method A Soil Cleanup Levels are summarized
in Table 1. Full analytical reports from the analytical laboratory, Fremont Analytical, are included as
Attachment A. Kane Environmental has reviewed QA/QC information included with these reports. No
factors that adversely affect data quality were noted, other than the reported detection limit for 1,2-
dibromoethane (EDB) exceeding the MTCA Method A Cleanup Level for Unrestricted Land Uses in select
soil samples analyzed.
5.1 Soil Results
All soil samples collected from beneath joints in product lines contained concentrations of benzene
exceeding the MTCA Method A Soil Cleanup Level. The sample collected from below the northernmost
joints in the product lines (N42E17:5.5ft) contained the highest concentrations of gasoline (8,840 mg/kg,
equivalent to parts per million (ppm)), benzene (78.7 ppm), toluene (497 ppm), ethylbenzene (153 ppm),
xylenes (869 ppm) and naphthalene (24.7 ppm) observed in samples collected during this scope of work,
all of which exceeded MTCA Method A Soil Cleanup Levels. The soil from which this sample was collected
was later removed during the soil hotspot excavation.
Soil samples collected from the southwestern portion of the UST excavation, including those collected from
below the southern ends of the west and middle USTs and from the south sidewall, contained gasoline
and/or benzene at concentrations exceeding MTCA Method A Soil Cleanup Levels. The sample collected
from the south excavation sidewall also contained naphthalene at a concentration exceeding the MTCA
Method A Soil Cleanup Level. Soil samples collected from other areas of the UST excavation, including the
soil samples collected from below the each of the UST fragments left in-place, either did not contain
gasoline or BTEX at concentrations in exceedance of MTCA Method A Soil Cleanup Levels, or did not
contain concentrations of these contaminants above laboratory reporting limits. Sampled soils in the bottom
and sidewalls of the UST excavation, including those displaying exceedances of MTCA Method A Soil
Cleanup Levels at the southern extent of the excavation, were left in-place following the completion of this
excavation.
Soil samples collected from the bottom and west sidewall of the soil hotspot excavation contained benzene
at concentrations of 1.09 and 0.145 ppm, respectively, both of which exceeded the MTCA Method A Soil
Cleanup Level. These samples and other sidewall and bottom samples collected from the hotspot
excavation also contained gasoline and other BTEX compounds at concentrations below MTCA Method A
Soil Cleanup Levels. These samples were left in place following the completion of this excavation.
Soil samples collected from below the dispenser islands (N05E13:3ft and N35E12:4ft) contained low
concentrations of gasoline or naphthalene that were below MTCA Method A Soil Cleanup Levels.
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No detections of diesel, heavy oil, MTBE, EDB, or EDC were reported in samples collected during this
scope of work.
Soil samples collected from the stockpile of UST overburden soils did not contain concentrations of
gasoline, BTEX, MTBE, EDB, EDC, or naphthalene at concentrations exceeding laboratory reporting limits,
with exception of one sample, which contained 0.0277 ppm of toluene and 0.0356 ppm of xylenes. Based
on these results, the stockpiled soils are classified as Category 2 soils (following Table 12.1 in Ecology,
2016).
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6.0 FINDINGS AND CONCLUSIONS
Kane Environmental has provided oversight for the assessment, decommissioning, and removal of three
12,000-gallon fiberglass USTs, two fuel dispensers, subsurface fiberglass product lines, and other features
related to a former gasoline service station located on the Property. To prevent the possible failure of a
sidewall of the UST excavation and resulting public safety hazards and damage to public utilities, the
northernmost four to five feet of each UST was left in place at the northern Property boundary. UST
inspection and site cleanup staff at the Washington State Department of Ecology and the City of Everett
have been informed and have acknowledged these circumstances.
Field observations and analytical results obtained from soil samples collected during removal of these USTs
and associated features indicate that a release of gasoline has occurred from this UST system. The release
or releases appear to have occurred at one or more joints in the fiberglass product lines. This finding is
supported by the elevated concentrations of benzene and gasoline reported in soil samples collected from
beneath product line joints, and the presence of field indicators of contamination associated with these
joints.
Approximately 56.65 tons of gasoline-contaminated soil, including the most contaminated soils encountered
during UST removal activities, have been removed from the Property as part of a remedial soil hotspot
excavation. Soil containing concentrations of gasoline, benzene, and naphthalene at concentrations
exceeding MTCA Method A Soil Cleanup Levels remain in the sidewalls of the UST and soil hotspot
excavations. This residual contamination is being addressed by a soil vapor extraction remediation system
that was subsequently installed and has been operating on the Property since March 2018.
The release identified as originating from the fuel transfer piping removed in November 2017, does not
account for the entirety of the gasoline contaminated soil and groundwater identified at deeper depths and
at other locations of the Property. Forensic analysis of lead speciation and gasoline additives in petroleum
contaminated soil and groundwater on the Property, reported by Apex Forensics (2018), concluded that
some of the gasoline released at the Property was manufactured prior to 1986, which was before installation
of the recent gas station infrastructure.
Underground Storage Tank Removal and Remedial Excavation Report 902 North Broadway, Everett, Washington Project #57302-2.2 Page 14
7.0 LIMITATIONS
Kane Environmental has performed this work in general accordance with generally accepted professional
practices using the standard of the industry today, for the nature and conditions of the work completed in
the same locality and at the same time as the work was performed, and with the terms and conditions as
set forth in our proposal.
Kane Environmental shall not be responsible for conditions or consequences arising from relevant facts
that were concealed, withheld, or not fully disclosed at the time the report was prepared. Facts and
conditions referenced in this report may change over time and the conclusions and recommendations set
forth herein are applicable only to the facts and conditions as described at the time the work was performed.
This Underground Storage Tank Removal and Remedial Excavation Report does not include other services
not specifically described in the scope of work in Section 1.5 of this report. Conclusions were made within
the operative constraints of the scope of work, budget, and schedule for this project.
Our assessment of the property may change as new data become available, either from persons familiar
with the site or during additional site studies, exploration or sampling. This report is intended for the
exclusive use of NAP Management Inc., G.P., and its designated assignees, for specific application to the
referenced property. It is not meant to represent a legal opinion. No other warranty, express or implied, is
made.
Underground Storage Tank Removal and Remedial Excavation Report 902 North Broadway, Everett, Washington Project #57302-2.2 Page 15
8.0 REFERENCES
Apex Forensics, November 8, 2018, Memorandum: Review of “Report Issued for NA Properties -
Everett/57302, Apex WO# A7L0258” 106 pgs.
Kane Environmental, Inc (Kane Environmental). 7 September 2016. Revised Remedial Investigation and
Feasibility Study Report. Prepared for Mr. Ben Pariser, NA Properties Management Company. 414
pgs, 9 figs.
Washington State Department of Ecology (Ecology). February 1991. Guidance for Site Checks and Site
Assessments for Underground Storage Tanks. Ecology Publication No. 90-52. 54 pgs.
Ecology. June 2016. Guidance for Remediation of Petroleum Contaminated Sites. Ecology Publication
No. 10-09-057.
FIGURES
Figure 1
Vicinity Map
UST Removal and Remedial Excavation
902 North Broadway
Everett, Washington
N
Kane Project #57302-2.2
DRAFT
DRAFT
Property
To
w
er S
treet
N
o
r
t
h
B
r
o
a
d
w
a
y
Figure 2
Site Plan
UST Removal and Remedial Excavation
902 North Broadway
Everett, Washington
Property Boundary
N
Approximate location of buried power line
Kane Project #57302-2.2
Former location of fiberglass UST, removed
(Solid outline shows location of fragment left in-place)
Former location of subsurface fiberglass product
piping, removed
Former location of fuel dispenser island, removed
DRAFT
DRAFT
Approximate location of Property
side sewer line
Approximate location of Property
subsurface electrical power line
N17E16:5ft
N05E13:3ft
N05E15:4ft
N30E22:5.5ft
N28E12:5ft
N29E17:8ft
N35E12:4ft
N42E17:5.5ft
N35E15:7ft
N35E15:3.5ft
N39E20:7.5ft
N40E32:9.5ft
N45E31:12.5ft
N46E41:12.5ft
N60E48:9ft
N71E40:12.5ft
N70E31:12ft
N72E21:12ft
N64E12:8ft
N50E20:12ft
Approximate Extent of
Soil Hotspot Excavation
(to 7-8 feet bgs)
Approximate Extent
of UST Excavation
Approximate Extent
of Soil Stockpile
SP-1-110917
SP-2-110917
SP-3-110917
Figure 3
Site Plan Detail with Soil
Sample Locations
UST Removal and Remedial Excavation
902 North Broadway
Everett, Washington
Property Boundary
Kane Project #57302-2.2
N
Soil sample location with concentrations
above MTCA Method A cleanup levels
Soil sample location with concentrations
below MTCA Method A cleanup levels
Soil sample location with concentrations
below laboratory reporting limit
Former location of fiberglass UST, removed
(Solid outline shows location of fragment left in-place)
Former location of subsurface fiberglass product
piping, removed
Former location of fuel dispenser, removed
Note: Grayed-out sample locations/labels have
been removed by over-excavation
DRAFT
DRAFT
TABLES
Table 1Summary of Petroleum Hydrocarbons and VOCs in SoilUST Removal and Remedial Excavation902 North BroadwayEverett, Washington Project #57302-2.2
Sam
ple
ID
Sam
ple
Dat
e
Sam
ple
Des
crip
tion
Sam
ple
Dep
th
(bel
ow g
roun
d su
rfac
e)G
asol
ine
Die
sel
Hea
vy O
il
Ben
zene
Tol
uene
Eth
ylbe
nzen
e
Tot
al X
ylen
es$
Met
hyl T
ertia
ry-B
utyl
Eth
er
(MT
BE
)
1,2-
Dib
rom
oeth
ane
(ED
B)R
1,2-
Dic
hlor
oeth
ane
(ED
C)
Nap
htha
lene
feet mg/kg mg/kg mg/kg mg/kg mg/kg mg/kg mg/kg mg/kg mg/kg mg/kg mg/kg
N05E13:3ft 11/8/2017 Below south dispenser island 3 5.49 - - <0.0214 <0.0214 <0.0267 <0.0801 <0.0534 <0.00534 <0.0214 <0.0534N05E15:4ft 11/8/2017 Below product line joints 4 <7.88 - - 0.104 0.168 <0.0394 <0.1182 <0.0788 <0.00788 <0.0315 0.153
N35E15:3.5ft 11/8/2017 Below product line joints 3.5 3.35 <20.3 <50.8 0.0943 0.280 0.0604 0.393 <0.0281 <0.00281 <0.0281 0.0495N35E12:4ft 11/8/2017 Below north dispenser island 4 <4.77 <19.9 <49.8 <0.0191 0.0489 <0.0238 <0.0717 <0.0477 <0.00477 <0.0191 0.0641
N50E20:12ft 11/9/2017 Below south end of west UST 12 <5.80 - - 0.126 0.468 0.0833 0.664 <0.0580 <0.0058 <0.0232 0.0823N72E21:12ft 11/9/2017 Below west UST fragment 12 <6.62 - - <0.0265 0.0329 <0.0331 0.199 - - - -N64E12:8ft 11/9/2017 West UST excavation sidewall 8 <6.27 - - <0.0251 <0.0251 <0.0314 0.0732 <0.0627 <0.00627 <0.0251 0.111
N70E31:12ft 11/9/2017 Below middle UST fragment 12 <6.67 - - <0.0267 <0.0267 <0.0333 <0.100 - - - -N45E31:12.5ft 11/9/2017 Below south end of middle UST 12.5 153† <19.7 <49.3 <0.0213 <0.0213 0.928 <0.0700 <0.0533 <0.00533 <0.0213 3.95N71E40:12.5ft 11/9/2017 Below east UST fragment 12.5 <4.83 - - <0.0193 <0.0193 <0.0242 <0.0725 - - - -N46E41:12.5ft 11/9/2017 Below south end of east UST 12.5 7.58 - - <0.0278 <0.0278 <0.0348 <0.104 <0.0696 <0.00696 <0.0278 <0.0696
N60E48:9ft 11/9/2017 East UST excavation sidewall 9.0 <6.66 - - <0.0266 <0.0266 <0.0333 <0.100 <0.0666 <0.00666 <0.0266 <0.0666N40E32:9.5ft 11/9/2017 South UST excavation sidewall 9.5 349† - - 0.558 0.147 2.74 0.960 <0.0567 <0.00567 <0.0227 9.60N42E17:5.5ft 11/9/2017 Below product line joints 5.5 8,840 165 <52.9 78.7 497 J 153 869 <0.772 <0.0772 0.309 24.7N39E20:7.5ft 11/13/2017 North hotspot excavation sidewall 7.5 <5.41 - - <0.0216 <0.0216 <0.0270 0.0661 - - - -N30E22:5.5ft 11/13/2017 East hotspot excavtion sidewall 5.5 <6.20 - - <0.0248 <0.0248 <0.0310 <0.0930 - - - -N29E17:8ft 11/13/2017 Hotspot excavation bottom 8 11.3 - - 1.09 2.28 0.263 1.207 - - - -N28E12:5ft 11/13/2017 West hotspot excavation sidewall 5 <5.15 - - 0.145 0.351 0.0591 0.2934 - - - -N17E16:5ft 11/13/2017 South hotspot excavation sidewall 5 <5.39 - - <0.0215 0.0524 <0.0269 <0.0808 - - - -
SP-1-110917 11/9/2017 N/A <4.33 - - <0.0173 <0.0173 <0.0217 <0.0650 <0.0433 <0.00433 <0.0217 <0.0433SP-2-110917 11/9/2017 N/A <6.89 - - <0.0276 0.0277 <0.0345 0.0356 <0.0689 <0.00689 <0.0276 <0.0689SP-3-110917 11/9/2017 N/A <8.10 - - <0.0324 <0.0324 <0.0405 <0.122 <0.0810 <0.00810 <0.0324 <0.0810
30/100* 0.03 7 6 9 0.1 0.005 (10.99) 5
Notes:All results reported in mg/kg (milligrams per kilogram).mg/kg = Milligrams per kilogram [equivalent to parts per million (ppm)].- = Not analyzed.Bold concentrations are detectable concentrations, below their Cleanup Level (if availiable).Shaded and Bold concentrations are detectable concentrations, exceeding their Cleanup Level .$ = Total xylenes shown are the sum of all reported detectable concentrations.* = 30 ppm is MTCA Method A Cleanup Level for gasoline range organics when benzene is present or the total of benzene, toluene and total xylenes is greater than 1%; 100 ppm otherwise.^ = Method A Cleanup Levels used where available. Method B Cleanup Levels (shown in parentheses) used if Method A Levels are not available.† = Laboratory identifies this detection as "Gasoline-Range Organics", described as "unresolved compounds eluting from toluene to dodecane (~C6-C12)". Gasoline reported as "not detected" in this sample.J = Estimated value.R = Method reporting limit exceedes Cleanup Level in select analyses.
2,000
Soil stockpile sample
MTCA Method A or Method B Soil Cleanup Level^
ATTACHMENT A LABORATORY ANALYTICAL REPORTS
November 17, 2017
Kane Environmental, Inc.Eric Nassau
Attention Eric Nassau:
RE: NA Properties Everett - 57302Work Order Number: 1711141
3815 Woodland Park Ave N, Ste. 102
Seattle, WA 98103
3600 Fremont Ave. N.
Seattle, WA 98103
T: (206) 352-3790
F: (206) 352-7178
Fremont Analytical, Inc. received 6 sample(s) on 11/8/2017 for the analyses presented in the following report.
Chelsea Ward
This report consists of the following:
- Case Narrative - Analytical Results - Applicable Quality Control Summary Reports - Chain of Custody
All analyses were performed consistent with the Quality Assurance program of Fremont Analytical, Inc. Please contact the laboratory if you should have any questions about the results.
Thank you for using Fremont Analytical.
Sincerely,
Project Manager
Diesel and Heavy Oil by NWTPH-Dx/Dx Ext.
Gasoline by NWTPH-Gx
Sample Moisture (Percent Moisture)
Volatile Organic Compounds by EPA Method 8260C
www.fremontanalytical.com Original
DoD/ELAP Certification #L17-135, ISO/IEC 17025:2005
ORELAP Certification: WA 100009-007 (NELAP Recognized)
Page 1 of 20
11/17/2017Date:
Project: NA Properties Everett - 57302
CLIENT: Kane Environmental, Inc.
Work Order: 1711141
Work Order Sample Summary
Lab Sample ID Client Sample ID Date/Time ReceivedDate/Time Collected1711141-001 N05E13: 3ft 11/08/2017 11:45 AM 11/08/2017 4:44 PM
1711141-002 N05E15: 4ft 11/08/2017 12:05 PM 11/08/2017 4:44 PM
1711141-003 N23E15: 2.5ft 11/08/2017 12:40 PM 11/08/2017 4:44 PM
1711141-004 N35E15: 3.5ft 11/08/2017 1:20 PM 11/08/2017 4:44 PM
1711141-005 N35E12: 4ft 11/08/2017 1:40 PM 11/08/2017 4:44 PM
1711141-006 N35E15: 7ft 11/08/2017 2:30 PM 11/08/2017 4:44 PM
Note: If no "Time Collected" is supplied, a default of 12:00AM is assignedOriginal Page 2 of 20
Project: NA Properties Everett - 57302
CLIENT: Kane Environmental, Inc.
11/17/2017
Case Narrative1711141
Date:
WO#:
I. SAMPLE RECEIPT:Samples receipt information is recorded on the attached Sample Receipt Checklist.
II. GENERAL REPORTING COMMENTS:Results are reported on a wet weight basis unless dry-weight correction is denoted in the units field on the analytical report ("mg/kg-dry" or "ug/kg-dry").
Matrix Spike (MS) and MS Duplicate (MSD) samples are tested from an analytical batch of "like" matrix to check for possible matrix effect. The MS and MSD will provide site specific matrix data only for those samples which are spiked by the laboratory. The sample chosen for spike purposes may or may not have been a sample submitted in this sample delivery group. The validity of the analytical procedures for which data is reported in this analytical report is determined by the Laboratory Control Sample (LCS) and the Method Blank (MB). The LCS and the MB are processed with the samples and the MS/MSD to ensure method criteria are achieved throughout the entire analytical process.
III. ANALYSES AND EXCEPTIONS:Exceptions associated with this report will be footnoted in the analytical results page(s) or the quality control summary page(s) and/or noted below.
Original
Page 3 of 20
11/17/2017
Qualifiers & Acronyms1711141
Date Reported:
WO#:
Qualifiers:
* - Flagged value is not within established control limitsB - Analyte detected in the associated Method BlankD - Dilution was requiredE - Value above quantitation rangeH - Holding times for preparation or analysis exceededI - Analyte with an internal standard that does not meet established acceptance criteria J - Analyte detected below Reporting LimitN - Tentatively Identified Compound (TIC)Q - Analyte with an initial or continuing calibration that does not meet established acceptance criteria (<20%RSD, <20% Drift or minimum RRF)S - Spike recovery outside accepted recovery limitsND - Not detected at the Reporting LimitR - High relative percent difference observed
Acronyms:
%Rec - Percent RecoveryCCB - Continued Calibration BlankCCV - Continued Calibration VerificationDF - Dilution FactorHEM - Hexane Extractable MaterialICV - Initial Calibration VerificationLCS/LCSD - Laboratory Control Sample / Laboratory Control Sample DuplicateMB or MBLANK - Method BlankMDL - Method Detection LimitMS/MSD - Matrix Spike / Matrix Spike DuplicatePDS - Post Digestion SpikeRef Val - Reference ValueRL - Reporting Limit RPD - Relative Percent Difference SD - Serial DilutionSGT - Silica Gel TreatmentSPK - SpikeSurr - Surrogate
Original
www.fremontanalytical.comPage 4 of 20
Project: NA Properties Everett - 57302
Client Sample ID: N05E13: 3ft
Collection Date: 11/8/2017 11:45:00 AM
Matrix: Soil
Client: Kane Environmental, Inc.
Lab ID: 1711141-001
Analyses Result Qual Units Date AnalyzedDFRL
Analytical Report
11/17/20171711141
Date Reported:
Work Order:
Gasoline by NWTPH-Gx Analyst: NGBatch ID: 18840
Gasoline 11/10/2017 6:19:32 AM5.34 mg/Kg-dry 15.49
Surr: 4-Bromofluorobenzene 11/10/2017 6:19:32 AM65 - 135 %Rec 1105
Surr: Toluene-d8 11/10/2017 6:19:32 AM65 - 135 %Rec 197.0
Volatile Organic Compounds by EPA Method 8260C Analyst: NGBatch ID: 18840
Methyl tert-butyl ether (MTBE) 11/10/2017 6:19:32 AM0.0534 mg/Kg-dry 1ND
1,2-Dichloroethane 11/10/2017 6:19:32 AM0.0214 mg/Kg-dry 1ND
Benzene 11/10/2017 6:19:32 AM0.0214 mg/Kg-dry 1ND
Toluene 11/10/2017 6:19:32 AM0.0214 mg/Kg-dry 1ND
1,2-Dibromoethane (EDB) 11/10/2017 6:19:32 AM0.00534 mg/Kg-dry 1ND
Ethylbenzene 11/10/2017 6:19:32 AM0.0267 mg/Kg-dry 1ND
m,p-Xylene 11/10/2017 6:19:32 AM0.0534 mg/Kg-dry 10.0800
o-Xylene 11/10/2017 6:19:32 AM0.0267 mg/Kg-dry 1ND
Naphthalene 11/16/2017 12:49:38 AM0.0534 mg/Kg-dry 10.287
Surr: Dibromofluoromethane 11/10/2017 6:19:32 AM56.5 - 129 %Rec 188.7
Surr: Toluene-d8 11/10/2017 6:19:32 AM64.5 - 151 %Rec 198.3
Surr: 1-Bromo-4-fluorobenzene 11/10/2017 6:19:32 AM43.2 - 143 %Rec 1100
Sample Moisture (Percent Moisture) Analyst: COBatch ID: R39850
Percent Moisture 11/10/2017 11:36:05 AM0.500 wt% 112.8
Original
Page 5 of 20
Project: NA Properties Everett - 57302
Client Sample ID: N05E15: 4ft
Collection Date: 11/8/2017 12:05:00 PM
Matrix: Soil
Client: Kane Environmental, Inc.
Lab ID: 1711141-002
Analyses Result Qual Units Date AnalyzedDFRL
Analytical Report
11/17/20171711141
Date Reported:
Work Order:
Gasoline by NWTPH-Gx Analyst: NGBatch ID: 18840
Gasoline 11/10/2017 7:24:13 PM7.88 mg/Kg-dry 1ND
Surr: 4-Bromofluorobenzene 11/10/2017 7:24:13 PM65 - 135 %Rec 195.7
Surr: Toluene-d8 11/10/2017 7:24:13 PM65 - 135 %Rec 1103
Volatile Organic Compounds by EPA Method 8260C Analyst: NGBatch ID: 18840
Methyl tert-butyl ether (MTBE) 11/10/2017 7:24:13 PM0.0788 mg/Kg-dry 1ND
1,2-Dichloroethane 11/10/2017 7:24:13 PM0.0315 mg/Kg-dry 1ND
Benzene 11/10/2017 7:24:13 PM0.0315 mg/Kg-dry 10.104
Toluene 11/10/2017 7:24:13 PM0.0315 mg/Kg-dry 10.168
1,2-Dibromoethane (EDB) 11/10/2017 7:24:13 PM0.00788 mg/Kg-dry 1ND
Ethylbenzene 11/10/2017 7:24:13 PM0.0394 mg/Kg-dry 1ND
m,p-Xylene 11/10/2017 7:24:13 PM0.0788 mg/Kg-dry 1ND
o-Xylene 11/10/2017 7:24:13 PM0.0394 mg/Kg-dry 1ND
Naphthalene 11/16/2017 1:20:02 AM0.0788 mg/Kg-dry 10.153
Surr: Dibromofluoromethane 11/10/2017 7:24:13 PM56.5 - 129 %Rec 189.1
Surr: Toluene-d8 11/10/2017 7:24:13 PM64.5 - 151 %Rec 188.5
Surr: 1-Bromo-4-fluorobenzene 11/10/2017 7:24:13 PM43.2 - 143 %Rec 191.3
Sample Moisture (Percent Moisture) Analyst: COBatch ID: R39850
Percent Moisture 11/10/2017 11:36:05 AM0.500 wt% 115.1
Original
Page 6 of 20
Project: NA Properties Everett - 57302
Client Sample ID: N35E15: 3.5ft
Collection Date: 11/8/2017 1:20:00 PM
Matrix: Soil
Client: Kane Environmental, Inc.
Lab ID: 1711141-004
Analyses Result Qual Units Date AnalyzedDFRL
Analytical Report
11/17/20171711141
Date Reported:
Work Order:
Diesel and Heavy Oil by NWTPH-Dx/Dx Ext. Analyst: SBBatch ID: 18837
Diesel (Fuel Oil) 11/9/2017 5:20:13 PM20.3 mg/Kg-dry 1ND
Heavy Oil 11/9/2017 5:20:13 PM50.8 mg/Kg-dry 1ND
Surr: 2-Fluorobiphenyl 11/9/2017 5:20:13 PM50 - 150 %Rec 176.2
Surr: o-Terphenyl 11/9/2017 5:20:13 PM50 - 150 %Rec 192.4
Gasoline by NWTPH-Gx Analyst: NGBatch ID: 18840
Gasoline 11/10/2017 8:24:46 PM2.81 mg/Kg-dry 13.35
Surr: 4-Bromofluorobenzene 11/10/2017 8:24:46 PM65 - 135 %Rec 197.3
Surr: Toluene-d8 11/10/2017 8:24:46 PM65 - 135 %Rec 197.8
Volatile Organic Compounds by EPA Method 8260C Analyst: NGBatch ID: 18840
Methyl tert-butyl ether (MTBE) 11/10/2017 8:24:46 PM0.0281 mg/Kg-dry 1ND
1,2-Dichloroethane 11/10/2017 8:24:46 PM0.0112 mg/Kg-dry 1ND
Benzene 11/10/2017 8:24:46 PM0.0112 mg/Kg-dry 10.0943
Toluene 11/10/2017 8:24:46 PM0.0112 mg/Kg-dry 10.280
1,2-Dibromoethane (EDB) 11/10/2017 8:24:46 PM0.00281 mg/Kg-dry 1ND
Ethylbenzene 11/10/2017 8:24:46 PM0.0141 mg/Kg-dry 10.0604
m,p-Xylene 11/10/2017 8:24:46 PM0.0281 mg/Kg-dry 10.283
o-Xylene 11/10/2017 8:24:46 PM0.0141 mg/Kg-dry 10.110
Naphthalene 11/16/2017 1:50:23 AM0.0281 mg/Kg-dry 10.0495
Surr: Dibromofluoromethane 11/10/2017 8:24:46 PM56.5 - 129 %Rec 186.6
Surr: Toluene-d8 11/10/2017 8:24:46 PM64.5 - 151 %Rec 192.3
Surr: 1-Bromo-4-fluorobenzene 11/10/2017 8:24:46 PM43.2 - 143 %Rec 193.0
Sample Moisture (Percent Moisture) Analyst: COBatch ID: R39850
Percent Moisture 11/10/2017 11:36:05 AM0.500 wt% 15.01
Original
Page 7 of 20
Project: NA Properties Everett - 57302
Client Sample ID: N35E12: 4ft
Collection Date: 11/8/2017 1:40:00 PM
Matrix: Soil
Client: Kane Environmental, Inc.
Lab ID: 1711141-005
Analyses Result Qual Units Date AnalyzedDFRL
Analytical Report
11/17/20171711141
Date Reported:
Work Order:
Diesel and Heavy Oil by NWTPH-Dx/Dx Ext. Analyst: SBBatch ID: 18837
Diesel (Fuel Oil) 11/9/2017 7:18:35 PM19.9 mg/Kg-dry 1ND
Heavy Oil 11/9/2017 7:18:35 PM49.8 mg/Kg-dry 1ND
Surr: 2-Fluorobiphenyl 11/9/2017 7:18:35 PM50 - 150 %Rec 186.5
Surr: o-Terphenyl 11/9/2017 7:18:35 PM50 - 150 %Rec 1102
Gasoline by NWTPH-Gx Analyst: NGBatch ID: 18840
Gasoline 11/10/2017 8:55:02 PM4.77 mg/Kg-dry 1ND
Surr: 4-Bromofluorobenzene 11/10/2017 8:55:02 PM65 - 135 %Rec 197.0
Surr: Toluene-d8 11/10/2017 8:55:02 PM65 - 135 %Rec 199.5
Volatile Organic Compounds by EPA Method 8260C Analyst: NGBatch ID: 18840
Methyl tert-butyl ether (MTBE) 11/10/2017 8:55:02 PM0.0477 mg/Kg-dry 1ND
1,2-Dichloroethane 11/10/2017 8:55:02 PM0.0191 mg/Kg-dry 1ND
Benzene 11/10/2017 8:55:02 PM0.0191 mg/Kg-dry 1ND
Toluene 11/10/2017 8:55:02 PM0.0191 mg/Kg-dry 10.0489
1,2-Dibromoethane (EDB) 11/10/2017 8:55:02 PM0.00477 mg/Kg-dry 1ND
Ethylbenzene 11/10/2017 8:55:02 PM0.0238 mg/Kg-dry 1ND
m,p-Xylene 11/10/2017 8:55:02 PM0.0477 mg/Kg-dry 1ND
o-Xylene 11/10/2017 8:55:02 PM0.0238 mg/Kg-dry 1ND
Naphthalene 11/16/2017 2:20:44 AM0.0477 mg/Kg-dry 10.0641
Surr: Dibromofluoromethane 11/10/2017 8:55:02 PM56.5 - 129 %Rec 187.1
Surr: Toluene-d8 11/10/2017 8:55:02 PM64.5 - 151 %Rec 192.5
Surr: 1-Bromo-4-fluorobenzene 11/10/2017 8:55:02 PM43.2 - 143 %Rec 192.6
Sample Moisture (Percent Moisture) Analyst: COBatch ID: R39850
Percent Moisture 11/10/2017 11:36:05 AM0.500 wt% 16.75
Original
Page 8 of 20
Project: NA Properties Everett - 57302
CLIENT: Kane Environmental, Inc.
Work Order: 1711141 QC SUMMARY REPORTDiesel and Heavy Oil by NWTPH-Dx/Dx Ext.
11/17/2017Date:
Sample ID MB-18837
Batch ID: 18837 Analysis Date: 11/9/2017
Prep Date: 11/9/2017
Analyte Result SPK value SPK Ref Val %REC RPD Ref Val %RPDLowLimit HighLimit RPDLimit Qual
Units: mg/Kg
RL
Client ID: MBLKS
RunNo: 39847
SeqNo: 767066
MBLKSampType:
Diesel (Fuel Oil) 20.0ND
Heavy Oil 50.0ND
Surr: 2-Fluorobiphenyl 20.00 79.9 50 15016.0
Surr: o-Terphenyl 20.00 98.4 50 15019.7
Sample ID LCS-18837
Batch ID: 18837 Analysis Date: 11/9/2017
Prep Date: 11/9/2017
Analyte Result SPK value SPK Ref Val %REC RPD Ref Val %RPDLowLimit HighLimit RPDLimit Qual
Units: mg/Kg
RL
Client ID: LCSS
RunNo: 39847
SeqNo: 767067
LCSSampType:
Diesel (Fuel Oil) 500.0 106 65 13520.0 0530
Surr: 2-Fluorobiphenyl 20.00 96.6 50 15019.3
Surr: o-Terphenyl 20.00 115 50 15022.9
Sample ID 1711141-004ADUP
Batch ID: 18837 Analysis Date: 11/9/2017
Prep Date: 11/9/2017
Analyte Result SPK value SPK Ref Val %REC RPD Ref Val %RPDLowLimit HighLimit RPDLimit Qual
Units: mg/Kg-dry
RL
Client ID: N35E15: 3.5ft
RunNo: 39847
SeqNo: 767069
DUPSampType:
Diesel (Fuel Oil) 3020.7 0ND
Heavy Oil 3051.8 0ND
Surr: 2-Fluorobiphenyl 20.70 82.8 50 150 017.1
Surr: o-Terphenyl 20.70 100 50 150 020.7
Sample ID 1711141-004AMS
Batch ID: 18837 Analysis Date: 11/9/2017
Prep Date: 11/9/2017
Analyte Result SPK value SPK Ref Val %REC RPD Ref Val %RPDLowLimit HighLimit RPDLimit Qual
Units: mg/Kg-dry
RL
Client ID: N35E15: 3.5ft
RunNo: 39847
SeqNo: 767070
MSSampType:
Diesel (Fuel Oil) 501.8 101 65 13520.1 0505
Surr: 2-Fluorobiphenyl 20.07 94.1 50 15018.9
Surr: o-Terphenyl 20.07 110 50 15022.2
Original Page 9 of 20
Project: NA Properties Everett - 57302
CLIENT: Kane Environmental, Inc.
Work Order: 1711141 QC SUMMARY REPORTDiesel and Heavy Oil by NWTPH-Dx/Dx Ext.
11/17/2017Date:
Sample ID 1711141-004AMS
Batch ID: 18837 Analysis Date: 11/9/2017
Prep Date: 11/9/2017
Analyte Result SPK value SPK Ref Val %REC RPD Ref Val %RPDLowLimit HighLimit RPDLimit Qual
Units: mg/Kg-dry
RL
Client ID: N35E15: 3.5ft
RunNo: 39847
SeqNo: 767070
MSSampType:
Sample ID 1711141-004AMSD
Batch ID: 18837 Analysis Date: 11/9/2017
Prep Date: 11/9/2017
Analyte Result SPK value SPK Ref Val %REC RPD Ref Val %RPDLowLimit HighLimit RPDLimit Qual
Units: mg/Kg-dry
RL
Client ID: N35E15: 3.5ft
RunNo: 39847
SeqNo: 767071
MSDSampType:
Diesel (Fuel Oil) 495.6 104 65 135 3019.8 0 505.4 1.49513
Surr: 2-Fluorobiphenyl 19.83 96.5 50 150 019.1
Surr: o-Terphenyl 19.83 112 50 150 022.1
Original Page 10 of 20
Project: NA Properties Everett - 57302
CLIENT: Kane Environmental, Inc.
Work Order: 1711141 QC SUMMARY REPORTGasoline by NWTPH-Gx
11/17/2017Date:
Sample ID LCS-18840
Batch ID: 18840 Analysis Date: 11/10/2017
Prep Date: 11/9/2017
Analyte Result SPK value SPK Ref Val %REC RPD Ref Val %RPDLowLimit HighLimit RPDLimit Qual
Units: mg/Kg
RL
Client ID: LCSS
RunNo: 39840
SeqNo: 766942
LCSSampType:
Gasoline 25.00 102 65 1355.00 025.5
Surr: Toluene-d8 1.250 97.9 65 1351.22
Surr: 4-Bromofluorobenzene 1.250 97.2 65 1351.22
Sample ID MB-18840
Batch ID: 18840 Analysis Date: 11/10/2017
Prep Date: 11/9/2017
Analyte Result SPK value SPK Ref Val %REC RPD Ref Val %RPDLowLimit HighLimit RPDLimit Qual
Units: mg/Kg
RL
Client ID: MBLKS
RunNo: 39840
SeqNo: 766943
MBLKSampType:
Gasoline 5.00ND
Surr: Toluene-d8 1.250 99.5 65 1351.24
Surr: 4-Bromofluorobenzene 1.250 93.8 65 1351.17
Sample ID 1711141-002BDUP
Batch ID: 18840 Analysis Date: 11/10/2017
Prep Date: 11/9/2017
Analyte Result SPK value SPK Ref Val %REC RPD Ref Val %RPDLowLimit HighLimit RPDLimit Qual
Units: mg/Kg-dry
RL
Client ID: N05E15: 4ft
RunNo: 39840
SeqNo: 767563
DUPSampType:
Gasoline 307.88 0ND
Surr: Toluene-d8 1.971 101 65 135 01.99
Surr: 4-Bromofluorobenzene 1.971 96.2 65 135 01.90
Sample ID 1711141-005BMS
Batch ID: 18840 Analysis Date: 11/10/2017
Prep Date: 11/9/2017
Analyte Result SPK value SPK Ref Val %REC RPD Ref Val %RPDLowLimit HighLimit RPDLimit Qual
Units: mg/Kg-dry
RL
Client ID: N35E12: 4ft
RunNo: 39840
SeqNo: 767566
MSSampType:
Gasoline 23.84 71.6 65 1354.77 017.1
Surr: Toluene-d8 1.192 98.7 65 1351.18
Surr: 4-Bromofluorobenzene 1.192 98.5 65 1351.17
Original Page 11 of 20
Project: NA Properties Everett - 57302
CLIENT: Kane Environmental, Inc.
Work Order: 1711141 QC SUMMARY REPORTGasoline by NWTPH-Gx
11/17/2017Date:
Sample ID 1711141-005BMSD
Batch ID: 18840 Analysis Date: 11/10/2017
Prep Date: 11/9/2017
Analyte Result SPK value SPK Ref Val %REC RPD Ref Val %RPDLowLimit HighLimit RPDLimit Qual
Units: mg/Kg-dry
RL
Client ID: N35E12: 4ft
RunNo: 39840
SeqNo: 767567
MSDSampType:
Gasoline 23.84 61.6 65 135 30 S4.77 0 17.07 15.114.7
Surr: Toluene-d8 1.192 98.3 65 135 01.17
Surr: 4-Bromofluorobenzene 1.192 99.9 65 135 01.19
NOTES:S - Outlying spike recovery(ies) observed. A duplicate analysis was performed and recovered within range.
Original Page 12 of 20
Project: NA Properties Everett - 57302
CLIENT: Kane Environmental, Inc.
Work Order: 1711141 QC SUMMARY REPORTSample Moisture (Percent Moisture)
11/17/2017Date:
Sample ID 1711132-018ADUP
Batch ID: R39850 Analysis Date: 11/10/2017
Prep Date: 11/10/2017
Analyte Result SPK value SPK Ref Val %REC RPD Ref Val %RPDLowLimit HighLimit RPDLimit Qual
Units: wt%
RL
Client ID: BATCH
RunNo: 39850
SeqNo: 767095
DUPSampType:
Percent Moisture 200.500 22.86 19.527.8
Sample ID 1711159-004ADUP
Batch ID: R39850 Analysis Date: 11/10/2017
Prep Date: 11/10/2017
Analyte Result SPK value SPK Ref Val %REC RPD Ref Val %RPDLowLimit HighLimit RPDLimit Qual
Units: wt%
RL
Client ID: BATCH
RunNo: 39850
SeqNo: 767115
DUPSampType:
Percent Moisture 200.500 34.57 2.8733.6
Original Page 13 of 20
Project: NA Properties Everett - 57302
CLIENT: Kane Environmental, Inc.
Work Order: 1711141 QC SUMMARY REPORTVolatile Organic Compounds by EPA Method 8260C
11/17/2017Date:
Sample ID MB-18912
Batch ID: 18912 Analysis Date: 11/15/2017
Prep Date: 11/15/2017
Analyte Result SPK value SPK Ref Val %REC RPD Ref Val %RPDLowLimit HighLimit RPDLimit Qual
Units: mg/Kg
RL
Client ID: MBLKS
RunNo: 39966
SeqNo: 769533
MBLKSampType:
Naphthalene 0.0500ND
Surr: Dibromofluoromethane 1.250 89.9 56.5 1291.12
Surr: Toluene-d8 1.250 97.7 64.5 1511.22
Surr: 1-Bromo-4-fluorobenzene 1.250 98.3 43.2 1431.23
Sample ID LCS-18912
Batch ID: 18912 Analysis Date: 11/15/2017
Prep Date: 11/15/2017
Analyte Result SPK value SPK Ref Val %REC RPD Ref Val %RPDLowLimit HighLimit RPDLimit Qual
Units: mg/Kg
RL
Client ID: LCSS
RunNo: 39966
SeqNo: 769532
LCSSampType:
Naphthalene 1.000 104 58.4 1600.0500 01.04
Surr: Dibromofluoromethane 1.250 95.8 56.5 1291.20
Surr: Toluene-d8 1.250 99.8 64.5 1511.25
Surr: 1-Bromo-4-fluorobenzene 1.250 104 43.2 1431.30
Sample ID 1711157-002BDUP
Batch ID: 18912 Analysis Date: 11/16/2017
Prep Date: 11/15/2017
Analyte Result SPK value SPK Ref Val %REC RPD Ref Val %RPDLowLimit HighLimit RPDLimit Qual
Units: mg/Kg-dry
RL
Client ID: BATCH
RunNo: 39966
SeqNo: 769513
DUPSampType:
Naphthalene 300.0593 0ND
Surr: Dibromofluoromethane 1.483 89.0 56.5 129 01.32
Surr: Toluene-d8 1.483 96.7 64.5 151 01.43
Surr: 1-Bromo-4-fluorobenzene 1.483 99.1 43.2 143 01.47
Sample ID 1711164-007BDUP
Batch ID: 18912 Analysis Date: 11/16/2017
Prep Date: 11/15/2017
Analyte Result SPK value SPK Ref Val %REC RPD Ref Val %RPDLowLimit HighLimit RPDLimit Qual
Units: mg/Kg-dry
RL
Client ID: BATCH
RunNo: 39966
SeqNo: 769523
DUPSampType:
Naphthalene 300.0680 0ND
Surr: Dibromofluoromethane 1.701 89.7 56.5 129 01.53
Original Page 14 of 20
Project: NA Properties Everett - 57302
CLIENT: Kane Environmental, Inc.
Work Order: 1711141 QC SUMMARY REPORTVolatile Organic Compounds by EPA Method 8260C
11/17/2017Date:
Sample ID 1711164-007BDUP
Batch ID: 18912 Analysis Date: 11/16/2017
Prep Date: 11/15/2017
Analyte Result SPK value SPK Ref Val %REC RPD Ref Val %RPDLowLimit HighLimit RPDLimit Qual
Units: mg/Kg-dry
RL
Client ID: BATCH
RunNo: 39966
SeqNo: 769523
DUPSampType:
Surr: Toluene-d8 1.701 97.8 64.5 151 01.66
Surr: 1-Bromo-4-fluorobenzene 1.701 98.5 43.2 143 01.67
Original Page 15 of 20
Project: NA Properties Everett - 57302
CLIENT: Kane Environmental, Inc.
Work Order: 1711141 QC SUMMARY REPORTVolatile Organic Compounds by EPA Method 8260C
11/17/2017Date:
Sample ID LCS-18840
Batch ID: 18840 Analysis Date: 11/10/2017
Prep Date: 11/9/2017
Analyte Result SPK value SPK Ref Val %REC RPD Ref Val %RPDLowLimit HighLimit RPDLimit Qual
Units: mg/Kg
RL
Client ID: LCSS
RunNo: 39839
SeqNo: 766932
LCSSampType:
Methyl tert-butyl ether (MTBE) 1.000 98.6 66.3 1450.0500 00.986
1,2-Dichloroethane 1.000 103 50.9 1620.0200 01.03
Benzene 1.000 114 64.3 1330.0200 01.14
Toluene 1.000 110 67.3 1380.0200 01.10
1,2-Dibromoethane (EDB) 1.000 112 50.5 1540.00500 01.12
Ethylbenzene 1.000 109 74 1290.0250 01.09
m,p-Xylene 2.000 115 70 1240.0500 02.29
o-Xylene 1.000 107 68.1 1390.0250 01.07
Surr: Dibromofluoromethane 1.250 97.7 56.5 1291.22
Surr: Toluene-d8 1.250 97.5 64.5 1511.22
Surr: 1-Bromo-4-fluorobenzene 1.250 102 43.2 1431.28
Sample ID MB-18840
Batch ID: 18840 Analysis Date: 11/10/2017
Prep Date: 11/9/2017
Analyte Result SPK value SPK Ref Val %REC RPD Ref Val %RPDLowLimit HighLimit RPDLimit Qual
Units: mg/Kg
RL
Client ID: MBLKS
RunNo: 39839
SeqNo: 766933
MBLKSampType:
Methyl tert-butyl ether (MTBE) 0.0500ND
1,2-Dichloroethane 0.0200ND
Benzene 0.0200ND
Toluene 0.0200ND
1,2-Dibromoethane (EDB) 0.00500ND
Ethylbenzene 0.0250ND
m,p-Xylene 0.0500ND
o-Xylene 0.0250ND
Surr: Dibromofluoromethane 1.250 93.2 56.5 1291.17
Surr: Toluene-d8 1.250 93.7 64.5 1511.17
Surr: 1-Bromo-4-fluorobenzene 1.250 89.5 43.2 1431.12
Original Page 16 of 20
Project: NA Properties Everett - 57302
CLIENT: Kane Environmental, Inc.
Work Order: 1711141 QC SUMMARY REPORTVolatile Organic Compounds by EPA Method 8260C
11/17/2017Date:
Sample ID 1711141-002BDUP
Batch ID: 18840 Analysis Date: 11/10/2017
Prep Date: 11/9/2017
Analyte Result SPK value SPK Ref Val %REC RPD Ref Val %RPDLowLimit HighLimit RPDLimit Qual
Units: mg/Kg-dry
RL
Client ID: N05E15: 4ft
RunNo: 39839
SeqNo: 767555
DUPSampType:
Methyl tert-butyl ether (MTBE) 300.0788 0ND
1,2-Dichloroethane 300.0315 0ND
Benzene 300.0315 0.1041 1.750.106
Toluene 300.0315 0.1681 3.030.173
1,2-Dibromoethane (EDB) 300.00788 0ND
Ethylbenzene 300.0394 0ND
m,p-Xylene 300.0788 0ND
o-Xylene 300.0394 0ND
Surr: Dibromofluoromethane 1.971 87.4 56.5 129 01.72
Surr: Toluene-d8 1.971 88.9 64.5 151 01.75
Surr: 1-Bromo-4-fluorobenzene 1.971 91.9 43.2 143 01.81
Sample ID 1711141-004BMS
Batch ID: 18840 Analysis Date: 11/10/2017
Prep Date: 11/9/2017
Analyte Result SPK value SPK Ref Val %REC RPD Ref Val %RPDLowLimit HighLimit RPDLimit Qual
Units: mg/Kg-dry
RL
Client ID: N35E15: 3.5ft
RunNo: 39839
SeqNo: 767557
MSSampType:
Methyl tert-butyl ether (MTBE) 0.5621 96.6 58.5 1670.0281 00.543
1,2-Dichloroethane 0.5621 106 51.3 1390.0112 00.596
Benzene 0.5621 117 63.5 1330.0112 0.094290.751
Toluene 0.5621 112 63.4 1320.0112 0.27960.908
1,2-Dibromoethane (EDB) 0.5621 106 50.4 1360.00281 00.593
Ethylbenzene 0.5621 125 54.5 1340.0141 0.060450.763
m,p-Xylene 1.124 124 53.1 1320.0281 0.28341.68
o-Xylene 0.5621 119 53.3 1390.0141 0.10990.778
Surr: Dibromofluoromethane 0.7026 92.6 56.5 1290.651
Surr: Toluene-d8 0.7026 92.0 64.5 1510.646
Surr: 1-Bromo-4-fluorobenzene 0.7026 100 43.2 1430.704
Original Page 17 of 20
Project: NA Properties Everett - 57302
CLIENT: Kane Environmental, Inc.
Work Order: 1711141 QC SUMMARY REPORTVolatile Organic Compounds by EPA Method 8260C
11/17/2017Date:
Sample ID 1711141-004BMSD
Batch ID: 18840 Analysis Date: 11/10/2017
Prep Date: 11/9/2017
Analyte Result SPK value SPK Ref Val %REC RPD Ref Val %RPDLowLimit HighLimit RPDLimit Qual
Units: mg/Kg-dry
RL
Client ID: N35E15: 3.5ft
RunNo: 39839
SeqNo: 767558
MSDSampType:
Methyl tert-butyl ether (MTBE) 0.5621 98.1 58.5 167 300.0281 0 0.5432 1.500.551
1,2-Dichloroethane 0.5621 109 51.3 139 300.0112 0 0.5964 2.410.611
Benzene 0.5621 122 63.5 133 300.0112 0.09429 0.7513 3.960.782
Toluene 0.5621 113 63.4 132 300.0112 0.2796 0.9075 1.040.917
1,2-Dibromoethane (EDB) 0.5621 106 50.4 136 300.00281 0 0.5933 0.8400.598
Ethylbenzene 0.5621 125 54.5 134 300.0141 0.06045 0.7626 0.1310.764
m,p-Xylene 1.124 124 53.1 132 300.0281 0.2834 1.678 0.2821.68
o-Xylene 0.5621 121 53.3 139 300.0141 0.1099 0.7776 1.470.789
Surr: Dibromofluoromethane 0.7026 94.7 56.5 129 00.665
Surr: Toluene-d8 0.7026 92.9 64.5 151 00.652
Surr: 1-Bromo-4-fluorobenzene 0.7026 98.7 43.2 143 00.693
Original Page 18 of 20
Date Received: 11/8/2017 4:44:00 PM
Client Name: KANE Work Order Number: 1711141
Sample Log-In Check List
Brianna BarnesLogged by:
Item Information
How was the sample delivered? Client
Is Chain of Custody complete? Yes No Not Present
Was an attempt made to cool the samples? Yes No NA
Are samples properly preserved? Yes No
Was preservative added to bottles? Yes No NA
Did all samples containers arrive in good condition(unbroken)? Yes No
Does paperwork match bottle labels? Yes No
Are matrices correctly identified on Chain of Custody? Yes No
Is it clear what analyses were requested? Yes No
Is there headspace in the VOA vials? Yes No NA
1.
2.
6.
10.
11.
12.
13.
14.
15.
16.
17. Were all holding times able to be met? Yes No
Chain of Custody
Log In
7. Were all items received at a temperature of >0°C to 10.0°C Yes No NA
8. Sample(s) in proper container(s)? Yes No
9. Sufficient sample volume for indicated test(s)? Yes No
Special Handling (if applicable)
18.
19.
Was client notified of all discrepancies with this order? Yes No NA
Person Notified: Date
Regarding:
Via: eMail Phone Fax In Person
Additional remarks:
Client Instructions:
By Whom:
Coolers are present? Yes No NA3.
Shipping container/cooler in good condition? Yes No4.
Custody Seals present on shipping container/cooler? (Refer to comments for Custody Seals not intact)
Yes No Not Required5.
*
Item # Temp ºC
Cooler 1.9
Sample 7.0
Page 1 of 1Note: DoD/ELAP and TNI require items to be received at 4°C +/- 2°C*
Original Page 19 of 20
Page 20 of 20
November 17, 2017
Kane Environmental, Inc.Eric Nassau
Attention Eric Nassau:
RE: NA Properties EverettWork Order Number: 1711164
3815 Woodland Park Ave N, Ste. 102
Seattle, WA 98103
3600 Fremont Ave. N.
Seattle, WA 98103
T: (206) 352-3790
F: (206) 352-7178
Fremont Analytical, Inc. received 15 sample(s) on 11/9/2017 for the analyses presented in the following report.
Chelsea Ward
This report consists of the following:
- Case Narrative - Analytical Results - Applicable Quality Control Summary Reports - Chain of Custody
All analyses were performed consistent with the Quality Assurance program of Fremont Analytical, Inc. Please contact the laboratory if you should have any questions about the results.
Thank you for using Fremont Analytical.
Sincerely,
Project Manager
Diesel and Heavy Oil by NWTPH-Dx/Dx Ext.
Gasoline by NWTPH-Gx
Sample Moisture (Percent Moisture)
Volatile Organic Compounds by EPA Method 8260C
www.fremontanalytical.com Original
DoD/ELAP Certification #L17-135, ISO/IEC 17025:2005
ORELAP Certification: WA 100009-007 (NELAP Recognized)
Page 1 of 31
11/17/2017Date:
Project: NA Properties Everett
CLIENT: Kane Environmental, Inc.
Work Order: 1711164
Work Order Sample Summary
Lab Sample ID Client Sample ID Date/Time ReceivedDate/Time Collected1711164-001 N50E20: 12ft 11/09/2017 8:45 AM 11/09/2017 4:47 PM
1711164-002 N72E21: 12ft 11/09/2017 9:25 AM 11/09/2017 4:47 PM
1711164-003 N64E12: 8ft 11/09/2017 9:55 AM 11/09/2017 4:47 PM
1711164-004 N70E31: 12ft 11/09/2017 10:30 AM 11/09/2017 4:47 PM
1711164-005 N45E31: 12.5ft 11/09/2017 11:30 AM 11/09/2017 4:47 PM
1711164-006 N71E40: 12.5ft 11/09/2017 12:10 PM 11/09/2017 4:47 PM
1711164-007 N46E41: 12.5ft 11/09/2017 12:25 PM 11/09/2017 4:47 PM
1711164-008 N60E45: 12.5ft 11/09/2017 1:00 PM 11/09/2017 4:47 PM
1711164-009 N60E48: 9ft 11/09/2017 1:15 PM 11/09/2017 4:47 PM
1711164-010 N40E32: 9.5ft 11/09/2017 1:30 PM 11/09/2017 4:47 PM
1711164-011 N42E17: 5.5ft 11/09/2017 1:45 PM 11/09/2017 4:47 PM
1711164-012 N59E29: 13ft 11/09/2017 2:00 PM 11/09/2017 4:47 PM
1711164-013 SP-1-110917 11/09/2017 2:20 PM 11/09/2017 4:47 PM
1711164-014 SP-2-110917 11/09/2017 2:30 PM 11/09/2017 4:47 PM
1711164-015 SP-3-110917 11/09/2017 2:40 PM 11/09/2017 4:47 PM
Note: If no "Time Collected" is supplied, a default of 12:00AM is assignedOriginal Page 2 of 31
Project: NA Properties Everett
CLIENT: Kane Environmental, Inc.
11/17/2017
Case Narrative1711164
Date:
WO#:
I. SAMPLE RECEIPT:Samples receipt information is recorded on the attached Sample Receipt Checklist.
II. GENERAL REPORTING COMMENTS:Results are reported on a wet weight basis unless dry-weight correction is denoted in the units field on the analytical report ("mg/kg-dry" or "ug/kg-dry").
Matrix Spike (MS) and MS Duplicate (MSD) samples are tested from an analytical batch of "like" matrix to check for possible matrix effect. The MS and MSD will provide site specific matrix data only for those samples which are spiked by the laboratory. The sample chosen for spike purposes may or may not have been a sample submitted in this sample delivery group. The validity of the analytical procedures for which data is reported in this analytical report is determined by the Laboratory Control Sample (LCS) and the Method Blank (MB). The LCS and the MB are processed with the samples and the MS/MSD to ensure method criteria are achieved throughout the entire analytical process.
III. ANALYSES AND EXCEPTIONS:Exceptions associated with this report will be footnoted in the analytical results page(s) or the quality control summary page(s) and/or noted below.
Original
Page 3 of 31
11/17/2017
Qualifiers & Acronyms1711164
Date Reported:
WO#:
Qualifiers:
* - Flagged value is not within established control limitsB - Analyte detected in the associated Method BlankD - Dilution was requiredE - Value above quantitation rangeH - Holding times for preparation or analysis exceededI - Analyte with an internal standard that does not meet established acceptance criteria J - Analyte detected below Reporting LimitN - Tentatively Identified Compound (TIC)Q - Analyte with an initial or continuing calibration that does not meet established acceptance criteria (<20%RSD, <20% Drift or minimum RRF)S - Spike recovery outside accepted recovery limitsND - Not detected at the Reporting LimitR - High relative percent difference observed
Acronyms:
%Rec - Percent RecoveryCCB - Continued Calibration BlankCCV - Continued Calibration VerificationDF - Dilution FactorHEM - Hexane Extractable MaterialICV - Initial Calibration VerificationLCS/LCSD - Laboratory Control Sample / Laboratory Control Sample DuplicateMB or MBLANK - Method BlankMDL - Method Detection LimitMS/MSD - Matrix Spike / Matrix Spike DuplicatePDS - Post Digestion SpikeRef Val - Reference ValueRL - Reporting Limit RPD - Relative Percent Difference SD - Serial DilutionSGT - Silica Gel TreatmentSPK - SpikeSurr - Surrogate
Original
www.fremontanalytical.comPage 4 of 31
Project: NA Properties Everett
Client Sample ID: N50E20: 12ft
Collection Date: 11/9/2017 8:45:00 AM
Matrix: Soil
Client: Kane Environmental, Inc.
Lab ID: 1711164-001
Analyses Result Qual Units Date AnalyzedDFRL
Analytical Report
11/17/20171711164
Date Reported:
Work Order:
Gasoline by NWTPH-Gx Analyst: MWBatch ID: 18912
Gasoline 11/16/2017 5:23:13 AM5.80 mg/Kg-dry 1ND
Surr: 4-Bromofluorobenzene 11/16/2017 5:23:13 AM65 - 135 %Rec 1105
Surr: Toluene-d8 11/16/2017 5:23:13 AM65 - 135 %Rec 199.2
Volatile Organic Compounds by EPA Method 8260C Analyst: MWBatch ID: 18912
Methyl tert-butyl ether (MTBE) 11/16/2017 5:23:13 AM0.0580 mg/Kg-dry 1ND
1,2-Dichloroethane 11/16/2017 5:23:13 AM0.0232 mg/Kg-dry 1ND
Benzene 11/16/2017 5:23:13 AM0.0232 mg/Kg-dry 10.126
Toluene 11/16/2017 5:23:13 AM0.0232 mg/Kg-dry 10.468
1,2-Dibromoethane (EDB) 11/16/2017 5:23:13 AM0.00580 mg/Kg-dry 1ND
Ethylbenzene 11/16/2017 5:23:13 AM0.0290 mg/Kg-dry 10.0833
m,p-Xylene 11/16/2017 5:23:13 AM0.0580 mg/Kg-dry 10.473
o-Xylene 11/16/2017 5:23:13 AM0.0290 mg/Kg-dry 10.191
Naphthalene 11/16/2017 5:23:13 AM0.0580 mg/Kg-dry 10.0823
Surr: Dibromofluoromethane 11/16/2017 5:23:13 AM56.5 - 129 %Rec 188.4
Surr: Toluene-d8 11/16/2017 5:23:13 AM64.5 - 151 %Rec 197.6
Surr: 1-Bromo-4-fluorobenzene 11/16/2017 5:23:13 AM43.2 - 143 %Rec 1101
Sample Moisture (Percent Moisture) Analyst: COBatch ID: R39843
Percent Moisture 11/10/2017 8:10:56 AM0.500 wt% 112.7
Original
Page 5 of 31
Project: NA Properties Everett
Client Sample ID: N72E21: 12ft
Collection Date: 11/9/2017 9:25:00 AM
Matrix: Soil
Client: Kane Environmental, Inc.
Lab ID: 1711164-002
Analyses Result Qual Units Date AnalyzedDFRL
Analytical Report
11/17/20171711164
Date Reported:
Work Order:
Gasoline by NWTPH-Gx Analyst: NGBatch ID: 18840
Gasoline 11/10/2017 3:13:47 AM6.62 mg/Kg-dry 1ND
Surr: 4-Bromofluorobenzene 11/10/2017 3:13:47 AM65 - 135 %Rec 1104
Surr: Toluene-d8 11/10/2017 3:13:47 AM65 - 135 %Rec 196.7
Volatile Organic Compounds by EPA Method 8260C Analyst: NGBatch ID: 18840
Benzene 11/10/2017 3:13:47 AM0.0265 mg/Kg-dry 1ND
Toluene 11/10/2017 3:13:47 AM0.0265 mg/Kg-dry 10.0329
Ethylbenzene 11/10/2017 3:13:47 AM0.0331 mg/Kg-dry 1ND
m,p-Xylene 11/10/2017 3:13:47 AM0.0662 mg/Kg-dry 10.141
o-Xylene 11/10/2017 3:13:47 AM0.0331 mg/Kg-dry 10.0582
Surr: Dibromofluoromethane 11/10/2017 3:13:47 AM56.5 - 129 %Rec 190.6
Surr: Toluene-d8 11/10/2017 3:13:47 AM64.5 - 151 %Rec 198.4
Surr: 1-Bromo-4-fluorobenzene 11/10/2017 3:13:47 AM43.2 - 143 %Rec 199.4
Sample Moisture (Percent Moisture) Analyst: COBatch ID: R39843
Percent Moisture 11/10/2017 8:10:56 AM0.500 wt% 110.8
Original
Page 6 of 31
Project: NA Properties Everett
Client Sample ID: N64E12: 8ft
Collection Date: 11/9/2017 9:55:00 AM
Matrix: Soil
Client: Kane Environmental, Inc.
Lab ID: 1711164-003
Analyses Result Qual Units Date AnalyzedDFRL
Analytical Report
11/17/20171711164
Date Reported:
Work Order:
Gasoline by NWTPH-Gx Analyst: MWBatch ID: 18912
Gasoline 11/16/2017 5:53:36 AM6.27 mg/Kg-dry 1ND
Surr: 4-Bromofluorobenzene 11/16/2017 5:53:36 AM65 - 135 %Rec 1105
Surr: Toluene-d8 11/16/2017 5:53:36 AM65 - 135 %Rec 198.8
Volatile Organic Compounds by EPA Method 8260C Analyst: MWBatch ID: 18912
Methyl tert-butyl ether (MTBE) 11/16/2017 5:53:36 AM0.0627 mg/Kg-dry 1ND
1,2-Dichloroethane 11/16/2017 5:53:36 AM0.0251 mg/Kg-dry 1ND
Benzene 11/16/2017 5:53:36 AM0.0251 mg/Kg-dry 1ND
Toluene 11/16/2017 5:53:36 AM0.0251 mg/Kg-dry 1ND
1,2-Dibromoethane (EDB) 11/16/2017 5:53:36 AM0.00627 mg/Kg-dry 1ND
Ethylbenzene 11/16/2017 5:53:36 AM0.0314 mg/Kg-dry 1ND
m,p-Xylene 11/16/2017 5:53:36 AM0.0627 mg/Kg-dry 10.0732
o-Xylene 11/16/2017 5:53:36 AM0.0314 mg/Kg-dry 1ND
Naphthalene 11/16/2017 5:53:36 AM0.0627 mg/Kg-dry 10.111
Surr: Dibromofluoromethane 11/16/2017 5:53:36 AM56.5 - 129 %Rec 188.6
Surr: Toluene-d8 11/16/2017 5:53:36 AM64.5 - 151 %Rec 1100
Surr: 1-Bromo-4-fluorobenzene 11/16/2017 5:53:36 AM43.2 - 143 %Rec 1101
Sample Moisture (Percent Moisture) Analyst: COBatch ID: R39843
Percent Moisture 11/10/2017 8:10:56 AM0.500 wt% 120.5
Original
Page 7 of 31
Project: NA Properties Everett
Client Sample ID: N70E31: 12ft
Collection Date: 11/9/2017 10:30:00 AM
Matrix: Soil
Client: Kane Environmental, Inc.
Lab ID: 1711164-004
Analyses Result Qual Units Date AnalyzedDFRL
Analytical Report
11/17/20171711164
Date Reported:
Work Order:
Gasoline by NWTPH-Gx Analyst: NGBatch ID: 18840
Gasoline 11/10/2017 3:44:48 AM6.67 mg/Kg-dry 1ND
Surr: 4-Bromofluorobenzene 11/10/2017 3:44:48 AM65 - 135 %Rec 1104
Surr: Toluene-d8 11/10/2017 3:44:48 AM65 - 135 %Rec 196.5
Volatile Organic Compounds by EPA Method 8260C Analyst: NGBatch ID: 18840
Benzene 11/10/2017 3:44:48 AM0.0267 mg/Kg-dry 1ND
Toluene 11/10/2017 3:44:48 AM0.0267 mg/Kg-dry 1ND
Ethylbenzene 11/10/2017 3:44:48 AM0.0333 mg/Kg-dry 1ND
m,p-Xylene 11/10/2017 3:44:48 AM0.0667 mg/Kg-dry 1ND
o-Xylene 11/10/2017 3:44:48 AM0.0333 mg/Kg-dry 1ND
Surr: Dibromofluoromethane 11/10/2017 3:44:48 AM56.5 - 129 %Rec 189.7
Surr: Toluene-d8 11/10/2017 3:44:48 AM64.5 - 151 %Rec 197.4
Surr: 1-Bromo-4-fluorobenzene 11/10/2017 3:44:48 AM43.2 - 143 %Rec 199.1
Sample Moisture (Percent Moisture) Analyst: COBatch ID: R39843
Percent Moisture 11/10/2017 8:10:56 AM0.500 wt% 128.4
Original
Page 8 of 31
Project: NA Properties Everett
Client Sample ID: N45E31: 12.5ft
Collection Date: 11/9/2017 11:30:00 AM
Matrix: Soil
Client: Kane Environmental, Inc.
Lab ID: 1711164-005
Analyses Result Qual Units Date AnalyzedDFRL
Analytical Report
11/17/20171711164
Date Reported:
Work Order:
Diesel and Heavy Oil by NWTPH-Dx/Dx Ext. Analyst: SBBatch ID: 18873
Diesel (Fuel Oil) 11/14/2017 4:16:58 AM19.7 mg/Kg-dry 1ND
Heavy Oil 11/14/2017 4:16:58 AM49.3 mg/Kg-dry 1ND
Surr: 2-Fluorobiphenyl 11/14/2017 4:16:58 AM50 - 150 %Rec 192.6
Surr: o-Terphenyl 11/14/2017 4:16:58 AM50 - 150 %Rec 1109
Gasoline by NWTPH-Gx Analyst: MWBatch ID: 18912
Gasoline 11/16/2017 12:30:02 PM5.33 mg/Kg-dry 1ND
Gasoline Range Organics C6-C12 D 11/16/2017 2:01:27 PM53.3 mg/Kg-dry 10153
Surr: 4-Bromofluorobenzene 11/16/2017 12:30:02 PM65 - 135 %Rec 1113
Surr: Toluene-d8 11/16/2017 12:30:02 PM65 - 135 %Rec 196.1
NOTES:GRO - Indicates the presence of unresolved compounds eluting from toluene to dodecane (~C6-C12).
Volatile Organic Compounds by EPA Method 8260C Analyst: MWBatch ID: 18912
Methyl tert-butyl ether (MTBE) 11/16/2017 12:30:02 PM0.0533 mg/Kg-dry 1ND
1,2-Dichloroethane 11/16/2017 12:30:02 PM0.0213 mg/Kg-dry 1ND
Benzene 11/16/2017 12:30:02 PM0.0213 mg/Kg-dry 1ND
Toluene 11/16/2017 12:30:02 PM0.0213 mg/Kg-dry 1ND
1,2-Dibromoethane (EDB) 11/16/2017 12:30:02 PM0.00533 mg/Kg-dry 1ND
Ethylbenzene 11/16/2017 12:30:02 PM0.0266 mg/Kg-dry 10.928
m,p-Xylene 11/16/2017 12:30:02 PM0.0533 mg/Kg-dry 1ND
o-Xylene 11/16/2017 12:30:02 PM0.0266 mg/Kg-dry 1ND
Naphthalene 11/16/2017 12:30:02 PM0.0533 mg/Kg-dry 13.95
Surr: Dibromofluoromethane 11/16/2017 12:30:02 PM56.5 - 129 %Rec 192.5
Surr: Toluene-d8 11/16/2017 12:30:02 PM64.5 - 151 %Rec 1103
Surr: 1-Bromo-4-fluorobenzene 11/16/2017 12:30:02 PM43.2 - 143 %Rec 1108
Sample Moisture (Percent Moisture) Analyst: COBatch ID: R39843
Percent Moisture 11/10/2017 8:10:56 AM0.500 wt% 113.6
Original
Page 9 of 31
Project: NA Properties Everett
Client Sample ID: N71E40: 12.5ft
Collection Date: 11/9/2017 12:10:00 PM
Matrix: Soil
Client: Kane Environmental, Inc.
Lab ID: 1711164-006
Analyses Result Qual Units Date AnalyzedDFRL
Analytical Report
11/17/20171711164
Date Reported:
Work Order:
Gasoline by NWTPH-Gx Analyst: NGBatch ID: 18840
Gasoline 11/10/2017 4:15:45 AM4.83 mg/Kg-dry 1ND
Surr: 4-Bromofluorobenzene 11/10/2017 4:15:45 AM65 - 135 %Rec 1103
Surr: Toluene-d8 11/10/2017 4:15:45 AM65 - 135 %Rec 197.0
Volatile Organic Compounds by EPA Method 8260C Analyst: NGBatch ID: 18840
Benzene 11/10/2017 4:15:45 AM0.0193 mg/Kg-dry 1ND
Toluene 11/10/2017 4:15:45 AM0.0193 mg/Kg-dry 1ND
Ethylbenzene 11/10/2017 4:15:45 AM0.0242 mg/Kg-dry 1ND
m,p-Xylene 11/10/2017 4:15:45 AM0.0483 mg/Kg-dry 1ND
o-Xylene 11/10/2017 4:15:45 AM0.0242 mg/Kg-dry 1ND
Surr: Dibromofluoromethane 11/10/2017 4:15:45 AM56.5 - 129 %Rec 189.9
Surr: Toluene-d8 11/10/2017 4:15:45 AM64.5 - 151 %Rec 197.7
Surr: 1-Bromo-4-fluorobenzene 11/10/2017 4:15:45 AM43.2 - 143 %Rec 198.0
Sample Moisture (Percent Moisture) Analyst: COBatch ID: R39843
Percent Moisture 11/10/2017 8:10:56 AM0.500 wt% 17.75
Original
Page 10 of 31
Project: NA Properties Everett
Client Sample ID: N46E41: 12.5ft
Collection Date: 11/9/2017 12:25:00 PM
Matrix: Soil
Client: Kane Environmental, Inc.
Lab ID: 1711164-007
Analyses Result Qual Units Date AnalyzedDFRL
Analytical Report
11/17/20171711164
Date Reported:
Work Order:
Gasoline by NWTPH-Gx Analyst: MWBatch ID: 18912
Gasoline 11/16/2017 6:24:02 AM6.96 mg/Kg-dry 17.58
Surr: 4-Bromofluorobenzene 11/16/2017 6:24:02 AM65 - 135 %Rec 1102
Surr: Toluene-d8 11/16/2017 6:24:02 AM65 - 135 %Rec 1100
Volatile Organic Compounds by EPA Method 8260C Analyst: MWBatch ID: 18912
Methyl tert-butyl ether (MTBE) 11/16/2017 6:24:02 AM0.0696 mg/Kg-dry 1ND
1,2-Dichloroethane 11/16/2017 6:24:02 AM0.0278 mg/Kg-dry 1ND
Benzene 11/16/2017 6:24:02 AM0.0278 mg/Kg-dry 1ND
Toluene 11/16/2017 6:24:02 AM0.0278 mg/Kg-dry 1ND
1,2-Dibromoethane (EDB) 11/16/2017 6:24:02 AM0.00696 mg/Kg-dry 1ND
Ethylbenzene 11/16/2017 6:24:02 AM0.0348 mg/Kg-dry 1ND
m,p-Xylene 11/16/2017 6:24:02 AM0.0696 mg/Kg-dry 1ND
o-Xylene 11/16/2017 6:24:02 AM0.0348 mg/Kg-dry 1ND
Naphthalene 11/16/2017 6:24:02 AM0.0696 mg/Kg-dry 1ND
Surr: Dibromofluoromethane 11/16/2017 6:24:02 AM56.5 - 129 %Rec 188.7
Surr: Toluene-d8 11/16/2017 6:24:02 AM64.5 - 151 %Rec 195.2
Surr: 1-Bromo-4-fluorobenzene 11/16/2017 6:24:02 AM43.2 - 143 %Rec 198.8
Sample Moisture (Percent Moisture) Analyst: COBatch ID: R39843
Percent Moisture 11/10/2017 8:10:56 AM0.500 wt% 126.5
Original
Page 11 of 31
Project: NA Properties Everett
Client Sample ID: N60E48: 9ft
Collection Date: 11/9/2017 1:15:00 PM
Matrix: Soil
Client: Kane Environmental, Inc.
Lab ID: 1711164-009
Analyses Result Qual Units Date AnalyzedDFRL
Analytical Report
11/17/20171711164
Date Reported:
Work Order:
Gasoline by NWTPH-Gx Analyst: MWBatch ID: 18912
Gasoline 11/16/2017 10:28:01 AM6.66 mg/Kg-dry 1ND
Surr: 4-Bromofluorobenzene 11/16/2017 10:28:01 AM65 - 135 %Rec 1106
Surr: Toluene-d8 11/16/2017 10:28:01 AM65 - 135 %Rec 197.2
Volatile Organic Compounds by EPA Method 8260C Analyst: MWBatch ID: 18912
Methyl tert-butyl ether (MTBE) 11/16/2017 10:28:01 AM0.0666 mg/Kg-dry 1ND
1,2-Dichloroethane 11/16/2017 10:28:01 AM0.0266 mg/Kg-dry 1ND
Benzene 11/16/2017 10:28:01 AM0.0266 mg/Kg-dry 1ND
Toluene 11/16/2017 10:28:01 AM0.0266 mg/Kg-dry 1ND
1,2-Dibromoethane (EDB) 11/16/2017 10:28:01 AM0.00666 mg/Kg-dry 1ND
Ethylbenzene 11/16/2017 10:28:01 AM0.0333 mg/Kg-dry 1ND
m,p-Xylene 11/16/2017 10:28:01 AM0.0666 mg/Kg-dry 1ND
o-Xylene 11/16/2017 10:28:01 AM0.0333 mg/Kg-dry 1ND
Naphthalene 11/16/2017 10:28:01 AM0.0666 mg/Kg-dry 1ND
Surr: Dibromofluoromethane 11/16/2017 10:28:01 AM56.5 - 129 %Rec 192.4
Surr: Toluene-d8 11/16/2017 10:28:01 AM64.5 - 151 %Rec 197.2
Surr: 1-Bromo-4-fluorobenzene 11/16/2017 10:28:01 AM43.2 - 143 %Rec 1102
Sample Moisture (Percent Moisture) Analyst: COBatch ID: R39843
Percent Moisture 11/10/2017 8:10:56 AM0.500 wt% 125.0
Original
Page 12 of 31
Project: NA Properties Everett
Client Sample ID: N40E32: 9.5ft
Collection Date: 11/9/2017 1:30:00 PM
Matrix: Soil
Client: Kane Environmental, Inc.
Lab ID: 1711164-010
Analyses Result Qual Units Date AnalyzedDFRL
Analytical Report
11/17/20171711164
Date Reported:
Work Order:
Gasoline by NWTPH-Gx Analyst: MWBatch ID: 18912
Gasoline 11/16/2017 1:31:00 PM5.67 mg/Kg-dry 1ND
Gasoline Range Organics C6-C12 D 11/16/2017 2:32:09 PM113 mg/Kg-dry 20349
Surr: 4-Bromofluorobenzene 11/16/2017 1:31:00 PM65 - 135 %Rec 1123
Surr: Toluene-d8 11/16/2017 1:31:00 PM65 - 135 %Rec 197.4
NOTES:GRO - Indicates the presence of unresolved compounds eluting from toluene to dodecane (~C6-C12).
Volatile Organic Compounds by EPA Method 8260C Analyst: MWBatch ID: 18912
Methyl tert-butyl ether (MTBE) 11/16/2017 1:31:00 PM0.0567 mg/Kg-dry 1ND
1,2-Dichloroethane 11/16/2017 1:31:00 PM0.0227 mg/Kg-dry 1ND
Benzene 11/16/2017 1:31:00 PM0.0227 mg/Kg-dry 10.558
Toluene 11/16/2017 1:31:00 PM0.0227 mg/Kg-dry 10.147
1,2-Dibromoethane (EDB) 11/16/2017 1:31:00 PM0.00567 mg/Kg-dry 1ND
Ethylbenzene D 11/16/2017 2:32:09 PM0.567 mg/Kg-dry 202.74
m,p-Xylene 11/16/2017 1:31:00 PM0.0567 mg/Kg-dry 10.960
o-Xylene 11/16/2017 1:31:00 PM0.0284 mg/Kg-dry 1ND
Naphthalene D 11/16/2017 2:32:09 PM1.13 mg/Kg-dry 209.60
Surr: Dibromofluoromethane 11/16/2017 1:31:00 PM56.5 - 129 %Rec 192.3
Surr: Toluene-d8 11/16/2017 1:31:00 PM64.5 - 151 %Rec 1107
Surr: 1-Bromo-4-fluorobenzene 11/16/2017 1:31:00 PM43.2 - 143 %Rec 1117
Sample Moisture (Percent Moisture) Analyst: COBatch ID: R39843
Percent Moisture 11/10/2017 8:10:56 AM0.500 wt% 120.2
Original
Page 13 of 31
Project: NA Properties Everett
Client Sample ID: N42E17: 5.5ft
Collection Date: 11/9/2017 1:45:00 PM
Matrix: Soil
Client: Kane Environmental, Inc.
Lab ID: 1711164-011
Analyses Result Qual Units Date AnalyzedDFRL
Analytical Report
11/17/20171711164
Date Reported:
Work Order:
Diesel and Heavy Oil by NWTPH-Dx/Dx Ext. Analyst: SBBatch ID: 18873
Diesel (Fuel Oil) 11/14/2017 4:46:28 AM21.1 mg/Kg-dry 1ND
Diesel Range Organics (C12-C24) 11/14/2017 4:46:28 AM21.1 mg/Kg-dry 1165
Heavy Oil 11/14/2017 4:46:28 AM52.9 mg/Kg-dry 1ND
Surr: 2-Fluorobiphenyl 11/14/2017 4:46:28 AM50 - 150 %Rec 1117
Surr: o-Terphenyl 11/14/2017 4:46:28 AM50 - 150 %Rec 1119
NOTES:DRO - Indicates the presence of unresolved compounds eluting from dodecane through tetracosane (~C12-C24).
Gasoline by NWTPH-Gx Analyst: MWBatch ID: 18912
Gasoline D 11/16/2017 11:59:31 AM772 mg/Kg-dry 2008,840
Surr: 4-Bromofluorobenzene D 11/16/2017 11:59:31 AM65 - 135 %Rec 200104
Surr: Toluene-d8 D 11/16/2017 11:59:31 AM65 - 135 %Rec 20095.5
Volatile Organic Compounds by EPA Method 8260C Analyst: MWBatch ID: 18912
Methyl tert-butyl ether (MTBE) D 11/16/2017 10:58:33 AM0.772 mg/Kg-dry 20ND
1,2-Dichloroethane D 11/16/2017 10:58:33 AM0.309 mg/Kg-dry 20ND
Benzene D 11/16/2017 11:59:31 AM3.09 mg/Kg-dry 20078.7
Toluene DE 11/16/2017 11:59:31 AM3.09 mg/Kg-dry 200497
1,2-Dibromoethane (EDB) D 11/16/2017 10:58:33 AM0.0772 mg/Kg-dry 20ND
Ethylbenzene D 11/16/2017 11:59:31 AM3.86 mg/Kg-dry 200153
m,p-Xylene D 11/16/2017 11:59:31 AM7.72 mg/Kg-dry 200639
o-Xylene D 11/16/2017 11:59:31 AM3.86 mg/Kg-dry 200230
Naphthalene D 11/16/2017 10:58:33 AM0.772 mg/Kg-dry 2024.7
Surr: Dibromofluoromethane D 11/16/2017 10:58:33 AM56.5 - 129 %Rec 2091.4
Surr: Toluene-d8 D 11/16/2017 10:58:33 AM64.5 - 151 %Rec 20103
Surr: 1-Bromo-4-fluorobenzene D 11/16/2017 10:58:33 AM43.2 - 143 %Rec 20103
NOTES:E - Estimated value. The amount exceeds the linear working range of the instrument.
Diluted due to matrix.
Sample Moisture (Percent Moisture) Analyst: COBatch ID: R39843
Percent Moisture 11/10/2017 8:10:56 AM0.500 wt% 17.08
Original
Page 14 of 31
Project: NA Properties Everett
Client Sample ID: SP-1-110917
Collection Date: 11/9/2017 2:20:00 PM
Matrix: Soil
Client: Kane Environmental, Inc.
Lab ID: 1711164-013
Analyses Result Qual Units Date AnalyzedDFRL
Analytical Report
11/17/20171711164
Date Reported:
Work Order:
Gasoline by NWTPH-Gx Analyst: NGBatch ID: 18840
Gasoline 11/10/2017 4:46:42 AM4.33 mg/Kg-dry 1ND
Surr: 4-Bromofluorobenzene 11/10/2017 4:46:42 AM65 - 135 %Rec 1102
Surr: Toluene-d8 11/10/2017 4:46:42 AM65 - 135 %Rec 196.8
Volatile Organic Compounds by EPA Method 8260C Analyst: NGBatch ID: 18840
Methyl tert-butyl ether (MTBE) 11/10/2017 4:46:42 AM0.0433 mg/Kg-dry 1ND
1,2-Dichloroethane 11/10/2017 4:46:42 AM0.0173 mg/Kg-dry 1ND
Benzene 11/10/2017 4:46:42 AM0.0173 mg/Kg-dry 1ND
Toluene 11/10/2017 4:46:42 AM0.0173 mg/Kg-dry 1ND
1,2-Dibromoethane (EDB) 11/10/2017 4:46:42 AM0.00433 mg/Kg-dry 1ND
Ethylbenzene 11/10/2017 4:46:42 AM0.0217 mg/Kg-dry 1ND
m,p-Xylene 11/10/2017 4:46:42 AM0.0433 mg/Kg-dry 1ND
o-Xylene 11/10/2017 4:46:42 AM0.0217 mg/Kg-dry 1ND
Naphthalene Q 11/10/2017 4:46:42 AM0.0433 mg/Kg-dry 1ND
Surr: Dibromofluoromethane 11/10/2017 4:46:42 AM56.5 - 129 %Rec 189.3
Surr: Toluene-d8 11/10/2017 4:46:42 AM64.5 - 151 %Rec 197.2
Surr: 1-Bromo-4-fluorobenzene 11/10/2017 4:46:42 AM43.2 - 143 %Rec 197.6
NOTES:Q - Indicates an analyte with a continuing calibration that does not meet established acceptance criteria (<20%RSD, <20% Drift or minimum RRF).
Sample Moisture (Percent Moisture) Analyst: COBatch ID: R39843
Percent Moisture 11/10/2017 8:10:56 AM0.500 wt% 15.57
Original
Page 15 of 31
Project: NA Properties Everett
Client Sample ID: SP-2-110917
Collection Date: 11/9/2017 2:30:00 PM
Matrix: Soil
Client: Kane Environmental, Inc.
Lab ID: 1711164-014
Analyses Result Qual Units Date AnalyzedDFRL
Analytical Report
11/17/20171711164
Date Reported:
Work Order:
Gasoline by NWTPH-Gx Analyst: NGBatch ID: 18840
Gasoline 11/10/2017 5:17:39 AM6.89 mg/Kg-dry 1ND
Surr: 4-Bromofluorobenzene 11/10/2017 5:17:39 AM65 - 135 %Rec 1104
Surr: Toluene-d8 11/10/2017 5:17:39 AM65 - 135 %Rec 196.1
Volatile Organic Compounds by EPA Method 8260C Analyst: NGBatch ID: 18840
Methyl tert-butyl ether (MTBE) 11/10/2017 5:17:39 AM0.0689 mg/Kg-dry 1ND
1,2-Dichloroethane 11/10/2017 5:17:39 AM0.0276 mg/Kg-dry 1ND
Benzene 11/10/2017 5:17:39 AM0.0276 mg/Kg-dry 1ND
Toluene 11/10/2017 5:17:39 AM0.0276 mg/Kg-dry 10.0277
1,2-Dibromoethane (EDB) 11/10/2017 5:17:39 AM0.00689 mg/Kg-dry 1ND
Ethylbenzene 11/10/2017 5:17:39 AM0.0345 mg/Kg-dry 1ND
m,p-Xylene 11/10/2017 5:17:39 AM0.0689 mg/Kg-dry 1ND
o-Xylene 11/10/2017 5:17:39 AM0.0345 mg/Kg-dry 10.0356
Naphthalene Q 11/10/2017 5:17:39 AM0.0689 mg/Kg-dry 1ND
Surr: Dibromofluoromethane 11/10/2017 5:17:39 AM56.5 - 129 %Rec 189.1
Surr: Toluene-d8 11/10/2017 5:17:39 AM64.5 - 151 %Rec 198.0
Surr: 1-Bromo-4-fluorobenzene 11/10/2017 5:17:39 AM43.2 - 143 %Rec 199.1
NOTES:Q - Indicates an analyte with a continuing calibration that does not meet established acceptance criteria (<20%RSD, <20% Drift or minimum RRF).
Sample Moisture (Percent Moisture) Analyst: COBatch ID: R39843
Percent Moisture 11/10/2017 8:10:56 AM0.500 wt% 18.68
Original
Page 16 of 31
Project: NA Properties Everett
Client Sample ID: SP-3-110917
Collection Date: 11/9/2017 2:40:00 PM
Matrix: Soil
Client: Kane Environmental, Inc.
Lab ID: 1711164-015
Analyses Result Qual Units Date AnalyzedDFRL
Analytical Report
11/17/20171711164
Date Reported:
Work Order:
Gasoline by NWTPH-Gx Analyst: NGBatch ID: 18840
Gasoline 11/10/2017 5:48:35 AM8.10 mg/Kg-dry 1ND
Surr: 4-Bromofluorobenzene 11/10/2017 5:48:35 AM65 - 135 %Rec 1103
Surr: Toluene-d8 11/10/2017 5:48:35 AM65 - 135 %Rec 198.0
Volatile Organic Compounds by EPA Method 8260C Analyst: NGBatch ID: 18840
Methyl tert-butyl ether (MTBE) 11/10/2017 5:48:35 AM0.0810 mg/Kg-dry 1ND
1,2-Dichloroethane 11/10/2017 5:48:35 AM0.0324 mg/Kg-dry 1ND
Benzene 11/10/2017 5:48:35 AM0.0324 mg/Kg-dry 1ND
Toluene 11/10/2017 5:48:35 AM0.0324 mg/Kg-dry 1ND
1,2-Dibromoethane (EDB) 11/10/2017 5:48:35 AM0.00810 mg/Kg-dry 1ND
Ethylbenzene 11/10/2017 5:48:35 AM0.0405 mg/Kg-dry 1ND
m,p-Xylene 11/10/2017 5:48:35 AM0.0810 mg/Kg-dry 1ND
o-Xylene 11/10/2017 5:48:35 AM0.0405 mg/Kg-dry 1ND
Naphthalene Q 11/10/2017 5:48:35 AM0.0810 mg/Kg-dry 1ND
Surr: Dibromofluoromethane 11/10/2017 5:48:35 AM56.5 - 129 %Rec 187.7
Surr: Toluene-d8 11/10/2017 5:48:35 AM64.5 - 151 %Rec 191.5
Surr: 1-Bromo-4-fluorobenzene 11/10/2017 5:48:35 AM43.2 - 143 %Rec 197.9
NOTES:Q - Indicates an analyte with a continuing calibration that does not meet established acceptance criteria (<20%RSD, <20% Drift or minimum RRF).
Sample Moisture (Percent Moisture) Analyst: COBatch ID: R39843
Percent Moisture 11/10/2017 8:10:56 AM0.500 wt% 17.08
Original
Page 17 of 31
Project: NA Properties Everett
CLIENT: Kane Environmental, Inc.
Work Order: 1711164 QC SUMMARY REPORTDiesel and Heavy Oil by NWTPH-Dx/Dx Ext.
11/17/2017Date:
Sample ID MB-18873
Batch ID: 18873 Analysis Date: 11/13/2017
Prep Date: 11/13/2017
Analyte Result SPK value SPK Ref Val %REC RPD Ref Val %RPDLowLimit HighLimit RPDLimit Qual
Units: mg/Kg
RL
Client ID: MBLKS
RunNo: 39893
SeqNo: 768060
MBLKSampType:
Diesel (Fuel Oil) 20.0ND
Heavy Oil 50.0ND
Surr: 2-Fluorobiphenyl 20.00 94.8 50 15019.0
Surr: o-Terphenyl 20.00 107 50 15021.4
Sample ID LCS-18873
Batch ID: 18873 Analysis Date: 11/13/2017
Prep Date: 11/13/2017
Analyte Result SPK value SPK Ref Val %REC RPD Ref Val %RPDLowLimit HighLimit RPDLimit Qual
Units: mg/Kg
RL
Client ID: LCSS
RunNo: 39893
SeqNo: 768061
LCSSampType:
Diesel (Fuel Oil) 500.0 102 65 13520.0 0511
Surr: 2-Fluorobiphenyl 20.00 99.2 50 15019.8
Surr: o-Terphenyl 20.00 112 50 15022.3
Sample ID 1711193-001ADUP
Batch ID: 18873 Analysis Date: 11/13/2017
Prep Date: 11/13/2017
Analyte Result SPK value SPK Ref Val %REC RPD Ref Val %RPDLowLimit HighLimit RPDLimit Qual
Units: mg/Kg-dry
RL
Client ID: BATCH
RunNo: 39893
SeqNo: 768063
DUPSampType:
Diesel (Fuel Oil) 3022.2 0ND
Heavy Oil 30 E55.5 3,254 2.363,180
Surr: 2-Fluorobiphenyl 22.20 101 50 150 022.5
Surr: o-Terphenyl 22.20 115 50 150 025.5
NOTES:E - Estimated value. The amount exceeds the linear working range of the instrument.
Sample ID 1711193-001AMS
Batch ID: 18873 Analysis Date: 11/13/2017
Prep Date: 11/13/2017
Analyte Result SPK value SPK Ref Val %REC RPD Ref Val %RPDLowLimit HighLimit RPDLimit Qual
Units: mg/Kg-dry
RL
Client ID: BATCH
RunNo: 39893
SeqNo: 768064
MSSampType:
Diesel (Fuel Oil) 511.0 127 65 13520.4 0649
Surr: 2-Fluorobiphenyl 20.44 105 50 15021.5
Original Page 18 of 31
Project: NA Properties Everett
CLIENT: Kane Environmental, Inc.
Work Order: 1711164 QC SUMMARY REPORTDiesel and Heavy Oil by NWTPH-Dx/Dx Ext.
11/17/2017Date:
Sample ID 1711193-001AMS
Batch ID: 18873 Analysis Date: 11/13/2017
Prep Date: 11/13/2017
Analyte Result SPK value SPK Ref Val %REC RPD Ref Val %RPDLowLimit HighLimit RPDLimit Qual
Units: mg/Kg-dry
RL
Client ID: BATCH
RunNo: 39893
SeqNo: 768064
MSSampType:
Surr: o-Terphenyl 20.44 124 50 15025.4
Sample ID 1711193-001AMSD
Batch ID: 18873 Analysis Date: 11/13/2017
Prep Date: 11/13/2017
Analyte Result SPK value SPK Ref Val %REC RPD Ref Val %RPDLowLimit HighLimit RPDLimit Qual
Units: mg/Kg-dry
RL
Client ID: BATCH
RunNo: 39893
SeqNo: 768065
MSDSampType:
Diesel (Fuel Oil) 506.8 106 65 135 3020.3 0 648.6 19.0536
Surr: 2-Fluorobiphenyl 20.27 106 50 150 021.5
Surr: o-Terphenyl 20.27 126 50 150 025.5
Sample ID 1711184-001ADUP
Batch ID: 18873 Analysis Date: 11/14/2017
Prep Date: 11/13/2017
Analyte Result SPK value SPK Ref Val %REC RPD Ref Val %RPDLowLimit HighLimit RPDLimit Qual
Units: mg/Kg-dry
RL
Client ID: BATCH
RunNo: 39893
SeqNo: 768077
DUPSampType:
Diesel (Fuel Oil) 3022.2 0ND
Heavy Oil 3055.5 0ND
Surr: 2-Fluorobiphenyl 22.22 98.2 50 150 021.8
Surr: o-Terphenyl 22.22 111 50 150 024.8
Original Page 19 of 31
Project: NA Properties Everett
CLIENT: Kane Environmental, Inc.
Work Order: 1711164 QC SUMMARY REPORTGasoline by NWTPH-Gx
11/17/2017Date:
Sample ID MB-18912
Batch ID: 18912 Analysis Date: 11/15/2017
Prep Date: 11/15/2017
Analyte Result SPK value SPK Ref Val %REC RPD Ref Val %RPDLowLimit HighLimit RPDLimit Qual
Units: mg/Kg
RL
Client ID: MBLKS
RunNo: 39963
SeqNo: 769478
MBLKSampType:
Gasoline 5.00ND
Surr: Toluene-d8 1.250 99.2 65 1351.24
Surr: 4-Bromofluorobenzene 1.250 102 65 1351.27
Sample ID LCS-18912
Batch ID: 18912 Analysis Date: 11/15/2017
Prep Date: 11/15/2017
Analyte Result SPK value SPK Ref Val %REC RPD Ref Val %RPDLowLimit HighLimit RPDLimit Qual
Units: mg/Kg
RL
Client ID: LCSS
RunNo: 39963
SeqNo: 769477
LCSSampType:
Gasoline 25.00 82.1 65 1355.00 020.5
Surr: Toluene-d8 1.250 100 65 1351.25
Surr: 4-Bromofluorobenzene 1.250 102 65 1351.28
Sample ID 1711157-002BDUP
Batch ID: 18912 Analysis Date: 11/16/2017
Prep Date: 11/15/2017
Analyte Result SPK value SPK Ref Val %REC RPD Ref Val %RPDLowLimit HighLimit RPDLimit Qual
Units: mg/Kg-dry
RL
Client ID: BATCH
RunNo: 39963
SeqNo: 769458
DUPSampType:
Gasoline 305.93 0ND
Surr: Toluene-d8 1.483 98.0 65 135 01.45
Surr: 4-Bromofluorobenzene 1.483 103 65 135 01.52
Sample ID 1711164-007BDUP
Batch ID: 18912 Analysis Date: 11/16/2017
Prep Date: 11/15/2017
Analyte Result SPK value SPK Ref Val %REC RPD Ref Val %RPDLowLimit HighLimit RPDLimit Qual
Units: mg/Kg-dry
RL
Client ID: N46E41: 12.5ft
RunNo: 39963
SeqNo: 769468
DUPSampType:
Gasoline 306.80 7.581 22.5ND
Surr: Toluene-d8 1.701 102 65 135 01.73
Surr: 4-Bromofluorobenzene 1.701 102 65 135 01.73
Original Page 20 of 31
Project: NA Properties Everett
CLIENT: Kane Environmental, Inc.
Work Order: 1711164 QC SUMMARY REPORTGasoline by NWTPH-Gx
11/17/2017Date:
Sample ID LCS-18840
Batch ID: 18840 Analysis Date: 11/10/2017
Prep Date: 11/9/2017
Analyte Result SPK value SPK Ref Val %REC RPD Ref Val %RPDLowLimit HighLimit RPDLimit Qual
Units: mg/Kg
RL
Client ID: LCSS
RunNo: 39840
SeqNo: 766942
LCSSampType:
Gasoline 25.00 102 65 1355.00 025.5
Surr: Toluene-d8 1.250 97.9 65 1351.22
Surr: 4-Bromofluorobenzene 1.250 97.2 65 1351.22
Sample ID MB-18840
Batch ID: 18840 Analysis Date: 11/10/2017
Prep Date: 11/9/2017
Analyte Result SPK value SPK Ref Val %REC RPD Ref Val %RPDLowLimit HighLimit RPDLimit Qual
Units: mg/Kg
RL
Client ID: MBLKS
RunNo: 39840
SeqNo: 766943
MBLKSampType:
Gasoline 5.00ND
Surr: Toluene-d8 1.250 99.5 65 1351.24
Surr: 4-Bromofluorobenzene 1.250 93.8 65 1351.17
Sample ID 1711141-002BDUP
Batch ID: 18840 Analysis Date: 11/10/2017
Prep Date: 11/9/2017
Analyte Result SPK value SPK Ref Val %REC RPD Ref Val %RPDLowLimit HighLimit RPDLimit Qual
Units: mg/Kg-dry
RL
Client ID: BATCH
RunNo: 39840
SeqNo: 767563
DUPSampType:
Gasoline 307.88 0ND
Surr: Toluene-d8 1.971 101 65 135 01.99
Surr: 4-Bromofluorobenzene 1.971 96.2 65 135 01.90
Sample ID 1711141-005BMS
Batch ID: 18840 Analysis Date: 11/10/2017
Prep Date: 11/9/2017
Analyte Result SPK value SPK Ref Val %REC RPD Ref Val %RPDLowLimit HighLimit RPDLimit Qual
Units: mg/Kg-dry
RL
Client ID: BATCH
RunNo: 39840
SeqNo: 767566
MSSampType:
Gasoline 23.84 71.6 65 1354.77 017.1
Surr: Toluene-d8 1.192 98.7 65 1351.18
Surr: 4-Bromofluorobenzene 1.192 98.5 65 1351.17
Original Page 21 of 31
Project: NA Properties Everett
CLIENT: Kane Environmental, Inc.
Work Order: 1711164 QC SUMMARY REPORTGasoline by NWTPH-Gx
11/17/2017Date:
Sample ID 1711141-005BMSD
Batch ID: 18840 Analysis Date: 11/10/2017
Prep Date: 11/9/2017
Analyte Result SPK value SPK Ref Val %REC RPD Ref Val %RPDLowLimit HighLimit RPDLimit Qual
Units: mg/Kg-dry
RL
Client ID: BATCH
RunNo: 39840
SeqNo: 767567
MSDSampType:
Gasoline 23.84 61.6 65 135 30 S4.77 0 17.07 15.114.7
Surr: Toluene-d8 1.192 98.3 65 135 01.17
Surr: 4-Bromofluorobenzene 1.192 99.9 65 135 01.19
NOTES:S - Outlying spike recovery(ies) observed. A duplicate analysis was performed and recovered within range.
Original Page 22 of 31
Project: NA Properties Everett
CLIENT: Kane Environmental, Inc.
Work Order: 1711164 QC SUMMARY REPORTSample Moisture (Percent Moisture)
11/17/2017Date:
Sample ID 1711164-001ADUP
Batch ID: R39843 Analysis Date: 11/10/2017
Prep Date: 11/10/2017
Analyte Result SPK value SPK Ref Val %REC RPD Ref Val %RPDLowLimit HighLimit RPDLimit Qual
Units: wt%
RL
Client ID: N50E20: 12ft
RunNo: 39843
SeqNo: 766975
DUPSampType:
Percent Moisture 200.500 12.66 20.010.4
Sample ID 1711167-007ADUP
Batch ID: R39843 Analysis Date: 11/10/2017
Prep Date: 11/10/2017
Analyte Result SPK value SPK Ref Val %REC RPD Ref Val %RPDLowLimit HighLimit RPDLimit Qual
Units: wt%
RL
Client ID: BATCH
RunNo: 39843
SeqNo: 766995
DUPSampType:
Percent Moisture 200.500 11.10 0.45611.2
Original Page 23 of 31
Project: NA Properties Everett
CLIENT: Kane Environmental, Inc.
Work Order: 1711164 QC SUMMARY REPORTVolatile Organic Compounds by EPA Method 8260C
11/17/2017Date:
Sample ID MB-18912
Batch ID: 18912 Analysis Date: 11/15/2017
Prep Date: 11/15/2017
Analyte Result SPK value SPK Ref Val %REC RPD Ref Val %RPDLowLimit HighLimit RPDLimit Qual
Units: mg/Kg
RL
Client ID: MBLKS
RunNo: 39966
SeqNo: 769533
MBLKSampType:
Methyl tert-butyl ether (MTBE) 0.0500ND
1,2-Dichloroethane 0.0200ND
Benzene 0.0200ND
Toluene 0.0200ND
1,2-Dibromoethane (EDB) 0.00500ND
Ethylbenzene 0.0250ND
m,p-Xylene 0.0500ND
o-Xylene 0.0250ND
Naphthalene 0.0500ND
Surr: Dibromofluoromethane 1.250 89.9 56.5 1291.12
Surr: Toluene-d8 1.250 97.7 64.5 1511.22
Surr: 1-Bromo-4-fluorobenzene 1.250 98.3 43.2 1431.23
Sample ID LCS-18912
Batch ID: 18912 Analysis Date: 11/15/2017
Prep Date: 11/15/2017
Analyte Result SPK value SPK Ref Val %REC RPD Ref Val %RPDLowLimit HighLimit RPDLimit Qual
Units: mg/Kg
RL
Client ID: LCSS
RunNo: 39966
SeqNo: 769532
LCSSampType:
Methyl tert-butyl ether (MTBE) 1.000 101 66.3 1450.0500 01.01
1,2-Dichloroethane 1.000 93.6 50.9 1620.0200 00.936
Benzene 1.000 97.1 64.3 1330.0200 00.971
Toluene 1.000 93.6 67.3 1380.0200 00.936
1,2-Dibromoethane (EDB) 1.000 93.1 50.5 1540.00500 00.931
Ethylbenzene 1.000 101 74 1290.0250 01.01
m,p-Xylene 2.000 102 70 1240.0500 02.04
o-Xylene 1.000 96.6 68.1 1390.0250 00.966
Naphthalene 1.000 104 58.4 1600.0500 01.04
Surr: Dibromofluoromethane 1.250 95.8 56.5 1291.20
Surr: Toluene-d8 1.250 99.8 64.5 1511.25
Surr: 1-Bromo-4-fluorobenzene 1.250 104 43.2 1431.30
Original Page 24 of 31
Project: NA Properties Everett
CLIENT: Kane Environmental, Inc.
Work Order: 1711164 QC SUMMARY REPORTVolatile Organic Compounds by EPA Method 8260C
11/17/2017Date:
Sample ID 1711157-002BDUP
Batch ID: 18912 Analysis Date: 11/16/2017
Prep Date: 11/15/2017
Analyte Result SPK value SPK Ref Val %REC RPD Ref Val %RPDLowLimit HighLimit RPDLimit Qual
Units: mg/Kg-dry
RL
Client ID: BATCH
RunNo: 39966
SeqNo: 769513
DUPSampType:
Methyl tert-butyl ether (MTBE) 300.0593 0ND
1,2-Dichloroethane 300.0237 0ND
Benzene 300.0237 0ND
Toluene 300.0237 0ND
1,2-Dibromoethane (EDB) 300.00593 0ND
Ethylbenzene 300.0297 0ND
m,p-Xylene 300.0593 0ND
o-Xylene 300.0297 0ND
Naphthalene 300.0593 0ND
Surr: Dibromofluoromethane 1.483 89.0 56.5 129 01.32
Surr: Toluene-d8 1.483 96.7 64.5 151 01.43
Surr: 1-Bromo-4-fluorobenzene 1.483 99.1 43.2 143 01.47
Sample ID 1711164-007BDUP
Batch ID: 18912 Analysis Date: 11/16/2017
Prep Date: 11/15/2017
Analyte Result SPK value SPK Ref Val %REC RPD Ref Val %RPDLowLimit HighLimit RPDLimit Qual
Units: mg/Kg-dry
RL
Client ID: N46E41: 12.5ft
RunNo: 39966
SeqNo: 769523
DUPSampType:
Methyl tert-butyl ether (MTBE) 300.0680 0ND
1,2-Dichloroethane 300.0272 0ND
Benzene 300.0272 0ND
Toluene 300.0272 0ND
1,2-Dibromoethane (EDB) 300.00680 0ND
Ethylbenzene 300.0340 0ND
m,p-Xylene 300.0680 0ND
o-Xylene 300.0340 0ND
Naphthalene 300.0680 0ND
Surr: Dibromofluoromethane 1.701 89.7 56.5 129 01.53
Surr: Toluene-d8 1.701 97.8 64.5 151 01.66
Surr: 1-Bromo-4-fluorobenzene 1.701 98.5 43.2 143 01.67
Original Page 25 of 31
Project: NA Properties Everett
CLIENT: Kane Environmental, Inc.
Work Order: 1711164 QC SUMMARY REPORTVolatile Organic Compounds by EPA Method 8260C
11/17/2017Date:
Sample ID LCS-18840
Batch ID: 18840 Analysis Date: 11/10/2017
Prep Date: 11/9/2017
Analyte Result SPK value SPK Ref Val %REC RPD Ref Val %RPDLowLimit HighLimit RPDLimit Qual
Units: mg/Kg
RL
Client ID: LCSS
RunNo: 39839
SeqNo: 766932
LCSSampType:
Methyl tert-butyl ether (MTBE) 1.000 98.6 66.3 1450.0500 00.986
1,2-Dichloroethane 1.000 103 50.9 1620.0200 01.03
Benzene 1.000 114 64.3 1330.0200 01.14
Toluene 1.000 110 67.3 1380.0200 01.10
1,2-Dibromoethane (EDB) 1.000 112 50.5 1540.00500 01.12
Ethylbenzene 1.000 109 74 1290.0250 01.09
m,p-Xylene 2.000 115 70 1240.0500 02.29
o-Xylene 1.000 107 68.1 1390.0250 01.07
Naphthalene 1.000 101 58.4 1600.0500 01.01
Surr: Dibromofluoromethane 1.250 97.7 56.5 1291.22
Surr: Toluene-d8 1.250 97.5 64.5 1511.22
Surr: 1-Bromo-4-fluorobenzene 1.250 102 43.2 1431.28
Sample ID MB-18840
Batch ID: 18840 Analysis Date: 11/10/2017
Prep Date: 11/9/2017
Analyte Result SPK value SPK Ref Val %REC RPD Ref Val %RPDLowLimit HighLimit RPDLimit Qual
Units: mg/Kg
RL
Client ID: MBLKS
RunNo: 39839
SeqNo: 766933
MBLKSampType:
Methyl tert-butyl ether (MTBE) 0.0500ND
1,2-Dichloroethane 0.0200ND
Benzene 0.0200ND
Toluene 0.0200ND
1,2-Dibromoethane (EDB) 0.00500ND
Ethylbenzene 0.0250ND
m,p-Xylene 0.0500ND
o-Xylene 0.0250ND
Naphthalene Q0.0500ND
Surr: Dibromofluoromethane 1.250 93.2 56.5 1291.17
Surr: Toluene-d8 1.250 93.7 64.5 1511.17
Surr: 1-Bromo-4-fluorobenzene 1.250 89.5 43.2 1431.12
Original Page 26 of 31
Project: NA Properties Everett
CLIENT: Kane Environmental, Inc.
Work Order: 1711164 QC SUMMARY REPORTVolatile Organic Compounds by EPA Method 8260C
11/17/2017Date:
Sample ID MB-18840
Batch ID: 18840 Analysis Date: 11/10/2017
Prep Date: 11/9/2017
Analyte Result SPK value SPK Ref Val %REC RPD Ref Val %RPDLowLimit HighLimit RPDLimit Qual
Units: mg/Kg
RL
Client ID: MBLKS
RunNo: 39839
SeqNo: 766933
MBLKSampType:
NOTES:Q - Indicates an analyte with a continuing calibration that does not meet established acceptance criteria (<20%RSD, <20% Drift or minimum RRF).
Sample ID 1711141-002BDUP
Batch ID: 18840 Analysis Date: 11/10/2017
Prep Date: 11/9/2017
Analyte Result SPK value SPK Ref Val %REC RPD Ref Val %RPDLowLimit HighLimit RPDLimit Qual
Units: mg/Kg-dry
RL
Client ID: BATCH
RunNo: 39839
SeqNo: 767555
DUPSampType:
Methyl tert-butyl ether (MTBE) 300.0788 0ND
1,2-Dichloroethane 300.0315 0ND
Benzene 300.0315 0.1041 1.750.106
Toluene 300.0315 0.1681 3.030.173
1,2-Dibromoethane (EDB) 300.00788 0ND
Ethylbenzene 300.0394 0ND
m,p-Xylene 300.0788 0ND
o-Xylene 300.0394 0ND
Naphthalene 30 Q0.0788 0.1001 7.350.0930
Surr: Dibromofluoromethane 1.971 87.4 56.5 129 01.72
Surr: Toluene-d8 1.971 88.9 64.5 151 01.75
Surr: 1-Bromo-4-fluorobenzene 1.971 91.9 43.2 143 01.81
NOTES:Q - Indicates an analyte with a continuing calibration that does not meet established acceptance criteria (<20%RSD, <20% Drift or minimum RRF).
Sample ID 1711141-004BMS
Batch ID: 18840 Analysis Date: 11/10/2017
Prep Date: 11/9/2017
Analyte Result SPK value SPK Ref Val %REC RPD Ref Val %RPDLowLimit HighLimit RPDLimit Qual
Units: mg/Kg-dry
RL
Client ID: BATCH
RunNo: 39839
SeqNo: 767557
MSSampType:
Methyl tert-butyl ether (MTBE) 0.5621 96.6 58.5 1670.0281 00.543
1,2-Dichloroethane 0.5621 106 51.3 1390.0112 00.596
Benzene 0.5621 117 63.5 1330.0112 0.094290.751
Toluene 0.5621 112 63.4 1320.0112 0.27960.908
1,2-Dibromoethane (EDB) 0.5621 106 50.4 1360.00281 00.593
Ethylbenzene 0.5621 125 54.5 1340.0141 0.060450.763
Original Page 27 of 31
Project: NA Properties Everett
CLIENT: Kane Environmental, Inc.
Work Order: 1711164 QC SUMMARY REPORTVolatile Organic Compounds by EPA Method 8260C
11/17/2017Date:
Sample ID 1711141-004BMS
Batch ID: 18840 Analysis Date: 11/10/2017
Prep Date: 11/9/2017
Analyte Result SPK value SPK Ref Val %REC RPD Ref Val %RPDLowLimit HighLimit RPDLimit Qual
Units: mg/Kg-dry
RL
Client ID: BATCH
RunNo: 39839
SeqNo: 767557
MSSampType:
m,p-Xylene 1.124 124 53.1 1320.0281 0.28341.68
o-Xylene 0.5621 119 53.3 1390.0141 0.10990.778
Naphthalene 0.5621 77.3 52.3 1240.0281 0.042140.477
Surr: Dibromofluoromethane 0.7026 92.6 56.5 1290.651
Surr: Toluene-d8 0.7026 92.0 64.5 1510.646
Surr: 1-Bromo-4-fluorobenzene 0.7026 100 43.2 1430.704
Sample ID 1711141-004BMSD
Batch ID: 18840 Analysis Date: 11/10/2017
Prep Date: 11/9/2017
Analyte Result SPK value SPK Ref Val %REC RPD Ref Val %RPDLowLimit HighLimit RPDLimit Qual
Units: mg/Kg-dry
RL
Client ID: BATCH
RunNo: 39839
SeqNo: 767558
MSDSampType:
Methyl tert-butyl ether (MTBE) 0.5621 98.1 58.5 167 300.0281 0 0.5432 1.500.551
1,2-Dichloroethane 0.5621 109 51.3 139 300.0112 0 0.5964 2.410.611
Benzene 0.5621 122 63.5 133 300.0112 0.09429 0.7513 3.960.782
Toluene 0.5621 113 63.4 132 300.0112 0.2796 0.9075 1.040.917
1,2-Dibromoethane (EDB) 0.5621 106 50.4 136 300.00281 0 0.5933 0.8400.598
Ethylbenzene 0.5621 125 54.5 134 300.0141 0.06045 0.7626 0.1310.764
m,p-Xylene 1.124 124 53.1 132 300.0281 0.2834 1.678 0.2821.68
o-Xylene 0.5621 121 53.3 139 300.0141 0.1099 0.7776 1.470.789
Naphthalene 0.5621 85.5 52.3 124 300.0281 0.04214 0.4768 9.220.523
Surr: Dibromofluoromethane 0.7026 94.7 56.5 129 00.665
Surr: Toluene-d8 0.7026 92.9 64.5 151 00.652
Surr: 1-Bromo-4-fluorobenzene 0.7026 98.7 43.2 143 00.693
Original Page 28 of 31
Date Received: 11/9/2017 4:47:00 PM
Client Name: KANE Work Order Number: 1711164
Sample Log-In Check List
Brianna BarnesLogged by:
Item Information
How was the sample delivered? Client
Is Chain of Custody complete? Yes No Not Present
Was an attempt made to cool the samples? Yes No NA
Are samples properly preserved? Yes No
Was preservative added to bottles? Yes No NA
Did all samples containers arrive in good condition(unbroken)? Yes No
Does paperwork match bottle labels? Yes No
Are matrices correctly identified on Chain of Custody? Yes No
Is it clear what analyses were requested? Yes No
Is there headspace in the VOA vials? Yes No NA
1.
2.
6.
10.
11.
12.
13.
14.
15.
16.
17. Were all holding times able to be met? Yes No
Chain of Custody
Log In
7. Were all items received at a temperature of >0°C to 10.0°C Yes No NA
8. Sample(s) in proper container(s)? Yes No
9. Sufficient sample volume for indicated test(s)? Yes No
Special Handling (if applicable)
18.
19.
Was client notified of all discrepancies with this order? Yes No NA
Person Notified: Date
Regarding:
Via: eMail Phone Fax In Person
Additional remarks:
Client Instructions:
By Whom:
Coolers are present? Yes No NA3.
Shipping container/cooler in good condition? Yes No4.
Custody Seals present on shipping container/cooler? (Refer to comments for Custody Seals not intact)
Yes No Not Required5.
*
Item # Temp ºC
Cooler 1.8
Sample 2.3
Page 1 of 1Note: DoD/ELAP and TNI require items to be received at 4°C +/- 2°C*
Original Page 29 of 31
Page 30 of 31
Page 31 of 31
November 27, 2017
Kane Environmental, Inc.Eric Nassau
Attention Eric Nassau:
RE: NA Properties Everett - 57302Work Order Number: 1711204
3815 Woodland Park Ave N, Ste. 102
Seattle, WA 98103
3600 Fremont Ave. N.
Seattle, WA 98103
T: (206) 352-3790
F: (206) 352-7178
Fremont Analytical, Inc. received 10 sample(s) on 11/13/2017 for the analyses presented in the following report.
Chelsea Ward
This report consists of the following:
- Case Narrative - Analytical Results - Applicable Quality Control Summary Reports - Chain of Custody
All analyses were performed consistent with the Quality Assurance program of Fremont Analytical, Inc. Please contact the laboratory if you should have any questions about the results.
Thank you for using Fremont Analytical.
Sincerely,
Project Manager
Diesel and Heavy Oil by NWTPH-Dx/Dx Ext.
Gasoline by NWTPH-Gx
Sample Moisture (Percent Moisture)
Volatile Organic Compounds by EPA Method 8260C
www.fremontanalytical.com Original
DoD/ELAP Certification #L17-135, ISO/IEC 17025:2005
ORELAP Certification: WA 100009-007 (NELAP Recognized)
Page 1 of 22
11/27/2017Date:
Project: NA Properties Everett - 57302
CLIENT: Kane Environmental, Inc.
Work Order: 1711204
Work Order Sample Summary
Lab Sample ID Client Sample ID Date/Time ReceivedDate/Time Collected1711204-001 N20 E17: 4ft 11/13/2017 10:08 AM 11/13/2017 3:56 PM
1711204-002 N39 E20: 7.5ft 11/13/2017 10:35 AM 11/13/2017 3:56 PM
1711204-003 N30 E22: 5.5ft 11/13/2017 10:55 AM 11/13/2017 3:56 PM
1711204-004 N29 E17:8ft 11/13/2017 11:25 AM 11/13/2017 3:56 PM
1711204-005 N28 E12: 5ft 11/13/2017 11:38 AM 11/13/2017 3:56 PM
1711204-006 N17 E16: 5ft 11/13/2017 11:56 AM 11/13/2017 3:56 PM
1711204-007 N14 E05: 1ft 11/13/2017 12:45 PM 11/13/2017 3:56 PM
1711204-008 N14 E05: 3.5ft 11/13/2017 12:55 PM 11/13/2017 3:56 PM
1711204-009 N04 E21: 5.5ft 11/13/2017 1:15 PM 11/13/2017 3:56 PM
1711204-010 N03 E05: 3.5ft 11/13/2017 1:35 PM 11/13/2017 3:56 PM
Note: If no "Time Collected" is supplied, a default of 12:00AM is assignedOriginal Page 2 of 22
Project: NA Properties Everett - 57302
CLIENT: Kane Environmental, Inc.
11/27/2017
Case Narrative1711204
Date:
WO#:
I. SAMPLE RECEIPT:Samples receipt information is recorded on the attached Sample Receipt Checklist.
II. GENERAL REPORTING COMMENTS:Results are reported on a wet weight basis unless dry-weight correction is denoted in the units field on the analytical report ("mg/kg-dry" or "ug/kg-dry").
Matrix Spike (MS) and MS Duplicate (MSD) samples are tested from an analytical batch of "like" matrix to check for possible matrix effect. The MS and MSD will provide site specific matrix data only for those samples which are spiked by the laboratory. The sample chosen for spike purposes may or may not have been a sample submitted in this sample delivery group. The validity of the analytical procedures for which data is reported in this analytical report is determined by the Laboratory Control Sample (LCS) and the Method Blank (MB). The LCS and the MB are processed with the samples and the MS/MSD to ensure method criteria are achieved throughout the entire analytical process.
III. ANALYSES AND EXCEPTIONS:Exceptions associated with this report will be footnoted in the analytical results page(s) or the quality control summary page(s) and/or noted below.
Original
Page 3 of 22
11/27/2017
Qualifiers & Acronyms1711204
Date Reported:
WO#:
Qualifiers:
* - Flagged value is not within established control limitsB - Analyte detected in the associated Method BlankD - Dilution was requiredE - Value above quantitation rangeH - Holding times for preparation or analysis exceededI - Analyte with an internal standard that does not meet established acceptance criteria J - Analyte detected below Reporting LimitN - Tentatively Identified Compound (TIC)Q - Analyte with an initial or continuing calibration that does not meet established acceptance criteria (<20%RSD, <20% Drift or minimum RRF)S - Spike recovery outside accepted recovery limitsND - Not detected at the Reporting LimitR - High relative percent difference observed
Acronyms:
%Rec - Percent RecoveryCCB - Continued Calibration BlankCCV - Continued Calibration VerificationDF - Dilution FactorHEM - Hexane Extractable MaterialICV - Initial Calibration VerificationLCS/LCSD - Laboratory Control Sample / Laboratory Control Sample DuplicateMB or MBLANK - Method BlankMDL - Method Detection LimitMS/MSD - Matrix Spike / Matrix Spike DuplicatePDS - Post Digestion SpikeRef Val - Reference ValueRL - Reporting Limit RPD - Relative Percent Difference SD - Serial DilutionSGT - Silica Gel TreatmentSPK - SpikeSurr - Surrogate
Original
www.fremontanalytical.comPage 4 of 22
Project: NA Properties Everett - 57302
Client Sample ID: N39 E20: 7.5ft
Collection Date: 11/13/2017 10:35:00 AM
Matrix: Soil
Client: Kane Environmental, Inc.
Lab ID: 1711204-002
Analyses Result Qual Units Date AnalyzedDFRL
Analytical Report
11/27/20171711204
Date Reported:
Work Order:
Gasoline by NWTPH-Gx Analyst: MWBatch ID: 18944
Gasoline 11/20/2017 1:47:53 AM5.41 mg/Kg-dry 1ND
Surr: 4-Bromofluorobenzene 11/20/2017 1:47:53 AM65 - 135 %Rec 1104
Surr: Toluene-d8 11/20/2017 1:47:53 AM65 - 135 %Rec 198.2
Volatile Organic Compounds by EPA Method 8260C Analyst: MWBatch ID: 18944
Benzene 11/20/2017 1:47:53 AM0.0216 mg/Kg-dry 1ND
Toluene 11/20/2017 1:47:53 AM0.0216 mg/Kg-dry 1ND
Ethylbenzene 11/20/2017 1:47:53 AM0.0270 mg/Kg-dry 1ND
m,p-Xylene 11/20/2017 1:47:53 AM0.0541 mg/Kg-dry 10.0661
o-Xylene 11/20/2017 1:47:53 AM0.0270 mg/Kg-dry 1ND
Surr: Dibromofluoromethane 11/20/2017 1:47:53 AM56.5 - 129 %Rec 192.0
Surr: Toluene-d8 11/20/2017 1:47:53 AM64.5 - 151 %Rec 197.4
Surr: 1-Bromo-4-fluorobenzene 11/20/2017 1:47:53 AM43.2 - 143 %Rec 1100
Sample Moisture (Percent Moisture) Analyst: COBatch ID: R39916
Percent Moisture 11/15/2017 10:00:12 AM0.500 wt% 15.91
Original
Page 5 of 22
Project: NA Properties Everett - 57302
Client Sample ID: N30 E22: 5.5ft
Collection Date: 11/13/2017 10:55:00 AM
Matrix: Soil
Client: Kane Environmental, Inc.
Lab ID: 1711204-003
Analyses Result Qual Units Date AnalyzedDFRL
Analytical Report
11/27/20171711204
Date Reported:
Work Order:
Gasoline by NWTPH-Gx Analyst: MWBatch ID: 18944
Gasoline 11/20/2017 2:18:15 AM6.20 mg/Kg-dry 1ND
Surr: 4-Bromofluorobenzene 11/20/2017 2:18:15 AM65 - 135 %Rec 1102
Surr: Toluene-d8 11/20/2017 2:18:15 AM65 - 135 %Rec 197.7
Volatile Organic Compounds by EPA Method 8260C Analyst: MWBatch ID: 18944
Benzene 11/20/2017 2:18:15 AM0.0248 mg/Kg-dry 1ND
Toluene 11/20/2017 2:18:15 AM0.0248 mg/Kg-dry 1ND
Ethylbenzene 11/20/2017 2:18:15 AM0.0310 mg/Kg-dry 1ND
m,p-Xylene 11/20/2017 2:18:15 AM0.0620 mg/Kg-dry 1ND
o-Xylene 11/20/2017 2:18:15 AM0.0310 mg/Kg-dry 1ND
Surr: Dibromofluoromethane 11/20/2017 2:18:15 AM56.5 - 129 %Rec 191.8
Surr: Toluene-d8 11/20/2017 2:18:15 AM64.5 - 151 %Rec 197.2
Surr: 1-Bromo-4-fluorobenzene 11/20/2017 2:18:15 AM43.2 - 143 %Rec 198.3
Sample Moisture (Percent Moisture) Analyst: COBatch ID: R39916
Percent Moisture 11/15/2017 10:00:12 AM0.500 wt% 17.09
Original
Page 6 of 22
Project: NA Properties Everett - 57302
Client Sample ID: N29 E17:8ft
Collection Date: 11/13/2017 11:25:00 AM
Matrix: Soil
Client: Kane Environmental, Inc.
Lab ID: 1711204-004
Analyses Result Qual Units Date AnalyzedDFRL
Analytical Report
11/27/20171711204
Date Reported:
Work Order:
Gasoline by NWTPH-Gx Analyst: MWBatch ID: 18944
Gasoline 11/20/2017 2:48:37 AM5.03 mg/Kg-dry 111.3
Surr: 4-Bromofluorobenzene 11/20/2017 2:48:37 AM65 - 135 %Rec 1102
Surr: Toluene-d8 11/20/2017 2:48:37 AM65 - 135 %Rec 198.8
Volatile Organic Compounds by EPA Method 8260C Analyst: MWBatch ID: 18944
Benzene 11/20/2017 2:48:37 AM0.0201 mg/Kg-dry 11.09
Toluene 11/20/2017 2:48:37 AM0.0201 mg/Kg-dry 12.28
Ethylbenzene 11/20/2017 2:48:37 AM0.0251 mg/Kg-dry 10.263
m,p-Xylene 11/20/2017 2:48:37 AM0.0503 mg/Kg-dry 10.969
o-Xylene 11/20/2017 2:48:37 AM0.0251 mg/Kg-dry 10.238
Surr: Dibromofluoromethane 11/20/2017 2:48:37 AM56.5 - 129 %Rec 191.3
Surr: Toluene-d8 11/20/2017 2:48:37 AM64.5 - 151 %Rec 197.5
Surr: 1-Bromo-4-fluorobenzene 11/20/2017 2:48:37 AM43.2 - 143 %Rec 198.0
Sample Moisture (Percent Moisture) Analyst: COBatch ID: R39916
Percent Moisture 11/15/2017 10:00:12 AM0.500 wt% 16.22
Original
Page 7 of 22
Project: NA Properties Everett - 57302
Client Sample ID: N28 E12: 5ft
Collection Date: 11/13/2017 11:38:00 AM
Matrix: Soil
Client: Kane Environmental, Inc.
Lab ID: 1711204-005
Analyses Result Qual Units Date AnalyzedDFRL
Analytical Report
11/27/20171711204
Date Reported:
Work Order:
Gasoline by NWTPH-Gx Analyst: MWBatch ID: 18944
Gasoline 11/20/2017 3:49:24 AM5.15 mg/Kg-dry 1ND
Surr: 4-Bromofluorobenzene 11/20/2017 3:49:24 AM65 - 135 %Rec 1102
Surr: Toluene-d8 11/20/2017 3:49:24 AM65 - 135 %Rec 197.8
Volatile Organic Compounds by EPA Method 8260C Analyst: MWBatch ID: 18944
Benzene 11/20/2017 3:49:24 AM0.0206 mg/Kg-dry 10.145
Toluene 11/20/2017 3:49:24 AM0.0206 mg/Kg-dry 10.351
Ethylbenzene 11/20/2017 3:49:24 AM0.0257 mg/Kg-dry 10.0591
m,p-Xylene 11/20/2017 3:49:24 AM0.0515 mg/Kg-dry 10.223
o-Xylene 11/20/2017 3:49:24 AM0.0257 mg/Kg-dry 10.0704
Surr: Dibromofluoromethane 11/20/2017 3:49:24 AM56.5 - 129 %Rec 191.6
Surr: Toluene-d8 11/20/2017 3:49:24 AM64.5 - 151 %Rec 198.7
Surr: 1-Bromo-4-fluorobenzene 11/20/2017 3:49:24 AM43.2 - 143 %Rec 198.4
Sample Moisture (Percent Moisture) Analyst: COBatch ID: R39916
Percent Moisture 11/15/2017 10:00:12 AM0.500 wt% 15.68
Original
Page 8 of 22
Project: NA Properties Everett - 57302
Client Sample ID: N17 E16: 5ft
Collection Date: 11/13/2017 11:56:00 AM
Matrix: Soil
Client: Kane Environmental, Inc.
Lab ID: 1711204-006
Analyses Result Qual Units Date AnalyzedDFRL
Analytical Report
11/27/20171711204
Date Reported:
Work Order:
Gasoline by NWTPH-Gx Analyst: MWBatch ID: 18944
Gasoline 11/20/2017 4:19:45 AM5.39 mg/Kg-dry 1ND
Surr: 4-Bromofluorobenzene 11/20/2017 4:19:45 AM65 - 135 %Rec 1100
Surr: Toluene-d8 11/20/2017 4:19:45 AM65 - 135 %Rec 197.9
Volatile Organic Compounds by EPA Method 8260C Analyst: MWBatch ID: 18944
Benzene 11/20/2017 4:19:45 AM0.0215 mg/Kg-dry 1ND
Toluene 11/20/2017 4:19:45 AM0.0215 mg/Kg-dry 10.0524
Ethylbenzene 11/20/2017 4:19:45 AM0.0269 mg/Kg-dry 1ND
m,p-Xylene 11/20/2017 4:19:45 AM0.0539 mg/Kg-dry 1ND
o-Xylene 11/20/2017 4:19:45 AM0.0269 mg/Kg-dry 1ND
Surr: Dibromofluoromethane 11/20/2017 4:19:45 AM56.5 - 129 %Rec 191.2
Surr: Toluene-d8 11/20/2017 4:19:45 AM64.5 - 151 %Rec 199.0
Surr: 1-Bromo-4-fluorobenzene 11/20/2017 4:19:45 AM43.2 - 143 %Rec 196.2
Sample Moisture (Percent Moisture) Analyst: COBatch ID: R39916
Percent Moisture 11/15/2017 10:00:12 AM0.500 wt% 16.10
Original
Page 9 of 22
Project: NA Properties Everett - 57302
Client Sample ID: N14 E05: 3.5ft
Collection Date: 11/13/2017 12:55:00 PM
Matrix: Soil
Client: Kane Environmental, Inc.
Lab ID: 1711204-008
Analyses Result Qual Units Date AnalyzedDFRL
Analytical Report
11/27/20171711204
Date Reported:
Work Order:
Diesel and Heavy Oil by NWTPH-Dx/Dx Ext. Analyst: SBBatch ID: 18880
Diesel (Fuel Oil) 11/14/2017 5:40:12 PM21.8 mg/Kg-dry 1ND
Heavy Oil 11/14/2017 5:40:12 PM54.6 mg/Kg-dry 1ND
Surr: 2-Fluorobiphenyl 11/14/2017 5:40:12 PM50 - 150 %Rec 1103
Surr: o-Terphenyl 11/14/2017 5:40:12 PM50 - 150 %Rec 1113
Gasoline by NWTPH-Gx Analyst: MWBatch ID: 18944
Gasoline 11/20/2017 4:50:11 AM7.95 mg/Kg-dry 1ND
Surr: 4-Bromofluorobenzene 11/20/2017 4:50:11 AM65 - 135 %Rec 198.1
Surr: Toluene-d8 11/20/2017 4:50:11 AM65 - 135 %Rec 1100
Volatile Organic Compounds by EPA Method 8260C Analyst: MWBatch ID: 18944
Benzene 11/20/2017 4:50:11 AM0.0318 mg/Kg-dry 1ND
Toluene 11/20/2017 4:50:11 AM0.0318 mg/Kg-dry 1ND
Ethylbenzene 11/20/2017 4:50:11 AM0.0398 mg/Kg-dry 1ND
m,p-Xylene 11/20/2017 4:50:11 AM0.0795 mg/Kg-dry 10.108
o-Xylene 11/20/2017 4:50:11 AM0.0398 mg/Kg-dry 10.0418
Surr: Dibromofluoromethane 11/20/2017 4:50:11 AM56.5 - 129 %Rec 191.9
Surr: Toluene-d8 11/20/2017 4:50:11 AM64.5 - 151 %Rec 196.9
Surr: 1-Bromo-4-fluorobenzene 11/20/2017 4:50:11 AM43.2 - 143 %Rec 194.4
Sample Moisture (Percent Moisture) Analyst: COBatch ID: R39916
Percent Moisture 11/15/2017 10:00:12 AM0.500 wt% 118.6
Original
Page 10 of 22
Project: NA Properties Everett - 57302
Client Sample ID: N04 E21: 5.5ft
Collection Date: 11/13/2017 1:15:00 PM
Matrix: Soil
Client: Kane Environmental, Inc.
Lab ID: 1711204-009
Analyses Result Qual Units Date AnalyzedDFRL
Analytical Report
11/27/20171711204
Date Reported:
Work Order:
Diesel and Heavy Oil by NWTPH-Dx/Dx Ext. Analyst: SBBatch ID: 18880
Diesel (Fuel Oil) 11/14/2017 7:39:03 PM22.3 mg/Kg-dry 1ND
Heavy Oil 11/14/2017 7:39:03 PM55.7 mg/Kg-dry 1ND
Surr: 2-Fluorobiphenyl 11/14/2017 7:39:03 PM50 - 150 %Rec 198.4
Surr: o-Terphenyl 11/14/2017 7:39:03 PM50 - 150 %Rec 1109
Gasoline by NWTPH-Gx Analyst: MWBatch ID: 18944
Gasoline 11/20/2017 8:23:23 AM9.44 mg/Kg-dry 190.3
Surr: 4-Bromofluorobenzene 11/20/2017 8:23:23 AM65 - 135 %Rec 1107
Surr: Toluene-d8 11/20/2017 8:23:23 AM65 - 135 %Rec 198.2
Volatile Organic Compounds by EPA Method 8260C Analyst: MWBatch ID: 18944
Benzene 11/20/2017 8:23:23 AM0.0378 mg/Kg-dry 10.327
Toluene 11/20/2017 8:23:23 AM0.0378 mg/Kg-dry 10.108
Ethylbenzene 11/20/2017 8:23:23 AM0.0472 mg/Kg-dry 10.872
m,p-Xylene 11/20/2017 8:23:23 AM0.0944 mg/Kg-dry 14.78
o-Xylene 11/20/2017 8:23:23 AM0.0472 mg/Kg-dry 10.651
Surr: Dibromofluoromethane 11/20/2017 8:23:23 AM56.5 - 129 %Rec 194.6
Surr: Toluene-d8 11/20/2017 8:23:23 AM64.5 - 151 %Rec 1100
Surr: 1-Bromo-4-fluorobenzene 11/20/2017 8:23:23 AM43.2 - 143 %Rec 1103
Sample Moisture (Percent Moisture) Analyst: COBatch ID: R39916
Percent Moisture 11/15/2017 10:00:12 AM0.500 wt% 122.8
Original
Page 11 of 22
Project: NA Properties Everett - 57302
Client Sample ID: N03 E05: 3.5ft
Collection Date: 11/13/2017 1:35:00 PM
Matrix: Soil
Client: Kane Environmental, Inc.
Lab ID: 1711204-010
Analyses Result Qual Units Date AnalyzedDFRL
Analytical Report
11/27/20171711204
Date Reported:
Work Order:
Diesel and Heavy Oil by NWTPH-Dx/Dx Ext. Analyst: SBBatch ID: 18880
Diesel (Fuel Oil) 11/14/2017 8:08:42 PM23.2 mg/Kg-dry 1ND
Heavy Oil 11/14/2017 8:08:42 PM58.1 mg/Kg-dry 1ND
Surr: 2-Fluorobiphenyl 11/14/2017 8:08:42 PM50 - 150 %Rec 193.0
Surr: o-Terphenyl 11/14/2017 8:08:42 PM50 - 150 %Rec 1103
Gasoline by NWTPH-Gx Analyst: MWBatch ID: 18944
Gasoline 11/20/2017 8:53:55 AM7.30 mg/Kg-dry 1ND
Surr: 4-Bromofluorobenzene 11/20/2017 8:53:55 AM65 - 135 %Rec 1103
Surr: Toluene-d8 11/20/2017 8:53:55 AM65 - 135 %Rec 198.3
Volatile Organic Compounds by EPA Method 8260C Analyst: MWBatch ID: 18944
Benzene 11/20/2017 8:53:55 AM0.0292 mg/Kg-dry 1ND
Toluene 11/20/2017 8:53:55 AM0.0292 mg/Kg-dry 1ND
Ethylbenzene 11/20/2017 8:53:55 AM0.0365 mg/Kg-dry 10.126
m,p-Xylene 11/20/2017 8:53:55 AM0.0730 mg/Kg-dry 10.502
o-Xylene 11/20/2017 8:53:55 AM0.0365 mg/Kg-dry 10.0517
Surr: Dibromofluoromethane 11/20/2017 8:53:55 AM56.5 - 129 %Rec 193.3
Surr: Toluene-d8 11/20/2017 8:53:55 AM64.5 - 151 %Rec 197.6
Surr: 1-Bromo-4-fluorobenzene 11/20/2017 8:53:55 AM43.2 - 143 %Rec 199.5
Sample Moisture (Percent Moisture) Analyst: COBatch ID: R39916
Percent Moisture 11/15/2017 10:00:12 AM0.500 wt% 121.2
Original
Page 12 of 22
Project: NA Properties Everett - 57302
CLIENT: Kane Environmental, Inc.
Work Order: 1711204 QC SUMMARY REPORTDiesel and Heavy Oil by NWTPH-Dx/Dx Ext.
11/27/2017Date:
Sample ID MB-18880
Batch ID: 18880 Analysis Date: 11/14/2017
Prep Date: 11/14/2017
Analyte Result SPK value SPK Ref Val %REC RPD Ref Val %RPDLowLimit HighLimit RPDLimit Qual
Units: mg/Kg
RL
Client ID: MBLKS
RunNo: 39912
SeqNo: 768447
MBLKSampType:
Diesel (Fuel Oil) 20.0ND
Heavy Oil 50.0ND
Surr: 2-Fluorobiphenyl 20.00 99.8 50 15020.0
Surr: o-Terphenyl 20.00 107 50 15021.4
Sample ID LCS-18880
Batch ID: 18880 Analysis Date: 11/14/2017
Prep Date: 11/14/2017
Analyte Result SPK value SPK Ref Val %REC RPD Ref Val %RPDLowLimit HighLimit RPDLimit Qual
Units: mg/Kg
RL
Client ID: LCSS
RunNo: 39912
SeqNo: 768448
LCSSampType:
Diesel (Fuel Oil) 500.0 100 65 13520.0 0502
Surr: 2-Fluorobiphenyl 20.00 107 50 15021.4
Surr: o-Terphenyl 20.00 119 50 15023.7
Sample ID 1711204-008ADUP
Batch ID: 18880 Analysis Date: 11/14/2017
Prep Date: 11/14/2017
Analyte Result SPK value SPK Ref Val %REC RPD Ref Val %RPDLowLimit HighLimit RPDLimit Qual
Units: mg/Kg-dry
RL
Client ID: N14 E05: 3.5ft
RunNo: 39912
SeqNo: 768450
DUPSampType:
Diesel (Fuel Oil) 3021.9 0ND
Heavy Oil 3054.7 0ND
Surr: 2-Fluorobiphenyl 21.90 107 50 150 023.4
Surr: o-Terphenyl 21.90 118 50 150 025.8
Sample ID 1711204-008AMS
Batch ID: 18880 Analysis Date: 11/14/2017
Prep Date: 11/14/2017
Analyte Result SPK value SPK Ref Val %REC RPD Ref Val %RPDLowLimit HighLimit RPDLimit Qual
Units: mg/Kg-dry
RL
Client ID: N14 E05: 3.5ft
RunNo: 39912
SeqNo: 768451
MSSampType:
Diesel (Fuel Oil) 558.9 116 65 13522.4 0649
Surr: 2-Fluorobiphenyl 22.36 106 50 15023.7
Surr: o-Terphenyl 22.36 119 50 15026.5
Original Page 13 of 22
Project: NA Properties Everett - 57302
CLIENT: Kane Environmental, Inc.
Work Order: 1711204 QC SUMMARY REPORTDiesel and Heavy Oil by NWTPH-Dx/Dx Ext.
11/27/2017Date:
Sample ID 1711204-008AMS
Batch ID: 18880 Analysis Date: 11/14/2017
Prep Date: 11/14/2017
Analyte Result SPK value SPK Ref Val %REC RPD Ref Val %RPDLowLimit HighLimit RPDLimit Qual
Units: mg/Kg-dry
RL
Client ID: N14 E05: 3.5ft
RunNo: 39912
SeqNo: 768451
MSSampType:
Sample ID 1711204-008AMSD
Batch ID: 18880 Analysis Date: 11/14/2017
Prep Date: 11/14/2017
Analyte Result SPK value SPK Ref Val %REC RPD Ref Val %RPDLowLimit HighLimit RPDLimit Qual
Units: mg/Kg-dry
RL
Client ID: N14 E05: 3.5ft
RunNo: 39912
SeqNo: 768452
MSDSampType:
Diesel (Fuel Oil) 591.2 109 65 135 3023.6 0 649.4 0.710645
Surr: 2-Fluorobiphenyl 23.65 114 50 150 027.1
Surr: o-Terphenyl 23.65 126 50 150 029.9
Original Page 14 of 22
Project: NA Properties Everett - 57302
CLIENT: Kane Environmental, Inc.
Work Order: 1711204 QC SUMMARY REPORTGasoline by NWTPH-Gx
11/27/2017Date:
Sample ID LCS-18944
Batch ID: 18944 Analysis Date: 11/19/2017
Prep Date: 11/17/2017
Analyte Result SPK value SPK Ref Val %REC RPD Ref Val %RPDLowLimit HighLimit RPDLimit Qual
Units: mg/Kg
RL
Client ID: LCSS
RunNo: 40027
SeqNo: 770777
LCSSampType:
Gasoline 25.00 81.6 65 1355.00 020.4
Surr: Toluene-d8 1.250 98.4 65 1351.23
Surr: 4-Bromofluorobenzene 1.250 103 65 1351.29
Sample ID MB-18944
Batch ID: 18944 Analysis Date: 11/19/2017
Prep Date: 11/17/2017
Analyte Result SPK value SPK Ref Val %REC RPD Ref Val %RPDLowLimit HighLimit RPDLimit Qual
Units: mg/Kg
RL
Client ID: MBLKS
RunNo: 40027
SeqNo: 770778
MBLKSampType:
Gasoline 5.00ND
Surr: Toluene-d8 1.250 97.7 65 1351.22
Surr: 4-Bromofluorobenzene 1.250 103 65 1351.29
Sample ID 1711252-003BDUP
Batch ID: 18944 Analysis Date: 11/20/2017
Prep Date: 11/17/2017
Analyte Result SPK value SPK Ref Val %REC RPD Ref Val %RPDLowLimit HighLimit RPDLimit Qual
Units: mg/Kg-dry
RL
Client ID: BATCH
RunNo: 40027
SeqNo: 770769
DUPSampType:
Gasoline 304.39 0ND
Surr: Toluene-d8 1.097 99.5 65 135 01.09
Surr: 4-Bromofluorobenzene 1.097 102 65 135 01.12
Sample ID 1711204-004BDUP
Batch ID: 18944 Analysis Date: 11/20/2017
Prep Date: 11/17/2017
Analyte Result SPK value SPK Ref Val %REC RPD Ref Val %RPDLowLimit HighLimit RPDLimit Qual
Units: mg/Kg-dry
RL
Client ID: N29 E17:8ft
RunNo: 40027
SeqNo: 770760
DUPSampType:
Gasoline 305.03 11.35 11.112.7
Surr: Toluene-d8 1.257 97.9 65 135 01.23
Surr: 4-Bromofluorobenzene 1.257 99.2 65 135 01.25
Original Page 15 of 22
Project: NA Properties Everett - 57302
CLIENT: Kane Environmental, Inc.
Work Order: 1711204 QC SUMMARY REPORTGasoline by NWTPH-Gx
11/27/2017Date:
Sample ID 1711204-008BMS
Batch ID: 18944 Analysis Date: 11/20/2017
Prep Date: 11/17/2017
Analyte Result SPK value SPK Ref Val %REC RPD Ref Val %RPDLowLimit HighLimit RPDLimit Qual
Units: mg/Kg-dry
RL
Client ID: N14 E05: 3.5ft
RunNo: 40027
SeqNo: 770764
MSSampType:
Gasoline 39.75 89.3 65 1357.95 035.5
Surr: Toluene-d8 1.988 97.0 65 1351.93
Surr: 4-Bromofluorobenzene 1.988 107 65 1352.13
Sample ID 1711204-008BMSD
Batch ID: 18944 Analysis Date: 11/20/2017
Prep Date: 11/17/2017
Analyte Result SPK value SPK Ref Val %REC RPD Ref Val %RPDLowLimit HighLimit RPDLimit Qual
Units: mg/Kg-dry
RL
Client ID: N14 E05: 3.5ft
RunNo: 40027
SeqNo: 770765
MSDSampType:
Gasoline 39.75 79.1 65 135 307.95 0 35.49 12.131.4
Surr: Toluene-d8 1.988 97.4 65 135 01.94
Surr: 4-Bromofluorobenzene 1.988 106 65 135 02.11
Original Page 16 of 22
Project: NA Properties Everett - 57302
CLIENT: Kane Environmental, Inc.
Work Order: 1711204 QC SUMMARY REPORTSample Moisture (Percent Moisture)
11/27/2017Date:
Sample ID 1711163-002ADUP
Batch ID: R39916 Analysis Date: 11/15/2017
Prep Date: 11/15/2017
Analyte Result SPK value SPK Ref Val %REC RPD Ref Val %RPDLowLimit HighLimit RPDLimit Qual
Units: wt%
RL
Client ID: BATCH
RunNo: 39916
SeqNo: 768484
DUPSampType:
Percent Moisture 200.500 18.98 2.7519.5
Sample ID 1711236-001ADUP
Batch ID: R39916 Analysis Date: 11/15/2017
Prep Date: 11/15/2017
Analyte Result SPK value SPK Ref Val %REC RPD Ref Val %RPDLowLimit HighLimit RPDLimit Qual
Units: wt%
RL
Client ID: BATCH
RunNo: 39916
SeqNo: 768501
DUPSampType:
Percent Moisture 200.500 8.590 2.488.38
Original Page 17 of 22
Project: NA Properties Everett - 57302
CLIENT: Kane Environmental, Inc.
Work Order: 1711204 QC SUMMARY REPORTVolatile Organic Compounds by EPA Method 8260C
11/27/2017Date:
Sample ID LCS-18944
Batch ID: 18944 Analysis Date: 11/19/2017
Prep Date: 11/17/2017
Analyte Result SPK value SPK Ref Val %REC RPD Ref Val %RPDLowLimit HighLimit RPDLimit Qual
Units: mg/Kg
RL
Client ID: LCSS
RunNo: 40026
SeqNo: 770748
LCSSampType:
Benzene 1.000 108 64.3 1330.0200 01.08
Toluene 1.000 107 67.3 1380.0200 01.07
Ethylbenzene 1.000 116 74 1290.0250 01.16
m,p-Xylene 2.000 112 70 1240.0500 02.25
o-Xylene 1.000 107 68.1 1390.0250 01.07
Surr: Dibromofluoromethane 1.250 101 56.5 1291.26
Surr: Toluene-d8 1.250 99.1 64.5 1511.24
Surr: 1-Bromo-4-fluorobenzene 1.250 104 43.2 1431.30
Sample ID MB-18944
Batch ID: 18944 Analysis Date: 11/19/2017
Prep Date: 11/17/2017
Analyte Result SPK value SPK Ref Val %REC RPD Ref Val %RPDLowLimit HighLimit RPDLimit Qual
Units: mg/Kg
RL
Client ID: MBLKS
RunNo: 40026
SeqNo: 770749
MBLKSampType:
Benzene 0.0200ND
Toluene 0.0200ND
Ethylbenzene 0.0250ND
m,p-Xylene 0.0500ND
o-Xylene 0.0250ND
Surr: Dibromofluoromethane 1.250 92.9 56.5 1291.16
Surr: Toluene-d8 1.250 98.0 64.5 1511.22
Surr: 1-Bromo-4-fluorobenzene 1.250 99.3 43.2 1431.24
Sample ID 1711252-003BDUP
Batch ID: 18944 Analysis Date: 11/20/2017
Prep Date: 11/17/2017
Analyte Result SPK value SPK Ref Val %REC RPD Ref Val %RPDLowLimit HighLimit RPDLimit Qual
Units: mg/Kg-dry
RL
Client ID: BATCH
RunNo: 40026
SeqNo: 770742
DUPSampType:
Benzene 300.0175 0ND
Toluene 300.0175 0ND
Ethylbenzene 300.0219 0ND
m,p-Xylene 300.0439 0ND
Original Page 18 of 22
Project: NA Properties Everett - 57302
CLIENT: Kane Environmental, Inc.
Work Order: 1711204 QC SUMMARY REPORTVolatile Organic Compounds by EPA Method 8260C
11/27/2017Date:
Sample ID 1711252-003BDUP
Batch ID: 18944 Analysis Date: 11/20/2017
Prep Date: 11/17/2017
Analyte Result SPK value SPK Ref Val %REC RPD Ref Val %RPDLowLimit HighLimit RPDLimit Qual
Units: mg/Kg-dry
RL
Client ID: BATCH
RunNo: 40026
SeqNo: 770742
DUPSampType:
o-Xylene 300.0219 0ND
Surr: Dibromofluoromethane 1.097 92.7 56.5 129 01.02
Surr: Toluene-d8 1.097 97.1 64.5 151 01.07
Surr: 1-Bromo-4-fluorobenzene 1.097 98.1 43.2 143 01.08
Sample ID 1711204-004BDUP
Batch ID: 18944 Analysis Date: 11/20/2017
Prep Date: 11/17/2017
Analyte Result SPK value SPK Ref Val %REC RPD Ref Val %RPDLowLimit HighLimit RPDLimit Qual
Units: mg/Kg-dry
RL
Client ID: N29 E17:8ft
RunNo: 40026
SeqNo: 770735
DUPSampType:
Benzene 300.0201 1.094 5.341.15
Toluene 300.0201 2.282 5.772.42
Ethylbenzene 300.0251 0.2634 5.820.279
m,p-Xylene 300.0503 0.9686 4.881.02
o-Xylene 300.0251 0.2381 6.950.255
Surr: Dibromofluoromethane 1.257 91.9 56.5 129 01.16
Surr: Toluene-d8 1.257 97.1 64.5 151 01.22
Surr: 1-Bromo-4-fluorobenzene 1.257 95.5 43.2 143 01.20
Sample ID 1711204-002BMS
Batch ID: 18944 Analysis Date: 11/20/2017
Prep Date: 11/17/2017
Analyte Result SPK value SPK Ref Val %REC RPD Ref Val %RPDLowLimit HighLimit RPDLimit Qual
Units: mg/Kg-dry
RL
Client ID: N39 E20: 7.5ft
RunNo: 40026
SeqNo: 770731
MSSampType:
Benzene 1.081 121 63.5 1330.0216 01.31
Toluene 1.081 123 63.4 1320.0216 01.33
Ethylbenzene 1.081 130 54.5 1340.0270 01.40
m,p-Xylene 2.162 123 53.1 1320.0541 0.066082.73
o-Xylene 1.081 120 53.3 1390.0270 01.30
Surr: Dibromofluoromethane 1.351 98.6 56.5 1291.33
Surr: Toluene-d8 1.351 100 64.5 1511.35
Surr: 1-Bromo-4-fluorobenzene 1.351 106 43.2 1431.43
Original Page 19 of 22
Project: NA Properties Everett - 57302
CLIENT: Kane Environmental, Inc.
Work Order: 1711204 QC SUMMARY REPORTVolatile Organic Compounds by EPA Method 8260C
11/27/2017Date:
Sample ID 1711204-002BMS
Batch ID: 18944 Analysis Date: 11/20/2017
Prep Date: 11/17/2017
Analyte Result SPK value SPK Ref Val %REC RPD Ref Val %RPDLowLimit HighLimit RPDLimit Qual
Units: mg/Kg-dry
RL
Client ID: N39 E20: 7.5ft
RunNo: 40026
SeqNo: 770731
MSSampType:
Sample ID 1711204-002BMSD
Batch ID: 18944 Analysis Date: 11/20/2017
Prep Date: 11/17/2017
Analyte Result SPK value SPK Ref Val %REC RPD Ref Val %RPDLowLimit HighLimit RPDLimit Qual
Units: mg/Kg-dry
RL
Client ID: N39 E20: 7.5ft
RunNo: 40026
SeqNo: 770732
MSDSampType:
Benzene 1.081 126 63.5 133 300.0216 0 1.309 3.851.36
Toluene 1.081 126 63.4 132 300.0216 0 1.329 2.171.36
Ethylbenzene 1.081 136 54.5 134 30 S0.0270 0 1.403 4.601.47
m,p-Xylene 2.162 128 53.1 132 300.0541 0.06608 2.730 3.652.83
o-Xylene 1.081 125 53.3 139 300.0270 0 1.295 3.911.35
Surr: Dibromofluoromethane 1.351 99.8 56.5 129 01.35
Surr: Toluene-d8 1.351 98.9 64.5 151 01.34
Surr: 1-Bromo-4-fluorobenzene 1.351 104 43.2 143 01.41
Original Page 20 of 22
Date Received: 11/13/2017 3:56:00 PM
Client Name: KANE Work Order Number: 1711204
Sample Log-In Check List
Clare GriggsLogged by:
Item Information
How was the sample delivered? Client
Is Chain of Custody complete? Yes No Not Present
Was an attempt made to cool the samples? Yes No NA
Are samples properly preserved? Yes No
Was preservative added to bottles? Yes No NA
Did all samples containers arrive in good condition(unbroken)? Yes No
Does paperwork match bottle labels? Yes No
Are matrices correctly identified on Chain of Custody? Yes No
Is it clear what analyses were requested? Yes No
Is there headspace in the VOA vials? Yes No NA
1.
2.
6.
10.
11.
12.
13.
14.
15.
16.
17. Were all holding times able to be met? Yes No
Chain of Custody
Log In
7. Were all items received at a temperature of >0°C to 10.0°C Yes No NA
8. Sample(s) in proper container(s)? Yes No
9. Sufficient sample volume for indicated test(s)? Yes No
Special Handling (if applicable)
18.
19.
Was client notified of all discrepancies with this order? Yes No NA
Person Notified: Date
Regarding:
Via: eMail Phone Fax In Person
Additional remarks:
Client Instructions:
By Whom:
Coolers are present? Yes No NA3.
Shipping container/cooler in good condition? Yes No4.
Custody Seals present on shipping container/cooler? (Refer to comments for Custody Seals not intact)
Yes No Not Required5.
*
Item # Temp ºC
Cooler 7.9
Sample 8.4
Page 1 of 1Note: DoD/ELAP and TNI require items to be received at 4°C +/- 2°C*
Original Page 21 of 22
Page 22 of 22
ATTACHMENT B FIELD PHOTOGRAPHS
UST Removal and Remedial Excavation Report | Field Photographs Project: 57302-2.2 Site Address: 902 North Broadway, Everett, Washington
Photograph 1 – 11/6/2017 – View of southern fuel dispenser and canopy prior to removal
Photograph 2 – 11/6/2017 – View into the base of the fuel dispenser shown in Photograph 1, showing the absence of a secondary containment sump.
UST Removal and Remedial Excavation Report | Field Photographs Project: 57302-2.2 Site Address: 902 North Broadway, Everett, Washington
Photograph 3 – 11/6/2017 – View within turbine vault on the middle UST, showing the plywood walls, dirt bottom, and absence of secondary containment.
Photograph 4 – 11/8/2017 – View of a jointed section of fiberglass product piping, showing a clean pull-apart disassembly at the joint.
UST Removal and Remedial Excavation Report | Field Photographs Project: 57302-2.2 Site Address: 902 North Broadway, Everett, Washington
Photograph 5 – 11/9/2017 – View of the middle UST in the initial stages of removal. The fragment of the west UST left in place is visible to the left, partially obscured by gravel.
Photograph 6 – 11/9/2017 – View of the east UST in the initial stages of removal.
UST Removal and Remedial Excavation Report | Field Photographs Project: 57302-2.2 Site Address: 902 North Broadway, Everett, Washington
Photograph 7 – 11/9/2017 - View of the fragment of the east UST left in-place.
Photograph 8 – 11/9/2017 – View looking south, of product lines entering the southwest corner of the excavation. Note the presence of gray petroleum staining in the soil immediately below the lines.
UST Removal and Remedial Excavation Report | Field Photographs Project: 57302-2.2 Site Address: 902 North Broadway, Everett, Washington
Photograph 9 – 11/13/2017 – View looking southeast, of the extent of the soil hotspot excavation.
ATTACHMENT C ECOLOGY UST SITE ASSESSMENT CHECKLIST
ECY 010-158 (Rev. Jan. 2015)
V. REASON FOR CONDUCTING SITE CHECK/SITE ASSESSMENT (check one)
Release investigation following permanent UST system closure (i.e. tank removal or closure-in-place).
Release investigation following a failed tank and/or line tightness test.
Release investigation following discovery of contaminated soil and/or groundwater.
Release investigation directed by Ecology to determine if the UST system is the source of offsite impacts.
UST system is undergoing a “change-in-service”, which is changing from storing a regulated substance (e.g. gasoline) to storing a non-regulated substance (e.g. water).
Directed by Ecology for UST system permanently closed or abandoned before 12/22/1988.
Other (describe):
I. UST FACILITY II. OWNER/OPERATOR INFORMATION Facility Compliance Tag #: Owner/Operator Name:
UST ID #: Business Name:
Site Name: Address:
Site Address: City: State: Zip:
City: Phone:
Phone: Email:
III. CERTIFIED SITE ASSESSOR Service Provider Name: Company Name:
Cell Phone: Email: Address:
Certification #: Exp. Date: City: State: Zip:
IV. TANK INFORMATION
TANK ID TANK CAPACITY LAST SUBSTANCE STORED DATE SITE CHECK OR ASSESSMENT CONDUCTED
SITE CHECK/SITE ASSESSMENT CHECKLIST FOR UNDERGROUND STORAGE TANKS
This checklist certifies that site check or site assessment activities were performed in accordance with Chapter 173-360 WAC. Instructions are found on the last page.
UST ID #: __________
County: __________
A4760, A8106
97637 N A Properties Inc
Former In & Out Texaco c/o NAP 7 Everett7524 SE 24th St, Ste 315
Mercer Island WA 98040
206-230-4990
902 North Broadway
Everett
Nathan Evenson Kane Environmental, Inc.
[email protected] PO Box 31936
Seattle WA 98103ICC00245994 2/11/2018
1
2
3
12,000 gal
12,000 gal
12,000 gal
Unleaded Gasoline
Unleaded Gasoline
Unleaded Gasoline
11/6/2017-11/9/2017
11/6/2017-11/9/2017
11/6/2017-11/9/2017
X
ATTACHMENT D UST RINSE AND INERTING CERTIFICATIONS
ATTACHMENT E SOIL DISPOSAL DOCUMENTATION