Twenty-first International
Symposium on
Capillary Chromatographyand Electrophoresis
Park City, Utah, USA
June 20-24,1999
UB/TIB Hannover 89
119 995 654
TABLE OF CONTENTS
LECTURES
M.J.E. Golay Award Lecture
M.J.E. Golay Award
Milestones of Progress: Evolution of Modern Liquid Chromatography.Csaba Horvath 1
Plenary Award Lecture
Electromigration Methods: Different Options for Analysis of
Small Organic Molecules.
Milos V. Novotnv 2
Oral Session A
Large Volume Injection: Ready for the Routine?
Nicholas H. Snow 3
Enrichment of Gaseous Samples with Polydimethylsiloxane Equilibrium and
Breakthrough Sampling.Carel A. Cramers. Hans-Gerd Janssen, Pat Sandra and Erik Baltussen 4
Miniaturized Extraction Methods for Capillary Gas Chromatography.
Ren6 J.J. Vreuls and Udo A. Th. Brinkman 5
Application of SPME Devices for Field Monitoring.Jacek Koziel, Laura Muller and Janusz Pawliszyn 6
Investigation of the Microhomogeneity ofSRMs UsingPFE with GC/MS and GC-
ECD Analysis.Michele M. Schantz. MarkVangel and Stephen A. Wise 7
Development and Application ofSPME Procedures for Monitoring of Volatile
Organic Compounds in Wastewater.
M. Abalos and Josep M. Bavona 8
New Strategies in Sample Preparation Based on Polydimethylsiloxane Sorption.
Erik Baltussen. Frank David, Pat Sandra and Carel A. Cramers 9
On-line Coupling of Supercritical Fluid Extraction with Microcolumn Separation
Techniques.Fernando M. Lancas 10
Rapid Sample Preparation for Chromatographic Analyses Using Accelerated Solvent
Extraction (ASE).Eric S. Francis. Richard E. Carlson, Bruce E. Richter and Robert J. Joyce ...
11
Selectivity Enhanced Sample Preparation Strategies for Chromatography.
Joseph M. Lew. Robert Panella, WayneHuhak and Robert Ravey 12
Strategies for Fast GC: Application Directed Selection Rules.
Hans-Gerd Janssen. Marieke van Deursen and Carel A. Cramers 13
Practical Approach to Fast Gas Chromatography Using Today's Analytical Toolbox.
Domenic J. Barsotti 14
Design Considerations and Operational Capabilities of Small, Fast GC Analyzers.Edward B. Overton. K.R. Carney, H.P. Dharmasena and N. Roques 15
LP-GC-MS: Low-Pressure Gas Chromatography Using MS or Ion-trap Detection:
New Exciting Concept in Gas Chromatography.Jaap de Zeeuw. Jan Peene, Hans-Gerd Janssen and Xianwen Lou 16
High-speed GC and GC/MS Using Vacuum-Outlet Operation and
Tunable/Programmable Column Selectivity.Richard Sacks. Andrew Grail and Carrie Leonard 17
Flash Chromatography: Use of Fast Oven Temperature Programming.Harold M. McNair and Gail L. Reed 18
Fast ChromatographyTTime-of-Flight Mass Spectrometry for Assessing Human
Exposure to Endocrine Disrupting Chemicals.
Donald G. Patterson. Jr.. Jean-Marie D. Dimandja and James Grainger 19
Advances in High-speed Multidimensional Gas Chromatography Coupled with
Chemometric Analysis.Robert E. Svnovec. Carlos G. Fraga, Wes W. C. Quigley and
Kevin J. Johnson 20
Comprehensive GC Method for the Screening and Confirmation of Pesticides and
Endocrine Disrupters.Bruce D. Quimbv 21
Tools for Reducing Analysis Time and Removing Unwanted Material from a GC/MS
System.John V. Hinshaw. Andrew Tipler and Adam Patkin 22
Rapid Analytical Separations by High-Resolution Ion Mobility Spectrometry.Herbert H. Hill. Jr. and Reid Asbury 23
Multicapillary GC Columns and Transverse Field Compensation Ion MobilitySpectrometry for the Detection of Explosives, Illicit Drugs and Chemical Warfare
Agents.Stephen Dav 24
Applications of Comprehensive Two-Dimensional Gas Chromatography to the
Identification of Petroleum in the Environment.
Glenn S. Frysinger and Richard B. Gaines 25
Flexible and Functional Delivery of Multidimensional and Comprehensive Gas
Chromatography by Using a Modulated Cryogenic System.
Philip Marriott and Russell Kinghorn 26
Test of Statistical Theory of Overlap for Column-Switching Chromatography.Clint Samuel, Janice Stewart and Joe M. Davis 27
Theory and Practice of Scaling Retention-Time Locked Methods for Speed,Resolution, and/or Capacity.
Matthew S. Klee and Bruce Quimby 28
Sol-gel Approach to Column Technology for High Resolution Gas Chromatography:Current State and Future Prospects.
Dongxin Wang, Wen-Hsin Chang, Anna Deakin, P. Allen Mitchell,James D. Hayes, Yeong D. Hong and Abdul Malik 29
From Xerogels to Aerogels. Sol-gel Derived Monolithic Porous Layers in OpenTubular Capillary Columns for Gas Chromatography.
Rov M.A. Lautamo 30
Analysis of Volatiles Emitted by Living Plants Under Stress Conditions.
Pat Sandra 31
Gas Chromatographic Techniques in the Analysis of Plant Volatiles.
WilfriedA.Konig 32
Gas Chromatographic Residue Analysis of Pesticides Including Endocrine DisruptersUsing ELCD,XSD, NPD, FPD and AED Detectors, Retention Time Locking and a
Pesticide Database.
Joanne M. Cook and Ghislain Gerard 33
Mass Spectrometry with Supersonic Molecular Beams.
Aviv Arnirav 34
Use ofGC-ECD to Identify and Quantify the Chemical Signatures from Buried
Landmines in Overlying Soils and Air.
Thomas F. Jenkins and Marianne E. Walsh 35
Gas Chromatography with Atomic Emission Detection as an Aid in the Identification
ofChemical Warfare Related Material.
John R. Stuff. William R. Creasy, Alex A. Rodriguez and H. Dupont Durst ..36
Applying Adsorption Gas Chromatography to Solve Analytical Challenges in the
Petrochemical Industry.Jim Luong. Terry Dahoy, Rony Van Meulebroeck and Bill Winniford 37
Eliminating Variances in Chromatographic Retention to Improve the Performance of
Detailed Hydrocarbon Analysis (DHA) of Naphthas and Other Petrochemical
Matrices.
Andrew Tipler 38
Gas Chromatography Coupled with Negative Ionization Microplasma Mass
Spectrometry.Cato Brede. Stig Pedersen-Bjergaard, Elsa Lundanes and Tyge Greibrokk
...39
Second Dimension Retention in GCxGC: A Chemical Difference.
John B. Phillips 40
Fast GC for the Analysis of Natural Matrices.
Luiei Mondello. Giovanni Zappia, Giacomo Dugo and Giovanni Dugo 41
V
Use ofFast GC/TOFMS for Rapid Method Development and Peak Deconvolution in
Petrochemical Samples.George A. Reiner. Robert R. Wehman, Jr. and William H. Cullen III 42
ORAL SESSIONS
Recent Developments in Microseparation Mass Spectrometry.
Karin E. Markides 43
Nanoscale Capillary Liquid Chromatography Coupled with a Hybrid Quadrupole
Time-of-FIight Mass Spectrometer for Fully Automated Analysis of ProteolyticDigests for Proteome Studies.
M. Arthur Moseley. Luke Tolley and James W. Jorgenson 44
Applications ofElectrospray Ionization TOFMS for Microcolumn Separations.Alan L. Rockwood, Edgar D. Lee, Mary E. Gimon-Kinsel. Baomin Xin,
Milton L. Lee and Joseph C-H. Sin 45
Electrospray Ionization - High Field Asymmetric Waveform Ion Mobility
Spectrometry - Mass Spectrometry.
Roger Guevremont. Randy W. Purves and David Barnett 46
Microchip Capillary Electrophoresis/Electrospray Ionization Coupled with Time-of-
Flight Mass Spectrometry.Mia M. Lazar. Stephen C. Jacobson, Robert S. Foote, Roswitha S. Ramseyand J. MichaelRamsey 47
Photothermal Reaction Control and Single Molecule Level Determination in the
Integrated Chemistry Lab for Separation and Analysis.Takehiko Kitamori 48
Expanding the Micro-fluidics Toolbox with Multiplexed Affinity Electrophoresis and
Solid-phase Extraction On-Chip.D. Jed Harrison. Cameron Skinner, Siew Bang Cheng, Said Attiya, Loranelle
Shultz-Lockyear, Richard 01esch.uk and Murray Paulson 49
Liquid Handling for Chromatographic Sample Preparation and SeparationTechniques on Microfabricated Analytical Devices.
J6re P. Kutter 50
Polymethylmethacrylate Microfabrication Device Using X-ray Lithography Joint with
Capillaries and Fiber Optics for Micro-electrophoresis.Shize D. Oi, Sean M. Ford, Steven A, Soper and Chantal Khan Malek 51
Liquid Core Waveguides. Exploitation for Use in Capillary Detection Schemes.
Purnendu K. Dasgupta. Brian J. Marquardt and Lloyd W. Burgess 52
Capillary Electrochromatography Using Capillary Arrays.Peon S. Anex. David W. Neyer, Hui Zhao and Richard N. Zare 53
CEC in Capillary Columns Packed with Sub-micron Particles.
Luis A. Colon and Kimberly J. Reynolds 54
Novel Packed Capillary Columns and Their Applications in CapillaryElectrochromatography.
Ziad El Rassi and Minquan Zhang 55
Molded Monolithic Capillary Columns for Electrochromatography.Frantisek Svec 56
Etched, Chemically Modified Fused Silica Capillaries as a Separation Medium in
Electrokinetic Chromatography.Joseph J. Pesek and Maria T. Matyska 57
Capillary Electrochromatography Using Sol-gel Bonded Continuous Bed Columns.
Oinglin Tang and Milton L. Lee 58
Evaluation of Isocratic and Gradient Elution Nano-LC and CEC.
James N. Alexander. IV. Janet B. Poli and Karin E. Markides 59
Gradient Elution Capillary Electrochromatography for the Separation of Carotenoid
Isomers.
Lane C. Sander and Matthias Pursch 60
Toward Practical Gradient Elution Electrochromatography.John G. Dorsev and Catherine A. Rimmer 61
Evaluation of an Integrated Capillary LC-CE System.
Magnus S. Anderson, Lars G. Blomberg. Jack Luo, Keith Hedman
and Frank Yang 62
Capillary Precolumn Microreactors for the On-line Identification and
Characterization ofProteins.
Joseph J. Dalluge. Maura Donohue and Lane C. Sander 63
Electrophoretic Focusing Preconcentration Technique in Continuous Buffer Systems
Employing Capillary Electrophoresis Separation Systems.Nolan A. Poison and Mark A. Hayes 64
High Sample Throughput in Micro-LC Using Selective On-line ImmunoaffinityExtraction.
Eric Schoenzetter, Valerie Pichon, Didier Thiebaut and Marie-Claire Hennion 65
Separation Tools for Purity Assessment of Combinatorial Chemistry Libraries.
NeboisaM. Diordievic. Fabrice Houdiere, Guido Lerch and Fiona Fitzpatrick 66
Development of Microseparations-based Tools for Library Screening.Vincent T. Remcho. Patrick T. Vallano and Gabriela Chirica 67
Raman Spectroscopic Detection for Microcolumn Separations.Andrew Ruddick, David N. Batchelder, Keith D. Bartle. Peter Myers,Suzanne D. Cooper and MarkM. Robson 68
Detection and Diagnosis of Capillary Separations with Microcoil NMR.
Zhixin Jessica Tan. Michael E. Lacey, Wayne P. Kelley, Andrew G. Webb
and Jonathan V. Sweedler 69
VII
Electrochemical Detection in Capillary Electrochromatography.Susanne R. Wallenborg. Ming X. Tan, Christopher G. Bailey and
Craig E. Lunte 70
Multianalyte CEAssays for Screening and Confirmation ofUrinary Drugs ofAbuse.
Wolfgang Thormann. Jitka Caslavska, Andreas Ramseier and
Christoph Siethoff 71
Capillary Electrochromatography for Toxic Drug Analysis.
Kiyokatsu Jinno 72
Potentials of Capillary Electrophoresis in Biotechnology: A Quality Control
Perspective.Wassim Nashabeh. Stacey Ma, Glenn Hunt, Lori Schalk,
Eleanor Canova-Davis and Andy Jones 73
Capillary Electrophoresis at Ultra-High Voltages.Katariina M. Hutterer and James W. Jorgenson 74
Possibilities and Problems of Surface Modification for Electrophoretic and
Chromatographic Microseparations.Gerhard Schomburg 75
Toward a Better Understanding of Sieving Properties of Polymer Solutions in
Capillary Electrophoresis of DNA.
Vladislav Dolnik and William A. Gurske 76
Sweeping of Analyte Zones in Electrokinetic Chromatography.Joselito P. Ouirino and Shigeru Terabe 77
Manipulating and Interpreting Molecular Recognition for Separation of Neutrals by
Cyclodextrin Distribution Capillary Electrochromatography.Michael J. Sepaniak. Shannon B. Fox and Mustafa Culha 78
Performance and Selectivity of Polymeric Pseudo-Stationary Phases in Electrokinetic
Chromatography.
Christopher P. Palmer 79
Electrokinetic Chromatography of Proteins Using Nonporous Reversed Phase
Particles.
Katherine B. Smith. Anup K. Singh, Joseph S. Schoeniger and
David W.Neyer 80
Ligand Exchange-Micellar Electrokinetic Chromatography and Its Applications.Tosbivuki Hobo. Zilin Chen and Jin-Ming Lin 81
Adjustment of Chromatographic Selectivity in Micellar Electrokinetic Capillary
Chromatography Using "Class F Organic Modifiers.
Joel T. Smith. Gerald I. Love and Athena Dawson 82
THEORY
POSTERS
1 Computational Chemical Analysis of the Molecular Recognition of Graphitic Carbon. T. Hanai...
83
2 Temporally Oriented Theory of Chromatographic Behavior. Kevin Lan and James W. Jorgenson ...84
SPME/POLYMER/MEMBRANE EXTRACTION3 Evaluation of Sorptive Enrichment for the Analysis of Phthalates in Air Samples. Bart Tienpont,
Frank David, Erik Baltussen. Freddy Vanwalleghem and Pat Sandra 85
4 Equilibrium Sorptive Enrichment (ESE) with Selective Detection for Trace Analysis of Environmental
Samples. Erik Baltussen. Frank David, Pat Sandra and Carel Cramers 865 Gas Chromatography/Mass Spectrometric Analysis of Abuse Drugs in Saliva Specimens After Solid
Phase Microextraction. Marcello Chiarotti. Nadia Fucci and Nadia De Giovanni .87
6 Sampling Rate Calibration for Non-equilibrium Sampling with SPME Fibers. Thomas F. Jenkins.
Daniel C. Leggett and Thomas A. Ranney 88
7 Analysis of Tricyclic Antidepressant Drugs in Human Urine by SPME/Microcolumn LC.Kivokatsu Jinno and Maki Kawazoe 89
8 Comparative Study of the Extraction Efficiency of Organophosphorus Pesticides in Water UsingSolid-Phase Microextraction (SPME) and Solid-Phase Extraction (SPE). Fernando M. Lancas.
Cristina A. Lacerda and Sueli Guandalini 90
9 Determination ofPhenols in Soils as Acetyl Derivatives by Solid Phase Microextraction/GC-MSD.
Maria Llompart. Belen Blanco and Rafael Cela 91
10 Method for the Determination of Environmental Endocrine Disrupters in Aqueous Samples UsingSPME-HPLC and SPME-GC. Eduardo P. Mateus and Fernando P. Santana 92
11 Characterization ofDifferent Juvenile Eucalyptus Hybrids and Clones by HS-SPME and HRGC.
Eduardo P. Mateus. Laura Carvalho, Helena Farrall and Rosa Paiva 93
12 SPME-GC/MS Analysis ofVolatiles Emitted by Creosote-treated Railway Wood Sleepers.Eduardo Mateus. Alexandra Branco Ribeiro and Dario ReimSo 94
13 Absorption of Explosive Vapors in Air on Polydimethsiloxane Particles - GC/MS. Yuwen Wang and
Harold M.McNair 95
14 Pulse Introduction Membrane Extraction (PIME) Coupled with Nitrogen Purging for Fast On-line
Extraction of Volatile Organics from Aqueous Matrices. Somenath Mitra. X. Guo and A. Sanjuan 96
15 Isolation and Separation of Alkylpyrazines in Roasted Cocoa Using Headspace SPME-GC.Glaucia F. Pini, Fabio Augusto, Antonio L.P. Valente. Edy S. Brito and Nelson H.P. Garcia 97
16 Evaluation of Solid-Phase Microextraction in Combination with Gas Chromatography (SPME-GC) as a
Tool for Quantitative Bioanalysis. Mohamed Abdel-Rehim. Margareta Bielenstein and
Torbjfirn Arvidsson 98
SOLID-PHASE EXTRACTION
17 Performance and Inertness of Different Materials for Enrichment of Sulfur Compounds from Air and
Gaseous Samples. Erik Baltussen. Frank David, Pat Sandra, Hans-Gerd Janssen and Carel Cramers .99
18 Determination and Quantification of Chlorophenolic Compounds in Environmental Samples byGC/ECD Using C18 Solid Phase Extraction (SPE) Preconcentration. Eniz C. Oliveira,Maria do Carmo, R. Peralba, Elina B. Caram2o and Ewelin M.P.N. Canizares 100
19 Determination ofOrganophosphorus Metabolites in Surface Water and Human Urine by Strong Anion
Exchange Disk. Ho-Yuan Chang. Hong-Chi Wu, Chun-Hsiung Kuei and Wei-Chao Lin 101
20 Fully Automated Analysis of Micro Pollutants in Water by On-line SPE-GC-MS. Siaak de Koning.
Ben Apon, Hans-Gerd Janssen and Udo A. Th. Brinkman 102
21 Investigation of Cyanobacterial Toxins Using Solid-phase Extraction and Micro-LC Techniques.Corinne Rivasseau, C6dric Robillot and Marie-Claire Hennion 103
22 Identification ofVolatile Degradation Products of Commercial Plastics by Solid Sorbent Trapping,Thermal Desorption and GC-MS Analysis. Marek E. Krzvmien. David J. Carlsson, Denis J. Worsfold,Mickael Merrier and Michael Day 104
23 Analysis of Wax Esters in Vegetable Oils by SPE-GC. Birgit Reiter,, Marion Lechner,and Eberhard Lorbeer 105
24 Trace-level Determination of Polar Flavor Compounds in Butter by Solid-phase Extraction and
GC-MS. Mohamed Adahchour, Rene" J.J. Vreuls. Arnold van der Heijden and
Udo A.Th. Brinkman 106
25 Use of a Drying Cartridge in On-line Solid-phase Extraction-Gas Chromatography-Mass Spectrometry.Ren6 J.J. Vreuls. Jens Dalluge, Thomas Hankemeier, Arjan J.H. Louter and Udo A.Th. Brinkman
..107
26 Study of the Adsorption Equilibrium of Selected Pesticides in Soils by Simultaneous Filtration and
Liquid Chromatographic Micro-Extraction. Rene" J.J. Vreuls, Lourdes Ramos, Udo A.Th. Brinkman
and Louis E. Sojo 108
ENHANCED LIQUID/SUPERCRITICAL FLUID EXTRACTION
27 New Methodologies of Sample Preparation for Environmental Analysis: ASE and SFE. Lfvia M. Assis.
Jair S. S. Pinto and Fernando M. Lancas 109
28 Accelerated Solvent Extraction (ASE): A New Approach for Environmental Sample Characterization.
Jair S.S. Pinto, Livia M. Assis and Fernando M. Lan9as 110
29 Closed-vessel Microwave-assisted Extraction of Polychlorinated Biphenyls in Biota. Nieves Cairo.
Isabel Garcia and Maria Llompart Ill
30 Pressurized Fluid Extraction of Industrially Relevant Matrices. Lisa J. Fitzpatrick and John R. Dean 112
31 Comparison of Mojonnier and Accelerated Solvent Extraction (ASE) Techniques using FAME Analysis.Eric S. Francis and Robert J. Joyce 113
32 Supercritical Carbon Dioxide Extraction Method for Multiresidue Analysis ofPesticides in Fruits.
Haroldo S. D6rea and Fernando M. Lancas 114
33 Determination of Coffee Oil Contents by Accelerated Solvent Extraction (ASE). Jair S.S. Pinto,Fernando M. Lancas. Suzana L. Nixdorf and Paulo L. Oliveira 115
34 Accelerated Solvent Extraction (ASE) of Herbicides and PAHs in Soil. Jair S.S. Pinto,Erivelton A. Celeghini and Fernando M. Lancas 116
35 On-Line Supercritical Fluid Extraction-Capillary Electrophoresis (SFE-CE) Determination of
Bergapten and Psoralen in Dorstenia brasiliensls Lam. Marcal A. Ruggiero, Janete H.Y. Vilegasand Fernando M. Lancas 117
36 Systematic Approach to Optimizing Sample Extractions and Large Volume GC Injections.Nicholas H, Snow 118
37 Analysis of Chlorophenoxy Acid Herbicides in Water by In-situ Methylation and In-vial Liquid-liquidExtraction Followed by GC-MS. M. Isabel Catalina, Rene" J.J. Vreuls and Udo A.Th. Brinkman
.. 119
COLUMN TECHNOLOGY38 Improve PLOT Column Mechanical Strength by In-Situ Polymerization. M. Mohnke, C. Duvekot,
J. Peene, Jaap de Zeeuw. Jim. Luong, T. Dahoy and L. Sieben 120
39 Reducing the Bleed of Thick-film Nonpolar Polysiloxane Capillary Columns by a Factor of2 to 4.
Jaap de Zeeuw. C. Duvekot and N. Vonk 121
40 Sol-gel Technology for Capillary GC Columns. Dan R. DiFeo, Jr.. Raoul Cervini and Gerard Sharp ..122
41 PEEK Coated Capillary HPLC Columns. Dan R. DiFeo. Jr.. James Mazaraki and Andrew Minett...
123
42 Further Study of the Packing Pressure Influence on the Slurry-Packing of Capillary (LC, CEC
and c-SFC) Columns. Silvia de Sousa Freitas and Fernando M. Lancas 124
43 Streaming Potential Characterization ofSilanols Present in Porous Silica and Organosilica Layersin GCPLOT Columns. Rov M.A. Lautamo and David Mao and Liying Yu 125
44 Direct Gas Chromatographic Separation of Highly Acidic, Basic and Polar Analytes on Open Tubular
Sol-gel Columns. Dongxin Wang, Wen-Hsin Chang and Abdul Malik 126
45 Effect of Chemistry of Monolithic Capillary Columns on Separations in CEC. Frantisek Svec.
Eric C. Peters, David Sykora, Miroslav Petro and Jean M.J. Frechet 127
X
46 Capillary Column Liquid Chromatography Using Sol-gel Bonded Continuous Bed Columns.
Qinglin Tang. Naijun Wu and Milton L. Lee 128
47 Entrapped Columns: Fritless Columns with Conventional HPLC Packing Materials. Gabriela Chirica,Patrick T. Vallano and Vincent T. Remcho 129
CAPILLARY GAS CHROMATOGRAPHYAND RELATED INSTRUMENTATION48 New GC Sampling and Detection Methods and Devices. Aviv Amirav 130
49 Lowering GCMS Detection Limits with the Ion Trap and Large Volume On-Column Injector.Jessie Butler and Rollen Anderson 131
50 Stability of Photoionization Detector Response of Volatile Organic Compounds. Roberto M. Cabrera
and Mehdi Siami 132
51 GC-MS Analysis Using a Mass Spectrometer Dump Valve. Dan R. DiFeo. Jr.. Peter Dawes,
Russell Kinghorn and Gerard Sharp 133
52 Novel GC-MS Column Changeover Device. Dan R. DiFeo. Jr.. Peter Dawes, Russell Kinghom and
Gerard Sharp 134
53 Validation of EPA Method 8270 by Automated Large Volume Injection. Larry Garretson 135
54 New Generation ofGas Filters for Gas Chromatography. H. Heijmans. P. Heijnsdijk, D. de Bruijneand Jaap de Zeeuw
,136
55 Organotin Analysis by GC/PFPD Using 610 nm and 430 nm Filters: Optimization of Some Detector
Parameters. A.F.L. Godoi, R. Favoreto, Maria Santiago-Silva 137
56 Pyrolysis: A Versatile GC Inletting Technique. Scott Adams and Joseph W. Walsh 138
57 Detection, Quantitation and Reproducibility of Pulsed-FIame Photometric Detector for Sulfur-
containing Compounds. William H. Robins. April J. Weekley and Bob W. Wright 139
CAPILLARY GAS CHROMATOGRAPHY APPLICATIONS
58 Determination of 1,3-Butadiene Migration from Chewing Gum to Simulated Saliva. Shirley Abrantes
and Grazieli SimSes 140
59 Extraction and Clean-up Method for the Determination of 20 Organochlorine Pesticide Residues in
Tomatoes by GLC-ECD. Maria Helena W. Morelli-Cardoso and Shirley Abrantes 141
60 Direct Measurement ofAtmospheric Formaldehyde Using Gas Chromatography-PulsedDischargeIonization Detection. Maxwell C. Hunter, Keith D. Bartle. Alastair C. Lewis and Paul W. Seakins 142
61 Odor Analysis in Pulp. Richard A. Borders. Russell F. Ross. Priscilla P. Massev and Tiffany H. Cao .143
62 Preliminary Studies of Brazilian Sweet Marjoram Oil. Maria Regina A. Rodrigues, Elina B. Caramao
and Ewelin M.P.N. Canizares 144
63 Analysis of ll-nor-9-carboxy-A'-Tetrahydrocannabinol in Human Urine by GC-MS/MS.
Marcello Chiarotti. Luisa Costamagna and Federica Umani Ronchi 145
64 Gas Chromatographic Residue Analysis of Pesticides Including Endocrine Disrupters Using ELCD,
XSD, NPD, FPD and AED Detectors, Retention Time Locking and a Pesticide Database.
Joanne M. Cook and Ghislain Gerard 146
65 GC-PFPD-MS, AMDIS and GC-MS-MS as Tools for Trace Level Detection and Confirmation -
A Comparative Study. Shai Pagan 147
66 Theory and Applications of Transverse Field Compensation Ion Mobility Spectrometry.
Stephen Day 148
67 Automatic Preparation and Analysis ofFatty Acid Methyl Esters. Siaak de Koning. Maurice Rijnen,
Geert Alkema and Hans-Gerd Janssen 149
68 Temperature Stable and Inert Non-polar Base-deactivated Capillary for Analyzing Traces ofAmines
and Alkanol Amines by Gas Chromatography. P. Heynsdijk, J. Buyten, N. Vonk and
Jaap de Zeeuw 150
69 B-Farnesene (an Aphid Alarm Pheromone) and Its Impact on Lady Beetle Behavior. E. Barcin Dogan.
Juan Carlos Medina, Milton L. Lee and Gary M. Booth 151
70 Simple GC/MS Technique for Analysis ofVapor-phase Mainstream Cigarette Smoke. J.Z. Done.
J.N. Glass and S.C. Moldoveanu 152
71 Direct Separation of Chiral Secondary Alcohols in Foods and Beverages Using GC with Cyclodextrin
Stationary Phases. Susan E. Ebeler. Gay Sun, Meera Datta and Roy Lautamo 153
72 Capillary GC Column Considerations for Specialty Gas Analysis. Allen K. Vickers, Jason Ellis and
Cameron George154
73 Total Petroleum Hydrocarbon Analysis Using Capillary GC: Affects and Considerations When Using
Small Diameter Columns. Cameron George. Dean Rood and Jason Ellis '. 155
74 Analysis ofOrganic Volatile Impurities Using USP 467 Methodologies. Alan D. Broske, Dennis Gere.
Domenic DiUbaldo and Courtney P. Milner 156
75 Analysis of Free Fatty Acids from c8 to c24. Alan D. Broske, Dennis Gere and Steve Hutt 157
76 Application of Thermal Desorption GC/FHR/MS for the Analysis of High-Temperature Resistant
Sol-gel Coatings. Paul Krusemann 158
77 HT-HRGC and HP-HTHRGC: Comparative Study for the Analysis of a Triterpene Compound.
Fernando M. Lancas and Jane de J.S. Moreira 159
78 Automated Derivatization of Polar Organic Compounds with N20-Bis(trimethylsilyl)-trifluoroacetamid
(BSTFA) in Environmental Analysis. Herbert Lepper 160
79 New Advances in State ofthe Art Capillary Gas Chromatographic Techniques for Polymer
Applications. Joseph M. Lew. Tom Connors, Rob Huff and Joanne Szydlowski 161
80 Analysis of Isomeric Chlorobenzenes at ppb Levels Using a GC/DD/FTIR System. Josefina Carpinteiro,
Pedro Landuy Maria Hermina Bollain. Maria Llompart. Isaac Rodriguez and Rafael Cela 162
81 Application of Capillary GC in the Study of the Reproductive Toxicology of Dibromoacetic Acid, a
Drinking Water Disinfectant Byproduct. M. Leonard Mole. Ashley E. Shearin and
Michael Holmes 163
82 Gas Chromatographic Separation of Enantiomeric Pacifigorgianes and (+/-)Tamariscene. Claudia Paul
and Wilfried A. K6nig 164
83 Investigation ofDiterpenes as Plant Constituents by Enantioselective Capillary Gas Chromatography.
Martin Pietsch and Wilfried A. K5nig 165
84 Optimizing the GC-AED Measurement ofCarbon, Hydrogen, Sulfur and Nitrogen in Petroleum
Liquids. Bruce P. Ouimbv and David A. Grudoski 166
85 Automated System to Monitor Ethylene Released from Plants, Fruits and Vegetables. Pham-Tuan Hai,
Joeri Vercammen, Christophe Devos and Pat Sandra 167
86 CGC-MS for the Determination of the Fatty Acid Position in Triglycerides After Enzymatic Hydrolysis.
Mieke Claeys, An Dermaux, Tom De Smaele, Christophe Devos and Pat Sandra 168
87 Trace Determination of Residual Chemical Warfare Agents in Chemical Neutralization Solutions.
John R. Stuff. Richard L. Cheicante, Kevin M. Morrissey, Jill L. Ruth and H. Dupont Durst 169
88 Method Development for Speciation Analysis ofMercury and Tin Compounds in Standard Reference
Materials Using GC-AED and GC-MS. Silke Tutschku. Michele M. Schantz and
Stephen A. Wise 170
89 Synthesis and Analysis by LC-UV, LC-MS and CGC-MS of Nitro-Polyaromatic Hydrocarbons.Gilbert Desmet, Yinine Zhao. Karel Lazou, Tom De Smaele, Frank David, Denis De Keukeleire and
Pat Sandra 171
HIGH-SPEED GAS CHROMATOGRAPHY
90 Electrospray High Resolution Ion Mobility Spectrometry - A Rapid Separation Technique.G. Reid Asbury. Joerg Klasmeier, Ching Wu and Herbert H. Hill, Jr 172
91 Rapid Separation of Explosives Using Solvating Gas Chromatography. Christopher R. gowerbank.
Philip A. Smith and Milton L. Lee 173
92 Determination of Urinary Polycyclic Aromatic Hydrocarbon Metabolites by Fast Gas Chromatography/
Time-of-Flight Mass Spectrometry and Comprehensive Two-Dimensional Gas Chromatography.
Jean-Marie D. Dimandia. Garrick C. Clouden. James Grainger and Donald G. Patterson. Jr 174
93 Blood Alcohol Analysis by Fast Gas Chromatography. Dennis R. Gere. Alan P. Broske.
Robert D. Trengove and Anthony Gray 175
XII
94 Separation of Leucine and Isoleucine by Electrospray Ionization-High Field Asymmetric WaveformIon Mobility Spectrometry/Mass Spectrometry. Roger Guevremont. David Barnett, Barbara Ellsand Randy W. Purves 176
95 Implementation of Flash Temperature Programming Technology in a Conventional Gas
Chromatograph. Karen E. LeBlanc and Stephen J. MacDonald 177
96 Utilization of an EZ Flash for Environmental Applications. Karen E. LeBlanc and
Stephen J. MacDonald 178
97 High-Speed GC-MS at the Turn of the Century: An Overview. Piet A. Leclercq 179
98 Improving Laboratory Productivity Using High Speed Gas Chromatography Analysis. Charles Lvle.
Michael Marrale and Elizabeth J. Tierney 180
99 Applications of the MicroFAST GC2. Edward B. Overton. K.R. Carney, H.P. Dharmasena andN. Roques 181
100 High-speed GC of Volatile Compounds Using Atmospheric Pressure Air as Carrier Gas. Andrew Grailand Richard P. Sacks 182
101 Temperature Programming for High-speed GC. Andrew Grail, Carrie Leonard, Gail Roberts,Tincuta Veriotti and Richard D. Sacks 183
102 High-speed GC/MS with Time-of-Flight MS and Adjustable GC Column Selectivity. Carrie Leonard,Andrew Grail, Tincuta Veriotti, Gail Roberts and Richard D. Sacks 184
103 High-speed GC Analysis of Complex, Wide-boiling-point Range Mixtures. Carrie Leonard and
Richard P. Sacks 185
104 Recent Developments in Instrumentation for Fast Capillary Gas Chromatography. Marieke van
Deursen. Hans-Gerd Janssen and Carel Cramers 186
105 Fast Gas Chromatogrpahy with Time-of-Flight Mass Spectrometry. Ren6 J.J. Vreuls. Jens Dalltlge andUdo A.Th. Brinkman 187
106 Fast GC Using Resistive Induced Column Heating: The EZ Flash Concept Jens Dalltlge, Rene- J.J.
Vreuls. Rob J.R. Veraart, Rahma Ou-Aissa and Udo A.Th. Brinkman 188
107 High Speed GC Capillary Columns. William Cooke and Joseph W. Walsh 189
108 Headspace Sample Preparation for Fast GC. Robert Westendorf. Glynda Smith and
Jerry Sainsbury 190
SUPERCRITICAL FLUID CHROMATOGRAPHY
109 Modifier Effects on Column Efficiency in Packed Column SFC. Wei Zou and John G. Dorsev 191
110 Analysis ofTocopherols From Olive By-products by Packed Capillary SFC. Elena Ibafiez. J. Palacios,J. Seflorans, G. Santa-Maria, J. Tabera and G. Reglero 192
111 Effect of Pore Size on Fast Chiral Separations Using Packed Capillary Column SFC with Neat CO: as
Mobile Phase. Yi Shen. Naijun Wu, Zhen Chen, Jerald S. Bradshaw and Milton L. Lee 193
112 Open Tubular SFC Determination of Steroid Hormones in Biological Samples. Maria Cecilia H. Tavares.
Sergio D. Garcia and Fernando M. Lancas 194
113 Porous and Nonporous Particles in Packed Capillary Column Solvating Gas Chromatography.Naiiun Wu. Qinglin Tang, Yi Shen and Milton L. Lee 195
CAPILLARY LIQUID CHROMATOGRAPHY AND LC-MS
114 Characterization ofHindered Amine Stabilizers (HAS) with Packed Capillary TemperatureProgrammed Liquid Chromatography. Thomas Andersen. Roger Trones, Tyge Greibrokk and
Dag R. Hegna 196
115 Innovations in the Design of a Gradient Capillary HPLC/MS System Incorporating Photodiode ArrayDetection. Steven A. Cohen. Jeffrey Holyoke, Theodore Dourdeville and Pennis PellaRovere 197
116 Determination ofPhenolic Derivatives of Antipyrine in Plasma Using HPLC-Tandem MS with Several
Types ofInterfaces. Stefan A.J. Coolen. Mark van Lieshout, Fred A. Huf, Jetse C. Reijenga and
Carel A. Cramers 198
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117 Performance of Various Injector Designs and Injection Techniques for HPLC Microcolumns with
Sample Volumes of5 nL to 5 //L. Marc D. Foster. Jon A. Nichols, Megan A. Arnold and
Stephen R. Bakalyar 199
118 Ion-exchange Chromatography ofProteins by Capillary HPLC and Capillary Electrokinetic
Chromatography with pH Gradient Elution. Julia A. Fruetel. Katherine B. Smith and
David W. Neyer 1 200
119 Performance of an Integrated Capillary LC-CE System. Keith Hedman. Frank Yang and
Todd Shirley 201
120 Capillary Liquid Chromatography on a Budget: Hot Liquid Chromatography. T. Scott Kephart and
Purnendu K. Dasgupta 202
121 Liquid Chromatography/EIectrospray Time-of-Flight Mass Spectrometry of Antifolate Polyglutamates.Mary E. Gimon-Kinsel and James C. Griener 203
122 Time-based Injector for HPLC and Micro-LC. Suzana L. Nixdorf, Carlos A.P Camara, Luis H. Mazo,Fernando M. Lancas and Paulo L.C. Oliveira 204
123 Fast Ultrahigh-Pressure Liquid Chromatography/Time-of-FlightMass Spectrometry. J. Andreas
Lippert. Baomin Xin and Milton L. Lee 205
124 Comparison of Nanospray/MS/MS and Nanoscale Capillary LC/MS/MS for Protein Identification
Studies. Jennifer M. Neugebauer and M. Arthur Moselev 206
125 Ultra-high Pressure Liquid Chromatography. Kamlesh D. Patel. Matthew Monroe and
James W. Jorgenson 207
126 Characterization of Recombinant Protein Variants by Peptide Mapping Using a Micro-LC Gradient
at 5 Microliters Per Minute. Jason L. Richardson. Lynn S. Sotos and Janice M. Davis 208
127 Peptide Mapping at Micro-, Capillary- and Nanoscale HPLC Level with a Dedicated Integrated
System. Jean-Pierre Salzmann. Johannes P.C. Vissers, Mario Ursem, Remco E.J. van Soestand
Jean-Pierre Chervet 209
128 TFA Free Nano LC/MS. Jean-Pierre Salzmann. Jean-Pierre Chervet and Johannes P.C. Vissers 210
129 Lasalocid as a Chiral Selector in Capillary LC-MS. Anna Sandberg. Karin E. Markides and
Eva Heldin 211
130 Insight Into the Recognition of an HTV Protease Inhibitor on a Molecular Imprinted Polymer.Nicholas H. Snow. Thomas P. O'Brien andNelu Grinberg 212
131 Synthesis and Characterization ofSuperficially Porous Silica Spheres for Use in UHPLC.
Jason C. Spusa. Kamlesh D. Patel and James W. Jorgenson 213
132 Use of Narrow-bore Column LC-MS* for the Confirmation ofGrowth-promotingAgents in
Biological Matrices. Alida A.M. Stolker. Paulus L.W.J. Schwillens, Marco H. Blokland and
LeendertA. van Ginkel 214
133 The Use of Constant Current Pulsed Discharge Electron Capture Detector in Reversed-Phase Packed
Capillary Liquid Chromatography. Kefa Sun, Steve Erskine, Bill Winniford and
Wayne E. Wentworth 215
134 Capillary-based Hyphenated Chemical Analyzers Using Liquid Chromatography with a Water Mobile
Phase. Robert E. Svnovec. Paul G. Vahey, Wes W.C. Quigley, Carlos G. Fraga, Brian J. Marquardtand Lloyd W. Burgess 216
135 On-line NMR as a Diagnostic Probe for Capillary Separations. Zhixin Jessica Tan- Michael E. Lacey,Wayne P. Kelley, Andrew G. Webb and Jonathan V. Sweedler 217
136 Very High Pressure Liquid Chromatography. Luke T. Tollev. M. Arthur Moseley and
James W. Jorgenson 218
137 Identification and Quantitation of Flavonoids in Plant Extracts Using Atmospheric Pressure Ionization
Mass Spectrometry. Mark van Lieshout and Neil Loftus 219
138 Some Practical Considerations in the Determination of Wheat Pentosans by HPIC Using Pulsed AmperometricDetection. Putt V. Viniamoori and Craig J. Dumstorff 220
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MULTIDIMENSIONAL CHROMATOGRAPHY139 Qualitative Analysis of Essential Oils by Comprehensive Two-Dimensional Gas Chromatography.
Jean-Marie P. Dimandia. Stephen B. Stanfill, Pavid L. Ashley, James Grainger and
Donald G. Patterson, Jr 221
140 Quantitation of Oxygenates, BTEX and Total Aromatics in Gasoline by Comprehensive Two-
Dimensional Gas Chromatography. Glen S. Frvsinger and Richard B. Gaines 222
141 Off-line Multidimensional Chromatography: GC and HPLC for PAH Separation and Detection.
Dennis R. Gere. Alan D. Broske, Robert P. Trengove and Anthony Gray 223
142 Two-dimensional Separation of Explosives and Interferents by Gas Chromatography-Ion Mobility
Spectrometry. Laura Markowski. Joerg Klasmeier, Ching Wu and Herbert H. Hill, Jr 224
143 GCxGC Using a Packed Modulator Tube and a Packed Capillary Column. Yafei Xu and
John B. Phillips 225
144 Headspace - Thermal Modulator Sampling System Coupled to GcxGC. Yafei Xu and
JohnB.Phillips 226
145 Protein/Peptide Analysis Using Automated Two-dimensional Capillary LC. Jean-Pierre Salzmann,
Johannes P.C. Vissers, Mario Ursem, Remco E.J. Van Soest and Jean-Pierre Chervet 227
146 Automated Sample Fractionation and Analysis Using a Modular LC-CapillaryGC System.
Frank David, Andreas Hoffmann and Pat Sandra 228
CAPILLARY ELECTROPHORESIS
147 Characterization ofLidocaine and Its Metabolites in Human Plasma Using Capillary Electrophoresis.Magnus S. Anderson. Hong Wan, Mohamed Abdel-Rehim and Lars G. Blomberg 229
148 Some Factors Affecting Enantiomeric Impurity Determination by Capillary Electrophoresis UsingUltraviolet and Laser Induced Fluorescence Detection. Hong Wan, Staffan Schmidt, Leon Carlsson
and Lars G. Blomberg 230
149 Study ofAllophycocyanin by Capillary Electrophoresis with Diode Laser-Induced Fluorescence
Detection. Pertti J. Viskari, Elizabeth D. Moody and Christa L. Colver 231
150 Dimerization Study of the N-Terminal Domain ofHuman Stat-4. Tad Guszczynski, Holly A. Baden,
David S. Waugh and Terry P. Copeland 232
151 Immobilization of Enzymes on Solid Supports for the Micro-Digestion of RNA with Capillary
Electrophoresis Analysis. Yolanda Y. Pavidson, Steven A. Soper, Lane C. Sander and
Joseph J. Dalluge 233
152 Clinical Serum Protein Capillary Zone Electrophoresis: Evaluation, Reference Value Determination
and Comparison to an Agarose Method. Jean-Pierre Emond 234
153 Determination ofIndividual Glucosinolates in Cabbage and Rapeseed by Capillary Electrophoresis
Via the Enzymatically Released Isothiocyanate Aglycone. Arron Karcher and Ziad El Rassi 235
154 Determination ofStepwise Binding Constants of Cyclodextrin by Capillary Electrophoresis.
Jo-Ying Hu and Chung-Hsiung Kuei 236
155 Capillary Electrophoretic Separation of Thio-containing DNA Fragments. David Mao, Living Yu,
Gay Sun, Rov Lautamo and Allen Vickers 237
156 Recent Progress in Four-Decay Detection for DNA Sequencing. Hui He and Linda B. McGown 238
157 High Performance Capillary Gel Electrophoresis as a Method to Separate Plasmid-DNA Cloning
Vectors with Very High Resolution (below 100 bp) and Its Application in Molecular Biology.
Nicole C. Meisner. Peter Hammerl and Klaus Pittertschatscher 239
158 Analysis ofSDS-Proteins in Biotechnology: GE or Page? Glenn Hunt, Lori Schalk and
WassimNashabeh ;• • •
240
159 Amperometric Detector for Analysis of Chlorophenols by Non-aqueous Capillary Electrophoresis.
An-Lac Nguyen. Abdelkader Hilmi and John H. Luong 241
160 Determination of Dissociation Constants of Labile Drug Compounds by Capillary Electrophoresis.
Eivor Ornskov. Karin E. Markides and Staffan Folestad 242
161 Whole-Column Imaging Detection in Capillary Electrophoresis. Jiaqi Wu, Qinglu Mao and
Janusz Pawliszvn_
243
162 Electrophoretic Focusing Preconcentration Technique in Continuous Buffer System Employing
Capillary Electrophoresis Separation Systems. Nolan A. Poison and Mark A. Hayes 244
163 Stacking Boundary in Capillary Electrophoresis. Joselito P. Ouirino and Shigeru Terabe 245
164 Considerations in the Analysis of Drugs and Peptides by CE-TOFMS. Jenny Samskog.
Magnus Wetterhall, Stefan Nilsson, Sven Jacobsson and Karin E. Markides 246
165 Comparison of Different Chiral Selectors for CE. Katleen Verleysen, Tine Van den Bosch and
Pat Sandra 247
166 Separation of Chlorophenols by Cyclodextrin Supported CZE-Monitoring of the Electrochemical
Dehalogenation of Pentachlorophenol. Klaus Scharwachter. OlafKranz, Jiirgen Voss and
Wilfried A. Konig 248
167 Determination ofReaction Kinetic Parameters by Capillary Electrophoresis. D6ra Viskv.
Marta Kraszni and Bela Noszal 249
168 Novel Fluorescence Detection Scheme for Capillary Electrophoresis of N-Methylcarbamates with
On-column Thermal Decomposition and Derivatization. Yuan Sheng Wu. Hian Kee Lee and
SamF.Y. Li 250
169 Matrix-Assisted Capillary Electrophoresis: Solvent Microextraction Coupled with Capillary
Electrophoresis by Using Ethylacetate as Sample Matrix. Wei Zhan. Tianlin Wang and
SamF.Y. Li 251
170 CE-SDS Non-gel Sieving of rhNGF: Method Optimization for Drug Product Analysis at 0.1 mg/mLConcentration. Michael Zhang. Kathy McCusker and Chulani Karunatilake 252
171 Experiments with Affinity Capillary Electrophoresis. Frederic Lynen, Yining Zhao. Chris Becu,Frans Borremans and Pat Sandra 253
MICELLAR ELECTROKINETIC CHROMATOGRAPHY
172 Stereo-selectivity of Copper(H) Complex as Chiral Selector and Separation Behavior ofAmino Acid
Enantiomers in Ligand Exchange-Micellar Electrokinetic Capillary Chromatography.Zilin Chen. Jin-Ming Lin, Katsumi Uchiyama and Toshiyuki Hobo 254
173 Measurement of Critical Micelle Concentration of Anionic Surfactants by Ligand Exchange-MicellarElectrokinetic Capillary Chromatography Using An Amino Acid Racemate as a Probe Compound.Zilin Chen. Jin-Ming Lin, Katsumi Uchiyama and Toshiyuki Hobo 255
174 Concentration Overload in Micellar Electrokinetic Chromatography: Distortion of Peak Profiles and
Efficiency Losses. Keith W. Smith, Troy H. Seals and Joe M. Davis 256
175 Influence of Organic-Modifier Concentration on Plate Number in Micellar Electrokinetic
Chromatography. 2. Acetonitrile. Troy H. Seals and Joe M. Davis 257
176 Application of Temperature and Applied Voltage Gradients in Micellar Electrokinetic CapillaryChromatography. Neboisa M. Diordievic. Fabrice Houdiere, Guido Lerch and Fiona Fitzpatrick ..
258
177 Novel Sulfonic Acid-Modified Starburst Dendrimer Used as a Pseudostationary Phase in Electrokinetic
Chromatography. Ann L. Gray and James T. Hsu 259
178 Micellar Electrokinetic Chromatography for Studying the Influence of P. aeruginosa Elastase Activityon Those ofHuman Neutrophil Elastase and Cathepsin G. Simona Viglio, Maurizio Luisetti,Anna Lupi, Giuseppe Zanaboni, Giuseppe Cetta and Paolo Iadarola 260
179 Determination of Water Soluble Vitamins by Micellar Electrokinetic Capillary Chromatography.Ana V.C. Simionato and Fernando M. Lancas 261
180 Explorations of Alkyl Polyalcohols as "Class I" Organic Modifiers to Adjust Selectivity in Micellar
Electrokinetic Capillary Chromatography. Gerald I. Love. Athena Dawson and Joel T. Smith...
262
181 Correlation of Drug Absorption with Migration Data from Capillary Electrophoresis Using Micellar
Electrolytes, Eivor Ornskov. Johan Gottfries, Karin E. Markides and Staffan Folestad 263
182 Altering Separation Selectivity in Electrokinetic Chromatography Using Mixtures of PolymericSurfactants. Christopher P. Palmer
,264
183 Ionic Silicone Polymer as a Pseudo-Stationary Phase for Micellar Electrokinetic Chromatography.Ting Chen and Christopher P. Palmer 265
184 Sulfonated Acrylamide Polymers as Pseudo-Stationary Phases in Electrokinetic Chromatography.Christopher J. Watson and Christopher P. Palmer 266
185 Sweeping with an Enhanced Electric Field of Neutral Analyte Zones in Electrokinetic Chromatography.Joselito P. Ouirino and Shigeru Terabe 267
186 Separation of Underivatized Carbohydrates by Micellar Electrokinetic Chromatography with Indirect
UV Detection. Chang Shu and John D. Lamb 268187 Determination of the Ginsenosides from Ginseng Drug Preparations and Ganoderic Acids from
Ganoderma Lucidum by High Performance Liquid Chromatography and Micellar Electrokinetic
Chromatography (MEKC). Wen-Fa Sve and Shu-huiWu 269
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188 Micellar Electrokinetic Capillary Chromatography of Carbamate Insecticides with MEGA-borate andSDS Surfactants. Tony Teeeler and Ziad El Rassi 270
189 Separation and Detection of Explosives on a Microchip, Using Micellar Electrokinetic Chromatographyand NER Indirect Laser Induced Fluorescence Detection. Susanne R. Wallenborg. Don W. Arnold
and Christopher G. Bailey 271
CAPILLARY ELECTROCHROMATOGRAPHY190 Performing CEC, CE and Nano-LC on a Single System. James N. Alexander IV. Janet B. Poli and
Karin E. Markides 272
191 Factors Affecting the Electroosmotic Flow in Capillary Electrochromatography. Keith P. Bartle.
Maria G. Cikalo, Peter Myers and Katherine E. Sealey 273
192 Effects ofDrying Capillary Columns During the Packing Procedure for CEC. Todd D. Maloney and
Luis A. Col6n 274
193 Innovations in Capillary CEC. Gerard P. Rozing, Monika M. Pittmann and Susan PiPrima 275
194 On-line and Off-line Preconcentration ofUrea Herbicides in Capillary Electrochromatography.Changming Yang and Ziad El Rassi 276
195 Preparation, Characterization and Application of Packed and Open Tubular Columns in CEC.
Csaba Horvath. Xian Huang, Emily Wen, Jian Zhang, Shuhong Zhang and Isabelle Gusev 277
196 Capillary Electrochromatography Using Linear Polymer-coated Columns. Hirokazu Sawada andKivokatsu Jinno 278
197 Electrokinetic Flow Through Packed Capillary Columns. Oi-Lie Luo and Joseph P. Andrade 279
198 Liquid Crystal Modified Capillary Columns for OTCEC. Maria T. Matvska. Joseph J. Pesek and
Anjali Katrekar 280
199 Capillary Electrochromatography (CEC) Separations ofCarotenoids. Matthias Pursch, Lane C. Sander
and Stephen A. Wise 281
200 Non-aqueous Packed Capillary Electrochromatography on C„ and CM Columns: Separation of RetinylEsters. Line Roed. Elsa Lundanes and Tyge Greibrokk 282
201 Interfacing Capillary Electrochromatography to Electrospray Ionization/Time-of-Flight Mass
Spectrometry rCEC-ESI/TOFMSt. Ulrike Selditz.Stefan Nilsson and Karin E. Markides 283
202 Molecular Imprinted Stationary Phases for Capillary HPLC and CEC. Patrick T. Vallano and
Vincent T. Remcho 284
203 Fast Capillary Electrochromatography and Capillary Electrochromatography/Time-of-FIight Mass
Spectrometry. Baomin Xin. J. Andreas Lippert, Milton L. Lee and Joseph C-H. Sin 285
204 CEC and CEC-MS for the Analysis of Triglycerides. An Dermaux, Yining Zhao and Pat Sandra 286
MICROCHIP SEPARATIONS
205 Evaluation of Surface Plasmon Resonance Detection of Solutes in a Microchip Channel.
Satoru Waseda, Takuya Shimosaka, Katsumi Uchiyama and Toshivuki Hobo 287
206 Towards Improved Optical Detection for Microchip Separations: Integration ofWaveguides and
MicroChannel Structures. Peter Friis, Karsten Hoppe, Rasmus K. Sandberg, J8rg HUbner,JftreP.Kutterand Otto Leistiko 288
207 Ultrasensitive Determination of Non-fluorescent Species in Micro Separation Media by Photothermal
Spectrometry. Tamao Odake, Jinjian Zheng, Marika Saito, Manabu Tokeshi, Tsuguo Sawada and
Takehiko Kitamori 289
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