EMTL-FINAL REPORT NO. 1491
FMI-EMTL-W/A NO. 3078
FINAL REPORT
HUMIDITY EFFECTS ON SOLUBLE CORE
MECHANICAL AND THERMAL PROPERTIES
(POLYVINYL ALCOHOL/MICROBALLOON COMPOSITE)
BY
THE ENERGY MATERIALS TESTING LABORATORY
A DIVISION OF FIBER MATERIALS INC.
5 MORIN STREET
BIDDEFORD, MAINE 04005
PREPARED FOR:
AEROJET ASRM DIVISION
P.O. BOX 736
IUKA, MS 38852-0736
ATTN: ROD BIZZELL
TEL: (601-423-0934)FAX: (601-423-5416)
PURCHASE ORDER NO. 100364
JANUARY 5, 1993
A _ OF FIllER MATERIALS, INC.BIO4DIEFOIID INDUIITRIAL PA.qK, IIIDDEFOIID, ME. OdllQO6
https://ntrs.nasa.gov/search.jsp?R=19990066705 2018-06-21T07:16:32+00:00Z
-__tzx_ d- TM04533
05 JAN" 1993
ASRM DEVELOPMENT TEST PLAN
HUMIDITY EFFECTS ON SOLUBLE CORE
MECHANICAL AND THERMAL PROPERTIES
VOLUME I
Contract No. NAS8-37800
DR-TM04
WBS 1.3.2.4
TYPE 3 THIS DOCUMENT
AVAILABLE FROM
ASRM DATA MANAGEMENTYELLOW CREEK. M8
_OF: 7-/_'f_
EMTL-FINAL REPORT NO. 1491
FMI-EMTL-W/A NO. 3078
FINAL REPORT
HUMIDITY EFFECTS ON SOI_UBLE CORE
MECHANICAL AND THERMAL PROPERTIES
(POLYVINYL ALCOHOL/MICROBALLOON COMPOSITE)
BY
THE ENERGY MATERIALS TESTING LABORATORY
A DIVISION OF FIBER MATERIALS INC.
5 MORIN STREET
BIDDEFORD, MAINE 04005
PREPARED FOR:
AEROJET ASRM DIVISION
P.O. BOX 736
IUKA, MS 38852-0736
ATTN: ROD BIZZELL
TEL: (601-423-0934)
FAX: (601-423-5416)
PURCHASE ORDER NO. 100364
JANUARY 5, 1993
A I[NVISION OF FLEER MATERIALS. _¢.BiOOIEFORD INOUSTIqlAL PARK, BIDOI[FOflD, ME.
TM04533
05 JAN 1993
THIS DOCUMENT WAS REVIEWED
BY S. SKLADANEK
/
Designee
TM0453305 JAN 1993
REVIEWED BY FLIGHT HARDWARE
SAFETY& RELIABILITY
S.T. PEACE, LMSC S&R
Designee
Section
TABLE OF CONTENTS
1 0
2 0
3 0
4 0
5 0
6 0
7 0
8.0
9.0
i0.0
INTRODUCTION .....................
OBJECTIVE .........................
PURPOSE ........................
PASS/FAIL CRITERIA ..................
SCOPE .........................
SPECIMEN MIXING ....................
SPECIMEN MOLDS ....................
SPECIMEN CURING ....................
SPECIMEN PREPARATION .................
STORAGE AND AGING OF SPECIMENS ............
ii.0 TENSILE AND COMPRESSIVE TEST APPARATUS ........
12.0 TENSILE AND COMPRESSIVE TEST PROCEDURES ........
13.0 TENSILE AND COMPRESSIVE DATA REDUCTION ........
14.0 TENSILE AND COMPRESSIVE TEST RESULTS .........
15.0 THERMAL EXPANSION MEASUREMENTS AND RESULTS ......
16.0 MICROSCOPIC EXAMINATION OF FRACTURE SURFACES .....
17.0 DISCUSSION/OBSERVATIONS ................
Pag_
1
1
1
1
2
4
5
i0
ll
12
13
17
21
22
37
45
48
FIGURE
D_ST OF FIGURES
I0
ll
12
13
14
15
PAGE
Tensile Specimen Mold Drawing ............ 6
Compressive Specimen Mold Drawing ........... 7
CTE Specimen Mold Drawing ............ 8Photograph Tensile and Compression Molds, Mixing of the
Binder solution, and the Curing Oven .......... 9
Photo Tensile and Compressive Test Facility ...... 14
Close Up View of Tensile and Compressive Setups .... 15
Tensile Test Fixture Drawing .............. 16
Graphical Summary of the Effect of Humidity and Loading
Rate on Tensile and Compressive Strength ........ 23
Graphical Summary of the Effect of Humidity and Loading
Rate on Tensile and Compressive Modulus ......... 24
Graphical Summary of the Effect of Humidity and Loading
Rate on Tensile and Compressive Poisson's Ratio .... 25
CTE facility ...................... 38
NIST Standard Reference Test .............. 39
Graphical Summary of Thermal Expansion Measurements . . 40
Microscopic Photographs of Fracture Surfaces ...... 46
Typical Tensile and Compression Specimen Failure Modes 47
LIST OF TABLES
TABLE PAGE
1 Tensile and Compressive Aging Conditions/Test Matrix 3
2 Thermal Expansion Aging Conditions and Test Matrix . . 3
3 Drying Oven Evaporation Rate Determination ...... i0
4 Effect of Humidity and Loading Rate on Tensile
Strength, Modulus and Poisson's Ratio ........ 26
5 Effect of Humidity and Loading Rate on Compressive
Strength, Modulus and Poisson's Ratio ......... 26
6-14 Individual Tensile Properties ........... 27-31
15-23 Individual Compressive Properties ......... 32-36
24 Effect of Humidity on CTE Measurement ......... 41
25-29 Individual CTE Measurements ............ 42-44
Microballon Certificate of Analysis ............. 54
Individual Batch Formulation Data .............. 57
Individual Curing/Aging Date and Time Summaries ....... 59
High Humidity Aging Wet and Dry Bulb Measurements ..... 71
Individual Dimensional Measurements . - - ...... 76
Curing and Drying Temperature vs Time Strip Charts ..... 88
Laboratory Ambient Humidity Strip Charts ......... 107
Tensile and Compression Strain Measurement Qualification . 109
Individual Tensile and Compressive Stress vs Strain Curves
(Raw Data) ........................ 112
Individual CTE curves (Raw Data) ............. 220
ii
1.0 INTRODUCTION
This document constitutes the final report for the study of
humidity effects and loading rate on soluble core (PVA/MB
composite material) mechanical and thermal properties under
Contract No. 100364. This report describes test results,
procedures employed, and any unusual occurrences or specific
observations associated with this test program.
This effort was performed by the Energy Materials Testing
laboratory (EMTL), a division of Fiber Materials, Inc. (FMI), 5
Morin Street, Biddeford Industrial Park, Biddeford, Maine.
Technical questions regarding the report can be directed to the
principle investigator Glenn Vaillancourt. The contract
administrator for this program was David Audie.
2.0 OBJECTIVE
The primary objective of this work was to determine if cured
soluble core filler material regains its tensile and compressive
strength after exposure to high humidity conditions and following
a drying cycle. Secondary objectives include measurements of
tensile and compressive modulus, and Poisson's ratio, and
coefficient of thermal expansion (CTE) for various moisture
exposure states, i
3.0 PURPOSE
The proposed facility for the manufacture of soluble cores at the
Yellow Creek site incorporates no capability for the control of
humidity. Recent physical property tests performed with the
soluble core filler material showed that prolonged exposure to
high humidity significantly degradates in strength. The purpose
of these tests is to determine if the product, process or
facility designs require modification to avoid imparting a highrisk condition to the ASRM. I
4.0 PASS/FAIL CRITERIA
The material tensile and compressive ultimate strength shallreturn to within one standard deviation of the baseline ultimate
strength after exposure to high humidity conditions followed by a
drying cycle at comparable cross-head speeds. CTE measurements
are required to support engineering analyses, i
5.0 SCOPE
In summary, EMTL performed the following tasks:
o Purchased the required materials for specimen fabrication.
o Fabricated molds and test fixturing.
o Mixed, molded, and cured the tensile, compressive and CTE
specimens.
o Aged the test specimens.
o Tested the specimens.
o Submitted final test report.
Tensile and compressive test were conducted to determine the
effects of high humidity (90%) and strain rates (0.05, 0.25, 2.0
in/min) on the tensile and compressive strength, modulus andPoisson's ratio of the material. These test also determined if
cured soluble core filler material regains its tensile and
compressive strength and modulus after exposure to high humidity
conditions and following a drying cycle. The drying cycle of
16±2 hours represents the soluble core barrier cure cycle
presently incorporated into the process.
EMTL conducted 32 tensile and 32 compressive tests at room
temperature after high humidity aging, after high humidity a_ing
then drying, and immediately after cure test conditions. Table 1
specifies the aging temperature, humidity level, drying time,
rate of testing, and number of tests that were conducted at each
condition.
EMTL also conducted 40 CTE tests after high humidity aging, after
high humidity aging then drying, immediately after cure, and
after a week under laboratory ambient conditions. Table 2
specifies the aging temperature, humidity level, drying time,
method of testing, and number of tests that were conducted at
each condition.
Thermal expansion measurements were performed over the range 70°F
to 250°F. Thermal Expansion was measured continuously over this
range.
TABLE 1
TENSILE AND COMPRESSIVE SPECIMEN AGING CONDITIONS AND TEST MATRIX
QTY
CO_4P
4
2
2
8
4
4
4
2
2
I QTYTEN
4
2
2
8
4
4
4
2
2
I AGING AGING AGING DURAT]ON DRYING TIME AT CROSSHEADTENP (OF) _N (_) (hrs) 180°F (HRS) SPEED (in/m_n)
90_5 90_10 120+-12 none O.OS
90_5 90_10 120_12 none 0.25
90_5 90_10 120_12 none 2.0
90_5 90_10 120_12 16_2 0.05
_o:s 9o_1o _2o:_2 _6:z o.zs
9o:s 9o.lo 12o:1z l_z 2.0
0.05
0.25
2.0
TABLE 2
THERMAL EXPANSION SPECIMEN AGING CONDITIONS AND TEST MATRIX
QTY
CTE
8
8
8
8
8
I IAGING I AGING AGING DURATION DRYING TIME AT I SPECIMEN
TENP (OF) I RN (_) (MRS) 1800F (HRS) I SIZE
90+5 90¢10
_.s 9o+-1o
70_5 <50
120+12 NONE P'L X. 75"D
120+_12 16+_2 P'L x. 75'fl)
170+..12 7"L x. 75"D
7"L x. 75"D
2"L x.25"SQ
6.0 SPECIMEN MIXING
The specimen PVA/MB mixture was formulated by weight in the
following percentages from the following materials.
75%
10%
10%
5%
Microballoons - Extendospheres SG - Hollow Microspheres,
from PQ Corp. See appendix for certificate of analysis.
Water
Ethanol - Alcohol, Anhydrous, Reagent. Specially Denatured
Alcohol Formula 3A, from VWR.
Polyvinyl Alcohol - Airvol 205, from Air Products.
Several replicate 5.5 Ib batches of this mixture were made during
the course of the program. The binder solution for the mixture
was made by combining 250±5 grams of tap water with 250±5 grams
of denatured ethanol in a liter beaker. This water ethanol
mixture was heated to 1300 ± 5°F and agitated on a magnetic
stirring hot plate. 125±2 grams of polyvinyl alcohol (PVA)
crystals were slowly added to the heated mixture and agitated
until the PVA crystals were fully dissolved.
1875±25 grams of microballoons were premeasured and placed into
an airtight i0 liter wide mouth container. The microballons were
slowly stirred by hand, with a spatula, while the binder solution
was added. Hand mixing continued for approximately 5 minutes
until a homogeneous PVA/MB consistency was obtained. If the
mixture was not immediately pressed into molds, it was sealed in
the air tight container and used within two weeks after mixing ordiscarded.
Presented in the appendix are the various batch numbers and their
corresponding formulation weights.
4
7 • 0 SPECIMEN MOLDS
All specimens were cast from PVC or aluminum molds dependent on
the specimen type. The internal surfaces of all molds were
sprayed with several coats of FREKOTE NO.I mold release
manufactured by the Dexter Corporation. The top of all molds
were kept open to provide a vapor path for the water/ethanol.
Each mold was firmly packed using a low density tamper (graphite
or glass phenolic rod), and compressing approximately two to
three times the volume of PVA/MB material into the molds.
The tensile mold was made of aluminum as per EMTL's drawing #
EMC-3915. Reference Figure i for the tensile mold drawing.
The compression molds were made of PVC pipe, 3"±0.0625" diameter
by 7" long faced off to length so that the centerline of the pipe
was perpendicular to the bottom edge of the pipe. One end of the
pipe was covered with a solid flat plate and the opposite end of
the pipe was covered with a plate that had a 3" cylindrical hole.
The pipe was held between these plates with 4 bolts. The hole in
the top plate allowed filling and packing of the mold. This
compression mold assembly was easily assembled and disassembled
easing the filling, packing, and specimen removal operation.
Reference Figure 2, EMTL DWG# EMC-3929, for the compressive mold
drawing.
The CTE molds were made of aluminum as per EMTL's drawing # EMC-
3925. Reference Figure 3 for the CTE mold drawing.
Reference Figure 4 for a photograph of the tensile and
compressive molds, mixing of the binder solution, and the curing
oven.
FIGURE [
7ENSELE SPECT.MEN MOLD DRAWING
I l
-I °ci
0
a F o l
O
,,6
J
I7"
./
i
ii iI ]1
ILl
im
'!im
tllt_
,, I|i
IIEli
lII.
FEGL'RE •
COM?RESS_VE SPECIMEN YOLD 3_ING
-I
a
L_ , , , l_
l'v
0
¢y
lt
oo_¢Uq
qP
!1_ L
,ill o L
,_ i, i i..... ! Ii_,
; |e.
.... !$
..... !! n_'1| ,_, II
II_ ,,j_i I III !I_I
i
I
_L_
FI6URE 3
CTE SPEC_HEN HOED DRAYING
i:tI
It:,i
oLt_
o
o
_/_ 1
(U8
I
!
/_Nill
II
I--
i"1I,-
1414.
za.
i-
FIGURE 4
PHOTOGRAPH OF TENSILE AND COMPRESSIVE MOLDS,MIXING OF BINDER SOLUTION AND CURING OVEN
8.0 SPECIMEN CURING
All samples were cured in the same oven at 250°F. The tensile
and CTE samples were cured for a minimum of 6 hours. The
compression samples were cured for a minimum of 9 hours. Strip
chart records of cure temperature vs time relating to specimen
type and number are presented in the appendix. Tabulations of
the date and time the specimens were placed into and removed from
the curing oven are summarized in the appendix.
The specifications for the drying oven were outlined in a sub-
specification of ASTM C495, ASTM C88. The oven was to be capable
of being continually heated at 230±9°F for 4 hours and the rate
of evaporation, at this range of temperature, was to be at least
25g/hr. The rate determined for this oven was 27.6g/hr. Thisrate was determined from the water loss from five 1 liter low-
form beakers, each containing 500g of water at 70±3°F, placed ateach corner and the center of the oven. The results of this
evaporation determination are presented in Table 3.
TABLE 3
DRYING OVEN EVAPORATION RATE DETERMINATION PER ASTM C88
BEAKER
NO.
WEIGHT
EMPTY
(g)
WEIGHT
FULL
(g)
WEIGHT AFTER 4
HRS AT 230°F (g)
EVAPORATION
RATE (g/hr)
1 303.1 803.6 695.3 27.1
2 309.1 809.3 662.9 36.6
3 297.1 797.8 693.7 26.0
4 409.5 909.6 802.6 26.8
908.9408.8 800.25 27.2
Note: Evaporation rate must be >25g/hr. AVE _ 26.7g/hr
Date: 4/20/92, Time in 13:05, Time out 17:05
I0
9.0 SPECIMEN PREPARATION
Each specimen, as it is removed from the molds was assigned a
unique identification. The specimen identification system that
was employed in this program was as follows:
TEN-75°F-9__0_-0.05- iReplicate Number
Crosshead Speed (in/min)
0.05
0.25
2.0
N/A for CTE
Aging Humidity Level (%)
5O
90
Dry
Test TemD {°F)
75
N/A for CTE
TVDe of Evaluation
TEN-Tension
CMP-Compression
CTE-Thermal Expansion
After the compression specimens were removed from the molds, the
end of the samples corresponding to the open end of the mold
required machining to remove the rough surfaces left by the
filling process. All compression samples were ground in the FMI
machine shop to their final dimensional requirements. Finish
machined specimens were weighed, and the post cured gravimetric
density in air calculated per ASTM-C559 to an accuracy of 1% or
better. The tensile and CTE specimens did not require any
machining after removal from the molds. The tensile and CTE
specimens were also dimensioned and weighed.
All of the samples underwent visual inspection for cracks, voids,
discolorations, inclusions, irregularities, and surface porosity.
Flawed specimens were excluded from further processing.
ii
i0.0 STORAGE AND AGING OF SPECIMENS
Baseline (Post Cured, Dry) Samples:
After the cure cycle, the baseline compression samples were
cooled in a desiccated, sealed chamber at ambient temperature for
6 hours minimum prior to final machining. After machining the
ends of the specimens flat and parallel, these samples were
reheated to 250°F for 4 hours to remove any moisture that might
have been absorbed during the time they were out of the
desiccator. After the redrying cycle, the baseline compression
samples were cooled again in a desiccated, sealed chamber at
ambient temperature for 6 hours minimum prior to testing.
Testing was conducted within five minutes after removal of the
specimens from the cool-down chamber.
After the cure cycle, the baseline tensile and CTE samples were
cooled in a desiccated, sealed chamber at ambient temperature for
6 hours minimum prior to testing. Unlike the compression
samples, these tensile and CTE samples required no further
preparation. Testing was conducted within five minutes after
removal of the specimens from the cool-down chamber.
Hiqh Humidity Aqed Samples:
High humidity aging at 90%RH, 90°F was accomplished with a
humidity chamber. The humidity level and temperature inside the
chamber was monitored daily through the use of dry and wet bulb
thermometer measurements to determine the relative humidity and
temperature inside the chamber. Tables of the humidity level,
wet and dry bulb measurements and dates are in the appendix.
These samples were weighed immediately after removal from the
high humidity chamber to determine the wet density of the samples
after high humidity conditioning. Testing was conducted within
five minutes after removal of the specimens from the humidity
chamber.
H_qh Humidity Aaed/Dried Samples:
After high humidity aging, some of the samples were to be dried
at 180°F for 16±2 hours. This was accomplished with the same
oven used for curing the samples.
After the drying cycle, these samples were cooled in a
desiccated, sealed chamber at ambient temperature for 6 hours
minimum prior to test. Testing was conducted within five minutes
after removal of the specimens from the cool-down chamber.
12
ll.0 TENSILE AND COMPRESSIVE TEST APPARATUS
The mechanical test equipment consisted of the following:
o 20,000 lb Electro-Mechanical Test Machine Model 1113.
o i0,000 ib Load Cell.
o 1,000 ib Load Cell.
o Load Cell Conditioner, No. LPM-700-000.
o Compressive Platens.
o Tensile Test Fixtures.
o I0 Channel Strain Gage Conditioner, 2100 System.
o Strain Gages, No. EA-13-10CBE-120, EA-13-250BG-120/LE.
o 12 Inch Vernier, 0.001" Resolution.
o Computerized Data Acquisition 386 System.
o High Humidity Chamber No. C08A-3-I0.
o Type K Thermocouples.
o I0 Channel Thermocouple Meter No. 650-KF-A-DSS
o Strip Chart Recorder No. 141/39/31/50
o Balance 4000 gram range No. GT4000.
Note: Two types of analog to digital (A/D) converters were used
for these tests. The A/D which provides the cleanest signal has
an operational limit of i0 Hz and was used for the tests
conducted at 0.05 and 0.25 in/min. In order to acquire data at
25 Hz an A/D which does not take time to filter the signals
before transmitting was necessary. The jagged stress vs strain
curves, for the 2.0 in/min tests, are due to the use of this
"non-filtering" A/D converter.
Figure 5 is a photographic record of the mechanical test facility
and the high humidity aging chambers. Figure 6 is a close up view
of the tensile and compressive setups. Figure 7 is the tensile
test fixture drawing.
13
FIGURE 5TENSILE AND COMPRESSIVETEST FACILITY AND
THE HIGH HUMIDITY AGING CHAMBERS
!
14
FIGURE 6CLOSE UP VIEW OF TENSILE AND COMPRESSIVE SETUPS
4
15
T-,3VRE
T'_ " r "I" "_NS[LE TEST FEXTURE DR_-_,,,__.X_.,
,,./\
0
k
p-
0
_ .C
.,1.6
12.0 TENSILE AND COMPRESSIVE TEST PROCEDURES
All testing was performed in accordance with the good engineering
practices established by the following accepted ASTM procedures
and the customers statement of work.
ASTM{ Title
C 31
C 39
C 307
C 495
C 469
E 4
E 6
E 29
E iii
Method of Making and Curing Concrete test Specimens in the
Field.
Test Method for Compressive Strength of Cylindrical
Concrete Specimens.
Tensile Strength of Chemical-Resistant Mortar, Grouts, and
Monolithic Surfacing.
Compressive Strength of Lightweight Insulating Concrete.
Static Modulus of Elasticity and Poisson's Ratio of
Concrete in Compression.
Practices for Load Verification of Testing Machines.
Terminology Relating to Methods of Mechanical Testing.
Indicating Which Places of Figures are to be Considered
Significant in Specifying Limiting Values.
Test Method for Young's Modulus.
Following is a brief description of the tensile and compressive
test procedures.
Compression Test Setup and Calibration
A i0,000 ib load cell and compression platens were installed in a
universal test machine. The crosshead displacement rate was set
at 0.05 in/min and verified with a dial indicator and a stop
watch. The load cell, strain gage, extensometer and LVDT signal
conditioners were connected to a data acquisition computer via an
analog to digital converter. These measurements were monitored
and recorded during testing at a sampling rate of 2 Hz for the
tests conducted at a crosshead speed of 0.05in/min, l0 Hz for the
test conducted at 0.25 in/min and 25 Hz for the tests conducted
at 2.0 in/min. Once all data acquisition and test equipment was
setup it was calibrated before any tests were conducted. The
load cell was calibrated initially with a proofing ring traceable
to NIST. During this calibration, a shunt-calibration was also
determined. This shunt calibration was checked before each run
to ensure that the calibration did not change during the course
of the program. Additionally, calibrated dead weights were
placed on the load cell to verify the load cell response. The
strain gages signals were calibrated with a shunt resistor. Theextensometers were calibrated with an extensometer calibrator.
The LVDT was calibrated with a LVDT calibrator.
17
Prior to actual specimen testing, a graphite qualificationspecimen was tested to verify compressive platen alignment. Thisspecimen was instrumented with axial 4 strain gages located at90° to each other around the specimens gage section. Thespecimen was placed between the compression platens and loaded to50% of its yield strength. The four gages were monitored duringtesting. Their output signals were recorded and used to determinethe amount of bending, if any, induced into the specimen. Thiscompressive setup was adjusted until it introduced less than 5%bending into the specimen.
This graphite specimen was also used to qualify the axialextensometers and the transverse LVDT that would be used tomeasure strain on the PVA/MB samples. A transverse strain gage
was added to the graphite qualification sample. The two axial
extensometers were place 180 ° to each other over two of the axial
strain gages. The transverse LVDT was positioned around the
circumference of the sample at mid height, near the transverse
strain gage. The graphite specimen was loaded to 50% of its
yield strength. The axial and transverse strain gage readings
were compared to the axial and transverse extensometer and LVDT
readings. All strain measurements were in agreement and the
results of this test are presented in the appendix.
PVA/MB Compression Specimen Testinq
The PVA/MB compression specimens were tested in accordance withASTM C495-86 and the statement of work. Two axial extensometers
were place on the specimen 180 ° from each other at the samples
mid height. The transverse LVDT was positioned around the
circumference of the sample just above the extensometers.
For the specimens conditioned at high humidity, compression
testing was conducted at room temperature within five minutes
after removal of the specimens from the high humidity chamber.
For the samples conditioned at high humidity, dried at 180°F,
then cooled to RT in a desiccated chamber, compression testing
was conducted at room temperature within five minutes after
removal of the specimens from the cool down chamber. For the
baseline specimens, after the redrying cycle following final
machining, the samples were cooled to RT in a desiccated chamber
for 6 hours minimum prior to testing. Compression testing was
conducted within five minutes after removal of the specimens from
the cool-down chamber.
Plots of stress vs strain were generated for each test and used
to calculate modulus and Poisson's ratio. The maximum load
obtained during testing was determined from the data printout
sheets and used to calculate ultimate compressive strength.
18
Tensile Test Setup and Calibration
A 1,000 ib load cell and tensile test fixtures were installed in
a universal test machine. The crosshead displacement rate was
set at 0.05 in/min and verified with a dial indicator and a stop
watch. The load cell, strain gage, extensometer and LVDT signal
conditioners were connected to a data acquisition computer via an
analog to digital converter. These measurements were monitored
and recorded during testing at a sampling rate of 2Hz for the
tests conducted at a crosshead speed of 0.05in/min, 10Hz for the
test conducted at 0.25 in/min and 30hz for the tests conducted at
2.0 in/min. Once all data acquisition and test equipment was
setup it was calibrated before any tests were conducted. The
load cell was calibrated initially with a proofing ring traceable
to NIST. During this calibration, a shunt-calibration was alsodetermined. This shunt calibration was checked before each run
to ensure that the calibration did not change during the course
of the program. Additionally, calibrated dead weights were hung
from the load cell to verify the load cell response. The strain
gages signals were calibrated with a shunt resistor. Theextensometers were calibrated with an extensometer calibrator.
The LVDT was calibrated with a LVDT calibrator.
Prior to actual specimen testing, a graphite qualification
specimen was tested to verify tensile grip alignment. This
specimen was instrumented with axial 4 strain gages located at
90 ° to each other around the specimens gage section. The
specimen was placed in the fixtures and loaded to 50% of its
yield strength. The four gages were monitored during testing.
Their output signals were recorded and used to determine the
amount of bending, if any, induced into the specimen. This setup
was adjusted until it introduced less than 5% bending into the
specimen.
This graphite specimen was also used to qualify the axialextensometers and the transverse LVDT that would be used to
measure strain on the PVA/MB samples. A transverse strain gage
was added to the graphite qualification sample. The two axial
extensometers were place 180 ° to each other over two of the axial
strain gages. The transverse LVDT was positioned around the
circumference of the sample at mid height, near the transverse
strain gage. The graphite specimen was loaded to 50% of its
yield strength. The axial and transverse strain gage readings
were compared to the axial and transverse extensometer and LVDT
readings. All strain measurements were in agreement and the
results of this test are presented in the appendix.
19
PVA/MB Tensile Specimen Testinq
The PVA/MB Tensile specimens were tested in accordance with the
statement of work. Two axial extensometers were place on the
specimen 180 ° from each other at the samples mid height. The
transverse LVDT was positioned around the circumference of the
sample between the extensometer arms.
For the specimens conditioned at high humidity, tensile testing
was conducted at room temperature within five minutes after
removal of the specimens from the high humidity chamber. For the
samples conditioned at high humidity, dried at 180°F, then cooled
to RT in a desiccated chamber, tensile testing was conducted at
room temperature within five minutes after removal of the
specimens from the cool down chamber. For the baseline specimens,
after the redrying cycle following final machining, the sampleswere cooled to RT in a desiccated chamber for 6 hours minimum
prior to testing. Tensile testing was conducted within five
minutes after removal of the specimens from the cool-down
chamber.
Plots of stress vs strain were generated for each test and used
to calculate modulus and Poisson's ratio. The maximum load
obtained during testing was determined from the data printout
sheets and used to calculate ultimate tensile strength.
20
13.0 TENSILE AND COMPRESSIVE TEST DATA REDUCTION
The results that were calculated for mechanical tests included
Ultimate Tensile and Compressive Strength, Modulus, and Poisson's
Ratio.
o Ultimate Strength of the matdrial was calculated from the
equation: US = P/A, where:
US = Ultimate Strength (psi)
P = Maximum load obtained during testing (ibs)
A = Cross-sectional area (in 2)
o Modulus of Elasticity was determined by drawing a tangent
line on top of the initial linear portion of the axial
stress/strain curve. The slope of this line represents the
modulus of the material and was calculated from the
equation: E =_a/A_, where:
E = Modulus of Elasticity (psi)
_a = Linear Increase in Stress (psi)
_ = Linear Increase in Strain (_)
o Poisson's Ratio is equal to the ratio of transverse strain
to axial strain over the same increment of stress.
Note: Ultimate compressive strength was defined as the first
drop in load, usually coinciding with a loud snap. All of the
compression tests were continued past this first drop in load.
Most of compression samples never loaded above the first load
drop value. However, some of the compression samples reloaded
above the first drop in load value. All of the ultimate
compressive strength data was reported at the first drop in load
value.
The volume of the tensile specimens was calculated as follows:
Density 6061 aluminum = 0.098 Ib/in 3.
Average weight of the 4 tensile molds = 1.737 ibs.
Therefore, volume of alum in the mold = _.7371bs in__/3= 17.724 in 3
0.098 Ibs
Volume of a solid mold based on surface dimensions is = 24.92 in 3
Therefore, the missing volume (volume of tensile specimen)3 3= 24.92 in 3 - 17.724 in = 7.196 in =117.9 cm 3.
21
14.0 TENSILE AND COMPRESSIVE TEST RESULTS
The effect of humidity and loading rate on tensile and
compressive properties is graphically summarized in Figures 8
through I0. The effects of humidity and loading rate are also
presented in tabular form in Tables 4 and 5. Tabulations of the
individual values are presented in Tables 6 through 23.
Tabulations of individual batch formulations, individual
cure/aging dates and times, individual dimensional measurements,
high humidity wet and dry bulb measurements, strip chart records
of cure temperature vs time, plots of the high humidity aging
conditions, drying cycle temperature vs time plots, and the
individual stress vs. strain curves are presented in the
appendix.
22
.--." _77 _.E a
_77._L-MRY OF EFFECT ,OF EL.'YII3_,. A.,D LOAD_._iiJ .:ZATE
0._; TE.NST.LE AND COHPRESS]_VE 5TRENgTE
CROSSHEAD VELocrrY, IN/MIN
1400
1200I,,,11r,/3
.1000
_ 8OO
r,/360O
40OZ
2OO
0
i r'_ Bae._ (=w) Lr'v'_ W,F, m i1.1, 1N_ Ol_
¢3:::3 tO=F, m I_1
0.05 0.25 2.0
Energy Ik=ted=leTeotlng L=bor=tory
CROSSHEAD VELocrrY, IN/MIN
23
.... L%R_ :5_ EFFECT ,."FHL_ID[7't' AND -_'AD[.,<.._.I-
ON TENSILE AND C OMPQ_SS[VE )!ODL'LUS
I.35 ., Qo'r, _
_4
_.25
_.2
_.15
0
0.05 0.25 2.0
CROSSHF_,_ VELOCITY, IN/]KIN
_-, .35 _ so_'. Mac
.3
_.25
.15.1
.05
0
0
0.05
Energy MatedaleTesting L=bor=tory
\\\\\
0.25
CROSSHEAD VELOCITY, IN/MIN
24
2.0
0 .4
.35
_.25
_, .2
.15
.1
.05
0
SL%__ARY OF EFFECT OF Ht_![D[TY A._D LOADING ,<%TE
ON TENSILE AND COMPRESSIVE PO[SSON'S _AT[O
t
.16 .14 "
0.05 0.25 2.0
CeOSSHZ_WLOCr_,_/mN
.4
_.25
.2
_.15
.05
0
0.05
Enemy MaterlaleTeetlng Laboratory
r-_-_ ¢oeF. m NH. 114B _
_'-'_ IIOeF, _ i_1
,, X >'X >,X _
× _
0.25 2.0
CeOSSH]U__crrr, n_/Kn_
25
iIiil_,mMt
TABLE 4
SUMMARY OF EFFECT OF HUMIDITY AND LOADING RATE
ON TENSILE DATA, NEAN VALUES
TEST TYPE AGING TEST TEHP CROSSHEAD STRENGTH NODULUS POISSON'SCONDITION (OF) SPEED (in/min) NEAN (psi) NEAN (n_,i) RATIO
TENSION BASELINE 75 0.05 314.3 .235 .112
BASELINE 75 0.25 323.0 .229 .122
BASELINE 75 2.00 326.2 .228 .0919
90_,,_H(DRIED) 75 0.05 382.2 .228 .118
90_RH(DRIED) 75 0.25 476.2 .282 .120
90_,Rfl(DRIED) 75 2.00 444.8 .270 .112
90°F 90YJ_H 75 0.05 153.7 .0780 .369
90°F 90_RH 75 0.25 175.6 .080_ .271
90°F 90_,RH 75 2.00 181.0 .09S3 .265
CORRELATION 75 0.05 295.5
TABLE 5
SUNNARY OF EFFECT OF NUNIDITY AND LOADIMG RATE
ON COMPRESSIVE DATA a MEAN VALUES
TEST TYPE AGING TEST TEMP CROSSHEAD STRENGTH NODULUS POISSOM'S
CONDITION (OF) SPEED (in/min) MEAN (psl) MEAN (rrli) RATIO
COtPRESSIVE BASELINE 75 0.05 911 .282 .161
BASELINE 75 0.25 951 .294 .140
BASELINE 75 2.00 921 .315 .150
90_J_N(DRIED) 75 0.05 874 .292 .140
90%RH(DRIED) 75 0.25 1021 .294 .133
90_,RN(DRIED) 75 2.00 1066 .287 .137
cK)°F 90_r,RH 75 0.05 526 .0952 .333
90°F 90Y,RN 75 0.25 575 .0956 .301
75 2.00 61990°F 90_¢RH .O988 .3O4
26
?ABLE 6
INDIVIDUAL TENSILE PROPERTY SUMNARY
AGED AT 90%RH, 90°F, THEN DRIED AT 180%
SPECIMEN NO.
TEN-75F-90_(DRIED)'O.OS'70
AGING
CONDITION
90Y,,RH(DRIED)
TEST
TEMP
(OF)
7'5
CROSSHEAD
SPEED
(in/min)
0,05
STRENGTH
(psi)
]79.8
NE_)ULUS
(msi)
.219
.221
POISSON'S
RATIO
.128
TEN-7SF-90_(DR[ED)-O.O5"71 90Y,RH(DRIEO) 7"5 0.05 348.7 .101
TEN-75F-90%(DRIED)-O.05"73 90Y,RH(ORIED) 7"5 0.05 ]70.4 .217 .118
TEN-75F-90_(DRIED)-O.05"74 90Y,RH(DRIED) 7"5 0.05 ]99.7 .242 .111
"_N-75F-90_(DRIED)-O.05-75 90Y,RH(DR[ED) 7"5 0.05 ]10.7 .186 .122
.-75F-90_(DRIED)-O.05-76 907=RH(ORIED 75 0.05 3_.7 .240 .120
TEN-75F-90_(DRIED)-0.05-77 907,,RH(ORiED) 7"5 0.05 403.5 .220 .119
TEN-75F-90_(DRIED)-O.O5-109 90Y,RH(DRiED) 7"5 0.05 407.5 .251 .119
TEN-75F-90_(DRIED)-O.O5-110 90Y=RH(ORIED) 7"5 0.05 42].6 .256 .124
AVE ]82.2 .228 .118
SO 34.8 .0216 .00787
CV (_) 9.10 9.47 6.67
TABLE 7
INDIVIDUAL TENSILE PROPERTY SUMMARY
AGED AT 90Y,,RN, 90°F, THEN DRIED AT 180°F
SPECIMEN NO. AGING TEST CROSSNEAD STRENGTH MODULUS POISSON'S
CONDITION TEMP SPEED (l_i) (mi) RATIO(OF) (in/m(n)
TEN-75F-90Z(DRXED)-0.25-106 90Y,RH(DRIED) 7"5 0.25 471.5 .2T'Z .113
TEN-75F-90Z(DRIED)-O.25-107 90_RH(DRIED) 7"5 0.25 414.2 .282 .120
TEN-75F-90_(DRIED)-0.25-108 90_Q_H(ORIED) 7'5 0.25 470.1 .281 .133
TEN-75F-90"4(ORIED)-0.25-116 90_;RH(DRIED) 75 0.25 549.0 .291 .112
AVE
SO
CV (Z)
476.2
55.4
11.6
.282
. O0 777
2.75
.120
• 0096,8
8.06
27
TABLE 8
INDIVIDUAL TENSILE PROPERTY SUNNARY
AGED AT QO_RH, 9oOF, THEN DRIED AT 1800F
SPECIMEN NO. AGING TEST CROSSHEAD STRENGTH NOOULUS POISSON'S
CONDITION TENP SPEED (PSi) (msi) RATIO(OF) (in/min)
TEN-75F-90%(DRIED)-2.00-111 9OY,RH(DRIED) 75 2.00 521.4 .263 .112
TEN-7SF-90_(DRIED)-2.00-112 9O_RH(DRIED) 75 2.00 454.0 .269 .112
TEN-75F-90_(DRIED)-2.00-113 90%,RH(DRIED) 75 2.00 397.7 .260 .117
TEN-75F-9O_(DRIED)-2.00-114 90Y,RN(DRIED) 75 2.00 503,6 .267 .1DO
TEN-75F-90_(DRIED)-2.00-115 90_RH(DRIED) 75 2.00 310.3 .282 .118
TEN-75F-9OX(DRIED)-2.OO-117 90_,,_H(DRIED) 75 2.00 4.81.8 .279 .112
AVE 4J,_.8 .270 .112
SD 78.8 .00876 .00640
CV (_) 17.7 3.24 5.71
28
TABLE 9
INDIVIDUAL TENB[LE PROPERTY S_RY
BASELINE SAMPLES (DRY), DWG# EMC-3915
SPECIMEN NO. AGING TEST CROSSHEAD STRENGTH MODULUS POISSOfl'S
CONDITION TEMP SPEED (psi) (ms i) RATXO(OF) (in/min)
TEM-75F-DRY-O.O5-48 BASELINE 75 0.05 338.4 .240 .104
TEN-75F-DRY*O.O5-49 BASELINE 75 O.OS 325.1 .245 .106
TEM-75F-DRY'O.05-50 BASELINE 75 0.05 330.0 .240 .100
TEN-75F-DRY-O.O5-51 BASELINE 75 0.05 302.8 .264 .114
TEN-75F-DRY-O.O5-56 BASELINE 75 0.05 296.6 .218 .100
TEN-75F-DRY-O.05-57 BASELINE 75 0.05 280.5 .231 .115
TEN-75F-DRY-O.O5-58 BASELINE 75 0.05 323.6 .223 .123
TEN-75F-DRY-O.05-59 BASELINE 75 0.05 317.7 .222 .137
AVE 314.3 .235 .112
SD 19.4 .0152 .0128
CV (_) 6.17 6.45 11.4
TABLE 10
INDIVIDUAL TENSILE PROPERTY SUMMARY
BASELINE SAMPLES DRY
SPECIMEN NO. AGING TEST CROSBNEAD STRENGTH NOOULUS POISSON'S
CONDiTiON TENP SPEED (ps, i) (msi) RATIO(OF) (in/min)
BASELINE 75 0.25 329.8 .250 .108TEN-75F-DRY-O.25-52
TEN-75F-DRY-0.25-53 BASELINE 75 0.25 283.4 .238 .129
TEN-75F-DRY-0.25-60 BASELINE 75 0.25 322.2 .188 .113
TEM-75F-DRY-0.25-61 BASELINE 75 0.25 365.9 .211 .150
TEM-75F-DRY-0.25-62 BASELINE 75 0.25 319.0 .255 .128
TEN-75F-DRY-O.25-63 BASELINE 75 0.25 252.0 .234
TEN-75F-ORY-0.25-64 BASELINE 75 0.25 403.4 .233 .101
TEN-75F-DRY-0.25-65 BASELINE 75 0.25 314.2 .222
AVE 323.0 .229 .122
SO 66.4 .0217 .0178
CV (_) 14.3 9.47 14.6
29
TABLE 11
INDIVIDUAL TENSILE PROPERTY SUMMARY
BASELINE SAMPLES DRY
SPECIMEN HO. AGING TEST CROSSNEAD STRENGTH MODULUS POISSON'S
CONDITION TEMP SPEED (psi) (ms i) RATIO(OF) (in/min)
TEN-73F-DRY-2.00-54 BASELINE 73 2.0 216.9 .256 .0855
TEN-73F-ORY-2.O0-55 BASELINE 75 2.0 349.2 .240 .0900
TEN-73F-DRY-2.00-_ BASELINE 73 2.0 400.2 .214 .107
TEN-75F-DRY-2.00-67 BASELINE 75 2.0 314.5 .207 .103
TEN-73F-DRY-2.00-68 BASELINE 73 2.0 350.0 .222 .0741
AVE
SO
CV (_)
326.2
_.320.9
• 228
• 02008.77
.0919
.0133
14.5
SPECIMEN NO.
TEN- 75 F-DRY-O. 05-1-OLD
TEN- 73F-DRY-O. 05-2-OLD
TABLE 9A - COMPARE TO TABLE 9
INDIVIDUAL TENSILE PROPERTY SUMMARY.
CORRELATION SAMPLES (DRY) TESTED USING OLD GEOMETRYTO COMPARE THIS PROGRAM WITH PREVIOUS PROGRAM DWG# ENg-3684.
AGING
CONDITION
CORRELATION
CORRELATION
CROSSNEADSPEED
(in/min)
0.05
TESTTEMP
(°F}
73
73
73
75
75
75
0.05
STRENGTH
(l_i)
264.8
288.5
TEN-75F-DRY-O.OS-3-OLD CORRELATION 0.05 326.4
TEN-75F-DRY-O.OS-4-OLD CORRELATION 0.05 311.4
CORRELATION 0.05 285.8
0.05 296.1
TEN-75F-ORY-O.OS-S-OLD
TEN-75F-DRY-O.OS-6-OLD CORRELATION
AVE 29S .S
SO 21.4
CV (X) 7.25
NODULUS
(mi)
POISSON'S
RATIO
Previous data obtained on May 1992, P.O# 100206, using specimen geometry of D_.dll ENB-3684 atso achieved an
average tensile strength of 295 pet. Therefore, tensile str_'41th data is reproducible using sam geometries
at different dates.
3O
TABLE 12INDIVIDUAL TENSILE PROPERTYSUMMARY
AGED AT 90Y.RH, 900F
SPECIMEN NO. AGINGCONDITION
TEST CROSSHEADTEMP SPEED(OF) (in/min)
STRENGTH(psi)
MOOULUS(mi)
POISSON'SRATIO
TEN-75F-90%-O.05-88 90_N, 90°F 75 0.05 165.8 .0840 .290
TEN-75F-90%-O.05"89 75 0.05 124.1 ,07_) .383
TEN-75F-90%-O.05"94 75 0.05 162.8 .0651 .409
TEN-75F-90%-O.05-96 90_RH, 900F 75 0.05 163.8 .0907 .390
TEN-75F-90%-O.05"98 90_RH, 900F 75 0.05 151.8 .0718 .373
AVE 153.7 .0780 .]69.SO 17.4 .0100 .0461CV (X) 11.3 12.8 12.5
TABLE 13INDIVIDUAL TENSILE PROPERTYSUMMARY
AGED AT 90_[,RH, 90°F
SPECIMEN NO. AGING TEST CROSSHEAD STRENGTH W3DULUS IM3ISSON'SCONDITION TEMP SPEED (psi) (nmi) RATIO
(OF) (in/min)
TEN-75F-90%-0.25-90 90_,.RH, 9O°F 75 0.25 158.0 .0678 .2_
TEN-75F-90¢-O. 25-_ 90_WHr 90°F
9O_RH, 90°F
75 0.25 201.6 .09O5 .249
TEN-75F-90%-0.25-101 75 0.25 201.2 .09_ .266
TEN-75F-90'4-0.25-102 9O_RH, 90% 75 0.25 161.7 .0_7 .306"
AVE 175.6 .0809 .271SO 30.5 .01/.8 .O2_,J,CV (Z) 17.4 18.3 8.99
SPECIMEN NO.
TEN- 75F-QO_-2.00-92
TEN- 75F-90_-2.00-93
TEN-75F-OOX-2.00-100
TEN-75F-90_- 2.00-103
TEN-75F-OOX-2.00-104
TABLE 16INDIVIDUAL TENSILE PROPERTY SUMMARY
AGEDAT 90"/,,RHf 90°F
AGINGCOMOITIOM
STRENGTH(l:_i)
TEST CROSSNE/_TENP SPEED(OF) (in/min)
75 2.00
75 2.00
75 2.00
75 2.00
75 2.00
AVESOCV (X)
POISSON'SRAT10
90e4RNf O0°F 188.6 .114
90¢RN, 90°F 196.9 .0778 .305
160.4 .110
203.6
155.7
qO3itNI 90°F
90"4RHf 90°F
90Y,RNf 90°F
.O842
.O9O3
.O953
.016016.8
181.021.712.0
.243
.263
.248
.265
.028110.6
31
TABLE 15
INDIVIDUAL COMPRESSIVE PROPERTY SUMMARY
AGED AT 90%RH, 90°F, THEN DRIED AT 180°F
SPECIMEN NO. AGING
CONDITION
TEST
TEMP(OF)
CROSSHEAD
SPEED
(in/min)
STRENGTH
(psi)
POISSON'S
RATIO
CMP-75F-90%(DRIED)-O.O5-1 90%RH(DRIED) 75 O.OS 826 .273 .145
CMP-75F-gO%(DRIED)-O.O5-2 90%._H(DRIED) 75 0.05 940 .286 .146
CMP-75F-90_(DRIED)-O.05-3 90XRH(DRIED) 75 0.05 882 .337 .142
CMP-75F-90_(DRIED)-O.OS-4 90_H(DRIED) 75 0.05 Q03 .322 .148
CMP-75F-90%(DRIED)-O.05-5 9O_(,RH(DRIED) 75 0.05 753 .234 .126
CMP-75F-90%(DRIED)-O.OS-6 90%,_H(DRIED 75 0.05 1011 .284 .128
CMP-75F-90_(DRIED)-O.O5-7 90Y,,RN(DRIED) 75 0.05 757 .312 .176
CMP-75F-90_(DRIED)'O.OS-8 90%RH(DRIED) 75 O.OS 1005 .315 .134
CMP-75F-90_(DRIED)-O.O5-9 90_H(DRIED) 75 0.05 835 .304 .138
CMP-75F-90_(DRIED)-O.OS-IO 90Y,RH(DRIED) 75 0.05 824 .252 .116
AVE 876 .292 .140
SD 91.8 .0326 .0161
CV (Z) 10.5 11.1 11.6
TABLE 16
INDIVIDUAL COMPRESSIVE PROPERTY SUMMARY
AGED AT 90_RH, 90°F, THEN DRIED AT 180°F
SPECIMEN NO. AGING TEST CROSSHEAD STRENGTH MOOULUS POISSON'S
CONDITION TEMP SPEED (psi) (li) RATIO(OF) (in/min)
CMP-75F-90%(DRIED)-O.25-11 90_RH(DRIED) 75 0.25 1105 .297 .136
CMP-75F-90%(DRIED)-O.25-12 90Y,RH(DRIED) 75 0.25 1022 .275 .138
CMP-75F-90%(DRIED)-0.25-13 90_RH(DRIED) 75 0.25 1006 .286 .124
90_H(ORIED) 75 0.25 1135 .321 .134CMP-75F-90"4(DRIED)-0.25-16
CMP-75F-90_(DRIED)-0.25-15 901(RH(DRIED) 75 0.25
AVE
SO
CV (Z)
839
1021
116
11.3
.29O
.296
.0172
5.84,
.134
• 133
• 0O540
4.06
32
TABLE 17
INDIVIDUAL COMPRESSIVE PROPERTY SUMMARY
AGED AT 90_RH, 90OF, THEN DRIED AT 1800F
SPECIMEN NO. AGING TEST CROSSHEAD STRENGTH MODULUS POISSOW'S
CONDITION TEMP SPEED (p4i) (msi) RATIO(OF) (inlmin)
CMP-TSF-90%(DRIED)-2.00-16 90%,RH(DRIED) 75 2.00 90S .299 .152
CMP-75F-90%(DRIED)-2.00-17 90Z,RH(DRIED) 75 2.00 1223 .292 .123
CMP-75F-90%(DRIED)-2.00-18 905QRH(DRIED) 75 2.00 1068 .282 .127
CMP-TSF-90Z(DRIED)-2.00-19 90_Q_H(DRIED) 75 2.00 953 .302 .175
CMP-TSF-90_(DRIED)-2.00-20 901¢RH(DRIED) 713 2.00 1182 .262 .107
AVE
SO
CV (%)
1066
138
13.0
.Z87
.0161
S._
• 137
• 0268
19.6
33
TABLE 18
INDIVIDUAL CC_4PRESSIVE PROPERTY SUMMARY
BASELINE SAMPLES (DRY)
SPECIMEN NO. AGINGCONDITION
TEST
TEMP
(°F)
CROSSHEAD
SPEED
(in/min)
STRENGTH
(psi)
MODULUS
(msi)
POISSO_'S
RATIO
CMP-75F-DRY'O.05"31 BASELINE 75 0.05 966 .285 .12B
CMP-75F-DRY-O.05-32 BASELINE 75 O.OS 907 .287 .144
CMP-75F-DRY-O.OS-33 BASELINE 75 0.05 875 .281 .133
CMP-75F-DRY-O.05-38 BASELINE 75 0.05 1009 .301 .155
CMP-75F-ORY-O.O5-39 BASELINE 75 0.05 968 .2_ .1_
CMP-75F-0RY-O.05-40 BASELINE 75 0.05 877 .293 .156
CMP-75F-DRY-O.05-41 BASELINE 75 O.OS 794 .260 .105
AVE 911 .282 .161
AD 71.0 .0196 .0208
CV (_) 7.79 6.96 16.7
TABLE 19
INDIVIDUAL COMPRESSIVE PROPERTY SUMMARYBASELINE SN4PLES DRY
SPECINEN NO. AGING TEST
CONDITION TENP(OF)
CMP-75F-DRY-0.25-63
CROSSHEAD STRENGTH
SPEED (pet)(in/min)
NCI)ULUS
(mt)
POISSO_'S
RATIO
BASELINE
CMP-75F-ORY-0.25-34 BASELINE 75 0.25 1071 .279 .115
CNP-75F-DRY-0.25-35 BASELINE 75 0.25 _ .292 --
CNP-75F-DRY-0.25-62 BASELINE 75 0.25 950 .289 .151
850 .304 .149
BASELINE
75
75CMP-75F-ORY-O.2S-4&
0.25
0.25
AVE
SO
CV (_)
916
80.8
8.50
.306
.296
.0112
3.80
.145
• 140.01_
12.0
34
TABLE 20
[ND[VIDUAL COMPRESSIVE PROPERTY SUMMARY
BASELINE SAMPLES DRY
SPECIMEN NO.
CMP-75F-DRY-2•O0"36
AGING
GONDITION
BASELINE
TEST
TEMP
(OF)
75
CROSSHEAD
SPEED
(inlmin)
2.0
STRENGTH
(psi)
889
MODULUS
(msi)
• 308
POISSON'S
RATIO
• 137
CMP-75F-DRY-2.00"37 BASELINE 75 2.0 1008 .298 .129
CMP-75F-DRY-2.00-65 BASELINE 75 2•0 846 .337 .1T7
CMP-75F-DRY-2.00"46 BASELINE 713 2.0 908 .320 ,17"2
CMP-75F-DRY-2.00-67 BASELINE 75 2.0 954 .31E •135
AVE 921 .315 .150SO 62.2 .0146 .0226
CV (%) 6.75 4.64 15.1
35
TABLE 21
INDIVIDUAL COMPRESSIVE PROPERTY SUMMARY
AGED AT 90_RH, 90°F
SPECIMEN NO. AGING TEST CROSSHEAD STRENGTH NOOULUS PO]SSON'S
CONDITION TEMP SPEED (psi) (ms i) RATIO(OF) (in/min)
CMP-75F-9OX-O.05"21 90T,RH, 90°F 7'5 0.05 473 0.0839 0.327
CMP-75F-90_'O.05"22 7'_ 0.05 51B .104 .330
CMP-75F-90_-O.05-23 75 0.05 553 .0944 .346
CMP-75F-90_-O•O5-24 9O_IRH, 90°F 75 0.05 584 .0992 .322
CMP-75F-90_-O.05-25 90_RH, 90°F 75 0.05 502 .0945 .342
AVE 526 .0952 .333
SO 43•4 .00745 •0102
CV (Z) 8.26 7.83 3•06
SPECIMEN NO.
TABLE 22
INDIVIDUAL COMPRESSIVE PROPERTY SUHNARYAGED AT 90_{_H, 90°F
AGING
CONDITION
STRENGTH
(psi)
NOOULUS
(rnsi)
POISSON'SRATIO
TEST CROSSHEAD
T_MP SPEED('F) (in/min)
75 0.25
75 0.25
75 0.25
AVE
SO
CV (_{)
CMP-75F-90Z-0.25-26 90_H, 9O°F 613 .0863 •287
CMP-75F-90X-0.25-27 589 .0934 .282
522
575
47.2
8.20
CMP- 75F-90_-0.25-28 .107
.O956
.0105
11.0
.334
.301
• 0287
9.53
TABLE 23
INDIVIDUAL COMPRESSIVE PROPERTY SUMMARY
AGED AT 90_RNf 90°F
SPECIMEN NO. AGZNG TEST
CONDITION T!MP('F)
CMP- 75F-90"4- 2.00- 29 907AN f 90°F 75
CMP- 75 F-90_-2.00- 30 90_glN f 90°F 75
CROSSNEAD STRENGTH
SPEED (psi)
(in/min)
2.00 616
2.00 622
AVE 619
SO 4.24
CV(X) .685
MODULUS POISSON*S
(li) RATIO
.0876 .255
.110 •352
.0988 .304
.0158 .068616.0 22.6
36
15.0 COEFFICIENT OF THERMAL EXPANSION MEASUREMENTS
Coefficient of Thermal Expansion measurements were made using the
quartz push rod dilatometer method (Figure ii) in accordance with
Test Specification ASTM E-228 entitled "Linear Thermal Expansion
of Solid Materials with a Vitreous Silica Dilatometer".
Sample heating and measurement was performed within the
isothermal zone of an insulated furnace, with controlled heating
rates that were limited to 5°F per minute. Sample temperature
was recorded with a Type K thermocouple, and length changes were
recorded with an LVDT displacement transducer.
Two sample sizes were measured for this program; 2.00 inches
length by 0.25 inch wide by 0.25 inch thick and; 7.0 inches longwith a 0.75 inch diameter.
Each specimen was tested over the range room temperature to250°F.
Prior to measurement of the PVA/MB samples a calibration test was
performed using the NIST fused silica standard reference
material, SRM 739-1. The results are shown in Figure 12.
The average CTE results for the PVA/MB samples are shown in
Figure 13 and Table 24. Tabulations of the individual values are
presented in Tables 25 thru 29.
Tabulations of individual batch formulations, individual
cure/aging dates and times, individual dimensional measurements,
high humidity wet and dry bulb measurements, strip chart records
of cure temperature vs time, plots of the high humidity aging
conditions, drying cycle temperature vs time plots, and the
individual expansion vs temperature curves are presented in the
appendix.
Thermal expansion is presented in percent, and is calculated at
each temperature as;
% Expansion - AL/L o x i00.
where:
AL = change in length (in)
L o = original length (in)
37
FIGURE iiCTE FACILITY
OUAR Z USii'LYDT SIGNAL J j
CONDITIONER AND
FURNACE CONTROL J J,
T/C
FURNACE
JlX-Y
RECORDER
GAS FLOW
OUT
r.9
Z
zmo..9cn_Zm
il.lln|n|l
I
I'i
l,,,l,,,l,,,l,,,l,,,l,,,l,,,l,,,l,,,i,i,l
" 0 0 C) 0 C} 0 0 0 "
I I i I
_uooaOduoisuudx._ IUmaoq.I.
39
o
oo_
I,,,,-I
TABLE 24
SUMMARY OF EFFECT OF HUMIDITY ON CTE OATA
TEST TYPE AGING
CONDITION
CTE (_) AT TEMPERATURE (OF)
75 100 1&O 180 250
CTE BASELINE 0 .0110 .0299 .0459 .0753
90_.RH(ORIEO) 0 .0101 .0284. .0_45 .0773
70°F SO%RH 0 .0048 .0045 -.0093 -.0159
90°F 90_RH 0 .0039 -.0166 -.0670 -.0700
CORRELATION O -.0049 .0006 .0154 .0393
41
TABLE 25
INDIVIDUAL THERMAL EXPANSION (CTE) SLINMARYBASELINE SAMPLES (DRY)
SPECIMEN NO. CTE (%) AT TEMPERATURE (OF)
75 100 140 180 250
CTE-DRY-36 BASELINE 0 .014 .033 .050 .086
37 " 0 .011 .029 .045 .076
38 " 0 .011 .030 .045 .075
39 " 0 .010 .02B .044 .077
40 " 0 .011 .030 .046 .077
41 " 0 .011 .030 .045 .068
42 " 0 .010 .029 ._ .071
43 " 0 .010 .030 .046 .072
AVE .0110 .0299 .0459 .0753
SO .001309 .001458 .001808 .005392
CV (_) 11.90 4.88 3.94 7.16
TABLE 26
INDIVIDUAL THERMAL EXPANSION (CTE) SLI4MARYAGED AT 900F 90_ RH
SPECIMEN NO.
CTE-90%-9
AGINGCONDITION
90°F 905_RH
CTE (_) AT TEMPERATURE (OF)
75 J 100
- .005
1/+0
- .044
180
- .091
250
-.068
10 " 0 .003 -.036 -.080 -.059
11 " 0 -.001 -.043 -.063 -.045
1Z " 0 .009 .003 -.050 -.062
13 " 0 .013 .003 -.063 -.083
14 " 0 .003 -.002 -.064 -.085
15 " 0 .005 .003 -.058 -.088
.0039
.005984153.44
- .0670
.013880
20.72
- .0166
• 023057138.90
AVE
SO
CV (Z)
-. 0700
.01_)
22.83
Note: CV(Z) value is not relevant in this type of analysis 10ut is presented for reference. As the thermal
expansion curve returns to zero percent expansion, CV(_) approaches infinity. A petter indication of the
data spread is reflected in the SO values,
42
TABLE 27
INDIVIDUAL THERMAL EXPANSION (CTE) SUMMARYAGED AT 90°F 90% RH THEN DRIED AT 180°F
SPECIMEN NO. AGINGCONDITION
75
CTE (%) AT TEMPERATURE (OF)
100 140 180 250
CTE-90%(DRIEO)-20 90_RH (DRIED) 0 .009 .024 .038 .066
21 " 0 •011 .028 .043 .074
22 " 0 .010 •029 .047 .082
23 " O .010 •028 •043 .078
24 " 0 •010 •031 .049 .083
25 " 0 .009 .029 .048 .082
26 " 0 .011 .029 •045 .078
27 " 0 .011 •029 .043 •075
.0284
.0019967.03
•0101•0008358.26
•0445•0035467.97
AVE$0CV (%)
.0773
.0056257.28
TABLE 28INDIVIDUAL THERMALEXPANSION (CTE) SUMMARY
AGED AT 700F 50% RH
SPECIMEN NO.
CTE-50%-28
AGINGCONDITION
35
AVESOCV (%)
70°F 50_g_N
75
CTE (%) AT TEMPERATURE(OF)
100
.004
140
.005
.004
180
- .012
.0O5
250
•024
29 " 0 .006 •007 -.003 -.006
30 " 0 .005 .002 -.017 -.033
31 " 0 .007 .008 -.007 -.019
32 " 0 .004 .004 ".009 ".012
33 " 0 ,004 .003 -,011 -.010
34 " 0 .003 .003 -.009 -.009
O! - .006
- .0093.004234
45.53
•0048.00128226.70
•0045•002070
46.00
- .014
-.0159.00899956._
Note: CV(%) value is not relevant in this type of armtysis but is presented for reference. As the thereatexpansion curve return= to zero percent expansion, CV(%) approaches infinity. A petter indication of thedata spreed is reflected in the SO values.
43
TABLE 29 COMPARE WITH TABLE 25
INDIVIDUAL THERMAL EXPANSION (CTE) SUMMARY
CORRELATION SAMPLES (0•25" BY 0•25" BY 2•0" LONG)
TESTED DRY FOR COI4PARISON TO LARGER SPECIMEN SIZE
SPECIMEN NO.
CTE-Dry-l-Sn_ll
2
3
4
5
6
AVE
SO
CV (X)
AGING
CONDITION
CTE (%) AT TEMPERATURE (oF)
75 100 140 180 250
CORRELATION 0 -•001 .002 .018 .048
" 0 -•003 .005 •025 .056
" 0 -.001 •006 .021 •053
" 0 -.004 -•003 •013 •049
" 0 -•007 .002 •010 •023
" 0 -•012 -.011 -.002 .012
•018-.005 • 003
- .006
-•0049
.0036O3
73.53
.001
.0006
•005423
903•86
•020
.0154
.00_1754.65
• 032
.041
.0393
.01560039.69
Note: CV(%) vatue is not relevant in this type of analysis but is presented for reference. As the thermal
expansion curve returns to zero percent expansion, CV(Z) approaches infinity, A better indication of thedata spread is reflected in the SD values•
44
16.0 MICROSCOPIC EXAMINATION OF FRACTURE SURFACES
Outer and inner surfaces of several specimens were
microscopically examined to verify that the microballons were not
crushed during the molding operation. No evidence of crushed
microballons was observed on these surfaces. The machined
surfaces of the specimens were also examined, and as expected,
the grinding operation opened microballons on these surfaces.
The fracture surface of the specimens were also examined, and as
expected, these surfaces also contain open microballons.
Photomicrographs were also taken of the specimens subjected to
high humidity conditions to determine if these samples appeared
to be anomalous. All photomicrographed samples showed no
anomalies. Reference Figure 14 for a representative sample of
these photomicrographs.
This examination was conducted using an Olympus SZ40
stereomicroscope.
Figure 15 is a photograph of typical tensile and compressivefailure modes.
45
FIGURE 14
PHOTOGRAPHS OF FRACTURE SURFACES
MAGNIFICATION = 55X
AS MOLDED SURFACE: TEN-75F-90%(DRIED)-0.05-77
FRACTURE SURFACE: TEN-75F-90%(DRIED)-0.05-77
46
FIGURE 15TYPICAL TENSILE AND COMPRESSION SPECIMEN FAILURE MODES
47
17.0 DISCUSSION/ OBSERVATIONS
Effect of Humidity and Loadinq Rate on Tensile and Compressive
Properties.
The primary objective of this work was to determine if cured
soluble core filler material regains its tensile and compressive
strength after redrying following exposure to high humidity
conditions.
The pass/fail criteria was that the material's tensile and
compressive ultimate strength shall return to within one standard
deviation of the baseline ultimate strength after exposure to
high humidity conditions followed by a drying cycle.
Figure 8 in section 14.0, shows that not only does the material
regain its tensile and compressive strength after high humidity
conditioning and redrying, but the conditioning cycle actually
increases the tensile and compressive strength. Similar
responses were noted for modulus and Poisson's ratio.
One possible explanation for this is that the high humidity
conditioning further distributes the binder (PVA) around the
microballons providing additional bonding sites and, therefore,
greater dry sample strength.
If this is true, then it follows that storing a pre-cured mixture
in a sealed container for a week, more or less, may improve the
distribution of binder (PVA) around the microballons and provide
stronger samples.
It may also be true that an increase in the amount of binder
(PVA) in a mixture will increase the strength of the samples.
The effect of mixture pre-cure storage time and PVA concentration
could be determined by testing samples where (I) The mixture pre-
cure storage time is varied and (2) The PVA concentration is
varied.
Figure 8 also shows that the samples conditioned at 90°F,90%RH
had lower tensile and compressive strengths than the dry samples
and that the high humidity condition is the primary factor
responsible for the large reductions in tensile and compressive
strength. Significant changes in modulus and Poisson's ratio
were also noted for increases in humidity level.
Also evident was increases in loading rate, increased the
ultimate tensile and compressive strength. The impact of loading
rate on modulus and Poisson's ratio was minimal.
48
Fillinq and Packinq of the Tensile and Compression Molds.
The method used to prepare uniformly compacted compression
specimens was to add the loose PVA/MB mix to the mold in
approximately 200 ml portions. Each portion was tamped and
compacted before the next was added. This process was continued
until the mold was completely filled.
Tensile samples were more difficult pack uniformly than the
compression samples because of the smaller diameter of the
tensile samples. We discovered that adding and packing the loose
material in =25 ml portions, resulted in uniformly compacted
tensile samples. We also realized that using a mold geometry
that allowed us to pack the material from one side, rather than
from the top to bottom, would have made it easier to create
uniformly compacted tensile samples.
Great care was taken to obtain tightly packed samples of uniform
density since we knew from previous work, with this PVA/MB
material, that the degree and uniformity of compaction has a
direct effect on the strength of the material. The difficulty we
encountered in creating uniform compacted laboratory tensile
samples underscores the difficulty we expected will be
encountered when large solid rocket motor molds are created with
the PVA/MB material.
It is our belief that the tensile and compressive properties, of
the PVA/MB material, is highly dependent upon the packing
uniformity and localized density of the material.
Some sort of automated packing system, which would insure maximum
compaction, would provide maximum strength properties and lowerthe coefficient of variance in the data.
Tensile and Compression Failure Modes.
All of the tensile specimens, aged at various conditions and
tested at various loading rates, failed in the expected reduced
cross-sectional area of the specimen. The compression samples
failed in what can be described as either a "cone and split" or
"simple flat crushing" sample failure mode. Reference Figure 15
for a photograph of typical tensile and compression specimen
failures.
49
Thermal Expansion
Moisture level has a significant influence on t e free thermal
expansion response of the material. Figure 13, in section 15,
shows acomparison of the effect of humidity level on thermal
expansion measurements.
Samples tested directly out of the cureoven and cooled in a
desiccated chamber, prior to testing, (baseline dry) expanded ina linear manner.
Samples tested after conditioning at 90°F, 90%RH, then redried at
180°F, and cooled in a desiccated chamber, expanded in a linear
manner like the baseline dry samples.
Samples tested after conditioning at 90°F, 90%RH, contracted
considerably before expanding. These samples were saturated with
water, during the high humidity conditioning, causing the sample
to swell. Therefore, during d_s/eilng, as the water was out
of the sample, the sample contracted. Once all of the water was
gone, the sample expanded as expected.
Samples conditioned at 70°F, 50%RH, under laboratory ambient
conditions, contracted like the high humidity samples but not to
the same magnitude, before expanding. These samples absorbed
some moisture, during the 7 day period in the lab, causing the
sample to swell. Therefore, during testing, as the water was
driven out of the sample, the sample contracted. Once all of the
water was gone, the sample expanded as expected.
The 2" long baseline dry correlation samples were anomalous.
These samples should have responded like the other baseline dry
samples. However, they behaved more like the 7" long samples
conditioned at 70°F, 50%RH. The smaller sample size must be the
cause. The small sample is more likely to contain proportionally
larger localized variations in density than the larger sample,
resulting in a greater effect on the CTE measurement. Another
possible reason for the discrepancy could be the contact force of
the LVDT. Although these are called "Free" thermal expansion
tests, there is a small force of =25 grams acting axially against
the specimen. This small load may be sufficient to effect the
CTE measurement on 2" long, i/4" by 1/4" square cross-section
samples. The cross-sectional area difference between the 2" long
(1/4" by i/4" square) samples and the 7" long (0.75" dia) samplesis a factor of 7 times.
5O
Current Proqram Compared to Previous Work
If one was to compare test results from the previous work (EMTL
Report # 1430) to the results from this program one would see
that the slightly higher humidity level of (95°F, 95%R@) vs
(90°F, 90%RH) caused a further reduction in tensile and
compressive strength. However, itshould be noted that the
tensile sample geometries were different for the two programs and
that the geometry differefce could account for some of the
strength difference. Also note that the previous programs dry
samples were stored under laboratory ambient conditions (70°F,
50%RH) and not in a desiccator.
General Observations
It was observed during the packing of the samples that the moist
mixture turns into a dry crust very rapidly (< 5min) once exposedto air.
For future reference, the specified cooldown period of 6 hours
before testing seems excessive. The small laboratory sized
samples, used in this program, cooled to room temperature within
30 minutes or less.
51
REFERENCES
I AEROJET ASRM, "Process Development Test Plan" WBS No. 1 4 3 4
DR-TM05, Type 3, page I.
52
APPENDIX
53
MICROBALLON CERTIFICATE OF ANALYSIS
54
p .
CUSTOMER :
DATE:P.O. #:
PRODUCT CODE-
PRODUCT :
LOT NUHBER :
Test Method
CERTIFICATE OF ANALYSIS
Fiber Materials Inc..
October 26, L992
72010 jSG
SG
ZI
Discription Resul t$
P,O,Box 2Cha_anoosa,Tennessee37
Te(ephone"615 629-7TELEX: 558
Cable: PAPAPPFAX: 615 698.._
U.S. STANDARD SIEVE
WT X OUER SIEUE
U ISUAL
hi/A
WEI GHT PER
MEASURED VOLUME
AI R PYCNOHETER
Y. LOSS OVENDRIED SAMPLE
PARTICLE SIZE DISTRIBUTION:
MEAN PARTICLE DIAMETER:
APP EA P_ANCE :
HELTING PO IN_:
BULK DENSITY:
SPECIFIC GRAVI T'f:
MO ISTURE :
I0 - 425 MICRONS
140 MICRONS
GRAY, FREE FLOWING
>2700 DEGREES F
24. I LBS/FT3
QUALITY CONTROL TECHNICIAN
55
_HIPPER:
,,,,,,,,,,, PACKING LIST "*_''''''''
THE PO CORPORATION
501 CI_MBERLAND BLDG. ?0
CHATTANCX]GA. TN 37404
SHIP TO: Fiber _aterials Inc.
5 Morin St/Biddeford Ind Pk
Biddeford. ME 04005
CUSTOMER P.O. NO: 77010 SHIP VIA: UPS
ORDERED SHIPPED DESCRIPTION
2150# haas) SAME E xtendosnhe res SG
ECEIVED BY:
56
INDIVIDUAL BATCH FORMULATION DATA
57
FORMULATION OF SOLUBLE CORE MIXTURE
BATCH MB
# (g)
I 1874.9
2 18T3.0
3 1877.0
4 1879.7 253.8
5 187_..0 253.8
6 1876.2 254.4
7 1879.3 254.1
8 1878.2 254.2
9 1875.5 251.2
10 1879.7 252.7
11 1875.9 251.7
12 1876.6 253.3
13 1877.7 255.1
14 1879.1 253.6
15 1875.6 252.2
16 1878.1 245.5
17 1874.3 251.8
(g_2o ETHANOL(g)
250.3 251.2
250.5 251.9
253.3 254.5
255.0
252.7
254.6
252.4
255.0
253.9
252.8
PVA
(g)
125.5
125.1
126.4
126.0
127.4
128.1
129.3
126.6
127.0
128.7
127.3
TOTAL
(g)
BINDER
TEMP (F)
BINDER MIX
TIME (min)
FILLER MIXING
TIME (min)
135.5 60 5
2428.9 138.2 45 5
2457.9 131.0 45 5
2453.7 131.9 70 5
2448.2 136.4 60 5
132.8 70 5
2443.6 136.4 60 5
2457.4 137.3 45 5
2439.5 136.4 60 5
2458.3 134.6 60 5
254.1 2610.1 131.0 60 5
255.9 127.7 134.6 75 5
253.2 128.9 2469.4 136.0 60 5
253.6 126.1 2460.7 136.5 60 5
254.2 129.6 2452.7 138.2 45 5
253.3
253.3
129.7
128.7
2458.1 138.6 60 5
2453.6 140.0 60 5
Note: Following statements apply for all batches.
Binder mix agitation speed: Stirred binder slowly with magnetic stirrer hot plate.
PVA addtion rate: Slowly added PVA to microballons by hand white stirring.
Fitter mixing speed: SLow mixed by hand.
Mixed filler storage time: For att compressions, there was no storage time. ALL compression batches werecompletely used or remainder discarded. For tensiles, storage time was less than 2 weeks.
JAB mixed all batches.
GMV packed all compresaiorl.
JAB packed tension #1 thru dKS. Not used.
GNV packed ter_ion #46 thru #117
GMV packed all CTE$
58
INDIVIDUAL CURING/AGING DATE AND TIME SUMMARIES
59
6O
61
.,p.
k-,-
'+"0.. m, o _ _ _ _ _ .+.o ., o, ....
Lit
_J0". +._
i+-<_
"-s.+,.,,
-I-
+++.<
N
O_ ++,,.s
Q_ z :I • l 31 I 11 II 11
t%1
o,_
z
mO_ll
z
_t
t_
It
Z
z
_M
I.I.I
|31.,-
++
0 P,,,li i
+-,,+ ...,,i ,
_ X
62
°°
|
i •
! °Z
|=
+
z a,.- '-
z
U 0 •
|
l
_ °i
l • I _ II I
0
i
i
ii
|
63
z
oo _° .... _ o.o° _ _ i
i,- +,-
C,
oo .° _° °o _ _°
+='
_-: |__
N
+++
N
!,
: : o,,_ ,
' = _81&o
I_I I 31 l,.,.,= ,,_ 8 o,,+,,+,.. , , +.+, .- _++,
z
mU
• I s • 11: •
0 0 i
i
4. z
I • I Z P. Z Z
i0
i
0*
Z
I
4U)--
.* Q.
0
E
64
_*i°_'__ i
°_-
. ° ." U"$ 0°
Z N
O _ * OOO
•* _ ,°
("k# N
Z
U
O
65
8_
Z R Z I :8 Z
OI
NU
66
67
zN u
z
N z
z
zm
_O
P
i
i i i i i
O
00
|
°
N
68
_ _i) t_ .- .- _ .2 z _ .-
i-
_J
C_C_I
- _,.i :
_J u
_ C_J
u _
tZ P_
_ f_J
NUL.Jii
C_J _tc_d
_0C_d
r_c__D
r_
aQ
L_t
¢._
I-Q_
C_
_J
_J
c_
Q.
cr_
o_
|
up
C_
_L_u
|
f,B
Q.
_U
Q¢
2E
69
|
m_
6
7O
HIGH HUMIDITY AGING WET AND DRY BULB MEASUREMENTS
71
HIGH HUMIDITY AGING WET AND DRY BULB MEASUREMENTS
SPECIMEN NO. DATE, TIME DRY BULB WET BULB RELATIVE
TEMP (°F) TEMP (°F) HUMIDITY (%)
CMP #I thru #I0 11106/92 14:00 90 87 90
11/09/92 08:00 90 87 90
11110192 08:00 90 87 90
11/11/92 08:00 90 87 90
11/11/92 16:00 90 87 90
Chamber #1
HIGH HUMIDITY AGING W_T AND DRY BULB MEASUREMENTS
SPECIMEN NO. DATE, TIME DRY BULB WET BULB RELATIVETEMP (OF) TEMP (OF) HUMIDITY (_)
aMP #11 thru #20 11/11192 16:00 90 87 90
11112/92 08:00 90 87 90
11/13/92 08:00 90 87 90
11/16/92 08:00 90 87 90
11/16/92 16:00 90 87 90
Chamloer #1
HIGH HUMIDITY AGING WET AND DRY BULB MEASUREMENTS
SPECIMEN NO. DATE, TIME DRY BLI_B WET BULB RELATIVETEMP ('F) TEMP (OF) HUMTDITY (X)
CMP #21 thru #30 11112192 08:00 90 87 90
11113192 138:00 90 87 90
11116192 08:00 90 87 90
11117192 08:00 90 87 90
Chamber #2
Note: Wet and dry bulb measurements only taken period|cstly.
High humidity chem_oer runs reliably for months without Klju=tment u preset conditions.
72
HIGH HUMIDITY AGING WET AND DRY BULB MEASUREMENTS
SPECIMEN NO. DATE, TIME DRY BULB WET BULB RELATIVE
TEMP (°F) TEMP (°F) HUMIDITY (%)
TEN #70 thru #85 12/09/92 16:00 90 87 90
12/10/92 08:00 90 87 90
12/11/92 08:00 90 87 90
12/14/92 08:00 90 87 90
12/15/92 16:00 90 87 90
Chanioer #I
HIGH HUMIDITY AGING WET AND DRY BULB MEASUREMENTS
SPECIMEN NO. DATE, TIME DRY BULB WET BULB RELATIVE
TEMP (OF) TEMP (OF) HUMIDITY (%)
TEN _ thru #93 12/10/92 08:00 90 87 90
12/11/92 08:00 90 87 90
12/14/92 08:00 90 87 90
12115/92 08:00 90 87 90
;h_r #1
HIGH HUMIDITY AGING WET AND DRY BULB MEASUREMENTS
SPECIMEN NO. DATE, TIME DRY BULB WET BULB RELATIVETEMP (OF) TEMP (°F) HUMIDITY (%)
TEN #94 thru #101 12/11/92 08:10 90 87 90
12/14/92 08:00 90 87 90
12115/92 08:00 90 87 90
12116192 08:00 90 87 90
;hasher #2
HIGH NUMIDITY AGIN G WI_T AND DRY BULB MEASUREMENTS
SPECIMEN NO.
TEN #102 thru 8105
hmber #2
DATE, TIME
12/11/92 15:20
12114192 08:00
DRY BULBTEMP (OF)
9O
9O
WET BULB
TEMP (OF)
87
87
RELATIVEHUMIDITY (%)
90
90
12115192 08:00 90 87 90
12116192 08:00 90 87 90
Note: Wet end dry bulb measurements onty taken periodicstly.
High humidity chamber runs reliably for months without adjustment ms preset conditions.
73
HIGH HUMIDITY AGING WET AND DRY BULB MEASUREMENTS
SPECIMEN NO. OATE, TIME DRY BULB
TEMP (°r)
WET BULB
TEMP (OF)
RELATIVE
HUMIDITY (%)
TEN #106 thru #109 12/17/92 08:30 go 87 90
12/18/92 08:00 90 87 90
12/21/92 08:00 90 87 90
12/22/92 15:30 90 87 90
_hant_er #I
HIGH HUMIDITY AGINq WET AND DRY BULB MEASUREMENTS
SPECIMEN NO. DATE, TIME DRY BULB WET BULB RELATIVETEMP (OF) TEMP (OF) HUMIDITY (%)
TEN #110 thru #113 12117/92 16:15 90 87 90
12/18/92 08:00 90 87 90
12/21/92 08:00 90 87 90
12/22/92 15:30 90 87 90
Ch anlbe r #1
HIGH HUMIDITY AGINq WET AND DRY BULB MEASUREMENTS
SPECIMEN NO. DATE, TIME DRY BULB WET BULB RELATIVETEMP (°F) TEMP (OF) HUMIDITY (%)
TEN #114 thru #117 12/18/92 15:45 90 87 90
12121/92 08:00 90 87 90
12/23/92 15:30 90 87 90
:hanC>er #1
Note: Wet and dry butb measurements onty taken periodicstty.
High humidity chan_Der runs retiabLy for months without adjustment as preset corw:litions.
74
HIGH HUMIDITY AGING WET AND ORY BULB MEASUREMENTS
SPECIMEN NO. DATE, TIME DRY BULB WET BULB RELATIVETEMP (OF) TEMP (OF) HUMIDITY (%)
CTE #9 thru #11 12/17/92 08:30 90 87 90
12/18/92 08:00 90 87 90
12/21/92 08:00 90 87 90
12/23/92 08:00 90 87 90
:ha_d:>er #1
HIGH HUMIDITY AGING WET AND DRY BULB MEASUREMENTS
SPECIMEN NO. DATE, TIME DRY BULB WET BULB RELATIVETEMP (OF) TEMP (OF) HUMIDITY (%)
CTE #12 thru #15 12117/92 16:15 90 87 90
12118192 08:00 90 87 90
12121/92 08:00 90 87 90
12123/92 08:00 90 87 90
12124/92 08:00 90 87 90
Chan_oe r #1
HIGH HUMIDITY AqlNq WET AMO DRY BULB MEASUREMENTS
SPECIMEN NO. DATE, TIME DRY BULB WET BULB RELATIVETEMP (OF) TEMP (OF) HUMIDITY (%)
CTE #20 thru #27 12/23/92 15:40 90 87 90
12/28/92 16:00 90 87 90
:hamber #1
Note: Wet mnd dry bulb memeurmmnte onty taken periodically.
High humidity chamber rurl retiabty for months without adjustment IS preset conditions.
75
INDIVIDUAL DIMENSIONAL MEASUREMENTS
76
z
N
z
N
N
• , , o
_ v
z C
_v
0
¢) ('M
Q.
0 (.I
77
78
uJ
N
¢2ze¢
N
z
u.I _.3
_ 0 °
• 0 ° 0
• -- •
v
=
O O f_l
Z_ _ _= =; _=_, _ E
79
8O
_=
o1[
,1[
N
x,C
N
zw
A
N
O _. ° .
!" ...
__=__J' uJ _
N _A
N
°, , ° ° O • •
Z
N(=1uJG.
_5
0 n
0 n
UJ I*U.I
O
_=_
I
e
61
¢=,
61
Q_
81
t_ _J F_ _ _ _t _ P_- CO aQ Lt_ _ L_o •
tv _m9C v
L_ L_ L_ i i i I I I I I I I i I i
_ c.3 i _ i i i i i i i i i i i
N i
,__^ I i i i , i i i i i i i i
ol °_
qLm,LD
OV
Z
_E L--
_ _ _ _ i ¸ _ _ u I I
0 _
0
_J
U
IcJ
U
LDO
Q8
-8U
L_
U
air
82
c,_
i
z
M
m
..,.,,
Z
_" ud O1
=¢._
-- E
(,J .,'_ _,.
W
O',
z z z • • •
M.I ,_,,.I
i'M i'M _ _ _ i'M
O
A
,.=,N
Z t
Ud ZG. UJ
O
ti
3U_d
O
,4-
fi
-8U
,IU
n,e
83
wz,z
9C
N
0Z9C
N
Z
NVbZ
Im
=P
ZN
_ _ O_ 0 _ F_ 0_ I_J _ _ql U_U_
_ w.'- p,
_i_ Lu q_J
i i i i i i : i i i
a_u..I r_N No_ _ i i i i i i : i i
DI _! ,_ v_p _l" _PI q_P ,4' _t _ _ _' ,_t _t
LP
_ ,jZ_j _ '_ _ -4_ '_t _IP -4r _ ,4" ,_P "_t _
_j _ _ uJ Lu
Ua_
84
,.=,
N
Z_J
t'_
UJ.-JNGr/Z
¢--,
N
85
z
-i0N
zN
F
z z _ _ _ _ 0 0 0 _ 0 o 0 0 _ o 0 o
_A
, : : : : :
: : : : : : :
_ _ _ _0 _ ;'5 _:
WJ A
A
S_ (_d _ IM N e_l i'M e_a N
I'M
, O rM _ -4" i_
86
z
u,J
,=C
o
e(
z
u
u
zi
e¢
==
:=
: : : : : : : : i : ' ' ' : : :
: : ' : : : : : : : i I : : :
: : : : : :
_._ °
_ _ _ _ _ __ _ _ _ : : : : : : : : : : : :
_ N _ ",_ _'_ _0 _ _ _ 0 ¸¢_ _ N _ ¢_ ¢M I'%1, ¢M _ _"_:
N
)-Q[
U
87
CURING AND DRYING TEMPERATURE VS TIME STRIP CHARTS
88
.... :-- __ .lO .........
. 1
-+ f •
o
• • i _
.... i •
"t- --+ ..... +.... -_o -T-L7--7.... +T--; ,- .-- T, + - ........... --'- _ _ ;_, .T .... ! ...... + ,.+ + ,- ..... i .... '
...... ++ - _ ...... I ..... '+ " t " - I ...... P .... , -I ..... + -I _ . + . . . - t • . u - - r ....... i , +._, _ i <._ t _ r- _ ....... +.... +-4'.................. -p- --t ......... _ ...... I" O '-r --T ..... _. ...... _" . ..... '+ ...... + :"J
_- f .... i :-- , - -_ i+ "- - [ ' , . " i " t_ _P ........ ' .........II ........, ' ' ............. r + " + 1-" r ++ +' . . .......
• _,--,r__ _ _ .... +"--I .... J + .... I .... - I- ' 0
._ L ........ _-- i-- , "i: .... + ' " :: " 17_'_"O
i:<.>I .-- + ' .... '-11.-'_.":-:::, " +.....i , _- ; " L " _.: !:-"+: " :- + -_ '-I- -i. :._--'"" .... '--'- ;----T '+ ;'."z'__+_............... ' ................." i'- ............. 7"........... l+'............................ , - I " i'r-----I-'---_
............ ' _ ..... _ "-I ..... i ....... _ ...' . .! ....... , ........ i" .......I .... , + ++ _ .... L+ + ,___ + '" _+" _ L ..... 11 I I ..... +
; - .." -"_ ...... t- "' .: t-- " --+' + ' " " ':. ,............ -I--- • ' '[ --i _ ,..... '. _ _.... ,._
..... r_' --." ' - .r -- T.......+.....[--- 0_.......... T .... "-''TT"-+-P-T+.._ . -_" ....... . " " "..... '........
|_.. . J -_..j:.-- _....r.r++ - ! + _. -- , .+- _ - f • _ +-- " , i . _ L_- _--_lJ'-J_+-_ ..... t ........ - ......... "-'--' ]" ........ ' " "" .........
...... _ I .... + "" r'll;q'-- t--_ _ I " I : " ' r -- I 1 ; _ I --+--_:"_(P__."_-" ........ t . ; . . + . . . . . , __ ,. +_L--.-i i.__.__u.u-._+..+J--.lU-.i-'.-,-...t.o- - 7"' --.;- ._i.._._.__,.,__,+_t ' ; .i_+..___+__' +____..i.---J-, _.--.
i IIIlll_!IIII
Iiltti! lillll
I !!!!!!
i iiiillIIIIII
! [llllli lll!ll
_ iiiiii
! i!!!:!P lliiii
i ;1;;;1
ijiiiJ'_III
Illllli IIIlll
iiii
i.i: as-D7
IIIlt i !l!ll
' I'-i-1-_ -i _lilllIli+lllllttl lililIlllilllll!+ Iltli
<Llill+lltlll _11!]
"' +.ri-t,- -H-lit,,.,,,,,,,
....... <- • i _. +_.LL-_ (--!- -Y+..... "o. _ .. --:'--'--_-GZ--T-T_--- _.... --___+T-- -.-5-T
_____:-_/-----!_- + _ e _ ....... , .........
............ 4 ......
+ .... + ....... : -: ....... ; .......
'+ ++.... ; .... +- _ ..... .- ; • .- r- ,7. T-'-+ ..+ . -- .................. :.-........ ,_---- -_--- -_L ? + p .... + ............
'+:;- +-++ -+ --- " :-:- - '-+i +-:+:=-+:- +:_. + ---+ ........ __ _p. +---b ++ --j - _V.
_----+--q---i_ .... : .... + ----7:- ...... -+ +'...+ --. _--- _-........ , .... + + - _-.... i .... ;.-.......... t ..... _ - -+---- : ...... +......... f . ', -- + --_ - . +. . ,i_. __ +
.................... p ...... + • ...... 4+-....... .p ........ L --- --L --- .+- I ...... ! .... +-+-+ ..... - ..... ',..... ++j----+--....... *.+-+ ..... ' - ___.,+_ + ,.--1 -- _ --.+.- + --""+"---_---+_ ' ----r .... -..k+ -- -L .... '__ _ +__+++._._.__J ............. J.__.__ +
i ..... + ...... + ----+ .... " t "--"---'- I .... -k .... L O . + .... + __ '- + L_ ... + . +. "P.. _ J +' ......
i--- - b+ +- +--- + ...... I- ...... L+---I- ........ q- ..... # + -'- • I P-'- +'- t - '-+ ..... i-- - _-- -F----L _,i_........ I- ............ :,,.--.__ _'-..[ ...+"...'_L:::. -+7TILTL:-. :_ +:" " [
.... - ------L ........... d ....... r ....... +-- : --,_--_ .... t .... f ..........I ......._..... +--.....T---_-+---_-_+i+<i,-..,m-....._--,----, .... +.... +........ ----b .... +. I_----i--_-_ ...... ---i-- .... I- ..... +-_.___._-_t...... +---- ,-,'i--- -i ...... t,..+,-LL - +-_- r .... ,.--- - k+-'-_ - _;,_<"-_---
i ............. --_ . _.._L__ i . _i.,i` . ,i _F _,i'__" ...... i- -- . . I _ " " _--" - - i-_" "_- "+'r-........ _- .......................... ,................................ +_-,F .... -;-;--_-m__-_-_. t._++ _.J..'+l - .f'_'_-T-L_--+_ ,'C__:,_T _.--_ "-'-----f----+ .... _ _..--_'.'.'.'.'.'.__.... '------_-------i--
+ < i kr ,+i" ..... • ..... i .................t -.+ .... -.4 . t -,_ -I ....... +"'_- -l i --:+--- -- i .... ,----J---[ .......... I--.... _.
, , . - , ......... =i .... t - " t ..... / .... +- - ,i ................
-+--.;t-_-- -.- -t-+ 1 _+'_r__'-_-'__+ ...... ___.___ .... t_ _,rm__,..+..... f_ +__ _-c_._i..;_ut.---++-. .--' i-_--+'- -_- -+-+i-4-u .-i- ,_---- i--......... i.-,--++-..-_+--+-i- .... -I.- ...... 7- ..... +i-___ _++,. -' ,--.-.I.-_.... l-
- _+---+-I--_-_-+ .- _-..... +--,-. .+ .... _ .... -i--.--_.- ,-,.+,- --( --+-4----,'-+I- -.--I+_ ...... -_- i..+-i-,,,..-_-._--...+-.,.+ i , + , + j + .
.4-
i
-I.-+
i-#-iI
i
_i
fI
I
1Ii
1
!I
_ T
4 -+_-_-;I --- -_" !TT. +
i li;Itl
_" !lilt'
i
I
+_ _.L.L+::-HI
: i i ij
: ::+ _J
i .,' i,
I. ;_i
: _-V
9O
,_ _ _ _ ___ _,.4_,,o , ; , , .... .... _ .... :--;,_ --..
" -2o _ - -__-i-_ /IC'-" _' - '[. .. " __ : ._. -' ' * i _ 1 - ' ......... . .... [-"
'." " ,--:-F' "- " ' _-: __ :-i- . .
i i
• ..... ]" " i i
- 0- _ ...... ,'I'- ......... r ................. , - - r C......... _ . f --_ ..... . ...........
i ...... L .....
. _- t" -- ;.. _ _. L __ !_ _ _! .... . .... ; .... ;L ..... i....... _c .............. __. _
! -_ - t • _ _ - ' ...... _ L........ -4--- --. ...... L_-__ " _--" -' .... _ 0....... ; | I . I _ " | "
"c r ..... !-" r- -r .... t-i--r ........ ---r----I,- I .... I - , "] . , c . r , , '- --, - . -_- I ........ • -_ .... i---L-r .... ;-- - : .... _ -_ -
:_ ....... _r , .... i ....... t I ......... _fr, "_'"_! ...... _ " - -
, . L ---| .... : " - ' ...........,.; .... _..:_:_it.L:_..k___:[ ._L_: :-i !_--
.-- --_" ._ ---' .... r'-- . "; .... . , - --r .... ;....... r- ," -_ ;,,¢. -.q-
- i"_-_'_l'_?'L " '"":' :-;L_ " :. _-.. :-.-:I- -:-,-:
91
, _ .... o _ "7"T_7 . ........... ' .
+ - -- _- - - _ --r .......... , _ _ .... I _ . .__ 1.......... .._ , _...... . ..... . _i- ! -]-°_- i .... i. :...-:.-.-_:-_+--_ :....: -+_-
" " z - I ........... , - _. " " ;-,_'I..._-- _: ';- - r ...... : "- .... + -, .... I: ........ _...... ,_,_ ,'_ ..... _ ......... :!-
.----T .... _ -,, _-_ ..... .... _..... .- _-- _y_._--, ,-_- :---_" .... , ........ + -- ---'I" - _ -_ ..... ! - - i " " _" - -T --. "-" q".... ' -
.. . l____I ......... , ___ I._.__I_. _ , -,- -
._-___'--.---_ _.__ -_ ........ r..... :-. -_, ..... i-''--- _ - I .... I_ . _- i t" r _ _ ,.... _ " r .... _..... , • ++--..r -
; " _- -__ i .o _- -7_ '. . i _ .,. "_._- -_-__J_-+_._--.-;. __,_2.2 _--..___.'.c-- . ';.--__._'_----_.-+Y_'-_-- _ _ _ _. :. ---_- ._ _-7, "_--_' ...... _ +-: ;--- -_- .... I--! ..... _..... I .... I ..... ; ---- .... ; + ...... "' - ', ..... _,--'r_ ..... ÷- I"--._. .... i+-+-L .... :_: .... -. :-- '--,_I ._.,--_-..----_- I-----!_-.-.._ .... I--L-_-....
.... -_"..... _'":--'--I-_- l .... i--- _---I-'-'-'[-.-'-_-_--.--I" I_----I-_' "_!-_-- _,_---_-_
--_----.-- :---- -_ --4.---_---,--'- .... 7 _L'__ "2 ji "_Z_ i
92
!-_:-:-i-_i--____,+ +_- -:- : ....... .....-::• +- ° ' 1" "
i - " _+ " " i ....... __--_ _:-:_ 4-- _ __ '................... _P ............... L .... "1.......
_2___;2__+.i..... -___:CL._I. -'--.2___2__--.-L.__._._--_.:-. - _ .... "" r .....
...... ::__-_L_ _ " _.--- L.L_.J_-: _. __:_:_'_.L.: :_ . _.'. _.+.-LL __:_J-_: .:,.,_:_: ,_..L _
........ ', -- 1 "--_"r-- ,1, rL-_'.T_ ..... _- - _; " -' - '_i - 4 - "-t --- "_.......... _-_ _ _ ..... -- ....... " -,...... ,-- "T-- _:--'-'--:--
....... :- I:__ , __" +"+;_-__:J_ _ _ _, . t ....... ,; ._._,_ .....
_ u............_ . ..... _ ............... _---. -_- - J--.-_ ...... Jr--...." " " ' ' I I "_ r+l _ I '
__ . ) .j.. . _ _ It+"_ .... " ..... I - .-l- .... , +--I .tj " " L.. L-I" ' I _ ..... ,._ .... ++......... _ . .._ _ - , . _ _ [ .......... + +-- ..+.-,
..... +...... ..... L- --- ........ " .... _-+--_ ............ +-.-- ----I- +_. ...... +-'1"-'--- -- +----- +'--- -+-- 4--;-'-+
.... +-- _++-r:-i .-4++- _]//_..: ,.- +. -+, ...... :L,_--,+-+'+-=---:q--
93
o
-. " • . . ._ ._ . r - t--...... t _,, L..- ........... ... : ---:. ..............
- " " i ..... o __ - . -- : .... __, _'/:__ _.----I--:-.-_ ....." • -b I "
....... '-- L_) - ', -_-_ .............
i-_-:_ I :-4 ---!- . _ ,L- _'. ..... ,_...... _- ...........-_--.-.._.----4---:_-_ ........ --P'..... i- _--Z; _----i.--:---i -r.T----:-_- --r-- ; -- - .... :i __ -i " ',a:_o_-F -i ...... --:,_,,.,_i.-::- i-----'.... r_ I ..... ', ....... :rl '-''_ "r'_- "-' ...... r.c'p_ ................. : ..... • _ _ ..... _ ........... : ,_'L_ , _.... I-, -- • ...... ;_r-_-,_._,- , _ _,,,,b ...... -,---------__ _-_.._L:L:-.... _-I_.-: .... p----tlh-_"_- -.---_.LT-:__ .]_i.,-_L -_....
_-!-._-_:-_', ... U. .--I- -- , ..... _- --I -- -._ i. .... 4-- ..... • ; ..... _....[ .. i ........ i-_ _...... ; .:.-,,_ i-- ...... - • _, - ....... ,---- -
:i-:_l-.- --: ..... _ .... L-_---t-_ ':,_I,_. ._-,- : ..... -,I - -_...... ; ...._-----_- f .... t .... ,-r _:Zj-____. ' " 4-,I-----+-- ........... r- ----I- .....
-_----_-I-:.. : :_--G-::'_.__Tm----[:--Z. -.._-_:'_---_ ..... : : -_'. .... ::L_:_ i :: -' "" :_I" _, , .... ; ---_- .... _ '---,4_- .......... r'- . _, :J .......
-" :F::. ": '" -+-'" _":"-, 0---,--" ..... 4-_ . . ,.-_rr--_ .... _-...... r ---_ _-T_::-_ .4----
94
- i
• . b . . L
_ "-.,4...........
I
_ _ f - ._
i
95
i l .... I
96
rL
• c
................. i -3L -- i ": __._ , t- -D.__--
i
b
t
• L.: ......
i - --t
- - - T "
...... -""1" .... _L . t . . , -
q .... ,.... _ ......... T ..... . -- -" , i " -" ] ............ _ _ L. _ . I .... . .... _.... _-.1'.. i. . -
-- T I" " '_" " I ..... F- . __..... ' .... i' "" i "- L ....... -I _ - - _ - " _ "- F'-- ' , _ . $_--- r ........ : ___:L__ '--., , ..... _ -- _' .... li,___ i.___.=,I.._-- T- --_"-'r-'---- _ " L
..... --' ......... ' I ' . .......... I'-T :" i
. -, -.+- :.... ,_:---:----.i - -- t....... l ........... "-i' .... i_- _. _ AIl__ ; _--_--
..........---'_----I:....T'-- -:....... _-_._ -, -- , _ "¢_.--:T._-+.!'- -- _ _._i ..... .'..! ..... , .... • " " " "..... _'- _-" --L
.......... _ _:-_:.h ,-- --!...... _ ' ---I .... -:_--. - ..... , "..... 3T-.L-::L ......... I-- _ - ,._ _ ............ ' ..... q--,_ ........ --:-7<-'l-------r _ -_ ...... o ,- - i .... -....... /--
- : ........ -_---l:'_t" ":_1..... 7 .... i - ,,- : ._: .... _. -._--_' - ..... l- :"[-::._:t. - _-- -1" --T-. i .... ' ..... : ......
-, -i- 1 -- ,:- .. .... i ....... _ " ' ..... - ......... l-_',""" - -F---- r " -_.-_I-- ................ , O- -: .... : _-_,_--V-_ "
...... F'__ _...,-- --, ........ ," ": ', • • .... l "-- :i,_:.:_"
::4:-;_.-_:_L__ _= . ! - ,-i-:-::: f::: : --"--::-:::4-,T--I- -- ....._ :-;.-::':-:I .':-_,"-Lq--7:
97
[
Z:
i
+
4-1
-k1I
I
J
!
t
i[
i
i
I"1--
1
•,_- I--
4! i ;"_m _
.0_ ;, i';:-'t 1"1-I-t'- _,--_
-_ _!'.l!Ld•
I_II-
98
•- [; .......
. . _ . . _
-- _ : - _: ::....- "__ L
} . :
1
; - ' .. - I ...... ! - - , - ' r--" ' " ..... ,
I-
. ... q_.. , _ .L ..-_ ....[................... ,.... ',---i-• o._ _ ......... ____ _.___ i_. _ -.... r---_- _--_ .....
..... I "'" I _" _ _ _ _ ' ......... I . -_ _ -_ - , - - *........... ;r -', _ " - _ , ,_ F k __ I_- I
....... --4 ............. -==__ _r--_F_--_.....: -
........ ,"-;-.._.-I--;"-I I_':.-4_......!-_---];--; r . _ ........... =__ .......:J._',G_-, ........ r--,- , .:_!....r_-.-:-:L-_:_:--_-i
........._,-,_-_.__- ....,_- , , ._ .,=.____._......._ __+....r_.__:._....... _ _,5-- ......... 1---r -- " I " , "" _'t .... , , _ l ' -,
__L--J-"t' "--.l.r- .I 0--'--- ',----'_ -_ _";-'-I "_- -I-__:';-'_'"---+--'-- }--i'---I-_ -' _-'-'"_"I-_-'"-I; "
99
' l " - -
_ . . .... ,t. . - F-)
.ii!
lO0
---I......i--' --F.-T----------7---]-; i; -_ ....
.;,__;.:,.. _, J_r_..-T...... _:-'- - ' .........', l_ . , -"
: -i-- :- F • i - , ,-
----_1-i --7i :: ;IT. ..........-- .............. '--- '- --r ............
i. _ ';'. " "" .__ _;_ ._.. -I i '"
' ____ L-..... _ .....:I--:---- -:-._ .... I" ,......................................- i " ._ . _] .....] ..... ; '" ".... i..... i ....... -
._ _, ___. --__-__Fc!._i;_i]_ __-- .i ! "_ - ..... :_-; :_-.:: '- i .......
--*£[___';_-___-A_-_'te--_--+ ........ i-.,- .... _---t ........ i .-i ---- .... i. -LL¢_._____._,-i-_,,, -4 , _.L_ ........ o ............... ÷"
I01
. + . o
i i -i
o _ _ .....
, - r --
+ -_ •
:_" : .. i '........... {-J ............ L. ....................................
.. __ _, 0 _, I : E - ""
_L_.,- ........ -=,__+_2_._LL_---.t.L:.___. =_LL-_.+_.._:'__L__i_.:__LLZ_ _!._-;_..:-_-. _2j.+_._+_Lz_; ....... o ._; . +, ...... +- t...... " 't .... _ " _ ' "1.... _.......... _ ......... ]' "_ ..... ; ................. _...... [ -r...... '[ ...... l_-. t- - ' ......... + ..... J - •
.... I .... t-- .--4-u_ --| ..... + - 1.-..... ! L.+ . .... : '---- , -_--- ,-_-.-" , -_ + --- 1 . --_+.... I " _ " - '___ .:.___ 3-..3- ........ .-.-L... __L ..... L:.-..--L. ..-._ _ __.,.... .... _._..... ___.__ _ _2 ._ _......... _, ....
F- _.--i -+-+-.-i .... I'- +-q"+"r---t _J- :- "_+,_-i-+'--_-,"-'+ ; .......... +-..... t-- + ++--+'•+-'--+ " •+ , , , . , , , ., + F . . ' + +
t ..... r ........... ;-.r+l. + • , P - + "I T-; " +;" .........
____ _..+ , .+- -.1..+..-- ----- + _ +-- +,-_ ...... _ -+ -- -+ ........_:_ . .... IT-_.._ ,. ' . ;,_-+L'_._ ....... , .... + .... -- .....
F-" :+--r--7--:--m----+--_.-:----='_= _---'+:--+'-'!.1_"- _ "'-''_': ---2 .... -- _-"_- ".'-_=,_ +-T_] "-'" '_7""t=''-- +'-"' ' .,r _i .... "P'-............ I'-" ..... '+ .... "+..... "+.... +--"........ '-'------','--r .... I'
!--=-=_-=+=-_-+r.;_._.,_ -t-+,, .-P +,:,_.,-,, ++-++I- -i--+..,-' +, tin= +-- + ,-:t +=:- r----:' "-----P------ --" _-'-1-+-_TI+---'--_. ....... _--;" "'r-:-. ........ -t ,-P--, -'*-.T ....... ._.r--:-+___1:,o ..... ++___ --I= --+r_,+_+_-f .T .... , .... q ...... _ ,,
..i ,.; ....... _IL _i_._ __. .......... _j+_ ._ ...... _ _._+ ,I. .... , _p_ i .... I._. +-++.. t_ .,. _ ++.+_I, :++.t_ _ '. _-.,.r ,,.,+.,].., J,_._ ..... j_ . .f. +.,.__-T._ _,J-'_4._ '-t,--'.--+l -- - i-,- ;-++.-]+ .... ]+-,--:I
__._L_ +'-"2',____.i _,_'.._'...]__ .: ....... _. .'_.. _, ,.._....x .£._...i_=_,. ._._ _.J_._ .__+. ..... .,..__.__+,_t L30"O.. _3 3P, _ ""+',=
--, +i.
TT] '::;_ +.+-.+..+.
-r-r,1 ,iiiI|i ,
_, ;ii:..
II1
t,I i!i!.
_li _
+_' iii!Ill
[li :::;
t t l _ g| II !:
-t41 ....
4-I
4-
i
!
-4.
II
F
iI
i
!-
$I
1{12
L . . • , •
l
- t "-" "---:. . -- - " I , .... " t" ' •
i. k. i:-_7 - " • I-_.L--L--'i-----:----,-----_---.....o-.... r-......e ...... '. . 7-.- _............... r- - : .. , , _t.....L- -_. 1...... . - -- I' ........ ' _- " -"
_: ..... .-]....I-:-_...-:_ ..__ ... -I-_ _'....i.......-.---:_ :_ _ _---.... F--- _.i_;_ _ " : , , .' ..... ! --bl,._-)¢ - " , ...... ____.._.____ _-_ e--------_O ....': " -- t.. - " ,-,. '-'e"._e'L'u=_L__- i . --.i--_---_ .... _---_"._ ,42,,_--;"--i --:- F _. : .... r ,- - 4--- 1-"'--'l-_-_:.--:-io:_-#il.-- _ -[--- | ._,,j,:_ll_.i,H_-_._ r....:_.-_ .,+--_---:L-___-'_:-_-- _ , - ..... '- ........ ' " . . -_ .... I---_ --, ....... 2---I •I--; I _ "_i_,,_- -i -4 ......--&_--_-_i_......_-:..,....L. ,_.u_._.L .____.,.: -- '.-___L__i,i_#-c-- - -,-------t-r--,-_,_T:-. •, .... I- _--.,' ,- - ' t>._,_.-----:r..... - _ ".... _, _ ' i_ i "r- ll_- i-] r -ilia- '- " -I [-- [ "rl'' : [ " " " i....... 'I T.` " " ' .... ] i "
i .... : .+ x_'i'_--- ',_ -- _-I_-F"--r-___ t- . .,_ . _ t "-_ "1 _- - ...... _" l -_ _'.
: . r-.. "_'-,_ -._ -- __..... _'---..- ._"_'--,-_,4.-..... :_--" :,,2, ................ ' .... _.... : _ l ; ....::-- -,....
-,---, '_. _'-.-t -u_- t--...... , .... .t- - ._. " __.... _- __.-[-,.-.,-._rb-- ;------k-----+-_ :-- -_-_-"
" 1 _ _ ÷. _ - I i." -_' _l_, , / ._- -i ...... @-+4 r-" f" ---p _-"r--T -" " ' t- ..... i--_--
, _ :--........ If_'_i_......... i - '.- ;_ ....! - i":C"_"_ '_I......i:......_ ...-.-_o_. , • .... t ..... -.0.._l'._--'--_-- _.-:_-_ ................
103
" (__-- 7""-'-_°, : ' -: -
t_
:_2-_2 -._.L.
- , .....,-- -7,..... i--0, : .... ! ....- _--_i .... ;.... ',__ ........ J"- '_-_--_ ........ r "- H ......... : .....
,.-i-.-_ ---:_----_:i_:-__---_-: ---i---: ; " ----I .... -_---'_.LY -'
,,-?-=_-_ .... J'_r :'- -- =_-'...... i V.--_ . i--:'_.=:-__-_ - _-.....:......
,-.-I--_:_- _-X_l-:-,-.-...._....v
104
. , .. .2
I -l
I i : ; --T -!- : ":
- - -Z __-. ......... ' '> _ '..- _ ...... p
iL-- _ -----, _--_ ..... _..... ;-.- _ ....
__.__._; i..... ...... _--L:L!-;L-." _-.._-. -I. " ,,____;__;_:- .... :_L
i ._ i ....... _-..... i..... t-;.... _-- i ..... I- " " .-+"- _" " _ ---1 -; - " --- -I .... i-_- _---,.-_ '-1- _ '.--- _....... , .... , _ i I : -r "
:--- _.... --'-_--_ ....--_--- ....._._- I.... 4--- _.... +--------i-c_--,-1-.......
I-- - .... ; - -- I ........... F °" -. .... ' " _ , l --- " ---,. - -_- - I ................ '.... _ .... : ....._----i " } - , , l'............. - -• -_ ' I ....... _ _-_ --[[....... _- .____.
.... :-,_---- ..... :,-----_ _. u--::7 .'-.-;.................. ' -I . t- 'k .... ' /
..... k_ / '. .... _4--,- 7:..... - - -' ' • _-,-......... _-...... '........ :"_ - ......... F - , _ ,_. ___ ..... _..,--_..... -I.-: - -_ --- .--P"""_-1_--b'- : _ _ ,,,_-._: __ ..,..L,_.L_I-_-", . _:_.o.._ .... I--,----'.--
_T
1
t
105
106
LABORATORY AMBIENT HUMIDITY STRIP CHARTS
107
108
TENSILE AND COMPRESSIVE STRAIN MEASUREMENT QUALIFICATIONS
109
E,-,
I--I
|
(sqI) (IV01
00
IiI_
O_
Z
00uOT---
\ J0 0 0 0
_,4 0 0 0 0
(sq[) (IVOq
"8
o"t-o
,6¢
.*
e-
UOll-a
_Jw_
111
INDIVIDUAL TENSILE AND COMPRESSIVE STRESS VS STRAIN PLOTS
CRAW DATA)
112
_ cO
i ,g,• ,i,
i,
, , i I , i i I , , . I . , , I , , , I , , ,
0 0 0 0 0 00 0 0 0 0 0
ISd 'SS._I.I.S
000
A°° 5o
oo
°i
oo
-%
0
i.e,_
o _QO
113
Z_0
O_b-q
000
0" 00
o
0 0 0 0 0 00 0 0 0 0 0
0
O0
> F.;.1ISd 'SS_IH.I.S
00
114
Io.E
U_
cO
00
ISd 'SS_I.I.S
115
_ ,...i
Z_
l:z:t • •m •m •• •• •
m •• •
I I
i I i i i ! i i , I , , , t , , , 1 , , ,
Q Q Q 0 Q0 0 0 0 00 _ _ _
ISd 'SS._I.I.S
000u3
oo
oo
°u
oo
-0
OUm i_
o _,_X-a
IIwl,-
116
0
000t.O
117
E_E_
O0r./'J o
°0°°°°
000Ln
--00
o
ooo
ooo
f
000
I18
E_
0"" i:::i
I
, i i I , , , I , , , I , , , I , , , I , , ,
0 0 0 0 0 00 0 0 0 0 0
IScl 'SS._I.I.S
00
1°
00
.0
0
1:
InEo
1-
0
gz
000
O0
_llml
GO
119
F,A"J_
_ °***°*°****
| .m.m*• •• •• •|o
, , , I , , , I , , , I , , , I , , , I , , ,
000
8
8
\
tOm,,l_
O_
0 0 0 0 0 0 0 e_0 0 0 0 0 0 _:o04 0 O0 _ _r 04 z _
ISd 'SS._I.I.S .,
120
or'2_
E-,,
l:::l
<
0
W
i,|,m •m •m •m •|,
, , , I , , , I , , , I , , , I , , , I , , ,
0 0 0 0 0 00 0 0 0 0 0O,4 0 O0 _0 "d" £N
ISd 'SS_I_I.I.S
00
- O0
8z
8
0 _T
o _,_00
w IQ
Wl--
121
OQ_
E-
0
O}
O}
0 0 0 0 0 00 0 0 0 0 0O4 0 CO _0 xl"
ISd 'SS,_I,I.S
000
mo
oo
CO
122
ISd 'SS_I.I.S
123
124
Oq =0
I
0I
%
0 0 0 0 0 00 0 0 0 0 0¢q 0 O0 _ _" ¢q
ISd 'SS_I.I.S
-0
,¢
0
I
EoRe,
O_
125
00
_°°°o°°0o
000
I
E0
RC
W--
QO
O0
0 0 0 0 0 0 0 e_0 0 0 0 0 0 uo
0 _ _ _ _ 1 _
ISd
126
m,b
q m
| •m •i •i •
| •
I I
00
, I , , * I , . , I , , * I , . , I , , I
0 0 0 0 00 0 0 0 00 _ _ _
ISd 'SS I.I.S
0
O_
0
O_m
O0
C@I_11--
127
_ aO00
=JISd 'SS_I.l.S o.CQWk-
128
000
0
000_p==,
0
01
i
ElJ
e-
129
O_ CO
E_E_
Z_
000U3
°° 5o
o
°o
oo
-0| °i0
--'r-'_ , , , I I I I I I I I I I I , , , , I , , , '
o o o o o o_A
0 _ 0
ISd 'SS_I.I.S
_5
C@
130
0 0 0 0 00 _ 00 _ _
ISd 'SS.';I_I.I.S
131
0
g
oo_ •
g
-0"_
-"'O0m I,.
w_O0
w__0
hi I-
OQ cO
J
i°| •|.| °|.
| •
m
! , , , , I , i , , I , , , , I , , , , I , , , ,
0 0 0 0 0U3 0 U3 0
IScl'SS._I.I.S
00
°° 5o
o
8o
O_
o .o
132
_Z
000
_Z
ISd 'SS._I_S_
0
0_
O0
COWJ-.
133
0_Z
_f_i •| •| .m •m •m *m •• •
! !
00
i I i , i I i , i I L , , I , , , I , , ,
0 0 0 0 00 0 0 0 00 _ _ _
ISd 'SS_t_t±S
(D _i.0
8
_,0
@@m _
o _
c@
134
_Z
• °• °
• •
! !
00o4
, I , , , I , , , { , , , { , , , { , , ,
0 0 0 0 00 0 0 0 00 _ _ _
ISd 'SS3_I±S
135
o° [¢ f
oo
8
O0m L_
o ,,,9,o.@S
um¢@
Ull..
0 0 0 0 0 00 0 0 0 0 0
0 O0 (.0 _ 0,I
ISd 'SS._EI.I.S
136
000
0
000
ua
I=oI_1i,-
E-Z
r,¢l r,_
\
• °• °• °
/
00
00
0"'. 0
°°0 0
°°°°°°0°°0
0 0 0 0 00 0 0 0 00 O0 cO _" 0,1
ISd ' SS.';I_I.I.S
0
_gw F-
137
138
_Z
_z
'\
q
i
i *i *I •I •a •n •| •. •
i
I i
00
* I * L | i ' ' ' I . , . I • . , I . i '
0 0 0 0 00 0 0 0 00 _ _ "_" 04
IScl 'SS_I_I.I.S
000 "u')
}°oo
o zo
ml
P,
00L-
o *_0O
Ull..
139
_Z
|°
|°
|°
a.
|°
|°i°
m
, , , I , , , L , , , I , , , I , , , l , , ,
0 0 0 0 0 00 0 0 0 0 0
ISd 'SS:;I_I,I.S
000t.D
&
oo '_5
r,o
UO
o ,ID_Q
wOCO
I,aJ J-,.
140
\\
x
\
00
0
0 0 0 0 0 00 0 0 0 0 0C_ 0 CO _0 _" Oq
Is
U3w3
EU
,°
000
ISd 'SS_I_I,I,S
141
0
0
O0m h.
eo
¢oI!-'
[-Z
• •• •
I I
00c'4at.==
, I , , , I , , , I 0 * , I , , i I L , ,
0 0 0 0 00 0 0 0 00 _ _ _
ISd 'SS._I.I.S
0 "00u3
-0 _ Ie_
0 E0 o
O
0
° o
000
m t_
o .oDU
_Q
142
ISd 'SS_I.I.S
00
143
_Z
144
_Z
eM
0.<
• \\
\
,-,, _..._2"
000L_O
00O_
--_
oooZ
.,<
000
_c
EQ.
EU0°°
0 0 0 0 0 00 0 0 0 0 0
ISd 'SS_[_I,I.S
0 ..o
_e
145
! !
00F.z.1
, I:, , , I , , , I * , * I , i i i I , ,
0 0 0 0 00 0 0 0 00 _ _ _
ISd 'SS_I_I.I.S
m,4,_
O0
QO
_g
146
\,
Iq
I
_" °
: :°*,° .*
0 0 0 0 00 0 0 0 00 OO _0 _ Cq
ISd 'SS t IJ.S
147
0
000u3
C_
<-
0 ie_
0 E0 o
C
C_
0
000
I : l_ J
, , , I ! I ! I , ! l I l , , I t , I I , I ,
0 0 0 0 0 00 0 0 0 0 0OW 0 CO _0 _" OW
ISd 'SS_[.I.S
00ou3
:ooi
oo
-0
OU,,m i_i_
o -_O_PX-i
CgbJ_
148
8
°_' ' ' I ' , , l , , , t , , , I , , , I , , , " --'*"
io0 0 0 0 0 0 00 0 0 0 0 0 o_
ISd 'SS._.I.S ..
149
<>
-- o o o o o o o _-,_0 0 0 0 0 0 ooO4 0 O0 _0 _" O4 X _
ISd 'SS3_I,l.ScO
150
0 0 0 0 0 00 0 0 0 0 0
T-" T'--
0
ISd 'SS,_I,I.S
151
_0X-J
>0 0 0 0 0 0
ISd 'SS_IJ.S
QQ;II-a
w_CO
I,aJI-,,
152
O0
\
\
"°
°° \-°
°°°.
".°
..
".°,
°°°
"'. o
\ -
0
%
000c_
0 0 0 0 0 00 0 0 0 0 0
ISd
153
0
cn_
O_
>
\\
i °bJ
_oW E
0i,i
000C_
154
E.-,
E_
Z \
r./"j
rQ
O_
x
0
0 0 0 0 0 00 0 0 0 0 0
ISd ' SS.';I_I.I.S
0
155
>
\
\
\
\
,\
\
\
ISd 'SS,_I,l,S
156
000 _
0000,1
O0
r._
Z0
• I
0I
_0
I0 oL_ E
o0,1 o
oo• e-
L_J
0.°o
000
0 0 0 0 0 00 0 0 0 00 O0 cO _" 0,1
ISd 'SS_t_IJ_S
157
oo
oog
,-1
O_
p.
-0
"° °
0 0 0 0 0 00 0 0 0 0 0
000Oq
ISd 'SS_I_I.I.S
0
I58
r_
r_
_Ld
0 0 0 0 0 00 0 0 0 0 0
ISd '$S,_tJ_S
159
160
%
m
_E_
L_
' i i , l , i , I l i , ' , l , I I I l I I i ' I , ' ' '
0 C) 0 0 0 00 0 0 0 0 C)
ISd 'SS._I.I.S
0
8z
0
00
O0X-a
cO
161
%
A0di
A
L
ISd 'SS_I.I.S
0 i
t-
0 e°
O0
wlcO
Ld J,-.
162
%
L_
-?
i
3!l •i •a *a •n •I •I •
I ! I
00
0 0 0 0 00 0 0 0 0
ISd 'SS._I_S
0
o _
QO
QOZ-a
163
%
164
%
o_
, , , I , , , , I , , , , l , , , ,I , , , , I , ,
165
%
n •
• •m •• •m •m •• •
I I I
00(£)
' I ' ' ' ' J I I l I I I ' , * I ' , ' , I * , , ,
0 0 0 0 00 0 0 0 0LO _" I"3 O_ ,-
0
ISd 'SS._I.I.S
166
o
or_
?"eN
_.4=P
O0to
o__3
¢0
| •| °| •| •
| °| •
I I l
(3 (3 C) O (3 (3
L_ ISd 'SS_I.I.S
, I, , , ,!,,,, I,, ,, I, , ,. I, ,, ,
(:3
ClO
16 7
%
00
.|0I.
I.
I.i*
m.n.
Ii
IlllIIli,IIiaaliIIlIIllIlilIi
0 0 0 0 00 0 0 0 0
'SS._I.I.SISd
0
_g
168
b
ii i
L.,,,I.,,,I, .,,I,,,,I,.,, I.,,,
0 0 0 0 0 00 0 0 0 0 0
ISd 'SS_I.I.S
169
0
ooO_
0 -'_'
orO
o
_u&,,
&,.
_o
_E_
p.
7
a •
| •
i •l •a •I •I •I •
Ill I li,,,,l,,i,li,,,l,,,,l,,,,
0 0 0 0 0 00 0 0 0 0 0_D u_) _I* re) 04 ,--
[Sd ' SS,_I,I.S
170
T,,0 r,-
o7
0_2
o_0_==_
O_,,I
oo
o _XX-a
COb/J--
%
| *• *I °• °• °
| ,m
[j i j i J I|ii|Jlli|| I Ji| |J II|i|i|
.CL-0 0 0 0 0 0 0 e_0 0 0 0 0 0 _q
_0
171
%E_ a3
o_T
o
172
[-.,g?
173
174
ISd 'SS_t_I,I.S
175
%
:>
ISd 'SS3_I&S
I
0
%
OU,m. kmm.
oo.
176
Z_
Z_
_Z
u_qm
Io.I
A
000
- 1,,lll,*lll*ll,l,*lll*l,ili,,l
00 0 0 0 0 00 0 0 0 0 0(,0 I13 _" it') _ ,,-"
ISd 'SS._I.I.S
?
Ic
¢
O0
CO
177
%
'I:
00 _-
_Bq_
g
| ,| •| , a|om °m .|o|o
m
,,,,l,,,,l,,,,l,,,,l,,,,l,,,i
0 0 0 0 0 00 0 0 0 0 0
ISd 'SS._I.I.S
0
178
UUm I,_¢_
_Ola.I I=-
N=..I
0
O_
_m
<Z
\
\
?. "\P.I
{
m
, , , , I , L! !__I , . , . I . , , i I i , , , I , , , I
0 0 0 0 0 00 0 0 0 0 0¢.0 If3 _" tO 04 _-
ISd 'SS._I.I.S
I
0
c
8z
o _t _,
_g
179
I-,,,4
.
0_
•.ISd'SS_I.I.S
0
180
m_gu
0_X.a
_oWl.-
00
0
1.81
182
183
\
, I , , , , I , , , , I , , , , I , , , , I , , .
0 0 0 0 00 0 0 0 0
ISd 'SS._I.I.S
184
0
8z
%D
O0m L-L--
o _-_
uO
Wh-
0 0 0 0 C) 0 0
UU
00A
l_e ro_ 0 C) 0 0 0 0 UU
_ eeull,-
-• - 185
0 0 0 0 00 0 0 0 0
ISd 'SS._I.I.S
186
8z
+;
| •| •
• °• °• °
m
I I !
00
, I , , , , [i , i , I . . , , i i i . . I i A i ,
0 0 0 0 00 0 0 0 0
ISd 'SS._I.I.S
187
0_--_
o_
0
gOi=_ i._
_3
188
_ eeIII I-.
189
.-. . 190
P
O_
0 0 0 0 0 0 0
__ o o o o o o
ISd 'SS_S
g_
191
I,=-4k \
i
illlilll l|lJll|lillilliL
0 0 0 0 0 00 0 0 0 0 0Q{:) _ _" re) C_l ,-"
ISd 'SS_I.I.S
0
O0
j:
_0
192
C) C) 0 0 0 00 C) C) 0 0 0(.0 IZ') _" I") 04 ,,--
ISd 'SS._I.I.S
193
_0
00
mq
| 0• 0a •l °• °• •
m
' I I i i I l I , I , LJ. I * , , , I I ¢ . LI , , ,_L
0 0 0 0 00 0 0 0 0
ISd
....... 0°° ............. ° .......................
0
'SS.';I I.I.S
194
O0m LL
O0
_0
I,..W
o
F.ll
+
00r,O
1o +
i +\, *T -_
\\
! : !l s• • •l • d
..2.2.1
0 0 0 0 0 00 0 0 0 0uO '_" tel C_ ,-
ISd' SS._I.I.S
00
@0l.a
w_
195
0oi
'I:
0 t
e-
J
n m
• °• °• °
• °• °n °w .
m
...°'°"
°.°.°°°
,°°°.°°
0 0 0 0 0 00 0 0 0 0 0
t13 _I" re) Cq ,,--
ISd 'SS I.I.S
0
k
196
gO
.,,x
_0
O_m_
,<
0 0 0 0 0 00 0 0 0 0 0
,< ISd SS._I.I.S
197
0
WOn .._i...
°X
,_ ISd 'SS._I.I.S
198
nq
i •m •m •• •• •• •m •w •
00
0e_
?
i
°°°,0,°0 ..... 0 ............ 0°
IIIII I i i l m I , i . i I , m , , I I I I I
0 0 0 0 00 0 0 0 0
ISd 'SS._I.I.S
199
I:
oo °I
, 0 r-.w
ool
b r r-
_-J
c0W_
0 0 0 0 00 _ 0 _ 0
o
o
F_
Z
i
0 0 0 0 0 0 0 00 _3 0 U3 0 113 0 Lr3_I" re) I"3 C_l C_I ,- --
ISd 'SS._I.I.S
201
00if3
00c_
00
00
01
"I0i0c-
OII
e-ll,..
I,,,,I
OQ
i
0 0 0 0 0 0 0 00 _ 0 _ 0 _ 0
ISd 'SS._I.I.S
00
gL'N
0 O0 L--L-
UOll.-I
202
I
ISd' SS._I.I.S
203
00
O
o
F-
0
0
ogI,.
i _,
1=..=I
.ez ,,,,l,,,,lJ,,,l,,,,l,.,,l.,.,l,,,,l,,.
0 0 0 0 0 0 0 00 _ 0 _ 0 _ 0
ISd 'SS_ttt.l.S
204
00I'0
ag
¢o
..0
0_
?I
q
i
.,,,I,,.,I,,,,I,,,,|,,.,I,,,,I,,,,I,., I
0 0 0 0 0 0 0 00 tO 0 t(_ 0 U') 0 u'_
•.ISd'SS_}I.I.S
00
00e_
205
"o0
0
0
?
0c
.o.c
W,-
L_
OO
W,W
OU
Ua
_0
i T "*'°o° °°
im
D
_BM i
q
|,|°
|°so..|°|°
m
illllllllal,lllllli
0 0 0 00 0 0 0(o u3 _" e,3
, ,, , I , , , ,
0 00 0
ISd 'SS._I.I.S
0
206
or,.)C,_,q
o• "h
%,.-
O0
_..J
s_go
wi--
I===4
O_
C_
nq
i •| •| •| •
| •| •
*,,il,,,,l,*,,l,,,,l,,,,l,,,,
0 0 0 0 0 00 0 0 0 0 0Q{) I._ _1" I_ Oq ,--
ISd ' SS.';I_I.I.S
207
Oee
8z
0
oo_-J
C_
" 0
-_ _\_j8 _
n
| °| °
| °
| °| °
u
I l I i i I I I
I
0 00 0
,,,,I,,,,I,,,,I,,,,
0 0 0 00 0 0 0_D u3 _" P'3
ISd 'SS_I.I.S
0x.,
I
0
_om h.g_
.,w
208
C_
O_
_n
;>.
N i
i •I ,i •
• •• •
i •I •
i
! ! !
00
,1,,,,I,,,,I,,,,I,,,,I,i,,
0 0 0 0 00 0 0 0 0
ISd 'SS_I.I.S
O_
e_
UUm L-I,--
o ,,_
209
v)
m
m
• o
ooc_
\
Q
O_,,,,I,,,,I,,,,I,,,,I,,,,I,,,,
0 0 0 0 0 0 •0 0 0 0 0 _o
.ISd 'SS_I.I.S
.m.
210
s_BR_0
Wh-
0O_I
¢sl
I
?
i
_5q
\
\%
\
a0
°° I
, i i i i i i , i i , , i i J i i i , J i i I i 1 1 1 1 1I
0 0 0 0 0 00 0 0 0 0 0
ISd 'SS_I.I.S
211
\
0
O0
UO
COwj..-
U_
[..,
|i
w
I ! I lilillilllllJlllll liJ|llll
0 0 0 0 0 00 0 0 0 0 0_0 uO _" M3 Oq ,---
ISd 'SS_I.I.S
212
o
0 L\
0O0
COWh-
E-wU]_Q
0°%CD
C_
>
I&l.
1(n
u I
,,,,l,,,,l,,,,l,,,,l,,,,l,i,,1
0 0 0 0 0 00 0 0 0 0 0
ISd 'SS_I.I.S
0 i
o.i
a_
0
_0
OUX-a
COW_
213
n m
qli
| •a °| •| °i tm •
, , , , I , ,, ,I ,, , , I, , ,, I, ,, , I , , , ,
0 0 0 0 0 0 •ww_
0 0 0 0 0 0 oo
ISd 'SS I.I.S
2:14Wh-
O_
Z0
oo0 I
C
0
0
..ISd 'SS._I.I.S
215
oou in
I
u
,,,,I,,,,I,,,,I,,,,I,,,,I,,,,I
0 0 0 0 0 00 0 0 0 0 0
\
0
IScI 'SS._I.I.S
O0
216
i
<>
0 oo0 i
or_o _
d
IiL,l,,,,l,,,,l,,,,i,,,,l,,i
0 0 0 0 _ 00 0 0 0 0 0
\
0
ISd 'SS_I_I.I.S
217
m.4,_OU
eo
O0.s._
[_
|.i,io o,ioi,io
i,,,I,,,,I,,,,I,,,,I,'''I'''!
0 0 0 0 0 00 0 0 0 0 0
ISd 'SS._I.I.S
218
Or]
i
00CO
_ 0 I
c 0
,._8 lo _,_,
: I
0 0 0 _ 0 0
0 0 0 0 0
ISd 'SS._I.I.S
219
O0
INDIVIDUAL CTE CURVES
220
x_
_O
_Z_ 0,,
0_
\0
¢N
221
Z
C_
l,,,l,,,l.,,l,,,l,,,l,,,l,,,l,*,l,,,l,,,l
r- CO ¢Z) _ CN 0 ¢N _ _) O0 _-• 0 0 0 0 0 0 0 0 "
I I I I
_uaaaaduo!suudx._ I_maaq&
.
_=_QU
00:Z-i
wil_O
I111...
222
223
Z.<
.<
. .
I,,,I,,,I,,,I*,,I,,,I*,.I*,.I,,,I,,,I,,, I
• -" _ CO _t" 04 C) C_l _" _) O0 ,'-• 0 o 0 o c) 0 o 0 "
I I I I
uo!Suedx_I I_Sm.toq,I,
C)U")
oI
O0m i._Im
ao=l-a
CO
224
E-%
\
0 0 0 0 0 0 C) 0
I I I I
_uoo.zOc:Tuo!su_dx_l [_maoq,L
0
I
0
L
O o,,0_,_
lad#-,
225
_Z00
_O
m
i_imw
N_
Im
l,,.l*,*l,,,li,,l,,,l,,,l,*,ii,,li,.l,,,l
• C) 0 C) 0 0 0 0 0 ,"I
I I I I
_uoo_Oduo!susdx_ psm_oq.I."
_g
0tO
O
O0m t.t_O0
•,,,, AOU
_Jull..
226
lllll,*,l,,,I,,,l*,,I.,*l*,,l,*,l,,,I,,,I
• 0 0 0 0 0 0 0 0 ,"I
I I I I
0
0
0
_,uao.taduo.lsuudx.w [era zaq,I,
227
.
li,,l,.,l,.,l,,,l,,,l,,.l.,.l,,,l,,.l.,,l
','- CO (.0 _t" _ 0 0,1 '_" (.0 CO ",-• 0 0 0 0 0 0 0 0 "
• • • • • • • • J
t I I I
_,uaaaaduo!suudx_l IUmaaqJ_
228
_m
00
_0
mm
m
R_i_lig
NZ
II
m
l*lilt,illi,l,,,l,,,l,.,l,,,l,,.l,,.l.,.l
_" O0 tO _ _ 0 _ _" tO aO _"" 0 0 0 0 0 0 0 0 "
• • • • • • • • J
I J J I
0
- 0
_uaoaacluo!su_dx_ I_maaq_L
OU
uOCO16/1'--
229
.<
OqP4
O0
I
I
I
0t..")tN
o
l'',l,,,l,,,l,,,l,,,l,,,l*,,l,,,l,,,l,i,l
"- OO _ _ _ 0 _ _ _ (1:) "_-• 0 0 0 0 0 0 0 0 I"
I I I I
_,uao;[aduo!su_cIx_l [_ux_eq_L
ot_
0
UUt.O0
UU
_OCO
nil i..
230
0u')
I
Inp.l,,il.,.l,,,l,,,l,,,l,,,l.,,l,,,l.,,l _P
0 0 0 0 0 0 ,-:." " " " I" I" I" I I :i-'°_
GOWb.-
231
li,illi.l..*l...l...l...l...l...l...l...l
uo!suudx_[ [_sm.I_qj_
ou
j=.
232
_z
_ o_oo
-- o_
o0
233
Z
0
0
CO0 0 0 0 0 0 0 0
I I I i
_.uoo.loduo!suedx_ TemZoq&
00t_
0
O,d
I
0
0
UUm L_
o o
UU
nil--
234
Z
O_
0.,_I0
0C#]
I11llml _2U lll_
II
l,,,l,,,l,,,l,,,l,,,l,,,l,,*l,,,l,,ilL, ii|
•- CO qO '_" (N 0 Cxl _ (D O0 ,-• 0 0 0 0 0 0 0 0 ,"
II I I I
lueoaOduo!su_dx._ I_U1_OqJ_
0- 0
0
0
°uO
e ••o,,.o
235
Z0k-,,I
Z
X
C_
::>,
I,,,I,,,I,,,I,,,i,,,I,,,I,,,IJ,,i,,.I,:l[
" 0 0 0 0 0 0 0 0 "
I I I I
%uoo_odUOTSU_dX_l I_m_oq,L
Q0a
I
00
0t_
m.,
uoLo o
,e_AlUo
_JcoWl,-,
236
k,,,,,4
Z
i
It!I .,-'- llm
iiili L-! IiU mill
I II I
I,,,I,1,1,,,I,,,I,,,I,,,I,,,I,,,I,,,I,,,I
•" iX:} _O _1" C_I 0 OW _1" {O O0 "-• 0 0 0 0 0 0 0 0 "
• • • • iP • • " I
I I I I
uo!su_dx] I_m_eq&
0- 0
0t,l")
d
0
om,,lOuo
m _
o_O0
IIi
237
I===I
Z
I
i..l m2U m/_..
I
I
1
I l*..l...l.,.l...l...l,,.l...l...l.,,li,il
•-- CO (_ _I" C_ 0 C_ _" tO (I_ ,--• 0 0 0 0 0 0 0 0 "
# • • • • • J •
I I I I
_u_oa_duo!suudx_ I_m.x_q,L
00if3
o
0U3
o IIu,WW#
ooI,.
238
Ill
iP"
I
Jlli_lllJtliJlllJallJlilJill|lllJlllJlil|
• C) 0 0 0 0 0 0 0 "• • • • • • • • J
J J I I
_uoO_Oduo_su_dx_l [_m_oq_L
239
!
0
° i
N i_t,,
WW_
oo3-J
a_ o"'-_q_ W J-,,.
I
I,,=.N
Z
1
l,,il:iilli,li,,l,,*l**,l*,,l.,.l.,*l*,*l
•- CO _ _i" ('_ 0 OW "_" CO (I_ ,"• 0 0 0 0 0 0 0 0 ,"
II I I I
_uoo_Oduo!su.udx_ I_Ui_oq&
O- O
r_
C:)_')
o .or..D.C.,)uu
O0,w,QUU
ull..
240
241
ICOZ_O
Z
0
_r
II
u
l,*ll,*,l*,,l,,.l,,,l,*,i,,,i,,*l,,.l.,,l
•- CO tO _ e4 0 _ _ _ _ "-• 0 0 0 0 0 0 0 0 ,"
I
I I I I
"_uea.TOduo!su_dx_I I_mJeqJ_
0- 0
0u3¢N
0
0
UUN L
gO.,_.QUU
_O
242
E-w
lllllllllllllllilllllllllllllllllllllllll
" 0 O 0 0 0 0 0 0 ,"I
I I I I
_,uao.Ia duoIsu_dx_ I_maoq£
i,e)
o4
t'N
,,,-- -Wuu
m inilliO
uI_e
WI-
243
E_
cO
0
Z
I',,I,,,I,,,I,,,I,,,I,,,I,,,I,*,l,lllllll
•- II_ _ _ (Xl 0 CXl _ _0 GO ,-
" 0 0 0 0 0 0 0 0 I"I I I I
_,uoo_Oduo!su_dx_I [_m:[oq_
0- 0
_0
0U_CN
0
O0m in,L-
244
E_
Z_0
Z
_I IIk
o
I
0- 0
• _1
{"4
4
m
r_ _ _r o
I
r__ 1 , , , i , , , ! o , , i, , , i , , , i , , , I , , , i , , , i , , , i , , i i 0 00 0 0 0 0 0 _
" " " I" I" I" I I u=
_,uaa_aduo!sa_dx._ I_m_aq& =*
245
["4
Z,--i0
Z
o_
O_
O_
0
E_i llq
iml__
IJl_l
I
Im
lii,lililtillililii,liliili,lii,ill,lilll
• 0 0 0 0 0 0 0 0 ,"!
I I I I
_,uoOZOduo!suadx_l. Iamzoq,l,
00
0
(N
o<. LN
0
,.,. ,_I.
o_
cOb.J J.n.
246
¢0
0
Z
X"
0
_Wi_a limw
N_
l,l,,,l,,,l,,,l,,,l,,,l,,,i,,ilJi,l,lil,,,l
• 0 0 0 0 0 0 0 0 ,"I
I I I I
_lua0aa du0!su_dx_ iemaaql
ml
0
I
0- 0
r'3
0U3C_
0tO
o _0
Ov
gOCO
w j--
247
l,,,l,.,l,,,l,t,l,,,l,,,l,,,l,,,l,,,l,,,l
• 0 0 0 0 0 0 0 0 I"I I I I
_,uao_aduo!suedx_I [em_aq.l.
248
O0
I=-IO0Z
0-0
O_ 0
o
O
I
249
Z
X
_Lo
r.)
0
a,
/
0
I
\
10
_0--' U")
4I
t
!
I°
250
Cf_
l,==i
Z
X
_o[,..
0
l,.*l.,,l,.,l..*|lill,*,]l..i,,,l,.,|t*,|
"- 00 tO _ eW 0 OW _ tO (D "-• 0 0 0 0 0 0 0 0 "
• • • • • • • • J
I I I I
uoIsuedx_l IUm.taq&• 251
m
0t5I
00r,')
(:3
(N
. (_I
¢I"- l,w
_ 0I$)
°{1o,.,,,i._.L-
Wl=-
N.=.I
Z.,<
X
.,<
\
I ,,, I, , , I ,, , I, , ,.I ,, ,I , . , I ,, , I . , , I , ,, I .., I
1'- O0 (Z) _t" O4 C) OW _I" tO GO ,-• C) C) 0 0 C) 0 0 0 "
• • • • • • • • J
I I I I
luooaoduoIsu_)dx_Il_)maoqJ_
00rO
0
CN
° _iou
A
co
252
E_
Z
C_
0
----mm
Imz
J
Illl|lll|lll[iLl|lll|llllilillllllll|ill|
,-- CO _0 _@ C_ 0 C_ _1" _ O0 ,--• 0 0 0 0 0 0 0 0 ,"
!I I I I
_uooaOduo!suudx._ [_m_oq_L
0- 0
_3
0- _3
_o
o
oO
OuL_00
UU
cg
253
(-,
E_
Z.<
b-
O<_J
,<
/
i_lil
IIII ]E
Io .
0- 0
0
C_
I,I[l**,l,, Lll,llll, I Jill[, Ill,ll*,,lllll I_O
0 O 0 O O 0 I ooX-'• " " I" I" I"
_uoo_ed _uo!s_dxN [_m.teq,L --""I_II-
254
0UO
° ._
Z
Z'-
0
0
b-
iN
_2
I
l,,,l.,.l.,,l,,.l,,,l,,,l,,,l,,,l,,.l,,,l
I- O0 r.O '_" ¢_1 ¢:) _ _" CZ) O0• 0 0 0 0 0 0 0 0 "
I I I J
+uoo+Oduo.tsuedx_i [uuuoq_
0- 0
0
¢N
CN
d
.oue)
o IDO0
gv
O0I!-'
wQ_g
255
Z
X
[_.r.v.1
¢:::1r,.v.lr.l.1
>
/
m
k'Ifi_lmw
MZ
U_
II
i I
l,,,l,,,li,,l,,,l,,,ll,,l,,,l,,,X'''l'i°l
• 0 0 0 0 0 0 0 0 I"i I I I
_uaoaacIuo!suudx._ I_UZaaq.l.
256
0- 0
No
I
0
Cq
oup
00
_Z
E;-'.-line
iill_
UIN,
I
Im
Iiil|lll|lllllJlililllil|lllilllJlll|lil_
" 0 0 C} 0 0 0 0 0 "
i I I I
uo!su_dx._ IerU_oqj_
0
o,.,
0uO
0
OQ
J_
257
E_
oimli I
Z_
_Z
?>=
ii_ lain
IIIIZ
f.31_
I
I,,,I,ii1,,,I,,,1,,,1_,*1.*,i**,1,**1,*,1
•--- (I) tO _1" C_l 0 C_ _" _0 (I_ ,--• 0 0 0 0 0 0 0 0 "
• • * * • * • * J
I I I I
UOTsu_dx_[ IUm.x_q&
0
0,I
0
0
oo
c:owj=-
258
),=..i
Jail|illilialill|illJlllJfll|lllilll|illJ
" C) 0 0 0 0 0 0 0 ,"• • • • • • • • I
I I I I
_u_oaeduo!suedx._ [_ma_qj_
259 "-
_m
mZ
iM
_z
u_
I
Im
l,,tl,,ilo,.l.,,l,,,l,i,l*,,li,,l,,,l'''l
' 0 0 0 0 0 0 0 0 I"I I I I
uo!suudx_ I_m.teqJ.
.o
0ff'j
0
O0+B _..
i,l,
COW_
260
E_
E_
\0
o_
Rr
',- GO (,0 _ _ (3 t'q '_" tO (10 "-• 0 0 0 (3 0 0 0 0 "
I I I I
_uao.xa duo!suudx_ [uu_._aq,L
0tD
°a..a_
_0_j-..
261
E_
r,-)
I.==I
_r--.. Img
NZ
i
l.,,l,,,l,,,l,,il,ltlli,l,lil,,,l,,,l,,,l
'-" _ (_D _t" CW 0 C_ '_" {0 (D "-" 0 0 0 0 0 0 0 0 "
I I I i
_,uoo.xodUOTsuudx_ IUm_oq.l.
C)L(3c_
0t(3
0
--,, ,WW_o
QuZ_
wo
h_ F=
262
E_
lug
ZE-
I.==I
m
R!i_l IIII
llllZ
Ul-
I
Ii
o,
Iii,I,,*I,,,I.,,I.,,I,,,Io,oi..,I.,.I.,,I
"" CO tO 'd" Cq 0 Cq "d" ¢D OO _-• 0 0 0 0 0 0 0 0 "
I I I I
%uooaeduo!suudx_ IUmaoq.l.
I
_Oor,3
0tO
i_0
tO
0
uu
C0
263
E_
E_
I=,=1
IiiIIIiiIiiiIiillllllllllll|lllllllllllll
•- CO r.O _" _ 0 O4 _" (D (10 --• 0 0 0 0 O 0 0 0 "
I I I I
"_uaa.Xaduo!Suudx.w IUm_[aq_
0
OU
{=@141I,-
264
TE_m F75 23725
75 62999
77 05870
78 66055
7_ 92139
81 06791
82 90484
85 03087
87 38_92
88 99679
90 05207
92 56172
94 54221
96.75505
99 51207101 57870
103 99350
106 17892
108 07525
IIi 40851
i15 36325
116 98627
i18 76972
120 72380
122 39142
124 51843
126 24479
128 77674
151 02814
135 12041
139 56579
142 22705
145 24009
148 30793
150 56558
153.51824
156.87649159.13743161.05842164.88626
167.61416
17_.04035
173.13263
175.40803
177.03006
179.59752
180.99413
181.57857
183.78898
185.12290
186.22910
189.48664
190.53278
193.66988
195.18265
198.55241
199.71800
202.91286
204.94639207.62837
209.31901
ExP %
-2 12592e-4
-5 69572e-4
-8 39294e-4
-1 08387e-5
-1 17515e-5
-I 25551e-3
-i 28218e-5
-i 23501e-3
- _L 17551e-5
-1 i0199e-5
-i 04018e-5
-9 50097e-4
-9 20494e-4
-8 86550e-4
-8 65934e-4
-8 95007e-4
-7 84719e-4
-6 61303e-4
-6 13729e-4
-5 17776e-4
-4 32130e-4
-2 34887e-4
-1 10767e-4
-5 05699e-53 55790e- 5
1 20922e-4
2 57867e-4
4. 57023e-4
9. 11164e-4
1. 48952e- 3
2. 39770e-3
5. 15652e-3
4. 19466e-3
5.13090e-3
5. 82680e-3
6. 75055e-3
7.81351e-38. 63665e-39. 63853e-3i. I095 le-2
i. 22101e-2
I. 36802e-2
I. 46436e-2
I. 60266e-2
i. 65709e-2
I. 81442e-2
i. 88544e-2
1. 92478e-2
2 03383e-2
2 08449e-2
2 14283e-2
2 30386e-2
2 35203e-2
2 49145e-2
2 56754e-2
2 71837e-2
2 78433e-2
2 92502e-2
3.01628e-2
3. 17232e-2
3. 27001e-2
265
?1_ 5530022! _:7_D_223 3378822_ 88090227 #838 !231 91560236 5123723'9 35150
_.)41 377S0
243 _8460
247 [6269
249 99228
252 75853
235, 52346
26O 58373
3
i
3
3
3
4
4
4
4
4
4
4
4
4
4
4
4
-__-'=4e- Z
:o,:__oe- 2
_773_e-2
_62_ie-2
11_93e-2
16255e-2
32348e-2
4<_826e-2
5c;574e-2
65'_01e-2
74_35e-2
82214e-2
98273e-2
92041e-2
95301e-2
97885e-2
CTE_ I
266
:-E-2._E-2_;=_5
76 59875 1
78 43432
79 69562
81 87326
84 34148
86 34943
88 98951
31 17060
94 72949
96 33656
99 95278
102 53597
106 43925
108 33356
111 37631
114 87809
117 86315
20 56190
23 43344
26 01809
28 66064
31 01621
133 14226
135 09600
137 73914
139 57823
142 27971
144 29126
147 22171
149 98102
151 93564
154 17688
156 70631
160 15516
162 45402
165 90316
169 29531
172.34172
173.54929
175.90649
177.86103
179.75793
181.02297
182.40292
184.18483
186 42702
188 38142
189 64620
191 14120
192 98048
194 82008
198 49812
200 33863
202 12058
204.13220
206.02920
208.09912
210.05424
212.29592
214.71052
87930e-4
-2 17146e-4
-7 23377e-4
-i 24236e-3
-i 90055e-3
-2 24239e-3
-2 51860e-5
-2 33i50e-3
-2 25598e-3
-2 28147e-3
-2 23127e-3
-2 13034e-3
-2 05486e-3
-i 99182e-3
-i 76442e-3
-I 58768e-3
-I 46149e-3
-I 09488e-3
-5 25861e-4
8 i1549e-5
8 65295e-4
1 64946e-3
2 45897e-3
3 23053e-3
4 21711e-3
5 03930e-3
6 35482e-3
7 26556e-3
8 36597e-3
9 83332e-3
1 09085e-2
1.18572e-2
1.32233e-2
1.49563e-2
1.59809e-2
1.78150e-2
1.97884e-2
2.12937e-2
2.20653e-2
2.34188e-2
2.44688e-2
2.54301e-2
2.62271e-2
2.70620e-2
2.79601e-2
2.92377e-2
3.02370e-2
3.09454e-2
3.18688e-2
3.27543e-2
3.37536e-2
3.53473e-2
3.66630e-2
3.75737e-2
3.85098e-2
3.95091e-2
4.07614e-2
4.20138e-2
4.31143e-2
4.44678e-2
267
225 22887
_27 58462Oo=_9 30892
252 29670
234 95951
237 6396[
240 22444
243 72706
247 05723
250 21448
-L_ZLe-2
4 92i!=e-2
5 03749e-2
5 i1972e-2
5 22722e-2
5 31449e-2
5 39797e-2
5 46499e-2
5 51177e-2
5 54969e-2
5 56230e-2
C?E D-
268
CTE-3,
TEMP,F
75 00352
79 59861
82 47222
85 34442
88 27059
_i 82479
97 04227
lOl 91476
107 47015
Iii 87553
114 84819
121 30621
124 38535
126 88630
130.92469
132 96740
136 03519
138 93491
141 60854
143 93645
147 73987
149 54797
152 78596
156 41386
157 59991
160 44160
163 05542
165 95231
169 41356
173 27288
175 87287
177 57341
179 724O3
181 25367
183.28929
184 93429
187 64927
189 12159
190 92792
193 08137
194 26530
195 11486
197.21277
198.50886
199.18255
201.28259
202.80443
204.67481
207.66471
210.33160
211.68075
212.47122
213.99660
215.52341
217.16273
218.06252
220.38830
221.i1542
LE-2986
EXm,%
[ 58643e-4
-I 66951e-4
-4 30735e-4
-6 43751e-4
-7 29791e-4
-7 39075e-4
-7 72149e-4
-7 67476e-4
-5 84455e-4-2 75614e-4
i 91609e-5
7 23434e-4
1 31023e-3
2 07417e-3
3 20767e-3
3 95847e-3
4 95142e-3
5 80459e-3
6 54331e-3
7 34516e-3
8 68151e-3
9 62248e-3
I 06790e-2
1 21421e-2
i 27779e-2
1.36564e-2
1.44839e-2
1.54386e-2
1.67111e-2
1.80983e-2
1.94208e-2
2.01078e-2
2.10999e-2
2.17487e-2
2.27533e-2
2.33768e-2
2.46867e-2
2.53355e-2
2.63399e-2
2.72304e-2
2.79423e-2
2.83112e-2
2.91382e-2
2.99391e-2
3.04474e-2
3.11983e-2
3.21263e-2
3.28896e-2
3.46187e-2
3.55985e-2
3.65518e-2
3.69841e-2
3.77851e-2
3.85355e-2
3.93620e-2
3.99848e-2
4.08628e-2
4.15108e-2
269
227 28_%_
_8 3_200
22 Q 15530
230 23345
230 91140
231 36608
,=32 15690
232 77753
234 08497
235 442_4
236 23346
236 68212
237 24790
238 38337
238 83132
239 73750
240 41544
241 77757
242 74371
244 39544
244 90178
245 52488
246 26122
247 51418
249 17265
d.
4
4
4
4
4
4
4
4
4
4
4
4
4
44
5
5
5
5
5
5
5
5
5
5
373_e-Z
427Z,%e-2
47_70e-Z
50978e-2
54923e-2
58483e-2
59884e-2
64080e-2
67640e-.2
71587e-2
78073e-2
82269e-2
85827e-2
88498e-2
92444e-2
96256e-2
00199e-2
03759e-2
08722e-2
i1651e-2
15474e-2
18906e-2
21578e-2
24758e-2
27689e-2
29101e-2
ErE -3
270
7_{-4, L5-2<
TEMP, F
76 45988 -
77 32131
78:8415
7g 27369
80 07514
90 70421
81 21711
81 84334
82 63677
83 48545
84 72612
85 62864
86 52927
88 62003
92 93191
94 92067
96 67942
99 74780
102 02747
106 07346
108 75173
111 48810
I13 83153
117 31833
119 83462
124 12571
126 41483
128 93772
132 02782
134 26782
137 08116
139 20923
140 93917
142 66770
144 39670
145 60761
[46 82230
146 99515
148 49935
150 52399
152.49148
154.69936
156.61302
158.99659
159.86793
161.84581
163.82323
165 10687
166 44246
167 37142
167 72468
169 18354
169 59205
171 44715
172 89231
174 93867
176 84949
178 48639
180.51859
[80.92899
_7
Ex_, %
7.82326e-5
3 42333e-5
i 84833e-4
2 8407le-4
3 20397e-4
3 31_88e-4
2 92392e-4
2 274_4e-4
4 7_454e-5
-i 83098e-4
-6 30841e-4
-9 50694e-4
-i 32139e-3
-i 96174e-3
-2 81051e-3
-3 12011e-3
-3 46732e-3
-3 94462e-3
-4 i1503e-3
-4 42928e-3
-4 63873e-3
-4 82289e-3
-4 81548e-3
-4 79793e-3
-4 75277e-3
-4 62263e-3
-4 53881e-3
-4 31569e-3
-4 20826e-3
-3 90822e-3
-3 55863e-3
-3 19478e-3
-2 77917e-3
-2 40170e-3
-2 01152e-3
-1.72187e-3
-1.33053e-3
-1.29278e-3
-8.00394e-4
-1.43917e-4
5.12687e-4
1.48656@-3
2.23227e-3
3.32016e-3
3.69957e-3
4.63583e-3
5.55938e-3
6.26838e-3
6.83742e-3
7.22941e-3
7.50829e-3
8.31859e-3
8.54650e-3
9.25421e-3
9.69588e-3
1.09370e-2
1.16065e-2
1.25944e-2
1.34542e-2
1.37330e-2
271
CTE -/
_T _ Z -_t _
:3_ i)iE5
;88 87452
i89 86347
l_O 92844
192 57255
£95 81884
l_7 57145
_9q 21165
20! 42000
202 82313
205 39135
:£07 $4445
210 74741_13 19190
2i5 18395
:216 75946
218 04924
219 73667
221 19364
222 76536
225 15460
227 42293
229 12312
230 86958
234 00879
236 85424
238 54593
240 81095
242.61362
244.47013
246.49430
248.58506
249.68782
251.82156
L
1
2
2
2
2
2
2
2
2
3
3
3
3
3
3
3
3
3
3
4
4
4
4
4
4
4
4
4
4
4
4
5_t_e-_
i :_3;52e-2
88_14e-2
Q8578e-2
06348e-2
22549e-2
32806e-2
43575e-2
5344[e-2
61926e-2
7656le-2
86736e-2
02809e-2
14703e-2
27879e-2
36615e-2
45358e-2
53456e-2
61050e-2
68769e-2
81174e-2
91801e-2
05331e-2
i1936e-2
26250e-2
38370e-2
47612e-2
57349e-2
65699e-2
73157e-2
79595e-2
88574e-2
93125e-2
98289e-2
272
84879O94
g799
104
L 09
].13
116
120
122
126
129
133
135
137
138
142144
147
150
152
156
158
161
165167
171
174
176
180
183
VE _545_
74 8Q420
76 24284
78 55412
_0 75747
82 55879
_8627
47103
_4584
06081
19050
41539
79096
32397
51001
03619
05372
86683
.03462
44036
38034
2413132917
73966
21261
01410
49478
11633
43716
03791
65339
61363
1003853741
48126
26691
93304
O651O
31392
_E-Ls,fi8
-4 57567e-6
-4 77005e-4
-1 07657e-3
-1 93221e-3
-2 63534e-3
-3 36288e-3
-4 18074e-3
-4 99874e-3
-5 75498e-3
-e 25806e-3
-_ 73507e-3
-6 94346e-3
-7 14680e-3
-6.96748e-3
-6 86345e-3
-6 73002e-3
-6 54945e-3
-6 40403e-3
-6 00572e-3
-5 40499e-3
-4 37420e-3
-3 73167e-3
-3 14044e-3
-2 31919e-3
-i 49026e-3
-8 98339e-4
i 08191e-4
1 i1680e-3
1 79628e-3
2 92939e-3
3 79846e-3
4 69207e-35 83815e-3
6 55540e-3
7 67500e-3
8 50559e-3
9 22229e-3
1 01154e-2
1 I0591e-2
187.42353
190.49942
1.93.56923
197.62322
201.15510
203.47537
205.50706
209.03397
212.16548
215.80804
218.17951
222.85855
225.80222
228.79985
232.42309
235.82274
240.35465
243.21895
248.31477
252.32899
253.98776
1 20387e-2
1.29574e-2
1.37366e-2
1.47544e-2
1.56213e-2
1.62881e-2
1.69048e-2
1.76575e-2
1.85380e-2
1.93158e-2
1.98429e-2
2.07450e-2
2.12580e-2
2.16948e-2
2.20286e-2
2.24898e-2
2.26437e-2
2.26495e-2
2.25990e-2
2.27035e-2
2.26487e-2
273
:TE-_. _E-2_8 _TE_P, :
73 96524
75 93778
74 19209
74 43880
75 55958
75 _0169
76 78162
77 31653
78 72947
80 29709
8_ 58645
83 55942
84 85463
86 32672
87 85739
90 18765
91 89054
93 37432
95 60204
97 71319
99 71129
101.77613
105 15605
108 02166
iii 47067
113 77157
i15 49958
118 43194
121 76614
124 12561
127 91905
131 94329
134 76317
140 07137
142 84436
146 31558
150 07849
152.22996
155.30225
159.71065
163.09159
165.52951
168.50101
173.20929
177.28027
180.30509
183.27602
187.40907
190.04374
193.63561
195.84682
198.17226
201.37397
205.08006
209.94420
212.96494
216.91000
220.56103
223.86294
227.44312
[_, %
-7 53597e-5
-e 7125[e-4
-[ 38439e-3
-2 26291e-3
-3 29637e-3
-4 16247e-3
-5 00450e-3
-5 85834e-3
-6 54556e-3
-7 21486e-3
-7 89259e-3
-8 68664e-3
-9 23715e-3
-9 68636e-3
-i 01102e-2
-1 06253e-2
-i i0497e-2
-i 12445e-2
-1 14921e-2
-i 17776e-2
-i 20247e-2
-i 20683e-2
-i 22300e-2
-I 23394e-2
-i 22468e-2
-I 21511e-2
-i 20285e-2
-I 19345e-2
-I 18416e-2
-i 17206e-2
-I 16289e-2
-i 15124e-2
-I 13672e-2
-I 07961e-2
-i 04218e-2
-9 84579e-3
-9 16876e-3
-8.57652e-3
-7.93583e-3
-6.95518e-3
-5.84457e-3
-5.26581e-3-4.31951e-3
-3.05975e-3
-1.92553e-3
-I.06843e-3
-1.34858e-4
i.i0097e-3
2.21356e-3
2.91649e-3
3.55946e-3
4.18942e-3
5.14783e-3
5.83772e-3
6.74083e-3
7.50888e-3
8.40170e-3
9.14264e-3
9.78272e-3
1.02312e-2
274
lZ__ .5i_C9
2a_._7_70
250. _9q2_
253, 1_302
.. LZ L'_e-Z:. Z 2"3 Se- 2
i. '. 4 5_'7e- 2
i . 15SaLe-2
i. i5_8_e-2
i. _.a605e- 2
2_
75 9457776 33637
76 19690
77 55095
77 95598
78 39040
?_ 51334
80 23430
_2 20097
83 32163
195 1958g
87 50279
'_0.21442
g2 o2027
95 4838099 14826
102 41606
106 03318
109 82042
113 84257
116 82811
118 79754
121 86382
123 89956
125 81861
127 45465
128 32114
130 42397
i32 81740
134 80808
137 55387
140 13411
i42 88067
144 81262
147 20908
149 43923
151 26587
154 35721
156 92302
158 23402
162 49763
164.38376
167.06704
171.03549
173.65928
176.75061
179.97154
183.99493
187.07640
191 08992
194 16987
196 68303
199 13518
201 17472
205 71680
208 69902
210 57149
213 59498215 74591
219 85259
222 11566
__--c,=<
E*= %
0 'SZ m..... =9e-4
-i 87898e-4
-6 04391e-4
-i 16588e-3
-i 59630e-3
-2 19225e-3
-2 55031e-5
-2 93213e-3
-3 53347e-3
-3 g2943e-3
-4 16394e-3
-4 33615e-3
-4 44820e-3
-4 4o671e-5
-4 36694e-3
-4 33018e-3
-4 22874e-3
-4 02753e-3
-3 85223e-3
-3 57671e-3
-3 41103e-3
-3 01406e-3
-2 45694e-3
-1 90858e-3
-i 39768e-3
-8 35184@-4
-6.99439e-4
I 29510e-5
8 00069e-4
1 55079e-3
2 48822e-3
3 52738e-3
4 47744e-3
5 20312e-3
6 04077e-3
6 96751e-3
7 84522e-3
8 81926e-3
9 61837e-3
1.04853e-2
1.19225e-2
1.28379e-2
1.36871e-2
1.49738e-2
1.57853e-2
I 67594e-2
1 79857e-2
1 92342e-2
2 00440e-2
2 11283e-2
2 19129e-2
2 27880e-2
2 36002e-2
2 42117e-2
2 55215e-2
2.65844e-2
2.72724e-2
2.80698e-2
2.86303e-22.93605e-2
2.98827e-2
276
_7 _ _ -: -_
"_30 4747 _
242 61142
'245 93338
24_ 93883
7:52 _o40
_. :Q4]-3e-2
3. i L_--e-Z
:. _ -Z-_2e- 2
3. _$635e-2
3. I_538e-2
3. 20045e-2
3. 2002 le-2
3.1c_49e-2
c-T ?
277
_E_P, r75:9928175 1897775 5188976 221687_ 7707678 009267_ B5353
_0 20m37
80 20781
82 13835
83 67361
85 38148
87 89037
93 66854
96 53312
99 28611
103 24899
104 92041
108 31278
ii0 09736
116 25160
119 36394
121.90628
125 26429
127 59286
131 19443
133 75298
136 83775
140 27978
142 09311
144 83264
146 82173
149 79647
152 12452
154 35300
156 52045
159.62351
162.20559
164.78976
167.25135
170.75493
172.34037
174.21106
176.84057
178.18924
180.82240
185.43159
187.66320
190.42051
193 10477
195 49698
197 48032
199 57890
2O2 73149
204 07597
2O7 39857
209 32140
213 15348
215 71465
217 51752
220 47763
-1.82028e-4
-6 [5940@-4
-1 34381e-3
-2 0337[e-3
-2 63421e-3
-3 21033e-3
-3 60720e-3
-4 I1972e-3
-4 1579_e-3
-4 e4595e-3
-4 98017e-3
-5 30191e-3
-5 67600e-3
-6 06823Q-3
-6 16224@-3
-6 17952e-3
-6 07122e-3
-5 88261e-3
-5 69683e-3
-5 54667e-3
-5 16131e-3
-4 80922e-3
-4 36689e-3
-3 61972e-3
-2 79432e-3
-I 70310e-3
-8 65324e-4
2 13984e-4
1 61164e-3
2 46340e-3
3 51776e-3
4 45854e-3
5 65285e-3
6 46550e-3
7 64827e-3
8 74185e-3
I 02676e-2
1.16794e-2
1.31423e-2
1.44140e-2
1.59136e-2
1.68040e-2
1.76557e-2
1.88250e-2
1.95372e-2
2.07959e-2
2.26764@-2
2.39357e-2
2.54238e-2
2.65293e-2
2.75077e-2
2.83081e-2
2.91212e-2
3.04555e-2
3.10656e-2
3.23487e-2
3.30727e-2
3.41891m-2
3.50906e-2
3.56873e-2
3.65244e-2
278
255
225._4Z}_
250.2_Z5:
2IS 24112
255 55140
237 91694
241 89603_4,: 5 23155
248 61660
03160
,/.£-efSe-Z
I _4424e-2
i c:'_9_e_ 2
4 937Vge_ /
4 0705oe-2
4 12094e-2
4 14080e-2
4 14152e-2
4. 3569e-2
279
CTE-9.
TEMO. F
70 88257
71 34881
72 I0568
72 g1556
74 58_31
76 48465
78 15289
80 05073
81.832
83 55927
85 97735
88 05329
89 55448
91 34632
92 96758
94 53384
96 3902397.7299
99.24064
100.8119
102 2691
103 3207
104 6648
107 1166
108 8095
ii0 8570
112 4399
114 1448
116 1954
118 9054
120 9705
124 2199
125 9409
128 0741
130 2709
132 5418
135.2662
136.8237
139.3973
142.8004
146.1975
149.3315
150.6574
151.9408
153.8025
154.9634
157 O011
158 3371
159 3233
161 5342
164 1987
164 9348
166.9964
169.4653
171.8241
174.1128
LE-2mq7
u_COrr.
0.000169
-0.00058
-0.00172
-0.00228
-0.00258
-0.00256-0.00254
-0 00246
-0 00219
-0 00236
-0 00259
-0 00320
-0 00389
-0 00495
-0 00626
-0 00789
-0 00984
-0 01192
-0 01381
-0 01607
-0 01847
-0 02049
-0 O2314
-0 02762
-0 03071
-0 03500
-0 03872
-0 O4333
-0 04801
-0.05603
-0.06254
-0.O7329
-0.07993
-0.08777
-0.09638
-0.10707
-0.12417
-0.13195
-0.14454
-0.16017
-0.17504
-0.19302
-0.20062
-0.21012
-0.21999
-0.22854
-0.23885
-0.24772
-0.25602
-0.26639
-0.27594
-0.28171
-0.28777
-0.29441
-O.30168
-0.30736
EXm, %0.000048
-0 00016
-0 00049
-0 00065
-0 00073
-0 00073
-0 00072
-0 00070
-0 00062
-0 00067
-0 00073
-0 00091
-000110
-0 00141
-0 00178
-0 00224
-0 00280
-0 00339
-0 00393
-0 00458
-0 00526
-0 00583
-0 00659
-0.00786
-0 00874
-0 00997
-0 01103
-0 01234
-0 01367
-0 01596
-0 01781
-0 02087
-O.02277
-0.02500
-0.02745
-0.03049
-0.03537
-0.03758
-0.04117
-0.04562
-0.04986
-0.05498
-0.05714
-0.05985
-0.06266
-0.06510
-0.06803
-0.07056
-0.07292
-0.07588
-0.07860
-0.08024
-0.08197
-0.08386
-0.08593
-0.08755
280
Z87
_89
[92
_94
Z96
_,gg
2O3
2O6
212
216
2[g
224
228
233
238
242
246
249
250
._Z.742: 3--_e -209'--- __DSo "'_5_ . _'748 _ 7_- - -,,.0928_
3619 -0 32_59 -0.09388
2972 -0 32975 -0.09393
8172 -0 32833 -0.09352
3548 -0 32635 -0.09296
8282 -0 32181 -0.0916707!0 -0 31721 -0.09036
8169 -0 31077 -0.08852
7165 -0 30643 -0.08728
6L61 -0 30209 -0.08605
7092 -0 2Q589 -0.08428
8844 -0 29003 -0.08261
0855 -0 28295 -0.08060
6862 -0 27548 -0.07847
3415 -0 26763 -0.07623
1143 -0.2601 -0.07409
3654 -0.25207 -0.07180
5100 -0.24511 -0.06982
4005 -0.23963 -0.06826
9366 -0.23746 -0.06764
281
CTE- i0, L
TEMD , F
72. 86256
74,4704
75.3291
76.01656
77 73313
79 85302
$2 65911
84 95107
88 85045
90 8582693.6748
97.2388
99.13537
100.6319
101.8406
103.1114
104.9080
107.518
109 5558
Iii 5979
i13 9362
115 7516
117 9195
119 9724
122 2712
_25 0412
127 9458
130 1363
132 2197
134 1302
136 3348
139 0924
143 2084
146 3281
149 6736
152 0612
154 7984
156 9397
158 7822
161 7494
163 9294
165.7502
167.9790
169.8519
171.4885
173.8151
176.4826
178.6204
182.1344
184.6085
87.1963
189.4378
192.0185
194.9938
197.5649
201.0447
203.6074
206.9668
E-2qq8
unc©rr.
0 000602
0 000934
0 001514
0 001o01
0 003187
0 004349
0 006089
0 007317
0 008939
0 009656
0 009808
0 009966
0 010110
0 009869
0 009689
0 008810
0 006665
0 003257
-0.00060
-0.00509
-0.01092
-0.01592
-0.02206
-0.02821
-0.03677
-0.04704
-0.06029
-0.06987
-0.08065
-0 09138
-0 10311
-0 12024
-0 14283
-0 16257
-0 18166
-0 19499
-0 20901
-0 21985
-0 22899
-0.243
-0.25099
-0.25682
-0.26347
-0.26848
-0.27253
-0.27658
-0.27998
-0.28155
-0.28254
-0.28277
-0.28281
-0.28267
-0.28163
-0.27938
-O.27688
-0.27265
-0.26888
-0.26383
EXP, %
0 000172
0 000266
0 000432
0 000542
0 000909
0 00L241
0 001737
0 002088
0 002551
0 002755
0 002799
0 002844
0 002885
0.002816
0.002765
0.002514
0.001902
0.000929
-0.00017
-0.00145
-0.00311
-0.00454
-0.00629
-0.00805
-0.01049
-0 01342
-0 01720
-0 01994
-0 02301
-0 02607
-0 02942
-0 03431
-0 04076
-0 04639
-0 05184
-0 05564
-0.05964
-0.06274
-0.06535
-0.06934
-0.07162
-0.07329
-0.07519
-0.07662
-0.07777
-O.O7893
-0.07990
-0.08035
-0.08063
-0.08069
-0.08071
-0.08067
-0.08037
-0.07973
-0.07901
-0.07781
-0.07673
-0.07529
282
2_= Zs_i -3
2]e 7530 -0
22! 5405 -0
_4 [564 -0
22_ 6029 -0
229 6764 -0
232 8708 -0
23_ 8681 -0
239 [504 -0
244 0618 -0
247 2041 -0
250 1164 -0
252 4605 -0
24_4 -0
24_13 -0
24153 -0
23712 -0
23316 -0
22837 -0
22446 -0
22023 -0
21754 -0
21242 -0
20934 -0
20626 -0
20421 -0
07124
0702406892
06767
06654
06517
06405
06285
0620806062
05974
05886
05827
C7 E-/e
283
CTE-ZI.
TEMP. F
74 94769
78 73716
_5 2177_
88 9056[
95 50£44
96 94689
9_ 63869
[02 2676
104 8900
108 6429
111 5945
114 9355
118 0989
121 4191
125 5221
127 7036
129 8886
131 9625
134 7701
136 6717
138 5187
141 2692
142 0595
143 2573
144 9697
147.2522
150.1640
153 2405
156 9420
160 8066
165 1279
168 4272
171 8437
175 7780
178 1164
181 2589
184.5778
188.3007
192:3754
196.1652
206.1058
209.2170
212.4469
215.2785
218 4585
221 4640
224 3003
227 6002
230 7824
236 3332
239.6265
242.4559
245.2850
249.8379
252.1424
252.4296
LE-2999
uncorr.
0.000058
-0.00028
-0.00025
-0.00003
0.000059
-0 00015
-0 00175
-0 00443
-0 00844
-0 01612
-0 02324
-0 03289
-0 04361
-0 05744-0 07558
-0 08737
-0 09847
-0 10881
-0 12175
-0 13208
-0 14185
-0 15472
-0 15751
-0 15923
-0.1614
-0.16445
-0.16802
-0.17311
-0.17959
-0.18791
-0.19681
-0.20329
-0.20933
-0.21518
-0.21856
-0.22193
-0.22449
-O.22667
-0.22739
-0.22767
-0.22704
-0.22516
-0.22252
-0.21912
-0.21497
-0.21125
-0.2069
-0.20173
-0.19713
-0.18982
-0.18598
-0.18302
-0.18012
-0.17712
-0.17574
-0.17574
ExP. %
0.000016
-0.00008
-0.00007
-0.00001
0.000016
-0 00004
-0 00050
-0 00126
-0 00240
-0 00459
-0 00662-0 00937
-0 01243
-0.01637
-0.02154
-0.02491
-0.02807
-0.03102
-0.03471
-0.03765
-0.04044
-0.04411
-0.04490
-0.04539
-0.04601
-0.04688
-0.04790
-0.04935
-0.05120
-0.05357
-0.05611
-0.05795
-0.05968
-0.06134
-0.06231
-0.06327
-0.06400
-0.06462
-0.06482
-0.06490
-0.06472
-0.06419
-0.06344
-0.06247
-0.06128
-0.06022
-0.05898
-0.05751
-0.05620
-0.05411
-0.05302
-0.05217
-0.05135
-0.05049
-0.05010
-0.05010 284
CTE-12.
TEMP, F
7O.59307
71.74858
73.30268
75.0097
77 27948
80 51359
85 90814
87 01905
91 45765
96 20536
101.2534
105.0655
108.5764
112.6191
116.0064
118.3024
121.1240
123.606
125.9835
128 4275
130 8215
154 4O55
137 1236
140 6257
144 4422
147 6354
149.9797
151.8590
154.5267
157.3938
150.2722
162.899
164.3147
168.5013
171.0221
174.1641
176.0159
178.0946
180;3540
182.6618
185.2011
187.7261
189.9382
192.3280
195.7576
198.1681
201.4437
203.9437
207.1281
210.1848
213.7506
217.1931
219.9400
223.9855
228.0205
232.2727
236.6981
240.7158
LE-3000
umcorr.
-0.00030
-0,00079
-0.00095
0 000524
0 003052
0 006633
0 011252
0 015549
0 021071
0 026408
0 032002
0 035358
0 037311
0 038262
0 038630
0 038918
0 038516
0 037665
0 035925
0 033423
0 030287
0 O23743
0 017503
0 008166
-0.00344
-0.01583
-0.02449
-0.03271
-0 04440
-0 05838
-0 O7331
-0 08640
-0 09431
-0 11778
-0 13164
-0 14942
-0.16018
-0.17068
-0.18187
-0.19231
-0.20286
-0.21221
-0.21941
-0.22705
-0.23512
-0.23965
-0.24443
-0.2468
-0.24872
-0.24956
-0.2497
-0.24914
-0.24808
-0.24504
-0.24111
-0.2361
-0.23115
-0.22576
EXP, %
-0.00008
-0.00022
-0.00027
0 000149
0 000863
0 001889
0 003204
0 004428
0 006000
0 007520
0 009113
0 010069
0 010625
0 010896
0 011001
0 011083
0 010968
0 010726
0 010230
0 009518
0.008625
0.006761
0.004984
0.002325
-0.00098
-0.00450
-0.00697
-0.00931
-0.01264
-0.01662
-0.02087
-0.02460
-0.02685
-0.03354
-0.03748
-0.04255
-0.04561
-0.04860
-0.05179
-0.05476
-0.05777
-0.06043
-0.06248
-0.06465
-0.06695
-0.06824
-0.06960
-0.07028
-0.07082
-0.07106
-0.07110
-0.07094
-0.07064
-0.06978
-0.06866
-0.06723
-0.06582
-0.06429
285
- 0. :3_0 l
..
286
CTE-i3.
TEMP, F
71 45834
73 45278
75 95199
78 32725
80 75688
83 18481
85 38618
88 94249
92 78951
95.2789
99.07529
103.3285
107 3612
II0 6620
114 1947
116 6470
119 2151
119 3860
119 4430
119 3853
119 6136
12i 8403
123 4995
126 2554
128 5571
131 3279
132 9493
135 6191
1381714
140 9723
143.8903
146.8776
149.8649
152.1063
154.5183
157.1808
160.2637
162.3896
164.8718
166.8215
169.6025
171.9692
174 3910
178 0445
181 1065
183 6285
187 3812
190 8844
194 6047
197 8536
200,4488
202 9234
205.2782
207.7990
210.5994
214.2554
217.8500
221.7295
LE-3001
u_corr.
-0.00163
-0.00111
0 001061
0 005077
0 009600
0 014442
0 018964
0 026226
0 032473
0 036489
0 041528
0 046507
0 0500230 051692
0 052664
0.052931
0 052882
0 052946
0 052946
0 053073
0 053074
0 052832
0 052015
0 048853
0 045244
0 039287
0 034849
0 026413
0 018612
0 007001
-0.00518
-0.01965
-0.03411
-0.04783
-0.06141
-0.07918
-0.1009
-0.I1435
-0.13041
-0.14292
-0.16152
-0.17733
-0.19275
-0.21446
-0.23223
-0.24505
-0.26396
-0.27888
-0.29169-0.30171
-0.30684
-0.31077
-0.31361
-0.31551
-0.31632
-0.31706
-0.31698
-0.31683
EXP, %
-0.00046
-0.00031
0 000302
0 001448
0 002738
0 004119
0 005410
0 007481
0 009263
0 010409
0 011846
0 013266
0 014269
0 014746
0 015025
0 015099
0 015085
0 015103
0 015103
0 015140
0 015140
0 015071
0 014838
0 013936
0 012906
0.011207
0.009941
0.007534
0.005309
0.001997
-0.00147
-0.00560
-0.00973
-0.01364
-0.01751
-0.02258
-0.02878
-0.03262
-0.03720
-0.04077
-0.04607
-0.05058
-0.05498
-0.06117
-0.06624
-0.06990
-0.07529
-0.07955
-0.08320
-0.08606
-0.08753
-0.08865
-0.08946
-0.09000
-0.09023-0.09044
-0.09042-0.09038
287
2Z<}.ZZSZ
2So._C521
243.0912
248.8773
251.6581
-3.3LLO _
-0.50609
-0.2991:_
-0.29275
-0.28986
-}.08873
-0.08751
-0.08554
-0.08350
-0.08268
288
CTE-14. L
TEMP, F
71.88793
77.3321
85.06849
97.96245
106.6159
114 2952
llq 5104
124 7830
127 7631
134 4126
136 4192
139 4579
142 3248
145 0201
147 3139
150 1814
154 0244
157 1221
161 7112
168 0216
173.1856
177 4883180 9872
183 2248
186 2073
190 1646
194 3509
199 3965
203 0656
208.7979
211.8356
216.4205
220.6042
224.5012
228.8563
235.3884
240.4308245.0146
249_1400
252.4059
253.4371
E-3002
uncorr.
0 049923
0 052082
0 055467
0 061373
0 063888
0 065682
0 065961
0 065734
0 065585
0 055299
0 050377
0 041546
0 031559
0.019474
0.010211
-0.00411
-0.02625
-0.04716
-0.07668
-0.12089
-0.16314
-0.19389
-0.21502
-0.2321
-0.2491
-0.26914
-0.28745
-0.30374
-0.31242-0.3209
-0.32271
-0 32366
-0 32352
-0 32302
-0 31992
-0 31118
-0 30447-0.29731
-0.29125
-0.28532
-0.28286
EXP, %
0 014221
0 014836
0 015800
0 017482
0 018199
0 018710
0 018789
0 018725
0 018682
0 015752
0 014350
0 011834
0 008989
0 005547
0 002908
-0.00117
-0.00747
-0.01343
-0.02184
-0.03443
-0.04647
-0.05523
-0.06125
-0.06611
-0.07095
-0.07666
-0.08188
-0.08652
-0.08899
-0.09141
-0.09192
-0.09219
-0.09215
-0.09201
-0.09113
-0.08864
-0.08673
-0.08469
-0.08296
-0.08127
-0.08057
289
CTE-15. LTEMP. F
75.2311978.[57_580.62441
82.3437
85.08916
87.4793990.2595
92.87018
g6.21342
99.38724
101.9396
105 2323
108 4764
112 0695
115 4956
i18 1818
121 6160
123 9071
126.4870
129.0188
130.5821
132.8944
135.1610
137.147
139.1305
138.4889
141.4751
144.7640
148.5415
153.4544
157.3874
161.3912
166.0991
169.5474
173.7024
177.7470
181.9154
184.90741881949
191.2957
194.7290
198.5614
201.4932
205.3318
208.3473
211.8662
216.6299
221.2694
224.1323
226.5316
230.4592
234.8378
239.1576
243.3653
248.2637
251.2263
252.6486
E-3003
uncorr.
-0.00072
-0.00133-0.00188
-0.00199
-0.00146
0 000588
0 004[02
0 007297
0 012085
0 016554
0 019876
0 023775
0 026531
0 028592
0 030017
0 030802
0 O31148
0 031167
0 030872
0.029370
0.027162
0.024390
0.020093
0.015033
0.010290
0.011808
0.003266
-0.00743
-0.02212
-0.04302
-0.06310
-0.08496
-0.11659
-0.14074
-0.16742
-0.19468
-0.22314
-0.23999
-0.25805
-0.27414
-0.28877
-0.30315
-0.31207
-0.31972
-0.32458
-0.32785
-0.32908
-0.32904
-0.32889
-0.32804
-0.32477
-0.32055
-0.31613
-0.31203
-0.30837
-0.30626
-0.30497
EXP. %
-0.00020
-0.00037
-0.00053
-0.00056
-0.00041
0 000167
0 001167
0 002076
0 003438
0 004710
0 005655
0 006764
0 007549
0 008135
0 008541
0 008764
0 008862
0 008868
0 008784
0 008357
0 007728
0.006939
0.005717
0.004277
0.002928
0.003359
0.000929
-0.00211
-0.00629
-0.01224
-0.01795
-0.02417
-0.03317
-0.04004
-0.04763
-0.O5539
-0.06349
-0.06828
-0.07342
-0.07800
-0.08216
-0.08625
-0.08879
-0.09097
-0.09235
-0.09328
-0.09363
-0.09362
-0.09358
-0.09333
-0.09240
-0.09120
-0.08995
-0.08878
-0.08774
-0.08714
-0.08677
290
_'g,
73 80358
76 70360
7m 26240
82 2L903
87 50705
93 !3618
_8 65160
ZOO 81236
1,O3 0 _ '_98_
105 01984
110 70589
115 53871
119 51889
[24 35176
129 07077
136 23478
139 36188
142 31848
145 67313
148 91408
151 30218
155 96497
158 01192
161 99219
163 75479
166 37033
169 27018
172 62509
175 86625
179 50534
182 51893
186 10107
188 48919
191 33216
194 06140
197 87090
200 94127
204 80753
208 90140
212 42659
215 89491
218 56720
222 43343
225.10565
228.97175
231.58717
233.86131
236.24927
238.35300
240.51363
242.56039
244.55033
246.48331
248.41626
250.17867
252.22558
252.96468
_ E - : ? 0
E,'<P,6
8
i
2
4
6
8
8
l
i
1
1
1
i
2
2
2
2
2
2
2
3
%
70277e-_
00849e-4
55886e-3
69574e-3
46434e-3
41337e-3
30827e-3
g579ge-3
82418e-3
0600Le-2
24950e-2
.45161e-2
,59057e-2
.78546e-2
.99478e-2
.28531e-2
.41704e-2
.53433e-2
66065e-2
78156e-2
86638e-2
99272e-206491e-2
3 19304e-2
3 26162e-2
3 35365e-2
3.45471e-2
3.54857e-2
3.64242e-2
3.76153e-2
3.86439e-2
3.99252e-2
4.07554e-2
4.17660e-2
4.27585e-2
4.42202e-2
4.53571e-2
4.69631e-2
4.84429e-2
4.98144e-2
5.11859e-2
5.22686e-2
5.39107e-2
5.50836e-2
5.68880e-2
5.79707e-2
5.90714e-2
6.01000e-2
6.09301e-2
6.17422e-2
6.26985e-2
6.35827e-2
6.45751e-2
6.56036e-2
6.65238e-2
6.72818e-2
6.76427e-2
291
:rZ-21. _Z-:},;=
7© 22649
71 54635
72 29209
74 07002
75 73292
77 28i16
7Q 05847
80 43466
82 52701
83 87457
85 19303
86 51188
,38 0600889 60798
90 98584
93 79305
97 17716
99 46935
102 50772
104 80097
107 66719
109 33014
iii 68070
114 14605
115 63627
117.52817
120.22288
122.57329
125.15305
126.87301
129.16646
132.43471
136.73510
138.59766
141.37911
143.73001
146.48221
148.54645
150.72525
152.21600
155.25529
157.03288
159.21207
162
165
167
169
172
175
177
179
181
183
186
190
195
196
199
202
204
206
.36610
.00375
.29739
.41908
.34357
.49693
.27428
.91130
57400
81020
33314
11763
21364
48184
52059
50175
50802
51419
%
203_60e-4
3 11649e-4
4 73568e-4
9 95509e-4
1 60757e-3
2 16562e-3
2 92179e-3
3 42584e-3
4 09!89e-3
4 90218e-3
5 53237e-3
6 01843e-3
6 59449e-3
7 27867e-3
7 90884e-3
9 13314e-3
i 00149e-2
1 14015e-2
1 27879e-2
1 37781e-2
1 51465e-2
1 57406e-2
1 67668e-2
1 77930e-2
i 85853e-2
1 94135e-2
2.05298e-2
2 161018-2
2 27804e-2
2 35186e-2
2 44367e-2
2 57149e-2
2 73712e-2
2 81093e-2
2 93156e-2
3 02157e-2
3 12959e-2
3 20700e-2
3 29341e-2
3.35282e-2
3.45723e-2
3.52203e-2
3.59403e-2
3.70024e-2
3.79925e-2
3.88386e-2
3.95946e-2
4.06387e-2
4.19530e-2
4.26911e-2
4.39155e-2
4.45996e-2
4.54638e-2
4.64179e-2
4.78220e-2
4.91183e-2
5.04145e-2
5.16568e-2
5.29711e-2
5.39614e-2
5.498788-2
292
218
_'aO
223
226
229
231
234
236
238
241
244247
o50
251
546e4
03691
78862
82655
29127
21480
33537
08680
32217
95924
13726
06088
27042
13650
74161
c
-q
5
6
6
6
6
6
6
6
7
7
;_250e-2
02_3e-2
1559_e-2
31082e-2
43686e-2
57731e-2
69435e-2
83120e-2
94824e-2
06887e-2
18412e-2
7 32096e-2
7 49743e-2
7.63967e-2
7.71530e-2
C?q -2-t
293
84879093_598
i00102104107III115118121124127129132136139[42146151155160163167170173176178181
7EMC, = EX=,
71.7088q
73 59745
75 82639
77 70438
80 31577
82 30074
05230
40300
06576
24205
56824
11979
16206
48613
92225
35922
04438
06654
62992
06773
86283
24039
.96044
.73652
30752
25674
14741
39916
89275
57918
34360
46344
49786
38937
56227
79289
88821
44104
%
-1.28_92e-
-3 48101e-
2 03261e-
7 46905e-
1 77814e-
2 64617e-
3 69391e-
4 96060e-
6 24408e-
7 _1853e-3
8.59523e-3
9.73444e-3
1.06025e-2
I 16693e-2
1 28443e-2
1 39833e-2
1 56468e-2
I 75991e-2
i 95686e-2
2.06716e-2
2 25334e-2
2 37624e-2
2 50460e-2
2 63837e-2
2 80290e-2
2 93130e-2
3 06509e-2
3.25856e-2
3 53150e-2
3 69245e-2
3 89861e-2
4 03245e-2
4 17545e-2
4 30564e-2
4 45749e-2
4 60755e-2
4 71239e-2
4.82090e-2
183.81902
186.76656
189.71282
192.31914
195.60536
199.00701
201.49747
205.34901
208.29400
211.35105
215.25693
219.21333
221.35791
223.73716
225.94623
227.92993
230.31087
231.43982
233.99476
236.54463
239.03466
241.35451
243.67689
4
5
4
4
3
3
3
3
3
4.94200e-2
5.07760e-2
5.21861e-2
5.34334e-2
5.50062e-2
5.65431e-2
5.78443e-2
5.97423e-2
6.12064e-2
6.27788e-2
6.48029e-2
6.71153e-2
6.85059e-2
6.96628e-2
7.07474e-2
7.16695e-2
7.27543e-2
7.34768e-2
7.44719e-2
7.56831e-2
7.70023e-2
7.82492e-2
7.93880e-2
294
i
295
204
207
209
212
215
218
222
225
229
231
235
237
240
243
245
248
[-E-23. _£-SOi_
73 03_23 -
75 16658
77 53054
7_ 61208
82 g666786 20935
98 _3300
_2 _8709
'_5 88499
99 76731
103 59471
106 14783
lOg 22247
113 16550
116 76290
120 94585
124 65846
128 31409
130 69172
133 58921
136 71876
140 37232
[43.73229
148.01802
150.10453
152.59446
155.42835
159.42587
163.01541
165.96574
169.05459
172.16622
175.05998
177.67008
181.09117
183.87304
188.68278
192.68237
198.48066
16251
87057
90630
69397
71536
2143904800
71026
08470
52966
13162
57326
.07146
.03380
.94039
.26310
250.59078
251.98317
, %
[.34_i8e-5
i 452_5e-4
11854e-4
i 27849e-3
2 39583e-3
3 64036e-3
4 77716e-3
6 36456e-3
7 5_167e-3
9 i9756e-3
i 09123e-2
i 21220e-2
I 35483e-2
l 52991e-2
1 69963e-2
1 92000e-2
2 09150e-2
2 26483e-2
2 37133e-2
2 49223e-2
2 62396e-2
2 78822e-2
2 92353e-2
3 09129e-2
3 17972e-2
3 27531e-2
3 36902e-2
3 53140e-2
3.66666e-2
3 76760e-2
3 88483e-2
4 02563e-2
4 13021e-2
4 24935e-2
4 40097e-2
4 51827e-2
4 71856e-2
4 89000e-2
5.14631e-2
5.39538e-2
5.54694e-2
5.66439e-2
5.80707e-2
5.96784e-2
6.10333e-2
6.30201e-2
6.50436e-2
6.70314e-2
6.85315e-2
7.04281e-2
7.17831e-2
7.31017e-2
7.46370e-2
7.62450e-2
7.74189e-2
7.88104e-2
7,94603e-2
296
88
_396
iOl104107109ill112I15I17i19121123126129133137
140
143
145
147
150
153
156
158
160
163
166
169
172
174
176
178
181
184
186
188
190
193
195
197
199
203
207
75 93400
77 30@07
@0 27335
@3 [770Q
84 e4iQ5
00836
02545
86496
53245
19863
75215
5g147
31333
24173
22799
87364
42497
52171
10513
82655
86543
69995
76417
79324
.53869
65815
89245
13788
63309
87002
25389
15195
70284
91836
47494
31688
89443
11038
32372
37003
35891
14300
49783
20047
24590
97125
35686
28876
79009
94775
46918
05153
_E-3¢_Z
-9._0500e-5
1 67048e-4
9
1
2
4
5
6
7
g
i
I
1
i
i
1
1
1
1
2
2
2
2
2
2
3
3
3
3
51030e-4
98811e-3
62487e-3
06023e-3
24224e-3
47816e-3
78_0oe-3
14823e-3
04197e-2
17460e-2
31807e-2
41795e-2
51604e-2
59778e-2
73398e-2
85018e-2
95180e-2
09707e-2
21507e-2
36760e-2
52018e-2
71999e-2
90527e-2
06690e-2
22856e-2
30298e-2
43374e-2
2
2
2
2
2
2
3.58454e-
3.70080e-
3.82802e-
3.96603e-
4.06597e-
4.18046e-
4.30224e-24.46940@-2
4.56754e-2
4.67653e-2
4.76378e-2
4.85101e-2
4.97459e-2
5.11276e-2
5.19632e-2
5.28719e-2
5.41619e-2
5.52521e-2
5.61063e-2
5.71606e-2
5.81780e-2
5.97952e-2
6.12678e-2
209.60679
211.36816
213.18477
216.53131
220.10666
222.94468
226.01196
229.69255
233.04127
6.24670e-2
6.32484e-2
6.41205e-2
6.58458e-2
6.76078e-2
6.89884e-2
7.03876e-2
7.254788-2
7.41827e-2
297
3Z,_fi_7_
2,_7249
251
== i:z
24 _.85
50580
82481
76020
7.8_ai3e-Z
8.04117e-2
8.1_i09e-2
8.30808e-2
8.37903@-2
298
72 95165
73 81170
75 76149
77 08004
78 39808
80 28822
81 83407
83 55206
84 92653
87 04498
88 47629
90 42252
91 79639
93 17043
94 42959
95 80355
97 69259
I00 09519
102 44120
i03 92774
i05 70157
107 47556
108 96278
ilO 44992
112 45282
114 51172
116 62925
11886013
120 46206
123.03647
125 21041
128 30033
130 98928
133 27768
137 22596
139 40092
143 O6268
145 98096
148.72785
150.44458
153.30491
154.45004
156.28147
158.22778
160.97561
162.97877
165.72651
167.78719
171.67938
175.28549
177.80364
182.32504
186.50189
189.59214
191.30912
193.48400
196.00224
197.77640
202.12582
204.18523
206.53183
Ex_,
-1.80547e-4
-L 26382e-4
-7 22!88e-5
5 41641e-5
2 88875e-4
8 30516e-4
1 40826e-3
I _67¢6e-3
2 40127e-3
3 17762e-3
3 71926e-3
4 53173e-3
5 09142e-3
5 61501e-3
6.17470e-3
6.71635e-3
7.49270e-5
8.82875e-3
i 00023e-2
i 09953e-2
1 18799e-2
1 27285e-2
i 35771e-2
1 44437e-2
1 54006e-2
i 66464e-2
1.76213e-2
1 88852e-2
1 97337e-2
2 i1240e-2
2 22975e-2
2 38322e-2
2 52585e-2
2 64862e-2
2 84361e-2
2 93930e-2
3.12888e-2
3.27331e-2
3.40331e-2
3.48636e-2
3.64343e-2
3.68496e-2
3.76801e-2
3.84745e-2
3.95759e-2
4.04786e-2
4.15980e-2
4.24646e-2
4.41437e-2
4.56784e-2
4.68339e-2
4.88740e-2
5.10045e-2
5.24669e-2
5.32433e-2
5.42182e-2
5.53557e-2
5.61681e-2
5.81903e-2
5.93277e-2
6.03749e-2
299
. ,
-'5 -4]_7
_ , 5174_
...... J_061
222 66678
225 35632
229 _0475
231 76491
274¢, 05372
_37 25792
_79 26125
240 97780
243 66649
n46 12721
248 12969
_.50 99027
252 59246
'D
t,
6
6
6
6
7
7
7
7
LL_4Z_--
ltSL'e-2
_,95Sae-Z
5i}_]cPe-2
5_899e-Z
7524_e-2
86620e-2
9961ge-2
15688e-2
3i937e-2
4313ie-2
59380e-2
7 68047e-2
7 76713e-2
7 91518e-2
8 03253e-2
8 13725e-2
8 28891e-2
8 36835e-2
g-l<
300
-E-Z= _E 55 4
-E_s, F
YL 5S867
74 16953
76 39706
77 99536
80 2L96L
82 27219
94 60455
8_ 59751
90 4663693 02892
'95 59017
98 03719
I00 71114
103 78324
106 28659
109 18792
LI2 26002
115 21877
117 85659
120 73855
123 12944
126 37146
128 87440
132 6288O
136 95281
140 53948
143 15882
145 94831
149 02434
152 49809
155 80105
159 15948
163 94524
167 75945
170 77695
174 82074
178 40850
181 88204185 07250
187 91682
190 82010
194 00752
197 93577
201 52309
205 10845
208 69228
212 10509
215 00662
216 94126
219 78535
222 97255
225.70132
228.77125
253.26450236.27720
258.78057
243.33303
246.46213
249.47876
252.43795
-4 L6472e-5
5 03820e-4
6 49176e-4
9 76191e-4
I 59363e-3
2 21101e-3
3 35451e-3
4 17140e-3
6 02281e-3
7 05755e-3
8 20113e-3
9 32653e-3
1 06152e-2
1 21036e-2
i 33197e-2
i 47173e-2
i 62057e-2
i 76035e-2
1 88014e-2
2 01808e-2
2 11974e-2
2 28309e-2
2 40652e-2
2 59166e-2
2 79858e-2
2 95106e-2
3 05816e-2
5 17797e-2
3 29416e-2
3 43394e-2
3 56646e-2
5 71349e-2
5 90411e-2
4 05115e-2
4 17822e-2
4 53616e-2
4 47957e-2
4 62117e-2
4 73917e-2
4 87712e-2
5.00237e-2
5.14396e-2
5.31096e-2
5.45800e-2
5.62137e-2
5.79743e-2
5.96805e-2
6.10781e-2
6.19857e-2
6.54014e-2
6.48354e-2
6.63237e-2
6.79934e-2
7.02623e-2
7.19320e-2
7.31300e-2
7.52355e-2
7.67421e-2
7.80853e-2
7.94467e-2
301
"7
,-33
86
90
90
9395
99
102
I05108
110
115
118
122
128
130
154
137145
147
150
154
156
160
162
166
170
174
177
180
184
187
192
196
199
204
208
211
214
218220
223
226
229
232
236
239
242
245
249
252
253
,- .
71 7024_
73 i4130
74 46459
77 11625
7g 47905
81 55_29
2_50!
47453
18026
40733
0L288
7882954445
03341
16032
40034
77184
92224
47015
05992
18976
85076
66151
54872
60392
64435
81932
59690
70858
11367
94280
86403
66999
41743
12823
64642
22400
68847
30922
52780
76172
15540
37572
32754
62694
33199
82356
89458
55820
39779
.46750
52101
18289
48054
71838
12870
42766
18264
_£-/'g15
-i.05397e-6
3 56378e-4
6 59873e-4
1 50218e-3
2 21870e-3
3 08096e-3
5 89001e-3
5 25562e-3
7 10831e-3
7 03517e-3
8 33021e-3
9 55229e-3
1 ii151e-2
1 23200e-2
1 38849e-2
1 53952e-2
1 64737e-2
1 89192e-2
2 01963e-2
2 19770e-2
2 47089e-2
2 59314e-2
2 73854e-2
2 84985e-2
3 05066e-2
3 19962e-2
3 31808e-2
3 44546e-2
3 54247e-2
3 66629e-2
3 77399e-2
3 90307e-2
4 02857e-2
4 14866e-2
4 24011e-2
4 35846e-2
4 48584e-2
4 61869e-2
4 80185e-2
4 97790e-2
5.10359e-2
5.29407e-2
5.47736e-2
5.61942e-2
5.77948e-2
5.96113e-2
6.09248e-2
6.25442e-2
6.38753e-2
6.53868e-2
6.69519e-2
6.89845e-2
7.02431e-2
7.17713e-2
7.31910e-2
7.46464e-2
7.62288e-2
7.66971e-2 302
85
89
96
LO[
105
L[O
116
121
[28
133
L38
142
146
L51
155
160
165
169
174
178
182
187
192
196
203
209
216
223
227
232
239
245
252
,:TE-Z__. _E-SC
TEM_. F E
74 61248
78 8L£31
80 81079
L4807
83700
62800
17098
48590
08538
98358
55500
25559
31905
16196
08853
82765
34246
62887
61483
ig537
55433
31462
32499
62165
08747
18405
92522
27409
78393
51604
41902
38911
46145
27191
56564
14223
-i.0!371e-4
-5 59_60e-5
6 91396e-4
2 54937e-3
4 06378e-3
3 93356e-3
4 03406e-3
4 02532e-3
4 1803_e-3
4 46715e-3
4 51291e-3
4 67290e-3
4 62954e-3
4 07826e-3
5 30751e-3
2 15794e-3
6 99801e-4
-8 49456e-4
-2 88651e-3
-4 77946e-3
-7 12598e-3
-9 39912e-3
-I 15651e-2
-1 36580e-2
-1 55694e-2
-I 73706e-2
-I 86289e-2
-i 97206e-2
-2 01958e-2
-2.02536e-2
-2.02205e-2
-2.02481e-2
-2.07626e-2
-2.19258e-2
-2.31445e-2
-2.41088e-2
303
CTE-2'S. LE-IO!7
TEMP F EXD
74 26685 -
78 55273
83 10283
87 g4777
'92 08583
g8 39246
105 44056
llO 07438
lit [0104
121 84600 7
128 65106 7
132 94799 7
139 93809 7
144 70243 7
151 27493 6
155 78526 5
160 71331 3
166 93796 1
173 40496 -i
178 52015 -3
185 43724 -5
189 44086 -7
196 14664 -8
202 70530 -9
211 59328 -9
218 12635 -9
222 80918 -8
229 69771 -7
234 02081 -6
240 92387 -5
245.38510 -5
252.26060 -5
, %
1.43999e-5
i 21606e-3
2 71855e-3
4 _I063e-3
6 i0298e-3
6 03831e-3
6 06611e-3
6 2S357e-3
6 87263e-3
18107e-3
57007e-3
60512e-3
65080e-3
45229e-3
42794e-3
27734e-3
89380e-3
47375e-3
289298-3
17057e-3
71465e-3
00264e-3
51529e-3
17763e-2
30556e-2
29790e-3
86295e-3
65875e-3
80873e-2
98475e-3
74986e-3
70464e-3
304
87
_2959_
i05i12ii9123130138144149156160165170173178182187191195203210216223232239246251
TZMP, F
70 58284 1
74 72582 1
79 56231 2
83 65188 4
97290 6
21621 6
57193 6
15365 6
22935 5
95056 5
55892 5
05074 5
75988 5
65018 4
16814 2
64926 9
29297 -7
05592 -3
58221 -5
O5082 -7
08931 -1
86866 -1
96515 -i
40075 -1
_5-f313
ExP. %
231!2e-4
13334e-3
81171e-3
49032e-3
43981e-3
85455e--3
85380e-3
22074e-3
_0527e-3
40441e-3
54680e-3
41826e-3
03742e-3
29459e-3
82902e-3
30256e-4
69220e-4
57126e-3
68616e-3
83717e-3
07651e-2
28797e-2
57174e-2
76693e-2
09810
79621
92445
89879
03997
86976
87224
30688
19391
02796
88841
-2 O0011e-2
-2.22063e-2-2.36347e-2
-2.56423e-2
-2.67462e-2
-2.79948e-2
-2.91892e-2
-3.10886e-2
-3.23734e-2
-3.29175e-2
-3.29374e-2
4--
305
TEM_, F
Z2 75LC'i
77 56862
81 92627
88 O0311
90 _8466
96 72131
_03 834_
_iO 37514
1,16 80017
121 61878
128 10137
134 87080
141 92730
149 27224
156 04447
162 81807
167 06600
173 03620
176 88294
181 93507
187 38903
193.70322
200.53318
206.21423
212.52554
221 18834
227 84292
234 61250
241 15256
245 85677
251 13612
251 59800
LE-I:L:Ex_. %
-9 13475e-
9 i8873e-
2 68806e-
5 84789e-
7 05744e-
7 21820e-
7 25205e-
7 15961e-
7 35629e-
7 _2575e-
7 67787e-
7 72990e-
7 61923e-
6 31602e-
4 290316-
1 23476e-
-7 359286-
-3 61054e-
-5 87019e-
-8 618046-
-i 15466e-
-I 425886-
-i 655556-
-I 77136e-
-i 82757e-
-i 836896-
5
4
3
3
3
3
3
3
3
3
33
3
3
3
3
4
33
3
2
2
2
2
2
2
-1 822656-2
-1.828286-2
-1.830306-2
-1.828656-2
-1.935416-2
-2.15404e-2
306
909499
[05[12120130137144151157167174
180
186
193
2OO
210
219
225
232
239
245
25O
CTE-32. _E-IO2
TEMP, : EX
74 88294
79 02058
85 51978
12353
37193
£2_24
55369
43988
81838
05714
45917
68333
32917
97295
07678
34388
52301
93361
46214
62600
14949
15921
53612
14243
20611
74824
56816
P. %
-2 2_846e-4
6 73826e- 4
2 89392e-3
4 84460e- 3
5 14740e-3
4 32655e-3
3 95653e-3
3 98444e-3
4 06489e-3
4 07185e-3
4 00857e-3
3 09418e-3
1 51029e-3
-3 81522e-4
-3 38122e-3
-6 45115e-3
-9 17562e-3
-i 16105e-2
-i 35746e-2
-i 49237e-2
-i 52431e-2
-i 51634e-2
-i 40662e-2
-I 29874e-2
-I 21627e-2
-i 20981e-2
-I 21402e-2
307
£TE-33.
TEMP, F
72 48621
77 13782
83 74196
88 22128
92 47090
96 89280
103 43951
ii0 27335
116 53292
121 18453
[27 96094
133 07197
140 19295
144 55742
151 62098
158 16768
165 00153
171 89280
178 09494
183 20597
189 35068
196 06967
203 30551
209 62251
214 67611
221.10796
227.71209
234.85507
241.15007
245.74425
250.56814
_E-302:
Exo, %
l 33400e-6
4 68933e-4
2 79821e-3
4 74889e-3
5 52417e-3
4 72593e-3
4 23395e-3
4 30244e-3
4 46169e-3
4 47715e-3
4 49143e-3
4 30770e-3
3 50794e-3
2 58314e-3
6 44047e-4
-i 60220e-3
-4 37309e-3
-7 16209e-3
-I 00230e-2
-1.20514e-2
-1.39538e-2
-1.53683e-2
-1.58787e-2
-1.59546e-2
-1.55958e-2
-1.42430e-2
-1.27456e-2
-1.13028e-2
-1.06915e-2
-1.06036e-2
-1.05702e-2
308
75 ,05274
79 5875£
85 99210
_0 32_96
_4 46m53
_ 33466
105 98946
I!2 76175
I19 14018
[26 02790
132 85553
140 08176
144 71805
151 63361
158 53897
167 54772
174 15123
180 98325
189 76146
196 27467
203 37595
212 61289
219 27958
225 79078
234 55035
241 57763
246 34941
250 48218
_-_:}--
Ex_,
3
3
I
3
2
1
-5
-3
-6
-9
-I
-i
-I
-I
-I
-I
-i
-9
-8
-8
%
2 '06210e-4
i 26753e-4
1 73786e-3
3 55324e-3
3 97712e-3
3 31460e-3
3 22625e-3
3 28224e-3
75496e-3
84682e-3
7@421e-3
57794e-3
95213e-3
47118e-3
52060e-4
62887e-3
44680e-3
31951e-3
24500e-2
39661e-2
47244e-248190e-2
42746e-2
28441e-2
08586e-2
44749e-3
97090e-3
90855e-3
309
rEMP, F
72 84782
77 61201
81 75192
86 06782
90 32544
'34 28694
98 93226
i05 q3409
112 36291
118 79338
126 02674
132 62834
142 15595
149 096Q8
155 74752
162 62347
169 72532
176 25301
182 66465
189 53554
196 40983
203 23101
210 11435
218 95358
225 55459
232 10365
238 82393
245 88587
252 42998
LE- 3921
E :'( _ , %7.34_DOe-5
4 30i25e-5
1 30972e-3
3 36827e-3
5 263_6e-3
5 45831e-3
4 72858e-3
4 59341e-3
4 6IeQ6e-3
4 _g426e-3
5 22087e-3
5 37583e-3
5 29192e-3
4 52321e-3
3 I0314e-3
9 04370e-4
I 98259e-3
4 90508e-3
8 06276e-3
1 12391e-2
I 37094e-2
1 54193e-2
I 62423e-2
i 62529e-2
I 62066e-2
1 51464e-2
1 42675e-2
i 38958e-2
I 37589e-2
310b
_EMC, F
73 =3289
75 37284
77 49242
_0 47237
83 16620
85 74562
89 84092
91 82i74
94 80270
97 72580
I01 50889
i05 62949
105 65555
108 04518
llO 96657
115 37436
I15 89701
i18 41907
121 68651
125 41512
127 99504
150 97328
135 72504
136 53264
139 62722
143 63814
146 56095
149 54075
153 15136
156 47535
159 05454
161 80567
166 58946
169 94243
172 86502
174 29840
176 47700
179.91606
183.69858
186.96572
189.83161
193.04126
196.82400
200.95027
204.33190
207.88631
210.92397
213.84765
216.94360
222.39050
226.57659
230.30378
233.62871
238.04370
241.36855
244.52236
248.13290
024
E×m. %
1.45423e-3
2.242_6e-3
2.96102e-3
4.23695e-3
5.4_512e-5
6.75345e-3
8 26541e-3
9 75549e-3
l 12835e-2
i 26496e-2
i 44831e-2
i 54557e-2
i 65883e-2
i 76108e-2
I 90489e-2
2 05074e-2
2 16738e-2
2 28962@-2
2 45521e-2
2 65458e-2
2 79302e-2
2 92781e-2
3 07164e-2
5 18124e-2
5 51422e-2
5 47233e-2
5 60173e-2
3 72571e-2
3.88747e-2
4 03484e-2
4 14986e-2
4 28288e-2
4 46074e-2
4 61169e-2
4 73569e-2
4.81480e-2
4.93167e-2
5.09524e-2
5.26418e-2
5.42056e-2
5.55717e-2
5.70635e-2
5.88070e-2
6.06221e-2
6.22039e-2
6.40736e-2
6.54756e-2
6.69857e-2
6.86578e-2
7.16786e-2
7.41422e-2
7.63000e-2
7.80079e-2
8.04893e-2
8.21791e-2
8.40133e-2
8.56128e-2 311
STE-37. _E-Z
TErnS. F
74 70765
76 596i7
7_ 22586
82 08289
84 65470
,_6 95877
90 53641
94 87214
98 12554
i01 09326
104 00541
106 57239
108 91272
Ill 88044
114 56153
116 89982
121 69530
124 49194
L26 89151
129 74533
131 80044
134 54173
136 59706
139 50875
142 13545
144 30515
146 47623
149 79003
152 13335
155 67726
158 01804
163 16144
166 58961
171 10147
173 55823
176 75767
179 89878
183 15654
185 27113
188 58493
192.63980
196 75093
200 51852
203 77123
209 08042
214 84317
218 78023
222 77309
225 22663
227 96356
231 78602
234 06825
236.17663
237.54256
239.82479
242.78883
244.89951
247.63736
EXP, %
5 82031e-4
i 05267e-3
l 93877e-3
3 00541e-3
3 92V%le-3
4 90343e-5
e 42158e-3
7 55_73e-3
8 58959e-3
i 00893e-2
i 14806e-2
1 27277e-2
1 40284e-2
1 50946e-2
i 64859e-2
1 78589e-2
i 90693e-2
2 12017e-2
2 25027e-2
2 34246e-2
2 47437e-2
2 56653e-2
2 68039e-2
2 77075e-2
2 89906e-2
30lllle-2
3 I0508e-2
3 18824e-2
3 31478e-2
3 39796e-2
3 52091e-2
3 62392e-2
3.81014e-2
3.94030e-2
4.12647e-2
4.220478-2
4.343408-2
4.47353e-2
4.58925e-2
4.66518e-2
4.79173e-2
4.95981e-2
5.13692e-2
5.30679e-2
5.46217e-2
5.69890e-2
5.98076e-2
6.17227e-2
6.37642e-2
6.49567e-2
6.64379e-2
6.83350e-2
6.94551e-2
7.07014e-2
7.16403e-2
7.27605e-2
7.44403e-2
7.55063e-2
7.69154e-2
312
252._035
313
-_E-_
TEMP, F
74 54082
75 84587
79 L5275
81 59286
85 82897
:B_ 42884
88 96955
90 87820
94 67£5
97 34358
LO0 23036
[02 83083105 25750
i08 84126
112 08017
114 73918
116 76308
118 73087
122 48386
125 02853
127 74486
130 28466
133 22846
]35 54049
138 59894
[41 48754
145 64270
147 72089
150 43418
154 06798
156 72183
159 95315
162 43533
164 45528
168 49034
172.06378
175 52348
177 25500
180 02349
182 21451
184 35093
185 73700
187 98655
190 i1994
191 96732
194 33394
196.52556
198.77572
202.17962
204.08584
206 96989
209 62737
211 88239
215 00392
217 49035
219 74445
222 80563
227 08515
229 33774
231 93365
= =-3C'::
3 45¢28e-4
[ Oe523e-3
I _9349e-3
2 95671e-3
3 85777e-3
5 06575e-3
6 16519e-3
7 1753qe-3
8 45437e-3
9 86036e-3
l 10858e-2
1 23300e-2
I 34659e-2
1 52332e-2
i 69470e-2
i 82635e-2
1 93097e-2
2 04284e-2
2 20324e-2
2 33673e-2
2 46837e-2
2 57288e-2
2 69361e-2
2 80722e-2
2 92792e-23 06134e-2
3 22709e-2
3 31358e-2
3 42711e-2
3 56037e-2
3 66124e-2
3 78733e-2
3 89005e-2
3 97112e-24 10430e-2
4 21946e-2
4 34007@-2
4 41034e-2
4 51118e-2
4.58679e-2
4.67871e-2
4.73999e-2
4.82283e-2
4.89664e-2
4.97413e-2
5.07143e-2
5.15066e-2
5.23712e-25.36681e-2
5.45334e-2
5.55959e-2
5.68219e-2
5.79762e-2
5.95272e-2
6.08079e-2
6.19079e-2
6.32779e-2
6.55147e-2
6.65242e-2
6.74967e-2
314
° ,
ZSs.=L4s5
24E.2L_,3}
244._S805
£4S.4£453
s. ae587e-2s.,O¢CSee-2
7.2k840e-2
_.34823e-2
7.45275e-2
7.526_0e-2
315
73.33626
75.39679
76.88483
78.77355
80.5180!
82.20626
84.43731
@6.15545
98.55608
90.84434
92.3£873
93 8[847
_7 13633
99 59563
102 91298
105 60150
107 94648
Ii0 23438
112 57964
114 46704
116 64051
118 64248
120 47240
123 61822
126 47795
128 47985
152 59837
134 37151
137 57465
139 51955
141 63580
142 95129
145 46821
148 95742
150 84529
153.47685
155.47907
157.82441
161.25699
163.14500
166.52043
168 23665
171 09715
173 95764
176 93272
179 44966
182 99657
185 68527
189.11756
191 46279
194 15124
197 41170
199 75667
201 81600
203 58904
206 16309
210 33868
213.19849
216.28683
218.23122
220.80484
-i. n_E71e-4
7_3665e-5
3 28728e-4
7 25440e-4
1 28480e-3
1 82599e-3
2 7lO21e-/
3 41400e-3
4 58847e-3
5 2807,3e-3
5 99457e-3
6 77069e-3
8 14218e-3
9 40559e-3
1 i0299e-2
1 21849e-2
1 33580e-2
1 44409e-2
1 54695e-2
I 64261e-2
1 74729e-2
1 83933e-2
1 94582e-2
2 09743e-2
2 24001e-2
2 33566e-2
2 51615e-2
2 59915e-2
2 74714e-2
2 83015e-2
2 93302e-2
2 99800e-2
3 10628e-2
3 26329e-2
3 33547e-2
3 43652e-2
3 51592e-2
3.61517e-2
3.74148e-2
3.80644e-2
3.92733e-2
3 99410e-2
4 09875e-2
4 20341e-2
4 30445e-2
4 41092e-2
4 54626e-2
4 65272e-2
4 79348e-2
4.89815e-2
5.01726e-2
5.16164e-2
5.27895e-2
5.36557e-2
5.45401e-2
5.56771e-2
5.75720e-2
5.89617@-2
6.05861e-2
6,16691e-2
6.30228e-2
316
22 _ _552 ! 0 3 L 2 q g
2 ] i gO0 !8
234 5_86q
237 73424
24_ 3944q
243 79683
245 74165
247 80080
249 34523
251 q7643
252 54822
t.77L54e-
_.86720e-
D_SSZe-
7 15777e-
7 35090e-
7 46279e-
7 54942e-
7 64507e-
7 715_5e-
7 85276e-
7 86886e-
2
22
2
2
2
2
2
2
2
2
2
317
=-40, LE-5,:929TEMP. F EX_,
73 97447
75 78i77
78 16558
80 21870
82 26829
84 55573
86 08541
88 43917
90 32518
93 08390
95 49425
97 90814
101 15318
103 26997
105 50525
107.63531
110.22692
112.58510
115.05912
116.65158
121.77467
124.61564
128.75870
132.97936
138 21475
141 84441
144 54477
147 12577
151 52027
154 92180
159 08199
162 36681
165 64809
169 62524
173 85174
176 97034
180.08806
183.37642
185.84247
189.48097
191.94968
194.65181
197.30797
201.48231
205.01915
207.60456
211.30408
214.25292
218.13901
221.79521
226.17293
229.58951
232.88141
235.81432
240.55011
243.70584
247.20020
250.33823
252.48595
%
L 9837Le-4
7 13113e-4
i 26121e-3
2 0995_e-3
2 86582e-3
3 79331e-3
4 50786e-3
5 6154_e-3
6 56293e-3
7 72278e-3
8 81209e-3
9 97357e-3
1 16724e-2
1 26368e-2
1 36728e-2
1 49078e-2
1 61767e-2
1 73746e-2
i 85899e-2
i 94124e-2
2 18964e-2
2 35611e-2
2 55806e-2
2 76537e-2
3 00830e-2
3.14192e-2
3.25613e-2
3.36137e-2
3.53071e-23.66805e-2
3 82848e-2
3 96226e-2
4 08882e-2
4 22769e-2
4 40614e-2
4 55263e-2
4 69731e-2
4.83831e-2
4.94361e-2
5.09526e-2
5.20597e-2
5.32379e-2
5.46508e-2
5.65438e-2
5.83315e-2
5.94742e-2
6.10626e-2
6.25825e-2
6.44588e-2
6.63362e-2
6.88597e-2
7.05398e-2
7.20219e-2
7.32170e-2
7.48367e-2
7.58864e-2
7.68081e-2
7.74970e-2
7.79199e-2
318
q_g7
i00104i08112[15120122126129133]371411451481531581621661691731761811821851891941982O2206210214219222225228231233237242246249
T'E-4L, '_E-ZC, Z _
TEMP,
74.5L046
76.56776
78.67942
81.18975
82.07010
95.12i00
86.60161
89 59229
9 .15752
06226
42056
88893
75676
50841
48870
61436
50232
77682
81334
94060
35806
39884
44389
03111
84590
00208
24206
06006
67619
92602
68619
53416
77921
97148
64731
17883
53260
40283
04415
.99713
.52705
.39728
.06218
70563
43848
80078
19918
59864
71909
1297413959
06429
ExP. %
1 9_882e-4
5 6014ie-4
l 12232e-3
1 84755e-3
2 48155e-3
3 35137e-3
3 _6729e-3
5 1085_e-3
5 85130e-3
7 02885e-3
8 53221e-3
1 03430e-2
l 22626e-2
1 42906e-2
i 63550e-2
1 80932e-2
2.07730e-2
2.19500e-2
2.40867e-2
2.57165e-2
2.70933e-2
2.89408e-2
3.04989e-2
3.20205e-2
3.36508e-2
3.54441e-2
3 75637e-2
3 89770e-2
4 06622e-2
4 17496e-2
4 31991e-2
4 43404e-2
4 61165e-2
4 68588e-2
4 80181e-2
4 94312e-2
5 16051e-2
5.33620e-2
5.51006e-2
5.72561e-2
5.87777e-2
6.05346e-2
6.27984e-2
6.43924e-2
6.55698e-2
6.68020e-2
6.73463e-2
6.78183e-2
6.81471e-2
6.82229e-2
6.82804e-2
6.81020e-2
319
-'£-4-.
TEMP, =74 9542 _
76 _5029
78 70812
81 79091
86 01317
89 71886
93 15727
_7 35428lOi 51505
106 86656
112 27459
116 19847
122 23582
126 507O1
132 31886
138 07244
141 83260
145 93481
151 06725
154 25870
158 13746
164 12238
170.10935
175 24061
177 86335
183 10795
189 49261
193 93891
198 55623
202 94455
208 12650
211 53994
215 81142
219 62547
223.15780
227.09337
230.80169
234.85994
240.01195
244.83097
248.50498
_E-l} ZO
E x P, %-3 45040e -=
3 30029e-4
8 58221e-4
i 89553e-3
3 46023e-3
5 02446e-3
6 6065_e-3
8 4979qe-i
i 03167e-2
1 30440e-2
1 58259e-2
i 80982e-2
2 10076e-2
2 30987e-2
2 57538e-2
2 84634e-2
3 02092e-2
3 21005e-2
3 41742e-2
3 55927e-2
3 71027e-2
3.97035e-2
4 21773e-2
4 43236e-2
4 54150e-2
4 76522e-2
5 03804e-2
5 22902e-2
5 42727e-2
5 62187e-2
5 87825e-2
6 06732e-2
6.27461e-2
6.47098e-2
6.63464e-2
6.78927e-2
6.92936e-2
7.03500e-2
7.12076e-2
7.13571e-2
7.13240e-2
320
73
76
,78
79
82
85
86
88
90
9497
99
102
t06
llO114
li7
119
121
124
127
132
135
138
143
147
152
;rE-43. .E-!C5
TEMP. = E×
858£_ 1
09509 5
33241 1
82413 1
98012 2
16045 3
76705 3
71818 4
44007 5
11297 7
78653 9
91030 l
14918 1
74126 1
58687
08852
07346
25453
72212
47725
63376
51177
66859
82486
30190
26182
77057
156.67287
160.97654
164.53441
167.11700
171.36326
175.49492
179.85608
183.47129
187.54575
190.30018
194.71911
198.50695
202.12291
205.50876
209.69877
213.19984
215.89744
218.76720
221.69437
224.56409
227.26132
229.90089
233.74534
236.61405
241.48992
244.47214
248.71565
i
840o9e-4
23937e-4
06212e-3
51[06e-3
661i4e-3
37969e-3
91864e-3
70959e-3
5548_e-3
13706e-3
04375e-3
01409e-2
14544e-2
39009e-2
i 58254e-2
1 77863e-2
1 94234e-2
2 05026e-2
2 14912e-2
2 28942e-2
2 43147e-2
2 63822e-2
2 79470e-2
2 92413e-2
3 15076e-2
3 32517e-2
3 53184e-2
3 69183e-2
3 85178e-2
3 99198e-2
4.10706e-2
4.26340e-2
4.42336e-2
4.59051e-2
4.73071e-2
4.89789e-2
5.00393e-2
5.19271e-2
5.36353e-2
5.54159e-2
5.68181e-2
5.89225e-2
6.05950e-2
6.19079e-2
6.32927e-2
6.47135e-2
6.60803e-2
6.72129e-2
6.81833e-2
6.95309e-2
7.03928e-2
7.13966e-2
7.16815e-2
7.18747e-2
" 321