SOURCE AREA ISCO EVALUATION CLEBURN STREET WELL SITE GRAND ISLAND, NEBRASKA
Contract No.: EP-S7-05-05 Task Order No.: 0041
Prepared for
U. S. Environmental Protection Agency Region 7
901 North 5th Street Kansas City, Kansas 66101
Prepared by HydroGeoLogic, Inc
6340 Glenwood, Suite 200 Overland Park, Kansas 66202
November 2010
U.S. EPA Region 7 Source Area ISCO Evaluation i November 2010
TABLE OF CONTENTS
Section Page
1.0 INTRODUCTION ................................................................................ 1-1 2.0 BACKGROUND .................................................................................. 2-1
2.1 SITE LOCATION AND DESCRIPTION ............................................ 2-1 2.2 PHYSICAL SITE SETTING ........................................................... 2-1
2.2.1 Site Soils and Geology .......................................................... 2-1 2.2.2 Regional and Site-Specific Hydrogeology ................................... 2-1
2.3 SUMMARY OF TREATABILITY STUDY FOR THE GROUNDWATER PLUME (2009) ............................................................................ 2-2
3.0 STUDY SETUP AND PROCEDURES ...................................................... 3-1
3.1 GROUNDWATER PROFILE SAMPLING ......................................... 3-1 3.2 PERMANENT INJECTION WELL INSTALLATION ........................... 3-2 3.3 CHEMICAL OXIDANT INJECTION ACTIVITIES .............................. 3-2 3.4 GROUNDWATER MONITORING PROGRAM ................................... 3-4
4.0 GROUNDWATER MONITORING AND EVALUATION ............................. 4-1
4.1 IDENTIFICATION OF WELLS AFFECTED BY OXIDANT .................. 4-1 4.2 VOLATILE ORGANIC COMPOUNDS ............................................. 4-3
5.0 SUMMARY AND RECOMMENDATIONS ............................................... 5-1
5.1 SUMMARY................................................................................ 5-1 5.2 RECOMMENDATIONS ................................................................ 5-1
6.0 REFERENCES .................................................................................... 6-1
LIST OF APPENDICES Appendix A Groundwater Profile Screening Data Appendix B Soil Boring Logs Appendix C Well Completion Records Appendix D Nebraska Well Registrations Appendix E Photographic Documentation Appendix F Analytical Data Results
U.S. EPA Region 7 Source Area ISCO Evaluation ii November 2010
LIST OF TABLES Table 3.1 Groundwater Monitoring Schedule Table 3.2 Injection Parameters Table 3.3 Chemical Oxidant Parameters Table 4.1 Metals Analytical Results in (December 2009 – July 2010) Table 4.2 VOC Analytical Results (December 2009 – July 2010)
LIST OF FIGURES Figure 2.1 Site Location Map Figure 2.2 Source Area Site Map Figure 2.3 Potentiometric Map (July 2010) Figure 2.4 Geologic Cross Section A-A’ Figure 2.5 Geologic Cross Section B-B’ Figure 2.6 Temporary Monitoring Well Locations, Plume TS - 2009 Figure 2.7 Chemical Oxidant Injection Locations, Plume TS - 2009 Figure 3.1 Groundwater Profile Sampling, December 2009 Figure 3.2 Injection Well Locations Figure 4.1 Injection Well and Monitoring Locations Figure 4.2 Baseline PCE Concentrations (December 2009) Figure 4.3 Post-Injection Monitoring of PCE (January 2010) Figure 4.4 Post-Injection Monitoring of PCE (July 2010) Figure 4.5 MW-2A PCE Trend Graph Figure 4.6 MW-12A PCE Trend Graph Figure 4.7 MW-12A TCE Trend Graph
U.S. EPA Region 7 Source Area ISCO Evaluation iii November 2010
LIST OF ACRONYMS AND ABBREVIATIONS AES Architect and Engineering Services ASR analytical services request bgs below ground surface CCL4 carbon tetrachloride cis-1,2-DCE cis-1,2-dichloroethene 1,1-DCE 1,1-dichloroethene DPT direct-push technology DQO data quality objective EPA U. S. Environmental Protection Agency ft/day feet per day GET groundwater extraction and treatment g/kg grams per kilogram gpm gallons per minute GSI Geotechnical Services, Inc. HCl hydrochloric acid HGL HydroGeoLogic, Inc. ISCO in situ chemical oxidation KMnO4 potassium permanganate
µg/kg micrograms per kilogram µg/L micrograms per liter mg/L milligrams per liter ml milliliter MCL maximum contaminant level OHM One Hour Martinizing PCE tetrachloroethene PNOD permanganate natural oxidant demand psi pounds per square inch PVC polyvinyl chloride
U.S. EPA Region 7 Source Area ISCO Evaluation iv November 2010
LIST OF ACRONYMS AND ABBREVIATIONS (continued) QA quality assurance QAPP Quality Assurance Project Plan QC quality control SAP Sampling and Analysis Plan SOP standard operating procedure TCE trichloroethene trans-1,2-DCE trans-1,2-dichloroethene TS treatability study USEPA United States Environmental Protection Agency VOC volatile organic compound
U.S. EPA Region 7 Source Area ISCO Evaluation 1-1 November 2010
SOURCE AREA ISCO EVALUATION CLEBURN STREET WELL SITE GRAND ISLAND, NEBRASKA
1.0 INTRODUCTION
The U.S. Environmental Protection Agency (EPA) Region 7 tasked HydroGeoLogic, Inc. (HGL) to conduct a pilot-scale in situ chemical oxidant injection (ISCO) treatability study (TS) at the Cleburn Street Well Site in Grand Island, Nebraska. Potassium permanganate (KMnO4) was chosen as the chemical oxidant due to its relatively low cost, ease of use, and demonstrated effectiveness in treating dissolved chlorinated volatile organic compound (VOC) contamination at other sites. This work is being executed under Architect and Engineering Services (AES) Contract EP-S7-05-05, Task Order 0041. The TS was performed to evaluate the effectiveness of ISCO in treating dissolved VOC contamination in the source area at the site. Pre-injection concentrations of tetrachloroethene (PCE), the primary contaminant of concern, in the source area groundwater ranged from 100,000 micrograms per liter (µg/L) to 160,000 µg/L. This report details the TS activities, which commenced in December 2009 and included five rounds of post-injection monitoring completed through July 2010. The report is organized as follows:
• Section 1 introduces the objectives of the TS.
• Section 2 provides background information for the site, including a summary of a previous TS conducted within the plume immediately downgradient of the source.
• Section 3 describes how the study was designed, and all field efforts conducted in support of the TS.
• Section 4 presents the results of the post-injection groundwater investigation.
• Section 5 provides recommendations for future use of ISCO at the site.
• Section 6 lists the references cited in the report.
All field activities were conducted in accordance with the procedures specified in the Final Sampling and Analysis Plan for Long-Term Response Action, Cleburn Street Well Site, Grand Island, Nebraska (SAP) dated January 2009 (HGL, 2009) and the SAP Addendum dated November 18, 2009 (HGL, 2009b). Any deviations from the referenced planning documents are discussed in Section 3. The purpose of the ISCO TS in the source area was to evaluate whether ISCO is effective in reducing levels of chlorinated VOCs in groundwater to below maximum contaminant levels (MCLs). Groundwater samples were collected before injections were completed to establish baseline VOC levels. After injection of the ISCO, five rounds of performance monitoring samples were collected to document post-injection contaminant levels in groundwater at the
HGL—Source Area ISCO Evaluation, Cleburn Street Well Site—Grand Island, NE
U.S. EPA Region 7 Source Area ISCO Evaluation 1-2 November 2010
source area. The findings of the post-injection monitoring will be used to determine whether changes in the chemical oxidant injection approach are needed, if the ISCO remedy is carried through to full scale implementation.
HGL -- Source Area ISCO Evaluation – Cleburn Street Well Site, Grand Island, NE
U.S. EPA Region 7 Source Area ISCO Evaluation 2-1 November 2010
2.0 BACKGROUND
2.1 SITE LOCATION AND DESCRIPTION
The Cleburn Street Well Site (site) is located near the downtown area of Grand Island, and is comprised of various locations in downtown Grand Island where PCE contamination of subsurface soils and groundwater has been identified. The site encompasses a developed area of approximately 144 city blocks (Figure 2.1) and land use consists of single family residences, light manufacturing, and retail shops. A Union Pacific railroad corridor passes through the site from southwest to northeast. The focus of this TS was the source area located on the west side of Eddy Street beneath the former One Hour Martinizing (OHM) building located at the southwest corner of Eddy Street and 4th Street (Figure 2.2).
2.2 PHYSICAL SITE SETTING
2.2.1 Site Soils and Geology
Surficial soils at the site consist of O’Neill and Pivot loams or O’Neill sandy loam characterized by dark grayish-brown, friable, sandy silt or silty sand that extend from the surface to approximately 3 feet below ground surface (bgs). Beneath the surficial soils are Quaternary alluvial sands and gravelly sands occasionally interbedded with thin clayey sand, sandy clay, silt, and silty sand layers. A prominent silt/silty sand unit occurs within the alluvium at a depth that ranges from 24 to 28 feet bgs at the top to 35 to 39 feet bgs at the bottom. This unit appears to be continuous beneath the site. The Quaternary alluvial deposits comprise the shallow aquifer which, in the vicinity of the site, extends to depths ranging from 87 to 94 feet bgs. Underlying the Quaternary alluvial deposits is a clay aquitard ranging from 144 to 153 feet in thickness.
2.2.2 Regional and Site-Specific Hydrogeology
Shallow groundwater underlying Grand Island occurs as an unconfined water table aquifer within the alluvial sands and gravels of the Grand Island Formation. The average depth to water is generally 20 feet bgs. Total thickness of the water table aquifer is about 70 feet within the study area. Hydraulic conductivity values range up to 670 feet per day (ft/day) (WJE, 1993). Pumping tests conducted during the design stage of EW-1 in the sand unit yielded a hydraulic conductivity value of 345 ft/day, which calculates to a linear groundwater velocity of 3.5 ft/day (GeoTrans, 2001). The Grand Island Formation aquifer is used regionally as a water supply source for irrigation and potable water. In the vicinity of the Cleburn Street Well Site plume, all water for private domestic use is supplied by the City of Grand Island. The city's municipal well field is located southeast of the city near the Platte River. The predominant regional groundwater flow direction within the shallow aquifer is to the northeast. Regional horizontal gradients of 4 to 7 feet per mile have been measured in the area (Woodward-Clyde, 1997 and 1998; URSG, 1999). However, an east/southeast flow component was documented by HGL during subsequent field efforts. Groundwater measurements were collected by HGL from the site monitoring well network the week of July
HGL—Source Area ISCO Evaluation, Cleburn Street Well Site—Grand Island, NE
U.S. EPA Region 7 Source Area ISCO Evaluation 2-2 November 2010
26, 2010, during the quarterly groundwater performance monitoring event. The groundwater extraction and treatment (GET) system had been shut down for approximately 7 months when these measurements were recorded; therefore, water levels were not influenced by pumping of the extraction wells .Water level measurements indicated that groundwater flow in the site area appears split between the regional northeast trend and an east/southeast component (Figure 2.3). It is possible that the intermittent pumping of the dewatering sump at the Eddy Street underpass contribute to this bidirectional flow. Cross sections were developed from the lithologic logging conducted during the installation of the monitoring wells completed in February and March 2009 and are included in the Well Installation and Testing and Evaluation of the Silt Layer, Cleburn Street Well Site (HGL, 2009a). These cross section maps are included as Figures 2.4 and 2.5. Cross sections from the Februaru/March 2009 investigation were compared to the lithology logged in two temporary boreholes in the study area (SB-01 and SB-02) that were advanced and logged before initiating the source area TS. The lithology was consistent with the lithology documented in the February/March 2009 study. The cross sections depict a silt/silty sand unit that occurs at approximately 28 feet to 39 feet bgs at the site. Much of the contamination beneath the site is contained within this silt/silty sand. The silt/silty sand unit then dips slightly to the northeast. The dipping of the silt/silty sand to the northeast combined with the groundwater flow direction appears to be controlling the migration of the PCE, causing it to migrate in a fan-shaped pattern that spans from the northeast to the east.
2.3 SUMMARY OF TREATABILITY STUDY FOR THE GROUNDWATER PLUME (2009)
A TS was conducted from June through August 2009 under Task Order 0019. This TS focused on the plume downgradient of the source on the east side of Eddy Street. The purpose of this TS was to determine whether ISCO injections in the plume would be effective in supplementing the existing GET system operating at the source A full discussion of the study and findings are detailed in the In Situ Chemical Oxidant Injection Evaluation submitted to EPA in November 2009 (HGL, 2009c). A brief review of this TS and the findings of the post-injection monitoring follows. The TS involved application of KMnO4 delivered through 20 injection points in the downgradient plume from the Cleburn Street source area. Three rounds of post injection sampling were conducted at 16 temporary and permanent wells located crossgradient, within, and downgradient of the injection zone. In June 2009, eight temporary monitoring wells were installed cross-gradient and immediately downgradient of the injection zone to supplement the existing monitoring well network and facilitate groundwater performance monitoring during the study (Figure 2.6). Wells were installed in clusters of two to monitor the upper and lower portion of the silt layer as well as the transition to sands at each location as follows:
HGL—Source Area ISCO Evaluation, Cleburn Street Well Site—Grand Island, NE
U.S. EPA Region 7 Source Area ISCO Evaluation 2-3 November 2010
• A-level wells (DPT-1-A, DPT-2-A, DPT-3-A, and DPT-4-A) were screened at 25 to 35 feet bgs to characterize contaminants in the upper sand and sandy silt/silty sand zone near the water table..
• B-level wells (DPT-1-B, DPT-2-B, DPT-3-B, and DPT-4-B) were screened at 35 to 45 feet bgs to characterize the lower sandy silt/silty sand and sand zone.
Injection points were arranged in three rows. The two outside rows consisted of seven injection locations and the middle row had six injection locations. The middle row was staggered between the outside rows. The rows were spaced five feet apart. Injection points within each row were spaced 10 feet apart. The injection sequence commenced at the northeastern corner and proceeded south following the injection point configuration shown in (Figure 2.7). Injections were completed beginning at hydraulically downgradient locations and moving upgradient. The KMnO4 solution was injected into the subsurface using a direct-push technology (DPT) rig to deliver the injectant at the proper interval. At each injection point, the DPT rods were advanced to depth with the DPT rig. The end of the rod was equipped with a 13-inch long injection tool with a series of four holes spaced one inch apart along its length. The injection tool was then exposed and the injectant was dispersed through the holes. Injection generally started at 31 feet bgs and moved upward to 20 feet bgs in one-foot increments (bottom-up injection approach). An average of 658 gallons of KMnO4 solution was injected per location. The total volume of KMnO4 solution injected was 13,154 gallons. Post-injection monitoring was conducted over a 2-month period from late June through late August 2009. Analytical results indicated that KMnO4 was effective in reducing PCE concentrations within the plume and could be used to reduce PCE concentrations at the source area. A final recommendation of the plume study was to focus future KMnO4 injections at the source area where it would have a greater benefit for reducing contamination. Based on the findings of the TS completed in the plume downgradient of the source, EPA determined that although the optimized GET system appeared to be controlling plume migration, it was not effectively remediating contamination in the source area. EPA subsequently tasked HGL to complete a TS in the source area, as recommended in the plume TS report.
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HGL—Source Area ISCO Evaluation—Cleburn Street Well Site, Grand Island, Nebraska
Figure 2.1Site Location Map
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Filename: X:/EPA009/Cleburn/Well InstallSite_Loc_Map.mxdProject: EP9019.11.01.16.01Revised: 11/05/10 STSource: ESRI StreetMap North America
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Figure 2.3Potentiometric Map
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³Filename: X:/EPA009/Cleburn/FSP/Potentiometric_Map_July_2010.mxdProject: EP9019.11.42.04Revised: 11/05/10 STSource: Grand Island Utilities Dept.HGL Database
HGL—Source Area ISCO Evaluation—Cleburn Street Well SiteGrand Island, Nebraska
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HGL—Cleburn Street Well Site, Grand Island, Nebraska
Source ISCO Evaluation Report
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HGL—Cleburn Street Well Site, Grand Island, Nebraska
Source ISCO Evaluation Report
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Temporary Monitoring WellClusterA - 25 to 35 feet bgsB - 35 to 45 feet bgs
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Monitoring Well!UP
Extraction Well+U
Soil Vapor Extraction Well#0
HGL—Source ISCO Evaluation Report—Cleburn Street Well SiteGrand Island, Nebraska
Legend
U.S. EPA Region 7
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Eddy Street
Frontage Road
Parking Lot
DPT-1A/1B
DPT-4A/4B
DPT-3A/3B
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MW102-BB
MW102-AA
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Figure 2.7Chemical Oxidant Injection Locations
Plume TS - 2009
³Filename: X:/EPA009/Cleburn/MapsChemical_Oxidant_Locations.mxdProject: EP9019.11.01.19.04Revised: 11/12/10 STSource: Grand Island Utilities Dept.HGL Database
HGL—Source ISCO Evaluation Report—Cleburn Street Well SiteGrand Island, Nebraska
Shallow Monitoring Well(102-AA)
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0 2010
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Existing Building
Curb Line
Intermediate Monitoring Well(102-BB)
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Temporary Monitoring WellClusterA - 25 to 35 feet bgsB - 35 to 45 feet bgs
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ISCO Injection Point"
Note:Injection interval is 20-31 feet below ground surface.
1
HGL—Source Area ISCO Evaluation, Cleburn Street Well Site—Grand Island, NE
U.S. EPA Region 7 Source Area ISCO Evaluation 3-1 November 2010
3.0 STUDY SETUP AND PROCEDURES
The TS activities for the source area ISCO evaluation were conducted from December 2009 through July 2010. The TS focused on a portion of the source area beneath the former OHM building and in the frontage road adjacent and east of the building (Figure 3.1). This area has historically been the most contaminated portion of the site. TS activities included the following:
• Limited characterization of the source area by conducting groundwater profile sampling.
• Installation of permanent injection wells.
• Injection of chemical oxidants into the subsurface.
• Collection of pre- and post-injection groundwater samples from the monitoring wells and injection wells.
The schedule for these activities is displayed in Table 3.1. A discussion and evaluation of the sample results is presented in Section 4.0.
3.1 GROUNDWATER PROFILE SAMPLING
The groundwater profile study was conducted December 3, 4, and 5, 2009. Groundwater samples were collected from temporary DPT wells emplaced at 10 locations (GW-01 through GW-10) in the source area to provide limited characterization of the area and determine optimal placement of permanent injection wells for the TS (Figure 3.1). Five groundwater samples were collected from each location to characterize the water column in and above the silt layer. Samples were collected at 4-foot intervals starting with the deepest interval: 36 to 40 feet bgs; 32 to 36 feet bgs; 28 to 32 feet bgs; 24 to 28 feet bgs; and 20 to 24 feet bgs,. No samples were collected from below 40 feet because previous investigations have identified the bottom of the silt layer, where much of the contamination appears to be bound, is approximately 40 feet bgs. The sampling apparatus was advanced to depth using the track-mounted DPT rig. Then, the 4-foot sampling screen was exposed, and the groundwater sample retrieved through disposable tubing using a foot valve as specified in the SAP Addendum (HGL, 2009b). Two to three casing volumes of water were purged from the tubing, field parameters were collected, and then the sample was collected at each depth interval. Tubing was removed and replaced between sample intervals To facilitate quick turn on the analysis, samples were screened for PCE and trichloroethene (TCE) by Platte Valley Laboratories, Inc. in Gibbon, Nebraska. All samples were collected and handled in accordance with the SAP Addendum (HGL, 2009b). After collection, all samples were labeled, placed in coolers, and iced, for temporary storage pending hand delivery to Platte Valley Laboratories.
HGL—Source Area ISCO Evaluation, Cleburn Street Well Site—Grand Island, NE
U.S. EPA Region 7 Source Area ISCO Evaluation 3-2 November 2010
The data was received within two days and reviewed by the field team. Figure 3.1 displays the PCE concentrations by depth. In general, PCE levels increased from west to east. Levels also were higher in the shallower intervals. In GW-10, the westernmost borehole, the highest PCE concentration was 11 µg/L in the 20 to 24 foot bgs interval. In GW-09, on the eastern portion of the study area, PCE was identified at 99,241 µg/L in the 20 to 24 foot bgs interval. TCE was detected in the five easternmost boreholes (GW-05 through GW-09) at much lower concentrations. The highest detection of TCE was identified in GW-07 at 184 µg/L in the 20 to 24 foot bgs interval. The screening data is included in Appendix A. After the sampling activities were completed, the casing and screens were withdrawn from the subsurface, the boreholes were backfilled with granular bentonite, and the surface condition at the well site restored.
3.2 PERMANENT INJECTION WELL INSTALLATION
Based on the data obtained from the groundwater profile sampling, ten locations were chosen to install the injection wells. The locations were adjusted as necessary to accommodate physical access limitations within the building (Figure 3.2). The wells were installed during the same field event as the groundwater profile investigation using the same subcontractor: GSI. The ten injection wells were constructed with 10-foot screens for delivery of the KMnO4. The screen interval for the ten injection wells extends from 22 feet bgs to 32 feet bgs for injection into the most contaminated interval in the subsurface as documented in the groundwater profile study. All of the injection wells were constructed using 2-inch schedule 40 polyvinyl chloride (PVC) casing and ten feet of PVC 0.010-inch milled slot screen. Wells were completed using a silica sand filter pack, a chip bentonite seal, and 28 percent solids bentonite slurry pressure-grouted using a tremmie pipe from the top of the bentonite seal to ground surface. All of the injection wells were finished at the surface with flush mount completion in concrete that matched the surrounding concrete floor of the facility. Appendix B includes Boring Logs for the new wells; Appendix C contains the Monitoring Well Construction Diagrams; and Appendix D includes the Nebraska Well Registration Forms. Well installation procedures were conducted in accordance with the SAP Addendum (HGL, 2009a).
3.3 CHEMICAL OXIDANT INJECTION ACTIVITIES
Two injection rounds were completed: one in December 2009 and the second in March 2010. KMnO4 was delivered through 14 permanent injection wells in the Cleburn Street source area: the 10 newly installed wells and four existing wells that are screened across the silt zone. Concentrated KMnO4 powder was shipped to the site in 5-gallon buckets (55.1 pounds of KMnO4 in each) by the Carus Chemical Company and stored in the secured remediation building. Water was provided by the city from a hydrant located at the transportation facility on the corner of West North Front Street and North Washington Street. To achieve a 2.0 percent KMnO4 mixture, approximately 16.7 pounds of KMnO4 powder was mixed with every 100
HGL—Source Area ISCO Evaluation, Cleburn Street Well Site—Grand Island, NE
U.S. EPA Region 7 Source Area ISCO Evaluation 3-3 November 2010
gallons of water in a mixing tank. Tables 3.2 and Table 3.3 summarize the injection and chemical oxidant parameters. The concentration of KMnO4 was based on soil testing conducted during the TS completed in the plume. It was determined from boring logs that soils beneath the building were similar to those encountered during this previous study. A key test to determine the percentage of KMnO4 required is based on the natural oxidant demand of the soil, which reflects the amount of KMnO4 that will be consumed by natural reducing agents during a given amount of time. The soil samples that had been tested for the plume TS had a 48-hour KMnO4 demand value of 0.4 grams per kilogram (g/kg). Natural oxidant demand of less than 10 g/kg at 48 hours is considered favorable for in situ chemical oxidation with KMnO4. GSI used two high density polyethylene tanks sized at 1,320 gallons and 500 gallons, to mix and store the KMnO4 solution. The two tanks were utilized so that while one tank was supplying KMnO4 to the injection wells, the other tank could be used to mix and prepare the solution to minimize delays. The tanks were filled with water from the city’s transportation department and transported back to the site. The solution was circulated in the tanks with a pump to keep the KMnO4 powder in solution. The equipment used by GSI is shown in Appendix D – Photographic Documentation. Pumps and fittings were provided with secondary containment. A neutralizing solution consisting of one part vinegar, one part hydrogen peroxide, and one part water was used to clean up equipment and neutralize KMnO4 spills. A 1½-inch rubber hose was used to connect the tanks to the injection header. Chemical oxidant was pumped from the tanks through a flexible hose to the injection header. The injection header was configured for four injection points. The injection header consisted of a gate valve, flow meter, and pressure gauge for each injection point. The pressure and flow rate to each injection point could be controlled by the injection header. Injection points (IW-1 through IW-10) were spaced approximately 10 feet apart (Figure 3.2). In addition, four existing wells (DPE-1 through DPE-4) supplemented the injection wells to target the silt zone. The four DPE wells are six inches in diameter and screened from approximately 31 to 36 feet bgs. They are spaced about 15 feet apart. The flow rate, total volume injected, and pressure were monitored throughout the injection process to determine the maximum rate at which oxidant could be delivered to the targeted zone. Nebraska regulations require that the pressure not exceed approximately 1 pound per square inch (psi) per foot of overburden. In general, KMnO4 could be delivered between 5 and 10 gallons per minute (gpm) to each well without exceeding the pressure requirements. The total volume of KMnO4 solution injected based on flow measurements was 34,500 gallons. Approximately 2,750 gallons were delivered to each of the 10 injection wells and 1,750 gallons were delivered to each of the four DPE wells as planned. Injection pressures were at or below the 1 psi/ft of overburden requirement.
HGL—Source Area ISCO Evaluation, Cleburn Street Well Site—Grand Island, NE
U.S. EPA Region 7 Source Area ISCO Evaluation 3-4 November 2010
3.4 GROUNDWATER MONITORING PROGRAM
The monitoring program for the KMnO4 injections at the Cleburn Street Well Site consisted of five separate monitoring events conducted over a 6-month period. Two monitoring events occurred after the December 2009 injection: January and March 2010. Three monitoring events occurred after the March 2010 injection: April, May, and July 2010. Groundwater samples were collected from permanent wells within the injection area. Downgradient wells on the east side of Eddy Street were sampled during the quarterly monitoring (scoped under a separate task). The location of each groundwater sampling point for the TS is shown on Figure 4.1. Samples were collected from the same wells for all five post-injection monitoring events. Groundwater samples were collected for VOCs and total metals analyses. VOC groundwater samples were analyzed using SW-846 Methods 5030B, and 8260B, EPA Method 624 and EPA Region 7 Standard Operating Procedure (SOP) 3280.13C. Metals were analyzed in accordance with EPA Method 200.7. VOC groundwater samples were collected in 40-milliliter (ml) vials. Ascorbic acid was added to remove the color interference from the KMnO4. Total metal samples were collected in 1-liter polyethylene containers and preserved with nitric acid to a pH of <2. The samples were analyzed by the EPA Region 7 laboratory. The target analytes for pre-injection and post-injection monitoring were arsenic, chromium, manganese, PCE, TCE, cis-1,2-dichloroethene (cis-1,2-DCE), and trans-1,2-dichloroethene (trans-1,2-DCE). Other analytes detected were noted as they pertained to quality assurance/quality control (QA/QC) and the overall analysis of the effectiveness of the KMnO4 injection.
TABLE(S)
HGL—Source Area ISCO Evaluation, Cleburn Street Well Site—Grand Island, NE
U.S. EPA Region 7 Source Area ISCO Evaluation 3-6 November 2010
Table 3.1 Injection and Performance Monitoring Schedule
Table 3.2
Injection Parameters
Table 3.3 Chemical Oxidant Parameters
Schedule Start Date End Date Groundwater Profile Study 12/3/2009 12/5/2009 Installation of Permanent Injection Wells 12/6/2009 12/11/2009 Baseline Monitoring Event 12/10/2009 12/11/2009 KMnO4 Injection – Round 1 12/16/2009 12/22/2009
• First Post-Injection Monitoring Event 1/19/2010 1/26/2010 • Second Post-Injection Monitoring Event 3/1/2010 3/4/2010
KMnO4 Injection – Round 2 3/8/2010 3/11/2010 • Third Post-Injection Monitoring Event 4/5/2010 4/8/2010 • Fourth Post-Injection Monitoring Event 5/3/2010 5/8/2010 • Fifth Post-Injection Monitoring Event 7/26/2010 8/2/2010
Injection Location Number of Injection Points
Injection Interval (feet bgs)
Injection Point Spacing (feet)
Percent Solution
(%)
Volume per Injection
Point (gallons)
Total Volume (gallons)
Injection Wells – 2” (IW-1 to IW-10) 10 22 to 32 ~10 2.0 2,750 27,500
Injection Wells - 6” (DPE-1 to DPE-4) 4 31 to 36 ~30 2.0 1,750 7,000
Chemical Oxidant Percent Solution
(%)
Volume per Injection
Point (gallons)
Total Volume (gallons)
Mass Oxidant per Injection
Point (pounds)
Total Mass of Oxidant (pounds)
KMnO4 2.0 2,750 27,500 459 4,590 1,750 7,000 292 1,168
FIGURE(S)
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4th Street
Eddy Street Underpass
N. Frontage Road (W
est)
Billiards / Bar(Active Business)
RemediationBuilding
Former One HourMartinizing
Retaining Wall
Retaining Wall
GW-09GW-08
GW-10
GW-03GW-04
GW-05
GW-02GW-06
GW-07
GW-01
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Figure 3.1Groundwater Profile Sampling
December 2009
³
Filename: X:/EPA009/Cleburn/MapsBaseline_PCE_Concentrations.mxdProject: EP9019.11.42.04Revised: 11/05/10 STSource:
0 20 40 60
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U.S. EPA Region 7
HGL—Source Area ISCO Evaluation Report—Cleburn Street Well SiteGrand Island, Nebraska
Legend
!.Groundwater Sample Location(profile)
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Retaining Wall
Concentration (PCE) in ppbDepth
20‐24' bgs24‐28' bgs28‐32' bgs32‐36' bgs36‐40' bgs
GW‐0638350385282384755533
GW‐10116NDNDND
GW‐048992354300140ND
GW‐0358911391970NDND
GW‐0215702102648912ND
GW‐01535NDNDND
Not DetectedND
6,4892,1021,570
1,9701,139
2,3543,001
23,84738,52838,350
GW‐048992354300140ND
2,3543,001
GW‐078330687471174362770253
83,30687,47117,4362,770
GW‐099924179508942841723218
99,24179,50894,2841,723
GW‐05118131091630120394ND
11,81310,91630,120
GW‐08222832699015191NDND
22,28326,99015,191
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Figure 3.2Injection Well Locations
³Filename: X:/EPA009/Cleburn/MapsInjection_Well_Locations.mxdProject: EP9019.11.42.04Revised: 11/05/10 STSource:
0 20 40 60
Feet
U.S. EPA Region 7
HGL—Source Area ISCO Evaluation Report—Cleburn Street Well SiteGrand Island, Nebraska
Legend
!H Permanganate Injection Wells
HGL—Source Area ISCO Evaluation, Cleburn Street Well Site—Grand Island, Nebraska
U.S. EPA Region 7 Source Area ISCO Evaluation 4-1 November 2010
4.0 GROUNDWATER MONITORING AND EVALUATION
A pre-injection baseline monitoring event was conducted in December 2009 to establish pre-injection contaminant concentrations within and downgradient of the injection area. The first KMnO4 injection was conducted from December 16 through December 22, 2009, followed by groundwater monitoring events at 4 weeks and 10 weeks. The second KMnO4 injection was conducted from March 8 through March 11 followed by groundwater monitoring events at 4 weeks, 8 weeks, and 20 weeks after oxidant injection. Other than the baseline monitoring event, groundwater samples were collected from 20 monitoring wells located within and downgradient of the injection zone in accordance with procedures described in the SAP Addendum (HGL, 2009b). The four DPE injection wells were not sampled for the baseline sampling event. The wells sampled for the TS cover multiple depth intervals as follows:
• 17 feet to 32 feet bgs – MW-2A and MW-12A • 19 feet to 29 feet bgs – ERT-14, ERT-15, and ERT-16 • 22 feet to 32 feet bgs – IW-1 through IW-10 (Both IWs and MWs) • 31 feet to 36 feet bgs – DPE-1, DPE-2, DPE-3, and DPE-4 (Both IWs and MWs) • 79 feet to 89 feet bgs – MW-2B
The well locations are shown on Figure 4.1.
4.1 IDENTIFICATION OF WELLS AFFECTED BY OXIDANT
Because KMnO4 is readily identifiable in groundwater samples by its pink-to-purple tint, visual inspection of the samples usually proves to be an excellent indicator along with the presence of specific metals. The discussion in this section focuses on the wells (other than injection wells) known to be affected by KMnO4. Based on the purple coloration and analytical data indicating elevated levels of manganese (found in KMnO4), the following wells were identified as locations affected by the KMnO4 injections:
• MW-2A • ERT-15 • ERT-16
Metals were analyzed in groundwater to gauge the effect the KMnO4 had on the aquifer materials (whether metals were mobilized as a result of injection), and what effect metal impurities contained in the KMnO4 injectant had on groundwater quality. The discussion below focuses on manganese, which is associated with KMnO4, and metals considered toxic (arsenic, chromium, and cadmium). Metals analytical data is presented in Table 4.1. Analytical reports are included in Appendix E.
HGL—Source Area ISCO Evaluation, Cleburn Street Well Site—Grand Island, NE
U.S. EPA Region 7 Source Area ISCO Evaluation 4-2 November 2010
Arsenic was not detected above the reporting limit of 25 µg/L (MCL for arsenic is 10 µg/L) in pre-injection (baseline) samples. During the entire post-injection monitoring period, arsenic was not detected at a concentration above the reporting limit, though the reporting limit ranged from 25 µg/L to 25,000 µg/L in the post-injection monitoring period. Reporting limits increased for all of the metals results due to elevated manganese concentrations from the injected KMnO4.
Arsenic
Chromium was detected in the pre-injection (baseline) sample from ERT-15 at 16 µg/L. This is below the MCL of 100 µg/L for total chromium.
Chromium
For the post-injection monitoring, chromium was detected in samples collected from all three monitoring wells affected by KMnO4. The general trend for these wells was for chromium concentrations to increase through the March post-injection sampling, then gradually decrease in the April, May, and July events. In ERT-15, total chromium peaked at 177 µg/L in March 2010 and decreased to 51 µg/L in May 2010. In ERT-16, total chromium peaked at 11,000 µg/L in March and decreased to 4,030 µg/L in May. In MW-2A, total chromium peaked at 14,500 µg/L in March and decreased to 4,030 µg/L in July 2010. In both ERT-16 and MW-2A, the levels still exceed the MCL and will need to be monitored in subsequent quarterly sampling events. An increase in chromium followed by a decrease is expected in wells influenced by KMnO4
injectant, due to precipitation of metals and mixing with groundwater not affected by KMnO4.
A high concentration of manganese is an indication that a well was directly affected by the KMnO4 injections. Very high concentrations of manganese were identified in MW-2A, ERT-16 and ERT-15. As a component of the injected KMnO4, the levels increased the most in January and April 2010, the first monitoring event after each injection. In MW-2A and ERT-15, the concentration increased from baseline levels of less than 10 µg/L for both wells to 417,000 µg/L in MW-2A and 325,000 µg/L in ERT-15 in April. There is no MCL for manganese. It is anticipated that high manganese concentrations will continue to decrease in the immediate area of the KMnO4 injections.
Manganese
Much lower levels of manganese were identified in MW-12A, ERT-14, and MW-2B. Only MW-2B appears to have been impacted by the KMnO4 injections. The manganese concentration rose from 5U in the baseline sample to 71 µg/L in March 2010. It has continued to drop in subsequent sampling events.
It should also be noted that cadmium was detected in IW-08 in the July 2010 sampling event. Data indicate it was detected at 3,860 µg/L, which is significantly above the MCL of 5 µg/L. However the duplicate sample for this event did not have a detection for cadmium (3,000 U). In addition, cadmium has not been detected in IW-08 or any of the other monitoring well locations throughout the post-injection monitoring period. Continued monitoring should be conducted for
Cadmium
HGL—Source Area ISCO Evaluation, Cleburn Street Well Site—Grand Island, NE
U.S. EPA Region 7 Source Area ISCO Evaluation 4-3 November 2010
cadmium to verify that this result is anamolous.
4.2 VOLATILE ORGANIC COMPOUNDS
For the VOC discussion, the 20 injection and monitoring wells sampled for the post-injection performance monitoring will be referred to collectively as monitoring wells. VOC results will be evaluated in all of the monitoring wells. VOCs of interest detected in groundwater samples from the MWs include PCE, and the degradation products TCE and cis-1,2-DCE. Other degradation products of TCE such as trans-1,2-DCE and vinyl chloride were not detected in groundwater samples. Carbon tetrachloride and its degradation product chloroform also were identified in several of the groundwater samples. The six analytical data packages for the entire study from December 2009 through July 2010 are included in Appendix E.
PCE was detected in all 16 of the wells sampled wells during the baseline event; however, levels were significantly variable from 5.2 µg/L in IW-01 on the western portion of the injection area to 140,000 µg/L in IW-09, approximately 40 feet to the northeast (Figure 4.2). The baseline data show that PCE concentrations generally increase from the southwest portion of the injection area to the northeast.
PCE
After the injections, PCE concentrations decreased in most of the wells impacted by KMnO4. In the first post-injection monitoring event in January 2010, many of the samples dropped to below the PCE reporting limit of 5 µg/L, although PCE was detected in six of the 20 samples at levels ranging from 11 µg/L in ERT-14 to 3,900 J in MW-2A (Figure 4.3). PCE concentrations remained much lower than the baseline data in the monitoring wells after the second injection event, but levels began to increase in the July 2010 sampling event. This was likely due to both the KMnO4 being consumed and dilution as it mixed with groundwater in the months after the final injection. The number of wells with detections of PCE rose from six in January to twelve in July. Concentrations ranged from 20 µg/L to 7,500 µg/L (Figure 4.4). In general, the PCE concentrations remained well below the baseline concentrations displayed on Figure 4.2. PCE concentrations in MW-2A are representative of the trend that occurred in the wells impacted by the KMnO4. Figure 4.5 displays the drop in PCE concentration in MW-2A after the first and second injections and the slow rise in PCE that began 4 months after the last injection. PCE concentrations in MW-12A are indicative of a cross-gradient monitoring well not impacted by the KMnO4. It is likely that PCE concentrations began to rise in MW-12A because contamination was pushed horizontally outward from the injection zone. The trend graph in Figure 4.6 shows PCE increases after each injection event, followed by a drop as natural easterly groundwater flow resumes when not influenced by injection pressure.
TCE was detected in five monitoring wells (IW-7 through IW-10, MW-2A) in the baseline event at levels ranging from 12 µg/L to 40 µg/L; all of which were above the MCL of 5 µg/L, but still significantly lower than the PCE concentrations in groundwater. TCE was not detected in any of
TCE
HGL—Source Area ISCO Evaluation, Cleburn Street Well Site—Grand Island, NE
U.S. EPA Region 7 Source Area ISCO Evaluation 4-4 November 2010
the wells affected by KMnO4. Of the wells not affected by KMnO4, only MW-12A contained TCE. The TCE levels fluctuated from 150 µg/L to 370 µg/L in MW-12A during the course of the TS. Similar to PCE, it appears that the TCE levels in this well may have increased as a result of the injections (Figure 4.7).
All detections of cis-1,2-DCE (a degradation product of TCE) were in samples from MW-12A, a MW that was not impacted by the source area injections. The cis-1,2-DCE was present in the baseline sampling event at 23 µg/L and fluctuated between 5.0 U and 22 µg/L in the post-injection events. All of the results were below the MCL for cis-1,2-DCE of 70 µg/L.
Cis-1,2-DCE
Carbon tetrachloride (CCl4) was not detected in any of the monitoring wells sampled during the baseline event. In the first post-injection sampling in January 2010, 12 of the 20 MWs had detections of CCl4 ranging from 21 µg/L in IW-08 to 1,200 µg/L in MW-2A. These detections are above the MCL for CCl4 of 5 µg/L. Based on this information, it appears the KMnO4 injections mobilized CCl4 that was bound in the silty material. In general, CCl4 concentrations peaked in the April 2010 post-injection sampling event, then began to trend downward. However, in the final sampling event in July 2010, 10 wells still had detections that exceeded the MCL, with concentrations ranging from 40 µg/L in IW-05 to 1,200 µg/L in ERT-16.
Carbon Tetrachloride
Chloroform, a degradation product of CCl4, was not detected in the monitoring wells sampled during the baseline event, but was detected after the two injection events. As with CCl4, chloroform was likely mobilized from the soil matrix by the KMnO4 injections. Chloroform was identified in 11 of the 20 wells sampled with detections ranging from 6 µg/L to 510 µg/L. There is no established MCL for chloroform but the MCL for total trihalomethanes, which includes chloroform, is 80 µg/L. In the final sampling event for the study in July 2010, 9 of the 20 wells had detections of chloroform and 8 of those detections were above 80 µg/L.
Chloroform
CCl4 and chloroform have not been identified in any of the downgradient monitoring wells sampled for the quarterly sitewide sampling.
TABLE(S)
Table 4.1Metals Analytical Results
ISCO Injection and Remedial Investigation - Cleburn Street Well SiteGrand Island, NE
Monitoring Well IDSampling Date Dec-09 Jan-10 Mar-10 Apr-10 May-10 Dec-09 Jan-10 Apr-10 May-10 Jul-10
Sample ID 4717-1 4758-7 4818-1 4846-2 4889-2 4981-4 4981-4-FD 4717-2 4758-5 4818-2 4818-2-FD 4846-4 4889-3 4981-3Coloration Clear Purple Purple Purple Purple Clear Purple Purple Purple Purple Purple Purple
Conductivity uS/cm NE 1300 8970 3110 9070 6990 2300 2300 1270 8000 3960 3960 8670 6750 2500Dissolved Oxygen mg/L NE 6.2 0.73 8.92 4.44 5.72 4.3 4.3 5.34 1.17 7.2 7.2 4.33 6.06 4.84
pH SU NE 6.91 7.57 7.26 7.72 7.52 7.46 7.46 7.12 7.25 7.26 7.26 7.53 7.32 7.15Temperature °C NE 13.86 13.91 11.72 13.66 14.52 26.57 26.57 13.42 14.6 11.74 11.74 13.38 14.55 25.62
Turbidity NTU NE 1.2 1.2 1.6 0 5.2 49 49 0 3.2 4.2 4.2 0 2 0
Alkalinity, total mg/L NE 117 236 218 226 210 188 188 142 227 202 202 230 225 194 Sulfate mg/L NE 194 10000 U 10000 U 10000 U 10000 U 10000 U 10000 U 181 10000 U 10000 U 10000 U 10000 U 10000 U 10000 U
Hardness (as CaCO3) mg/L NE 346 13200 U 1370 1320 U 1320 U 1300 U 1300 U 304 13200 U 1320 U 1320 U 1320 U 1320 U 1300 UTotal Dissolved Solids mg/L NE 738 11400 6150 15200 8300 736 2390 742 10300 6450 6450 12900 8030 2830 Total Organic Carbon mg/L NE 1.4 7.2 1.27 J 1.5 NA NA NA 1.2 11.1 1.89 1.71 1.51 NA NA
Aluminum ug/L NE 50 U 50000 U 5000 U 5000 U 5000 U 5000 U 5000 U 50 U 50000 U 5000 U 5000 U 5000 U 5000 U 5000 UAntimony ug/L 6 50 U 50000 U 5000 U 5000 U 5000 U 5000 U 5000 U 50 U 50000 U 5000 U 5000 U 5000 U 5000 U 5000 UArsenic ug/L 10 25 U 25000 U 2500 U 2500 U 2500 U 2500 U 2500 U 25 U 25000 U 2500 U 2500 U 2500 U 2500 U 2500 UBarium ug/L 2000 106 10000 U 1000 U 1000 U 1000 U 1000 U 1000 U 92 10000 U 1000 U 1000 U 1000 U 1000 U 1000 U
Beryllium ug/L 4 3 U 3000 U 300 U 300 U 300 U 300 U 300 U 3 U 3000 U 300 U 300 U 300 U 300 U 300 UCadmium ug/L 5 3 U 3000 U 300 U 300 U 300 U 300 U 300 U 3 U 3000 U 300 U 300 U 300 U 300 U 300 UCalcium mg/L NE 97.9 2000 U 218 200 U 200 U 200 U 200 U 86.2 2000 U 200 U 200 U 200 U 200 U 200 U
Chromium ug/L 100 15 U 15000 U 1500 U 1500 U 1500 U 1500 U 1500 U 15 U 15000 U 1500 U 1500 U 1500 U 1500 U 1500 UCobalt ug/L NE 10 U 10000 U 1000 U 1000 U 1000 U 1000 U 1000 U 10 U 10000 U 1000 U 1000 U 1000 U 1000 U 1000 UCopper ug/L 1300 5 U 5000 U 500 U 500 U 500 U 500 U 500 U 5 U 5000 U 500 U 500 U 500 U 500 U 500 U
Iron ug/L NE 50 U 50000 U 5000 U 5000 U 5000 U 5000 U 5000 U 50 U 50000 U 5000 U 5000 U 5000 U 5000 U 5000 ULead ug/L 15 50 U 50000 U 5000 U 5000 U 5000 U 5000 U 5000 U 50 U 50000 U 5000 U 5000 U 5000 U 5000 U 5000 U
Magnesium mg/L NE 24.6 2000 U 200 U 200 U 200 U 200 U 200 U 21.6 2000 U 200 U 200 U 200 U 200 U 200 UManganese ug/L NE 21 285000 364000 354000 393000 351000 282000 12 319000 370000 361000 232000 371000 321000
Molybdenum ug/L NE 15 U 15000 U 1500 U 1500 U 1500 U 1500 U 1500 U 15 U 15000 U 1500 U 1500 U 1500 U 1500 U 1500 UNickel ug/L NE 20 U 20000 U 2000 U 2000 U 2000 U 2000 U 2000 U 20 U 20000 U 2000 U 2000 U 2000 U 2000 U 2000 U
Potassium mg/L NE 17.1 2000 U 1210 2670 1660 736 598 13.1 2000 U 1280 1170 2010 1500 642 Selenium ug/L 50 50 U 50000 U 5000 U 5000 U 5000 U 5000 U 5000 U 50 U 50000 U 5000 U 5000 U 5000 U 5000 U 5000 U
Silver ug/L NE 25 U 25000 U 2500 U 2500 U 2500 U 2500 U 2500 U 25 U 25000 U 2500 U 2500 U 2500 U 2500 U 2500 USodium mg/L NE 102 5000 U 500 U 500 U 500 U 500 U 500 U 118 5000 U 500 U 500 U 500 U 500 U 500 UThallium ug/L 2 50 U 50000 U 5000 U 5000 U 5000 U 5000 U 5000 U 50 U 50000 U 5000 U 5000 U 5000 U 5000 U 5000 UTitanium ug/L NE 20 U 20000 U 2000 U 2000 U 2000 U 2000 U 2000 U 20 U 20000 U 2000 U 2000 U 2000 U 2000 U 2000 UVanadium ug/L NE 10 U 10000 U 1000 U 1000 U 1000 U 1000 U 1000 U 10 U 10000 U 1000 U 1000 U 1000 U 1000 U 1000 U
Zinc ug/L NE 25 U 25000 U 2500 U 2500 U 2500 U 4500 2500 U 25 U 25000 U 2500 U 2500 U 2500 U 2500 U 2500 U
Units MCL
PurpleField Parameters
IW-1Jul-10
Geochemical Parameters
Total Metals
Mar-10IW-2
Cleburn RI Report Page 1 of 7 HydroGeoLogic, Inc. 11/12/2010
Table 4.1Metals Analytical Results
ISCO Injection and Remedial Investigation - Cleburn Street Well SiteGrand Island, NE
Monitoring Well IDSampling Date
Sample IDColoration
Conductivity uS/cm NEDissolved Oxygen mg/L NE
pH SU NETemperature °C NE
Turbidity NTU NE
Alkalinity, total mg/L NESulfate mg/L NE
Hardness (as CaCO3) mg/L NETotal Dissolved Solids mg/L NETotal Organic Carbon mg/L NE
Aluminum ug/L NEAntimony ug/L 6Arsenic ug/L 10Barium ug/L 2000
Beryllium ug/L 4Cadmium ug/L 5Calcium mg/L NE
Chromium ug/L 100Cobalt ug/L NECopper ug/L 1300
Iron ug/L NELead ug/L 15
Magnesium mg/L NEManganese ug/L NE
Molybdenum ug/L NENickel ug/L NE
Potassium mg/L NESelenium ug/L 50
Silver ug/L NESodium mg/L NEThallium ug/L 2Titanium ug/L NEVanadium ug/L NE
Zinc ug/L NE
Units MCL
Field Parameters
Geochemical Parameters
Total Metals
Dec-09 Mar-10 Dec-09 Jan-10 Mar-10 Apr-10 May-10 Jul-10 Dec-09 Jan-10 Mar-10 Apr-10 May-10 Jul-104717-3 4758-4 4758-4-FD 4818-4 4846-5 4846-5-FD 4889-4 4889-4-FD 4981-10 4981-10-FD 4717-5 4758-6 4818-5 4846-6 4889-5 4981-5 4717-4 4758-1 4818-6 4846-7 4889-6 4981-6Clear Purple Clear Purple Purple Purple Purple Purple Clear Purple Purple Purple Purple Purple
1180 6060 6060 4590 8250 8250 8100 8100 3920 3920 1140 6270 5360 8920 9210 4920 1480 8310 1630 9470 8270 23504.4 4.1 4.1 9.63 3.42 3.42 5.15 5.15 4.82 4.82 2.67 2.35 8.56 3.43 4.98 6.47 2.54 1.22 5.02 2.76 7.94 8.857.23 7.47 7.47 7.56 7.54 7.54 7.55 7.55 7.57 7.57 6.94 7.27 7.33 6.58 6.57 7.28 6.98 5.82 6.01 5.9 6.03 6.9613.31 13.65 13.65 12.03 12.78 12.78 14.68 14.68 28 28 12.08 13.95 11.83 12.73 14.6 25.84 13.24 10.66 11.97 12.11 14.27 25
0 0 0 3.9 0 0 3.6 3.6 0 0 0 0 3.4 0 1.6 0 0.2 11.6 56.4 1.2 2.2 31.8
162 281 283 259 288 285 256 259 248 248 156 255 289 329 317 239 130 180 139 299 138 208 213 10000 U 10000 U 10000 U 10000 U 10000 U 10000 U 10000 U 10000 U 10000 U 221 10000 U 10000 U 10000 U 10000 U 10000 U 169 10000U 10000 U 10000 U 10000 U 10000 U256 13200 U 13200 U 1320 U 1320 U 1320 U 1320 U 1320 U 13000 U 13000 U 275 13200 U 1320 U 1320 U 1320 U 13000 U 361 13200 U 1320 U 1620 1320 U 1300 U692 7400 7330 7060 12800 12600 10200 9470 4840 4820 712 7610 8280 14000 11900 6440 856 8540 4730 14100 9660 2250 1.4 9 9 1.63 1.73 1.69 NA NA NA NA 1.5 8.9 1.54 1.68 NA NA 2.1 9.6 1 U 2.29 NA NA
50 U 50000 U 50000 U 5000 U 5000 U 5000 U 5000 U 5000 U 50000 U 50000 U 50 U 50000 U 5000 U 5000 U 5000 U 50000 U 50 U 50000 U 5000 U 5000 U 5000 U 5000 U50 U 50000 U 50000 U 5000 U 5000 U 5000 U 5000 U 5000 U 50000 U 50000 U 50 U 50000 U 5000 U 5000 U 5000 U 50000 U 50 U 50000 U 5000 U 5000 U 5000 U 5000 U25 U 25000 U 19600 2500 U 2500 U 2500 U 2500 U 2500 U 25000 U 25000 U 25 U 25000 U 2500 U 2500 U 2500 U 25000 U 25 U 25000 U 2500 U 2500 U 2500 U 2500 U69 10000 U 10000 U 1000 U 1000 U 1000 U 1000 U 1000 U 10000 U 10000 U 83 10000 U 1000 U 1000 U 1000 U 10000 U 90 10000 U 1000 U 1000 U 1000 U 1000 U3 U 3000 U 3000 U 300 U 300 U 300 U 300 U 300 U 3000 U 3000 U 3 U 3000 U 300 U 300 U 300 U 3000 U 3 U 3000 U 300 U 300 U 300 U 300 U3 U 3000 U 3000 U 300 U 300 U 300 U 300 U 300 U 3000 U 3000 U 3 U 3000 U 300 U 300 U 300 U 3000 U 3 U 3000 U 300 U 300 U 300 U 300 U73.3 2000 U 2000 U 200 U 200 U 200 U 200 U 200 U 2000 U 2000 U 78.4 2000 U 200 U 200 U 200 U 2000 U 103 2000 U 200 U 318 200 U 200 U15 U 15000 U 15000 U 1500 U 1500 U 1500 U 1500 U 1500 U 15000 U 15000 U 15 U 15000 U 1500 U 1500 U 1500 U 15000 U 15 U 15000 U 1500 U 1500 U 1500 U 1500 U10 U 10000 U 10000 U 1000 U 1000 U 1000 U 1000 U 1000 U 10000 U 10000 U 10 U 10000 U 1000 U 1000 U 1000 U 10000 U 10 U 10000 U 1000 U 1000 U 1000 U 1000 U5 U 5000 U 5000 U 500 U 500 U 500 U 500 U 500 U 5000 U 5000 U 5 U 5000 U 500 U 500 U 500 U 5000 U 5 U 5000 U 500 U 500 U 500 U 500 U50 U 50000 U 50000 U 5000 U 5000 U 5000 U 5000 U 5000 U 50000 U 50000 U 50 U 50000 U 5000 U 5000 U 5000 U 50000 U 51 50000 U 5000 U 5000 U 5000 U 5000 U50 U 50000 U 50000 U 5000 U 5000 U 5000 U 5000 U 5000 U 50000 U 50000 U 50 U 50000 U 5000 U 5000 U 5000 U 50000 U 50 U 50000 U 5000 U 5000 U 5000 U 5000 U17.6 2000 U 2000 U 200 U 200 U 200 U 200 U 200 U 2000 U 2000 U 19.3 2000 U 200 U 200 U 200 U 2000 U 25.2 2000 U 200 U 200 U 200 U 200 U35 301000 214000 332000 331000 393000 316000 354000 397000 398000 18 347000 420000 297000 304000 371000 20 291000 349000 387000 305000 214000
15 U 15000 U 15000 U 1500 U 1500 U 1500 U 1500 U 1500 U 15000 U 15000 U 15 U 15000 U 1500 U 1500 U 1500 U 15000 U 15 U 7500 U 1500 U 1500 U 1500 U 1500 U20 U 20000 U 20000 U 2000 U 2000 U 2000 U 2000 U 2000 U 20000 U 20000 U 20 U 20000 U 2000 U 2000 U 2000 U 20000 U 20 U 20000 U 2000 U 2000 U 2000 U 2000 U11.3 2000 U 2000 U 1140 2440 2430 1820 1790 2000 U 2000 U 13.4 2000 U 1590 2420 2200 2000 U 13.5 2000 U 773 2690 1970 608 50 U 50000 U 50000 U 5000 U 5000 U 5000 U 5000 U 5000 U 50000 U 50000 U 50 U 50000 U 5000 U 5000 U 5000 U 50000 U 50 U 50000 U 5000 U 5000 U 5000 U 5000 U25 U 25000 U 25000 U 2500 U 2500 U 2500 U 2500 U 2500 U 25000 U 25000 U 25 U 25000 U 2500 U 2500 U 2500 U 25000 U 25 U 25000 U 2500 U 2500 U 2500 U 2500 U112 5000 U 5000 U 500 U 500 U 500 U 500 U 500 U 5000 U 5000 U 123 5000 U 500 U 500 U 500 U 5000 U 164 5000 U 500 U 500 U 500 U 500 U50 U 50000 U 50000 U 5000 U 5000 U 5000 U 5000 U 5000 U 50000 U 50000 U 50 U 50000 U 5000 U 5000 U 5000 U 50000 U 50 U 50000 U 5000 U 5000 U 5000 U 5000 U20 U 20000 U 20000 U 2000 U 2000 U 2000 U 2000 U 2000 U 20000 U 20000 U 20 U 20000 U 2000 U 2000 U 2000 U 20000 U 20 U 20000 U 2000 U 2000 U 2000 U 2000 U10 U 10000 U 10000 U 1000 U 1000 U 1000 U 1000 U 1000 U 10000 U 10000 U 10 U 10000 U 1000 U 1000 U 1000 U 10000 U 10 U 10000 U 1000 U 1000 U 1000 U 1000 U25 U 25000 U 25000 U 2500 U 2500 U 2500 U 2500 U 2500 U 25000 U 25000 U 25 U 25000 U 2500 U 2500 U 2500 U 25000 U 25 U 25000 U 2500 U 2500 U 2500 U 2500 U
Purple Purple
Jan-10 May-10Apr-10IW-3
Jul-10IW-04 IW-05
PurplePurple
Cleburn RI Report Page 2 of 7 HydroGeoLogic, Inc. 11/12/2010
Table 4.1Metals Analytical Results
ISCO Injection and Remedial Investigation - Cleburn Street Well SiteGrand Island, NE
Monitoring Well IDSampling Date
Sample IDColoration
Conductivity uS/cm NEDissolved Oxygen mg/L NE
pH SU NETemperature °C NE
Turbidity NTU NE
Alkalinity, total mg/L NESulfate mg/L NE
Hardness (as CaCO3) mg/L NETotal Dissolved Solids mg/L NETotal Organic Carbon mg/L NE
Aluminum ug/L NEAntimony ug/L 6Arsenic ug/L 10Barium ug/L 2000
Beryllium ug/L 4Cadmium ug/L 5Calcium mg/L NE
Chromium ug/L 100Cobalt ug/L NECopper ug/L 1300
Iron ug/L NELead ug/L 15
Magnesium mg/L NEManganese ug/L NE
Molybdenum ug/L NENickel ug/L NE
Potassium mg/L NESelenium ug/L 50
Silver ug/L NESodium mg/L NEThallium ug/L 2Titanium ug/L NEVanadium ug/L NE
Zinc ug/L NE
Units MCL
Field Parameters
Geochemical Parameters
Total Metals
Dec-09 Jan-10 Mar-10 Apr-10 May-10 Jul-10 Dec-09 Jan-10 Mar-10 Apr-10 May-10 Jul-10 Dec-09 Jan-10 Mar-104717-6 4758-2 4818-8 4846-8 4889-7 4981-7 4717-9 4758-3 4818-9 4846-9 4889-8 4981-8 4717-14 4758-9 4818-10 4846-12 4846-12-FD 4889-10 4889-10-FD 4981-22 4981-22-FDClear Purple Purple Purple Purple Purple Clear Purple Purple Purple Purple Purple Clear Purple Purple
1090 7710 6250 6900 7680 5850 1520 8390 7720 9520 10400 986 1460 6590 4300 9010 9010 5960 5960 4150 41501.77 0 2.9 2.38 2.55 3.18 4.66 0 0 1.23 1.23 3.09 4.28 7.29 17.56 10.78 10.78 8.6 8.6 23.82 23.826.9 6.08 5.82 5.75 5.65 6 7.19 3.4 3.58 2.26 2.45 4 6.91 7.06 6.4 7.35 7.35 6.82 6.82 5.97 5.97
12.56 12.24 12 12.63 16.11 28.18 10.61 10.12 9.49 11.38 17.81 31.03 10.37 14.04 11.83 12.47 12.47 15.66 15.66 24.52 24.521.5 4.7 2.1 0 3.1 15.2 1.4 72.9 38.9 9.2 134 77 0 0 0 0 0 0 0 5 5
142 269 156 202 203 227 154 4 U 2 U 2 U 2.00 U 2.00 U 139 314 271 260 263 273 271 127 126 209 10000 U 10000 U 10000 U 10000 U 10000 U 259 10000 U 10000 U 10000 U 10000 U 10000 U 246 10000 U 10000 U 10000 U 10000 U 10000 U 10000 U 10000 U 10000 U307 13200 U 2040 1600 2190 13000 U 395 13200 U 1870 1540 1620 13000 U 347 13200 U 1320 U 1320 U 1320 U 1320 U 1320 U 13000 U 13000 U708 8410 6840 10100 8210 7450 900 6610 8340 11000 9900 7920 888 8280 3670 12100 12600 6080 6620 3830 2300 1.5 15.2 1.21 1.96 NA NA 2.5 20.2 2.1 J 2.1 NA NA 1.8 13.4 2.02 J 3 U 3 U NA NA NA NA
117 50000 U 5000 U 5000 U 5000 U 50000 U 50 U 50000 U 40600 36200 43100 58100 50 U 50000 U 5000 U 5000 U 5000 U 5000 U 5000 U 50000 U 50000 U50 U 50000 U 5000 U 5000 U 5000 U 50000 U 50 U 50000 U 5000 U 5000 U 5000 U 50000 U 50 U 50000 U 5000 U 5000 U 5000 U 5000 U 5000 U 50000 U 50000 U25 U 25000 U 2500 U 2500 U 2500 U 25000 U 25 U 25000 U 2500 U 2500 U 2500 U 25000 U 25 U 25000 U 2500 U 2500 U 2500 U 2500 U 2500 U 25000 U 25000 U70 10000 U 1000 U 1000 U 1000 U 10000 U 94 10000 U 1000 U 1000 U 1000 U 10000 U 92 10000 U 1000 U 1000 U 1000 U 1000 U 1000 U 10000 U 10000 U3 U 3000 U 300 U 300 U 300 U 3000 U 3 U 3000 U 300 U 300 U 300 U 3000 U 3 U 3000 U 300 U 300 U 300 U 300 U 300 U 3000 U 3000 U3 U 3000 U 300 U 300 U 300 U 3000 U 3 U 3000 U 300 U 300 U 300 U 3000 U 3 U 3000 U 300 U 300 U 300 U 300 U 300 U 3860 3000 U87.8 2000 U 487 310 547 2000 U 113 2000 U 419 287 319 2000 U 99 2000 U 200 U 200 U 200 U 200 U 200 U 2000 U 2000 U15 U 15000 U 1500 U 1500 U 1500 U 15000 U 15 U 15000 U 1500 U 1500 U 1500 U 15000 U 15 U 15000 U 1500 U 1500 U 1500 U 1500 U 1500 U 15000 U 15000 U10 U 10000 U 1000 U 1000 U 1000 U 10000 U 10 U 10000 U 1000 U 1000 U 1000 U 10000 U 10 U 10000 U 1000 U 1000 U 1000 U 1000 U 1000 U 10000 U 10000 U5 U 5000 U 500 U 500 U 500 U 5000 U 5 U 5000 U 500 U 500 U 500 U 5000 U 5 U 5000 U 500 U 500 U 500 U 500 U 500 U 5000 U 5000 U116 50000 U 5000 U 5000 U 5000 U 50000 U 50 U 50000 U 5000 U 5000 U 5000 U 50000 U 50 U 50000 U 5000 U 5000 U 5000 U 5000 U 5000 U 50000 U 50000 U50 U 50000 U 5000 U 5000 U 5000 U 50000 U 50 U 50000 U 5000 U 5000 U 5000 U 50000 U 50 U 50000 U 5000 U 5000 U 5000 U 5000 U 5000 U 50000 U 50000 U21.3 2000 U 200 U 200 U 200 U 2000 U 27.4 2000 U 200 U 200 U 200 U 2000 U 24.3 2000 U 200 U 200 U 200 U 200 U 200 U 2000 U 2000 U30 362000 402000 449000 383000 420000 54 341000 344000 451000 417000 398000 27 422000 312000 295000 262000 265000 349000 355000 353000
15 U 15000 U 1500 U 1500 U 1500 U 15000 U 15 U 15000 U 1500 U 1500 U 1500 U 15000 U 15 U 15000 U 1500 U 1500 U 1500 U 1500 U 1500 U 15000 U 15000 U20 U 20000 U 2000 U 2000 U 2000 U 20000 U 23 20000 U 2000 U 2000 U 2000 U 20000 U 20 U 20000 U 2000 U 2000 U 2000 U 2000 U 2000 U 20000 U 20000 U11.8 2000 U 664 1660 1170 2000 U 14.4 2000 U 928 2080 1740 2000 U 14.1 2000 U 865 2460 2350 1160 1440 2000 U 2000 U50 U 50000 U 5000 U 5000 U 5000 U 50000 U 50 U 50000 U 5000 U 5000 U 5000 U 50000 U 50 U 50000 U 5000 U 5000 U 5000 U 5000 U 5000 U 50000 U 50000 U25 U 25000 U 2500 U 2500 U 2500 U 25000 U 25 U 25000 U 2500 U 2500 U 2500 U 25000 U 25 U 25000 U 2500 U 2500 U 2500 U 2500 U 2500 U 25000 U 25000 U97.7 5000 U 500 U 500 U 500 U 5000 U 154 5000 U 500 U 500 U 500 U 5000 U 154 5000 U 500 U 500 U 500 U 500 U 500 U 5000 U 5000 U50 U 50000 U 5000 U 5000 U 5000 U 50000 U 50 U 50000 U 5000 U 5000 U 5000 U 50000 U 50 U 50000 U 5000 U 5000 U 5000 U 5000 U 5000 U 50000 U 50000 U20 U 20000 U 2000 U 2000 U 2000 U 20000 U 20 U 20000 U 2000 U 2000 U 2000 U 20000 U 20 U 20000 U 2000 U 2000 U 2000 U 2000 U 2000 U 20000 U 20000 U10 U 10000 U 1000 U 1000 U 1000 U 10000 U 10 U 10000 U 1000 U 1000 U 1000 U 10000 U 10 U 10000 U 1000 U 1000 U 1000 U 1000 U 1000 U 10000 U 10000 U25 U 25000 U 2500 U 2500 U 2500 U 25000 U 25 U 25000 U 2500 U 2500 U 2500 U 25000 U 25 U 25000 U 2500 U 2500 U 2500 U 2500 U 2500 U 25000 U 25000 U
Jul-10May-10Apr-10IW-06 IW-7 IW-08
PurplePurplePurple
Cleburn RI Report Page 3 of 7 HydroGeoLogic, Inc. 11/12/2010
Table 4.1Metals Analytical Results
ISCO Injection and Remedial Investigation - Cleburn Street Well SiteGrand Island, NE
Monitoring Well IDSampling Date
Sample IDColoration
Conductivity uS/cm NEDissolved Oxygen mg/L NE
pH SU NETemperature °C NE
Turbidity NTU NE
Alkalinity, total mg/L NESulfate mg/L NE
Hardness (as CaCO3) mg/L NETotal Dissolved Solids mg/L NETotal Organic Carbon mg/L NE
Aluminum ug/L NEAntimony ug/L 6Arsenic ug/L 10Barium ug/L 2000
Beryllium ug/L 4Cadmium ug/L 5Calcium mg/L NE
Chromium ug/L 100Cobalt ug/L NECopper ug/L 1300
Iron ug/L NELead ug/L 15
Magnesium mg/L NEManganese ug/L NE
Molybdenum ug/L NENickel ug/L NE
Potassium mg/L NESelenium ug/L 50
Silver ug/L NESodium mg/L NEThallium ug/L 2Titanium ug/L NEVanadium ug/L NE
Zinc ug/L NE
Units MCL
Field Parameters
Geochemical Parameters
Total Metals
Dec-09 Jan-10 Mar-10 Apr-10 May-10 Jul-10 Dec-09 Apr-10 May-10 Jul-10 Jan-10 Mar-10 Jul-104717-17 4758-11 4818-11 4846-11 4889-11 4981-9 4717-16 4758-10 4758-10-FD 4818-12 4818-12-FD 4846-14 4889-12 4981-11 4717-11 4717-11-FD 4758-15 4818-23 4846-17 4846-17-FD 4889-20 4889-20-FD 4981-1Clear Purple Purple Purple Purple Purple Clear Purple Purple Purple Clear Clear Clear
1760 8930 8040 8580 10000 4210 1690 6850 6850 6240 6240 9270 9020 5160 1450 1450 1240 1020 805 805 971 971 3901.02 0.19 27.24 5.86 6.33 8.37 1.89 2.95 2.95 5.72 5.72 13.44 6.22 5.94 6.2 6.2 0.52 5.61 6.9 6.9 4.4 4.4 4.216.93 5.67 4.85 6.07 5.88 5.14 6.89 5.92 5.92 5.72 5.72 6.91 6.67 6.04 6.66 6.66 6.43 6.68 6.69 6.69 7.01 7.01 6.6222.66 12.35 10.23 11.57 16.55 26.5 9.84 12.07 12.07 10.53 10.53 11.8 15.09 25.25 14.49 14.49 16.71 15.44 14.87 14.87 15.38 15.38 25.773.5 12.7 80.3 0 39.5 16.5 0 37.4 37.4 3 3 0 0.1 2.5 0 0 2 20.3 0 0 0 0 0
134 186 42.4 309 166 13.8 136 352 351 192 193 249 288 164 88.9 89 40.6 75.6 69.9 69.2 78.2 77.7 57.5 267 10000 U 10000 U 10000 U 10000 U 10000 U 275 10000 U 10000 U 10000 U 10000 U 10000 U 10000 U 10000 U 139 148 168 101 81.5 81.8 92.8 106 45.3 448 13200 U 2050 1350 2040 1400 386 13200 U 13200 U 1320 U 1320 U 1320 U 1370 13000 U 397 420 319 293 245 228 293 285 111 1060 9880 7390 11300 10500 4210 1020 7270 7300 5540 5540 11900 10600 5500 928 926 805 664 553 J 525 680 680 271 2.6 15.2 1.95 3 U NA NA 2.6 12.2 12.2 1.63 1.64 3 U NA NA 1.2 1.4 2 1.8 3 U 3 U NA NA NA
50 U 50000 U 9730 5000 U 5000 U 8920 50 U 50000 U 50000 U 5000 U 5000 U 5000 U 5000 U 50000 U 60 65 500 U 50 U 77 50 U 50 U 50 U 54 50 U 50000 U 5000 U 5000 U 5000 U 5000 U 50 U 50000 U 50000 U 5000 U 5000 U 5000 U 5000 U 50000 U 50 U 50 U 500 U 50 U 50 U 50 U 50 U 50 U 50 U25 U 25000 U 2500 U 2500 U 2500 U 2500 U 25 U 25000 U 25000 U 2500 U 2500 U 2500 U 2500 U 25000 U 25 U 25 U 250 U 25 U 25 U 25 U 25 U 25 U 25 U92 10000 U 1000 U 1000 U 1000 U 1000 U 96 10000 U 10000 U 1000 U 1000 U 1000 U 1000 U 10000 U 167 175 156 186 162 145 170 166 101 3 U 3000 U 300 U 300 U 300 U 300 U 3 U 3000 U 3000 U 300 U 300 U 300 U 300 U 3000 U 3 U 3 U 30 U 3 U 3 U 3 U 3 U 3 U 3 U3 U 3000 U 300 U 300 U 300 U 300 U 3 U 3000 U 3000 U 300 U 300 U 300 U 300 U 3000 U 3 U 3 U 30 U 3 U 3 U 3 U 3 U 3 U 3 U127 2000 U 492 212 486 238 110 2000 U 2000 U 200 U 200 U 302 220 2000 U 112 119 90.1 83.4 69.1 64.3 83.4 81.8 31.9 15 U 15000 U 1500 U 1500 U 1500 U 1500 U 15 U 15000 U 15000 U 1500 U 1500 U 1500 U 1500 U 15000 U 15 U 15 U 150 U 15 U 461 16 15 U 15 U 15 10 U 10000 U 1000 U 1000 U 1000 U 1000 U 10 U 10000 U 10000 U 1000 U 1000 U 1000 U 1000 U 10000 U 10 U 10 U 100 U 10 U 10 U 10 U 10 U 10 U 10 U5 U 5000 U 500 U 500 U 500 U 500 U 5 U 5000 U 5000 U 500 U 500 U 500 U 500 U 5000 U 5 U 5 U 50 UJ 5 U 7 5 U 5 U 5 U 5 U50 U 50000 U 5000 U 5000 U 5000 U 5000 U 50 U 50000 U 50000 U 5000 U 5000 U 5000 U 5000 U 50000 U 109 123 500 U 63 2350 123 50 U 50 U 128 50 U 50000 U 5000 U 5000 U 5000 U 5000 U 50 U 50000 U 50000 U 5000 U 5000 U 5000 U 5000 U 50000 U 50 U 50 U 500 U 50 U 50 U 50 U 50 U 50 U 50 U31.7 2000 U 200 U 200 U 200 U 200 U 27 2000 U 2000 U 200 U 200 U 200 U 200 U 2000 U 28.5 29.8 22.9 20.7 17.6 16.3 20.6 19.7 7.60 15 380000 269000 391000 314000 254000 20 356000 311000 323000 303000 267000 355000 365000 14 15 50 UJ 24 6 5 9 5 U 5 U
15 U 15000 U 1500 U 1500 U 1500 U 1500 U 15 U 15000 U 15000 U 1500 U 1500 U 1500 U 1500 U 15000 U 15 U 15 U 150 U 15 U 15 U 15 U 15 U 15 U 15 U37 20000 U 2000 U 2000 U 2000 U 2000 U 20 U 20000 U 20000 U 2000 U 2000 U 2000 U 2000 U 20000 U 85 66 250 J 142 41 33.1 27 25 20 U
14.2 2000 U 904 2670 1600 489 14.8 2000 U 2000 U 1090 1030 2380 1850 2000 U 22.5 23.6 20 U 17.2 14.6 13.8 16.8 16.4 10.1 50 U 50000 U 5000 U 5000 U 5000 U 5000 U 50 U 50000 U 50000 U 5000 U 5000 U 5000 U 5000 U 50000 U 50 U 50 U 500 U 50 U 50 U 50 U 50 U 50 U 50 U25 U 25000 U 2500 U 2500 U 2500 U 2500 U 25 U 25000 U 25000 U 2500 U 2500 U 2500 U 2500 U 25000 U 25 U 25 U 250 U 25 U 25 U 25 U 25 U 25 U 25 U175 5000 U 500 U 2270 500 U 500 U 180 5000 U 5000 U 500 U 500 U 500 U 500 U 5000 U 110 114 77 63.7 55.1 50.6 69.8 66.1 31.8 50 U 50000 U 5000 U 5000 U 5000 U 5000 U 50 U 50000 U 50000 U 5000 U 5000 U 5000 U 5000 U 50000 U 50 U 50 U 500 UJ 50 U 50 U 50 U 50 U 50 U 50 U20 U 20000 U 2000 U 2000 U 2000 U 2000 U 20 U 20000 U 20000 U 2000 U 2000 U 2000 U 2000 U 20000 U 20 U 20 U 200 U 20 U 20 U 20 U 20 U 20 U 20 U10 U 10000 U 1000 U 1000 U 1000 U 1000 U 10 U 10000 U 10000 U 1000 U 1000 U 1000 U 1000 U 10000 U 10 U 10 U 100 U 10 U 10 U 10 U 10 U 10 U 10 U25 U 25000 U 2500 U 2500 U 2500 U 2500 U 25 U 25000 U 25000 U 2500 U 2500 U 2500 U 2500 U 25000 U 25 U 25 U 250 UJ 25 U 25 U 25 U 25 U 25 U 25 U
Mar-10IW-09
Dec-09Jan-10 May-10IW-10 ERT-14
Apr-10
Purple Purple Clear Clear Clear
Cleburn RI Report Page 4 of 7 HydroGeoLogic, Inc. 11/12/2010
Table 4.1Metals Analytical Results
ISCO Injection and Remedial Investigation - Cleburn Street Well SiteGrand Island, NE
Monitoring Well IDSampling Date
Sample IDColoration
Conductivity uS/cm NEDissolved Oxygen mg/L NE
pH SU NETemperature °C NE
Turbidity NTU NE
Alkalinity, total mg/L NESulfate mg/L NE
Hardness (as CaCO3) mg/L NETotal Dissolved Solids mg/L NETotal Organic Carbon mg/L NE
Aluminum ug/L NEAntimony ug/L 6Arsenic ug/L 10Barium ug/L 2000
Beryllium ug/L 4Cadmium ug/L 5Calcium mg/L NE
Chromium ug/L 100Cobalt ug/L NECopper ug/L 1300
Iron ug/L NELead ug/L 15
Magnesium mg/L NEManganese ug/L NE
Molybdenum ug/L NENickel ug/L NE
Potassium mg/L NESelenium ug/L 50
Silver ug/L NESodium mg/L NEThallium ug/L 2Titanium ug/L NEVanadium ug/L NE
Zinc ug/L NE
Units MCL
Field Parameters
Geochemical Parameters
Total Metals
Dec-09 Jan-10 Mar-10 Apr-10 May-10 Jul-10 Jan-10 Mar-10 Apr-10 May-10 Jul-10 Dec-09 Jan-10 Apr-10 May-10 Jul-104717-10 4758-16 4818-19 4846-1 4889-1 4981-2 4717-7 4717-7-FD 4758-8 4818-7 4846-10 4889-9 4981-12 4717-15 4758-13 4818-17 4818-17-FD 4846-15 4889-13 4981-17Clear Pink Pink Pink Purple Pink Purple Purple Purple Purple Purple Clear Purple Purple Purple Purple
1360 1040 1190 830 894 436 1710 1710 5940 2470 7040 8810 4580 1890 1990 2850 2850 3090 3910 423012.64 0 6.05 4.93 9.6 3.81 6.57 6.57 0 4.4 1.74 2.28 7.76 5.42 0 0 0 3.6 2.9 4.746.77 6.54 6.7 6.76 6.78 6.67 7.3 7.3 6.26 5.8 5.94 6.09 6.02 7.03 6.29 6.31 6.31 6.47 6.77 6.114.48 16.66 15.27 14.75 15.81 28.49 12.37 12.37 13.52 11.64 11.82 15.37 24.28 12.97 14.61 12.7 12.7 12.56 14.65 29.46
0 0 4.9 0 0 0 0 0 2.1 2.9 3.1 17.3 21.3 0.1 92.8 147.8 147.8 0 11.9 46.7
106 109 89.9 87.3 85.5 51.2 109 108 234 240 226 233 213 132 134 147 148 233 272 262 161 1000 U 162 122 125 55.3 109 138 10000 U 10000 U 10000 U 10000 U 10000 U 271 1000 U 10000 U 10000 U 10000 U 10000 U 10000 U391 13200 U 361 262 279 1300 U 359 363 13200 U 1910 2240 1770 1300 U 361 3070 1320 U 1400 1580 1670 2000 844 801 820 493 440 313 982 976 6940 6530 10800 10300 4260 1140 1670 2190 2320 3160 3690 3910 1.6 4.1 2.96 2.37 J NA NA 1.5 1.1 15.2 1.94 3 U NA NA 3 7.1 3.18 2.96 3 U NA NA
50 U 50000 U 50 U 50 U 50 U 5000 U 50 U 50 U 50000 U 5000 U 5000 U 5000 U 6520 50 U 5000 U 5000 U 5000 U 5000 U 5000 U 5000 U50 U 50000 U 50 U 50 U 50 U 5000 U 50 U 50 U 50000 U 5000 U 5000 U 5000 U 5000 U 50 U 5000 U 5000 U 5000 U 5000 U 5000 U 5000 U25 U 25000 U 25 U 25 U 25 U 2500 U 25 U 25 U 25000 U 2500 U 2500 U 2500 U 2500 U 25 U 2500 U 2500 U 2500 U 2500 U 2500 U 2500 U102 10000 U 86 86 81 1000 U 117 120 10000 U 1000 U 1000 U 1000 U 1000 U 62 3290 1000 U 1000 U 1000 U 1000 U 1000 U3 U 3000 U 3 U 3 U 3 U 300 U 3 U 3 U 3000 U 300 U 300 U 300 U 300 U 3 U 300 U 300 U 300 U 300 U 300 U 300 U3 U 3000 U 3 U 3 U 3 U 300 U 3 U 3 U 3000 U 300 U 300 U 300 U 300 U 3 U 300 U 300 U 300 U 300 U 300 U 300 U110 2000 U 103 73.7 79.3 200 U 101 102 2000 U 437 569 379 200 U 103 898 200 U 231 302 338 461 16 15000 U 177 90 51 1500 U 15 U 15 U 15000 U 11000 2730 2070 4030 15 U 1500 U 10800 14500 11500 7030 8900
10 U 10000 U 10 U 10 U 10 U 1000 U 10 U 10 U 10000 U 1000 U 1000 U 1000 U 1000 U 10 U 1000 U 1000 U 1000 U 1000 U 1000 U 1000 U5 U 5000 U 5 U 5 U 5 U 500 U 5 U 5 U 5000 U 500 U 500 U 500 U 500 U 7 500 U 500 U 500 U 500 U 500 U 500 U58 50000 U 50 U 50 U 50 U 5000 U 50 U 50 U 50000 U 5000 U 5000 U 5000 U 5000 U 101 5000 U 7350 9120 5000 U 5000 U 5000 U
50 U 50000 U 50 U 50 U 50 U 5000 U 50 U 50 U 50000 U 5000 U 5000 U 5000 U 5000 U 50 U 5000 U 5000 U 5000 U 5000 U 5000 U 5000 U28.3 2000 U 25.3 18.9 19.7 200 U 26 26.2 2000 U 200 U 200 U 200 U 200 U 25.1 202 200 U 200 U 200 U 200 U 200 U5 U 316000 6950 18900 4410 500 U 7 8 368000 308000 417000 200000 339000 5 13400 174000 259000 325000 265000 294000 15 U 15000 U 15 U 15 U 15 U 1500 U 15 U 15 U 15000 U 1500 U 1500 U 1500 U 1500 U 15 U 1500 U 1500 U 1500 U 1500 U 1500 U 1500 U20 U 20000 U 37 J 20 U 20 U 2000 U 15 U 30.8 20000 U 5310 2400 2650 2920 34 2000 U 2410 J 3310 J 2000 U 2000 U 3870 19.7 2000 U 16.7 13.5 14.2 200 U 11.9 12 2000 U 344 1190 889 962 12.9 200 U 200 U 200 U 200 U 208 200 U50 U 50000 U 50 U 50 U 50 U 5000 U 50 U 50 U 50000 U 5000 U 5000 U 5000 U 5000 U 50 U 5000 U 5000 U 5000 U 5000 U 5000 U 5000 U25 U 25000 U 25 U 25 U 25 U 2500 U 25 U 25 U 25000 U 2500 U 2500 U 2500 U 2500 U 25 U 2500 U 2500 U 2500 U 2500 U 2500 U 2500 U92.5 5000 U 70.9 57.9 64.9 500 U 166 164 5000 U 500 U 500 U 500 U 500 U 247 1150 500 U 500 U 500 U 500 U 500 U50 U 50000 U 50 U 50 U 50 U 5000 U 50 U 50 U 50000 U 5000 U 5000 U 5000 U 5000 U 50 U 5000 U 5000 U 5000 U 5000 U 5000 U 5000 U20 U 20000 U 20 U 20 U 20 U 2000 U 20 U 20 U 20000 U 2000 U 2000 U 2000 U 2000 U 20 U 2000 U 2000 U 2000 U 2000 U 2000 U 2000 U10 U 10000 U 10 U 10 U 10 U 1000 U 10 U 10 U 10000 U 1000 U 1000 U 1000 U 1000 U 10 U 1000 U 1000 U 1000 U 1000 U 1000 U 1000 U25 U 25000 U 25 U 25 U 25 U 2500 U 25 U 25 U 25000 U 2500 U 2500 U 2500 U 2500 U 25 U 2500 U 2500 U 2500 U 2500 U 2500 U 2500 U
Mar-10Dec-09ERT-15 ERT-16 MW-2A
Clear Purple
Cleburn RI Report Page 5 of 7 HydroGeoLogic, Inc. 11/12/2010
Table 4.1Metals Analytical Results
ISCO Injection and Remedial Investigation - Cleburn Street Well SiteGrand Island, NE
Monitoring Well IDSampling Date
Sample IDColoration
Conductivity uS/cm NEDissolved Oxygen mg/L NE
pH SU NETemperature °C NE
Turbidity NTU NE
Alkalinity, total mg/L NESulfate mg/L NE
Hardness (as CaCO3) mg/L NETotal Dissolved Solids mg/L NETotal Organic Carbon mg/L NE
Aluminum ug/L NEAntimony ug/L 6Arsenic ug/L 10Barium ug/L 2000
Beryllium ug/L 4Cadmium ug/L 5Calcium mg/L NE
Chromium ug/L 100Cobalt ug/L NECopper ug/L 1300
Iron ug/L NELead ug/L 15
Magnesium mg/L NEManganese ug/L NE
Molybdenum ug/L NENickel ug/L NE
Potassium mg/L NESelenium ug/L 50
Silver ug/L NESodium mg/L NEThallium ug/L 2Titanium ug/L NEVanadium ug/L NE
Zinc ug/L NE
Units MCL
Field Parameters
Geochemical Parameters
Total Metals
Dec-09 Jan-10 Mar-10 Apr-10 May-10 Jul-10 Dec-09 Jan-10 Mar-10 Apr-10 May-10 Jul-10 Jan-10 Mar-10 Apr-10 May-10 Jul-10 Mar-10 Apr-10 May-10 Jul-104717-18 4758-14 4818-20 4846-18 4889-19 4981-19 4717-13 4758-12 4818-16 4846-16 4889-17 4981-18 4758-17 4818-15 4846-21 4889-15 4981-13 4758-18 4758-18-FD 4818-14 4846-22 4889-16 4981-14Clear Clear Clear Clear Clear Clear Clear Clear Clear Clear Clear Clear Purple Purple Purple Purple Purple Purple Purple Purple Purple
854 1010 1300 902 937 772 490 411 721 514 503 571 5050 3670 5000 7090 5210 4770 4770 1970 4450 5110 30900 0 0 0 1.73 2.19 0 0 0 0 0.57 1.7 0 0.76 3.97 2.34 3.75 0 0 1.92 4 4.62 5.43
6.63 6.61 6.72 6.56 6.9 6.75 6.92 6.84 7.1 6.76 7.11 6.64 6.59 6.97 6.57 6.94 6.67 7.41 7.41 7.29 7.6 8.17 7.9413.68 12.44 13.55 13.15 14.54 27.98 11.3 13.88 12.19 13 14.29 25.6 11.93 12.97 16.54 15.62 26.26 13.45 13.45 13.25 15.37 14.22 23.2616.5 2.6 3.3 0 0 1.5 3.3 3.1 26.3 0 0 0.1 65.1 28.5 51.3 113 36.1 32.3 32.3 11.3 0.5 13.5 55.8
164 81 132 157 140 93.0 146 143 139 144 142 146 423 260 221 476 367 251 252 176 204 216 241 98 119 114 62.7 J 67.2 42.5 33 32.9 30.4 J 33.7 33.3 35.3 J 10000 U 10000 U 10000 U 10000 U 10000 U 10000 U 10000 U 10000 U 10000 U 10000 U 10000 U221 132 U 291 213 251 171 201 161 185 200 206 1300 U 13200 U 1320 U 1320 U 1650 1500 13200 U 13200 U 1320 U 1320 U 1320 U 1300 U527 715 738 500 584 484 312 296 290 322 323 358 5490 3150 6620 6310 4420 6030 6000 1580 6000 6160 2890 2.8 2.8 2.96 2.66 NA NA 1 U 1 U 3.87 1.15 NA NA 17.6 1.64 1.52 NA NA NC NC 1.51 1 U NA NA
2590 500 U 657 159 519 50 U 256 500 UJ 371 216 50 U 5000 U 50000 U 5000 U 5000 U 5000 U 5000 U 50000 U 50000 U 5000 U 5000 U 5000 U 5000 U50 U 500 U 50 U 50 U 50 U 50 U 50 U 500 UJ 50 U 50 U 50 U 5000 U 50000 U 5000 U 5000 U 5000 U 5000 U 50000 U 50000 U 5000 U 5000 U 5000 U 5000 U25 U 250 U 25 U 25 U 25 U 25 UJ 25 U 250 UJ 25 U 25 U 25 U 2500 U 25000 U 2500 U 2500 U 2500 U 2500 U 25000 U 25000 U 2500 U 2500 U 2500 U 2500 U270 100 U 255 192 223 160 335 366 J 269 358 359 1000 U 10000 U 1000 U 1000 U 1000 U 1000 U 10000 U 10000 U 1000 U 1000 U 1000 U 1000 U3 U 30 U 3 U 3 U 3 U 3 U 3 U 30 UJ 3 U 3 U 3 U 300 U 3000 U 300 U 300 U 300 U 300 U 3000 U 3000 U 300 U 300 U 300 U 300 U3 U 30 U 3 U 3 U 3 U 3 U 3 U 30 UJ 3 U 3 U 3 U 300 U 3000 U 300 U 300 U 300 U 300 U 3000 U 3000 U 300 U 300 U 300 U 300 U63.9 20 U 85.5 61.8 73.9 51.8 64.3 64.6 J 61.2 63.6 66.1 200 U 2000 U 200 U 200 U 332 281 2000 U 2000 U 200 U 200 U 200 U 200 U15 U 150 U 15 U 15 U 15 U 15 U 15 U 150 UJ 15 U 15 U 15 U 1500 U 15000 U 1820 1500 U 5430 4150 15000 U 15000 U 1500 U 1500 U 1500 U 1500 U10 U 100 U 10 U 10 U 10 U 10 U 10 U 100 UJ 10 U 10 U 10 U 1000 U 10000 U 1000 U 1000 U 1000 U 1000 U 10000 U 10000 U 1000 U 1000 U 1000 U 1000 U5 U 50 U 5 U 5 U 5 U 5 U 5 U 50 UJ 5 U 5 U 5 U 500 U 5000 U 500 U 500 U 500 U 500 U 5000 U 5000 U 500 U 500 U 500 U 500 U2230 500 U 728 167 477 56 260 500 UJ 600 293 95 5000 U 50000 U 5000 U 5000 U 5000 U 5000 U 50000 U 50000 U 5000 U 5000 U 5000 U 5000 U50 U 500 U 50 U 50 U 50 U 50 U 50 U 500 UJ 50 U 50 U 50 U 5000 U 50000 U 5000 U 5000 U 5000 U 5000 U 50000 U 50000 U 5000 U 5000 U 5000 U 5000 U15 20 U 18.8 14.3 16.2 10.1 9.86 20 UJ 7.9 9.91 9.95 200 U 2000 U 200 U 200 U 200 U 200 U 2000 U 2000 U 200 U 200 U 200 U 200 U382 499 208 45 184 91 5 U 7 71 16 10 500 U 127000 237000 416000 319000 337000 309000 163000 209000 544000 367000 32400 15 U 150 U 15 U 15 U 15 U 15 U 15 U 150 UJ 15 U 15 U 15 U 1500 U 15000 U 1500 U 1500 U 1500 U 1500 U 15000 U 15000 U 1500 U 1500 U 1500 U 1500 U21 200 U 20 J 20 U 20 U 20 U 20 U 200 UJ 20 U 20 U 20 U 2000 U 20000 U 2000 U 2000 U 2000 U 2000 U 20000 U 20000 U 2000 U 2000 U 2000 U 2000 U
10.1 20 U 10.6 8.22 8.45 7.06 10 20 UJ 11.6 10.1 9.69 200 U 2000 U 644 1530 1470 778 2000 U 2000 U 352 1370 1170 200 U50 U 500 U 50 U 50 U 50 U 50 U 50 U 500 UJ 50 U 50 U 50 U 5000 U 50000 U 5000 U 5000 U 5000 U 5000 U 50000 U 50000 U 5000 U 5000 U 5000 U 5000 U25 U 250 U 25 U 25 U 25 U 25 U 25 U 250 UJ 25 U 25 U 25 U 2500 U 25000 U 2500 U 2500 U 2500 U 2500 U 25000 U 25000 U 2500 U 2500 U 2500 U 2500 U78.3 50 U 138 91.5 90.4 72.3 13.3 50 UJ 51.7 14.1 12.3 500 U 5000 U 500 U 500 U 500 U 500 U 5000 U 5000 U 500 U 500 U 500 U 500 U50 U 500 U 50 U 50 U 50 U 50 UJ 50 U 500 UJ 50 U 50 U 50 U 5000 U 50000 U 5000 U 5000 U 5000 U 5000 U 50000 U 50000 U 5000 U 5000 U 5000 U 5000 U48.6 200 U 20 U 20 U 20 U 20 U 20 U 200 UJ 20 U 20 U 20 U 2000 U 20000 U 2000 U 2000 U 2000 U 2000 U 20000 U 20000 U 2000 U 2000 U 2000 U 2000 U10 U 100 U 10 U 10 U 10 U 10 U 10 U 100 UJ 10 U 10 U 10 U 1000 U 10000 U 1000 U 1000 U 1000 U 1000 U 10000 U 10000 U 1000 U 1000 U 1000 U 1000 U25 U 250 U 25 U 25 U 25 U 25 U 25 U 250 UJ 54 27 25 U 2500 U 25000 U 2500 U 2500 U 2500 U 2500 U 25000 U 25000 U 2500 U 2500 U 2500 U 2500 U
Jan-10DPE-2MW-2B DPE-1MW-12A
Purple
Cleburn RI Report Page 6 of 7 HydroGeoLogic, Inc. 11/12/2010
Table 4.1Metals Analytical Results
ISCO Injection and Remedial Investigation - Cleburn Street Well SiteGrand Island, NE
Monitoring Well IDSampling Date
Sample IDColoration
Conductivity uS/cm NEDissolved Oxygen mg/L NE
pH SU NETemperature °C NE
Turbidity NTU NE
Alkalinity, total mg/L NESulfate mg/L NE
Hardness (as CaCO3) mg/L NETotal Dissolved Solids mg/L NETotal Organic Carbon mg/L NE
Aluminum ug/L NEAntimony ug/L 6Arsenic ug/L 10Barium ug/L 2000
Beryllium ug/L 4Cadmium ug/L 5Calcium mg/L NE
Chromium ug/L 100Cobalt ug/L NECopper ug/L 1300
Iron ug/L NELead ug/L 15
Magnesium mg/L NEManganese ug/L NE
Molybdenum ug/L NENickel ug/L NE
Potassium mg/L NESelenium ug/L 50
Silver ug/L NESodium mg/L NEThallium ug/L 2Titanium ug/L NEVanadium ug/L NE
Zinc ug/L NE
Units MCL
Field Parameters
Geochemical Parameters
Total Metals
Jan-10 Mar-10 Apr-10 May-10 Jul-10 Jan-10 Mar-10 Apr-10 May-10 Jul-10 Dec-09 Mar-10 Apr-10 May-10 Jul-104758-19 4818-22 4846-20 4889-14 4981-15 4758-45 4818-21 4846-19 4889-18 4981-16 4758-20-FB 4818-26-FB 4846-26-FB 4889-24-FB 4981-24-FB Key
Purple Purple Purple Purple Purple Purple Purple Purple Purple Purple Clear Clear Clear Clear ClearBold concentrations denote detections.
7920 4430 7220 7890 6570 7680 8080 7810 7020 5170 NA NA NA NA NA Shaded cells denote concentrations in excess of the MCL.
0 2.38 8.83 2.8 4.46 0 4.13 6.13 9.19 5.68 NA NA NA NA NA MCL - Maximum Contaminant Level
6.51 6.81 6.7 6.96 6.47 8.49 6.85 8.55 9.17 8.34 NA NA NA NA NA NE - No MCL established
11.95 15.01 14.4 15.14 26.11 11.77 14.52 12.4 13.96 27.55 NA NA NA NA NA NA - No analysis requested for specified analyte.
53.6 21.8 0 41.1 24.7 52.8 3.1 0 22.4 37.5 NA NA NA NA NA NC - Analysis not completed by laboratory
U - Nondetect
302 241 245 347 398 343 372 256 566 692 2 U NA NA NA NA UJ - Nondetect
10000 U 10000 U 10000 U 10000 U 10000 U 10000 U 10000 U 10000 U 10000 U 10000 U 1 U NA NA NA NA J - Value is estimated.
13200 U 1320 U 1320 U 1870 13000 U 13200 U 1320 U 1320 U 1320 U 1300 U 13.2 U NA 13.2 U NA 13 U ug/L - micrograms per liter
8610 4110 9320 8870 6350 9920 8960 20000 8280 4970 2 U NA NA NA NA mg/L - milligrams per liter
NC 1.15 1 U NA NA NC 1.47 1 U NA NA 1 U 1 U 1 U NA NA SU = Standard Units
°C - Degrees Celsius
50000 U 5000 U 5000 U 5000 U 50000 U 50000 U 5000 U 5000 U 5000 U 5000 U 50 U 50 U 50 U 50 U 50 U NTU - Nephelometric Turbidity Units
50000 U 5000 U 5000 U 5000 U 50000 U 50000 U 5000 U 5000 U 5000 U 5000 U 50 U 50 U 50 U 50 U 50 U CaCO3 - Calcium Carbonate
25000 U 2500 U 2500 U 2500 U 25000 U 25000 U 2500 U 2500 U 2500 U 2500 U 25 U 25 U 25 U 25 U 25 U uS/cm - microSiemens per centimeter
10000 U 1000 U 1000 U 1000 U 10000 U 10000 U 1000 U 1000 U 1000 U 1000 U 10 U 10 U 10 U 10 U 10 U3000 U 300 U 300 U 300 U 3000 U 3000 U 300 U 300 U 300 U 300 U 3 U 3 U 3 U 3 U 3 U3000 U 300 U 300 U 300 U 3000 U 3000 U 300 U 300 U 300 U 300 U 3 U 3 U 3 U 3 U 3 U2000 U 200 U 200 U 421 2000 U 2000 U 200 U 200 U 200 U 200 U 2 U 2 U 2 U 2.00 U 2.00 U15000 U 1500 1500 U 1500 U 15000 U 15000 U 1500 U 1500 U 1500 U 1500 U 15 U 15 U 15 U 15 U 15 U10000 U 1000 U 1000 U 1000 U 10000 U 10000 U 1000 U 1000 U 1000 U 1000 U 10 U 10 U 10 U 10 U 10 U5000 U 500 U 500 U 500 U 5000 U 5000 U 500 U 500 U 500 U 500 U 5 U 5 U 5 U 5 U 5 U50000 U 5000 U 5000 U 5000 U 50000 U 50000 U 5000 U 5000 U 5000 U 5000 U 50 U 50 U 112 50 U 50 U50000 U 5000 U 5000 U 5000 U 50000 U 50000 U 5000 U 5000 U 5000 U 5000 U 50 U 50 U 50 U 50 U 50 U2000 U 200 U 200 U 200 U 2000 U 2000 U 200 U 200 U 200 U 200 U 2 U 2 U 2 U 2.00 U 2.00 U278000 298000 378000 341000 351000 353000 296000 287000 321000 350000 5 U 5 U 5 U 5 U 5 U15000 U 1500 U 1500 U 1500 U 15000 U 15000 U 1500 U 1500 U 1500 U 1500 U 15 U 15 U 15 U 15 U 15 U20000 U 2000 U 2000 U 2000 U 20000 U 21700 2000 U 2000 U 2000 U 2000 U 37.2 U 20 U 20 U 20 U 20 U2000 U 790 1770 1150 2000 U 2000 U 1480 3730 1720 1290 2 U 2 U 2 U 2.00 U 2.00 U50000 U 5000 U 5000 U 5000 U 50000 U 50000 U 5000 U 5000 U 5000 U 5000 U 50 U 50 U 50 U 50 U 50 U25000 U 2500 U 2500 U 2500 U 25000 U 25000 U 2500 U 2500 U 2500 U 2500 U 25 U 25 U 25 U 25 U 25 U5000 U 500 U 500 U 500 U 5000 U 5000 U 500 U 500 U 500 U 500 U 5 U 5 U 5 U 5.00 U 5.00 U50000 U 5000 U 5000 U 5000 U 50000 U 50000 U 5000 U 5000 U 5000 U 5000 U 50 U 50 U 50 U 50 U 50 U20000 U 2000 U 2000 U 2000 U 20000 U 20000 U 2000 U 2000 U 2000 U 2000 U 20 U 20 U 20 U 20 U 20 U10000 U 1000 U 1000 U 1000 U 10000 U 10000 U 1000 U 1000 U 1000 U 1000 U 10 U 10 U 10 U 10 U 10 U25000 U 2500 U 2500 U 2500 U 25000 U 25000 U 2500 U 2500 U 2500 U 2500 U 25 U 25 U 25 U 25 U 25 U
DPE-4DPE-3 Field Blank
Cleburn RI Report Page 7 of 7 HydroGeoLogic, Inc. 11/12/2010
Table 4.2VOC Analytical Results
ISCO Injection and Remedial Investigation - Cleburn Street Well SiteGrand Island, NE
Monitoring Well IDSampling Date Dec-09 Jan-10 Mar-10 Apr-10 May-10 Dec-09 Jan-10 Apr-10 May-10 Jul-10 Dec-09 Jan-10 Mar-10
Sample ID 4717-1 4766-107 4818-1 4862-102 4890-102 4982-104 4982-104-FD 4717-2 4766-105 4818-2 4818-2-FD 4862-104 4890-103 4982-103 4717-3 4766-104 4818-4 4862-105 4862-105-FD 4890-104 4890-104-FD 4982-110 4982-110-FDColoration Clear Purple Purple Purple Purple Clear Purple Purple Purple Purple Clear Purple Purple Purple Purple
1,1,1-Trichloroethane 200 5.0 U 5.0 U 25000 U 10 U 10 U 5 UJ 20 U 5.0 U 5.0 U 25000 U 25000 U 10 U 10 U 5 U 5.0 U 5.0 U 25000 U 10 U 10 U 10 U 10 U 50 U 50 U1,1,2,2-Tetrachloroethane NE 5.0 U 5.0 U 25000 U 10 U 10 U 5 UJ 20 U 5.0 U 5.0 U 25000 U 25000 U 10 U 10 U 5 U 5.0 U 5.0 U 25000 U 10 UJ 10 UJ 10 U 10 U 50 U 50 U
1,1,2-Trichloroethane 5 5.0 U 5.0 U 25000 U 10 U 10 U 5 UJ 20 U 5.0 U 5.0 U 25000 U 25000 U 10 U 10 U 5 U 5.0 U 5.0 U 25000 U 10 UJ 10 UJ 10 U 10 U 50 U 50 U1,1,2-Trichlorotrifluoroethane NE 5.0 U 5.0 U 25000 U 10 U 10 U 5 UJ 20 U 5.0 U 5.0 U 25000 U 25000 U 10 U 10 U 5 U 5.0 U 5.0 U 25000 U 10 U 10 U 10 U 10 U 50 U 50 U
1,1-Dichloroethane 5 5.0 U 5.0 U 25000 U 10 U 10 U 5 UJ 20 U 5.0 U 5.0 U 25000 U 25000 U 10 U 10 U 5 U 5.0 U 5.0 U 25000 U 10 U 10 U 10 U 10 U 50 U 50 U1,1-Dichloroethene 7 5.0 U 5.0 U 25000 U 10 U 10 U 5 UJ 20 U 5.0 U 5.0 U 25000 U 25000 U 10 U 10 U 5 U 5.0 U 5.0 U 25000 U 10 U 10 U 10 U 10 U 50 U 50 U
1,2,3-Trichlorobenzene NE 5.0 UJ 5.0 U 25000 U 10 U 10 U 5 UJ 20 U 5.0 UJ 5.0 U 25000 U 25000 U 10 U 10 U 5 U 5.0 UJ 5.0 U 25000 U 10 UJ 10 UJ 10 U 10 U 50 U 50 U1,2,4-Trichlorobenzene 70 5.0 UJ 5.0 U 25000 U 10 U 10 U 5 UJ 20 U 5.0 UJ 5.0 U 25000 U 25000 U 10 U 10 U 5 U 5.0 UJ 5.0 U 25000 U 10 UJ 10 UJ 10 U 10 U 50 U 50 U
1,2-Dibromo-3-Chloropropane 0.2 5.0 UJ 5.0 U 25000 U 10 U 10 U 5 UJ 20 U 5.0 UJ 5.0 U 25000 U 25000 U 10 U 10 U 5 U 5.0 UJ 5.0 U 25000 U 10 UJ 10 UJ 10 U 10 U 50 U 50 U1,2-Dibromoethane 0.05 5.0 UJ 5.0 U 25000 U 10 U 10 U 5 UJ 20 U 5.0 UJ 5.0 U 25000 U 25000 U 10 U 10 U 5 U 5.0 UJ 5.0 U 25000 U 10 UJ 10 UJ 10 U 10 U 50 U 50 U1,2-Dichlorobenzene 600 5.0 U 5.0 U 25000 U 10 U 10 U 5 UJ 20 U 5.0 U 5.0 U 25000 U 25000 U 10 U 10 U 5 U 5.0 UJ 5.0 U 25000 U 10 UJ 10 UJ 10 U 10 U 50 U 50 U1,2-Dichloroethane NE 5.0 UJ 5.0 U 25000 U 10 U 10 U 5 U 20 U 5.0 UJ 5.0 U 25000 U 25000 U 10 U 10 U 5 U 5.0 UJ 5.0 U 25000 U 10 UJ 10 UJ 10 U 10 U 50 U 50 U
1,2-Dichloropropane 5 5.0 U 5.0 U 25000 U 10 U 10 U 5 UJ 20 U 5.0 U 5.0 U 25000 U 25000 U 10 U 10 U 5 UJ 5.0 U 5.0 U 25000 U 10 UJ 10 UJ 10 U 10 U 50 U 50 U1,3-Dichlorobenzene NE 5.0 U 5.0 U 25000 U 10 U 10 U 5 UJ 20 U 5.0 U 5.0 U 25000 U 25000 U 10 U 10 U 5 U 5.0 UJ 5.0 U 25000 U 10 UJ 10 UJ 10 U 10 U 50 U 50 U1,4-Dichlorobenzene 75 5.0 U 5.0 U 25000 U 10 U 10 U 5 UJ 20 U 5.0 U 5.0 U 25000 U 25000 U 10 U 10 U 5 U 5.0 UJ 5.0 U 25000 U 10 UJ 10 UJ 10 U 10 U 50 U 50 U
2-Butanone (Methyl Ethyl Ketone) NE 5.0 U 42 25000 U 10 UJ 10 U 5 UJ 20 U 5.0 U 74 25000 U 25000 U 10 UJ 10 U 5 U 5.0 U 21 25000 U 10 UJ 10 UJ 22 22 50 U 50 UJ2-Hexanone NE 5.0 UJ 5.0 U 25000 U 10 U 10 U 5 UJ 20 U 5.0 UJ 5.0 U 25000 U 25000 U 10 U 10 U 5 U 5.0 UJ 5.0 U 25000 U 10 UJ 10 UJ 10 U 10 U 50 U 50 UJ
4-Methyl-2-Pentanone (Methyl Isobutyl Ketone) NE 5.0 UJ 5.0 U 25000 U 10 U 10 U 5 U 20 U 5.0 UJ 5.0 U 25000 U 25000 U 10 U 10 U 5 U 5.0 UJ 5.0 U 25000 U 10 UJ 10 UJ 10 U 10 U 50 U 50 UAcetone NE 5.0 U 180 J 25000 U 110 J 230 15 J 32 5.0 U 210 25000 U 25000 U 120 J 300 39 J 5.0 U 54 25000 U 130 J 120 J 210 200 63 64 JBenzene 5 5.0 U 5.0 U 25000 U 10 U 10 U 5 UJ 20 U 5.0 U 5.0 U 25000 U 25000 U 10 U 10 U 5 UJ 5.0 U 5.0 U 25000 U 10 UJ 10 UJ 10 U 10 U 50 U 50 U
Bromodichloromethane* 80 5.0 U 5.0 U 25000 U 10 U 10 U 5 U 20 U 5.0 U 5.0 U 25000 U 25000 U 10 U 10 U 5 U 5.0 UJ 5.0 U 25000 U 10 UJ 10 UJ 10 U 10 U 50 U 50 UBromoform* 80 5.0 UJ 5.0 U 25000 U 10 U 10 U 5 UJ 20 U 5.0 UJ 5.0 U 25000 U 25000 U 10 U 10 U 5 U 5.0 UJ 5.0 U 25000 U 10 UJ 10 UJ 10 U 10 U 50 U 50 U
Bromomethane NE 5.0 U 5.0 U 25000 U 10 U 10 U 5 UJ 20 U 5.0 U 5.0 U 25000 U 25000 U 10 U 10 U 5 U 5.0 U 5.0 U 25000 U 10 U 10 U 10 U 10 U 50 U 50 UCarbon Disulfide NE 5.0 U 5.0 U 25000 U 10 U 10 U 5 UJ 20 U 5.0 U 5.0 U 25000 U 25000 U 10 U 10 U 5 U 5.0 U 5.0 U 25000 U 10 U 10 U 10 U 10 U 50 U 50 U
Carbon Tetrachloride 5 5.0 U 5.0 U 25000 U 10 U 10 U 5 UJ 20 U 5.0 U 5.0 U 25000 U 25000 U 10 U 10 U 5 U 5.0 U 5.0 U 25000 U 10 U 10 U 10 U 10 U 50 U 50 UChlorobenzene 100 5.0 U 5.0 U 25000 U 10 U 10 U 5 UJ 20 U 5.0 U 5.0 U 25000 U 25000 U 10 U 10 U 5 U 5.0 U 5.0 U 25000 U 10 UJ 10 UJ 10 U 10 U 50 U 50 UChloroethane NE 5.0 U 5.0 U 25000 U 10 U 10 U 5 UJ 20 U 5.0 U 5.0 U 25000 U 25000 U 10 U 10 U 5 UJ 5.0 U 5.0 U 25000 U 10 U 10 U 10 U 10 U 50 U 50 UChloroform* 80 5.0 U 5.0 U 25000 U 10 U 10 U 5 UJ 20 U 5.0 U 5.0 U 25000 U 25000 U 10 U 10 U 5 U 5.0 U 5.0 U 25000 U 10 U 10 U 10 U 10 U 50 U 50 U
Chloromethane NE 5.0 U 5.0 U 25000 U 10 U 10 U 5 UJ 20 U 5.0 U 5.0 U 25000 U 25000 U 10 U 10 U 5 UJ 5.0 U 5.0 U 25000 U 10 U 10 U 10 U 10 U 50 U 50 Ucis-1,2-Dichloroethene 70 5.0 U 5.0 U 25000 U 10 U 10 U 5 UJ 20 U 5.0 U 5.0 U 25000 U 25000 U 10 U 10 U 5 U 5.0 U 5.0 U 25000 U 10 U 10 U 10 U 10 U 50 U 50 U
cis-1,3-Dichloropropene NE 5.0 U 5.0 U 25000 UJ 10 U 10 U 5 U 20 U 5.0 U 5.0 U 25000 U 25000 U 10 U 10 U 5 U 5.0 U 5.0 U 25000 U 10 UJ 10 UJ 10 U 10 U 50 U 50 UCyclohexane NE 5.0 U 5.0 U 25000 U 10 U 10 U 5 UJ 20 U 5.0 U 5.0 U 25000 U 25000 U 10 U 10 U 5 UJ 5.0 U 5.0 U 25000 U 10 U 10 U 10 U 10 U 50 U 50 U
Dibromochloromethane* 80 5.0 UJ 5.0 U 25000 U 10 U 10 U 5 UJ 20 U 5.0 UJ 5.0 U 25000 U 25000 U 10 U 10 U 5 U 5.0 UJ 7.6 25000 U 10 UJ 10 UJ 10 U 10 U 50 U 50 UDichlorodifluoromethane NE 5.0 UJ 10 U 25000 UJ 10 U 10 U 5 UJ 20 U 5.0 UJ 10 U 25000 UJ 25000 UJ 10 U 10 U 5 UJ 5.0 UJ 10 U 25000 UJ 10 U 10 U 10 U 10 U 50 U 50 U
Ethyl Benzene 700 5.0 U 5.0 U 25000 U 10 U 10 U 5 UJ 20 U 5.0 U 5.0 U 25000 U 25000 U 10 U 10 U 5 U 5.0 U 5.0 U 25000 U 10 UJ 10 UJ 10 U 10 U 50 U 50 UIsopropylbenzene NE 5.0 U 5.0 U 25000 U 10 U 10 U 5 UJ 20 U 5.0 U 5.0 U 25000 U 25000 U 10 U 10 U 5 U 5.0 U 5.0 U 25000 U 10 UJ 10 UJ 10 U 10 U 50 U 50 U
m and/or p-Xylene 10000 10 U 10 U 50000 U 20 U 20 U 10 UJ 40 U 10 U 10 U 50000 U 50000 U 20 U 20 U 10 U 10 U 10 U 50000 U 20 UJ 20 UJ 20 U 20 U 100 U 100 UMethyl Acetate NE 5.0 U 5.0 U 25000 U 10 U 10 U 5 UJ 20 U 5.0 U 5.0 U 25000 U 25000 U 10 U 10 U 5 UJ 5.0 U 5.0 U 25000 U 10 U 10 U 10 U 10 U 50 U 50 UJ
Methyl tert-butyl ether NE 10 U 10 U 50000 UJ 20 U 20 U 10 UJ 40 U 10 U 10 U 50000 U 50000 U 20 U 20 U 10 U 10 UJ 10 U 50000 U 20 U 20 U 20 U 20 U 100 U 100 UMethylcyclohexane NE 5.0 U 5.0 U 25000 U 10 U 10 U 5 U 20 U 5.0 U 5.0 U 25000 U 25000 U 10 U 10 U 5 U 5.0 U 5.0 U 25000 U 10 UJ 10 UJ 10 U 10 U 50 U 50 UMethylene Chloride 5 5.0 U 5.0 U 25000 U 10 U 10 U 5 UJ 20 U 5.0 U 5.0 U 25000 U 25000 U 10 U 10 U 5 U 5.0 U 5.0 U 25000 U 10 U 10 U 10 U 10 U 50 U 50 U
Naphthalene NE 10 UJ 10 U 50000 U 20 U 20 U 10 UJ 40 U 10 UJ 10 U 50000 U 50000 U 20 U 20 U 10 U 10 UJ 10 U 50000 U 20 UJ 20 UJ 20 U 20 U 100 U 100 Uo-Xylene 10000 5.0 U 5.0 U 25000 U 10 U 10 U 5 UJ 20 U 5.0 U 5.0 U 25000 U 25000 U 10 U 10 U 5 U 5.0 U 5.0 U 25000 U 10 UJ 10 UJ 10 U 10 U 50 U 50 UStyrene 100 5.0 U 5.0 U N/A R 10 U 10 U 5 UJ 20 U 5.0 U 5.0 U 25000 U 25000 U 10 U 10 U 5 U 5.0 U 5.0 U 25000 U 10 UJ 10 UJ 10 U 10 U 50 U 50 U
Tetrachloroethene 5 5.2 5.0 U 25000 U 10 U 10 U 7.8 J 20 U 4500 5.0 U 25000 U 25000 U 10 U 10 U 690 4100 5.0 U 25000 U 10 UJ 10 UJ 10 U 10 U 95 110 Toluene 1000 5.0 U 5.0 U 25000 U 10 U 10 U 5 U 20 U 5.0 U 5.0 U 25000 U 25000 U 10 U 10 U 5 U 5.0 U 5.0 U 25000 U 10 UJ 10 UJ 10 U 10 U 50 U 50 U
trans-1,2-Dichloroethene 100 5.0 U 5.0 U 25000 UJ 10 U 10 U 5 UJ 20 U 5.0 U 5.0 U 25000 U 25000 U 10 U 10 U 5 U 5.0 U 5.0 U 25000 U 10 U 10 U 10 U 10 U 50 U 50 Utrans-1,3-Dichloropropene NE 5.0 U 5.0 U 25000 UJ 10 U 10 U 5 UJ 20 U 5.0 U 5.0 U 25000 U 25000 U 10 U 10 U 5 U 5.0 UJ 5.0 U 25000 U 10 UJ 10 UJ 10 U 10 U 50 U 50 U
Trichloroethene 5 5.0 U 5.0 U 25000 U 10 U 10 U 5 U 20 U 5.0 U 5.0 U 25000 U 25000 U 10 U 10 U 5 U 5.0 U 5.0 U 25000 U 10 UJ 10 UJ 10 U 10 U 50 U 50 UTrichlorofluoromethane NE 5.0 U 5.0 U 25000 U 10 U 10 U 5 UJ 20 U 5.0 U 5.0 U 25000 U 25000 U 10 U 10 U 5 U 5.0 U 5.0 U 25000 U 10 U 10 U 10 U 10 U 50 U 50 U
Vinyl Chloride 2 5.0 U 5.0 U 25000 UJ 10 U 10 U 5 UJ 20 U 5.0 U 5.0 U 25000 U 25000 U 10 U 10 U 5 U 5.0 U 5.0 U 25000 U 10 U 10 U 10 U 10 U 50 U 50 U
PurplePurplePurplePurple
MCLIW-2IW-1
Jul-10 Apr-10Mar-10IW-3
May-10 Jul-10
Cleburn RI Report Page 1 of 7 HydroGeoLogic, Inc. 11/12/2010
Table 4.2VOC Analytical Results
ISCO Injection and Remedial Investigation - Cleburn Street Well SiteGrand Island, NE
Monitoring Well IDSampling Date
Sample IDColoration
1,1,1-Trichloroethane 2001,1,2,2-Tetrachloroethane NE
1,1,2-Trichloroethane 51,1,2-Trichlorotrifluoroethane NE
1,1-Dichloroethane 51,1-Dichloroethene 7
1,2,3-Trichlorobenzene NE1,2,4-Trichlorobenzene 70
1,2-Dibromo-3-Chloropropane 0.21,2-Dibromoethane 0.051,2-Dichlorobenzene 6001,2-Dichloroethane NE
1,2-Dichloropropane 51,3-Dichlorobenzene NE1,4-Dichlorobenzene 75
2-Butanone (Methyl Ethyl Ketone) NE2-Hexanone NE
4-Methyl-2-Pentanone (Methyl Isobutyl Ketone) NEAcetone NEBenzene 5
Bromodichloromethane* 80Bromoform* 80
Bromomethane NECarbon Disulfide NE
Carbon Tetrachloride 5Chlorobenzene 100Chloroethane NEChloroform* 80
Chloromethane NEcis-1,2-Dichloroethene 70
cis-1,3-Dichloropropene NECyclohexane NE
Dibromochloromethane* 80Dichlorodifluoromethane NE
Ethyl Benzene 700Isopropylbenzene NE
m and/or p-Xylene 10000Methyl Acetate NE
Methyl tert-butyl ether NEMethylcyclohexane NEMethylene Chloride 5
Naphthalene NEo-Xylene 10000Styrene 100
Tetrachloroethene 5Toluene 1000
trans-1,2-Dichloroethene 100trans-1,3-Dichloropropene NE
Trichloroethene 5Trichlorofluoromethane NE
Vinyl Chloride 2
MCL Dec-09 Jan-10 Mar-10 Apr-10 May-10 Jul-10 Dec-09 Jan-10 Mar-10 Apr-10 May-10 Jul-10 Dec-09 Jan-10 Mar-10 Apr-10 May-10 Jul-10 Dec-09 Jan-10 Mar-10 Apr-10 May-10 Jul-104717-5 4766-106 4818-5 4862-106 4890-105 4982-105 4717-4 4766-101 4818-6 4862-107 4890-106 4982-106 4717-6 4766-102 4818-8 4862-108 4890-107 4982-107 4717-9 4766-103 4818-9 4862-109 4890-108 4982-108Clear Purple Purple Purple Purple Purple Clear Purple Purple Purple Purple Purple Clear Purple Purple Purple Purple Purple Clear Purple Purple Purple Purple Purple5.0 U 5.0 U 25000 U 10 U 10 U 20 U 5.0 U 24 25000 U 39 10 U 20 U 5.0 U 9.4 25000 U 19 J 13 20 U 10 15 25000 U 54 J 35 35 5.0 U 5.0 U 25000 U 10 UJ 10 U 20 U 5.0 U 5.0 U 25000 U 10 UJ 10 U 20 U 5.0 U 5.0 U 25000 U 10 UJ 10 U 20 U 5.0 U 5.0 U 25000 U 10 UJ 10 U 20 U5.0 U 5.0 U 25000 U 10 UJ 10 U 20 U 5.0 U 5.0 U 25000 U 10 UJ 10 U 20 U 5.0 U 5.0 U 25000 U 10 UJ 10 U 20 U 5.0 U 5.0 U 25000 U 10 UJ 10 U 20 U5.0 U 5.0 U 25000 U 10 U 10 U 20 U 5.0 U 5.0 U 25000 U 10 U 10 U 20 U 5.0 U 5.0 U 25000 U 10 UJ 10 U 20 U 5.0 U 5.0 U 25000 U 10 UJ 10 U 20 U5.0 U 5.0 U 25000 U 10 U 10 U 20 U 5.0 U 5.0 U 25000 U 10 U 10 U 20 U 5.0 U 5.0 U 25000 U 10 UJ 10 U 20 U 5.0 U 5.0 U 25000 U 10 UJ 10 U 20 U5.0 U 5.0 U 25000 U 10 U 10 U 20 U 5.0 U 5.0 U 25000 U 10 U 10 U 20 U 5.0 U 5.0 U 25000 U 10 UJ 10 U 20 U 5.0 U 5.0 U 25000 U 10 UJ 10 U 20 U5.0 UJ 5.0 U 25000 U 10 UJ 10 U 20 U 5.0 UJ 5.0 U 25000 U 10 UJ 10 U 20 U 5.0 UJ 5.0 U 25000 U 10 UJ 10 U 20 U 5.0 UJ 5.0 U 25000 U 10 UJ 10 U 20 U5.0 UJ 5.0 U 25000 U 10 UJ 10 U 20 U 5.0 UJ 5.0 U 25000 U 10 UJ 10 U 20 U 5.0 UJ 5.0 U 25000 U 10 UJ 10 U 20 U 5.0 UJ 5.0 U 25000 U 10 UJ 10 U 20 U5.0 UJ 5.0 U 25000 U 10 UJ 10 U 20 U 5.0 UJ 5.0 U 25000 U 10 UJ 10 U 20 U 5.0 UJ 5.0 U 25000 U 10 UJ 10 U 20 U 5.0 UJ 5.0 U 25000 U 10 UJ 10 U 20 U5.0 UJ 5.0 U 25000 U 10 UJ 10 U 20 U 5.0 UJ 5.0 U 25000 U 10 UJ 10 U 20 U 5.0 UJ 5.0 U 25000 U 10 UJ 10 U 20 U 5.0 UJ 5.0 U 25000 U 10 UJ 10 U 20 U5.0 U 5.0 U 25000 U 10 UJ 10 U 20 U 5.0 U 14 25000 U 10 UJ 10 U 20 U 5.0 U 6.4 25000 U 10 UJ 10 U 20 U 5.0 U 8.1 25000 U 10 UJ 10 U 20 U5.0 UJ 5.0 U 25000 U 10 UJ 10 U 20 U 5.0 UJ 5.0 U 25000 U 10 UJ 10 U 20 U 5.0 UJ 5.0 U 25000 U 10 UJ 10 U 20 U 5.0 UJ 5.0 U 25000 U 10 UJ 10 U 20 U5.0 U 5.0 U 25000 U 10 UJ 10 U 20 U 5.0 U 5.0 U 25000 U 10 UJ 10 U 20 U 5.0 U 5.0 U 25000 U 10 UJ 10 U 20 U 5.0 U 5.0 U 25000 U 10 UJ 10 U 20 U5.0 U 5.0 U 25000 U 10 UJ 10 U 20 U 5.0 U 5.0 U 25000 U 10 UJ 10 U 20 U 5.0 U 5.0 U 25000 U 10 UJ 10 U 20 U 5.0 U 5.0 U 25000 U 10 UJ 10 U 20 U5.0 U 5.0 U 25000 U 10 UJ 10 U 20 U 5.0 U 5.0 U 25000 U 10 UJ 10 U 20 U 5.0 U 5.0 U 25000 U 10 UJ 10 U 20 U 5.0 U 5.0 U 25000 U 10 UJ 10 U 20 U5.0 U 23 25000 U 10 UJ 10 U 20 U 5.0 U 54 25000 U 12 J 10 U 20 U 5.0 U 110 25000 U 10 UJ 24 20 U 5.0 U 180 25000 U 10 UJ 31 20 UJ5.0 UJ 5.0 U 25000 U 10 UJ 10 U 20 U 5.0 UJ 5.0 U 25000 U 10 UJ 10 U 20 U 5.0 UJ 5.0 U 25000 U 10 UJ 10 U 20 U 5.0 UJ 5.0 U 25000 U 10 UJ 10 U 20 UJ5.0 UJ 5.0 U 25000 U 10 UJ 10 U 20 U 5.0 UJ 5.0 U 25000 U 10 UJ 10 U 20 U 5.0 UJ 5.0 U 25000 U 10 UJ 10 U 20 U 5.0 UJ 5.0 U 25000 U 10 UJ 10 U 20 U5.0 U 63 J 25000 U 58 J 230 70 5.0 U 210 25000 U 200 J 100 34 5.0 U 420 25000 U 280 J 850 490 5.0 U 490 25000 U 240 J 580 200 J5.0 U 5.0 U 25000 U 10 UJ 10 U 20 U 5.0 U 5.0 U 25000 U 10 UJ 10 U 20 U 5.0 U 5.0 U 25000 U 10 UJ 10 U 20 U 5.0 U 5.0 U 25000 U 10 UJ 10 U 20 U5.0 U 5.0 U 25000 U 10 UJ 10 U 20 U 5.0 U 8.3 25000 U 10 UJ 10 U 20 U 5.0 U 9.9 25000 U 10 UJ 10 20 U 5.0 U 21 25000 U 12 J 15 20 U5.0 UJ 5.0 U 25000 U 10 UJ 10 U 20 U 5.0 UJ 5.0 U 25000 U 10 UJ 10 U 20 U 5.0 UJ 5.0 U 25000 U 10 UJ 10 U 20 U 5.0 UJ 5.0 U 25000 U 10 UJ 10 U 20 U5.0 U 5.0 U 25000 U 10 U 10 U 20 U 5.0 U 5.0 U 25000 U 10 U 10 U 20 U 5.0 U 5.0 U 25000 U 10 UJ 10 U 20 U 5.0 U 5.0 U 25000 U 10 UJ 10 U 20 U5.0 U 5.0 U 25000 U 10 U 10 U 20 U 5.0 U 5.0 U 25000 U 10 U 10 U 20 U 5.0 U 5.0 U 25000 U 10 UJ 10 U 20 U 5.0 U 5.0 U 25000 U 10 UJ 10 U 20 U5.0 U 5.0 U 25000 U 200 110 20 U 5.0 U 73 25000 U 570 83 40 5.0 U 46 25000 U 200 J 160 180 5.0 U 97 25000 U 910 J 610 760 J5.0 U 5.0 U 25000 U 10 UJ 10 U 20 U 5.0 U 5.0 U 25000 U 10 UJ 10 U 20 U 5.0 U 5.0 U 25000 U 10 UJ 10 U 20 U 5.0 U 5.0 U 25000 U 10 UJ 10 U 20 U5.0 U 5.0 U 25000 U 10 U 10 U 20 U 5.0 U 5.0 U 25000 U 10 U 10 U 20 U 5.0 U 5.0 U 25000 U 10 UJ 10 U 20 U 5.0 U 5.0 U 25000 U 10 UJ 10 U 20 U5.0 U 5.0 U 25000 U 10 U 10 U 20 U 5.0 U 110 25000 U 190 54 20 U 5.0 U 140 25000 U 160 J 170 170 5.0 U 240 25000 U 510 J 390 270 5.0 U 5.0 U 25000 U 10 U 10 U 20 U 5.0 U 5.0 U 25000 U 10 U 10 U 20 U 5.0 U 5.0 U 25000 U 10 UJ 10 U 20 U 5.0 U 5.1 25000 U 14 J 10 U 20 U5.0 U 5.0 U 25000 U 10 U 10 U 20 U 5.0 U 5.0 U 25000 U 10 U 10 U 20 U 5.0 U 5.0 U 25000 U 10 UJ 10 U 20 U 5.0 U 5.0 U 25000 U 10 UJ 10 U 20 U5.0 U 5.0 U 25000 U 10 UJ 10 U 20 U 5.0 U 5.0 U 25000 U 10 UJ 10 U 20 U 5.0 U 5.0 U 25000 U 10 UJ 10 U 20 U 5.0 U 5.0 U 25000 U 10 UJ 10 U 20 U5.0 U 5.0 U 25000 U 10 U 10 U 20 U 5.0 U 5.0 U 25000 U 10 U 10 U 20 U 5.0 U 5.0 U 25000 U 10 UJ 10 U 20 U 5.0 U 5.0 U 25000 U 10 UJ 10 U 20 U5.0 UJ 7.6 25000 U 10 UJ 10 U 20 U 5.0 UJ 7.1 25000 U 10 UJ 10 U 20 U 5.0 UJ 8.1 25000 U 10 UJ 10 U 20 U 5.0 UJ 12 25000 U 10 UJ 10 U 20 U5.0 UJ 10 U 25000 UJ 10 U 10 U 20 U 5.0 UJ 10 U 25000 UJ 10 U 10 U 20 U 5.0 UJ 10 U 25000 UJ 10 UJ 10 U 20 U 5.0 UJ 10 U 25000 UJ 10 UJ 10 U 20 U5.0 U 5.0 U 25000 U 10 UJ 10 U 20 U 5.0 U 5.0 U 25000 U 10 UJ 10 U 20 U 5.0 U 5.0 U 25000 U 10 UJ 10 U 20 U 5.0 U 5.0 U 25000 U 10 UJ 10 U 20 U5.0 U 5.0 U 25000 U 10 UJ 10 U 20 U 5.0 U 5.0 U 25000 U 10 UJ 10 U 20 U 5.0 U 5.0 U 25000 U 10 UJ 10 U 20 U 5.0 U 5.0 U 25000 U 10 UJ 10 U 20 U10 U 10 U 50000 U 20 UJ 20 U 40 U 10 U 10 U 50000 U 20 UJ 20 U 40 U 10 U 10 U 50000 U 20 UJ 20 U 40 U 10 U 10 U 50000 U 20 UJ 20 U 40 U5.0 U 5.0 U 25000 U 10 U 10 U 20 U 5.0 U 5.0 U 25000 U 10 U 10 U 20 U 5.0 U 5.0 U 25000 U 10 UJ 10 U 20 U 5.0 U 5.0 U 25000 U 10 UJ 10 U 20 UJ10 U 10 U 50000 U 20 U 20 U 40 U 10 U 10 U 50000 U 20 U 20 U 40 U 10 U 10 U 50000 U 20 UJ 20 U 40 U 10 U 10 U 50000 U 20 UJ 20 U 40 U5.0 U 5.0 U 25000 U 10 UJ 10 U 20 U 5.0 U 5.0 U 25000 U 10 UJ 10 U 20 U 5.0 U 5.0 U 25000 U 10 UJ 10 U 20 U 5.0 U 5.0 U 25000 U 10 UJ 10 U 20 U5.0 U 5.0 U 25000 U 10 U 10 U 20 U 5.0 U 5.0 U 25000 U 10 U 10 U 20 U 5.0 U 5.0 U 25000 U 10 UJ 10 U 20 U 5.0 U 5.0 U 25000 U 10 UJ 10 U 20 U10 UJ 10 U 50000 U 20 UJ 20 U 40 U 10 UJ 10 U 50000 U 20 UJ 20 U 40 U 10 UJ 10 U 50000 U 20 UJ 20 U 40 U 10 UJ 10 U 50000 U 20 UJ 20 U 40 U5.0 U 5.0 U 25000 U 10 UJ 10 U 20 U 5.0 U 5.0 U 25000 U 10 UJ 10 U 20 U 5.0 U 5.0 U 25000 U 10 UJ 10 U 20 U 5.0 U 5.0 U 25000 U 10 UJ 10 U 20 U5.0 U 5.0 U 25000 U 10 UJ 10 U 20 U 5.0 U 5.0 U 25000 U 10 UJ 10 U 20 U 5.0 U 5.0 U 25000 U 10 UJ 10 U 20 U 5.0 U 5.0 U 25000 U 10 UJ 10 U 20 U6200 5.0 U 25000 U 10 UJ 10 U 20 U 18000 5.0 U 25000 U 30 J 370 33000 13000 5.0 U 25000 U 10 UJ 10 U 43 39000 5.0 U 25000 U 11 J 17 29 5.0 U 5.0 U 25000 U 10 UJ 10 U 20 U 5.0 U 5.0 U 25000 U 10 UJ 10 U 20 U 5.0 U 5.0 U 25000 U 10 UJ 10 U 20 U 5.0 U 5.0 U 25000 U 10 UJ 10 U 20 U5.0 U 5.0 U 25000 U 10 U 10 U 20 U 5.0 U 5.0 U 25000 U 10 U 10 U 20 U 5.0 U 5.0 U 25000 U 10 UJ 10 U 20 U 5.0 U 5.0 U 25000 U 10 UJ 10 U 20 U5.0 U 5.0 U 25000 U 10 UJ 10 U 20 U 5.0 U 5.0 U 25000 U 10 UJ 10 U 20 U 5.0 U 5.0 U 25000 U 10 UJ 10 U 20 U 5.0 U 5.0 U 25000 U 10 UJ 10 U 20 U5.0 U 5.0 U 25000 U 10 UJ 10 U 20 U 5.0 U 5.0 U 25000 U 10 UJ 10 U 20 U 5.0 U 5.0 U 25000 U 10 UJ 10 U 20 U 13 5.0 U 25000 U 10 UJ 10 U 20 U5.0 U 5.0 U 25000 U 10 U 10 U 20 U 5.0 U 5.0 U 25000 U 10 U 10 U 20 U 5.0 U 5.0 U 25000 U 10 UJ 10 U 20 U 5.0 U 5.0 U 25000 U 10 UJ 10 U 20 U5.0 U 5.0 U 25000 U 10 U 10 U 20 U 5.0 U 5.0 U 25000 U 10 U 10 U 20 U 5.0 U 5.0 U 25000 U 10 UJ 10 U 20 U 5.0 U 5.0 U 25000 U 10 UJ 10 U 20 U
IW-05 IW-06 IW-7IW-04
Cleburn RI Report Page 2 of 7 HydroGeoLogic, Inc. 11/12/2010
Table 4.2VOC Analytical Results
ISCO Injection and Remedial Investigation - Cleburn Street Well SiteGrand Island, NE
Monitoring Well IDSampling Date
Sample IDColoration
1,1,1-Trichloroethane 2001,1,2,2-Tetrachloroethane NE
1,1,2-Trichloroethane 51,1,2-Trichlorotrifluoroethane NE
1,1-Dichloroethane 51,1-Dichloroethene 7
1,2,3-Trichlorobenzene NE1,2,4-Trichlorobenzene 70
1,2-Dibromo-3-Chloropropane 0.21,2-Dibromoethane 0.051,2-Dichlorobenzene 6001,2-Dichloroethane NE
1,2-Dichloropropane 51,3-Dichlorobenzene NE1,4-Dichlorobenzene 75
2-Butanone (Methyl Ethyl Ketone) NE2-Hexanone NE
4-Methyl-2-Pentanone (Methyl Isobutyl Ketone) NEAcetone NEBenzene 5
Bromodichloromethane* 80Bromoform* 80
Bromomethane NECarbon Disulfide NE
Carbon Tetrachloride 5Chlorobenzene 100Chloroethane NEChloroform* 80
Chloromethane NEcis-1,2-Dichloroethene 70
cis-1,3-Dichloropropene NECyclohexane NE
Dibromochloromethane* 80Dichlorodifluoromethane NE
Ethyl Benzene 700Isopropylbenzene NE
m and/or p-Xylene 10000Methyl Acetate NE
Methyl tert-butyl ether NEMethylcyclohexane NEMethylene Chloride 5
Naphthalene NEo-Xylene 10000Styrene 100
Tetrachloroethene 5Toluene 1000
trans-1,2-Dichloroethene 100trans-1,3-Dichloropropene NE
Trichloroethene 5Trichlorofluoromethane NE
Vinyl Chloride 2
MCL Dec-09 Jan-10 Mar-10 Dec-09 Jan-10 Mar-10 Apr-10 May-10 Jul-10 Dec-09 Jan-10 Apr-10 May-10 Jul-104717-14 4766-109 4818-10 4862-112 4862-112-FD 4890-110 4890-110-FD 4982-122 4982-122-FD 4717-17 4766-111 4818-11 4862-111 4890-111 4982-109 4717-16 4766-110 4818-12 4818-12-FD 4862-114 4890-112 4982-111Clear Purple Purple Clear Purple Purple Purple Purple Purple Clear Purple Purple Purple Purple7.0 5.0 U 13000 U 10 UJ 10 UJ 10 U 10 U 20 U 20 U 13 19 13000 U 10 UJ 35 64 28 25 25000 U 25000 U 10 UJ 20 26
5.0 U 5.0 U 13000 U 10 UJ 10 UJ 10 U 10 U 20 U 20 U 5.0 U 5.0 U 13000 U 10 UJ 10 U 20 U 5.0 U 5.0 U 25000 U 25000 U 10 UJ 10 U 20 U5.0 U 5.0 U 13000 U 10 UJ 10 UJ 10 U 10 U 20 U 20 U 5.0 U 5.0 U 13000 U 10 UJ 10 U 20 U 5.0 U 5.0 U 25000 U 25000 U 10 UJ 10 U 20 U5.0 U 5.0 U 13000 U 10 UJ 10 UJ 10 U 10 U 20 U 20 U 5.0 U 5.0 U 13000 U 10 UJ 10 U 20 U 5.0 U 5.0 U 25000 U 25000 U 10 UJ 10 U 20 U5.0 U 5.0 U 13000 U 10 UJ 10 UJ 10 U 10 U 20 U 20 U 5.0 U 5.0 U 13000 U 10 UJ 10 U 20 U 5.0 U 5.0 U 25000 U 25000 U 10 UJ 10 U 20 U5.0 U 5.0 U 13000 U 10 UJ 10 UJ 10 U 10 U 20 U 20 U 5.0 U 5.0 U 13000 U 10 UJ 10 U 20 U 5.0 U 5.0 U 25000 U 25000 U 10 UJ 10 U 20 U5.0 UJ 5.0 U 13000 U 10 UJ 10 UJ 10 U 10 U 20 U 20 U 5.0 UJ 5.0 U 13000 U 10 UJ 10 U 20 U 5.0 UJ 5.0 U 25000 U 25000 U 10 UJ 10 U 20 U5.0 UJ 5.0 U 13000 U 10 UJ 10 UJ 10 U 10 U 20 U 20 U 5.0 UJ 5.0 U 13000 U 10 UJ 10 U 20 U 5.0 UJ 5.0 U 25000 U 25000 U 10 UJ 10 U 20 U5.0 UJ 5.0 U 13000 U 10 UJ 10 UJ 10 U 10 U 20 U 20 U 5.0 UJ 5.0 U 13000 U 10 UJ 10 U 20 U 5.0 UJ 5.0 U 25000 U 25000 U 10 UJ 10 U 20 U5.0 UJ 5.0 U 13000 U 10 UJ 10 UJ 10 U 10 U 20 U 20 U 5.0 UJ 5.0 U 13000 U 10 UJ 10 U 20 U 5.0 UJ 5.0 U 25000 U 25000 U 10 UJ 10 UJ 20 U5.0 U 5.0 U 13000 U 10 UJ 10 UJ 10 U 10 U 20 U 20 U 5.1 19 13000 U 10 UJ 20 20 U 5.0 U 7.6 25000 U 25000 U 10 UJ 10 U 20 U5.0 UJ 5.0 U 13000 U 10 UJ 10 UJ 10 U 10 U 20 U 20 U 5.0 UJ 5.0 U 13000 U 10 UJ 10 U 20 U 5.0 UJ 5.0 U 25000 U 25000 U 10 UJ 10 U 20 U5.0 U 5.0 U 13000 U 10 UJ 10 UJ 10 U 10 U 20 U 20 U 5.0 U 5.0 U 13000 U 10 UJ 10 U 20 U 5.0 U 5.0 U 25000 U 25000 U 10 UJ 10 UJ 20 U5.0 U 5.0 U 13000 U 10 UJ 10 UJ 10 U 10 U 20 U 20 U 5.0 U 5.0 U 13000 U 10 UJ 10 U 20 U 5.0 U 5.0 U 25000 U 25000 U 10 UJ 10 U 20 U5.0 U 5.0 U 13000 U 10 UJ 10 UJ 10 U 10 U 20 U 20 U 5.0 U 5.0 U 13000 U 10 UJ 10 U 20 U 5.0 U 5.0 U 25000 U 25000 U 10 UJ 10 U 20 U5.0 U 20 13000 U 10 UJ 10 UJ 16 16 20 UJ 20 UJ 5.0 U 41 13000 U 10 UJ 28 20 UJ 5.0 U 34 25000 U 25000 U 10 UJ 10 U 20 UJ5.0 UJ 5.0 U 13000 U 10 UJ 10 UJ 10 U 10 U 20 UJ 20 UJ 5.0 UJ 5.0 U 13000 U 10 UJ 10 U 20 UJ 5.0 UJ 5.0 U 25000 U 25000 U 10 UJ 10 U 20 UJ5.0 UJ 5.0 U 13000 U 10 UJ 10 UJ 10 U 10 U 20 U 20 U 5.0 UJ 5.0 U 13000 U 10 UJ 10 U 20 U 5.0 UJ 5.0 U 25000 U 25000 U 10 UJ 10 U 20 U5.0 U 250 13000 U 110 J 120 J 270 290 52 J 53 J 5.0 U 580 13000 U 300 J 790 88 J 5.0 U 370 25000 U 25000 U 160 J 600 120 J5.0 U 5.0 U 13000 U 10 UJ 10 UJ 10 U 10 U 20 U 20 U 5.0 U 5.0 U 13000 U 10 UJ 10 U 20 U 5.0 U 5.0 U 25000 U 25000 U 10 UJ 10 U 20 U5.0 U 5.0 U 13000 U 10 UJ 10 UJ 10 U 10 U 20 U 20 U 5.0 U 14 13000 U 10 UJ 12 20 U 5.0 U 5.6 25000 U 25000 U 10 UJ 10 U 20 U5.0 UJ 5.0 U 13000 U 10 UJ 10 UJ 10 U 10 U 20 U 20 U 5.0 UJ 5.0 U 13000 U 10 UJ 10 U 20 U 5.0 UJ 5.0 U 25000 U 25000 U 10 UJ 10 U 20 U5.0 U 5.0 U 13000 U 10 UJ 10 UJ 10 U 10 U 20 U 20 U 5.0 U 5.0 U 13000 U 10 UJ 10 U 20 U 5.0 U 5.0 U 25000 U 25000 U 10 UJ 10 U 20 U5.0 U 5.0 U 13000 U 10 UJ 10 UJ 10 U 10 U 20 U 20 U 5.0 U 5.0 U 13000 U 10 UJ 10 U 20 U 5.0 U 5.0 U 25000 U 25000 U 10 UJ 10 U 20 U5.0 U 21 13000 U 10 UJ 10 UJ 69 69 320 320 5.0 U 320 13000 U 210 J 210 240 5.0 U 940 25000 U 25000 U 60 J 94 96 5.0 U 5.0 U 13000 U 10 UJ 10 UJ 10 U 10 U 20 U 20 U 5.0 U 5.0 U 13000 U 10 UJ 10 U 20 U 5.0 U 5.0 U 25000 U 25000 U 10 UJ 10 U 20 U5.0 U 5.0 U 13000 U 10 UJ 10 UJ 10 U 10 U 20 U 20 U 5.0 U 5.0 U 13000 U 10 UJ 10 U 20 U 5.0 U 5.0 U 25000 U 25000 U 10 UJ 10 U 20 U5.0 U 5.0 U 13000 U 10 UJ 10 UJ 14 15 71 72 5.0 U 170 13000 U 64 J 240 180 5.0 U 45 25000 U 25000 U 10 UJ 130 110 5.0 U 5.0 U 13000 U 10 UJ 10 UJ 10 U 10 U 20 U 20 U 5.0 U 5.0 U 13000 U 10 UJ 10 U 20 U 5.0 U 5.0 U 25000 U 25000 U 10 UJ 10 U 20 U5.0 U 5.0 U 13000 U 10 UJ 10 UJ 10 U 10 U 20 U 20 U 5.0 U 5.0 U 13000 U 10 UJ 10 U 20 U 5.0 U 5.0 U 25000 U 25000 U 10 UJ 10 U 20 U5.0 U 5.0 U 13000 U 10 UJ 10 UJ 10 U 10 U 20 U 20 U 5.0 U 5.0 U 13000 U 10 UJ 10 U 20 U 5.0 U 5.0 U 25000 U 25000 U 10 UJ 10 U 20 U5.0 U 5.0 U 13000 U 10 UJ 10 UJ 10 U 10 U 20 U 20 U 5.0 U 5.0 U 13000 U 10 UJ 10 U 20 U 5.0 U 5.0 U 25000 U 25000 U 10 UJ 10 U 20 U5.0 UJ 5.0 U 13000 U 10 UJ 10 UJ 10 U 10 U 20 U 20 U 5.0 UJ 10 13000 U 10 UJ 10 U 20 U 5.0 UJ 5.0 25000 U 25000 U 10 UJ 10 U 20 U5.0 UJ 10 U 13000 UJ 10 UJ 10 UJ 10 U 10 U 20 U 20 U 5.0 UJ 10 U 13000 U 10 UJ 10 U 20 U 5.0 UJ 10 U 25000 U 25000 U 10 UJ 10 U 20 U5.0 U 5.0 U 13000 U 10 UJ 10 UJ 10 U 10 U 20 U 20 U 5.0 U 5.0 U 13000 U 10 UJ 10 U 20 U 5.0 U 5.0 U 25000 U 25000 U 10 UJ 10 UJ 20 U5.0 U 5.0 U 13000 U 10 UJ 10 UJ 10 U 10 U 20 U 20 U 5.0 U 5.0 U 13000 U 10 UJ 10 U 20 U 5.0 U 5.0 U 25000 U 25000 U 10 UJ 10 U 20 U10 U 10 U 25000 U 20 UJ 20 UJ 20 U 20 U 40 U 40 U 10 U 10 U 25000 U 20 UJ 20 U 40 U 10 U 10 U 50000 U 50000 U 20 UJ 20 U 40 U5.0 U 5.0 U 13000 U 10 UJ 10 UJ 10 U 10 U 20 UJ 20 UJ 5.0 U 5.0 U 13000 U 10 UJ 10 U 20 UJ 5.0 U 5.0 U 25000 U 25000 U 10 UJ 10 U 20 UJ10 U 10 U 25000 U 20 UJ 20 UJ 20 U 20 U 40 U 40 U 10 U 10 U 25000 U 20 UJ 20 U 40 U 10 U 10 U 50000 U 50000 U 20 UJ 20 U 40 U5.0 U 5.0 U 13000 U 10 UJ 10 UJ 10 U 10 U 20 U 20 U 5.0 U 5.0 U 13000 U 10 UJ 10 U 20 U 5.0 U 5.0 U 25000 U 25000 U 10 UJ 10 U 20 U5.0 U 5.0 U 13000 U 10 UJ 10 UJ 10 U 10 U 20 U 20 U 5.0 U 5.0 U 13000 U 10 UJ 10 U 20 U 5.0 U 5.0 U 25000 U 25000 U 10 UJ 10 U 20 U10 UJ 10 U 25000 U 20 UJ 20 UJ 20 U 20 U 40 U 40 U 10 UJ 10 U 25000 U 20 UJ 20 U 40 U 10 UJ 10 U 50000 U 50000 U 20 UJ 20 U 40 U5.0 U 5.0 U 13000 U 10 UJ 10 UJ 10 U 10 U 20 U 20 U 5.0 U 5.0 U 13000 U 10 UJ 10 U 20 U 5.0 U 5.0 U 25000 U 25000 U 10 UJ 10 U 20 U5.0 U 5.0 U 13000 U 10 UJ 10 UJ 10 U 10 U 20 U 20 U 5.0 U 5.0 U 13000 U 10 UJ 10 U 20 U 5.0 U 5.0 U 25000 U 25000 U 10 UJ 10 U 20 U39000 5.0 U 13000 U 10 UJ 10 UJ 10 10 U 6000 6000 140000 77 13000 U 10 UJ 600 7500 J 74000 120 25000 U 25000 U 10 UJ 10 U 3200 J5.0 U 5.0 U 13000 U 10 UJ 10 UJ 10 U 10 U 20 U 20 U 5.0 U 5.0 U 13000 U 10 UJ 10 U 20 U 5.0 U 5.0 U 25000 U 25000 U 10 UJ 10 U 20 U5.0 U 5.0 U 13000 U 10 UJ 10 UJ 10 U 10 U 20 U 20 U 5.0 U 5.0 U 13000 U 10 UJ 10 U 20 U 5.0 U 5.0 U 25000 U 25000 U 10 UJ 10 U 20 U5.0 U 5.0 U 13000 U 10 UJ 10 UJ 10 U 10 U 20 U 20 U 5.0 U 5.0 U 13000 U 10 UJ 10 U 20 U 5.0 U 5.0 U 25000 U 25000 U 10 UJ 10 U 20 U12 5.0 U 13000 U 10 UJ 10 UJ 10 U 10 U 20 U 20 U 20 5.0 U 13000 U 10 UJ 10 U 20 U 39 5.0 U 25000 U 25000 U 10 UJ 10 U 20 U
5.0 U 5.0 U 13000 U 10 UJ 10 UJ 10 U 10 U 20 U 20 U 5.0 U 5.0 U 13000 U 10 UJ 10 U 20 U 5.0 U 5.0 U 25000 U 25000 U 10 UJ 10 U 20 U5.0 U 5.0 U 13000 U 10 UJ 10 UJ 10 U 10 U 20 U 20 U 5.0 U 5.0 U 13000 U 10 UJ 10 U 20 U 5.0 U 5.0 U 25000 U 25000 U 10 UJ 10 U 20 U
Purple PurplePurple Purple
Jul-10IW-08
Mar-10May-10IW-09
Apr-10IW-10
Cleburn RI Report Page 3 of 7 HydroGeoLogic, Inc. 11/12/2010
Table 4.2VOC Analytical Results
ISCO Injection and Remedial Investigation - Cleburn Street Well SiteGrand Island, NE
Monitoring Well IDSampling Date
Sample IDColoration
1,1,1-Trichloroethane 2001,1,2,2-Tetrachloroethane NE
1,1,2-Trichloroethane 51,1,2-Trichlorotrifluoroethane NE
1,1-Dichloroethane 51,1-Dichloroethene 7
1,2,3-Trichlorobenzene NE1,2,4-Trichlorobenzene 70
1,2-Dibromo-3-Chloropropane 0.21,2-Dibromoethane 0.051,2-Dichlorobenzene 6001,2-Dichloroethane NE
1,2-Dichloropropane 51,3-Dichlorobenzene NE1,4-Dichlorobenzene 75
2-Butanone (Methyl Ethyl Ketone) NE2-Hexanone NE
4-Methyl-2-Pentanone (Methyl Isobutyl Ketone) NEAcetone NEBenzene 5
Bromodichloromethane* 80Bromoform* 80
Bromomethane NECarbon Disulfide NE
Carbon Tetrachloride 5Chlorobenzene 100Chloroethane NEChloroform* 80
Chloromethane NEcis-1,2-Dichloroethene 70
cis-1,3-Dichloropropene NECyclohexane NE
Dibromochloromethane* 80Dichlorodifluoromethane NE
Ethyl Benzene 700Isopropylbenzene NE
m and/or p-Xylene 10000Methyl Acetate NE
Methyl tert-butyl ether NEMethylcyclohexane NEMethylene Chloride 5
Naphthalene NEo-Xylene 10000Styrene 100
Tetrachloroethene 5Toluene 1000
trans-1,2-Dichloroethene 100trans-1,3-Dichloropropene NE
Trichloroethene 5Trichlorofluoromethane NE
Vinyl Chloride 2
MCL Jan-10 Mar-10 Jul-10 Dec-09 Jan-10 Mar-10 Apr-10 May-10 Jul-10 Jan-10 Mar-10 Apr-10 May-10 Jul-104717-11 4717-11-FD 4766-115 4818-23 4846-17 4846-17-FD 4889-20 4889-20-FD 4981-1 4717-10 4766-116 4818-19 4862-101 4890-101 4982-102 4717-7 4717-7-FD 4766-108 4818-7 4862-110 4890-109 4982-112
Clear Clear Clear Clear Pink Punk Pink Purple Pink Purple Purple Purple Purple Purple5.0 U 5.0 U 5.0 U 5.0 U 5.0 U 5.0 U 5.0 U 5.0 U 5.0 U 5.0 U 5.0 U 100 U 5.0 U 10 U 5 U 5.0 U 5.0 U 5.0 U 25000 U 20 J 12 39 5.0 U 5.0 U 5.0 U 5.0 U 5.0 U 5.0 U 5.0 U 5.0 U 5.0 U 5.0 U 5.0 U 100 U 5.0 U 10 U 5 UJ 5.0 U 5.0 U 5.0 U 25000 U 10 UJ 10 U 20 U5.0 U 5.0 U 5.0 U 5.0 U 5.0 U 5.0 U 5.0 U 5.0 U 5.0 U 5.0 U 5.0 U 100 U 5.0 UJ 10 U 5 UJ 5.0 U 5.0 U 5.0 U 25000 U 10 UJ 10 U 20 U5.0 U 5.0 U 5.0 U 5.0 U 5.0 U 5.0 U 5.0 U 5.0 U 5.0 U 5.0 U 5.0 U 100 U 5.0 U 10 U 5 U 5.0 U 5.0 U 5.0 U 25000 U 10 UJ 10 U 20 U5.0 U 5.0 U 5.0 U 5.0 U 5.0 U 5.0 U 5.0 U 5.0 U 5.0 U 5.0 U 5.0 U 100 U 5.0 U 10 U 5 U 5.0 U 5.0 U 5.0 U 25000 U 10 UJ 10 U 20 U5.0 U 5.0 U 5.0 U 5.0 U 5.0 U 5.0 U 5.0 U 5.0 U 5.0 U 5.0 U 5.0 U 100 U 5.0 U 10 U 5 U 5.0 U 5.0 U 5.0 U 25000 U 10 UJ 10 U 20 U5.0 UJ 5.0 UJ 5.0 U 5.0 U 5.0 U 5.0 U 5.0 U 5.0 U 5.0 U 5.0 UJ 5.0 U 100 U 5.0 U 10 U 5 UJ 5.0 UJ 5.0 UJ 5.0 U 25000 U 10 UJ 10 U 20 U5.0 UJ 5.0 UJ 5.0 U 5.0 U 5.0 U 5.0 U 5.0 U 5.0 U 5.0 U 5.0 UJ 5.0 U 100 U 5.0 U 10 U 5 U 5.0 UJ 5.0 UJ 5.0 U 25000 U 10 UJ 10 U 20 U5.0 UJ 5.0 UJ 5.0 U 5.0 U 5.0 U 5.0 U 5.0 U 5.0 U 5.0 U 5.0 UJ 5.0 U 100 U 5.0 U 10 U 5 UJ 5.0 UJ 5.0 UJ 5.0 U 25000 U 10 UJ 10 U 20 U5.0 UJ 5.0 UJ 5.0 U 5.0 U 5.0 U 5.0 U 5.0 U 5.0 U 5.0 U 5.0 U 5.0 U 100 U 5.0 UJ 10 UJ 5 UJ 5.0 UJ 5.0 UJ 5.0 U 25000 U 10 UJ 10 U 20 U5.0 U 5.0 U 5.0 U 5.0 U 5.0 U 5.0 U 5.0 U 5.0 U 5.0 U 5.0 U 5.0 U 100 U 5.0 U 10 U 5 U 5.0 U 5.0 U 5.0 U 25000 U 10 UJ 10 U 20 U5.0 UJ 5.0 UJ 5.0 U 5.0 U 5.0 U 5.0 U 5.0 U 5.0 U 5.0 U 5.0 UJ 5.0 U 100 U 5.0 U 10 U 5 U 5.0 UJ 5.0 UJ 5.0 U 25000 U 10 UJ 10 U 20 U5.0 U 5.0 U 5.0 U 5.0 U 5.0 U 5.0 U 5.0 U 5.0 U 5.0 U 5.0 U 5.0 U 100 U 5.0 U 10 U 5 UJ 5.0 U 5.0 U 5.0 U 25000 U 10 UJ 10 U 20 U5.0 U 5.0 U 5.0 U 5.0 U 5.0 U 5.0 U 5.0 U 5.0 U 5.0 U 5.0 U 5.0 U 100 U 5.0 U 10 UJ 5 U 5.0 U 5.0 U 5.0 U 25000 U 10 UJ 10 U 20 U5.0 U 5.0 U 5.0 U 5.0 U 5.0 U 5.0 U 5.0 U 5.0 U 5.0 U 5.0 U 5.0 U 100 U 5.0 U 10 U 5 U 5.0 U 5.0 U 5.0 U 25000 U 10 UJ 10 U 20 U5.0 U 5.0 U 5.0 U 5.0 U 5.0 U 5.0 U 5.0 U 5.0 U 5.0 UJ 5.0 U 5.0 U 100 U 5.0 U 10 U 5 U 5.0 U 5.0 U 17 25000 U 10 UJ 10 U 20 UJ5.0 UJ 5.0 UJ 5.0 U 5.0 U 5.0 U 5.0 U 5.0 U 5.0 U 5.0 UJ 5.0 UJ 5.0 U 100 U 5.0 U 10 U 5 UJ 5.0 UJ 5.0 UJ 5.0 U 25000 U 10 UJ 10 U 20 UJ5.0 UJ 5.0 UJ 5.0 U 5.0 U 5.0 U 5.0 U 5.0 U 5.0 U 5.0 U 5.0 UJ 5.0 U 100 U 5.0 UJ 10 U 5 UJ 5.0 UJ 5.0 UJ 5.0 U 25000 U 10 UJ 10 U 20 U5.0 U 5.0 U 5.0 U 5.0 U 5.0 U 5.0 U 5.0 U 5.0 U 5.0 UJ 5.0 U 23 U 100 U 8.8 16 9 J 5.0 U 5.0 U 240 25000 U 190 J 510 100 J5.0 U 5.0 U 5.0 U 5.0 U 5.0 U 5.0 U 5.0 U 5.0 U 5.0 U 5.0 U 5.0 U 100 U 5.0 U 10 U 5 UJ 5.0 U 5.0 U 5.0 U 25000 U 10 UJ 10 U 20 U5.0 U 5.0 U 5.0 U 5.0 U 5.0 U 5.0 U 5.0 U 5.0 U 5.0 U 5.0 U 5.0 U 100 U 5.0 U 10 U 5 U 5.0 U 5.0 U 5.0 U 25000 U 10 UJ 10 U 20 U5.0 UJ 5.0 UJ 5.0 U 5.0 U 5.0 U 5.0 U 5.0 U 5.0 U 5.0 U 5.0 UJ 5.0 U 100 U 5.0 UJ 10 U 5 UJ 5.0 UJ 5.0 UJ 5.0 U 25000 U 10 UJ 10 U 20 U5.0 U 5.0 U 5.0 U 5.0 U 5.0 U 5.0 U 5.0 U 5.0 U 5.0 U 5.0 U 5.0 U 100 U 5.0 U 10 U 5 U 5.0 U 5.0 U 5.0 U 25000 U 10 UJ 10 U 20 U5.0 U 5.0 U 5.0 U 5.0 U 5.0 U 5.0 U 5.0 U 5.0 U 5.0 U 5.0 U 5.0 U 100 U 5.0 U 10 U 5 U 5.0 U 5.0 U 5.0 U 25000 U 10 UJ 10 U 20 U5.0 U 5.0 U 5.0 U 5.0 U 5.0 U 5.0 U 5.0 U 5.0 U 5.0 UJ 5.0 U 5.0 U 100 U 5.0 U 10 U 5 U 5.0 U 5.0 U 5.0 U 25000 U 540 J 380 1200 5.0 U 5.0 U 5.0 U 5.0 U 5.0 U 5.0 U 5.0 U 5.0 U 5.0 U 5.0 U 5.0 U 100 U 5.0 U 10 U 5 U 5.0 U 5.0 U 5.0 U 25000 U 10 UJ 10 U 20 U5.0 U 5.0 U 5.0 U 5.0 U 5.0 U 5.0 U 5.0 U 5.0 U 5.0 U 5.0 U 5.0 U 100 U 5.0 U 10 UJ 5 UJ 5.0 U 5.0 U 5.0 U 25000 U 10 UJ 10 U 20 U5.0 U 5.0 U 5.0 U 5.0 U 5.0 U 5.0 U 5.0 U 5.0 U 5.0 U 5.0 U 5.0 U 100 U 5.0 U 10 U 5 U 5.0 U 5.0 U 19 25000 U 150 J 200 390 5.0 U 5.0 U 5.0 U 5.0 U 5.0 U 5.0 U 5.0 U 5.0 U 5.0 U 5.0 U 5.0 U 100 U 5.0 U 10 U 5 UJ 5.0 U 5.0 U 5.0 U 25000 U 10 UJ 10 U 20 U5.0 U 5.0 U 5.0 U 5.0 U 5.0 U 5.0 U 5.0 U 5.0 U 5.0 U 5.0 U 5.0 U 100 U 5.0 U 10 U 5 U 5.0 U 5.0 U 5.0 U 25000 U 10 UJ 10 U 20 U5.0 U 5.0 U 5.0 U 5.0 U 5.0 U 5.0 U 5.0 U 5.0 U 5.0 U 5.0 U 5.0 U 100 U 5.0 U 10 U 5 U 5.0 U 5.0 U 5.0 U 25000 U 10 UJ 10 U 20 U5.0 U 5.0 U 5.0 U 5.0 U 5.0 U 5.0 U 5.0 U 5.0 U 5.0 U 5.0 U 5.0 U 100 U 5.0 U 10 U 5 UJ 5.0 U 5.0 U 5.0 U 25000 U 10 UJ 10 U 20 U5.0 UJ 5.0 UJ 5.0 U 5.0 U 5.0 U 5.0 U 5.0 U 5.0 U 5.0 U 5.0 UJ 5.0 U 100 U 5.0 U 10 U 5 UJ 5.0 UJ 5.0 UJ 5.0 U 25000 U 10 UJ 10 U 20 U5.0 UJ 5.0 UJ 10 U 5.0 U 5.0 U 5.0 U 5.0 U 5.0 U 5.0 U 5.0 UJ 10 U 100 UJ 5.0 U 10 U 5 UJ 5.0 UJ 5.0 UJ 10 U 25000 UJ 10 UJ 10 U 20 U5.0 U 5.0 U 5.0 U 5.0 U 5.0 U 5.0 U 5.0 U 5.0 U 5.0 U 5.0 U 5.0 U 100 U 5.0 U 10 U 5 U 5.0 U 5.0 U 5.0 U 25000 U 10 UJ 10 U 20 U5.0 U 5.0 U 5.0 U 5.0 U 5.0 U 5.0 U 5.0 U 5.0 U 5.0 U 5.0 U 5.0 U 100 U 5.0 U 10 U 5 U 5.0 U 5.0 U 5.0 U 25000 U 10 UJ 10 U 20 U10 U 10 U 10 U 10 U 10 U 10 U 10 U 10 U 10 U 10 U 10 U 200 U 10 U 20 U 10 U 10 U 10 U 10 U 50000 U 20 UJ 20 U 40 U5.0 U 5.0 U 5.0 U 5.0 U 5.0 U 5.0 U 5.0 U 5.0 U 5.0 U 5.0 U 5.0 U 100 U 5.0 UJ 10 U 5 UJ 5.0 U 5.0 U 5.0 U 25000 U 10 UJ 10 U 20 UJ10 U 10 U 10 U 10 U 10 U 10 U 10 UJ 10 UJ 10 U 10 U 10 U 200 U 10 U 20 U 10 U 10 U 10 U 10 U 50000 U 20 UJ 20 U 40 U5.0 U 5.0 U 5.0 U 5.0 U 5.0 U 5.0 U 5.0 U 5.0 U 5.0 U 5.0 U 5.0 U 100 U 5.0 U 10 U 5 U 5.0 U 5.0 U 5.0 U 25000 U 10 UJ 10 U 20 U5.0 U 5.0 U 5.0 U 5.0 U 5.0 U 5.0 U 5.0 U 5.0 U 5.0 U 5.0 U 5.0 U 100 U 5.0 UJ 10 U 5 U 5.0 U 5.0 U 5.0 U 25000 U 10 UJ 10 U 20 U10 UJ 10 UJ 10 U 10 U 10 U 10 U 10 U 10 U 10 U 10 UJ 10 U 200 U 10 UJ 20 U 10 UJ 10 UJ 10 UJ 10 U 50000 U 20 UJ 20 U 40 U5.0 U 5.0 U 5.0 U 5.0 U 5.0 U 5.0 U 5.0 U 5.0 U 5.0 U 5.0 U 5.0 U 100 U 5.0 U 10 U 5 U 5.0 U 5.0 U 5.0 U 25000 U 10 UJ 10 U 20 U5.0 U 5.0 U 5.0 U 5.0 U 5.0 U 5.0 U 5.0 U 5.0 U 5.0 U 5.0 U 5.0 U 100 U 5.0 U 10 U 5 U 5.0 U 5.0 U 5.0 U 25000 U 10 UJ 10 U 20 U350 370 11 11 7.8 7.0 11 11 5.0 U 6.7 5.0 U 100 U 5.0 U 10 U 5 U 11000 11000 97 25000 U 10 UJ 34 2000 5.0 U 5.0 U 5.0 U 5.0 U 5.0 U 5.0 U 5.0 U 5.0 U 5.0 U 5.0 U 5.0 U 100 U 5.0 U 10 U 5 U 5.0 U 5.0 U 5.0 U 25000 U 10 UJ 10 U 20 U5.0 U 5.0 U 5.0 U 5.0 U 5.0 U 5.0 U 5.0 U 5.0 U 5.0 U 5.0 U 5.0 U 100 U 5.0 U 10 U 5 U 5.0 U 5.0 U 5.0 U 25000 U 10 UJ 10 U 20 U5.0 U 5.0 U 5.0 U 5.0 U 5.0 U 5.0 U 5.0 U 5.0 U 5.0 U 5.0 U 5.0 U 100 U 5.0 U 10 U 5 UJ 5.0 U 5.0 U 5.0 U 25000 U 10 UJ 10 U 20 U5.0 U 5.0 U 5.0 U 5.0 U 5.0 U 5.0 U 5.0 U 5.0 U 5.0 U 5.0 U 5.0 U 100 U 5.0 U 10 U 5 U 5.0 U 5.0 U 5.0 U 25000 U 10 UJ 10 U 20 U5.0 U 5.0 U 5.0 U 5.0 U 5.0 U 5.0 U 5.0 U 5.0 U 5.0 U 5.0 U 5.0 U 100 U 5.0 U 10 U 5 U 5.0 U 5.0 U 5.0 U 25000 U 10 UJ 10 U 20 U5.0 U 5.0 U 5.0 U 5.0 U 5.0 U 5.0 U 5.0 U 5.0 U 5.0 U 5.0 U 5.0 U 100 U 5.0 U 10 U 5 U 5.0 U 5.0 U 5.0 U 25000 U 10 UJ 10 U 20 U
Clear ClearClear Clear
ERT-14Dec-09Dec-09 May-10
ERT-15Apr-10
ERT-16
Cleburn RI Report Page 4 of 7 HydroGeoLogic, Inc. 11/12/2010
Table 4.2VOC Analytical Results
ISCO Injection and Remedial Investigation - Cleburn Street Well SiteGrand Island, NE
Monitoring Well IDSampling Date
Sample IDColoration
1,1,1-Trichloroethane 2001,1,2,2-Tetrachloroethane NE
1,1,2-Trichloroethane 51,1,2-Trichlorotrifluoroethane NE
1,1-Dichloroethane 51,1-Dichloroethene 7
1,2,3-Trichlorobenzene NE1,2,4-Trichlorobenzene 70
1,2-Dibromo-3-Chloropropane 0.21,2-Dibromoethane 0.051,2-Dichlorobenzene 6001,2-Dichloroethane NE
1,2-Dichloropropane 51,3-Dichlorobenzene NE1,4-Dichlorobenzene 75
2-Butanone (Methyl Ethyl Ketone) NE2-Hexanone NE
4-Methyl-2-Pentanone (Methyl Isobutyl Ketone) NEAcetone NEBenzene 5
Bromodichloromethane* 80Bromoform* 80
Bromomethane NECarbon Disulfide NE
Carbon Tetrachloride 5Chlorobenzene 100Chloroethane NEChloroform* 80
Chloromethane NEcis-1,2-Dichloroethene 70
cis-1,3-Dichloropropene NECyclohexane NE
Dibromochloromethane* 80Dichlorodifluoromethane NE
Ethyl Benzene 700Isopropylbenzene NE
m and/or p-Xylene 10000Methyl Acetate NE
Methyl tert-butyl ether NEMethylcyclohexane NEMethylene Chloride 5
Naphthalene NEo-Xylene 10000Styrene 100
Tetrachloroethene 5Toluene 1000
trans-1,2-Dichloroethene 100trans-1,3-Dichloropropene NE
Trichloroethene 5Trichlorofluoromethane NE
Vinyl Chloride 2
MCL Dec-09 Jan-10 Apr-10 May-10 Jul-10 Dec-09 Jan-10 Mar-10 Apr-10 May-10 Jul-10 Dec-09 Jan-10 Mar-10 Apr-10 May-10 Jul-10 Jan-10 Mar-10 Apr-10 May-10 Jul-104717-15 4766-113 4818-17 4818-17-FD 4862-115 4890-113 4982-117 4717-18 4766-114 4818-20 4648-18 4889-19 4981-19 4717-13 4766-112 4818-16 4846-16 4889-17 4981-18 4766-117 4818-15 4862-121 4890-115 4982-113Clear Purple Purple Purple Purple Clear Clear Clear Clear Clear Clear Clear Clear Clear Clear Clear Clear Purple Purple Purple Purple Purple30 30 25000 U 25000 U 55 42 100 U 5.0 U 5.0 U 5.0 U 5.0 U 5.0 U 5.0 UJ 5.0 U 5.0 U 5.0 U 5.0 U 5.0 U 5.0 U 5.0 U 13000 U 5.0 U 10 U 20 U
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Purple
DPE-1MW-2A MW-12A MW-2BMar-10
Cleburn RI Report Page 5 of 7 HydroGeoLogic, Inc. 11/12/2010
Table 4.2VOC Analytical Results
ISCO Injection and Remedial Investigation - Cleburn Street Well SiteGrand Island, NE
Monitoring Well IDSampling Date
Sample IDColoration
1,1,1-Trichloroethane 2001,1,2,2-Tetrachloroethane NE
1,1,2-Trichloroethane 51,1,2-Trichlorotrifluoroethane NE
1,1-Dichloroethane 51,1-Dichloroethene 7
1,2,3-Trichlorobenzene NE1,2,4-Trichlorobenzene 70
1,2-Dibromo-3-Chloropropane 0.21,2-Dibromoethane 0.051,2-Dichlorobenzene 6001,2-Dichloroethane NE
1,2-Dichloropropane 51,3-Dichlorobenzene NE1,4-Dichlorobenzene 75
2-Butanone (Methyl Ethyl Ketone) NE2-Hexanone NE
4-Methyl-2-Pentanone (Methyl Isobutyl Ketone) NEAcetone NEBenzene 5
Bromodichloromethane* 80Bromoform* 80
Bromomethane NECarbon Disulfide NE
Carbon Tetrachloride 5Chlorobenzene 100Chloroethane NEChloroform* 80
Chloromethane NEcis-1,2-Dichloroethene 70
cis-1,3-Dichloropropene NECyclohexane NE
Dibromochloromethane* 80Dichlorodifluoromethane NE
Ethyl Benzene 700Isopropylbenzene NE
m and/or p-Xylene 10000Methyl Acetate NE
Methyl tert-butyl ether NEMethylcyclohexane NEMethylene Chloride 5
Naphthalene NEo-Xylene 10000Styrene 100
Tetrachloroethene 5Toluene 1000
trans-1,2-Dichloroethene 100trans-1,3-Dichloropropene NE
Trichloroethene 5Trichlorofluoromethane NE
Vinyl Chloride 2
MCL Jan-10 Mar-10 Apr-10 May-10 Jul-10 Jan-10 Mar-10 Apr-10 May-10 Jul-10 Jan-10 Mar-10 Apr-10 May-10 Jul-10 Dec-09 Mar-10 Apr-10 May-10 Jul-104766-118 4818-14 4862-122 4890-116 4982-114 4766-119 4818-22 4862-120 4890-114 4982-115 4766-120 4818-21 4862-119 4890-118 4982-116 4717-19-FB 4818-26-FB 4862-126-FB 4890-124-FB 4982-124-FBPurple Purple Purple Purple Purple Purple Purple Purple Purple Purple Purple Purple Purple Purple Purple Clear Clear Clear Clear Clear5.0 U 13000 U 5.0 U 10 U 20 U 35 25000 U 16 24 94 J 5.0 U 25000 U 5.0 U 11 50 U 5.0 U 5.0 U 5.0 U 5.0 UJ 20 U5.0 U 13000 U 5.0 UJ 10 U 20 U 5.0 U 25000 U 5.0 UJ 10 U 20 U 5.0 U 25000 U 5.0 UJ 10 U 50 U 5.0 U 5.0 U 5.0 U 5.0 UJ 20 U5.0 U 13000 U 5.0 UJ 10 U 20 U 5.0 U 25000 U 5.0 UJ 10 U 20 U 5.0 U 25000 U 5.0 UJ 10 U 50 U 5.0 U 5.0 U 5.0 U 5.0 UJ 20 U5.0 U 13000 U 5.0 U 10 U 20 U 5.0 U 25000 U 5.0 U 10 U 20 UJ 5.0 U 25000 U 5.0 U 10 U 50 U 5.0 U 5.0 U 5.0 U 5.0 UJ 20 U5.0 U 13000 U 5.0 U 10 U 20 U 5.0 U 25000 U 5.0 U 10 U 20 UJ 5.0 U 25000 U 5.0 U 10 U 50 U 5.0 U 5.0 U 5.0 U 5.0 UJ 20 U5.0 U 13000 U 5.0 U 10 U 20 U 5.0 U 25000 U 5.0 U 10 U 20 UJ 5.0 U 25000 U 5.0 U 10 U 50 U 5.0 U 5.0 U 5.0 U 5.0 UJ 20 U5.0 U 13000 U 5.0 U 10 U 20 U 5.0 U 25000 U 5.0 U 10 U 20 U 5.0 U 25000 U 5.0 U 10 U 50 U 5.0 UJ 5.0 U 5.0 U 5.0 UJ 20 U5.0 U 13000 U 5.0 U 10 U 20 U 5.0 U 25000 U 5.0 U 10 U 20 U 5.0 U 25000 U 5.0 U 10 U 50 U 5.0 UJ 5.0 U 5.0 U 5.0 UJ 20 U5.0 U 13000 U 5.0 UJ 10 U 20 U 5.0 U 25000 U 5.0 UJ 10 U 20 U 5.0 U 25000 U 5.0 UJ 10 U 50 U 5.0 UJ 5.0 U 5.0 U 5.0 UJ 20 U5.0 U 13000 U 5.0 UJ 10 UJ 20 U 5.0 U 25000 U 5.0 UJ 10 UJ 20 U 5.0 U 25000 U 5.0 UJ 10 UJ 50 U 5.0 UJ 5.0 U 5.0 U 5.0 UJ 20 U5.0 U 13000 U 5.0 U 10 U 20 U 5.0 U 25000 U 5.0 U 10 U 20 U 5.0 U 25000 U 5.0 U 10 U 50 U 5.0 U 5.0 U 5.0 U 5.0 UJ 20 U5.0 U 13000 U 5.0 UJ 10 U 20 U 5.0 U 25000 U 5.0 UJ 10 U 20 U 5.0 U 25000 U 5.0 UJ 10 U 50 U 5.0 UJ 5.0 U 5.0 U 5.0 UJ 20 U5.0 U 13000 U 5.0 UJ 10 UJ 20 U 5.0 U 25000 U 5.0 UJ 10 UJ 20 U 5.0 U 25000 U 5.0 UJ 10 UJ 50 U 5.0 U 5.0 U 5.0 U 5.0 UJ 20 U5.0 U 13000 U 5.0 U 10 U 20 U 5.0 U 25000 U 5.0 U 10 U 20 U 5.0 U 25000 U 5.0 U 10 U 50 U 5.0 U 5.0 U 5.0 U 5.0 UJ 20 U5.0 U 13000 U 5.0 U 10 U 20 U 5.0 U 25000 U 5.0 U 10 U 20 U 5.0 U 25000 U 5.0 U 10 U 50 U 5.0 U 5.0 U 5.0 U 5.0 UJ 20 U67 13000 U 5.0 UJ 10 U 20 UJ 24 25000 U 5.0 UJ 10 U 20 UJ 120 25000 U 5.0 UJ 10 U 50 U 5.0 U 5.0 U 5.0 U 5.0 UJ 20 UJ
5.0 U 13000 U 5.0 UJ 10 U 20 UJ 5.0 U 25000 U 5.0 UJ 10 U 20 UJ 5.0 U 25000 U 5.0 UJ 10 U 50 U 5.0 UJ 5.0 U 5.0 U 5.0 UJ 20 UJ5.0 U 13000 U 5.0 UJ 10 U 20 U 5.0 U 25000 U 5.0 UJ 10 U 20 U 5.0 U 25000 U 5.0 UJ 10 U 50 U 5.0 UJ 5.0 U 5.0 U 5.0 UJ 20 U56 13000 U 9.5 J 47 31 J 200 25000 U 34 J 230 67 J 150 25000 U 14 J 42 60 5.0 U 5.0 U 5.0 U 6.2 J 20 UJ
5.0 U 13000 U 5.0 UJ 10 U 20 U 5.0 U 25000 U 5.0 UJ 10 U 20 U 5.0 U 25000 U 5.0 UJ 10 U 50 U 5.0 U 5.0 U 5.0 U 5.0 UJ 20 U5.0 U 13000 U 5.0 UJ 10 U 20 U 5.0 25000 U 5.0 UJ 10 U 20 U 5.0 U 25000 U 5.0 UJ 10 U 50 U 5.0 U 5.0 U 5.0 U 5.0 UJ 20 U5.0 U 13000 U 5.0 UJ 10 U 20 U 5.0 U 25000 U 5.0 UJ 10 U 20 U 5.0 U 25000 U 5.0 UJ 10 U 50 U 5.0 UJ 5.0 U 5.0 U 5.0 UJ 20 U5.0 U 13000 U 5.0 U 10 U 20 U 5.0 U 25000 U 5.0 U 10 U 20 UJ 5.0 U 25000 U 5.0 U 10 U 50 U 5.0 U 5.0 U 5.0 U 5.0 UJ 20 U5.0 U 13000 U 5.0 U 10 U 20 U 5.0 U 25000 U 5.0 U 10 U 20 UJ 5.0 U 25000 U 5.0 U 10 U 50 U 5.0 U 5.0 U 5.0 U 5.0 UJ 20 U5.0 U 13000 U 5.0 U 10 U 20 U 41 25000 U 98 98 270 J 5.0 U 25000 U 5.0 U 240 250 5.0 U 5.0 U 5.0 U 5.0 UJ 20 U5.0 U 13000 U 5.0 U 10 U 20 U 5.0 U 25000 U 5.0 U 10 U 20 U 5.0 U 25000 U 5.0 U 10 U 50 U 5.0 U 5.0 U 5.0 U 5.0 UJ 20 U5.0 U 13000 U 5.0 U 10 U 20 U 5.0 U 25000 U 5.0 U 10 U 20 UJ 5.0 U 25000 U 5.0 U 10 U 50 U 5.0 U 5.0 U 5.0 U 5.0 UJ 20 U5.0 U 13000 U 5.0 U 10 U 20 U 120 25000 U 45 100 410 J 5.0 U 25000 U 5.0 U 26 50 U 5.0 U 5.0 U 5.0 U 5.0 UJ 20 U5.0 U 13000 U 5.0 U 10 U 20 U 5.0 U 25000 U 5.0 U 10 U 20 UJ 5.0 U 25000 U 5.0 U 10 U 50 U 5.0 U 5.0 U 5.0 U 5.0 UJ 20 U5.0 U 13000 U 5.0 U 10 U 20 U 5.0 U 25000 U 5.0 U 10 U 20 UJ 5.0 U 25000 U 5.0 U 10 U 50 U 5.0 U 5.0 U 5.0 U 5.0 UJ 20 U5.0 U 13000 U 5.0 UJ 10 U 20 U 5.0 U 25000 U 5.0 UJ 10 U 20 U 5.0 U 25000 U 5.0 UJ 10 U 50 U 5.0 U 5.0 U 5.0 U 5.0 UJ 20 U5.0 U 13000 U 5.0 U 10 U 20 U 5.0 U 25000 U 5.0 U 10 U 20 UJ 5.0 U 25000 U 5.0 U 10 U 50 U 5.0 U 5.0 U 5.0 U 5.0 UJ 20 U5.0 U 13000 U 5.0 UJ 10 U 20 U 5.0 U 25000 U 5.0 UJ 10 U 20 U 5.0 U 25000 U 5.0 UJ 10 U 50 U 5.0 UJ 5.0 U 5.0 U 5.0 UJ 20 U10 U 13000 U 5.0 U 10 U 20 U 10 U 25000 U 5.0 U 10 U 20 UJ 10 U 25000 U 5.0 U 10 U 50 U 5.0 UJ 5.0 UJ 5.0 U 5.0 UJ 20 U5.0 U 13000 U 5.0 U 10 UJ 20 U 5.0 U 25000 U 5.0 U 10 UJ 20 U 5.0 U 25000 U 5.0 U 10 UJ 50 U 5.0 U 5.0 U 5.0 U 5.0 UJ 20 U5.0 U 13000 U 5.0 U 10 U 20 U 5.0 U 25000 U 5.0 U 10 U 20 U 5.0 U 25000 U 5.0 U 10 U 50 U 5.0 U 5.0 U 5.0 U 5.0 UJ 20 U10 U 25000 U 10 U 20 U 40 U 10 U 50000 U 10 U 20 U 40 U 10 U 50000 U 10 U 20 U 100 U 10 U 10 U 10 U 10 UJ 40 U5.0 U 13000 U 5.0 UJ 10 U 20 UJ 5.0 U 25000 U 5.0 UJ 10 U 20 UJ 5.0 U 25000 U 5.0 UJ 10 U 50 U 5.0 U 5.0 U 5.0 U 5.0 UJ 20 UJ10 U 25000 U 10 U 20 U 40 U 10 U 50000 U 10 U 20 U 40 UJ 10 U 50000 U 10 U 20 U 100 U 10 U 10 U 10 U 10 UJ 40 U5.0 U 13000 U 5.0 UJ 10 U 20 U 5.0 U 25000 U 5.0 UJ 10 U 20 U 5.0 U 25000 U 5.0 UJ 10 U 50 U 5.0 U 5.0 U 5.0 U 5.0 UJ 20 U5.0 U 13000 U 5.0 U 10 U 20 U 5.0 U 25000 U 5.0 U 10 U 20 UJ 5.0 U 25000 U 5.0 U 10 U 50 U 5.0 U 5.0 U 5.0 UJ 5.0 UJ 20 U10 U 25000 U 10 UJ 20 U 40 U 10 U 50000 U 10 UJ 20 U 40 U 10 U 50000 U 10 UJ 20 U 100 U 10 UJ 10 U 10 U 10 UJ 40 U5.0 U 13000 U 5.0 U 10 U 20 U 5.0 U 25000 U 5.0 U 10 U 20 U 5.0 U 25000 U 5.0 U 10 U 50 U 5.0 U 5.0 U 5.0 U 5.0 UJ 20 U5.0 U 13000 U 5.0 U 10 U 20 U 5.0 U 25000 U 5.0 U 10 U 20 U 5.0 U 25000 U 5.0 U 10 U 50 U 5.0 U 5.0 U 5.0 U 5.0 UJ 20 U5.0 U 13000 U 5.0 U 10 U 20 43 25000 U 55 10 U 20 U 5.0 U 25000 U 5.0 U 10 U 50 U 5.0 U 5.0 U 5.0 U 5.0 UJ 88 5.0 U 13000 U 5.0 UJ 10 U 20 U 5.0 U 25000 U 5.0 UJ 10 U 20 U 5.0 U 25000 U 5.0 UJ 10 U 50 U 5.0 U 5.0 U 5.0 U 5.0 UJ 20 U5.0 U 13000 U 5.0 U 10 U 20 U 5.0 U 25000 U 5.0 U 10 U 20 UJ 5.0 U 25000 U 5.0 U 10 U 50 U 5.0 U 5.0 U 5.0 U 5.0 UJ 20 U5.0 U 13000 U 5.0 U 10 U 20 U 5.0 U 25000 U 5.0 U 10 U 20 U 5.0 U 25000 U 5.0 U 10 U 50 U 5.0 U 5.0 U 5.0 U 5.0 UJ 20 U5.0 U 13000 U 5.0 UJ 10 U 20 U 5.0 U 25000 U 5.0 UJ 10 U 20 U 5.0 U 25000 U 5.0 UJ 10 U 50 U 5.0 U 5.0 U 5.0 U 5.0 UJ 20 U5.0 U 13000 U 5.0 U 10 U 20 U 5.0 U 25000 U 5.0 U 10 U 20 UJ 5.0 U 25000 U 5.0 U 10 U 50 U 5.0 U 5.0 U 5.0 U 5.0 UJ 20 U5.0 U 13000 U 5.0 U 10 U 20 U 5.0 U 25000 U 5.0 U 10 U 20 UJ 5.0 U 25000 U 5.0 U 10 U 50 U 5.0 U 5.0 U 5.0 U 5.0 UJ 20 U
DPE-2 DPE-3 DPE-4 Field Blank
Cleburn RI Report Page 6 of 7 HydroGeoLogic, Inc. 11/12/2010
Table 4.2VOC Analytical Results
ISCO Injection and Remedial Investigation - Cleburn Street Well SiteGrand Island, NE
Monitoring Well IDSampling Date
Sample IDColoration
1,1,1-Trichloroethane 2001,1,2,2-Tetrachloroethane NE
1,1,2-Trichloroethane 51,1,2-Trichlorotrifluoroethane NE
1,1-Dichloroethane 51,1-Dichloroethene 7
1,2,3-Trichlorobenzene NE1,2,4-Trichlorobenzene 70
1,2-Dibromo-3-Chloropropane 0.21,2-Dibromoethane 0.051,2-Dichlorobenzene 6001,2-Dichloroethane NE
1,2-Dichloropropane 51,3-Dichlorobenzene NE1,4-Dichlorobenzene 75
2-Butanone (Methyl Ethyl Ketone) NE2-Hexanone NE
4-Methyl-2-Pentanone (Methyl Isobutyl Ketone) NEAcetone NEBenzene 5
Bromodichloromethane* 80Bromoform* 80
Bromomethane NECarbon Disulfide NE
Carbon Tetrachloride 5Chlorobenzene 100Chloroethane NEChloroform* 80
Chloromethane NEcis-1,2-Dichloroethene 70
cis-1,3-Dichloropropene NECyclohexane NE
Dibromochloromethane* 80Dichlorodifluoromethane NE
Ethyl Benzene 700Isopropylbenzene NE
m and/or p-Xylene 10000Methyl Acetate NE
Methyl tert-butyl ether NEMethylcyclohexane NEMethylene Chloride 5
Naphthalene NEo-Xylene 10000Styrene 100
Tetrachloroethene 5Toluene 1000
trans-1,2-Dichloroethene 100trans-1,3-Dichloropropene NE
Trichloroethene 5Trichlorofluoromethane NE
Vinyl Chloride 2
MCL Dec-09 Jan-10 Mar-10 Apr-10 May-10 Jul-104717-21-FB 4766-121-FB 4818-27-FB 4862-129-FB 4889-52-FB 4982-153-FB
Clear Clear Clear Clear Clear Clear5.0 U 5.0 U 5.0 U 5.0 U 5.0 U 20 U5.0 U 5.0 U 5.0 U 5.0 U 5.0 U 20 U5.0 U 5.0 U 5.0 U 5.0 U 5.0 U 20 U5.0 U 5.0 U 5.0 U 5.0 U 5.0 U 20 U5.0 U 5.0 U 5.0 U 5.0 U 5.0 U 20 U5.0 U 5.0 U 5.0 U 5.0 U 5.0 U 20 U5.0 UJ 5.0 U 5.0 U 5.0 U 5.0 U 20 U5.0 UJ 5.0 U 5.0 U 5.0 U 5.0 U 20 U5.0 UJ 5.0 U 5.0 U 5.0 U 5.0 U 20 U5.0 UJ 5.0 U 5.0 U 5.0 U 5.0 U 20 U5.0 U 5.0 U 5.0 U 5.0 U 5.0 U 20 U5.0 UJ 5.0 U 5.0 U 5.0 U 5.0 U 20 U5.0 U 5.0 U 5.0 U 5.0 U 5.0 U 20 U5.0 U 5.0 U 5.0 U 5.0 U 5.0 U 20 U5.0 U 5.0 U 5.0 U 5.0 U 5.0 U 20 U5.0 U 5.0 U 5.0 U 5.0 U 5.0 U 20 UJ5.0 UJ 5.0 U 5.0 U 5.0 U 5.0 U 20 UJ5.0 UJ 5.0 U 5.0 U 5.0 U 5.0 U 20 U5.0 U 17 5.0 U 35 5.0 U 43 J5.0 U 5.0 U 5.0 U 5.0 U 5.0 U 20 U5.0 U 5.0 U 5.0 U 5.0 U 5.0 U 20 U5.0 UJ 5.0 U 5.0 U 5.0 U 5.0 U 20 U5.0 U 5.0 U 5.0 U 5.0 U 5.0 U 20 U5.0 U 5.0 U 5.0 U 5.0 U 5.0 U 20 U5.0 U 5.0 U 5.0 U 5.0 U 5.0 U 20 U5.0 U 5.0 U 5.0 U 5.0 U 5.0 U 20 U5.0 U 5.0 U 5.0 U 5.0 U 5.0 U 20 U5.0 U 5.0 U 5.0 U 5.0 U 5.0 U 20 U5.0 U 5.0 U 5.0 U 5.0 U 5.0 U 20 U5.0 U 5.0 U 5.0 U 5.0 U 5.0 U 20 U5.0 U 5.0 U 5.0 U 5.0 U 5.0 U 20 U5.0 U 5.0 U 5.0 U 5.0 U 5.0 U 20 U5.0 UJ 5.0 U 5.0 U 5.0 U 5.0 U 20 U5.0 UJ 10 U 5.0 UJ 5.0 U 5.0 UJ 20 U5.0 U 5.0 U 5.0 U 5.0 U 5.0 U 20 U5.0 U 5.0 U 5.0 U 5.0 U 5.0 U 20 U10 U 10 U 10 U 10 U 10 U 40 U5.0 U 5.0 U 5.0 U 5.0 U 5.0 U 20 UJ10 U 10 U 10 U 10 U 10 U 40 U5.0 U 5.0 U 5.0 U 5.0 U 5.0 U 20 U5.0 U 5.0 U 5.0 U 5.0 UJ 5.0 U 20 U10 UJ 10 U 10 U 10 U 10 U 40 U5.0 U 5.0 U 5.0 U 5.0 U 5.0 U 20 U5.0 U 5.0 U 5.0 U 5.0 U 5.0 U 20 U5.0 U 5.0 U 5.0 U 5.0 U 5.0 U 20 U5.0 U 5.0 U 5.0 U 5.0 U 5.0 U 20 U5.0 U 5.0 U 5.0 U 5.0 U 5.0 U 20 U5.0 U 5.0 U 5.0 U 5.0 U 5.0 U 20 U5.0 U 5.0 U 5.0 U 5.0 U 5.0 U 20 U5.0 U 5.0 U 5.0 U 5.0 U 5.0 U 20 U5.0 U 5.0 U 5.0 U 5.0 U 5.0 U 20 U
Bold values are detected compounds.Shaded cells denote exceedances of MCL.* - These compound are part of the total trihalomethane (TTHM) group. The MCL for TTHM is 80 µg/L. TTHM includes bromodichloromethane, bromoform, chloroform and dibromochloromethane. U - NondetectNote: The MCL for xylenes reflects the value for total xylenes. UJ - NondetectNE - No MCL established J - Value is estimatedMCL - Maximum Contaminant Level µg/L - micrograms per liter
Trip Blank
Cleburn RI Report Page 7 of 7 HydroGeoLogic, Inc. 11/12/2010
FIGURE(S)
!
!
!
!
!
!
!
!
!
!
!
!
!
!
!
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!
!
!
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!A
!A
!A
!A
!A
!>
!>
!>
!H
!H
!H
!H
!A!H
!>
!H
!H
!H
!H
!H
!H
!H
!H
!H
!H
!H
!H
!H
!H
4th Street
Eddy Street
DPE-03
IW-09
IW-10IW-08
IW-06
IW-07
IW-05
IW-04IW-03
IW-02
IW-01
EW-3
EW-2
EW-1
SVE-8
SVE-1
SVE-2
SVE-3
SVE-4
MW-2B
MW-2A
MW-13A
MW-12A
DPE-04
DPE-02
DPE-01ERT-16
ERT-15
ERT-14
Figure 4.1Injection Well and
Monitoring Locations
³Filename: X:/EPA009/Cleburn/Annual ReportInjection_Well_Locations.mxdProject: EP9019.11.42.04Revised: 11/05/10 STSource:
0 20 40 60
Feet
U.S. EPA Region 7
HGL—Source Area ISCO Evaluation Report—Cleburn Street Well SiteGrand Island, Nebraska
Legend
!H Permanganate Injection Wells
!H Soil Vapor Extraction Well
!A Monitoring Well
!> Extraction Well
! ! ! Treated Water Discharge Line
Soil Vapor Extraction Line
Groundwater Extraction Line
! (N
! (N
! (N
! (N
! (N
! (N
! (N
!.
!.
!.
!.
!.
!.
!.
!.
!.
!.
!.
!.
!.
!.
4th Street
Eddy Street
N. Frontage Road (W
est)
Billiards / Bar(Active Business)
Former One HourMartinizing
RemediationBuilding
MW-2B(7.2)
MW-2A(46,000)
MW-13A(NS)
MW-12A(39)
DPE-04 (NS)
DPE-02 (NS)
DPE-01 (NS)
DPE-03 (NS)
IW-09(140,000)
IW-10(74,000)
IW-08(39,000)
IW-06(13,000)
IW-07(39,000)
IW-05(18,000)
IW-04(6,200)IW-03
(4,100)
IW-02(4,500)
IW-01(5.2)
ERT-16(11,000)
ERT-15(6.7)
ERT-14(370)
Figure 4.2Baseline PCE Concentrations
(December 2009)
³Filename: X:/EPA009/Cleburn/MapsBaseline_PCE_Concentrations.mxdProject: EP9019.11.42.04Revised: 11/05/10 STSource:
0 20 40 60
Feet
U.S. EPA Region 7
HGL—Source Area ISCO Evaluation Report—Cleburn Street Well SiteGrand Island, Nebraska
Legend
!. Permanganate Injection/Monitoring Wells
! (N Monitoring Well
PCE Concentration in Micrograms Per Liter (µg/L)
IW-10(140,000)
Not Sampled(NS)
! (N
! (N
! (N
! (N
! (N
! (N
! (N
!.
!.
!.
!.
!.
!.
!.
!.
!.
!.
!.
!.
!.
!.
4th Street
Eddy StreetN
. Frontage Road(West)
RemediationBuilding
Former One HourMartinizing
Billards / Bar(Active Business)
MW-2B(ND)
MW-2A(3,900 J)
MW-13A(ND)
MW-12A(2,400)
DPE-04(ND)
DPE-02(ND)
DPE-01(ND)
DPE-03(43)IW-09
(77)IW-10(120)IW-08
(ND)
IW-06(ND)
IW-07(ND)
IW-05(ND)
IW-04(ND)
IW-03(ND)
IW-02(ND)
IW-01(ND)
ERT-16
ERT-15(ND)
ERT-14(11)
Figure 4.3Post-Injection
Monitoring of PCE(January 2010)
³Filename: X:/EPA009/Cleburn/Annual ReportPost_Injection_Monitoring_PCE.mxdProject: EP9019.11.42.04Revised: 11/05/10 STSource:
0 20 40 60
Feet
U.S. EPA Region 7
HGL—Source Area ISCO Evaluation Report—Cleburn Street Well SiteGrand Island, Nebraska
Legend
!. Permanganate Injection/Monitoring Wells
! (N Monitoring Well
PCE Concentration in Micrograms Per Liter (µg/L)
IW-10(120)
Note:J = estimated concentration
! (N
! (N
! (N
! (N
! (N
! (N
! (N
!.
!.
!.
!.
!.
!.
!.
!.
!.
!.
!.
!.
!.
!.
4th Street
Eddy Street
N. Frontage Road (W
est)
Billards / Bar(Active Business)
RemediationBuilding
Former One HourMartinizing
MW-2B(ND)
MW-2A(1,600)
MW-13A(ND)
MW-12A(2,100)
DPE-04(ND)
DPE-02(20)
DPE-01(37)
DPE-03(ND)
IW-09(7,500)
IW-10(3,200)
IW-08(6,000)
IW-06(43)
IW-07(29)
IW-05(ND)
IW-04(ND)
IW-03(110)
IW-02(690)
IW-01(ND)
ERT-16(2,000)
ERT-15(ND)
ERT-14(ND)
Figure 4.4Post-Injection
Monitoring of PCE(July 2010)
³Filename: X:/EPA009/Cleburn/MapsPost_Injection_Monitoring_PCE_July_2010.mxdProject: EP9019.11.42.04Revised: 11/05/10 STSource:
0 20 40 60
Feet
U.S. EPA Region 7
HGL—Source Area ISCO Evaluation Report—Cleburn Street Well SiteGrand Island, Nebraska
Legend
!. Permanganate Injection/Monitoring Wells
! (N Monitoring Well
PCE Concentration in Micrograms Per Liter (µg/L)
IW-10(120)
20000
25000
30000
35000
40000
45000
50000
Concen
tration (µg/L)
Figure 4.5 ‐MW‐2A ‐ PCE Results
0
5000
10000
15000
20000
Dec‐09 Jan‐10 Feb‐10 Mar‐10 Apr‐10 May‐10 Jun‐10 Jul‐10
C
Date
1st Injectionof Permanganate
2nd Injectionof Permanganate
2000
2500
3000
3500
4000
4500
Concen
tration (µg/L)
Figure 4.6 ‐MW‐12A ‐ PCE Results
0
500
1000
1500
Dec‐09 Jan‐10 Feb‐10 Mar‐10 Apr‐10 May‐10 Jun‐10 Jul‐10
C
Date
1st Injectionof Permanganate
2nd Injectionof Permanganate
200
250
300
350
400
Concen
tration (µg/L)
Figure 4.7 ‐MW‐12A ‐ TCE Results
0
50
100
150
Dec‐09 Jan‐10 Feb‐10 Mar‐10 Apr‐10 May‐10 Jun‐10 Jul‐10
C
Date
1st Injectionof Permanganate
2nd Injectionof Permanganate
HGL—Source Area ISCO Evaluation, Cleburn Street Well Site—Grand Island, Nebraska
U.S. EPA Region 7 Source Area ISCO Evaluation 5-1 November 2010
5.0 SUMMARY AND RECOMMENDATIONS
5.1 SUMMARY
This source area TS involved application of 2 percent KMnO4 delivered through 14 permanent injection wells in the Cleburn Street source area. A limited groundwater profile study was conducted in December 2009 to determine the placement of ten of the injection wells. Four of the injection wells were existing wells that were screened across the silt zone. Two injections were performed: one in December 2009 and the second in March 2010. Five rounds of post-injection sampling were conducted with two sampling rounds after the first injection and three sampling rounds after the second injection. Based on the results of the groundwater profile study, the injection screen interval for the 10 permanent wells was set from 22 feet bgs to 32 feet bgs to target the highest levels of PCE in the saturated sands and upper portion of the silt layer. The four existing wells used for injection are screened from 31 to 36 feet bgs within the silt zone and located approximately 20 feet downgradient and east of the newly installed injection wells. For each injection event, 34,500 gallons of 2 percent KMnO4 were delivered through the14 permanent wells. A review of the data through July 2010 from the 20 wells sampled for post-injection performance monitoring indicates that the KMnO4 injections resulted in reduction of PCE in groundwater. Water quality parameters did not show any permanent affect on groundwater quality; noted effects were short-lived and dissipated as the KMnO4 was consumed. In addition, quarterly sampling of wells downgradient of the source (conducted under a separate subtask), showed no noticeable increases or decreases in PCE concentrations. It does appear that the KMnO4 injections have caused a release of CCl4 and chloroform from the injection interval. Before the TS and in the baseline groundwater sampling event, CCl4 and chloroform were not considered a contaminant of interest. It is not clear if these two chemicals originated at the site or if they migrated from an upgradient location and became bound in silt. Since 2006, CCl4 has been detected only one time in 16 quarterly sampling events of the entire monitoring well network. It was detected at 1.4 µg/L in MW-2A, below the MCL of 5 µg/L.
5.2 RECOMMENDATIONS
KMnO4 was effective in reducing PCE concentrations in the source area and could be used in a full-scale approach to reduce PCE concentrations. Groundwater profile data indicate that PCE contamination in groundwater both increased in concentration and migrated vertically from western portion of the study area to the eastern portion of the study area. It appears that the upgradient boundary has been delineated on the southwest portion of the injection zone. However, additional characterization (including subsurface soil and groundwater sampling) is needed to the north, west, and northwest of the source area injection zone to fully characterize the nature and extent of the subsurface contamination. This information is also required to inform the design of full-scale implementation of the potential ISCO remedy.
HGL—Source Area ISCO Evaluation, Cleburn Street Well Site—Grand Island, Nebraska
U.S. EPA Region 7 Source Area ISCO Evaluation 5-2 November 2010
Once full characterization is completed, injection in the source area should follow an outside-in/downgradient-upgradient injection pattern where injections are first conducted at the downgradient outer edges of the groundwater plume. This reduces the likelihood of contaminants being pushed outward horizontally, as occurred during the TS. Injection of KMnO4 should focus on the poorly graded sand portion of the aquifer and the upper fringe of the sandy silt/silty sand where much of the contamination appears to reside beneath the building. Injection directly into the low permeability sandy silt/silty sand layer is problematic, as it will be difficult to achieve even distribution of KMnO4. If additional characterization sampling indicates that the sandy silt/silty sand layer beneath the building is highly contaminated, the injection design may include an option to inject directly into this layer using low pressure over a longer injection period. This approach may be effective in reducing the likelihood of creating preferential pathways, and prevent upwelling of chemical into the building through injection and monitoring wells. Because CCl4 and chloroform were identified at levels above the MCL after injection activities, additional remediation alternatives may be needed to supplement (or replace) full-scale implementation of KMnO4, because KMnO4 is not effective in treating CCl4 and chloroform. The Remedial Investigation/Feasibility Study that is under way at the Cleburn Street Well Site will provide recommendations for the remediation of these contaminants. One alternative may be to utilize the existing groundwater extraction and treatment system in combination with the KMnO4 injections to remediate subsurface contamination. In the near term, additional monitoring is needed to evaluate the levels and migration of CCl4 and chloroform.
HGL—Source Area ISCO Evaluation, Cleburn Street Well Site—Grand Island, Nebraska
U.S. EPA Region 7 Source Area ISCO Evaluation 6-1 November 2010
6.0 REFERENCES
GeoTrans, Inc., 2001, Remediation System Evaluation, Cleburn Street Well Superfund Site, Grand Island, Nebraska.
HydroGeoLogic, Inc. (HGL), 2009. Sampling and Analysis Plan, Cleburn Street Well site Long
Term Response Action, Grand Island, Nebraska. January.
HGL, 2009a, Well Installation and Testing and Evaluation of the Silt Layer, Cleburn Street Well site, Grand Island, Nebraska. May.
HGL, 2009b, Sampling and Analysis Plan Addendum #1, Cleburn Street Well site, Grand Island, Nebraska. November 18.
HGL, 2009c, In Situ Chemical Oxidant Injection Evaluation, Cleburn Street Well site, Grand Island, Nebraska. November.
Nebraska Code of Regulations, Title 178-Chapter 12 Regulations Governing Water Well Construction, Pump Installation, and Water Well Abandonment Standards.
United States Department of Agriculture (USDA), Natural Resource Conservation Service.
(http://websoilsurvey.nrcs.usda.gov/app/WebSoilSurvey.aspx).
URS Greiner Woodward Clyde Federal Services (URSG), 1999. June 1998 Sampling Event for the LTM Program. Final Report. Cornhusker Army Ammunition Plant. Prepared for USACE. February.
Watkins-Johnson Environmental, Inc. (WJE), 1993. Site Characterization Document,
Cornhusker Army Ammunition Plant Remedial Investigation and Feasibility Study. Prepared for USACE. June.
Woodward-Clyde, 1997. 1996 Annual Long-Term Monitoring Final Report. Cornhusker Army
Ammunition Plant. Prepared for USACE. July. Woodward-Clyde, 1998. October 1997 Annual Sampling Event for the LTM Program. Final
Report. Cornhusker Army Ammunition Plant. Prepared for USACE. March.
APPENDIX A
GROUNDWATER PROFILE SCREENING DATA
APPENDIX B
SOIL BORING LOGS
APPENDIX C
WELL COMPLETION REPORTS
APPENDIX D
NEBRASKA WELL REGISTRATIONS
APPENDIX E
PHOTOGRAPHIC DOCUMENTATION
Cleburn Street Well SiteGrand Island, Nebraska
Photograph No.: 1Photographer: B. Mehnert Date: 12/2/2009 Contract: EPA AES
Direction: West Time: 1206 Project No. EP9019
Description: Coring concrete through floor in building for groundwater sampling and injection wells.
Ph t h B M h t D t 12/2/2009 C t t EPA AES
1
Photograph No.: 2Photographer: B. Mehnert Date: 12/2/2009 Contract: EPA AES
Direction: Down Time: 1221 Project No. EP9019
Description: Cored hole through three layers of poured concrete (approximately 6 inches thick in total).
Cleburn Street Well SiteGrand Island, Nebraska
Photograph No.: 3Photographer: B. Mehnert Date: 12/2/2009 Contract: EPA AES
Direction: Northwest Time: 1326 Project No. EP9019
Description: Geologist logging soil cores from SB-01.
Ph t h B M h t D t 12/4/2009 C t t EPA AES
2
Photograph No.: 4Photographer: B. Mehnert Date: 12/4/2009 Contract: EPA AES
Direction: East Time: 1137 Project No. EP9019
Description: Purging groundwater from temporary boreholes for groundwater profile sampling.
Cleburn Street Well SiteGrand Island, Nebraska
Photograph No.: 5Photographer: B. Mehnert Date: 12/8/2009 Contract: EPA AES
Direction: Northeast Time: 1215 Project No. EP9019
Description: Drilling injection wells with specialized drilling rig for low clearance.
Ph t h B M h t D t 12/16/2009 C t t EPA AES
3
Photograph No.: 6Photographer: B. Mehnert Date: 12/16/2009 Contract: EPA AES
Direction: Southeast Time: 1552 Project No. EP9019
Description: Manifold injection system pumping potassium permanganate to four injection wells simultaneously.
Cleburn Street Well SiteGrand Island, Nebraska
Photograph No.: 7Photographer: B. Mehnert Date: 12/16/200 Contract: EPA AES
Direction: Northeast Time: 1612 Project No. EP9019
Description: Adding potassium permanganate solid to water tank and mixing with pump.
Ph t h B M h t D t 12/16/2009 C t t EPA AES
4
Photograph No.: 8Photographer: B. Mehnert Date: 12/16/2009 Contract: EPA AES
Direction: North Time: 1712 Project No. EP9019
Description: Adding potassium permanganate powder into water tank to create 2% solution.
Cleburn Street Well SiteGrand Island, Nebraska
Photograph No.: 9Photographer: B. Mehnert Date: 12/18/2009 Contract: EPA AES
Direction: South Time: 1511 Project No. EP9019
Description: Potassium permanganate being pumped into injection well.
Ph t h B M h t D t 12/18/2009 C t t EPA AES
5
Photograph No.: 10Photographer: B. Mehnert Date: 12/18/2009 Contract: EPA AES
Direction: South Time: 1512 Project No. EP9019
Description: Digital flow meter calculates flow and total volume pumped into each injection well.
Cleburn Street Well SiteGrand Island, Nebraska
Photograph No.: 11Photographer: B. Mehnert Date: 12/21/2009 Contract: EPA AES
Direction: North Time: 1544 Project No. EP9019
D i ti P t i t l t kDescription: Potassium permanganate supply tanks.
6
Photograph No.: 12Photographer: B. Mehnert Date: 12/21/2009 Contract: EPA AES
Direction: South Time: 1545 Project No. EP9019
Description: Truck-mounted potassium permanganate tanks supplying the manifold system with 2% solution.
APPENDIX F
ANALYTICAL DATA RESULTS
DECEMBER 2009
Page 1 of 23
01/14/2010Date:
4717
DS07ES
Cleburn Street Well LTRA
DeAndre SingletarySUPR/IANE
Transmittal of Sample Analysis Results for ASR #:
Project ID:
Project Description:
Michael F. Davis, ChiefChemical Analysis and Response Branch, Environmental Services Division
To:
Enclosed are the analytical data for the above-referenced Analytical Services Request (ASR) andProject. The Regional Laboratory has reviewed and verified the results in accordance with proceduresdescribed in our Quality Manual (QM). In addition to all of the analytical results, this transmittalcontains pertinent information that may have influenced the reported results and documents anydeviations from the established requirements of the QM.
Please contact us within 14 days of receipt of this package if you determine there is a need for anychanges. Please complete the enclosed Customer Satisfaction Survey and Data Disposition/SampleRelease memo for this ASR as soon as possible. The process of disposing of the samples for this ASRwill be initiated 30 days from the date of this transmittal unless an alternate release date is specifiedon the Data Disposition/Sample Release memo.
If you have any questions or concerns relating to this data package, contact our customer service lineat 913-551-5295.
Enclosures
cc: Analytical Data File.
United States Environmental Protection AgencyRegion 7
901 N. 5th StreetKansas City, KS 66101
Subject:
From:
Page 2 of 23
4717ASR Number: 01/14/2010
DeAndre Singletary SUPR/IANE 913-551-7373
DS07ES
Cleburn Street Well LTRA
Grand Island Nebraska Superfund
07ES CLEBURN STREET WELL - 1 HR MARTINIZINGGW RESORATION
07ESSite ID: 02
Site Cleanup Support
Base-line ISCO Pilot Test - Source Area (3 Week)
Project Manager: Org: Phone:
Project ID:
Project Desc:
Location: State: Program:
Site Name: Site OU:
Purpose:
__ = Field SampleFB = Field BlankFD = Field Duplicate
QC Codes identify the type of sample for quality control purpose.
Degrees CelsiusNephelometric Turbidity UnitsStandard Units (pH)Milligrams per LiterMicrograms per LiterMicromhos per Centimeter
Specific units in which results arereported.
The identification of the analyte is acceptable; the reported value is anestimate.The analyte was not detected at or above the reporting limit.The analyte was not detected at or above the reporting limit. The reportinglimit is an estimate.
Specific codes used in conjunction with data values to provide additional information on the quality of reported results, or used to explain the absence of a specific value.
Summary of Project Information
Explanation of Codes, Units and Qualifiers used on this report
Sample QC Codes: Units:
J
UUJ
=
==
Data Qualifiers:
= Values have been reviewed and found acceptable for use. (Blank)
Deg CNTUSU
mg/Lug/L
umhos/cm
======
2009073QAPP Number:
302DD2CGPRA PRC:
Page 3 of 23
1
2
3
4
5
6
7
7
9
10
11
11
13
14
15
16
17
18
19
21
SampleNo
__
__
__
__
__
__
__
FD
__
__
__
FD
__
__
__
__
__
__
FB
FB
QCCode
Water
Water
Water
Water
Water
Water
Water
Water
Water
Water
Water
Water
Water
Water
Water
Water
Water
Water
Water
Water
Matrix
IW-1
IW-2
IW-3
IW-05
IW-04
IW-06
ERT-16
ERT-16/Field Duplicate of sample7IW-7
ERT-15
ERT-14
ERT-14/Field Duplicate of sample11MW-2B
IW-08
MW-2A
IW-10
IW-09
MW-12
Field Blank sample
VOA Trip Blank sample
Location DescriptionExternal
Sample No
12/10/2009
12/10/2009
12/10/2009
12/10/2009
12/10/2009
12/10/2009
12/10/2009
12/10/2009
12/10/2009
12/11/2009
12/11/2009
12/11/2009
12/11/2009
12/11/2009
12/11/2009
12/11/2009
12/11/2009
12/11/2009
12/11/2009
12/03/2009
Start Date
10:40
12:46
14:55
16:20
18:10
19:30
18:45
18:45
09:30
10:50
10:50
12:30
13:35
13:10
14:50
16:30
16:40
18:30
06:36
Start Time
12/11/2009
End Date
18:45
End Time
12/11/2009
12/11/2009
12/11/2009
12/15/2009
12/15/2009
12/15/2009
12/15/2009
12/15/2009
12/15/2009
12/15/2009
12/15/2009
12/15/2009
12/15/2009
12/15/2009
12/15/2009
12/15/2009
12/15/2009
12/15/2009
12/15/2009
12/15/2009
ReceiptDate
4717 01/14/2010
DS07ESProject ID: Cleburn Street Well LTRAProject Desc:
ASR Number: Sample Information Summary
-
-
-
-
-
-
-
-
-
-
-
-
-
-
-
-
-
-
-
-
Page 4 of 23
1
1
1
1
1
Alkalinity in Water by Titration
Anions in Water by Ion Chromatography
Conductivity by Field Measurement
Hardness in Water by Calculation
Metals in Water by ICP
Region 7 EPA Laboratory - Kansas City, Ks.
Region 7 ESAT Contract Lab (In-House)
(Field Measurement)
Region 7 ESAT Contract Lab (In-House)
Region 7 ESAT Contract Lab (In-House)
Lab:
Lab:
Lab:
Lab:
Lab:
EPA Region 7 RLAB Method 3132.1E
Region 7 RLAB Method 3135.12A
Measurement of field parameter
EPA Region 7 RLAB Method 3122.3C
EPA Region 7 RLAB Method 3122.3C
Method:
Method:
Method:
Method:
Method:
(N/A)
Comments:
Comments:
Comments:
Comments:
1-__ 2-__ 3-__ 4-__ 5-__ 6-__ 7-__7-FD 9-__ 10-__ 11-__ 11-FD 13-__ 14-__15-__ 16-__ 17-__ 18-__ 19-FB
1-__ 2-__ 3-__ 4-__ 5-__ 6-__ 7-__7-FD 9-__ 10-__ 11-__ 11-FD 13-__ 14-__15-__ 16-__ 17-__ 18-__ 19-FB
4-__ 5-__ 6-__ 7-__ 7-FD 9-__ 10-__11-__ 11-FD 13-__ 14-__ 15-__ 16-__ 17-__18-__
1-__ 2-__ 3-__ 4-__ 5-__ 6-__ 7-__7-FD 9-__ 10-__ 11-__ 11-FD 13-__ 14-__15-__ 16-__ 17-__ 18-__ 19-FB
Samples:
Samples:
Samples:
Samples:
4717ASR Number: 01/14/2010
DS07ESProject ID: Cleburn Street Well LTRAProject Desc
RLAB Approved Analysis Comments
Analysis Comments About Results For This Analysis
Page 5 of 23
1
1
1
1
pH of Water by Field Measurement
TDS or Total Dissolved Solids
Temperature of Water by Field Measurement
Total Dissolved Oxygen in Water by Field Measurement
(Field Measurement)
Region 7 EPA Laboratory - Kansas City, Ks.
(Field Measurement)
(Field Measurement)
Lab:
Lab:
Lab:
Lab:
Measurement of field parameter
EPA Region 7 RLAB Method 3142.2B
Measurement of field parameter
Measurement of field parameter
Method:
Method:
Method:
Method:
(N/A)
(N/A)
Comments:
Comments:
Comments:
Comments:
1-__ 2-__ 3-__ 4-__ 5-__ 6-__ 7-__7-FD 9-__ 10-__ 11-__ 11-FD 13-__ 14-__15-__ 16-__ 17-__ 18-__ 19-FB
4-__ 5-__ 6-__ 7-__ 7-FD 9-__ 10-__11-__ 11-FD 13-__ 14-__ 15-__ 16-__ 17-__18-__
1-__ 2-__ 3-__ 4-__ 5-__ 6-__ 7-__7-FD 9-__ 10-__ 11-__ 11-FD 13-__ 14-__15-__ 16-__ 17-__ 18-__ 19-FB
4-__ 5-__ 6-__ 7-__ 7-FD 9-__ 10-__11-__ 11-FD 13-__ 14-__ 15-__ 16-__ 17-__18-__
4-__ 5-__ 6-__ 7-__ 7-FD 9-__ 10-__11-__ 11-FD 13-__ 14-__ 15-__ 16-__ 17-__18-__
Samples:
Samples:
Samples:
Samples:
Samples:
4717ASR Number: 01/14/2010
DS07ESProject ID: Cleburn Street Well LTRAProject Desc
RLAB Approved Analysis Comments
Analysis Comments About Results For This Analysis
Page 6 of 23
1
1
1
Total Organic Carbon in Water
Turbidity of Water by Field Measurement
VOCs in Water by GC/MS
REAP Contract Lab (Out-Source)
(Field Measurement)
Region 7 ESAT Contract Lab (In-House)
Lab:
Lab:
Lab:
Similar to EPA SW846 Method 9060 or StandardMethods (20th Edtion) 5310 B, C,or D (see comments)
Measurement of field parameter
EPA Region 7 RLAB Method 3230.1F
Method:
Method:
Method:
(N/A)
(N/A)
091216: Naphthalene (34.3%) was J-coded in sample 18. Although the analytes inquestion have been positively identified in the samples, the quantitation is an estimate (J-coded) due to the continuing calibration check not meeting accuracy specifications. Theactual concentration for these analytes may be higher than the reported value. Dichlorodifluoromethane (23.8%), 4-Methly-2-Pentanone (67.5%), 2-Hexanone (96.5%),Dibromochloromethane (22.9%), Bromoform (32.3%), 1,2-Dibromo-3-Chloropropane(39.6%), 1,2,4-Trichlorobenzene (32.0%), Naphthalene (34.3%) and 1,2,3-Trichlorobenzene (33.5%) were UJ-coded in samples 1, 2, 3, 4, 5, 6, 7, 7-FD, 9, 11, 11-FD,13, 14, 15 , 16, 17, 19-FB and 21-FB. Dichlorodifluoromethane, 4-Methly-2-Pentanone, 2-Hexanone, Dibromochloromethane, Bromoform, 1,2-Dibromo-3-Chloropropane, 1,2,4-Trichlorobenzene, and 1,2,3-Trichlorobenzene were UJ-coded in sample 18. These analyteswere not found in the samples at or above the reporting limit, however, the reporting limit
Comments:
Comments:
Comments:
Comments:
1-__ 2-__ 3-__ 4-__ 5-__ 6-__ 7-__7-FD 9-__ 10-__ 11-__ 11-FD 13-__ 14-__15-__ 16-__ 17-__ 18-__ 19-FB
4-__ 5-__ 6-__ 7-__ 7-FD 9-__ 10-__11-__ 11-FD 13-__ 14-__ 15-__ 16-__ 17-__18-__
1-__ 2-__ 3-__ 4-__ 5-__ 6-__ 7-__7-FD 9-__ 10-__ 11-__ 11-FD 13-__ 14-__15-__ 16-__ 17-__ 18-__ 19-FB 21-FB
Samples:
Samples:
Samples:
4717ASR Number: 01/14/2010
DS07ESProject ID: Cleburn Street Well LTRAProject Desc
RLAB Approved Analysis Comments
Analysis Comments About Results For This Analysis
Page 7 of 23
is an estimate (UJ-coded) due to low recovery of these analytes in the laboratory controlsample. The actual reporting limit for these analytes may be higher than the reportedvalue. Dichlorodifluoromethane (21.2%), 4-Methyl-2-Pentanone (57.1%), 2-Hexanone (99.3%),Dibromochloromethane (20.8%), Bromoform (27.8%), 1,2-Dibromo-3-Chloropropane(41.5%), 1,2,4-Trichlorobenzene (40.8%), Naphthalene (49.6%) and 1,2,3-Trichlorobenzene (53.4%) were UJ-coded in sample 10. These analytes were not found inthe samples at or above the reporting limit, however, the reporting limit is an estimate (UJ-coded) due to low recovery of these analytes in the laboratory control sample. The actualreporting limit for these analytes may be higher than the reported value. 990-LCS: 1,2-Dichloroethane (81%, 84-117%), 4-Methyl-2-Pentanone (32%, 76-123%),2-Hexanone (4%, 64-127%), Dibromochloromethane (77%, 86-119%), 1,2-Dibromethane(86%, 87-114%), Bromoform (68%, 83-119%), 1,2-Dibromo-3-Chloropropane (61%, 71-125%), 1,2,4-Trichlorobenzene (68%, 82-116%), Naphthalene (66%, 80-123%) and1,2,3-Trichlorobenzene (67%, 82-116%) were UJ-coded in samples 1, 2, 3, 4, 5, 6, 7, 7-FD, 9, 11, 11-FD, 13, 14, 15, 16, 17, 19-FB and 21-FB. 1,2-Dichloroethane, 4-Methyl-2-Pentanone, 2-Hexanone, Dibromochloromethane, 1,2-Dibromethane, Bromoform, 1,2-Dibromo-3-Chloropropane, 1,2,4-Trichlorobenzene, and 1,2,3-Trichlorobenzene were UJ-coded in sample 18. These analytes were not found in the samples at or above thereporting limit, however, the reporting limit is an estimate (UJ-coded) due to low recoveryof these analytes in the laboratory control sample. The actual reporting limit for theseanalytes may be higher than the reported value. Naphthalene was J-coded in sample 18. Although the analytes in question have beenpositively identified in the samples, the quantitation is an estimate (J-coded) due to lowrecovery of these analytes in the laboratory control sample. The actual concentration forthese analytes may be higher than the reported value. 991-LCS: 1,2-Dichloroethane (80%, 84-117%), 4-Methyl-2-Pentanone (43%, 76-123%),2-Hexanone (1%, 64-127%), Dibromochloromethane (79%, 86-119%), Bromoform (72%,83-119%), 1,2-Dibromo-3-Chloropropane (58%, 71-125%), 1,2,4-Trichlorobenzene (59%,82-116%), Naphthalene (50%, 80-123%) and 1,2,3-Trichlorobenzene (47%, 82-116%)were UJ-coded in sample 10. These analytes were not found in the sample at or above thereporting limit, however, the reporting limit is an estimate (UJ-coded) due to low recoveryof these analytes in the laboratory control sample. The actual reporting limit for theseanalytes may be higher than the reported value. Bromoform (64% & 62%, 77-122%), 1,2-Dibromo-3-Chloropropane (58% & 54%, 62-135%), Dibromochloromethane (75% & 72%, 86-118%), 1,2-Dibromoethane (88% &83%, 90-114%), 1,2-Dichlorobenzene (87% & 82%, 88-116%), 1,3-Dichlorobenzene(87%, 91-115%), 1,4-Dichlorobenzene (88%, 89-116%), 1,2-Dichloroethane (82% &78%, 83-121%), trans-1,3-Dichloropropene (81%, 84-117%), 2-Hexanone (1% & 1%, 55-126%), 4-Methyl-2-Pentanone (42% & 40%, 79-125%), Naphthalene (58% & 56%, 72-131%), 1,2,3-Trichlorobenzene (57% & 53%, 77-121%) and 1,24-Trichlorobenzene (64%& 60%, 74-121%) were UJ-coded in sample 3. These analytes were not found in thesample at or above the reporting limit, however, the reporting limit is an estimate (UJ-coded) due to low recovery of these analytes in the laboratory matrix spike. The actual
4717ASR Number: 01/14/2010
DS07ESProject ID: Cleburn Street Well LTRAProject Desc
RLAB Approved Analysis Comments
Analysis Comments About Results For This Analysis
Page 8 of 23
reporting limit for these analytes may be higher than the reported value. Tetrachloroethene: The Concentration Spiked is less than 50 percent of the Final Result forthe original sample. It may be inappropriate to qualify data based on this spike recovery. 3-MS/MSD: Bromodichloromethane (6.5 RPD, 6.1 PCL) and Methyl tert-butyl ether (6.6RPD, 5.4 PCL) were UJ-coded in sample 3. These analytes were not found in the sample ator above the reporting limit, however, the reporting limit is an estimate (UJ-coded) due topoor precision obtained for these analytes in the laboratory matrix spike and matrix spikeduplicate. The actual reporting limit for these analytes may be higher than the reportedvalue.
4717ASR Number: 01/14/2010
DS07ESProject ID: Cleburn Street Well LTRAProject Desc
RLAB Approved Analysis Comments
Analysis Comments About Results For This Analysis
Page 9 of 23
1
1
1
1
1
1
1
1
1
1
1
Alkalinity in Water by Titration
Anions in Water by Ion Chromatography
Conductivity by Field Measurement
Hardness in Water by Calculation
Metals in Water by ICP
pH of Water by Field Measurement
TDS or Total Dissolved Solids
Temperature of Water by Field Measurement
Total Dissolved Oxygen in Water by Field Measurement
Total Organic Carbon in Water
Turbidity of Water by Field Measurement
Analysis/ Analyte
Alkalinity, total
Sulfate
Conductivity
Hardness as CaCO3
Aluminum
Antimony
Arsenic
Barium
Beryllium
Cadmium
Calcium
Chromium
Cobalt
Copper
Iron
Lead
Magnesium
Manganese
Molybdenum
Nickel
Potassium
Selenium
Silver
Sodium
Thallium
Titanium
Vanadium
Zinc
pH
Solids, total dissolved
Temperature
Dissolved Oxygen
Total Organic Carbon
Turbidity
mg/L
mg/L
umhos/cm
mg/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
mg/L
ug/L
ug/L
ug/L
ug/L
ug/L
mg/L
ug/L
ug/L
ug/L
mg/L
ug/L
ug/L
mg/L
ug/L
ug/L
ug/L
ug/L
SU
mg/L
Deg C
mg/L
mg/L
NTU
Units 1-__ 2-__ 3-__ 4-__
117 142 162 130
194 181 213 169
1480
346 304 256 361
50 U 50 U 50 U 50 U
50 U 50 U 50 U 50 U
25 U 25 U 25 U 25 U
106 92 69 90
3 U 3 U 3 U 3 U
3 U 3 U 3 U 3 U
97.9 86.2 73.3 103
15 U 15 U 15 U 15 U
10 U 10 U 10 U 10 U
5 U 5 U 5 U 5 U
50 U 50 U 50 U 51
50 U 50 U 50 U 50 U
24.6 21.6 17.6 25.2
21 12 35 20
15 U 15 U 15 U 15 U
20 U 20 U 20 U 20 U
17.1 13.1 11.3 13.5
50 U 50 U 50 U 50 U
25 U 25 U 25 U 25 U
102 118 112 164
50 U 50 U 50 U 50 U
20 U 20 U 20 U 20 U
10 U 10 U 10 U 10 U
25 U 25 U 25 U 25 U
6.98
738 742 692 856
13.24
2.54
1.4 1.2 1.4 2.1
0.2
4717ASR Number: 01/14/2010
DS07ESProject ID: Cleburn Street Well LTRAProject Desc:
RLAB Approved Sample Analysis Results
Page 10 of 23
1 VOCs in Water by GC/MS
Analysis/ Analyte
Acetone
Benzene
Bromodichloromethane
Bromoform
Bromomethane
2-Butanone
Carbon Disulfide
Carbon Tetrachloride
Chlorobenzene
Chloroethane
Chloroform
Chloromethane
Cyclohexane
1,2-Dibromo-3-Chloropropane
Dibromochloromethane
1,2-Dibromoethane
1,2-Dichlorobenzene
1,3-Dichlorobenzene
1,4-Dichlorobenzene
Dichlorodifluoromethane
1,1-Dichloroethane
1,2-Dichloroethane
1,1-Dichloroethene
cis-1,2-Dichloroethene
trans-1,2-Dichloroethene
1,2-Dichloropropane
cis-1,3-Dichloropropene
trans-1,3-Dichloropropene
Ethyl Benzene
2-Hexanone
Isopropylbenzene
Methyl Acetate
Methyl tert-butyl ether
Methylcyclohexane
Methylene Chloride
4-Methyl-2-Pentanone
Naphthalene
Styrene
1,1,2,2-Tetrachloroethane
Tetrachloroethene
Toluene
1,2,3-Trichlorobenzene
1,2,4-Trichlorobenzene
1,1,1-Trichloroethane
1,1,2-Trichloroethane
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
Units 1-__ 2-__ 3-__ 4-__
5.0 U 5.0 U 5.0 U 5.0 U
5.0 U 5.0 U 5.0 U 5.0 U
5.0 U 5.0 U 5.0 UJ 5.0 U
5.0 UJ 5.0 UJ 5.0 UJ 5.0 UJ
5.0 U 5.0 U 5.0 U 5.0 U
5.0 U 5.0 U 5.0 U 5.0 U
5.0 U 5.0 U 5.0 U 5.0 U
5.0 U 5.0 U 5.0 U 5.0 U
5.0 U 5.0 U 5.0 U 5.0 U
5.0 U 5.0 U 5.0 U 5.0 U
5.0 U 5.0 U 5.0 U 5.0 U
5.0 U 5.0 U 5.0 U 5.0 U
5.0 U 5.0 U 5.0 U 5.0 U
5.0 UJ 5.0 UJ 5.0 UJ 5.0 UJ
5.0 UJ 5.0 UJ 5.0 UJ 5.0 UJ
5.0 UJ 5.0 UJ 5.0 UJ 5.0 UJ
5.0 U 5.0 U 5.0 UJ 5.0 U
5.0 U 5.0 U 5.0 UJ 5.0 U
5.0 U 5.0 U 5.0 UJ 5.0 U
5.0 UJ 5.0 UJ 5.0 UJ 5.0 UJ
5.0 U 5.0 U 5.0 U 5.0 U
5.0 UJ 5.0 UJ 5.0 UJ 5.0 UJ
5.0 U 5.0 U 5.0 U 5.0 U
5.0 U 5.0 U 5.0 U 5.0 U
5.0 U 5.0 U 5.0 U 5.0 U
5.0 U 5.0 U 5.0 U 5.0 U
5.0 U 5.0 U 5.0 U 5.0 U
5.0 U 5.0 U 5.0 UJ 5.0 U
5.0 U 5.0 U 5.0 U 5.0 U
5.0 UJ 5.0 UJ 5.0 UJ 5.0 UJ
5.0 U 5.0 U 5.0 U 5.0 U
5.0 U 5.0 U 5.0 U 5.0 U
10 U 10 U 10 UJ 10 U
5.0 U 5.0 U 5.0 U 5.0 U
5.0 U 5.0 U 5.0 U 5.0 U
5.0 UJ 5.0 UJ 5.0 UJ 5.0 UJ
10 UJ 10 UJ 10 UJ 10 UJ
5.0 U 5.0 U 5.0 U 5.0 U
5.0 U 5.0 U 5.0 U 5.0 U
5.2 4500 4100 18000
5.0 U 5.0 U 5.0 U 5.0 U
5.0 UJ 5.0 UJ 5.0 UJ 5.0 UJ
5.0 UJ 5.0 UJ 5.0 UJ 5.0 UJ
5.0 U 5.0 U 5.0 U 5.0 U
5.0 U 5.0 U 5.0 U 5.0 U
4717ASR Number: 01/14/2010
DS07ESProject ID: Cleburn Street Well LTRAProject Desc:
RLAB Approved Sample Analysis Results
Page 11 of 23
Analysis/ Analyte
Trichloroethene
Trichlorofluoromethane
1,1,2-Trichlorotrifluoroethane
Vinyl Chloride
m and/or p-Xylene
o-Xylene
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
Units 1-__ 2-__ 3-__ 4-__
5.0 U 5.0 U 5.0 U 5.0 U
5.0 U 5.0 U 5.0 U 5.0 U
5.0 U 5.0 U 5.0 U 5.0 U
5.0 U 5.0 U 5.0 U 5.0 U
10 U 10 U 10 U 10 U
5.0 U 5.0 U 5.0 U 5.0 U
4717ASR Number: 01/14/2010
DS07ESProject ID: Cleburn Street Well LTRAProject Desc:
RLAB Approved Sample Analysis Results
Page 12 of 23
1
1
1
1
1
1
1
1
1
1
1
Alkalinity in Water by Titration
Anions in Water by Ion Chromatography
Conductivity by Field Measurement
Hardness in Water by Calculation
Metals in Water by ICP
pH of Water by Field Measurement
TDS or Total Dissolved Solids
Temperature of Water by Field Measurement
Total Dissolved Oxygen in Water by Field Measurement
Total Organic Carbon in Water
Turbidity of Water by Field Measurement
Analysis/ Analyte
Alkalinity, total
Sulfate
Conductivity
Hardness as CaCO3
Aluminum
Antimony
Arsenic
Barium
Beryllium
Cadmium
Calcium
Chromium
Cobalt
Copper
Iron
Lead
Magnesium
Manganese
Molybdenum
Nickel
Potassium
Selenium
Silver
Sodium
Thallium
Titanium
Vanadium
Zinc
pH
Solids, total dissolved
Temperature
Dissolved Oxygen
Total Organic Carbon
Turbidity
mg/L
mg/L
umhos/cm
mg/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
mg/L
ug/L
ug/L
ug/L
ug/L
ug/L
mg/L
ug/L
ug/L
ug/L
mg/L
ug/L
ug/L
mg/L
ug/L
ug/L
ug/L
ug/L
SU
mg/L
Deg C
mg/L
mg/L
NTU
Units 5-__ 6-__ 7-__ 7-FD
156 142 109 108
221 209 109 138
1140 1090 1710 1710
275 307 359 363
50 U 117 50 U 50 U
50 U 50 U 50 U 50 U
25 U 25 U 25 U 25 U
83 70 117 120
3 U 3 U 3 U 3 U
3 U 3 U 3 U 3 U
78.4 87.8 101 102
15 U 15 U 15 U 15 U
10 U 10 U 10 U 10 U
5 U 5 U 5 U 5 U
50 U 116 50 U 50 U
50 U 50 U 50 U 50 U
19.3 21.3 26.0 26.2
18 30 7 8
15 U 15 U 15 U 15 U
20 U 20 U 20 U 30.8
13.4 11.8 11.9 12.0
50 U 50 U 50 U 50 U
25 U 25 U 25 U 25 U
123 97.7 166 164
50 U 50 U 50 U 50 U
20 U 20 U 20 U 20 U
10 U 10 U 10 U 10 U
25 U 25 U 25 U 25 U
6.94 6.90 7.30 7.30
712 708 982 976
12.08 12.56 12.37 12.37
2.67 1.77 6.57 6.57
1.5 1.5 1.5 1.1
0 1.5 0.0 0.0
4717ASR Number: 01/14/2010
DS07ESProject ID: Cleburn Street Well LTRAProject Desc:
RLAB Approved Sample Analysis Results
Page 13 of 23
1 VOCs in Water by GC/MS
Analysis/ Analyte
Acetone
Benzene
Bromodichloromethane
Bromoform
Bromomethane
2-Butanone
Carbon Disulfide
Carbon Tetrachloride
Chlorobenzene
Chloroethane
Chloroform
Chloromethane
Cyclohexane
1,2-Dibromo-3-Chloropropane
Dibromochloromethane
1,2-Dibromoethane
1,2-Dichlorobenzene
1,3-Dichlorobenzene
1,4-Dichlorobenzene
Dichlorodifluoromethane
1,1-Dichloroethane
1,2-Dichloroethane
1,1-Dichloroethene
cis-1,2-Dichloroethene
trans-1,2-Dichloroethene
1,2-Dichloropropane
cis-1,3-Dichloropropene
trans-1,3-Dichloropropene
Ethyl Benzene
2-Hexanone
Isopropylbenzene
Methyl Acetate
Methyl tert-butyl ether
Methylcyclohexane
Methylene Chloride
4-Methyl-2-Pentanone
Naphthalene
Styrene
1,1,2,2-Tetrachloroethane
Tetrachloroethene
Toluene
1,2,3-Trichlorobenzene
1,2,4-Trichlorobenzene
1,1,1-Trichloroethane
1,1,2-Trichloroethane
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
Units 5-__ 6-__ 7-__ 7-FD
5.0 U 5.0 U 5.0 U 5.0 U
5.0 U 5.0 U 5.0 U 5.0 U
5.0 U 5.0 U 5.0 U 5.0 U
5.0 UJ 5.0 UJ 5.0 UJ 5.0 UJ
5.0 U 5.0 U 5.0 U 5.0 U
5.0 U 5.0 U 5.0 U 5.0 U
5.0 U 5.0 U 5.0 U 5.0 U
5.0 U 5.0 U 5.0 U 5.0 U
5.0 U 5.0 U 5.0 U 5.0 U
5.0 U 5.0 U 5.0 U 5.0 U
5.0 U 5.0 U 5.0 U 5.0 U
5.0 U 5.0 U 5.0 U 5.0 U
5.0 U 5.0 U 5.0 U 5.0 U
5.0 UJ 5.0 UJ 5.0 UJ 5.0 UJ
5.0 UJ 5.0 UJ 5.0 UJ 5.0 UJ
5.0 UJ 5.0 UJ 5.0 UJ 5.0 UJ
5.0 U 5.0 U 5.0 U 5.0 U
5.0 U 5.0 U 5.0 U 5.0 U
5.0 U 5.0 U 5.0 U 5.0 U
5.0 UJ 5.0 UJ 5.0 UJ 5.0 UJ
5.0 U 5.0 U 5.0 U 5.0 U
5.0 UJ 5.0 UJ 5.0 UJ 5.0 UJ
5.0 U 5.0 U 5.0 U 5.0 U
5.0 U 5.0 U 5.0 U 5.0 U
5.0 U 5.0 U 5.0 U 5.0 U
5.0 U 5.0 U 5.0 U 5.0 U
5.0 U 5.0 U 5.0 U 5.0 U
5.0 U 5.0 U 5.0 U 5.0 U
5.0 U 5.0 U 5.0 U 5.0 U
5.0 UJ 5.0 UJ 5.0 UJ 5.0 UJ
5.0 U 5.0 U 5.0 U 5.0 U
5.0 U 5.0 U 5.0 U 5.0 U
10 U 10 U 10 U 10 U
5.0 U 5.0 U 5.0 U 5.0 U
5.0 U 5.0 U 5.0 U 5.0 U
5.0 UJ 5.0 UJ 5.0 UJ 5.0 UJ
10 UJ 10 UJ 10 UJ 10 UJ
5.0 U 5.0 U 5.0 U 5.0 U
5.0 U 5.0 U 5.0 U 5.0 U
6200 13000 11000 11000
5.0 U 5.0 U 5.0 U 5.0 U
5.0 UJ 5.0 UJ 5.0 UJ 5.0 UJ
5.0 UJ 5.0 UJ 5.0 UJ 5.0 UJ
5.0 U 5.0 U 5.0 U 5.0 U
5.0 U 5.0 U 5.0 U 5.0 U
4717ASR Number: 01/14/2010
DS07ESProject ID: Cleburn Street Well LTRAProject Desc:
RLAB Approved Sample Analysis Results
Page 14 of 23
Analysis/ Analyte
Trichloroethene
Trichlorofluoromethane
1,1,2-Trichlorotrifluoroethane
Vinyl Chloride
m and/or p-Xylene
o-Xylene
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
Units 5-__ 6-__ 7-__ 7-FD
5.0 U 5.0 U 5.0 U 5.0 U
5.0 U 5.0 U 5.0 U 5.0 U
5.0 U 5.0 U 5.0 U 5.0 U
5.0 U 5.0 U 5.0 U 5.0 U
10 U 10 U 10 U 10 U
5.0 U 5.0 U 5.0 U 5.0 U
4717ASR Number: 01/14/2010
DS07ESProject ID: Cleburn Street Well LTRAProject Desc:
RLAB Approved Sample Analysis Results
Page 15 of 23
1
1
1
1
1
1
1
1
1
1
1
Alkalinity in Water by Titration
Anions in Water by Ion Chromatography
Conductivity by Field Measurement
Hardness in Water by Calculation
Metals in Water by ICP
pH of Water by Field Measurement
TDS or Total Dissolved Solids
Temperature of Water by Field Measurement
Total Dissolved Oxygen in Water by Field Measurement
Total Organic Carbon in Water
Turbidity of Water by Field Measurement
Analysis/ Analyte
Alkalinity, total
Sulfate
Conductivity
Hardness as CaCO3
Aluminum
Antimony
Arsenic
Barium
Beryllium
Cadmium
Calcium
Chromium
Cobalt
Copper
Iron
Lead
Magnesium
Manganese
Molybdenum
Nickel
Potassium
Selenium
Silver
Sodium
Thallium
Titanium
Vanadium
Zinc
pH
Solids, total dissolved
Temperature
Dissolved Oxygen
Total Organic Carbon
Turbidity
mg/L
mg/L
umhos/cm
mg/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
mg/L
ug/L
ug/L
ug/L
ug/L
ug/L
mg/L
ug/L
ug/L
ug/L
mg/L
ug/L
ug/L
mg/L
ug/L
ug/L
ug/L
ug/L
SU
mg/L
Deg C
mg/L
mg/L
NTU
Units 9-__ 10-__ 11-__ 11-FD
154 106 88.9 89.0
259 161 139 148
1520 1360 1450 1450
395 391 397 420
50 U 50 U 60 65
50 U 50 U 50 U 50 U
25 U 25 U 25 U 25 U
94 102 167 175
3 U 3 U 3 U 3 U
3 U 3 U 3 U 3 U
113 110 112 119
15 U 16 15 U 15 U
10 U 10 U 10 U 10 U
5 U 5 U 5 U 5 U
50 U 58 109 123
50 U 50 U 50 U 50 U
27.4 28.3 28.5 29.8
54 5 U 14 15
15 U 15 U 15 U 15 U
23 20 U 85 66
14.4 19.7 22.5 23.6
50 U 50 U 50 U 50 U
25 U 25 U 25 U 25 U
154 92.5 110 114
50 U 50 U 50 U 50 U
20 U 20 U 20 U 20 U
10 U 10 U 10 U 10 U
25 U 25 U 25 U 25 U
7.19 6.77 6.66 6.66
900 844 928 926
10.61 14.48 14.49 14.49
4.66 12.64 6.20 6.20
2.5 1.6 1.2 1.4
1.4 0 0.0 0.0
4717ASR Number: 01/14/2010
DS07ESProject ID: Cleburn Street Well LTRAProject Desc:
RLAB Approved Sample Analysis Results
Page 16 of 23
1 VOCs in Water by GC/MS
Analysis/ Analyte
Acetone
Benzene
Bromodichloromethane
Bromoform
Bromomethane
2-Butanone
Carbon Disulfide
Carbon Tetrachloride
Chlorobenzene
Chloroethane
Chloroform
Chloromethane
Cyclohexane
1,2-Dibromo-3-Chloropropane
Dibromochloromethane
1,2-Dibromoethane
1,2-Dichlorobenzene
1,3-Dichlorobenzene
1,4-Dichlorobenzene
Dichlorodifluoromethane
1,1-Dichloroethane
1,2-Dichloroethane
1,1-Dichloroethene
cis-1,2-Dichloroethene
trans-1,2-Dichloroethene
1,2-Dichloropropane
cis-1,3-Dichloropropene
trans-1,3-Dichloropropene
Ethyl Benzene
2-Hexanone
Isopropylbenzene
Methyl Acetate
Methyl tert-butyl ether
Methylcyclohexane
Methylene Chloride
4-Methyl-2-Pentanone
Naphthalene
Styrene
1,1,2,2-Tetrachloroethane
Tetrachloroethene
Toluene
1,2,3-Trichlorobenzene
1,2,4-Trichlorobenzene
1,1,1-Trichloroethane
1,1,2-Trichloroethane
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
Units 9-__ 10-__ 11-__ 11-FD
5.0 U 5.0 U 5.0 U 5.0 U
5.0 U 5.0 U 5.0 U 5.0 U
5.0 U 5.0 U 5.0 U 5.0 U
5.0 UJ 5.0 UJ 5.0 UJ 5.0 UJ
5.0 U 5.0 U 5.0 U 5.0 U
5.0 U 5.0 U 5.0 U 5.0 U
5.0 U 5.0 U 5.0 U 5.0 U
5.0 U 5.0 U 5.0 U 5.0 U
5.0 U 5.0 U 5.0 U 5.0 U
5.0 U 5.0 U 5.0 U 5.0 U
5.0 U 5.0 U 5.0 U 5.0 U
5.0 U 5.0 U 5.0 U 5.0 U
5.0 U 5.0 U 5.0 U 5.0 U
5.0 UJ 5.0 UJ 5.0 UJ 5.0 UJ
5.0 UJ 5.0 UJ 5.0 UJ 5.0 UJ
5.0 UJ 5.0 U 5.0 UJ 5.0 UJ
5.0 U 5.0 U 5.0 U 5.0 U
5.0 U 5.0 U 5.0 U 5.0 U
5.0 U 5.0 U 5.0 U 5.0 U
5.0 UJ 5.0 UJ 5.0 UJ 5.0 UJ
5.0 U 5.0 U 5.0 U 5.0 U
5.0 UJ 5.0 UJ 5.0 UJ 5.0 UJ
5.0 U 5.0 U 5.0 U 5.0 U
5.0 U 5.0 U 5.0 U 5.0 U
5.0 U 5.0 U 5.0 U 5.0 U
5.0 U 5.0 U 5.0 U 5.0 U
5.0 U 5.0 U 5.0 U 5.0 U
5.0 U 5.0 U 5.0 U 5.0 U
5.0 U 5.0 U 5.0 U 5.0 U
5.0 UJ 5.0 UJ 5.0 UJ 5.0 UJ
5.0 U 5.0 U 5.0 U 5.0 U
5.0 U 5.0 U 5.0 U 5.0 U
10 U 10 U 10 U 10 U
5.0 U 5.0 U 5.0 U 5.0 U
5.0 U 5.0 U 5.0 U 5.0 U
5.0 UJ 5.0 UJ 5.0 UJ 5.0 UJ
10 UJ 10 UJ 10 UJ 10 UJ
5.0 U 5.0 U 5.0 U 5.0 U
5.0 U 5.0 U 5.0 U 5.0 U
39000 6.7 350 370
5.0 U 5.0 U 5.0 U 5.0 U
5.0 UJ 5.0 UJ 5.0 UJ 5.0 UJ
5.0 UJ 5.0 UJ 5.0 UJ 5.0 UJ
10 5.0 U 5.0 U 5.0 U
5.0 U 5.0 U 5.0 U 5.0 U
4717ASR Number: 01/14/2010
DS07ESProject ID: Cleburn Street Well LTRAProject Desc:
RLAB Approved Sample Analysis Results
Page 17 of 23
Analysis/ Analyte
Trichloroethene
Trichlorofluoromethane
1,1,2-Trichlorotrifluoroethane
Vinyl Chloride
m and/or p-Xylene
o-Xylene
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
Units 9-__ 10-__ 11-__ 11-FD
13 5.0 U 5.0 U 5.0 U
5.0 U 5.0 U 5.0 U 5.0 U
5.0 U 5.0 U 5.0 U 5.0 U
5.0 U 5.0 U 5.0 U 5.0 U
10 U 10 U 10 U 10 U
5.0 U 5.0 U 5.0 U 5.0 U
4717ASR Number: 01/14/2010
DS07ESProject ID: Cleburn Street Well LTRAProject Desc:
RLAB Approved Sample Analysis Results
Page 18 of 23
1
1
1
1
1
1
1
1
1
1
1
Alkalinity in Water by Titration
Anions in Water by Ion Chromatography
Conductivity by Field Measurement
Hardness in Water by Calculation
Metals in Water by ICP
pH of Water by Field Measurement
TDS or Total Dissolved Solids
Temperature of Water by Field Measurement
Total Dissolved Oxygen in Water by Field Measurement
Total Organic Carbon in Water
Turbidity of Water by Field Measurement
Analysis/ Analyte
Alkalinity, total
Sulfate
Conductivity
Hardness as CaCO3
Aluminum
Antimony
Arsenic
Barium
Beryllium
Cadmium
Calcium
Chromium
Cobalt
Copper
Iron
Lead
Magnesium
Manganese
Molybdenum
Nickel
Potassium
Selenium
Silver
Sodium
Thallium
Titanium
Vanadium
Zinc
pH
Solids, total dissolved
Temperature
Dissolved Oxygen
Total Organic Carbon
Turbidity
mg/L
mg/L
umhos/cm
mg/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
mg/L
ug/L
ug/L
ug/L
ug/L
ug/L
mg/L
ug/L
ug/L
ug/L
mg/L
ug/L
ug/L
mg/L
ug/L
ug/L
ug/L
ug/L
SU
mg/L
Deg C
mg/L
mg/L
NTU
Units 13-__ 14-__ 15-__ 16-__
146 139 132 136
33.0 246 271 275
490 1460 1890 1690
201 347 361 386
256 50 U 50 U 50 U
50 U 50 U 50 U 50 U
25 U 25 U 25 U 25 U
335 92 62 96
3 U 3 U 3 U 3 U
3 U 3 U 3 U 3 U
64.3 99.0 103 110
15 U 15 U 15 U 15 U
10 U 10 U 10 U 10 U
5 U 5 U 7 5 U
260 50 U 101 50 U
50 U 50 U 50 U 50 U
9.86 24.3 25.1 27.0
5 U 27 5 20
15 U 15 U 15 U 15 U
20 U 20 U 34 20 U
10.0 14.1 12.9 14.8
50 U 50 U 50 U 50 U
25 U 25 U 25 U 25 U
13.3 154 247 180
50 U 50 U 50 U 50 U
20 U 20 U 20 U 20 U
10 U 10 U 10 U 10 U
25 U 25 U 25 U 25 U
6.92 6.91 7.03 6.89
312 888 1140 1020
11.30 10.37 12.97 9.84
0 4.28 5.42 1.89
1 U 1.8 3 2.6
3.3 0 0.1 0
4717ASR Number: 01/14/2010
DS07ESProject ID: Cleburn Street Well LTRAProject Desc:
RLAB Approved Sample Analysis Results
Page 19 of 23
1 VOCs in Water by GC/MS
Analysis/ Analyte
Acetone
Benzene
Bromodichloromethane
Bromoform
Bromomethane
2-Butanone
Carbon Disulfide
Carbon Tetrachloride
Chlorobenzene
Chloroethane
Chloroform
Chloromethane
Cyclohexane
1,2-Dibromo-3-Chloropropane
Dibromochloromethane
1,2-Dibromoethane
1,2-Dichlorobenzene
1,3-Dichlorobenzene
1,4-Dichlorobenzene
Dichlorodifluoromethane
1,1-Dichloroethane
1,2-Dichloroethane
1,1-Dichloroethene
cis-1,2-Dichloroethene
trans-1,2-Dichloroethene
1,2-Dichloropropane
cis-1,3-Dichloropropene
trans-1,3-Dichloropropene
Ethyl Benzene
2-Hexanone
Isopropylbenzene
Methyl Acetate
Methyl tert-butyl ether
Methylcyclohexane
Methylene Chloride
4-Methyl-2-Pentanone
Naphthalene
Styrene
1,1,2,2-Tetrachloroethane
Tetrachloroethene
Toluene
1,2,3-Trichlorobenzene
1,2,4-Trichlorobenzene
1,1,1-Trichloroethane
1,1,2-Trichloroethane
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
Units 13-__ 14-__ 15-__ 16-__
5.0 U 5.0 U 5.0 U 5.0 U
5.0 U 5.0 U 5.0 U 5.0 U
5.0 U 5.0 U 5.0 U 5.0 U
5.0 UJ 5.0 UJ 5.0 UJ 5.0 UJ
5.0 U 5.0 U 5.0 U 5.0 U
5.0 U 5.0 U 5.0 U 5.0 U
5.0 U 5.0 U 5.0 U 5.0 U
5.0 U 5.0 U 5.0 U 5.0 U
5.0 U 5.0 U 5.0 U 5.0 U
5.0 U 5.0 U 5.0 U 5.0 U
5.0 U 5.0 U 5.0 U 5.0 U
5.0 U 5.0 U 5.0 U 5.0 U
5.0 U 5.0 U 5.0 U 5.0 U
5.0 UJ 5.0 UJ 5.0 UJ 5.0 UJ
5.0 UJ 5.0 UJ 5.0 UJ 5.0 UJ
5.0 UJ 5.0 UJ 5.0 UJ 5.0 UJ
5.0 U 5.0 U 5.0 U 5.0 U
5.0 U 5.0 U 5.0 U 5.0 U
5.0 U 5.0 U 5.0 U 5.0 U
5.0 UJ 5.0 UJ 5.0 UJ 5.0 UJ
5.0 U 5.0 U 5.0 U 5.0 U
5.0 UJ 5.0 UJ 5.0 UJ 5.0 UJ
5.0 U 5.0 U 5.0 U 5.0 U
5.0 U 5.0 U 5.0 U 5.0 U
5.0 U 5.0 U 5.0 U 5.0 U
5.0 U 5.0 U 5.0 U 5.0 U
5.0 U 5.0 U 5.0 U 5.0 U
5.0 U 5.0 U 5.0 U 5.0 U
5.0 U 5.0 U 5.0 U 5.0 U
5.0 UJ 5.0 UJ 5.0 UJ 5.0 UJ
5.0 U 5.0 U 5.0 U 5.0 U
5.0 U 5.0 U 5.0 U 5.0 U
10 U 10 U 10 U 10 U
5.0 U 5.0 U 5.0 U 5.0 U
5.0 U 5.0 U 5.0 U 5.0 U
5.0 UJ 5.0 UJ 5.0 UJ 5.0 UJ
10 UJ 10 UJ 10 UJ 10 UJ
5.0 U 5.0 U 5.0 U 5.0 U
5.0 U 5.0 U 5.0 U 5.0 U
7.2 39000 46000 74000
5.0 U 5.0 U 5.0 U 5.0 U
5.0 UJ 5.0 UJ 5.0 UJ 5.0 UJ
5.0 UJ 5.0 UJ 5.0 UJ 5.0 UJ
5.0 U 7.0 30 28
5.0 U 5.0 U 5.0 U 5.0 U
4717ASR Number: 01/14/2010
DS07ESProject ID: Cleburn Street Well LTRAProject Desc:
RLAB Approved Sample Analysis Results
Page 20 of 23
Analysis/ Analyte
Trichloroethene
Trichlorofluoromethane
1,1,2-Trichlorotrifluoroethane
Vinyl Chloride
m and/or p-Xylene
o-Xylene
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
Units 13-__ 14-__ 15-__ 16-__
5.0 U 12 40 39
5.0 U 5.0 U 5.0 U 5.0 U
5.0 U 5.0 U 5.0 U 5.0 U
5.0 U 5.0 U 5.0 U 5.0 U
10 U 10 U 10 U 10 U
5.0 U 5.0 U 5.0 U 5.0 U
4717ASR Number: 01/14/2010
DS07ESProject ID: Cleburn Street Well LTRAProject Desc:
RLAB Approved Sample Analysis Results
Page 21 of 23
1
1
1
1
1
1
1
1
1
1
1
Alkalinity in Water by Titration
Anions in Water by Ion Chromatography
Conductivity by Field Measurement
Hardness in Water by Calculation
Metals in Water by ICP
pH of Water by Field Measurement
TDS or Total Dissolved Solids
Temperature of Water by Field Measurement
Total Dissolved Oxygen in Water by Field Measurement
Total Organic Carbon in Water
Turbidity of Water by Field Measurement
Analysis/ Analyte
Alkalinity, total
Sulfate
Conductivity
Hardness as CaCO3
Aluminum
Antimony
Arsenic
Barium
Beryllium
Cadmium
Calcium
Chromium
Cobalt
Copper
Iron
Lead
Magnesium
Manganese
Molybdenum
Nickel
Potassium
Selenium
Silver
Sodium
Thallium
Titanium
Vanadium
Zinc
pH
Solids, total dissolved
Temperature
Dissolved Oxygen
Total Organic Carbon
Turbidity
mg/L
mg/L
umhos/cm
mg/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
mg/L
ug/L
ug/L
ug/L
ug/L
ug/L
mg/L
ug/L
ug/L
ug/L
mg/L
ug/L
ug/L
mg/L
ug/L
ug/L
ug/L
ug/L
SU
mg/L
Deg C
mg/L
mg/L
NTU
Units 17-__ 18-__ 19-FB 21-FB
134 164 2.00 U
267 98.0 1.0 U
1760 854
448 221 13.2 U
50 U 2590 50 U
50 U 50 U 50 U
25 U 25 U 25 U
92 270 10 U
3 U 3 U 3 U
3 U 3 U 3 U
127 63.9 2.00 U
15 U 15 U 15 U
10 U 10 U 10 U
5 U 5 U 5 U
50 U 2230 50 U
50 U 50 U 50 U
31.7 15.0 2.00 U
15 382 5 U
15 U 15 U 15 U
37 21 20 U
14.2 10.1 2.00 U
50 U 50 U 50 U
25 U 25 U 25 U
175 78.3 5.00 U
50 U 50 U 50 U
20 U 48.6 20 U
10 U 10 U 10 U
25 U 25 U 25 U
6.93 6.63
1060 527 7
22.66 13.68
1.02 0.00
2.6 2.8 1 U
3.5 16.5
4717ASR Number: 01/14/2010
DS07ESProject ID: Cleburn Street Well LTRAProject Desc:
RLAB Approved Sample Analysis Results
Page 22 of 23
1 VOCs in Water by GC/MS
Analysis/ Analyte
Acetone
Benzene
Bromodichloromethane
Bromoform
Bromomethane
2-Butanone
Carbon Disulfide
Carbon Tetrachloride
Chlorobenzene
Chloroethane
Chloroform
Chloromethane
Cyclohexane
1,2-Dibromo-3-Chloropropane
Dibromochloromethane
1,2-Dibromoethane
1,2-Dichlorobenzene
1,3-Dichlorobenzene
1,4-Dichlorobenzene
Dichlorodifluoromethane
1,1-Dichloroethane
1,2-Dichloroethane
1,1-Dichloroethene
cis-1,2-Dichloroethene
trans-1,2-Dichloroethene
1,2-Dichloropropane
cis-1,3-Dichloropropene
trans-1,3-Dichloropropene
Ethyl Benzene
2-Hexanone
Isopropylbenzene
Methyl Acetate
Methyl tert-butyl ether
Methylcyclohexane
Methylene Chloride
4-Methyl-2-Pentanone
Naphthalene
Styrene
1,1,2,2-Tetrachloroethane
Tetrachloroethene
Toluene
1,2,3-Trichlorobenzene
1,2,4-Trichlorobenzene
1,1,1-Trichloroethane
1,1,2-Trichloroethane
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
Units 17-__ 18-__ 19-FB 21-FB
5.0 U 5.0 U 5.0 U 5.0 U
5.0 U 9.3 5.0 U 5.0 U
5.0 U 5.0 U 5.0 U 5.0 U
5.0 UJ 5.0 UJ 5.0 UJ 5.0 UJ
5.0 U 5.0 U 5.0 U 5.0 U
5.0 U 5.0 U 5.0 U 5.0 U
5.0 U 5.0 U 5.0 U 5.0 U
5.0 U 5.0 U 5.0 U 5.0 U
5.0 U 5.0 U 5.0 U 5.0 U
5.0 U 5.0 U 5.0 U 5.0 U
5.0 U 5.0 U 5.0 U 5.0 U
5.0 U 5.0 U 5.0 U 5.0 U
5.0 U 16 5.0 U 5.0 U
5.0 UJ 5.0 UJ 5.0 UJ 5.0 UJ
5.0 UJ 5.0 UJ 5.0 UJ 5.0 UJ
5.0 UJ 5.0 UJ 5.0 UJ 5.0 UJ
5.1 5.0 U 5.0 U 5.0 U
5.0 U 5.0 U 5.0 U 5.0 U
5.0 U 5.0 U 5.0 U 5.0 U
5.0 UJ 5.0 UJ 5.0 UJ 5.0 UJ
5.0 U 5.0 U 5.0 U 5.0 U
5.0 UJ 5.0 UJ 5.0 UJ 5.0 UJ
5.0 U 5.0 U 5.0 U 5.0 U
5.0 U 23 5.0 U 5.0 U
5.0 U 5.0 U 5.0 U 5.0 U
5.0 U 5.0 U 5.0 U 5.0 U
5.0 U 5.0 U 5.0 U 5.0 U
5.0 U 5.0 U 5.0 U 5.0 U
5.0 U 76 5.0 U 5.0 U
5.0 UJ 5.0 UJ 5.0 UJ 5.0 UJ
5.0 U 19 5.0 U 5.0 U
5.0 U 5.0 U 5.0 U 5.0 U
10 U 10 U 10 U 10 U
5.0 U 8.7 5.0 U 5.0 U
5.0 U 5.0 U 5.0 U 5.0 U
5.0 UJ 5.0 UJ 5.0 UJ 5.0 UJ
10 UJ 28 J 10 UJ 10 UJ
5.0 U 5.0 U 5.0 U 5.0 U
5.0 U 5.0 U 5.0 U 5.0 U
140000 39 5.0 U 5.0 U
5.0 U 40 5.0 U 5.0 U
5.0 UJ 5.0 UJ 5.0 UJ 5.0 UJ
5.0 UJ 5.0 UJ 5.0 UJ 5.0 UJ
13 5.0 U 5.0 U 5.0 U
5.0 U 5.0 U 5.0 U 5.0 U
4717ASR Number: 01/14/2010
DS07ESProject ID: Cleburn Street Well LTRAProject Desc:
RLAB Approved Sample Analysis Results
Page 23 of 23
Analysis/ Analyte
Trichloroethene
Trichlorofluoromethane
1,1,2-Trichlorotrifluoroethane
Vinyl Chloride
m and/or p-Xylene
o-Xylene
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
Units 17-__ 18-__ 19-FB 21-FB
20 260 5.0 U 5.0 U
5.0 U 5.0 U 5.0 U 5.0 U
5.0 U 5.0 U 5.0 U 5.0 U
5.0 U 5.0 U 5.0 U 5.0 U
10 U 220 10 U 10 U
5.0 U 46 5.0 U 5.0 U
4717ASR Number: 01/14/2010
DS07ESProject ID: Cleburn Street Well LTRAProject Desc:
RLAB Approved Sample Analysis Results
4717
DS07ESProject ID:
Cleburn Street Well LTRA
DeAndre SingletarySUPR/IANE
United States Environmental Protection AgencyRegion VII
901 N. 5th StreetKansas City, KS 66101
__/__/____
Data Disposition/Sample Release for ASR #:
Project Description:
Subject:
Kaye DollmannENSV/RLAB
I have received and reviewed the Transmittal of Sample Analysis Results for the above-referencedAnalytical Services Request(ASR) and have indicated my findings below by checking one of theboxes for Data Disposition.
I understand all samples will be disposed upon receipt of this form, unless samples are requestedto be held. If I do not return this form all samples will be disposed of on ___________________.
"RELEASED" - Read-only to all Region 7 employees and contractors that have R7LIMS"Customer" account. All Samples may be disposed of upon receipt of this form if not requested tobe held.
"Project Manager Accessible" - Available on the LAN in R7LIMS for my use only. All Samples maybe disposed of upon receipt of this form if not requested to be held.
"Archived" - THIS DATA IS OF A SENSITIVE NATURE. Any future reports must be requestedthrough the laboratory. All samples may be disposed of upon receipt of the form if not requestedto be held.
Date:
From:
To:
Hold Samples - I have determined that the samples need to be held until ______________, afterwhich time they will be disposed of in accordance with applicable regulations. The reason for the hold is:
Samples are associated with a legal proceeding.
Question/Concern with data - possible reanalysis requested.
Other:________________________________________________________________
JANUARY 2010
Page 1 of 48
03/02/2010Date:
4758
MP7ES02
Cleburn Street well sampling
Mary PetersonSUPR/IANE
Transmittal of Sample Analysis Results for ASR #:
Project ID:
Project Description:
Michael F. Davis, ChiefChemical Analysis and Response Branch, Environmental Services Division
To:
Enclosed are the analytical data for the above-referenced Analytical Services Request (ASR) andProject. The Regional Laboratory has reviewed and verified the results in accordance with proceduresdescribed in our Quality Manual (QM). In addition to all of the analytical results, this transmittalcontains pertinent information that may have influenced the reported results and documents anydeviations from the established requirements of the QM.
Please contact us within 14 days of receipt of this package if you determine there is a need for anychanges. Please complete the enclosed Customer Satisfaction Survey and Data Disposition/SampleRelease memo for this ASR as soon as possible. The process of disposing of the samples for this ASRwill be initiated 30 days from the date of this transmittal unless an alternate release date is specifiedon the Data Disposition/Sample Release memo.
If you have any questions or concerns relating to this data package, contact our customer service lineat 913-551-5295.
Enclosures
cc: Analytical Data File.
United States Environmental Protection AgencyRegion 7
901 N. 5th StreetKansas City, KS 66101
Subject:
From:
Page 2 of 48
4758ASR Number: 03/02/2010
Mary Peterson SUPR/IANE 913-551-7882
MP7ES02
Cleburn Street well sampling
Grand Island Nebraska Superfund
CLEBURN STREET WELL - 1 HR MARTINIZING GWRESORATION
07ESSite ID: 02
Site Cleanup Support
ISCO Post Injection event and Quarterly Performance monitoring.
Project Manager: Org: Phone:
Project ID:
Project Desc:
Location: State: Program:
Site Name: Site OU:
Purpose:
__ = Field SampleFB = Field BlankFD = Field Duplicate
QC Codes identify the type of sample for quality control purpose.
Degrees CelsiusNephelometric Turbidity UnitsStandard Units (pH)Milligrams per LiterMicrograms per LiterMicromhos per Centimeter
Specific units in which results arereported.
The identification of the analyte is acceptable; the reported value is anestimate.The analyte was not detected at or above the reporting limit.The analyte was not detected at or above the reporting limit. The reportinglimit is an estimate.
Specific codes used in conjunction with data values to provide additional information on the quality of reported results, or used to explain the absence of a specific value.
Summary of Project Information
Explanation of Codes, Units and Qualifiers used on this report
Sample QC Codes: Units:
J
UUJ
=
==
Data Qualifiers:
= Values have been reviewed and found acceptable for use. (Blank)
Deg CNTUSU
mg/Lug/L
umhos/cm
======
2009073QAPP Number:
302DD2CGPRA PRC:
Page 3 of 48
1
2
3
4
4
5
6
7
8
9
10
10
11
12
13
14
15
16
17
18
18
19
20
21
21
23
24
25
26
27
28
29
30
31
32
33
34
35
35
37
38
39
SampleNo
__
__
__
__
FD
__
__
__
__
__
__
FD
__
__
__
__
__
__
__
__
FD
__
FB
__
FD
__
__
__
__
__
__
__
__
__
__
__
__
__
FD
__
__
__
QCCode
Water
Water
Water
Water
Water
Water
Water
Water
Water
Water
Water
Water
Water
Water
Water
Water
Water
Water
Water
Water
Water
Water
Water
Water
Water
Water
Water
Water
Water
Water
Water
Water
Water
Water
Water
Water
Water
Water
Water
Water
Water
Water
Matrix
IW-5
IW-6
IW-7
IW-3
IW-3/Field Duplicate of sample 4
IW-2
IW-4
IW-1
ERT-16
IW-8
IW-10
IW-10/Field Duplicate of sample10IW-9
MW-2B
MW-2A
MW-12A
ERT-14
ERT-15
DPE-1
DPE-2
DPE-2/Field Duplicate of sample18DPE-3
Field Blank sample
MW-108BB
MW-108BB/Field Duplicate ofsample 21MW-11B
MW-11A
MW-107AA
MW-107BB
MW-106CC
MW-106BB
MW-9A
MW-10A
MW-10B
MW-103CC
MW-103BB
MW-103AA
MW-104BB
MW-104BB/Field Duplicate ofsample 35MW-104AA
MW-101AA
MW-105BB
Location DescriptionExternal
Sample No
01/19/2010
01/19/2010
01/19/2010
01/20/2010
01/20/2010
01/20/2010
01/20/2010
01/20/2010
01/20/2010
01/20/2010
01/21/2010
01/21/2010
01/21/2010
01/21/2010
01/21/2010
01/24/2010
01/24/2010
01/24/2010
01/25/2010
01/25/2010
01/25/2010
01/25/2010
01/21/2010
01/22/2010
01/22/2010
01/22/2010
01/22/2010
01/22/2010
01/22/2010
01/22/2010
01/22/2010
01/22/2010
01/23/2010
01/23/2010
01/23/2010
01/23/2010
01/23/2010
01/23/2010
01/23/2010
01/23/2010
01/23/2010
01/24/2010
Start Date
11:45
15:30
18:15
09:00
09:00
10:35
11:45
14:20
15:35
18:00
09:35
09:35
11:30
14:00
16:05
14:50
16:05
17:20
10:50
12:20
12:20
08:00
10:55
10:55
11:35
12:15
14:25
15:05
16:20
17:00
17:45
09:05
09:55
12:15
14:00
14:45
14:45
15:50
16:45
09:15
Start Time
End Date
End Time
01/21/2010
01/21/2010
01/21/2010
01/21/2010
01/21/2010
01/21/2010
01/21/2010
01/21/2010
01/21/2010
01/22/2010
01/22/2010
01/22/2010
01/22/2010
01/22/2010
01/22/2010
01/26/2010
01/26/2010
01/26/2010
01/26/2010
01/26/2010
01/26/2010
01/26/2010
01/22/2010
01/26/2010
01/26/2010
01/26/2010
01/26/2010
01/26/2010
01/26/2010
01/26/2010
01/26/2010
01/26/2010
01/26/2010
01/26/2010
01/26/2010
01/26/2010
01/26/2010
01/26/2010
01/26/2010
01/26/2010
01/26/2010
01/26/2010
ReceiptDate
4758 03/02/2010
MP7ES02Project ID: Cleburn Street well samplingProject Desc:
ASR Number: Sample Information Summary
-
-
-
-
-
-
-
-
-
-
-
-
-
-
-
-
-
-
-
-
-
-
-
-
-
-
-
-
-
-
-
-
-
-
-
-
-
-
-
-
-
-
Page 4 of 48
40
41
42
43
44
45
46
46
48
49
50
50
52
53
54
55
56
68
69
70
SampleNo
__
__
__
__
__
__
__
FD
__
__
__
FD
__
__
__
__
__
FB
FB
FB
QCCode
Water
Water
Water
Water
Water
Water
Water
Water
Water
Water
Water
Water
Water
Water
Water
Water
Water
Water
Water
Water
Matrix
MW-8A
MW-8B
MW-102AA
MW-102BB
Cleburn Street well
DPE-4
MW-13A
MW-13A/Field Duplicate of sample46DPT-1A
DPT-1B
DPT-4B
DPT-4B/Field Duplicate of sample50DPT-4A
DPT-3B
DPT-3A
DPT-2B
DPT-2A
VOA Trip Blank sample 1
VOA Trip Blank sample 2
VOA Trip Blank sample 3
Location DescriptionExternal
Sample No
01/24/2010
01/24/2010
01/24/2010
01/24/2010
01/25/2010
01/25/2010
01/26/2010
01/26/2010
01/26/2010
01/26/2010
01/26/2010
01/26/2010
01/26/2010
01/26/2010
01/26/2010
01/26/2010
01/26/2010
01/13/2010
01/13/2010
01/13/2010
Start Date
09:55
11:20
13:15
14:00
13:40
16:00
09:50
09:50
11:05
11:45
12:50
12:50
14:15
14:50
15:30
16:05
12:00
11:57
12:04
Start Time
01/19/2010
01/20/2010
01/20/2010
End Date
14:40
08:20
17:30
End Time
01/26/2010
01/26/2010
01/26/2010
01/26/2010
01/26/2010
01/26/2010
01/28/2010
01/28/2010
01/28/2010
01/28/2010
01/28/2010
01/28/2010
01/28/2010
01/28/2010
01/28/2010
01/28/2010
01/28/2010
01/21/2010
01/21/2010
01/22/2010
ReceiptDate
4758 03/02/2010
MP7ES02Project ID: Cleburn Street well samplingProject Desc:
ASR Number: Sample Information Summary
-
-
-
-
-
-
-
-
-
-
-
-
-
-
-
-
-
-
-
-
Page 5 of 48
1
1
1
1
Alkalinity in Water by Titration
Anions in Water by Ion Chromatography
Conductivity by Field Measurement
Hardness in Water by Calculation
Region 7 EPA Laboratory - Kansas City, Ks.
Region 7 ESAT Contract Lab (In-House)
(Field Measurement)
Region 7 ESAT Contract Lab (In-House)
Lab:
Lab:
Lab:
Lab:
EPA Region 7 RLAB Method 3132.1E
Region 7 RLAB Method 3135.12A
Measurement of field parameter
Method:
Method:
Method:
Dilutions were necessary in order to obtain valid results due to matrix interferences.This was to prevent instrument damage. The reporting limits were elevated 1000 times dueto dilutions in samples 13 and 16. The reporting limits were raised 10000 times due todilutions in samples 1, 2, 3, 4, 4 FD, 5, 6, 7, 8, 9, 10, 10 FD, 11, 17, 18, 18 FD, 19, and45.
(N/A)
Comments:
Comments:
Comments:
1-__ 2-__ 3-__ 4-__ 4-FD 5-__ 6-__7-__ 8-__ 9-__ 10-__ 10-FD 11-__ 12-__13-__ 14-__ 15-__ 16-__ 17-__ 18-__ 18-FD19-__ 20-FB 45-__
1-__ 2-__ 3-__ 4-__ 4-FD 5-__ 6-__7-__ 8-__ 9-__ 10-__ 10-FD 11-__ 12-__13-__ 14-__ 15-__ 16-__ 17-__ 18-__ 18-FD19-__ 20-FB 45-__
1-__ 2-__ 3-__ 4-__ 4-FD 5-__ 6-__7-__ 8-__ 9-__ 10-__ 10-FD 11-__ 12-__13-__ 14-__ 15-__ 16-__ 17-__ 18-__ 18-FD19-__ 21-__ 21-FD 23-__ 24-__ 25-__ 26-__27-__ 28-__ 29-__ 31-__ 33-__ 34-__ 35-__35-FD 37-__ 38-__ 39-__ 40-__ 41-__ 42-__43-__ 44-__ 45-__ 46-__ 46-FD 48-__ 49-__50-__ 50-FD 52-__ 53-__ 55-__ 56-__
Samples:
Samples:
Samples:
4758ASR Number: 03/02/2010
MP7ES02Project ID: Cleburn Street well samplingProject Desc
RLAB Approved Analysis Comments
Analysis Comments About Results For This Analysis
Page 6 of 48
1 Metals in Water by ICP-AES
Region 7 ESAT Contract Lab (In-House)Lab:
EPA Region 7 RLAB Method 3122.3C
EPA Region 7 RLAB Method 3122.3C
Method:
Method:
Dilutions were necessary in order to obtain valid results due to matrix interferences. Thereporting limits were elevated (X times) due to dilutions in samples 1-11(1000), 4FD &10FD(1000), 12(10), 13(100), 14(10), 15(10), 16-19(1000), 18FD(1000), and 45(1000).
Slight nickel (20.2) contamination was found in the laboratory method blank, 951MB. Onlysamples containing this analyte at a level greater than ten times the contamination level ofthe blank are reported without being qualified. All samples that contained this analyte butat a level less than ten times the contamination in the blank have the result U-codedindicating that the reporting limit has been raised to the level found in the sample.Samples affected were: 20FB.
Aluminum (72, 76-127), beryllium (69, 77-105), cadmium (68, 77-105), cobalt (68, 70-102), copper (72, 79-105), sodium (75, 84-109), iron (74, 76-109), magnesium (73, 85-108), potassium (69, 85-112), titanium (71, 78-112), and vanadium (69, 76-105) wereUJ-coded in sample 12. These analytes were not found in the sample at or above thereporting limit; however, the reporting limit is an estimate (UJ-coded) due to low recoveryof these analytes in the laboratory matrix spike duplicate. The actual reporting limit forthese analytes may be higher than the reported value.
Barium (56, 70-114) and calcium (45, 81-110) were J-coded in sample 12. Although theanalytes in question have been positively identified in the sample, the quantitation is anestimate (J-coded) due to low recovery of these analytes in the laboratory matrix spikeduplicate. The actual concentration for these analytes may be higher than the reportedvalue.
Nickel (64, 70-102) was J-coded in sample 15. Although the analyte in question has beenpositively identified in the sample, the quantitation is an estimate (J-coded) due to lowrecovery of this analyte in the laboratory matrix spike. The actual concentration for thisanalyte may be higher than the reported value.
Comments:
Comments:
1-__ 2-__ 3-__ 4-__ 4-FD 5-__ 6-__7-__ 8-__ 9-__ 10-__ 10-FD 11-__ 12-__13-__ 14-__ 15-__ 16-__ 17-__ 18-__ 18-FD19-__ 20-FB 45-__
1-__ 2-__ 3-__ 4-__ 4-FD 5-__ 6-__7-__ 8-__ 9-__ 10-__ 10-FD 11-__ 12-__13-__ 14-__ 15-__ 16-__ 17-__ 18-__ 18-FD19-__ 20-FB 45-__
Samples:
Samples:
4758ASR Number: 03/02/2010
MP7ES02Project ID: Cleburn Street well samplingProject Desc
RLAB Approved Analysis Comments
Analysis Comments About Results For This Analysis
Page 7 of 48
1
1
pH of Water by Field Measurement
TDS or Total Dissolved Solids
(Field Measurement)
Region 7 EPA Laboratory - Kansas City, Ks.
Lab:
Lab:
Measurement of field parameter
EPA Region 7 RLAB Method 3142.2B
Method:
Method:
Aluminum (34, 5.8), antimony (28, 5.0), arsenic (15, 5.0), beryllium (30, 5.4), cadmium(31, 5.0), chromium (27, 5.3), cobalt (32, 5.0), copper (32, 5.0), iron (33, 5.0), lead (29,5.3), magnesium (32, 5.0), molybdenum (27, 5.4), nickel (7.8, 5.0), potassium (31, 5.0),selenium (39, 6.5), silver (35, 5.9), sodium (32, 5.0), thallium (31, 5.2), titanium (31,5.0), vanadium (33, 5.0), and zinc (33, 5.0) were UJ-coded in sample 12. These analyteswere not found in the sample at or above the reporting limit, however, the reporting limit isan estimate (UJ-coded) due to poor precision obtained for these analytes in the laboratorymatrix spike and matrix spike duplicate. The actual reporting limit for these analytes maybe higher than the reported value.
Barium (32, 5.0) and calcium (31, 5.0) were J-coded in sample 12. Although the analytesin question have been positively identified in the sample, the quantitation is an estimate (J-coded) due to poor precision obtained for these analytes in the laboratory matrix spike andmatrix spike duplicate.
Copper (5.5, 5.0), thallium (18, 5.2), and zinc (7.4, 5.0) were UJ-coded in sample 15.These analytes were not found in the sample at or above the reporting limit, however, thereporting limit is an estimate (UJ-coded) due to poor precision obtained for these analytesin the laboratory matrix spike and matrix spike duplicate. The actual reporting limit forthese analytes may be higher than the reported value.
Nickel (24, 5.0) was J-coded in sample 15. Although the analyte in question has beenpositively identified in the sample, the quantitation is an estimate (J-coded) due to poorprecision obtained for this analyte in the laboratory matrix spike and matrix spikeduplicate.
(N/A)Comments:
1-__ 2-__ 3-__ 4-__ 4-FD 5-__ 6-__7-__ 8-__ 9-__ 10-__ 10-FD 11-__ 12-__13-__ 14-__ 15-__ 16-__ 17-__ 18-__ 18-FD19-__ 21-__ 21-FD 23-__ 24-__ 25-__ 26-__27-__ 28-__ 29-__ 31-__ 33-__ 34-__ 35-__35-FD 37-__ 38-__ 39-__ 40-__ 41-__ 42-__43-__ 44-__ 45-__ 46-__ 46-FD 48-__ 49-__50-__ 50-FD 52-__ 53-__ 55-__ 56-__
1-__ 2-__ 3-__ 4-__ 4-FD 5-__ 6-__
Samples:
Samples:
4758ASR Number: 03/02/2010
MP7ES02Project ID: Cleburn Street well samplingProject Desc
RLAB Approved Analysis Comments
Analysis Comments About Results For This Analysis
Page 8 of 48
1
1
1
Temperature of Water by Field Measurement
Total Organic Carbon in Water
Turbidity of Water by Field Measurement
(Field Measurement)
REAP Contract Lab (Out-Source)
(Field Measurement)
Lab:
Lab:
Lab:
Measurement of field parameter
Similar to EPA SW846 Method 9060 or StandardMethods (20th Edtion) 5310 B, C,or D (see comments)
Measurement of field parameter
Method:
Method:
Method:
(N/A)
(N/A)
Comments:
Comments:
Comments:
7-__ 8-__ 9-__ 10-__ 10-FD 11-__ 12-__13-__ 14-__ 15-__ 16-__ 17-__ 18-__ 18-FD19-__ 20-FB 45-__
1-__ 2-__ 3-__ 4-__ 4-FD 5-__ 6-__7-__ 8-__ 9-__ 10-__ 10-FD 11-__ 12-__13-__ 14-__ 15-__ 16-__ 17-__ 18-__ 18-FD19-__ 21-__ 21-FD 23-__ 24-__ 25-__ 26-__27-__ 28-__ 29-__ 31-__ 33-__ 34-__ 35-__35-FD 37-__ 38-__ 39-__ 40-__ 41-__ 42-__43-__ 44-__ 45-__ 46-__ 46-FD 48-__ 49-__50-__ 50-FD 52-__ 53-__ 55-__ 56-__
1-__ 2-__ 3-__ 4-__ 4-FD 5-__ 6-__7-__ 8-__ 9-__ 10-__ 10-FD 11-__ 12-__13-__ 14-__ 15-__ 16-__ 17-__ 20-FB
1-__ 2-__ 3-__ 4-__ 4-FD 5-__ 6-__7-__ 8-__ 9-__ 10-__ 10-FD 11-__ 12-__13-__ 14-__ 15-__ 16-__ 17-__ 18-__ 18-FD19-__ 21-__ 21-FD 23-__ 24-__ 25-__ 26-__27-__ 28-__ 29-__ 31-__ 33-__ 34-__ 35-__35-FD 37-__ 38-__ 39-__ 40-__ 41-__ 42-__43-__ 44-__ 45-__ 46-__ 46-FD 48-__ 49-__50-__ 50-FD 52-__ 53-__ 55-__ 56-__
Samples:
Samples:
Samples:
Samples:
4758ASR Number: 03/02/2010
MP7ES02Project ID: Cleburn Street well samplingProject Desc
RLAB Approved Analysis Comments
Analysis Comments About Results For This Analysis
Page 9 of 48
1 VOCs in Water by GC/MS
Region 7 ESAT Contract Lab (In-House)Lab:
EPA Region 7 RLAB Method 3230.1FMethod:
(N/A)
Reporting Limits:Twenty-two of the samples contained potassium permanganate. These samples werediluted to keep the column from being damaged. The resulting reporting limit for thesesamples were 5000 times higher than the normal reporting limit. Acetone (+20.7%) was UJ-coded in samples 32, 20-FB, 68-FB, 69-FB, 70-FB, 12, 14, 21,21-FD, 23, 24, 25, 26, 27, 28, and 29. This analyte was not found in the samples at orabove the reporting limit, however, the reporting limit is an estimate (UJ-coded) due to thecontinuing calibration check not meeting accuracy specifications. The actual reporting limitfor this analyte may be higher than the reported value. Styrene (68% & 64%, 83%-121%) was UJ-coded in sample 41. This analyte was notfound in the sample at or above the reporting limit, however, the reporting limit is anestimate (UJ-coded) due to low recovery of this analyte in the laboratory matrix spike. Theactual reporting limit for this analyte may be higher than the reported value. Carbon Disulfide (20RPD, 15PCL) was UJ-coded in sample 32. This analyte was not foundin the sample at or above the reporting limit, however, the reporting limit is an estimate(UJ-coded) due to poor precision obtained for this analyte in the laboratory matrix spikeand matrix spike duplicate. The actual reporting limit for this analyte may be higher thanthe reported value.
Comments:
Comments:
1-__ 2-__ 3-__ 4-__ 4-FD 5-__ 6-__7-__ 8-__ 9-__ 10-__ 10-FD 11-__ 12-__13-__ 14-__ 15-__ 16-__ 17-__ 18-__ 18-FD19-__ 20-FB 21-__ 21-FD 23-__ 24-__ 25-__26-__ 27-__ 28-__ 29-__ 30-__ 31-__ 32-__33-__ 34-__ 35-__ 35-FD 37-__ 38-__ 39-__40-__ 41-__ 42-__ 43-__ 44-__ 45-__ 46-__46-FD 48-__ 49-__ 50-__ 50-FD 52-__ 53-__54-__ 55-__ 56-__ 68-FB 69-FB 70-FB
Samples:
4758ASR Number: 03/02/2010
MP7ES02Project ID: Cleburn Street well samplingProject Desc
RLAB Approved Analysis Comments
Analysis Comments About Results For This Analysis
Page 10 of 48
1
1
1
1
1
1
1
1
1
1
1
Alkalinity in Water by Titration
Anions in Water by Ion Chromatography
Conductivity by Field Measurement
Hardness in Water by Calculation
Metals in Water by ICP-AES
pH of Water by Field Measurement
TDS or Total Dissolved Solids
Temperature of Water by Field Measurement
Total Organic Carbon in Water
Turbidity of Water by Field Measurement
VOCs in Water by GC/MS
Analysis/ Analyte
Alkalinity, total
Sulfate
Conductivity
Hardness as CaCO3
Aluminum
Antimony
Arsenic
Barium
Beryllium
Cadmium
Calcium
Chromium
Cobalt
Copper
Iron
Lead
Magnesium
Manganese
Molybdenum
Nickel
Potassium
Selenium
Silver
Sodium
Thallium
Titanium
Vanadium
Zinc
pH
Solids, total dissolved
Temperature
Total Organic Carbon
Turbidity
Acetone
Benzene
mg/L
mg/L
umhos/cm
mg/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
mg/L
ug/L
ug/L
ug/L
ug/L
ug/L
mg/L
ug/L
ug/L
ug/L
mg/L
ug/L
ug/L
mg/L
ug/L
ug/L
ug/L
ug/L
SU
mg/L
Deg C
mg/L
NTU
ug/L
ug/L
Units 1-__ 2-__ 3-__ 4-__
180 269 4.00 U 281
10000 U 10000 U 10000 U 10000 U
8310 7710 8390 6060
13200 U 13200 U 13200 U 13200 U
50000 U 50000 U 50000 U 50000 U
50000 U 50000 U 50000 U 50000 U
25000 U 25000 U 25000 U 25000 U
10000 U 10000 U 10000 U 10000 U
3000 U 3000 U 3000 U 3000 U
3000 U 3000 U 3000 U 3000 U
2000 U 2000 U 2000 U 2000 U
15000 U 15000 U 15000 U 15000 U
10000 U 10000 U 10000 U 10000 U
5000 U 5000 U 5000 U 5000 U
50000 U 50000 U 50000 U 50000 U
50000 U 50000 U 50000 U 50000 U
2000 U 2000 U 2000 U 2000 U
291000 362000 341000 301000
7500 U 15000 U 15000 U 15000 U
20000 U 20000 U 20000 U 20000 U
2000 U 2000 U 2000 U 2000 U
50000 U 50000 U 50000 U 50000 U
25000 U 25000 U 25000 U 25000 U
5000 U 5000 U 5000 U 5000 U
50000 U 50000 U 50000 U 50000 U
20000 U 20000 U 20000 U 20000 U
10000 U 10000 U 10000 U 10000 U
25000 U 25000 U 25000 U 25000 U
5.82 6.08 3.40 7.47
8540 8410 6610 7400
10.66 12.24 10.12 13.65
9.6 15.2 20.2 9
11.6 5.3 72.9 0.0
25000 U 25000 U 25000 U 25000 U
25000 U 25000 U 25000 U 25000 U
4758ASR Number: 03/02/2010
MP7ES02Project ID: Cleburn Street well samplingProject Desc:
RLAB Approved Sample Analysis Results
Page 11 of 48
Analysis/ Analyte
Bromodichloromethane
Bromoform
Bromomethane
2-Butanone
Carbon Disulfide
Carbon Tetrachloride
Chlorobenzene
Chloroethane
Chloroform
Chloromethane
Cyclohexane
1,2-Dibromo-3-Chloropropane
Dibromochloromethane
1,2-Dibromoethane
1,2-Dichlorobenzene
1,3-Dichlorobenzene
1,4-Dichlorobenzene
Dichlorodifluoromethane
1,1-Dichloroethane
1,2-Dichloroethane
1,1-Dichloroethene
cis-1,2-Dichloroethene
trans-1,2-Dichloroethene
1,2-Dichloropropane
cis-1,3-Dichloropropene
trans-1,3-Dichloropropene
Ethyl Benzene
2-Hexanone
Isopropylbenzene
Methyl Acetate
Methyl tert-butyl ether
Methylcyclohexane
Methylene Chloride
4-Methyl-2-Pentanone
Naphthalene
Styrene
1,1,2,2-Tetrachloroethane
Tetrachloroethene
Toluene
1,2,3-Trichlorobenzene
1,2,4-Trichlorobenzene
1,1,1-Trichloroethane
1,1,2-Trichloroethane
Trichloroethene
Trichlorofluoromethane
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
Units 1-__ 2-__ 3-__ 4-__
25000 U 25000 U 25000 U 25000 U
25000 U 25000 U 25000 U 25000 U
25000 U 25000 U 25000 U 25000 U
25000 U 25000 U 25000 U 25000 U
25000 U 25000 U 25000 U 25000 U
25000 U 25000 U 25000 U 25000 U
25000 U 25000 U 25000 U 25000 U
25000 U 25000 U 25000 U 25000 U
25000 U 25000 U 25000 U 25000 U
25000 U 25000 U 25000 U 25000 U
25000 U 25000 U 25000 U 25000 U
25000 U 25000 U 25000 U 25000 U
25000 U 25000 U 25000 U 25000 U
25000 U 25000 U 25000 U 25000 U
25000 U 25000 U 25000 U 25000 U
25000 U 25000 U 25000 U 25000 U
25000 U 25000 U 25000 U 25000 U
25000 U 25000 U 25000 U 25000 U
25000 U 25000 U 25000 U 25000 U
25000 U 25000 U 25000 U 25000 U
25000 U 25000 U 25000 U 25000 U
25000 U 25000 U 25000 U 25000 U
25000 U 25000 U 25000 U 25000 U
25000 U 25000 U 25000 U 25000 U
25000 U 25000 U 25000 U 25000 U
25000 U 25000 U 25000 U 25000 U
25000 U 25000 U 25000 U 25000 U
25000 U 25000 U 25000 U 25000 U
25000 U 25000 U 25000 U 25000 U
25000 U 25000 U 25000 U 25000 U
50000 U 50000 U 50000 U 50000 U
25000 U 25000 U 25000 U 25000 U
25000 U 25000 U 25000 U 25000 U
25000 U 25000 U 25000 U 25000 U
50000 U 50000 U 50000 U 50000 U
25000 U 25000 U 25000 U 25000 U
25000 U 25000 U 25000 U 25000 U
25000 U 25000 U 25000 U 25000 U
25000 U 25000 U 25000 U 25000 U
25000 U 25000 U 25000 U 25000 U
25000 U 25000 U 25000 U 25000 U
25000 U 25000 U 25000 U 25000 U
25000 U 25000 U 25000 U 25000 U
25000 U 25000 U 25000 U 25000 U
25000 U 25000 U 25000 U 25000 U
4758ASR Number: 03/02/2010
MP7ES02Project ID: Cleburn Street well samplingProject Desc:
RLAB Approved Sample Analysis Results
Page 12 of 48
Analysis/ Analyte
1,1,2-Trichlorotrifluoroethane
Vinyl Chloride
m and/or p-Xylene
o-Xylene
ug/L
ug/L
ug/L
ug/L
Units 1-__ 2-__ 3-__ 4-__
25000 U 25000 U 25000 U 25000 U
25000 U 25000 U 25000 U 25000 U
50000 U 50000 U 50000 U 50000 U
25000 U 25000 U 25000 U 25000 U
4758ASR Number: 03/02/2010
MP7ES02Project ID: Cleburn Street well samplingProject Desc:
RLAB Approved Sample Analysis Results
Page 13 of 48
1
1
1
1
1
1
1
1
1
1
1
Alkalinity in Water by Titration
Anions in Water by Ion Chromatography
Conductivity by Field Measurement
Hardness in Water by Calculation
Metals in Water by ICP-AES
pH of Water by Field Measurement
TDS or Total Dissolved Solids
Temperature of Water by Field Measurement
Total Organic Carbon in Water
Turbidity of Water by Field Measurement
VOCs in Water by GC/MS
Analysis/ Analyte
Alkalinity, total
Sulfate
Conductivity
Hardness as CaCO3
Aluminum
Antimony
Arsenic
Barium
Beryllium
Cadmium
Calcium
Chromium
Cobalt
Copper
Iron
Lead
Magnesium
Manganese
Molybdenum
Nickel
Potassium
Selenium
Silver
Sodium
Thallium
Titanium
Vanadium
Zinc
pH
Solids, total dissolved
Temperature
Total Organic Carbon
Turbidity
Acetone
Benzene
mg/L
mg/L
umhos/cm
mg/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
mg/L
ug/L
ug/L
ug/L
ug/L
ug/L
mg/L
ug/L
ug/L
ug/L
mg/L
ug/L
ug/L
mg/L
ug/L
ug/L
ug/L
ug/L
SU
mg/L
Deg C
mg/L
NTU
ug/L
ug/L
Units 4-FD 5-__ 6-__ 7-__
283 227 255 236
10000 U 10000 U 10000 U 10000 U
6060 8000 6270 8970
13200 U 13200 U 13200 U 13200 U
50000 U 50000 U 50000 U 50000 U
50000 U 50000 U 50000 U 50000 U
19600 25000 U 25000 U 25000 U
10000 U 10000 U 10000 U 10000 U
3000 U 3000 U 3000 U 3000 U
3000 U 3000 U 3000 U 3000 U
2000 U 2000 U 2000 U 2000 U
15000 U 15000 U 15000 U 15000 U
10000 U 10000 U 10000 U 10000 U
5000 U 5000 U 5000 U 5000 U
50000 U 50000 U 50000 U 50000 U
50000 U 50000 U 50000 U 50000 U
2000 U 2000 U 2000 U 2000 U
214000 319000 347000 285000
15000 U 15000 U 15000 U 15000 U
20000 U 20000 U 20000 U 20000 U
2000 U 2000 U 2000 U 2000 U
50000 U 50000 U 50000 U 50000 U
25000 U 25000 U 25000 U 25000 U
5000 U 5000 U 5000 U 5000 U
50000 U 50000 U 50000 U 50000 U
20000 U 20000 U 20000 U 20000 U
10000 U 10000 U 10000 U 10000 U
25000 U 25000 U 25000 U 25000 U
7.47 7.25 7.27 7.57
7330 10300 7610 11400
13.65 14.6 13.95 13.91
9 11.1 8.9 7.2
0.0 3.2 0.0 1.2
25000 U 25000 U 25000 U 25000 U
25000 U 25000 U 25000 U 25000 U
4758ASR Number: 03/02/2010
MP7ES02Project ID: Cleburn Street well samplingProject Desc:
RLAB Approved Sample Analysis Results
Page 14 of 48
Analysis/ Analyte
Bromodichloromethane
Bromoform
Bromomethane
2-Butanone
Carbon Disulfide
Carbon Tetrachloride
Chlorobenzene
Chloroethane
Chloroform
Chloromethane
Cyclohexane
1,2-Dibromo-3-Chloropropane
Dibromochloromethane
1,2-Dibromoethane
1,2-Dichlorobenzene
1,3-Dichlorobenzene
1,4-Dichlorobenzene
Dichlorodifluoromethane
1,1-Dichloroethane
1,2-Dichloroethane
1,1-Dichloroethene
cis-1,2-Dichloroethene
trans-1,2-Dichloroethene
1,2-Dichloropropane
cis-1,3-Dichloropropene
trans-1,3-Dichloropropene
Ethyl Benzene
2-Hexanone
Isopropylbenzene
Methyl Acetate
Methyl tert-butyl ether
Methylcyclohexane
Methylene Chloride
4-Methyl-2-Pentanone
Naphthalene
Styrene
1,1,2,2-Tetrachloroethane
Tetrachloroethene
Toluene
1,2,3-Trichlorobenzene
1,2,4-Trichlorobenzene
1,1,1-Trichloroethane
1,1,2-Trichloroethane
Trichloroethene
Trichlorofluoromethane
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
Units 4-FD 5-__ 6-__ 7-__
25000 U 25000 U 25000 U 25000 U
25000 U 25000 U 25000 U 25000 U
25000 U 25000 U 25000 U 25000 U
25000 U 25000 U 25000 U 25000 U
25000 U 25000 U 25000 U 25000 U
25000 U 25000 U 25000 U 25000 U
25000 U 25000 U 25000 U 25000 U
25000 U 25000 U 25000 U 25000 U
25000 U 25000 U 25000 U 25000 U
25000 U 25000 U 25000 U 25000 U
25000 U 25000 U 25000 U 25000 U
25000 U 25000 U 25000 U 25000 U
25000 U 25000 U 25000 U 25000 U
25000 U 25000 U 25000 U 25000 U
25000 U 25000 U 25000 U 25000 U
25000 U 25000 U 25000 U 25000 U
25000 U 25000 U 25000 U 25000 U
25000 U 25000 U 25000 U 25000 U
25000 U 25000 U 25000 U 25000 U
25000 U 25000 U 25000 U 25000 U
25000 U 25000 U 25000 U 25000 U
25000 U 25000 U 25000 U 25000 U
25000 U 25000 U 25000 U 25000 U
25000 U 25000 U 25000 U 25000 U
25000 U 25000 U 25000 U 25000 U
25000 U 25000 U 25000 U 25000 U
25000 U 25000 U 25000 U 25000 U
25000 U 25000 U 25000 U 25000 U
25000 U 25000 U 25000 U 25000 U
25000 U 25000 U 25000 U 25000 U
50000 U 50000 U 50000 U 50000 U
25000 U 25000 U 25000 U 25000 U
25000 U 25000 U 25000 U 25000 U
25000 U 25000 U 25000 U 25000 U
50000 U 50000 U 50000 U 50000 U
25000 U 25000 U 25000 U 25000 U
25000 U 25000 U 25000 U 25000 U
25000 U 25000 U 25000 U 25000 U
25000 U 25000 U 25000 U 25000 U
25000 U 25000 U 25000 U 25000 U
25000 U 25000 U 25000 U 25000 U
25000 U 25000 U 25000 U 25000 U
25000 U 25000 U 25000 U 25000 U
25000 U 25000 U 25000 U 25000 U
25000 U 25000 U 25000 U 25000 U
4758ASR Number: 03/02/2010
MP7ES02Project ID: Cleburn Street well samplingProject Desc:
RLAB Approved Sample Analysis Results
Page 15 of 48
Analysis/ Analyte
1,1,2-Trichlorotrifluoroethane
Vinyl Chloride
m and/or p-Xylene
o-Xylene
ug/L
ug/L
ug/L
ug/L
Units 4-FD 5-__ 6-__ 7-__
25000 U 25000 U 25000 U 25000 U
25000 U 25000 U 25000 U 25000 U
50000 U 50000 U 50000 U 50000 U
25000 U 25000 U 25000 U 25000 U
4758ASR Number: 03/02/2010
MP7ES02Project ID: Cleburn Street well samplingProject Desc:
RLAB Approved Sample Analysis Results
Page 16 of 48
1
1
1
1
1
1
1
1
1
1
1
Alkalinity in Water by Titration
Anions in Water by Ion Chromatography
Conductivity by Field Measurement
Hardness in Water by Calculation
Metals in Water by ICP-AES
pH of Water by Field Measurement
TDS or Total Dissolved Solids
Temperature of Water by Field Measurement
Total Organic Carbon in Water
Turbidity of Water by Field Measurement
VOCs in Water by GC/MS
Analysis/ Analyte
Alkalinity, total
Sulfate
Conductivity
Hardness as CaCO3
Aluminum
Antimony
Arsenic
Barium
Beryllium
Cadmium
Calcium
Chromium
Cobalt
Copper
Iron
Lead
Magnesium
Manganese
Molybdenum
Nickel
Potassium
Selenium
Silver
Sodium
Thallium
Titanium
Vanadium
Zinc
pH
Solids, total dissolved
Temperature
Total Organic Carbon
Turbidity
Acetone
Benzene
mg/L
mg/L
umhos/cm
mg/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
mg/L
ug/L
ug/L
ug/L
ug/L
ug/L
mg/L
ug/L
ug/L
ug/L
mg/L
ug/L
ug/L
mg/L
ug/L
ug/L
ug/L
ug/L
SU
mg/L
Deg C
mg/L
NTU
ug/L
ug/L
Units 8-__ 9-__ 10-__ 10-FD
234 314 352 351
10000 U 10000 U 10000 U 10000 U
5946 6590 6850 6850
13200 U 13200 U 13200 U 13200 U
50000 U 50000 U 50000 U 50000 U
50000 U 50000 U 50000 U 50000 U
25000 U 25000 U 25000 U 25000 U
10000 U 10000 U 10000 U 10000 U
3000 U 3000 U 3000 U 3000 U
3000 U 3000 U 3000 U 3000 U
2000 U 2000 U 2000 U 2000 U
15000 U 15000 U 15000 U 15000 U
10000 U 10000 U 10000 U 10000 U
5000 U 5000 U 5000 U 5000 U
50000 U 50000 U 50000 U 50000 U
50000 U 50000 U 50000 U 50000 U
2000 U 2000 U 2000 U 2000 U
368000 422000 356000 311000
15000 U 15000 U 15000 U 15000 U
20000 U 20000 U 20000 U 20000 U
2000 U 2000 U 2000 U 2000 U
50000 U 50000 U 50000 U 50000 U
25000 U 25000 U 25000 U 25000 U
5000 U 5000 U 5000 U 5000 U
50000 U 50000 U 50000 U 50000 U
20000 U 20000 U 20000 U 20000 U
10000 U 10000 U 10000 U 10000 U
25000 U 25000 U 25000 U 25000 U
6.26 7.06 5.92 5.92
6940 8280 7270 7300
13.52 14.04 12.07 12.07
15.2 13.4 12.2 12.2
2.1 0.0 37.4 37.4
25000 U 25000 U 25000 U 25000 U
25000 U 25000 U 25000 U 25000 U
4758ASR Number: 03/02/2010
MP7ES02Project ID: Cleburn Street well samplingProject Desc:
RLAB Approved Sample Analysis Results
Page 17 of 48
Analysis/ Analyte
Bromodichloromethane
Bromoform
Bromomethane
2-Butanone
Carbon Disulfide
Carbon Tetrachloride
Chlorobenzene
Chloroethane
Chloroform
Chloromethane
Cyclohexane
1,2-Dibromo-3-Chloropropane
Dibromochloromethane
1,2-Dibromoethane
1,2-Dichlorobenzene
1,3-Dichlorobenzene
1,4-Dichlorobenzene
Dichlorodifluoromethane
1,1-Dichloroethane
1,2-Dichloroethane
1,1-Dichloroethene
cis-1,2-Dichloroethene
trans-1,2-Dichloroethene
1,2-Dichloropropane
cis-1,3-Dichloropropene
trans-1,3-Dichloropropene
Ethyl Benzene
2-Hexanone
Isopropylbenzene
Methyl Acetate
Methyl tert-butyl ether
Methylcyclohexane
Methylene Chloride
4-Methyl-2-Pentanone
Naphthalene
Styrene
1,1,2,2-Tetrachloroethane
Tetrachloroethene
Toluene
1,2,3-Trichlorobenzene
1,2,4-Trichlorobenzene
1,1,1-Trichloroethane
1,1,2-Trichloroethane
Trichloroethene
Trichlorofluoromethane
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
Units 8-__ 9-__ 10-__ 10-FD
25000 U 25000 U 25000 U 25000 U
25000 U 25000 U 25000 U 25000 U
25000 U 25000 U 25000 U 25000 U
25000 U 25000 U 25000 U 25000 U
25000 U 25000 U 25000 U 25000 U
25000 U 25000 U 25000 U 25000 U
25000 U 25000 U 25000 U 25000 U
25000 U 25000 U 25000 U 25000 U
25000 U 25000 U 25000 U 25000 U
25000 U 25000 U 25000 U 25000 U
25000 U 25000 U 25000 U 25000 U
25000 U 25000 U 25000 U 25000 U
25000 U 25000 U 25000 U 25000 U
25000 U 25000 U 25000 U 25000 U
25000 U 25000 U 25000 U 25000 U
25000 U 25000 U 25000 U 25000 U
25000 U 25000 U 25000 U 25000 U
25000 U 25000 U 25000 U 25000 U
25000 U 25000 U 25000 U 25000 U
25000 U 25000 U 25000 U 25000 U
25000 U 25000 U 25000 U 25000 U
25000 U 25000 U 25000 U 25000 U
25000 U 25000 U 25000 U 25000 U
25000 U 25000 U 25000 U 25000 U
25000 U 25000 U 25000 U 25000 U
25000 U 25000 U 25000 U 25000 U
25000 U 25000 U 25000 U 25000 U
25000 U 25000 U 25000 U 25000 U
25000 U 25000 U 25000 U 25000 U
25000 U 25000 U 25000 U 25000 U
50000 U 50000 U 50000 U 50000 U
25000 U 25000 U 25000 U 25000 U
25000 U 25000 U 25000 U 25000 U
25000 U 25000 U 25000 U 25000 U
50000 U 50000 U 50000 U 50000 U
25000 U 25000 U 25000 U 25000 U
25000 U 25000 U 25000 U 25000 U
25000 U 25000 U 25000 U 25000 U
25000 U 25000 U 25000 U 25000 U
25000 U 25000 U 25000 U 25000 U
25000 U 25000 U 25000 U 25000 U
25000 U 25000 U 25000 U 25000 U
25000 U 25000 U 25000 U 25000 U
25000 U 25000 U 25000 U 25000 U
25000 U 25000 U 25000 U 25000 U
4758ASR Number: 03/02/2010
MP7ES02Project ID: Cleburn Street well samplingProject Desc:
RLAB Approved Sample Analysis Results
Page 18 of 48
Analysis/ Analyte
1,1,2-Trichlorotrifluoroethane
Vinyl Chloride
m and/or p-Xylene
o-Xylene
ug/L
ug/L
ug/L
ug/L
Units 8-__ 9-__ 10-__ 10-FD
25000 U 25000 U 25000 U 25000 U
25000 U 25000 U 25000 U 25000 U
50000 U 50000 U 50000 U 50000 U
25000 U 25000 U 25000 U 25000 U
4758ASR Number: 03/02/2010
MP7ES02Project ID: Cleburn Street well samplingProject Desc:
RLAB Approved Sample Analysis Results
Page 19 of 48
1
1
1
1
1
1
1
1
1
1
1
Alkalinity in Water by Titration
Anions in Water by Ion Chromatography
Conductivity by Field Measurement
Hardness in Water by Calculation
Metals in Water by ICP-AES
pH of Water by Field Measurement
TDS or Total Dissolved Solids
Temperature of Water by Field Measurement
Total Organic Carbon in Water
Turbidity of Water by Field Measurement
VOCs in Water by GC/MS
Analysis/ Analyte
Alkalinity, total
Sulfate
Conductivity
Hardness as CaCO3
Aluminum
Antimony
Arsenic
Barium
Beryllium
Cadmium
Calcium
Chromium
Cobalt
Copper
Iron
Lead
Magnesium
Manganese
Molybdenum
Nickel
Potassium
Selenium
Silver
Sodium
Thallium
Titanium
Vanadium
Zinc
pH
Solids, total dissolved
Temperature
Total Organic Carbon
Turbidity
Acetone
Benzene
mg/L
mg/L
umhos/cm
mg/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
mg/L
ug/L
ug/L
ug/L
ug/L
ug/L
mg/L
ug/L
ug/L
ug/L
mg/L
ug/L
ug/L
mg/L
ug/L
ug/L
ug/L
ug/L
SU
mg/L
Deg C
mg/L
NTU
ug/L
ug/L
Units 11-__ 12-__ 13-__ 14-__
186 143 134 81.0
10000 U 32.9 1000 U 119
8930 411 1990 1010
13200 U 161 3070 132 U
50000 U 500 UJ 5000 U 500 U
50000 U 500 UJ 5000 U 500 U
25000 U 250 UJ 2500 U 250 U
10000 U 366 J 3290 100 U
3000 U 30 UJ 300 U 30 U
3000 U 30 UJ 300 U 30 U
2000 U 64.6 J 898 20 U
15000 U 150 UJ 1500 U 150 U
10000 U 100 UJ 1000 U 100 U
5000 U 50 UJ 500 U 50 U
50000 U 500 UJ 5000 U 500 U
50000 U 500 UJ 5000 U 500 U
2000 U 20 UJ 202 20 U
380000 7 13400 499
15000 U 150 UJ 1500 U 150 U
20000 U 200 UJ 2000 U 200 U
2000 U 20 UJ 200 U 20 U
50000 U 500 UJ 5000 U 500 U
25000 U 250 UJ 2500 U 250 U
5000 U 50 UJ 1150 50 U
50000 U 500 UJ 5000 U 500 U
20000 U 200 UJ 2000 U 200 U
10000 U 100 UJ 1000 U 100 U
25000 U 250 UJ 2500 U 250 U
5.67 6.84 6.21 6.61
9880 296 1670 715
12.35 13.88 14.61 12.44
15.2 1 U 7.1 2.8
12.7 3.1 92.8 2.6
25000 U 5.0 UJ 25000 U 5.0 UJ
25000 U 5.0 U 25000 U 5.0 U
4758ASR Number: 03/02/2010
MP7ES02Project ID: Cleburn Street well samplingProject Desc:
RLAB Approved Sample Analysis Results
Page 20 of 48
Analysis/ Analyte
Bromodichloromethane
Bromoform
Bromomethane
2-Butanone
Carbon Disulfide
Carbon Tetrachloride
Chlorobenzene
Chloroethane
Chloroform
Chloromethane
Cyclohexane
1,2-Dibromo-3-Chloropropane
Dibromochloromethane
1,2-Dibromoethane
1,2-Dichlorobenzene
1,3-Dichlorobenzene
1,4-Dichlorobenzene
Dichlorodifluoromethane
1,1-Dichloroethane
1,2-Dichloroethane
1,1-Dichloroethene
cis-1,2-Dichloroethene
trans-1,2-Dichloroethene
1,2-Dichloropropane
cis-1,3-Dichloropropene
trans-1,3-Dichloropropene
Ethyl Benzene
2-Hexanone
Isopropylbenzene
Methyl Acetate
Methyl tert-butyl ether
Methylcyclohexane
Methylene Chloride
4-Methyl-2-Pentanone
Naphthalene
Styrene
1,1,2,2-Tetrachloroethane
Tetrachloroethene
Toluene
1,2,3-Trichlorobenzene
1,2,4-Trichlorobenzene
1,1,1-Trichloroethane
1,1,2-Trichloroethane
Trichloroethene
Trichlorofluoromethane
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
Units 11-__ 12-__ 13-__ 14-__
25000 U 5.0 U 25000 U 5.0 U
25000 U 5.0 U 25000 U 5.0 U
25000 U 5.0 U 25000 U 5.0 U
25000 U 5.0 U 25000 U 5.0 U
25000 U 5.0 U 25000 U 5.0 U
25000 U 5.0 U 25000 U 5.0 U
25000 U 5.0 U 25000 U 5.0 U
25000 U 5.0 U 25000 U 5.0 U
25000 U 5.0 U 25000 U 5.0 U
25000 U 5.0 U 25000 U 5.0 U
25000 U 5.0 U 25000 U 10
25000 U 5.0 U 25000 U 5.0 U
25000 U 5.0 U 25000 U 5.0 U
25000 U 5.0 U 25000 U 5.0 U
25000 U 5.0 U 25000 U 5.0 U
25000 U 5.0 U 25000 U 5.0 U
25000 U 5.0 U 25000 U 5.0 U
25000 U 5.0 U 25000 U 5.0 U
25000 U 5.0 U 25000 U 5.0 U
25000 U 5.0 U 25000 U 5.0 U
25000 U 5.0 U 25000 U 5.0 U
25000 U 5.0 U 25000 U 21
25000 U 5.0 U 25000 U 5.0 U
25000 U 5.0 U 25000 U 5.0 U
25000 U 5.0 U 25000 U 5.0 U
25000 U 5.0 U 25000 U 5.0 U
25000 U 5.0 U 25000 U 9.8
25000 U 5.0 U 25000 U 5.0 U
25000 U 5.0 U 25000 U 6.1
25000 U 5.0 U 25000 U 5.0 U
50000 U 10 U 50000 U 10 U
25000 U 5.0 U 25000 U 5.0 U
25000 U 5.0 U 25000 U 5.0 U
25000 U 5.0 U 25000 U 5.0 U
50000 U 10 U 50000 U 17
25000 U 5.0 U 25000 U 5.0 U
25000 U 5.0 U 25000 U 5.0 U
25000 U 5.0 U 25000 U 2600
25000 U 5.0 U 25000 U 6.4
25000 U 5.0 U 25000 U 5.0 U
25000 U 5.0 U 25000 U 5.0 U
25000 U 5.0 U 25000 U 5.0 U
25000 U 5.0 U 25000 U 5.0 U
25000 U 5.0 U 25000 U 220
25000 U 5.0 U 25000 U 5.0 U
4758ASR Number: 03/02/2010
MP7ES02Project ID: Cleburn Street well samplingProject Desc:
RLAB Approved Sample Analysis Results
Page 21 of 48
Analysis/ Analyte
1,1,2-Trichlorotrifluoroethane
Vinyl Chloride
m and/or p-Xylene
o-Xylene
ug/L
ug/L
ug/L
ug/L
Units 11-__ 12-__ 13-__ 14-__
25000 U 5.0 U 25000 U 5.0 U
25000 U 5.0 U 25000 U 5.0 U
50000 U 10 U 50000 U 29
25000 U 5.0 U 25000 U 10
4758ASR Number: 03/02/2010
MP7ES02Project ID: Cleburn Street well samplingProject Desc:
RLAB Approved Sample Analysis Results
Page 22 of 48
1
1
1
1
1
1
1
1
1
1
1
Alkalinity in Water by Titration
Anions in Water by Ion Chromatography
Conductivity by Field Measurement
Hardness in Water by Calculation
Metals in Water by ICP-AES
pH of Water by Field Measurement
TDS or Total Dissolved Solids
Temperature of Water by Field Measurement
Total Organic Carbon in Water
Turbidity of Water by Field Measurement
VOCs in Water by GC/MS
Analysis/ Analyte
Alkalinity, total
Sulfate
Conductivity
Hardness as CaCO3
Aluminum
Antimony
Arsenic
Barium
Beryllium
Cadmium
Calcium
Chromium
Cobalt
Copper
Iron
Lead
Magnesium
Manganese
Molybdenum
Nickel
Potassium
Selenium
Silver
Sodium
Thallium
Titanium
Vanadium
Zinc
pH
Solids, total dissolved
Temperature
Total Organic Carbon
Turbidity
Acetone
Benzene
mg/L
mg/L
umhos/cm
mg/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
mg/L
ug/L
ug/L
ug/L
ug/L
ug/L
mg/L
ug/L
ug/L
ug/L
mg/L
ug/L
ug/L
mg/L
ug/L
ug/L
ug/L
ug/L
SU
mg/L
Deg C
mg/L
NTU
ug/L
ug/L
Units 15-__ 16-__ 17-__ 18-__
40.6 109 423 251
168 1000 U 10000 U 10000 U
1240 1040 5050 4770
319 13200 U 13200 U 13200 U
500 U 50000 U 50000 U 50000 U
500 U 50000 U 50000 U 50000 U
250 U 25000 U 25000 U 25000 U
156 10000 U 10000 U 10000 U
30 U 3000 U 3000 U 3000 U
30 U 3000 U 3000 U 3000 U
90.1 2000 U 2000 U 2000 U
150 U 15000 U 15000 U 15000 U
100 U 10000 U 10000 U 10000 U
50 UJ 5000 U 5000 U 5000 U
500 U 50000 U 50000 U 50000 U
500 U 50000 U 50000 U 50000 U
22.9 2000 U 2000 U 2000 U
50 U 316000 127000 309000
150 U 15000 U 15000 U 15000 U
250 J 20000 U 20000 U 20000 U
20 U 2000 U 2000 U 2000 U
500 U 50000 U 50000 U 50000 U
250 U 25000 U 25000 U 25000 U
77.0 5000 U 5000 U 5000 U
500 UJ 50000 U 50000 U 50000 U
200 U 20000 U 20000 U 20000 U
100 U 10000 U 10000 U 10000 U
250 UJ 25000 U 25000 U 25000 U
6.43 6.54 6.59 7.41
805 801 5490 6030
16.71 16.66 11.93 13.45
2 4.1 17.6
2.0 0.0 65.1 32.3
5.0 U 25000 U 25000 U 25000 U
5.0 U 25000 U 25000 U 25000 U
4758ASR Number: 03/02/2010
MP7ES02Project ID: Cleburn Street well samplingProject Desc:
RLAB Approved Sample Analysis Results
Page 23 of 48
Analysis/ Analyte
Bromodichloromethane
Bromoform
Bromomethane
2-Butanone
Carbon Disulfide
Carbon Tetrachloride
Chlorobenzene
Chloroethane
Chloroform
Chloromethane
Cyclohexane
1,2-Dibromo-3-Chloropropane
Dibromochloromethane
1,2-Dibromoethane
1,2-Dichlorobenzene
1,3-Dichlorobenzene
1,4-Dichlorobenzene
Dichlorodifluoromethane
1,1-Dichloroethane
1,2-Dichloroethane
1,1-Dichloroethene
cis-1,2-Dichloroethene
trans-1,2-Dichloroethene
1,2-Dichloropropane
cis-1,3-Dichloropropene
trans-1,3-Dichloropropene
Ethyl Benzene
2-Hexanone
Isopropylbenzene
Methyl Acetate
Methyl tert-butyl ether
Methylcyclohexane
Methylene Chloride
4-Methyl-2-Pentanone
Naphthalene
Styrene
1,1,2,2-Tetrachloroethane
Tetrachloroethene
Toluene
1,2,3-Trichlorobenzene
1,2,4-Trichlorobenzene
1,1,1-Trichloroethane
1,1,2-Trichloroethane
Trichloroethene
Trichlorofluoromethane
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
Units 15-__ 16-__ 17-__ 18-__
5.0 U 25000 U 25000 U 25000 U
5.0 U 25000 U 25000 U 25000 U
5.0 U 25000 U 25000 U 25000 U
5.0 U 25000 U 25000 U 25000 U
5.0 U 25000 U 25000 U 25000 U
5.0 U 25000 U 25000 U 25000 U
5.0 U 25000 U 25000 U 25000 U
5.0 U 25000 U 25000 U 25000 U
5.0 U 25000 U 25000 U 25000 U
5.0 U 25000 U 25000 U 25000 U
5.0 U 25000 U 25000 U 25000 U
5.0 U 25000 U 25000 U 25000 U
5.0 U 25000 U 25000 U 25000 U
5.0 U 25000 U 25000 U 25000 U
5.0 U 25000 U 25000 U 25000 U
5.0 U 25000 U 25000 U 25000 U
5.0 U 25000 U 25000 U 25000 U
5.0 U 25000 U 25000 U 25000 U
5.0 U 25000 U 25000 U 25000 U
5.0 U 25000 U 25000 U 25000 U
5.0 U 25000 U 25000 U 25000 U
5.0 U 25000 U 25000 U 25000 U
5.0 U 25000 U 25000 U 25000 U
5.0 U 25000 U 25000 U 25000 U
5.0 U 25000 U 25000 U 25000 U
5.0 U 25000 U 25000 U 25000 U
5.0 U 25000 U 25000 U 25000 U
5.0 U 25000 U 25000 U 25000 U
5.0 U 25000 U 25000 U 25000 U
5.0 U 25000 U 25000 U 25000 U
10 U 50000 U 50000 U 50000 U
5.0 U 25000 U 25000 U 25000 U
5.0 U 25000 U 25000 U 25000 U
5.0 U 25000 U 25000 U 25000 U
10 U 50000 U 50000 U 50000 U
5.0 U 25000 U 25000 U 25000 U
5.0 U 25000 U 25000 U 25000 U
12 25000 U 25000 U 25000 U
5.0 U 25000 U 25000 U 25000 U
5.0 U 25000 U 25000 U 25000 U
5.0 U 25000 U 25000 U 25000 U
5.0 U 25000 U 25000 U 25000 U
5.0 U 25000 U 25000 U 25000 U
5.0 U 25000 U 25000 U 25000 U
5.0 U 25000 U 25000 U 25000 U
4758ASR Number: 03/02/2010
MP7ES02Project ID: Cleburn Street well samplingProject Desc:
RLAB Approved Sample Analysis Results
Page 24 of 48
Analysis/ Analyte
1,1,2-Trichlorotrifluoroethane
Vinyl Chloride
m and/or p-Xylene
o-Xylene
ug/L
ug/L
ug/L
ug/L
Units 15-__ 16-__ 17-__ 18-__
5.0 U 25000 U 25000 U 25000 U
5.0 U 25000 U 25000 U 25000 U
10 U 50000 U 50000 U 50000 U
5.0 U 25000 U 25000 U 25000 U
4758ASR Number: 03/02/2010
MP7ES02Project ID: Cleburn Street well samplingProject Desc:
RLAB Approved Sample Analysis Results
Page 25 of 48
1
1
1
1
1
1
1
1
1
1
1
Alkalinity in Water by Titration
Anions in Water by Ion Chromatography
Conductivity by Field Measurement
Hardness in Water by Calculation
Metals in Water by ICP-AES
pH of Water by Field Measurement
TDS or Total Dissolved Solids
Temperature of Water by Field Measurement
Total Organic Carbon in Water
Turbidity of Water by Field Measurement
VOCs in Water by GC/MS
Analysis/ Analyte
Alkalinity, total
Sulfate
Conductivity
Hardness as CaCO3
Aluminum
Antimony
Arsenic
Barium
Beryllium
Cadmium
Calcium
Chromium
Cobalt
Copper
Iron
Lead
Magnesium
Manganese
Molybdenum
Nickel
Potassium
Selenium
Silver
Sodium
Thallium
Titanium
Vanadium
Zinc
pH
Solids, total dissolved
Temperature
Total Organic Carbon
Turbidity
Acetone
Benzene
mg/L
mg/L
umhos/cm
mg/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
mg/L
ug/L
ug/L
ug/L
ug/L
ug/L
mg/L
ug/L
ug/L
ug/L
mg/L
ug/L
ug/L
mg/L
ug/L
ug/L
ug/L
ug/L
SU
mg/L
Deg C
mg/L
NTU
ug/L
ug/L
Units 18-FD 19-__ 20-FB 21-__
252 302 2.00 U
10000 U 10000 U 1.0 U
4770 7920 629
13200 U 13200 U 13.2 U
50000 U 50000 U 50 U
50000 U 50000 U 50 U
25000 U 25000 U 25 U
10000 U 10000 U 10 U
3000 U 3000 U 3 U
3000 U 3000 U 3 U
2000 U 2000 U 2 U
15000 U 15000 U 15 U
10000 U 10000 U 10 U
5000 U 5000 U 5 U
50000 U 50000 U 50 U
50000 U 50000 U 50 U
2000 U 2000 U 2 U
163000 278000 5 U
15000 U 15000 U 15 U
20000 U 20000 U 37.2 U
2000 U 2000 U 2 U
50000 U 50000 U 50 U
25000 U 25000 U 25 U
5000 U 5000 U 5 U
50000 U 50000 U 50 U
20000 U 20000 U 20 U
10000 U 10000 U 10 U
25000 U 25000 U 25 U
7.41 6.51 6.60
6000 8610 2 U
13.45 11.95 11.39
1 U
32.3 53.6 4.1
25000 U 25000 U 5.0 UJ 5.0 UJ
25000 U 25000 U 5.0 U 5.0 U
4758ASR Number: 03/02/2010
MP7ES02Project ID: Cleburn Street well samplingProject Desc:
RLAB Approved Sample Analysis Results
Page 26 of 48
Analysis/ Analyte
Bromodichloromethane
Bromoform
Bromomethane
2-Butanone
Carbon Disulfide
Carbon Tetrachloride
Chlorobenzene
Chloroethane
Chloroform
Chloromethane
Cyclohexane
1,2-Dibromo-3-Chloropropane
Dibromochloromethane
1,2-Dibromoethane
1,2-Dichlorobenzene
1,3-Dichlorobenzene
1,4-Dichlorobenzene
Dichlorodifluoromethane
1,1-Dichloroethane
1,2-Dichloroethane
1,1-Dichloroethene
cis-1,2-Dichloroethene
trans-1,2-Dichloroethene
1,2-Dichloropropane
cis-1,3-Dichloropropene
trans-1,3-Dichloropropene
Ethyl Benzene
2-Hexanone
Isopropylbenzene
Methyl Acetate
Methyl tert-butyl ether
Methylcyclohexane
Methylene Chloride
4-Methyl-2-Pentanone
Naphthalene
Styrene
1,1,2,2-Tetrachloroethane
Tetrachloroethene
Toluene
1,2,3-Trichlorobenzene
1,2,4-Trichlorobenzene
1,1,1-Trichloroethane
1,1,2-Trichloroethane
Trichloroethene
Trichlorofluoromethane
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
Units 18-FD 19-__ 20-FB 21-__
25000 U 25000 U 5.0 U 5.0 U
25000 U 25000 U 5.0 U 5.0 U
25000 U 25000 U 5.0 U 5.0 U
25000 U 25000 U 5.0 U 5.0 U
25000 U 25000 U 5.0 U 5.0 U
25000 U 25000 U 5.0 U 5.0 U
25000 U 25000 U 5.0 U 5.0 U
25000 U 25000 U 5.0 U 5.0 U
25000 U 25000 U 5.0 U 5.0 U
25000 U 25000 U 5.0 U 5.0 U
25000 U 25000 U 5.0 U 5.0 U
25000 U 25000 U 5.0 U 5.0 U
25000 U 25000 U 5.0 U 5.0 U
25000 U 25000 U 5.0 U 5.0 U
25000 U 25000 U 5.0 U 5.0 U
25000 U 25000 U 5.0 U 5.0 U
25000 U 25000 U 5.0 U 5.0 U
25000 U 25000 U 5.0 U 5.0 U
25000 U 25000 U 5.0 U 5.0 U
25000 U 25000 U 5.0 U 5.0 U
25000 U 25000 U 5.0 U 5.0 U
25000 U 25000 U 5.0 U 5.0 U
25000 U 25000 U 5.0 U 5.0 U
25000 U 25000 U 5.0 U 5.0 U
25000 U 25000 U 5.0 U 5.0 U
25000 U 25000 U 5.0 U 5.0 U
25000 U 25000 U 5.0 U 5.0 U
25000 U 25000 U 5.0 U 5.0 U
25000 U 25000 U 5.0 U 5.0 U
25000 U 25000 U 5.0 U 5.0 U
50000 U 50000 U 10 U 10 U
25000 U 25000 U 5.0 U 5.0 U
25000 U 25000 U 5.0 U 5.0 U
25000 U 25000 U 5.0 U 5.0 U
50000 U 50000 U 10 U 10 U
25000 U 25000 U 5.0 U 5.0 U
25000 U 25000 U 5.0 U 5.0 U
25000 U 25000 U 5.0 U 5.0 U
25000 U 25000 U 5.0 U 5.0 U
25000 U 25000 U 5.0 U 5.0 U
25000 U 25000 U 5.0 U 5.0 U
25000 U 25000 U 5.0 U 5.0 U
25000 U 25000 U 5.0 U 5.0 U
25000 U 25000 U 5.0 U 5.0 U
25000 U 25000 U 5.0 U 5.0 U
4758ASR Number: 03/02/2010
MP7ES02Project ID: Cleburn Street well samplingProject Desc:
RLAB Approved Sample Analysis Results
Page 27 of 48
Analysis/ Analyte
1,1,2-Trichlorotrifluoroethane
Vinyl Chloride
m and/or p-Xylene
o-Xylene
ug/L
ug/L
ug/L
ug/L
Units 18-FD 19-__ 20-FB 21-__
25000 U 25000 U 5.0 U 5.0 U
25000 U 25000 U 5.0 U 5.0 U
50000 U 50000 U 10 U 10 U
25000 U 25000 U 5.0 U 5.0 U
4758ASR Number: 03/02/2010
MP7ES02Project ID: Cleburn Street well samplingProject Desc:
RLAB Approved Sample Analysis Results
Page 28 of 48
1
1
1
1
1
Conductivity by Field Measurement
pH of Water by Field Measurement
Temperature of Water by Field Measurement
Turbidity of Water by Field Measurement
VOCs in Water by GC/MS
Analysis/ Analyte
Conductivity
pH
Temperature
Turbidity
Acetone
Benzene
Bromodichloromethane
Bromoform
Bromomethane
2-Butanone
Carbon Disulfide
Carbon Tetrachloride
Chlorobenzene
Chloroethane
Chloroform
Chloromethane
Cyclohexane
1,2-Dibromo-3-Chloropropane
Dibromochloromethane
1,2-Dibromoethane
1,2-Dichlorobenzene
1,3-Dichlorobenzene
1,4-Dichlorobenzene
Dichlorodifluoromethane
1,1-Dichloroethane
1,2-Dichloroethane
1,1-Dichloroethene
cis-1,2-Dichloroethene
trans-1,2-Dichloroethene
1,2-Dichloropropane
cis-1,3-Dichloropropene
trans-1,3-Dichloropropene
Ethyl Benzene
2-Hexanone
Isopropylbenzene
Methyl Acetate
Methyl tert-butyl ether
Methylcyclohexane
Methylene Chloride
4-Methyl-2-Pentanone
Naphthalene
umhos/cm
SU
Deg C
NTU
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
Units 21-FD 23-__ 24-__ 25-__
629 319 773 1930
6.60 7.18 6.85 6.68
11.39 10.80 12.52 12.01
4.1 3.4 1.7 0.0
5.0 UJ 5.0 UJ 5.0 UJ 5.0 UJ
5.0 U 5.0 U 5.0 U 5.0 U
5.0 U 5.0 U 5.0 U 5.0 U
5.0 U 5.0 U 5.0 U 5.0 U
5.0 U 5.0 U 5.0 U 5.0 U
5.0 U 5.0 U 5.0 U 5.0 U
5.0 U 5.0 U 5.0 U 5.0 U
5.0 U 5.0 U 5.0 U 5.0 U
5.0 U 5.0 U 5.0 U 5.0 U
5.0 U 5.0 U 5.0 U 5.0 U
5.0 U 5.0 U 5.0 U 5.0 U
5.0 U 5.0 U 5.0 U 5.0 U
5.0 U 5.0 U 5.0 U 5.0 U
5.0 U 5.0 U 5.0 U 5.0 U
5.0 U 5.0 U 5.0 U 5.0 U
5.0 U 5.0 U 5.0 U 5.0 U
5.0 U 5.0 U 5.0 U 5.0 U
5.0 U 5.0 U 5.0 U 5.0 U
5.0 U 5.0 U 5.0 U 5.0 U
5.0 U 5.0 U 5.0 U 5.0 U
5.0 U 5.0 U 5.0 U 5.0 U
5.0 U 5.0 U 5.0 U 5.0 U
5.0 U 5.0 U 5.0 U 5.0 U
5.0 U 5.0 U 5.0 U 5.0 U
5.0 U 5.0 U 5.0 U 5.0 U
5.0 U 5.0 U 5.0 U 5.0 U
5.0 U 5.0 U 5.0 U 5.0 U
5.0 U 5.0 U 5.0 U 5.0 U
5.0 U 5.0 U 5.0 U 5.0 U
5.0 U 5.0 U 5.0 U 5.0 U
5.0 U 5.0 U 5.0 U 5.0 U
5.0 U 5.0 U 5.0 U 5.0 U
10 U 10 U 10 U 10 U
5.0 U 5.0 U 5.0 U 5.0 U
5.0 U 5.0 U 5.0 U 5.0 U
5.0 U 5.0 U 5.0 U 5.0 U
10 U 10 U 10 U 10 U
4758ASR Number: 03/02/2010
MP7ES02Project ID: Cleburn Street well samplingProject Desc:
RLAB Approved Sample Analysis Results
Page 29 of 48
Analysis/ Analyte
Styrene
1,1,2,2-Tetrachloroethane
Tetrachloroethene
Toluene
1,2,3-Trichlorobenzene
1,2,4-Trichlorobenzene
1,1,1-Trichloroethane
1,1,2-Trichloroethane
Trichloroethene
Trichlorofluoromethane
1,1,2-Trichlorotrifluoroethane
Vinyl Chloride
m and/or p-Xylene
o-Xylene
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
Units 21-FD 23-__ 24-__ 25-__
5.0 U 5.0 U 5.0 U 5.0 U
5.0 U 5.0 U 5.0 U 5.0 U
5.0 U 5.0 U 5.0 U 5.0 U
5.0 U 5.0 U 5.0 U 5.0 U
5.0 U 5.0 U 5.0 U 5.0 U
5.0 U 5.0 U 5.0 U 5.0 U
5.0 U 5.0 U 5.0 U 5.0 U
5.0 U 5.0 U 5.0 U 5.0 U
5.0 U 5.0 U 5.0 U 5.0 U
5.0 U 5.0 U 5.0 U 5.0 U
5.0 U 5.0 U 5.0 U 5.0 U
5.0 U 5.0 U 5.0 U 5.0 U
10 U 10 U 10 U 10 U
5.0 U 5.0 U 5.0 U 5.0 U
4758ASR Number: 03/02/2010
MP7ES02Project ID: Cleburn Street well samplingProject Desc:
RLAB Approved Sample Analysis Results
Page 30 of 48
1
1
1
1
1
Conductivity by Field Measurement
pH of Water by Field Measurement
Temperature of Water by Field Measurement
Turbidity of Water by Field Measurement
VOCs in Water by GC/MS
Analysis/ Analyte
Conductivity
pH
Temperature
Turbidity
Acetone
Benzene
Bromodichloromethane
Bromoform
Bromomethane
2-Butanone
Carbon Disulfide
Carbon Tetrachloride
Chlorobenzene
Chloroethane
Chloroform
Chloromethane
Cyclohexane
1,2-Dibromo-3-Chloropropane
Dibromochloromethane
1,2-Dibromoethane
1,2-Dichlorobenzene
1,3-Dichlorobenzene
1,4-Dichlorobenzene
Dichlorodifluoromethane
1,1-Dichloroethane
1,2-Dichloroethane
1,1-Dichloroethene
cis-1,2-Dichloroethene
trans-1,2-Dichloroethene
1,2-Dichloropropane
cis-1,3-Dichloropropene
trans-1,3-Dichloropropene
Ethyl Benzene
2-Hexanone
Isopropylbenzene
Methyl Acetate
Methyl tert-butyl ether
Methylcyclohexane
Methylene Chloride
4-Methyl-2-Pentanone
Naphthalene
umhos/cm
SU
Deg C
NTU
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
Units 26-__ 27-__ 28-__ 29-__
8.06 427 734 475
6.60 6.90 6.67 6.58
12.18 12.66 12.73 13.07
3.8 2.8 1.3 3.7
5.0 UJ 5.0 UJ 5.0 UJ 5.0 UJ
5.0 U 5.0 U 5.0 U 5.0 U
5.0 U 5.0 U 5.0 U 5.0 U
5.0 U 5.0 U 5.0 U 5.0 U
5.0 U 5.0 U 5.0 U 5.0 U
5.0 U 5.0 U 5.0 U 5.0 U
5.0 U 5.0 U 5.0 U 5.0 U
5.0 U 5.0 U 5.0 U 5.0 U
5.0 U 5.0 U 5.0 U 5.0 U
5.0 U 5.0 U 5.0 U 5.0 U
5.0 U 5.0 U 5.0 U 5.0 U
5.0 U 5.0 U 5.0 U 5.0 U
5.0 U 5.0 U 5.0 U 5.0 U
5.0 U 5.0 U 5.0 U 5.0 U
5.0 U 5.0 U 5.0 U 5.0 U
5.0 U 5.0 U 5.0 U 5.0 U
5.0 U 5.0 U 5.0 U 5.0 U
5.0 U 5.0 U 5.0 U 5.0 U
5.0 U 5.0 U 5.0 U 5.0 U
5.0 U 5.0 U 5.0 U 5.0 U
5.0 U 5.0 U 5.0 U 5.0 U
5.0 U 5.0 U 5.0 U 5.0 U
5.0 U 5.0 U 5.0 U 5.0 U
5.0 U 5.0 U 5.0 U 5.0 U
5.0 U 5.0 U 5.0 U 5.0 U
5.0 U 5.0 U 5.0 U 5.0 U
5.0 U 5.0 U 5.0 U 5.0 U
5.0 U 5.0 U 5.0 U 5.0 U
5.0 U 5.0 U 5.0 U 5.0 U
5.0 U 5.0 U 5.0 U 5.0 U
5.0 U 5.0 U 5.0 U 5.0 U
5.0 U 5.0 U 5.0 U 5.0 U
10 U 10 U 10 U 10 U
5.0 U 5.0 U 5.0 U 5.0 U
5.0 U 5.0 U 5.0 U 5.0 U
5.0 U 5.0 U 5.0 U 5.0 U
10 U 10 U 10 U 10 U
4758ASR Number: 03/02/2010
MP7ES02Project ID: Cleburn Street well samplingProject Desc:
RLAB Approved Sample Analysis Results
Page 31 of 48
Analysis/ Analyte
Styrene
1,1,2,2-Tetrachloroethane
Tetrachloroethene
Toluene
1,2,3-Trichlorobenzene
1,2,4-Trichlorobenzene
1,1,1-Trichloroethane
1,1,2-Trichloroethane
Trichloroethene
Trichlorofluoromethane
1,1,2-Trichlorotrifluoroethane
Vinyl Chloride
m and/or p-Xylene
o-Xylene
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
Units 26-__ 27-__ 28-__ 29-__
5.0 U 5.0 U 5.0 U 5.0 U
5.0 U 5.0 U 5.0 U 5.0 U
14 5.0 U 5.0 U 5.0 U
5.0 U 5.0 U 5.0 U 5.0 U
5.0 U 5.0 U 5.0 U 5.0 U
5.0 U 5.0 U 5.0 U 5.0 U
5.0 U 5.0 U 5.0 U 5.0 U
5.0 U 5.0 U 5.0 U 5.0 U
5.0 U 5.0 U 5.0 U 5.0 U
5.0 U 5.0 U 5.0 U 5.0 U
5.0 U 5.0 U 5.0 U 5.0 U
5.0 U 5.0 U 5.0 U 5.0 U
10 U 10 U 10 U 10 U
5.0 U 5.0 U 5.0 U 5.0 U
4758ASR Number: 03/02/2010
MP7ES02Project ID: Cleburn Street well samplingProject Desc:
RLAB Approved Sample Analysis Results
Page 32 of 48
1
1
1
1
1
Conductivity by Field Measurement
pH of Water by Field Measurement
Temperature of Water by Field Measurement
Turbidity of Water by Field Measurement
VOCs in Water by GC/MS
Analysis/ Analyte
Conductivity
pH
Temperature
Turbidity
Acetone
Benzene
Bromodichloromethane
Bromoform
Bromomethane
2-Butanone
Carbon Disulfide
Carbon Tetrachloride
Chlorobenzene
Chloroethane
Chloroform
Chloromethane
Cyclohexane
1,2-Dibromo-3-Chloropropane
Dibromochloromethane
1,2-Dibromoethane
1,2-Dichlorobenzene
1,3-Dichlorobenzene
1,4-Dichlorobenzene
Dichlorodifluoromethane
1,1-Dichloroethane
1,2-Dichloroethane
1,1-Dichloroethene
cis-1,2-Dichloroethene
trans-1,2-Dichloroethene
1,2-Dichloropropane
cis-1,3-Dichloropropene
trans-1,3-Dichloropropene
Ethyl Benzene
2-Hexanone
Isopropylbenzene
Methyl Acetate
Methyl tert-butyl ether
Methylcyclohexane
Methylene Chloride
4-Methyl-2-Pentanone
Naphthalene
umhos/cm
SU
Deg C
NTU
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
Units 30-__ 31-__ 32-__ 33-__
472 746
6.74 6.7
12.68 13.02
4.6 6.6
5.0 U 5.0 U 5.0 UJ 5.0 U
5.0 U 5.0 U 5.0 U 5.0 U
5.0 U 5.0 U 5.0 U 5.0 U
5.0 U 5.0 U 5.0 U 5.0 U
5.0 U 5.0 U 5.0 U 5.0 U
5.0 U 5.0 U 5.0 U 5.0 U
5.0 U 5.0 U 5.0 UJ 5.0 U
5.0 U 5.0 U 5.0 U 5.0 U
5.0 U 5.0 U 5.0 U 5.0 U
5.0 U 5.0 U 5.0 U 5.0 U
5.0 U 5.0 U 5.0 U 5.0 U
5.0 U 5.0 U 5.0 U 5.0 U
5.0 U 5.0 U 5.0 U 5.0 U
5.0 U 5.0 U 5.0 U 5.0 U
5.0 U 5.0 U 5.0 U 5.0 U
5.0 U 5.0 U 5.0 U 5.0 U
5.0 U 5.0 U 5.0 U 5.0 U
5.0 U 5.0 U 5.0 U 5.0 U
5.0 U 5.0 U 5.0 U 5.0 U
5.0 U 5.0 U 5.0 U 5.0 U
5.0 U 5.0 U 5.0 U 5.0 U
5.0 U 5.0 U 5.0 U 5.0 U
5.0 U 5.0 U 5.0 U 5.0 U
5.0 U 5.0 U 5.0 U 5.0 U
5.0 U 5.0 U 5.0 U 5.0 U
5.0 U 5.0 U 5.0 U 5.0 U
5.0 U 5.0 U 5.0 U 5.0 U
5.0 U 5.0 U 5.0 U 5.0 U
5.0 U 5.0 U 5.0 U 5.0 U
5.0 U 5.0 U 5.0 U 5.0 U
5.0 U 5.0 U 5.0 U 5.0 U
5.0 U 5.0 U 5.0 U 5.0 U
10 U 10 U 10 U 10 U
5.0 U 5.0 U 5.0 U 5.0 U
5.0 U 5.0 U 5.0 U 5.0 U
5.0 U 5.0 U 5.0 U 5.0 U
10 U 10 U 10 U 10 U
4758ASR Number: 03/02/2010
MP7ES02Project ID: Cleburn Street well samplingProject Desc:
RLAB Approved Sample Analysis Results
Page 33 of 48
Analysis/ Analyte
Styrene
1,1,2,2-Tetrachloroethane
Tetrachloroethene
Toluene
1,2,3-Trichlorobenzene
1,2,4-Trichlorobenzene
1,1,1-Trichloroethane
1,1,2-Trichloroethane
Trichloroethene
Trichlorofluoromethane
1,1,2-Trichlorotrifluoroethane
Vinyl Chloride
m and/or p-Xylene
o-Xylene
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
Units 30-__ 31-__ 32-__ 33-__
5.0 U 5.0 U 5.0 U 5.0 U
5.0 U 5.0 U 5.0 U 5.0 U
5.0 U 5.0 U 5.0 U 5.0 U
5.0 U 5.0 U 5.0 U 5.0 U
5.0 U 5.0 U 5.0 U 5.0 U
5.0 U 5.0 U 5.0 U 5.0 U
5.0 U 5.0 U 5.0 U 5.0 U
5.0 U 5.0 U 5.0 U 5.0 U
5.0 U 5.0 U 5.0 U 5.0 U
5.0 U 5.0 U 5.0 U 5.0 U
5.0 U 5.0 U 5.0 U 5.0 U
5.0 U 5.0 U 5.0 U 5.0 U
10 U 10 U 10 U 10 U
5.0 U 5.0 U 5.0 U 5.0 U
4758ASR Number: 03/02/2010
MP7ES02Project ID: Cleburn Street well samplingProject Desc:
RLAB Approved Sample Analysis Results
Page 34 of 48
1
1
1
1
1
Conductivity by Field Measurement
pH of Water by Field Measurement
Temperature of Water by Field Measurement
Turbidity of Water by Field Measurement
VOCs in Water by GC/MS
Analysis/ Analyte
Conductivity
pH
Temperature
Turbidity
Acetone
Benzene
Bromodichloromethane
Bromoform
Bromomethane
2-Butanone
Carbon Disulfide
Carbon Tetrachloride
Chlorobenzene
Chloroethane
Chloroform
Chloromethane
Cyclohexane
1,2-Dibromo-3-Chloropropane
Dibromochloromethane
1,2-Dibromoethane
1,2-Dichlorobenzene
1,3-Dichlorobenzene
1,4-Dichlorobenzene
Dichlorodifluoromethane
1,1-Dichloroethane
1,2-Dichloroethane
1,1-Dichloroethene
cis-1,2-Dichloroethene
trans-1,2-Dichloroethene
1,2-Dichloropropane
cis-1,3-Dichloropropene
trans-1,3-Dichloropropene
Ethyl Benzene
2-Hexanone
Isopropylbenzene
Methyl Acetate
Methyl tert-butyl ether
Methylcyclohexane
Methylene Chloride
4-Methyl-2-Pentanone
Naphthalene
umhos/cm
SU
Deg C
NTU
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
Units 34-__ 35-__ 35-FD 37-__
793 645 645 1860
6.73 6.58 6.58 6.52
14.96 14.34 14.34 14.85
1.1 2.7 2.7 4.6
5.0 U 5.0 U 5.0 U 5.0 U
5.0 U 5.0 U 5.0 U 5.0 U
5.0 U 5.0 U 5.0 U 5.0 U
5.0 U 5.0 U 5.0 U 5.0 U
5.0 U 5.0 U 5.0 U 5.0 U
5.0 U 5.0 U 5.0 U 5.0 U
5.0 U 5.0 U 5.0 U 5.0 U
5.0 U 5.0 U 5.0 U 5.0 U
5.0 U 5.0 U 5.0 U 5.0 U
5.0 U 5.0 U 5.0 U 5.0 U
5.0 U 5.0 U 5.0 U 5.0 U
5.0 U 5.0 U 5.0 U 5.0 U
5.0 U 5.0 U 5.0 U 5.0 U
5.0 U 5.0 U 5.0 U 5.0 U
5.0 U 5.0 U 5.0 U 5.0 U
5.0 U 5.0 U 5.0 U 5.0 U
5.0 U 5.0 U 5.0 U 5.0 U
5.0 U 5.0 U 5.0 U 5.0 U
5.0 U 5.0 U 5.0 U 5.0 U
5.0 U 5.0 U 5.0 U 5.0 U
5.0 U 5.0 U 5.0 U 5.0 U
5.0 U 5.0 U 5.0 U 5.0 U
5.0 U 5.0 U 5.0 U 5.0 U
5.0 U 5.0 U 5.0 U 5.0 U
5.0 U 5.0 U 5.0 U 5.0 U
5.0 U 5.0 U 5.0 U 5.0 U
5.0 U 5.0 U 5.0 U 5.0 U
5.0 U 5.0 U 5.0 U 5.0 U
5.0 U 5.0 U 5.0 U 5.0 U
5.0 U 5.0 U 5.0 U 5.0 U
5.0 U 5.0 U 5.0 U 5.0 U
5.0 U 5.0 U 5.0 U 5.0 U
10 U 10 U 10 U 10 U
5.0 U 5.0 U 5.0 U 5.0 U
5.0 U 5.0 U 5.0 U 5.0 U
5.0 U 5.0 U 5.0 U 5.0 U
10 U 10 U 10 U 10 U
4758ASR Number: 03/02/2010
MP7ES02Project ID: Cleburn Street well samplingProject Desc:
RLAB Approved Sample Analysis Results
Page 35 of 48
Analysis/ Analyte
Styrene
1,1,2,2-Tetrachloroethane
Tetrachloroethene
Toluene
1,2,3-Trichlorobenzene
1,2,4-Trichlorobenzene
1,1,1-Trichloroethane
1,1,2-Trichloroethane
Trichloroethene
Trichlorofluoromethane
1,1,2-Trichlorotrifluoroethane
Vinyl Chloride
m and/or p-Xylene
o-Xylene
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
Units 34-__ 35-__ 35-FD 37-__
5.0 U 5.0 U 5.0 U 5.0 U
5.0 U 5.0 U 5.0 U 5.0 U
5.0 U 5.0 U 5.0 U 13
5.0 U 5.0 U 5.0 U 5.0 U
5.0 U 5.0 U 5.0 U 5.0 U
5.0 U 5.0 U 5.0 U 5.0 U
5.0 U 5.0 U 5.0 U 5.0 U
5.0 U 5.0 U 5.0 U 5.0 U
5.0 U 5.0 U 5.0 U 5.0 U
5.0 U 5.0 U 5.0 U 5.0 U
5.0 U 5.0 U 5.0 U 5.0 U
5.0 U 5.0 U 5.0 U 5.0 U
10 U 10 U 10 U 10 U
5.0 U 5.0 U 5.0 U 5.0 U
4758ASR Number: 03/02/2010
MP7ES02Project ID: Cleburn Street well samplingProject Desc:
RLAB Approved Sample Analysis Results
Page 36 of 48
1
1
1
1
1
Conductivity by Field Measurement
pH of Water by Field Measurement
Temperature of Water by Field Measurement
Turbidity of Water by Field Measurement
VOCs in Water by GC/MS
Analysis/ Analyte
Conductivity
pH
Temperature
Turbidity
Acetone
Benzene
Bromodichloromethane
Bromoform
Bromomethane
2-Butanone
Carbon Disulfide
Carbon Tetrachloride
Chlorobenzene
Chloroethane
Chloroform
Chloromethane
Cyclohexane
1,2-Dibromo-3-Chloropropane
Dibromochloromethane
1,2-Dibromoethane
1,2-Dichlorobenzene
1,3-Dichlorobenzene
1,4-Dichlorobenzene
Dichlorodifluoromethane
1,1-Dichloroethane
1,2-Dichloroethane
1,1-Dichloroethene
cis-1,2-Dichloroethene
trans-1,2-Dichloroethene
1,2-Dichloropropane
cis-1,3-Dichloropropene
trans-1,3-Dichloropropene
Ethyl Benzene
2-Hexanone
Isopropylbenzene
Methyl Acetate
Methyl tert-butyl ether
Methylcyclohexane
Methylene Chloride
4-Methyl-2-Pentanone
Naphthalene
umhos/cm
SU
Deg C
NTU
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
Units 38-__ 39-__ 40-__ 41-__
654 658 907 426
6.54 6.42 6.23 6.74
14.06 12.76 13.36 12.27
1.5 0.0 1.8 3.3
5.0 U 5.0 U 5.0 U 5.0 U
5.0 U 5.0 U 5.0 U 5.0 U
5.0 U 5.0 U 5.0 U 5.0 U
5.0 U 5.0 U 5.0 U 5.0 U
5.0 U 5.0 U 5.0 U 5.0 U
5.0 U 5.0 U 5.0 U 5.0 U
5.0 U 5.0 U 5.0 U 5.0 U
5.0 U 5.0 U 5.0 U 5.0 U
5.0 U 5.0 U 5.0 U 5.0 U
5.0 U 5.0 U 5.0 U 5.0 U
5.0 U 5.0 U 5.0 U 5.0 U
5.0 U 5.0 U 5.0 U 5.0 U
5.0 U 5.0 U 5.0 U 5.0 U
5.0 U 5.0 U 5.0 U 5.0 U
5.0 U 5.0 U 5.0 U 5.0 U
5.0 U 5.0 U 5.0 U 5.0 U
5.0 U 5.0 U 5.0 U 5.0 U
5.0 U 5.0 U 5.0 U 5.0 U
5.0 U 5.0 U 5.0 U 5.0 U
5.0 U 5.0 U 5.0 U 5.0 U
5.0 U 5.0 U 5.0 U 5.0 U
5.0 U 5.0 U 5.0 U 5.0 U
5.0 U 5.0 U 5.0 U 5.0 U
5.0 U 5.0 U 5.0 U 5.0 U
5.0 U 5.0 U 5.0 U 5.0 U
5.0 U 5.0 U 5.0 U 5.0 U
5.0 U 5.0 U 5.0 U 5.0 U
5.0 U 5.0 U 5.0 U 5.0 U
5.0 U 5.0 U 5.0 U 5.0 U
5.0 U 5.0 U 5.0 U 5.0 U
5.0 U 5.0 U 5.0 U 5.0 U
5.0 U 5.0 U 5.0 U 5.0 U
10 U 10 U 10 U 10 U
5.0 U 5.0 U 5.0 U 5.0 U
5.0 U 5.0 U 5.0 U 5.0 U
5.0 U 5.0 U 5.0 U 5.0 U
10 U 10 U 10 U 10 U
4758ASR Number: 03/02/2010
MP7ES02Project ID: Cleburn Street well samplingProject Desc:
RLAB Approved Sample Analysis Results
Page 37 of 48
Analysis/ Analyte
Styrene
1,1,2,2-Tetrachloroethane
Tetrachloroethene
Toluene
1,2,3-Trichlorobenzene
1,2,4-Trichlorobenzene
1,1,1-Trichloroethane
1,1,2-Trichloroethane
Trichloroethene
Trichlorofluoromethane
1,1,2-Trichlorotrifluoroethane
Vinyl Chloride
m and/or p-Xylene
o-Xylene
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
Units 38-__ 39-__ 40-__ 41-__
5.0 U 5.0 U 5.0 U 5.0 UJ
5.0 U 5.0 U 5.0 U 5.0 U
5.0 U 5.0 U 5.0 U 5.0 U
5.0 U 5.0 U 5.0 U 5.0 U
5.0 U 5.0 U 5.0 U 5.0 U
5.0 U 5.0 U 5.0 U 5.0 U
5.0 U 5.0 U 5.0 U 5.0 U
5.0 U 5.0 U 5.0 U 5.0 U
5.0 U 5.0 U 5.0 U 5.0 U
5.0 U 5.0 U 5.0 U 5.0 U
5.0 U 5.0 U 5.0 U 5.0 U
5.0 U 5.0 U 5.0 U 5.0 U
10 U 10 U 10 U 10 U
5.0 U 5.0 U 5.0 U 5.0 U
4758ASR Number: 03/02/2010
MP7ES02Project ID: Cleburn Street well samplingProject Desc:
RLAB Approved Sample Analysis Results
Page 38 of 48
1
1
1
1
1
1
1
1
1
1
Alkalinity in Water by Titration
Anions in Water by Ion Chromatography
Conductivity by Field Measurement
Hardness in Water by Calculation
Metals in Water by ICP-AES
pH of Water by Field Measurement
TDS or Total Dissolved Solids
Temperature of Water by Field Measurement
Turbidity of Water by Field Measurement
VOCs in Water by GC/MS
Analysis/ Analyte
Alkalinity, total
Sulfate
Conductivity
Hardness as CaCO3
Aluminum
Antimony
Arsenic
Barium
Beryllium
Cadmium
Calcium
Chromium
Cobalt
Copper
Iron
Lead
Magnesium
Manganese
Molybdenum
Nickel
Potassium
Selenium
Silver
Sodium
Thallium
Titanium
Vanadium
Zinc
pH
Solids, total dissolved
Temperature
Turbidity
Acetone
Benzene
Bromodichloromethane
Bromoform
mg/L
mg/L
umhos/cm
mg/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
mg/L
ug/L
ug/L
ug/L
ug/L
ug/L
mg/L
ug/L
ug/L
ug/L
mg/L
ug/L
ug/L
mg/L
ug/L
ug/L
ug/L
ug/L
SU
mg/L
Deg C
NTU
ug/L
ug/L
ug/L
ug/L
Units 42-__ 43-__ 44-__ 45-__
343
10000 U
15.60 703 524 7680
13200 U
50000 U
50000 U
25000 U
10000 U
3000 U
3000 U
2000 U
15000 U
10000 U
5000 U
50000 U
50000 U
2000 U
353000
15000 U
21700
2000 U
50000 U
25000 U
5000 U
50000 U
20000 U
10000 U
25000 U
6.48 6.45 6.01 8.49
9920
13.05 12.07 14.50 11.77
2.1 0.0 0.0 52.5
25000 U 5.0 U 5.0 U 25000 U
25000 U 5.0 U 5.0 U 25000 U
25000 U 5.0 U 5.0 U 25000 U
25000 U 5.0 U 5.0 U 25000 U
4758ASR Number: 03/02/2010
MP7ES02Project ID: Cleburn Street well samplingProject Desc:
RLAB Approved Sample Analysis Results
Page 39 of 48
Analysis/ Analyte
Bromomethane
2-Butanone
Carbon Disulfide
Carbon Tetrachloride
Chlorobenzene
Chloroethane
Chloroform
Chloromethane
Cyclohexane
1,2-Dibromo-3-Chloropropane
Dibromochloromethane
1,2-Dibromoethane
1,2-Dichlorobenzene
1,3-Dichlorobenzene
1,4-Dichlorobenzene
Dichlorodifluoromethane
1,1-Dichloroethane
1,2-Dichloroethane
1,1-Dichloroethene
cis-1,2-Dichloroethene
trans-1,2-Dichloroethene
1,2-Dichloropropane
cis-1,3-Dichloropropene
trans-1,3-Dichloropropene
Ethyl Benzene
2-Hexanone
Isopropylbenzene
Methyl Acetate
Methyl tert-butyl ether
Methylcyclohexane
Methylene Chloride
4-Methyl-2-Pentanone
Naphthalene
Styrene
1,1,2,2-Tetrachloroethane
Tetrachloroethene
Toluene
1,2,3-Trichlorobenzene
1,2,4-Trichlorobenzene
1,1,1-Trichloroethane
1,1,2-Trichloroethane
Trichloroethene
Trichlorofluoromethane
1,1,2-Trichlorotrifluoroethane
Vinyl Chloride
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
Units 42-__ 43-__ 44-__ 45-__
25000 U 5.0 U 5.0 U 25000 U
25000 U 5.0 U 5.0 U 25000 U
25000 U 5.0 U 5.0 U 25000 U
25000 U 5.0 U 5.0 U 25000 U
25000 U 5.0 U 5.0 U 25000 U
25000 U 5.0 U 5.0 U 25000 U
25000 U 5.0 U 5.0 U 25000 U
25000 U 5.0 U 5.0 U 25000 U
25000 U 5.0 U 5.0 U 25000 U
25000 U 5.0 U 5.0 U 25000 U
25000 U 5.0 U 5.0 U 25000 U
25000 U 5.0 U 5.0 U 25000 U
25000 U 5.0 U 5.0 U 25000 U
25000 U 5.0 U 5.0 U 25000 U
25000 U 5.0 U 5.0 U 25000 U
25000 U 5.0 U 5.0 U 25000 U
25000 U 5.0 U 5.0 U 25000 U
25000 U 5.0 U 5.0 U 25000 U
25000 U 5.0 U 5.0 U 25000 U
25000 U 5.0 U 5.0 U 25000 U
25000 U 5.0 U 5.0 U 25000 U
25000 U 5.0 U 5.0 U 25000 U
25000 U 5.0 U 5.0 U 25000 U
25000 U 5.0 U 5.0 U 25000 U
25000 U 5.0 U 5.0 U 25000 U
25000 U 5.0 U 5.0 U 25000 U
25000 U 5.0 U 5.0 U 25000 U
25000 U 5.0 U 5.0 U 25000 U
50000 U 10 U 10 U 50000 U
25000 U 5.0 U 5.0 U 25000 U
25000 U 5.0 U 5.0 U 25000 U
25000 U 5.0 U 5.0 U 25000 U
50000 U 10 U 10 U 50000 U
25000 U 5.0 U 5.0 U 25000 U
25000 U 5.0 U 5.0 U 25000 U
25000 U 5.0 U 5.0 U 25000 U
25000 U 5.0 U 5.0 U 25000 U
25000 U 5.0 U 5.0 U 25000 U
25000 U 5.0 U 5.0 U 25000 U
25000 U 5.0 U 5.0 U 25000 U
25000 U 5.0 U 5.0 U 25000 U
25000 U 5.0 U 5.0 U 25000 U
25000 U 5.0 U 5.0 U 25000 U
25000 U 5.0 U 5.0 U 25000 U
25000 U 5.0 U 5.0 U 25000 U
4758ASR Number: 03/02/2010
MP7ES02Project ID: Cleburn Street well samplingProject Desc:
RLAB Approved Sample Analysis Results
Page 40 of 48
Analysis/ Analyte
m and/or p-Xylene
o-Xylene
ug/L
ug/L
Units 42-__ 43-__ 44-__ 45-__
50000 U 10 U 10 U 50000 U
25000 U 5.0 U 5.0 U 25000 U
4758ASR Number: 03/02/2010
MP7ES02Project ID: Cleburn Street well samplingProject Desc:
RLAB Approved Sample Analysis Results
Page 41 of 48
1
1
1
1
1
Conductivity by Field Measurement
pH of Water by Field Measurement
Temperature of Water by Field Measurement
Turbidity of Water by Field Measurement
VOCs in Water by GC/MS
Analysis/ Analyte
Conductivity
pH
Temperature
Turbidity
Acetone
Benzene
Bromodichloromethane
Bromoform
Bromomethane
2-Butanone
Carbon Disulfide
Carbon Tetrachloride
Chlorobenzene
Chloroethane
Chloroform
Chloromethane
Cyclohexane
1,2-Dibromo-3-Chloropropane
Dibromochloromethane
1,2-Dibromoethane
1,2-Dichlorobenzene
1,3-Dichlorobenzene
1,4-Dichlorobenzene
Dichlorodifluoromethane
1,1-Dichloroethane
1,2-Dichloroethane
1,1-Dichloroethene
cis-1,2-Dichloroethene
trans-1,2-Dichloroethene
1,2-Dichloropropane
cis-1,3-Dichloropropene
trans-1,3-Dichloropropene
Ethyl Benzene
2-Hexanone
Isopropylbenzene
Methyl Acetate
Methyl tert-butyl ether
Methylcyclohexane
Methylene Chloride
4-Methyl-2-Pentanone
Naphthalene
umhos/cm
SU
Deg C
NTU
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
Units 46-__ 46-FD 48-__ 49-__
636 636 1150 692
6.63 6.63 6.70 6.63
12.32 12.32 14.75 13.20
1.2 1.2 0.0 2.6
5.0 U 5.0 U 25000 U 5.0 U
5.0 U 5.0 U 25000 U 5.0 U
5.0 U 5.0 U 25000 U 5.0 U
5.0 U 5.0 U 25000 U 5.0 U
5.0 U 5.0 U 25000 U 5.0 U
5.0 U 5.0 U 25000 U 5.0 U
5.0 U 5.0 U 25000 U 5.0 U
5.0 U 5.0 U 25000 U 5.0 U
5.0 U 5.0 U 25000 U 5.0 U
5.0 U 5.0 U 25000 U 5.0 U
5.0 U 5.0 U 25000 U 5.0 U
5.0 U 5.0 U 25000 U 5.0 U
5.0 U 5.0 U 25000 U 5.0 U
5.0 U 5.0 U 25000 U 5.0 U
5.0 U 5.0 U 25000 U 5.0 U
5.0 U 5.0 U 25000 U 5.0 U
5.0 U 5.0 U 25000 U 5.0 U
5.0 U 5.0 U 25000 U 5.0 U
5.0 U 5.0 U 25000 U 5.0 U
5.0 U 5.0 U 25000 U 5.0 U
5.0 U 5.0 U 25000 U 5.0 U
5.0 U 5.0 U 25000 U 5.0 U
5.0 U 5.0 U 25000 U 5.0 U
5.0 U 5.0 U 25000 U 5.0 U
5.0 U 5.0 U 25000 U 5.0 U
5.0 U 5.0 U 25000 U 5.0 U
5.0 U 5.0 U 25000 U 5.0 U
5.0 U 5.0 U 25000 U 5.0 U
5.0 U 5.0 U 25000 U 5.0 U
5.0 U 5.0 U 25000 U 5.0 U
5.0 U 5.0 U 25000 U 5.0 U
5.0 U 5.0 U 25000 U 5.0 U
10 U 10 U 50000 U 10 U
5.0 U 5.0 U 25000 U 5.0 U
5.0 U 5.0 U 25000 U 5.0 U
5.0 U 5.0 U 25000 U 5.0 U
10 U 10 U 50000 U 10 U
4758ASR Number: 03/02/2010
MP7ES02Project ID: Cleburn Street well samplingProject Desc:
RLAB Approved Sample Analysis Results
Page 42 of 48
Analysis/ Analyte
Styrene
1,1,2,2-Tetrachloroethane
Tetrachloroethene
Toluene
1,2,3-Trichlorobenzene
1,2,4-Trichlorobenzene
1,1,1-Trichloroethane
1,1,2-Trichloroethane
Trichloroethene
Trichlorofluoromethane
1,1,2-Trichlorotrifluoroethane
Vinyl Chloride
m and/or p-Xylene
o-Xylene
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
Units 46-__ 46-FD 48-__ 49-__
5.0 U 5.0 U 25000 U 5.0 U
5.0 U 5.0 U 25000 U 5.0 U
27 30 25000 U 17
5.0 U 5.0 U 25000 U 5.0 U
5.0 U 5.0 U 25000 U 5.0 U
5.0 U 5.0 U 25000 U 5.0 U
5.0 U 5.0 U 25000 U 5.0 U
5.0 U 5.0 U 25000 U 5.0 U
5.0 U 5.0 U 25000 U 5.0 U
5.0 U 5.0 U 25000 U 5.0 U
5.0 U 5.0 U 25000 U 5.0 U
5.0 U 5.0 U 25000 U 5.0 U
10 U 10 U 50000 U 10 U
5.0 U 5.0 U 25000 U 5.0 U
4758ASR Number: 03/02/2010
MP7ES02Project ID: Cleburn Street well samplingProject Desc:
RLAB Approved Sample Analysis Results
Page 43 of 48
1
1
1
1
1
Conductivity by Field Measurement
pH of Water by Field Measurement
Temperature of Water by Field Measurement
Turbidity of Water by Field Measurement
VOCs in Water by GC/MS
Analysis/ Analyte
Conductivity
pH
Temperature
Turbidity
Acetone
Benzene
Bromodichloromethane
Bromoform
Bromomethane
2-Butanone
Carbon Disulfide
Carbon Tetrachloride
Chlorobenzene
Chloroethane
Chloroform
Chloromethane
Cyclohexane
1,2-Dibromo-3-Chloropropane
Dibromochloromethane
1,2-Dibromoethane
1,2-Dichlorobenzene
1,3-Dichlorobenzene
1,4-Dichlorobenzene
Dichlorodifluoromethane
1,1-Dichloroethane
1,2-Dichloroethane
1,1-Dichloroethene
cis-1,2-Dichloroethene
trans-1,2-Dichloroethene
1,2-Dichloropropane
cis-1,3-Dichloropropene
trans-1,3-Dichloropropene
Ethyl Benzene
2-Hexanone
Isopropylbenzene
Methyl Acetate
Methyl tert-butyl ether
Methylcyclohexane
Methylene Chloride
4-Methyl-2-Pentanone
Naphthalene
umhos/cm
SU
Deg C
NTU
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
Units 50-__ 50-FD 52-__ 53-__
721 721 1620 693
6.63 6.63 6.93 6.66
14.64 14.64 15.78 15.82
2.6 2.6 0.9 2.2
5.0 U 5.0 U 5.0 U 5.0 U
5.0 U 5.0 U 5.0 U 5.0 U
5.0 U 5.0 U 5.0 U 5.0 U
5.0 U 5.0 U 5.0 U 5.0 U
5.0 U 5.0 U 5.0 U 5.0 U
5.0 U 5.0 U 5.0 U 5.0 U
5.0 U 5.0 U 5.0 U 5.0 U
5.0 U 5.0 U 5.0 U 5.0 U
5.0 U 5.0 U 5.0 U 5.0 U
5.0 U 5.0 U 5.0 U 5.0 U
5.0 U 5.0 U 5.0 U 5.0 U
5.0 U 5.0 U 5.0 U 5.0 U
5.0 U 5.0 U 5.0 U 5.0 U
5.0 U 5.0 U 5.0 U 5.0 U
5.0 U 5.0 U 5.0 U 5.0 U
5.0 U 5.0 U 5.0 U 5.0 U
5.0 U 5.0 U 5.0 U 5.0 U
5.0 U 5.0 U 5.0 U 5.0 U
5.0 U 5.0 U 5.0 U 5.0 U
5.0 U 5.0 U 5.0 U 5.0 U
5.0 U 5.0 U 5.0 U 5.0 U
5.0 U 5.0 U 5.0 U 5.0 U
5.0 U 5.0 U 5.0 U 5.0 U
5.0 U 5.0 U 5.0 U 5.0 U
5.0 U 5.0 U 5.0 U 5.0 U
5.0 U 5.0 U 5.0 U 5.0 U
5.0 U 5.0 U 5.0 U 5.0 U
5.0 U 5.0 U 5.0 U 5.0 U
5.0 U 5.0 U 5.0 U 5.0 U
5.0 U 5.0 U 5.0 U 5.0 U
5.0 U 5.0 U 5.0 U 5.0 U
5.0 U 5.0 U 5.0 U 5.0 U
10 U 10 U 10 U 10 U
5.0 U 5.0 U 5.0 U 5.0 U
5.0 U 5.0 U 5.0 U 5.0 U
5.0 U 5.0 U 5.0 U 5.0 U
10 U 10 U 10 U 10 U
4758ASR Number: 03/02/2010
MP7ES02Project ID: Cleburn Street well samplingProject Desc:
RLAB Approved Sample Analysis Results
Page 44 of 48
Analysis/ Analyte
Styrene
1,1,2,2-Tetrachloroethane
Tetrachloroethene
Toluene
1,2,3-Trichlorobenzene
1,2,4-Trichlorobenzene
1,1,1-Trichloroethane
1,1,2-Trichloroethane
Trichloroethene
Trichlorofluoromethane
1,1,2-Trichlorotrifluoroethane
Vinyl Chloride
m and/or p-Xylene
o-Xylene
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
Units 50-__ 50-FD 52-__ 53-__
5.0 U 5.0 U 5.0 U 5.0 U
5.0 U 5.0 U 5.0 U 5.0 U
5.0 U 5.0 U 26 5.0 U
5.0 U 5.0 U 5.0 U 5.0 U
5.0 U 5.0 U 5.0 U 5.0 U
5.0 U 5.0 U 5.0 U 5.0 U
5.0 U 5.0 U 5.0 U 5.0 U
5.0 U 5.0 U 5.0 U 5.0 U
5.0 U 5.0 U 5.0 U 5.0 U
5.0 U 5.0 U 5.0 U 5.0 U
5.0 U 5.0 U 5.0 U 5.0 U
5.0 U 5.0 U 5.0 U 5.0 U
10 U 10 U 10 U 10 U
5.0 U 5.0 U 5.0 U 5.0 U
4758ASR Number: 03/02/2010
MP7ES02Project ID: Cleburn Street well samplingProject Desc:
RLAB Approved Sample Analysis Results
Page 45 of 48
1
1
1
1
1
Conductivity by Field Measurement
pH of Water by Field Measurement
Temperature of Water by Field Measurement
Turbidity of Water by Field Measurement
VOCs in Water by GC/MS
Analysis/ Analyte
Conductivity
pH
Temperature
Turbidity
Acetone
Benzene
Bromodichloromethane
Bromoform
Bromomethane
2-Butanone
Carbon Disulfide
Carbon Tetrachloride
Chlorobenzene
Chloroethane
Chloroform
Chloromethane
Cyclohexane
1,2-Dibromo-3-Chloropropane
Dibromochloromethane
1,2-Dibromoethane
1,2-Dichlorobenzene
1,3-Dichlorobenzene
1,4-Dichlorobenzene
Dichlorodifluoromethane
1,1-Dichloroethane
1,2-Dichloroethane
1,1-Dichloroethene
cis-1,2-Dichloroethene
trans-1,2-Dichloroethene
1,2-Dichloropropane
cis-1,3-Dichloropropene
trans-1,3-Dichloropropene
Ethyl Benzene
2-Hexanone
Isopropylbenzene
Methyl Acetate
Methyl tert-butyl ether
Methylcyclohexane
Methylene Chloride
4-Methyl-2-Pentanone
Naphthalene
umhos/cm
SU
Deg C
NTU
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
Units 54-__ 55-__ 56-__ 68-FB
670 1310
6.64 6.81
16.01 16.23
2.3 0.6
5.0 U 5.0 U 5.0 U 5.0 UJ
5.0 U 5.0 U 5.0 U 5.0 U
5.0 U 5.0 U 5.0 U 5.0 U
5.0 U 5.0 U 5.0 U 5.0 U
5.0 U 5.0 U 5.0 U 5.0 U
5.0 U 5.0 U 5.0 U 5.0 U
5.0 U 5.0 U 5.0 U 5.0 U
5.0 U 5.0 U 5.0 U 5.0 U
5.0 U 5.0 U 5.0 U 5.0 U
5.0 U 5.0 U 5.0 U 5.0 U
5.0 U 5.0 U 5.0 U 5.0 U
5.0 U 5.0 U 5.0 U 5.0 U
5.0 U 5.0 U 5.0 U 5.0 U
5.0 U 5.0 U 5.0 U 5.0 U
5.0 U 5.0 U 5.0 U 5.0 U
5.0 U 5.0 U 5.0 U 5.0 U
5.0 U 5.0 U 5.0 U 5.0 U
5.0 U 5.0 U 5.0 U 5.0 U
5.0 U 5.0 U 5.0 U 5.0 U
5.0 U 5.0 U 5.0 U 5.0 U
5.0 U 5.0 U 5.0 U 5.0 U
5.0 U 5.0 U 5.0 U 5.0 U
5.0 U 5.0 U 5.0 U 5.0 U
5.0 U 5.0 U 5.0 U 5.0 U
5.0 U 5.0 U 5.0 U 5.0 U
5.0 U 5.0 U 5.0 U 5.0 U
5.0 U 5.0 U 5.0 U 5.0 U
5.0 U 5.0 U 5.0 U 5.0 U
5.0 U 5.0 U 5.0 U 5.0 U
5.0 U 5.0 U 5.0 U 5.0 U
5.0 U 5.0 U 5.0 U 5.0 U
5.0 U 5.0 U 5.0 U 5.0 U
10 U 10 U 10 U 10 U
5.0 U 5.0 U 5.0 U 5.0 U
5.0 U 5.0 U 5.0 U 5.0 U
5.0 U 5.0 U 5.0 U 5.0 U
10 U 10 U 10 U 10 U
4758ASR Number: 03/02/2010
MP7ES02Project ID: Cleburn Street well samplingProject Desc:
RLAB Approved Sample Analysis Results
Page 46 of 48
Analysis/ Analyte
Styrene
1,1,2,2-Tetrachloroethane
Tetrachloroethene
Toluene
1,2,3-Trichlorobenzene
1,2,4-Trichlorobenzene
1,1,1-Trichloroethane
1,1,2-Trichloroethane
Trichloroethene
Trichlorofluoromethane
1,1,2-Trichlorotrifluoroethane
Vinyl Chloride
m and/or p-Xylene
o-Xylene
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
Units 54-__ 55-__ 56-__ 68-FB
5.0 U 5.0 U 5.0 U 5.0 U
5.0 U 5.0 U 5.0 U 5.0 U
33 5.0 U 81 5.0 U
5.0 U 5.0 U 5.0 U 5.0 U
5.0 U 5.0 U 5.0 U 5.0 U
5.0 U 5.0 U 5.0 U 5.0 U
5.0 U 5.0 U 5.0 U 5.0 U
5.0 U 5.0 U 5.0 U 5.0 U
5.0 U 5.0 U 5.0 U 5.0 U
5.0 U 5.0 U 5.0 U 5.0 U
5.0 U 5.0 U 5.0 U 5.0 U
5.0 U 5.0 U 5.0 U 5.0 U
10 U 10 U 10 U 10 U
5.0 U 5.0 U 5.0 U 5.0 U
4758ASR Number: 03/02/2010
MP7ES02Project ID: Cleburn Street well samplingProject Desc:
RLAB Approved Sample Analysis Results
Page 47 of 48
1 VOCs in Water by GC/MS
Analysis/ Analyte
Acetone
Benzene
Bromodichloromethane
Bromoform
Bromomethane
2-Butanone
Carbon Disulfide
Carbon Tetrachloride
Chlorobenzene
Chloroethane
Chloroform
Chloromethane
Cyclohexane
1,2-Dibromo-3-Chloropropane
Dibromochloromethane
1,2-Dibromoethane
1,2-Dichlorobenzene
1,3-Dichlorobenzene
1,4-Dichlorobenzene
Dichlorodifluoromethane
1,1-Dichloroethane
1,2-Dichloroethane
1,1-Dichloroethene
cis-1,2-Dichloroethene
trans-1,2-Dichloroethene
1,2-Dichloropropane
cis-1,3-Dichloropropene
trans-1,3-Dichloropropene
Ethyl Benzene
2-Hexanone
Isopropylbenzene
Methyl Acetate
Methyl tert-butyl ether
Methylcyclohexane
Methylene Chloride
4-Methyl-2-Pentanone
Naphthalene
Styrene
1,1,2,2-Tetrachloroethane
Tetrachloroethene
Toluene
1,2,3-Trichlorobenzene
1,2,4-Trichlorobenzene
1,1,1-Trichloroethane
1,1,2-Trichloroethane
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
Units 69-FB 70-FB
5.0 UJ 5.0 UJ
5.0 U 5.0 U
5.0 U 5.0 U
5.0 U 5.0 U
5.0 U 5.0 U
5.0 U 5.0 U
5.0 U 5.0 U
5.0 U 5.0 U
5.0 U 5.0 U
5.0 U 5.0 U
5.0 U 5.0 U
5.0 U 5.0 U
5.0 U 5.0 U
5.0 U 5.0 U
5.0 U 5.0 U
5.0 U 5.0 U
5.0 U 5.0 U
5.0 U 5.0 U
5.0 U 5.0 U
5.0 U 5.0 U
5.0 U 5.0 U
5.0 U 5.0 U
5.0 U 5.0 U
5.0 U 5.0 U
5.0 U 5.0 U
5.0 U 5.0 U
5.0 U 5.0 U
5.0 U 5.0 U
5.0 U 5.0 U
5.0 U 5.0 U
5.0 U 5.0 U
5.0 U 5.0 U
10 U 10 U
5.0 U 5.0 U
5.0 U 5.0 U
5.0 U 5.0 U
10 U 10 U
5.0 U 5.0 U
5.0 U 5.0 U
5.0 U 5.0 U
5.0 U 5.0 U
5.0 U 5.0 U
5.0 U 5.0 U
5.0 U 5.0 U
5.0 U 5.0 U
4758ASR Number: 03/02/2010
MP7ES02Project ID: Cleburn Street well samplingProject Desc:
RLAB Approved Sample Analysis Results
Page 48 of 48
Analysis/ Analyte
Trichloroethene
Trichlorofluoromethane
1,1,2-Trichlorotrifluoroethane
Vinyl Chloride
m and/or p-Xylene
o-Xylene
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
Units 69-FB 70-FB
5.0 U 5.0 U
5.0 U 5.0 U
5.0 U 5.0 U
5.0 U 5.0 U
10 U 10 U
5.0 U 5.0 U
4758ASR Number: 03/02/2010
MP7ES02Project ID: Cleburn Street well samplingProject Desc:
RLAB Approved Sample Analysis Results
4758
MP7ES02Project ID:
Cleburn Street well sampling
Mary PetersonSUPR/IANE
United States Environmental Protection AgencyRegion VII
901 N. 5th StreetKansas City, KS 66101
__/__/____
Data Disposition/Sample Release for ASR #:
Project Description:
Subject:
Kaye DollmannENSV/RLAB
I have received and reviewed the Transmittal of Sample Analysis Results for the above-referencedAnalytical Services Request(ASR) and have indicated my findings below by checking one of theboxes for Data Disposition.
I understand all samples will be disposed upon receipt of this form, unless samples are requestedto be held. If I do not return this form all samples will be disposed of on ___________________.
"RELEASED" - Read-only to all Region 7 employees and contractors that have R7LIMS"Customer" account. All Samples may be disposed of upon receipt of this form if not requested tobe held.
"Project Manager Accessible" - Available on the LAN in R7LIMS for my use only. All Samples maybe disposed of upon receipt of this form if not requested to be held.
"Archived" - THIS DATA IS OF A SENSITIVE NATURE. Any future reports must be requestedthrough the laboratory. All samples may be disposed of upon receipt of the form if not requestedto be held.
Date:
From:
To:
Hold Samples - I have determined that the samples need to be held until ______________, afterwhich time they will be disposed of in accordance with applicable regulations. The reason for the hold is:
Samples are associated with a legal proceeding.
Question/Concern with data - possible reanalysis requested.
Other:________________________________________________________________
Page 1 of 27
03/29/2010Date:
4766
MP7ES02
Cleburn Street well sampling
Mary PetersonSUPR/IANE
Transmittal of Sample Analysis Results for ASR #:
Project ID:
Project Description:
Michael F. Davis, ChiefChemical Analysis and Response Branch, Environmental Services Division
To:
Enclosed are the analytical data for the above-referenced Analytical Services Request (ASR) andProject. The Regional Laboratory has reviewed and verified the results in accordance with proceduresdescribed in our Quality Manual (QM). In addition to all of the analytical results, this transmittalcontains pertinent information that may have influenced the reported results and documents anydeviations from the established requirements of the QM.
Please contact us within 14 days of receipt of this package if you determine there is a need for anychanges. Please complete the enclosed Customer Satisfaction Survey and Data Disposition/SampleRelease memo for this ASR as soon as possible. The process of disposing of the samples for this ASRwill be initiated 30 days from the date of this transmittal unless an alternate release date is specifiedon the Data Disposition/Sample Release memo.
If you have any questions or concerns relating to this data package, contact our customer service lineat 913-551-5295.
Enclosures
cc: Analytical Data File.
United States Environmental Protection AgencyRegion 7
901 N. 5th StreetKansas City, KS 66101
Subject:
From:
Page 2 of 27
4766ASR Number: 03/29/2010
Mary Peterson SUPR/IANE 913-551-7882
MP7ES02
Cleburn Street well sampling
Grand Island Nebraska Superfund
CLEBURN STREET WELL - 1 HR MARTINIZING GWRESORATION
07ESSite ID: 02
Site Cleanup Support
Resesarch purpose to investigate new preservative (ascorbic acid)
ISCO Post Injection event and Quarterly Performance monitoring.
100 series samples are preserved in the field. 200 serie are preserved in the lab(~24 hours later).
Project Manager: Org: Phone:
Project ID:
Project Desc:
Location: State: Program:
Site Name: Site OU:
Purpose:
__ = Field SampleFB = Field Blank
QC Codes identify the type of sample for quality control purpose.
Micrograms per Liter
Specific units in which results arereported.
The identification of the analyte is acceptable; the reported value is anestimate.The analyte was not detected at or above the reporting limit.The analyte was not detected at or above the reporting limit. The reportinglimit is an estimate.
Specific codes used in conjunction with data values to provide additional information on the quality of reported results, or used to explain the absence of a specific value.
Summary of Project Information
Explanation of Codes, Units and Qualifiers used on this report
Sample QC Codes: Units:
J
UUJ
=
==
Data Qualifiers:
= Values have been reviewed and found acceptable for use. (Blank)
ug/L =
2009073QAPP Number:
302DD2CGPRA PRC:
Page 3 of 27
101
102
103
104
105
106
107
108
109
110
111
112
113
114
115
116
117
118
119
120
121
122
201
202
203
204
205
206
207
208
209
210
211
212
213
214
215
216
217
218
219
220
SampleNo
__
__
__
__
__
__
__
__
__
__
__
__
__
__
__
__
__
__
__
__
FB
FB
__
__
__
__
__
__
__
__
__
__
__
__
__
__
__
__
__
__
__
__
QCCode
Water
Water
Water
Water
Water
Water
Water
Water
Water
Water
Water
Water
Water
Water
Water
Water
Water
Water
Water
Water
Water
Water
Water
Water
Water
Water
Water
Water
Water
Water
Water
Water
Water
Water
Water
Water
Water
Water
Water
Water
Water
Water
Matrix
IW-5
IW-6
IW-7
IW-3
IW-2
IW-4
IW-1
ERT-16
IW-8
IW-10
IW-9
4758-12
MW-2A
MW-12A
ERT-14
ERT-15
DPE-1
DPE-2
DPE-3
DPE-4
EPA prepared VOA Trip Blanksample #1EPA prepared VOA Trip Blanksample #2IW-5
IW-6
IW-7
IW-3
IW-2
IW-4
IW-1
ERT-16
IW-8
IW-10
IW-9
MW-2B
MW-2A
MW-12A
ERT-14
ERT-15
DPE-1
DPE-2
DPE-3
DPE-4
Location DescriptionExternal
Sample No
01/19/2010
01/19/2010
01/19/2010
01/20/2010
01/20/2010
01/20/2010
01/20/2010
01/20/2010
01/20/2010
01/21/2010
01/21/2010
01/21/2010
01/21/2010
01/24/2010
01/24/2010
01/24/2010
01/25/2010
01/25/2010
01/25/2010
01/25/2010
01/19/2010
01/20/2010
01/19/2010
01/19/2010
01/19/2010
01/20/2010
01/20/2010
01/20/2010
01/20/2010
01/20/2010
01/20/2010
01/21/2010
01/21/2010
01/21/2010
01/21/2010
01/24/2010
01/24/2010
01/24/2010
01/25/2010
01/25/2010
01/25/2010
01/25/2010
Start Date
11:45
15:30
18:15
09:00
10:35
11:45
14:20
15:35
18:00
09:35
11:30
14:00
16:05
14:50
16:05
17:20
10:50
12:20
14:35
16:00
14:30
08:35
11:45
15:30
18:15
09:00
10:35
11:45
14:20
15:35
18:00
09:35
11:30
14:00
16:05
14:50
16:05
17:20
10:50
12:20
14:35
16:00
Start Time
End Date
End Time
01/21/2010
01/21/2010
01/21/2010
01/21/2010
01/21/2010
01/21/2010
01/21/2010
01/21/2010
01/22/2010
01/22/2010
01/22/2010
01/22/2010
01/22/2010
01/26/2010
01/26/2010
01/26/2010
01/26/2010
01/26/2010
01/26/2010
01/26/2010
01/21/2010
01/21/2010
01/21/2010
01/21/2010
01/21/2010
01/21/2010
01/21/2010
01/21/2010
01/21/2010
01/21/2010
01/22/2010
01/22/2010
01/22/2010
01/22/2010
01/22/2010
01/26/2010
01/26/2010
01/26/2010
01/26/2010
01/26/2010
01/26/2010
01/26/2010
ReceiptDate
4766 03/29/2010
MP7ES02Project ID: Cleburn Street well samplingProject Desc:
ASR Number: Sample Information Summary
-
-
-
-
-
-
-
-
-
-
-
-
-
-
-
-
-
-
-
-
-
-
-
-
-
-
-
-
-
-
-
-
-
-
-
-
-
-
-
-
-
-
Page 4 of 27
1 VOCs in Water by GC/MS
Region 7 EPA Laboratory - Kansas City, Ks.Lab:
EPA Region 7 RLAB Method 3230.1FMethod:
Analyst Notes:100-series had 1.5g Ascorbic Acid in VOA vial added at time of sample collection in thefield.200-series had 1.5g Ascorbic Acid in VOA vial added at time of sample arrival in the lab. Samples 205-208, 210-213, and 217-219 were preserved 1 day after collection.Samples 201-203, 209, and 214-216 were preserved 2 days after collection.Sample 220 was preserved 4 days after collection.Sample 204 was preserved 9 days after collection. Sample 204 data was similar to 104,and was not qualified due to late preservation/analysis. (Samples 204 and 209 weremistakenly stored in a separate area.) All samples were injected within 14 days of collection.pH of preserved samples was ~ 4 or less.
100 series samples appeared clear, except for 101, which was dark purple. Ascorbic acidwas added to sample 101 on arrival into the lab (2 days after collection). 200 series samples appeared dark purple (estimate range 0.015 - 1.5% KMnO4 by eye),except for samples 201, 212, 214, and 215 which were clear.
Note tentatively identified compound at 40ug/L or more, and others, in samples: 101, 103,110, 111, 201, 203, 210, and 211.
Acetone was J-coded in samples 106, 107, 206, 207, and 113. Although the analyte inquestion has been positively identified in the samples, the quantitation is an estimate (J-coded) due to the continuing calibration check not meeting accuracy specifications. Theactual concentration for this analyte may be higher than the reported value.
Acetone was UJ-coded in samples 112. This analyte was not found in the samples at orabove the reporting limit, however, the reporting limit is an estimate (UJ-coded) due to thecontinuing calibration check not meeting accuracy specifications. The actual reporting limitfor this analyte may be higher than the reported value.
Slight Acetone contamination was found in the laboratory method blank. Only samplescontaining this analyte at a level greater than ten times the contamination level of theblank are reported without being qualified. All samples that contained this analyte but at alevel less than ten times the contamination in the blank have the result U-coded indicatingthat the reporting limit has been raised to the level found in the sample. Samples affected
Comments:
101-__ 102-__ 103-__ 104-__ 105-__ 106-__ 107-__108-__ 109-__ 110-__ 111-__ 112-__ 113-__ 114-__115-__ 116-__ 117-__ 118-__ 119-__ 120-__ 121-FB122-FB 201-__ 202-__ 203-__ 204-__ 205-__ 206-__207-__ 208-__ 209-__ 210-__ 211-__ 212-__ 213-__214-__ 215-__ 216-__ 217-__ 218-__ 219-__ 220-__
Samples:
4766ASR Number: 03/29/2010
MP7ES02Project ID: Cleburn Street well samplingProject Desc
RLAB Approved Analysis Comments
Analysis Comments About Results For This Analysis
Page 5 of 27
were: 116 and 216.
2-Butanone and Carbon Tetrachloride were J-coded in sample 202. Although the analytein question has been positively identified in the sample, the quantitation is an estimate (J-coded) due to high recovery of this analyte in the laboratory matrix spike. The actualconcentration for this analyte may be lower than the reported value.
4766ASR Number: 03/29/2010
MP7ES02Project ID: Cleburn Street well samplingProject Desc
RLAB Approved Analysis Comments
Analysis Comments About Results For This Analysis
Page 6 of 27
1 VOCs in Water by GC/MS
Analysis/ Analyte
Acetone
Benzene
Bromodichloromethane
Bromoform
Bromomethane
2-Butanone
Carbon Disulfide
Carbon Tetrachloride
Chlorobenzene
Chloroethane
Chloroform
Chloromethane
Cyclohexane
1,2-Dibromo-3-Chloropropane
Dibromochloromethane
1,2-Dibromoethane
1,2-Dichlorobenzene
1,3-Dichlorobenzene
1,4-Dichlorobenzene
Dichlorodifluoromethane
1,1-Dichloroethane
1,2-Dichloroethane
1,1-Dichloroethene
cis-1,2-Dichloroethene
trans-1,2-Dichloroethene
1,2-Dichloropropane
cis-1,3-Dichloropropene
trans-1,3-Dichloropropene
Ethyl Benzene
2-Hexanone
Isopropylbenzene
Methyl Acetate
Methyl tert-butyl ether
Methylcyclohexane
Methylene Chloride
4-Methyl-2-Pentanone
Naphthalene
Styrene
1,1,2,2-Tetrachloroethane
Tetrachloroethene
Toluene
1,2,3-Trichlorobenzene
1,2,4-Trichlorobenzene
1,1,1-Trichloroethane
1,1,2-Trichloroethane
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
Units 101-__ 102-__ 103-__ 104-__
210 420 490 54
5.0 U 5.0 U 5.0 U 5.0 U
8.3 9.9 21 5.0 U
5.0 U 5.0 U 5.0 U 5.0 U
5.0 U 5.0 U 5.0 U 5.0 U
54 110 180 21
5.0 U 5.0 U 5.0 U 5.0 U
73 46 97 5.0 U
5.0 U 5.0 U 5.0 U 5.0 U
5.0 U 5.0 U 5.0 U 5.0 U
110 140 240 5.0 U
5.0 U 5.0 U 5.1 5.0 U
5.0 U 5.0 U 5.0 U 5.0 U
5.0 U 5.0 U 5.0 U 5.0 U
7.1 8.1 12 7.6
5.0 U 5.0 U 5.0 U 5.0 U
14 6.4 8.1 5.0 U
5.0 U 5.0 U 5.0 U 5.0 U
5.0 U 5.0 U 5.0 U 5.0 U
10 U 10 U 10 U 10 U
5.0 U 5.0 U 5.0 U 5.0 U
5.0 U 5.0 U 5.0 U 5.0 U
5.0 U 5.0 U 5.0 U 5.0 U
5.0 U 5.0 U 5.0 U 5.0 U
5.0 U 5.0 U 5.0 U 5.0 U
5.0 U 5.0 U 5.0 U 5.0 U
5.0 U 5.0 U 5.0 U 5.0 U
5.0 U 5.0 U 5.0 U 5.0 U
5.0 U 5.0 U 5.0 U 5.0 U
5.0 U 5.0 U 5.0 U 5.0 U
5.0 U 5.0 U 5.0 U 5.0 U
5.0 U 5.0 U 5.0 U 5.0 U
10 U 10 U 10 U 10 U
5.0 U 5.0 U 5.0 U 5.0 U
5.0 U 5.0 U 5.0 U 5.0 U
5.0 U 5.0 U 5.0 U 5.0 U
10 U 10 U 10 U 10 U
5.0 U 5.0 U 5.0 U 5.0 U
5.0 U 5.0 U 5.0 U 5.0 U
5.0 U 5.0 U 5.0 U 5.0 U
5.0 U 5.0 U 5.0 U 5.0 U
5.0 U 5.0 U 5.0 U 5.0 U
5.0 U 5.0 U 5.0 U 5.0 U
24 9.4 15 5.0 U
5.0 U 5.0 U 5.0 U 5.0 U
4766ASR Number: 03/29/2010
MP7ES02Project ID: Cleburn Street well samplingProject Desc:
RLAB Approved Sample Analysis Results
Page 7 of 27
Analysis/ Analyte
Trichloroethene
Trichlorofluoromethane
1,1,2-Trichlorotrifluoroethane
Vinyl Chloride
m and/or p-Xylene
o-Xylene
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
Units 101-__ 102-__ 103-__ 104-__
5.0 U 5.0 U 5.0 U 5.0 U
5.0 U 5.0 U 5.0 U 5.0 U
5.0 U 5.0 U 5.0 U 5.0 U
5.0 U 5.0 U 5.0 U 5.0 U
10 U 10 U 10 U 10 U
5.0 U 5.0 U 5.0 U 5.0 U
4766ASR Number: 03/29/2010
MP7ES02Project ID: Cleburn Street well samplingProject Desc:
RLAB Approved Sample Analysis Results
Page 8 of 27
1 VOCs in Water by GC/MS
Analysis/ Analyte
Acetone
Benzene
Bromodichloromethane
Bromoform
Bromomethane
2-Butanone
Carbon Disulfide
Carbon Tetrachloride
Chlorobenzene
Chloroethane
Chloroform
Chloromethane
Cyclohexane
1,2-Dibromo-3-Chloropropane
Dibromochloromethane
1,2-Dibromoethane
1,2-Dichlorobenzene
1,3-Dichlorobenzene
1,4-Dichlorobenzene
Dichlorodifluoromethane
1,1-Dichloroethane
1,2-Dichloroethane
1,1-Dichloroethene
cis-1,2-Dichloroethene
trans-1,2-Dichloroethene
1,2-Dichloropropane
cis-1,3-Dichloropropene
trans-1,3-Dichloropropene
Ethyl Benzene
2-Hexanone
Isopropylbenzene
Methyl Acetate
Methyl tert-butyl ether
Methylcyclohexane
Methylene Chloride
4-Methyl-2-Pentanone
Naphthalene
Styrene
1,1,2,2-Tetrachloroethane
Tetrachloroethene
Toluene
1,2,3-Trichlorobenzene
1,2,4-Trichlorobenzene
1,1,1-Trichloroethane
1,1,2-Trichloroethane
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
Units 105-__ 106-__ 107-__ 108-__
210 63 J 180 J 240
5.0 U 5.0 U 5.0 U 5.0 U
5.0 U 5.0 U 5.0 U 5.0 U
5.0 U 5.0 U 5.0 U 5.0 U
5.0 U 5.0 U 5.0 U 5.0 U
74 23 42 17
5.0 U 5.0 U 5.0 U 5.0 U
5.0 U 5.0 U 5.0 U 5.0 U
5.0 U 5.0 U 5.0 U 5.0 U
5.0 U 5.0 U 5.0 U 5.0 U
5.0 U 5.0 U 5.0 U 19
5.0 U 5.0 U 5.0 U 5.0 U
5.0 U 5.0 U 5.0 U 5.0 U
5.0 U 5.0 U 5.0 U 5.0 U
5.0 U 7.6 5.0 U 5.0 U
5.0 U 5.0 U 5.0 U 5.0 U
5.0 U 5.0 U 5.0 U 5.0 U
5.0 U 5.0 U 5.0 U 5.0 U
5.0 U 5.0 U 5.0 U 5.0 U
10 U 10 U 10 U 10 U
5.0 U 5.0 U 5.0 U 5.0 U
5.0 U 5.0 U 5.0 U 5.0 U
5.0 U 5.0 U 5.0 U 5.0 U
5.0 U 5.0 U 5.0 U 5.0 U
5.0 U 5.0 U 5.0 U 5.0 U
5.0 U 5.0 U 5.0 U 5.0 U
5.0 U 5.0 U 5.0 U 5.0 U
5.0 U 5.0 U 5.0 U 5.0 U
5.0 U 5.0 U 5.0 U 5.0 U
5.0 U 5.0 U 5.0 U 5.0 U
5.0 U 5.0 U 5.0 U 5.0 U
5.0 U 5.0 U 5.0 U 5.0 U
10 U 10 U 10 U 10 U
5.0 U 5.0 U 5.0 U 5.0 U
5.0 U 5.0 U 5.0 U 5.0 U
5.0 U 5.0 U 5.0 U 5.0 U
10 U 10 U 10 U 10 U
5.0 U 5.0 U 5.0 U 5.0 U
5.0 U 5.0 U 5.0 U 5.0 U
5.0 U 5.0 U 5.0 U 97
5.0 U 5.0 U 5.0 U 5.0 U
5.0 U 5.0 U 5.0 U 5.0 U
5.0 U 5.0 U 5.0 U 5.0 U
5.0 U 5.0 U 5.0 U 5.0 U
5.0 U 5.0 U 5.0 U 5.0 U
4766ASR Number: 03/29/2010
MP7ES02Project ID: Cleburn Street well samplingProject Desc:
RLAB Approved Sample Analysis Results
Page 9 of 27
Analysis/ Analyte
Trichloroethene
Trichlorofluoromethane
1,1,2-Trichlorotrifluoroethane
Vinyl Chloride
m and/or p-Xylene
o-Xylene
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
Units 105-__ 106-__ 107-__ 108-__
5.0 U 5.0 U 5.0 U 5.0 U
5.0 U 5.0 U 5.0 U 5.0 U
5.0 U 5.0 U 5.0 U 5.0 U
5.0 U 5.0 U 5.0 U 5.0 U
10 U 10 U 10 U 10 U
5.0 U 5.0 U 5.0 U 5.0 U
4766ASR Number: 03/29/2010
MP7ES02Project ID: Cleburn Street well samplingProject Desc:
RLAB Approved Sample Analysis Results
Page 10 of 27
1 VOCs in Water by GC/MS
Analysis/ Analyte
Acetone
Benzene
Bromodichloromethane
Bromoform
Bromomethane
2-Butanone
Carbon Disulfide
Carbon Tetrachloride
Chlorobenzene
Chloroethane
Chloroform
Chloromethane
Cyclohexane
1,2-Dibromo-3-Chloropropane
Dibromochloromethane
1,2-Dibromoethane
1,2-Dichlorobenzene
1,3-Dichlorobenzene
1,4-Dichlorobenzene
Dichlorodifluoromethane
1,1-Dichloroethane
1,2-Dichloroethane
1,1-Dichloroethene
cis-1,2-Dichloroethene
trans-1,2-Dichloroethene
1,2-Dichloropropane
cis-1,3-Dichloropropene
trans-1,3-Dichloropropene
Ethyl Benzene
2-Hexanone
Isopropylbenzene
Methyl Acetate
Methyl tert-butyl ether
Methylcyclohexane
Methylene Chloride
4-Methyl-2-Pentanone
Naphthalene
Styrene
1,1,2,2-Tetrachloroethane
Tetrachloroethene
Toluene
1,2,3-Trichlorobenzene
1,2,4-Trichlorobenzene
1,1,1-Trichloroethane
1,1,2-Trichloroethane
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
Units 109-__ 110-__ 111-__ 112-__
250 370 580 5.0 UJ
5.0 U 5.0 U 5.0 U 5.0 U
5.0 U 5.6 14 5.0 U
5.0 U 5.0 U 5.0 U 5.0 U
5.0 U 5.0 U 5.0 U 5.0 U
20 34 41 5.0 U
5.0 U 5.0 U 5.0 U 5.0 U
21 940 320 5.0 U
5.0 U 5.0 U 5.0 U 5.0 U
5.0 U 5.0 U 5.0 U 5.0 U
5.0 U 45 170 5.0 U
5.0 U 5.0 U 5.0 U 5.0 U
5.0 U 5.0 U 5.0 U 5.0 U
5.0 U 5.0 U 5.0 U 5.0 U
5.0 U 5.0 10 5.0 U
5.0 U 5.0 U 5.0 U 5.0 U
5.0 U 7.6 19 5.0 U
5.0 U 5.0 U 5.0 U 5.0 U
5.0 U 5.0 U 5.0 U 5.0 U
10 U 10 U 10 U 10 U
5.0 U 5.0 U 5.0 U 5.0 U
5.0 U 5.0 U 5.0 U 5.0 U
5.0 U 5.0 U 5.0 U 5.0 U
5.0 U 5.0 U 5.0 U 5.0 U
5.0 U 5.0 U 5.0 U 5.0 U
5.0 U 5.0 U 5.0 U 5.0 U
5.0 U 5.0 U 5.0 U 5.0 U
5.0 U 5.0 U 5.0 U 5.0 U
5.0 U 5.0 U 5.0 U 5.0 U
5.0 U 5.0 U 5.0 U 5.0 U
5.0 U 5.0 U 5.0 U 5.0 U
5.0 U 5.0 U 5.0 U 5.0 U
10 U 10 U 10 U 10 U
5.0 U 5.0 U 5.0 U 5.0 U
5.0 U 5.0 U 5.0 U 5.0 U
5.0 U 5.0 U 5.0 U 5.0 U
10 U 10 U 10 U 10 U
5.0 U 5.0 U 5.0 U 5.0 U
5.0 U 5.0 U 5.0 U 5.0 U
5.0 U 120 77 5.0 U
5.0 U 5.0 U 5.0 U 5.0 U
5.0 U 5.0 U 5.0 U 5.0 U
5.0 U 5.0 U 5.0 U 5.0 U
5.0 U 25 19 5.0 U
5.0 U 5.0 U 5.0 U 5.0 U
4766ASR Number: 03/29/2010
MP7ES02Project ID: Cleburn Street well samplingProject Desc:
RLAB Approved Sample Analysis Results
Page 11 of 27
Analysis/ Analyte
Trichloroethene
Trichlorofluoromethane
1,1,2-Trichlorotrifluoroethane
Vinyl Chloride
m and/or p-Xylene
o-Xylene
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
Units 109-__ 110-__ 111-__ 112-__
5.0 U 5.0 U 5.0 U 5.0 U
5.0 U 5.0 U 5.0 U 5.0 U
5.0 U 5.0 U 5.0 U 5.0 U
5.0 U 5.0 U 5.0 U 5.0 U
10 U 10 U 10 U 10 U
5.0 U 5.0 U 5.0 U 5.0 U
4766ASR Number: 03/29/2010
MP7ES02Project ID: Cleburn Street well samplingProject Desc:
RLAB Approved Sample Analysis Results
Page 12 of 27
1 VOCs in Water by GC/MS
Analysis/ Analyte
Acetone
Benzene
Bromodichloromethane
Bromoform
Bromomethane
2-Butanone
Carbon Disulfide
Carbon Tetrachloride
Chlorobenzene
Chloroethane
Chloroform
Chloromethane
Cyclohexane
1,2-Dibromo-3-Chloropropane
Dibromochloromethane
1,2-Dibromoethane
1,2-Dichlorobenzene
1,3-Dichlorobenzene
1,4-Dichlorobenzene
Dichlorodifluoromethane
1,1-Dichloroethane
1,2-Dichloroethane
1,1-Dichloroethene
cis-1,2-Dichloroethene
trans-1,2-Dichloroethene
1,2-Dichloropropane
cis-1,3-Dichloropropene
trans-1,3-Dichloropropene
Ethyl Benzene
2-Hexanone
Isopropylbenzene
Methyl Acetate
Methyl tert-butyl ether
Methylcyclohexane
Methylene Chloride
4-Methyl-2-Pentanone
Naphthalene
Styrene
1,1,2,2-Tetrachloroethane
Tetrachloroethene
Toluene
1,2,3-Trichlorobenzene
1,2,4-Trichlorobenzene
1,1,1-Trichloroethane
1,1,2-Trichloroethane
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
Units 113-__ 114-__ 115-__ 116-__
93 J 5.0 U 5.0 U 23 U
5.0 U 5.0 U 5.0 U 5.0 U
5.0 U 5.0 U 5.0 U 5.0 U
5.0 U 5.0 U 5.0 U 5.0 U
5.0 U 5.0 U 5.0 U 5.0 U
15 5.0 U 5.0 U 5.0 U
5.0 U 5.0 U 5.0 U 5.0 U
33 5.0 U 5.0 U 5.0 U
5.0 U 5.0 U 5.0 U 5.0 U
5.0 U 5.0 U 5.0 U 5.0 U
23 5.0 U 5.0 U 5.0 U
5.0 U 5.0 U 5.0 U 5.0 U
5.0 U 11 5.0 U 5.0 U
5.0 U 5.0 U 5.0 U 5.0 U
5.0 U 5.0 U 5.0 U 5.0 U
5.0 U 5.0 U 5.0 U 5.0 U
5.0 U 5.0 U 5.0 U 5.0 U
5.0 U 5.0 U 5.0 U 5.0 U
5.0 U 5.0 U 5.0 U 5.0 U
10 U 10 U 10 U 10 U
5.0 U 5.0 U 5.0 U 5.0 U
5.0 U 5.0 U 5.0 U 5.0 U
5.0 U 5.0 U 5.0 U 5.0 U
5.0 U 22 5.0 U 5.0 U
5.0 U 5.0 U 5.0 U 5.0 U
5.0 U 5.0 U 5.0 U 5.0 U
5.0 U 5.0 U 5.0 U 5.0 U
5.0 U 5.0 U 5.0 U 5.0 U
5.0 U 12 5.0 U 5.0 U
5.0 U 5.0 U 5.0 U 5.0 U
5.0 U 6.7 5.0 U 5.0 U
5.0 U 5.0 U 5.0 U 5.0 U
10 U 10 U 10 U 10 U
5.0 U 6.2 5.0 U 5.0 U
5.0 U 5.0 U 5.0 U 5.0 U
5.0 U 5.0 U 5.0 U 5.0 U
10 U 18 10 U 10 U
5.0 U 5.0 U 5.0 U 5.0 U
5.0 U 5.0 U 5.0 U 5.0 U
3900 J 2400 11 5.0 U
5.0 U 7.3 5.0 U 5.0 U
5.0 U 5.0 U 5.0 U 5.0 U
5.0 U 5.0 U 5.0 U 5.0 U
30 5.0 U 5.0 U 5.0 U
5.0 U 5.0 U 5.0 U 5.0 U
4766ASR Number: 03/29/2010
MP7ES02Project ID: Cleburn Street well samplingProject Desc:
RLAB Approved Sample Analysis Results
Page 13 of 27
Analysis/ Analyte
Trichloroethene
Trichlorofluoromethane
1,1,2-Trichlorotrifluoroethane
Vinyl Chloride
m and/or p-Xylene
o-Xylene
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
Units 113-__ 114-__ 115-__ 116-__
5.0 U 210 5.0 U 5.0 U
5.0 U 5.0 U 5.0 U 5.0 U
5.0 U 5.0 U 5.0 U 5.0 U
5.0 U 5.0 U 5.0 U 5.0 U
10 U 38 10 U 10 U
5.0 U 11 5.0 U 5.0 U
4766ASR Number: 03/29/2010
MP7ES02Project ID: Cleburn Street well samplingProject Desc:
RLAB Approved Sample Analysis Results
Page 14 of 27
1 VOCs in Water by GC/MS
Analysis/ Analyte
Acetone
Benzene
Bromodichloromethane
Bromoform
Bromomethane
2-Butanone
Carbon Disulfide
Carbon Tetrachloride
Chlorobenzene
Chloroethane
Chloroform
Chloromethane
Cyclohexane
1,2-Dibromo-3-Chloropropane
Dibromochloromethane
1,2-Dibromoethane
1,2-Dichlorobenzene
1,3-Dichlorobenzene
1,4-Dichlorobenzene
Dichlorodifluoromethane
1,1-Dichloroethane
1,2-Dichloroethane
1,1-Dichloroethene
cis-1,2-Dichloroethene
trans-1,2-Dichloroethene
1,2-Dichloropropane
cis-1,3-Dichloropropene
trans-1,3-Dichloropropene
Ethyl Benzene
2-Hexanone
Isopropylbenzene
Methyl Acetate
Methyl tert-butyl ether
Methylcyclohexane
Methylene Chloride
4-Methyl-2-Pentanone
Naphthalene
Styrene
1,1,2,2-Tetrachloroethane
Tetrachloroethene
Toluene
1,2,3-Trichlorobenzene
1,2,4-Trichlorobenzene
1,1,1-Trichloroethane
1,1,2-Trichloroethane
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
Units 117-__ 118-__ 119-__ 120-__
240 56 200 150
5.0 U 5.0 U 5.0 U 5.0 U
5.0 U 5.0 U 5.0 5.0 U
5.0 U 5.0 U 5.0 U 5.0 U
5.0 U 5.0 U 5.0 U 5.0 U
78 67 24 120
5.0 U 5.0 U 5.0 U 5.0 U
25 5.0 U 41 5.0 U
5.0 U 5.0 U 5.0 U 5.0 U
5.0 U 5.0 U 5.0 U 5.0 U
110 5.0 U 120 5.0 U
5.0 U 5.0 U 5.0 U 5.0 U
5.0 U 5.0 U 5.0 U 5.0 U
5.0 U 5.0 U 5.0 U 5.0 U
5.0 U 5.0 U 5.0 U 5.0 U
5.0 U 5.0 U 5.0 U 5.0 U
5.0 U 5.0 U 5.0 U 5.0 U
5.0 U 5.0 U 5.0 U 5.0 U
5.0 U 5.0 U 5.0 U 5.0 U
10 U 10 U 10 U 10 U
5.0 U 5.0 U 5.0 U 5.0 U
5.0 U 5.0 U 5.0 U 5.0 U
5.0 U 5.0 U 5.0 U 5.0 U
5.0 U 5.0 U 5.0 U 5.0 U
5.0 U 5.0 U 5.0 U 5.0 U
5.0 U 5.0 U 5.0 U 5.0 U
5.0 U 5.0 U 5.0 U 5.0 U
5.0 U 5.0 U 5.0 U 5.0 U
5.0 U 5.0 U 5.0 U 5.0 U
5.0 U 5.0 U 5.0 U 5.0 U
5.0 U 5.0 U 5.0 U 5.0 U
5.0 U 5.0 U 5.0 U 5.0 U
10 U 10 U 10 U 10 U
5.0 U 5.0 U 5.0 U 5.0 U
5.0 U 5.0 U 5.0 U 5.0 U
5.0 U 5.0 U 5.0 U 5.0 U
10 U 10 U 10 U 10 U
5.0 U 5.0 U 5.0 U 5.0 U
5.0 U 5.0 U 5.0 U 5.0 U
5.0 U 5.0 U 43 5.0 U
5.0 U 5.0 U 5.0 U 5.0 U
5.0 U 5.0 U 5.0 U 5.0 U
5.0 U 5.0 U 5.0 U 5.0 U
5.0 U 5.0 U 35 5.0 U
5.0 U 5.0 U 5.0 U 5.0 U
4766ASR Number: 03/29/2010
MP7ES02Project ID: Cleburn Street well samplingProject Desc:
RLAB Approved Sample Analysis Results
Page 15 of 27
Analysis/ Analyte
Trichloroethene
Trichlorofluoromethane
1,1,2-Trichlorotrifluoroethane
Vinyl Chloride
m and/or p-Xylene
o-Xylene
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
Units 117-__ 118-__ 119-__ 120-__
5.0 U 5.0 U 5.0 U 5.0 U
5.0 U 5.0 U 5.0 U 5.0 U
5.0 U 5.0 U 5.0 U 5.0 U
5.0 U 5.0 U 5.0 U 5.0 U
10 U 10 U 10 U 10 U
5.0 U 5.0 U 5.0 U 5.0 U
4766ASR Number: 03/29/2010
MP7ES02Project ID: Cleburn Street well samplingProject Desc:
RLAB Approved Sample Analysis Results
Page 16 of 27
1 VOCs in Water by GC/MS
Analysis/ Analyte
Acetone
Benzene
Bromodichloromethane
Bromoform
Bromomethane
2-Butanone
Carbon Disulfide
Carbon Tetrachloride
Chlorobenzene
Chloroethane
Chloroform
Chloromethane
Cyclohexane
1,2-Dibromo-3-Chloropropane
Dibromochloromethane
1,2-Dibromoethane
1,2-Dichlorobenzene
1,3-Dichlorobenzene
1,4-Dichlorobenzene
Dichlorodifluoromethane
1,1-Dichloroethane
1,2-Dichloroethane
1,1-Dichloroethene
cis-1,2-Dichloroethene
trans-1,2-Dichloroethene
1,2-Dichloropropane
cis-1,3-Dichloropropene
trans-1,3-Dichloropropene
Ethyl Benzene
2-Hexanone
Isopropylbenzene
Methyl Acetate
Methyl tert-butyl ether
Methylcyclohexane
Methylene Chloride
4-Methyl-2-Pentanone
Naphthalene
Styrene
1,1,2,2-Tetrachloroethane
Tetrachloroethene
Toluene
1,2,3-Trichlorobenzene
1,2,4-Trichlorobenzene
1,1,1-Trichloroethane
1,1,2-Trichloroethane
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
Units 121-FB 122-FB 201-__ 202-__
17 21 250 500 J
5.0 U 5.0 U 5.0 U 5.0 U
5.0 U 5.0 U 8.3 10
5.0 U 5.0 U 5.0 U 5.0 U
5.0 U 5.0 U 5.0 U 5.0 U
5.0 U 5.0 U 54 98 J
5.0 U 5.0 U 5.0 U 5.0 U
5.0 U 5.0 U 72 45 J
5.0 U 5.0 U 5.0 U 5.0 U
5.0 U 5.0 U 5.0 U 5.0 U
5.0 U 5.0 U 110 140
5.0 U 5.0 U 5.0 U 5.0 U
5.0 U 5.0 U 5.0 U 5.0 U
5.0 U 5.0 U 5.0 U 5.0 U
5.0 U 5.0 U 6.7 7.7
5.0 U 5.0 U 5.0 U 5.0 U
5.0 U 5.0 U 14 5.8
5.0 U 5.0 U 5.0 U 5.0 U
5.0 U 5.0 U 5.0 U 5.0 U
10 U 10 U 5.0 U 10 U
5.0 U 5.0 U 5.0 U 5.0 U
5.0 U 5.0 U 5.0 U 5.0 U
5.0 U 5.0 U 5.0 U 5.0 U
5.0 U 5.0 U 5.0 U 5.0 U
5.0 U 5.0 U 5.0 U 5.0 U
5.0 U 5.0 U 5.0 U 5.0 U
5.0 U 5.0 U 5.0 U 5.0 U
5.0 U 5.0 U 5.0 U 5.0 U
5.0 U 5.0 U 5.0 U 5.0 U
5.0 U 5.0 U 5.0 U 5.0 U
5.0 U 5.0 U 5.0 U 5.0 U
5.0 U 5.0 U 5.0 U 5.0 U
10 U 10 U 10 U 10 U
5.0 U 5.0 U 5.0 U 5.0 U
5.0 U 5.0 U 5.0 U 5.0 U
5.0 U 5.0 U 5.0 U 5.0 U
10 U 10 U 10 U 10 U
5.0 U 5.0 U 5.0 U 5.0 U
5.0 U 5.0 U 5.0 U 5.0 U
5.0 U 5.0 U 460 5.0 U
5.0 U 5.0 U 5.0 U 5.0 U
5.0 U 5.0 U 5.0 U 5.0 U
5.0 U 5.0 U 5.0 U 5.0 U
5.0 U 5.0 U 24 9.2
5.0 U 5.0 U 5.0 U 5.0 U
4766ASR Number: 03/29/2010
MP7ES02Project ID: Cleburn Street well samplingProject Desc:
RLAB Approved Sample Analysis Results
Page 17 of 27
Analysis/ Analyte
Trichloroethene
Trichlorofluoromethane
1,1,2-Trichlorotrifluoroethane
Vinyl Chloride
m and/or p-Xylene
o-Xylene
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
Units 121-FB 122-FB 201-__ 202-__
5.0 U 5.0 U 5.0 U 5.0 U
5.0 U 5.0 U 5.0 U 5.0 U
5.0 U 5.0 U 5.0 U 5.0 U
5.0 U 5.0 U 5.0 U 5.0 U
10 U 10 U 10 U 10 U
5.0 U 5.0 U 5.0 U 5.0 U
4766ASR Number: 03/29/2010
MP7ES02Project ID: Cleburn Street well samplingProject Desc:
RLAB Approved Sample Analysis Results
Page 18 of 27
1 VOCs in Water by GC/MS
Analysis/ Analyte
Acetone
Benzene
Bromodichloromethane
Bromoform
Bromomethane
2-Butanone
Carbon Disulfide
Carbon Tetrachloride
Chlorobenzene
Chloroethane
Chloroform
Chloromethane
Cyclohexane
1,2-Dibromo-3-Chloropropane
Dibromochloromethane
1,2-Dibromoethane
1,2-Dichlorobenzene
1,3-Dichlorobenzene
1,4-Dichlorobenzene
Dichlorodifluoromethane
1,1-Dichloroethane
1,2-Dichloroethane
1,1-Dichloroethene
cis-1,2-Dichloroethene
trans-1,2-Dichloroethene
1,2-Dichloropropane
cis-1,3-Dichloropropene
trans-1,3-Dichloropropene
Ethyl Benzene
2-Hexanone
Isopropylbenzene
Methyl Acetate
Methyl tert-butyl ether
Methylcyclohexane
Methylene Chloride
4-Methyl-2-Pentanone
Naphthalene
Styrene
1,1,2,2-Tetrachloroethane
Tetrachloroethene
Toluene
1,2,3-Trichlorobenzene
1,2,4-Trichlorobenzene
1,1,1-Trichloroethane
1,1,2-Trichloroethane
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
Units 203-__ 204-__ 205-__ 206-__
530 89 220 69 J
5.0 U 5.0 U 5.0 U 5.0 U
23 5.0 U 5.0 U 5.0 U
5.0 U 5.0 U 5.0 U 5.0 U
5.0 U 5.0 U 5.0 U 5.0 U
170 14 66 28
5.0 U 5.0 U 5.0 U 5.0 U
85 5.0 U 5.0 U 5.0 U
5.0 U 5.0 U 5.0 U 5.0 U
5.0 U 5.0 U 5.0 U 5.0 U
250 5.0 U 5.0 U 5.0 U
5.0 U 5.0 U 5.0 U 5.0 U
5.0 U 5.0 U 5.0 U 5.0 U
5.0 U 5.0 U 5.0 U 5.0 U
12 6.9 5.0 U 7.5
5.0 U 5.0 U 5.0 U 5.0 U
6.9 5.0 U 5.0 U 5.0 U
5.0 U 5.0 U 5.0 U 5.0 U
5.0 U 5.0 U 5.0 U 5.0 U
10 U 10 U 10 U 10 U
5.0 U 5.0 U 5.0 U 5.0 U
5.0 U 5.0 U 5.0 U 5.0 U
5.0 U 5.0 U 5.0 U 5.0 U
5.0 U 5.0 U 5.0 U 5.0 U
5.0 U 5.0 U 5.0 U 5.0 U
5.0 U 5.0 U 5.0 U 5.0 U
5.0 U 5.0 U 5.0 U 5.0 U
5.0 U 5.0 U 5.0 U 5.0 U
5.0 U 5.0 U 5.0 U 5.0 U
5.0 U 5.0 U 5.0 U 5.0 U
5.0 U 5.0 U 5.0 U 5.0 U
5.0 U 5.0 U 5.0 U 5.0 U
10 U 10 U 10 U 10 U
5.0 U 5.0 U 5.0 U 5.0 U
5.0 U 5.0 U 5.0 U 5.0 U
5.0 U 5.0 U 5.0 U 5.0 U
10 U 10 U 10 U 10 U
5.0 U 5.0 U 5.0 U 5.0 U
5.0 U 5.0 U 5.0 U 5.0 U
5.0 U 5.0 U 5.0 U 5.0 U
5.0 U 5.0 U 5.0 U 5.0 U
5.0 U 5.0 U 5.0 U 5.0 U
5.0 U 5.0 U 5.0 U 5.0 U
14 5.0 U 5.0 U 5.0 U
5.0 U 5.0 U 5.0 U 5.0 U
4766ASR Number: 03/29/2010
MP7ES02Project ID: Cleburn Street well samplingProject Desc:
RLAB Approved Sample Analysis Results
Page 19 of 27
Analysis/ Analyte
Trichloroethene
Trichlorofluoromethane
1,1,2-Trichlorotrifluoroethane
Vinyl Chloride
m and/or p-Xylene
o-Xylene
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
Units 203-__ 204-__ 205-__ 206-__
5.0 U 5.0 U 5.0 U 5.0 U
5.0 U 5.0 U 5.0 U 5.0 U
5.0 U 5.0 U 5.0 U 5.0 U
5.0 U 5.0 U 5.0 U 5.0 U
10 U 10 U 10 U 10 U
5.0 U 5.0 U 5.0 U 5.0 U
4766ASR Number: 03/29/2010
MP7ES02Project ID: Cleburn Street well samplingProject Desc:
RLAB Approved Sample Analysis Results
Page 20 of 27
1 VOCs in Water by GC/MS
Analysis/ Analyte
Acetone
Benzene
Bromodichloromethane
Bromoform
Bromomethane
2-Butanone
Carbon Disulfide
Carbon Tetrachloride
Chlorobenzene
Chloroethane
Chloroform
Chloromethane
Cyclohexane
1,2-Dibromo-3-Chloropropane
Dibromochloromethane
1,2-Dibromoethane
1,2-Dichlorobenzene
1,3-Dichlorobenzene
1,4-Dichlorobenzene
Dichlorodifluoromethane
1,1-Dichloroethane
1,2-Dichloroethane
1,1-Dichloroethene
cis-1,2-Dichloroethene
trans-1,2-Dichloroethene
1,2-Dichloropropane
cis-1,3-Dichloropropene
trans-1,3-Dichloropropene
Ethyl Benzene
2-Hexanone
Isopropylbenzene
Methyl Acetate
Methyl tert-butyl ether
Methylcyclohexane
Methylene Chloride
4-Methyl-2-Pentanone
Naphthalene
Styrene
1,1,2,2-Tetrachloroethane
Tetrachloroethene
Toluene
1,2,3-Trichlorobenzene
1,2,4-Trichlorobenzene
1,1,1-Trichloroethane
1,1,2-Trichloroethane
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
Units 207-__ 208-__ 209-__ 210-__
190 J 250 310 J 390 J
5.0 U 5.0 U 5.0 U 5.0 U
5.0 U 5.0 U 5.0 U 5.5
5.0 U 5.0 U 5.0 U 5.0 U
5.0 U 5.0 U 5.0 U 5.0 U
39 19 18 33
5.0 U 5.0 U 5.0 U 5.0 U
5.0 U 5.9 21 800
5.0 U 5.0 U 5.0 U 5.0 U
5.0 U 5.0 U 5.0 U 5.0 U
5.0 U 34 5.0 U 44
5.0 U 5.0 U 5.0 U 5.0 U
5.0 U 5.0 U 5.0 U 5.0 U
5.0 U 5.0 U 5.0 U 5.0 U
5.0 U 5.2 5.0 U 5.1
5.0 U 5.0 U 5.0 U 5.0 U
5.0 U 5.0 U 5.0 U 7.0
5.0 U 5.0 U 5.0 U 5.0 U
5.0 U 5.0 U 5.0 U 5.0 U
10 U 10 U 10 U 10 U
5.0 U 5.0 U 5.0 U 5.0 U
5.0 U 5.0 U 5.0 U 5.0 U
5.0 U 5.0 U 5.0 U 5.0 U
5.0 U 5.0 U 5.0 U 5.0 U
5.0 U 5.0 U 5.0 U 5.0 U
5.0 U 5.0 U 5.0 U 5.0 U
5.0 U 5.0 U 5.0 U 5.0 U
5.0 U 5.0 U 5.0 U 5.0 U
5.0 U 5.0 U 5.0 U 5.0 U
5.0 U 5.0 U 5.0 U 5.0 U
5.0 U 5.0 U 5.0 U 5.0 U
5.0 U 5.0 U 5.0 U 5.0 U
10 U 10 U 10 U 10 U
5.0 U 5.0 U 5.0 U 5.0 U
5.0 U 5.0 U 5.0 U 5.0 U
5.0 U 5.0 U 5.0 U 5.0 U
10 U 10 U 10 U 10 U
5.0 U 5.0 U 5.0 U 5.0 U
5.0 U 5.0 U 5.0 U 5.0 U
5.0 U 5.0 U 5.0 U 5.0 U
5.0 U 5.0 U 5.0 U 5.0 U
5.0 U 5.0 U 5.0 U 5.0 U
5.0 U 5.0 U 5.0 U 5.0 U
5.0 U 5.5 5.0 U 25
5.0 U 5.0 U 5.0 U 5.0 U
4766ASR Number: 03/29/2010
MP7ES02Project ID: Cleburn Street well samplingProject Desc:
RLAB Approved Sample Analysis Results
Page 21 of 27
Analysis/ Analyte
Trichloroethene
Trichlorofluoromethane
1,1,2-Trichlorotrifluoroethane
Vinyl Chloride
m and/or p-Xylene
o-Xylene
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
Units 207-__ 208-__ 209-__ 210-__
5.0 U 5.0 U 5.0 U 5.0 U
5.0 U 5.0 U 5.0 U 5.0 U
5.0 U 5.0 U 5.0 U 5.0 U
5.0 U 5.0 U 5.0 U 5.0 U
10 U 10 U 10 U 10 U
5.0 U 5.0 U 5.0 U 5.0 U
4766ASR Number: 03/29/2010
MP7ES02Project ID: Cleburn Street well samplingProject Desc:
RLAB Approved Sample Analysis Results
Page 22 of 27
1 VOCs in Water by GC/MS
Analysis/ Analyte
Acetone
Benzene
Bromodichloromethane
Bromoform
Bromomethane
2-Butanone
Carbon Disulfide
Carbon Tetrachloride
Chlorobenzene
Chloroethane
Chloroform
Chloromethane
Cyclohexane
1,2-Dibromo-3-Chloropropane
Dibromochloromethane
1,2-Dibromoethane
1,2-Dichlorobenzene
1,3-Dichlorobenzene
1,4-Dichlorobenzene
Dichlorodifluoromethane
1,1-Dichloroethane
1,2-Dichloroethane
1,1-Dichloroethene
cis-1,2-Dichloroethene
trans-1,2-Dichloroethene
1,2-Dichloropropane
cis-1,3-Dichloropropene
trans-1,3-Dichloropropene
Ethyl Benzene
2-Hexanone
Isopropylbenzene
Methyl Acetate
Methyl tert-butyl ether
Methylcyclohexane
Methylene Chloride
4-Methyl-2-Pentanone
Naphthalene
Styrene
1,1,2,2-Tetrachloroethane
Tetrachloroethene
Toluene
1,2,3-Trichlorobenzene
1,2,4-Trichlorobenzene
1,1,1-Trichloroethane
1,1,2-Trichloroethane
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
Units 211-__ 212-__ 213-__ 214-__
500 5.0 U 88 5.0 U
5.0 U 5.0 U 5.0 U 5.0 U
15 5.0 U 5.0 U 5.0 U
5.0 U 5.0 U 5.0 U 5.0 U
5.0 U 5.0 U 5.0 U 5.0 U
36 5.0 U 14 5.0 U
5.0 U 5.0 U 5.0 U 5.0 U
250 5.0 U 23 5.0 U
5.0 U 5.0 U 5.0 U 5.0 U
5.0 U 5.0 U 5.0 U 5.0 U
170 5.0 U 19 5.0 U
5.0 U 5.0 U 5.0 U 5.0 U
5.0 U 5.0 U 5.0 U 10
5.0 U 5.0 U 5.0 U 5.0 U
9.2 5.0 U 5.0 U 5.0 U
5.0 U 5.0 U 5.0 U 5.0 U
18 5.0 U 5.0 U 5.0 U
5.0 U 5.0 U 5.0 U 5.0 U
5.0 U 5.0 U 5.0 U 5.0 U
10 U 10 U 10 U 10 U
5.0 U 5.0 U 5.0 U 5.0 U
5.0 U 5.0 U 5.0 U 5.0 U
5.0 U 5.0 U 5.0 U 5.0 U
5.0 U 5.0 U 5.0 U 21
5.0 U 5.0 U 5.0 U 5.0 U
5.0 U 5.0 U 5.0 U 5.0 U
5.0 U 5.0 U 5.0 U 5.0 U
5.0 U 5.0 U 5.0 U 5.0 U
5.0 U 5.0 U 5.0 U 9.8
5.0 U 5.0 U 5.0 U 5.0 U
5.0 U 5.0 U 5.0 U 5.0 U
5.0 U 5.0 U 5.0 U 5.0 U
10 U 10 U 10 U 10 U
5.0 U 5.0 U 5.0 U 5.0 U
5.0 U 5.0 U 5.0 U 5.0 U
5.0 U 5.0 U 5.0 U 5.0 U
10 U 10 U 10 U 15
5.0 U 5.0 U 5.0 U 5.0 U
5.0 U 5.0 U 5.0 U 5.0 U
5.0 U 5.0 U 1700 2200
5.0 U 5.0 U 5.0 U 6.5
5.0 U 5.0 U 5.0 U 5.0 U
5.0 U 5.0 U 5.0 U 5.0 U
19 5.0 U 24 5.0 U
5.0 U 5.0 U 5.0 U 5.0 U
4766ASR Number: 03/29/2010
MP7ES02Project ID: Cleburn Street well samplingProject Desc:
RLAB Approved Sample Analysis Results
Page 23 of 27
Analysis/ Analyte
Trichloroethene
Trichlorofluoromethane
1,1,2-Trichlorotrifluoroethane
Vinyl Chloride
m and/or p-Xylene
o-Xylene
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
Units 211-__ 212-__ 213-__ 214-__
5.0 U 5.0 U 5.0 U 200
5.0 U 5.0 U 5.0 U 5.0 U
5.0 U 5.0 U 5.0 U 5.0 U
5.0 U 5.0 U 5.0 U 5.0 U
10 U 10 U 10 U 32
5.0 U 5.0 U 5.0 U 11
4766ASR Number: 03/29/2010
MP7ES02Project ID: Cleburn Street well samplingProject Desc:
RLAB Approved Sample Analysis Results
Page 24 of 27
1 VOCs in Water by GC/MS
Analysis/ Analyte
Acetone
Benzene
Bromodichloromethane
Bromoform
Bromomethane
2-Butanone
Carbon Disulfide
Carbon Tetrachloride
Chlorobenzene
Chloroethane
Chloroform
Chloromethane
Cyclohexane
1,2-Dibromo-3-Chloropropane
Dibromochloromethane
1,2-Dibromoethane
1,2-Dichlorobenzene
1,3-Dichlorobenzene
1,4-Dichlorobenzene
Dichlorodifluoromethane
1,1-Dichloroethane
1,2-Dichloroethane
1,1-Dichloroethene
cis-1,2-Dichloroethene
trans-1,2-Dichloroethene
1,2-Dichloropropane
cis-1,3-Dichloropropene
trans-1,3-Dichloropropene
Ethyl Benzene
2-Hexanone
Isopropylbenzene
Methyl Acetate
Methyl tert-butyl ether
Methylcyclohexane
Methylene Chloride
4-Methyl-2-Pentanone
Naphthalene
Styrene
1,1,2,2-Tetrachloroethane
Tetrachloroethene
Toluene
1,2,3-Trichlorobenzene
1,2,4-Trichlorobenzene
1,1,1-Trichloroethane
1,1,2-Trichloroethane
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
Units 215-__ 216-__ 217-__ 218-__
5.0 U 24 U 250 49
5.0 U 5.0 U 5.0 U 5.0 U
5.0 U 5.0 U 5.0 U 5.0 U
5.0 U 5.0 U 5.0 U 5.0 U
5.0 U 5.0 U 5.0 U 5.0 U
5.0 U 5.0 U 95 68
5.0 U 5.0 U 5.0 U 5.0 U
5.0 U 5.0 U 28 5.0 U
5.0 U 5.0 U 5.0 U 5.0 U
5.0 U 5.0 U 5.0 U 5.0 U
5.0 U 5.0 U 120 5.0 U
5.0 U 5.0 U 5.0 U 5.0 U
5.0 U 5.0 U 5.0 U 5.0 U
5.0 U 5.0 U 5.0 U 5.0 U
5.0 U 5.0 U 5.0 U 5.0 U
5.0 U 5.0 U 5.0 U 5.0 U
5.0 U 5.0 U 5.0 U 5.0 U
5.0 U 5.0 U 5.0 U 5.0 U
5.0 U 5.0 U 5.0 U 5.0 U
10 U 10 U 10 U 10 U
5.0 U 5.0 U 5.0 U 5.0 U
5.0 U 5.0 U 5.0 U 5.0 U
5.0 U 5.0 U 5.0 U 5.0 U
5.0 U 5.0 U 5.0 U 5.0 U
5.0 U 5.0 U 5.0 U 5.0 U
5.0 U 5.0 U 5.0 U 5.0 U
5.0 U 5.0 U 5.0 U 5.0 U
5.0 U 5.0 U 5.0 U 5.0 U
5.0 U 5.0 U 5.0 U 5.0 U
5.0 U 5.0 U 5.0 U 5.0 U
5.0 U 5.0 U 5.0 U 5.0 U
5.0 U 5.0 U 5.0 U 5.0 U
10 U 10 U 10 U 10 U
5.0 U 5.0 U 5.0 U 5.0 U
5.0 U 5.0 U 5.0 U 5.0 U
5.0 U 5.0 U 5.0 U 5.0 U
10 U 10 U 10 U 10 U
5.0 U 5.0 U 5.0 U 5.0 U
5.0 U 5.0 U 5.0 U 5.0 U
10 5.0 U 5.0 U 5.0 U
5.0 U 5.0 U 5.0 U 5.0 U
5.0 U 5.0 U 5.0 U 5.0 U
5.0 U 5.0 U 5.0 U 5.0 U
5.0 U 5.0 U 5.0 U 5.0 U
5.0 U 5.0 U 5.0 U 5.0 U
4766ASR Number: 03/29/2010
MP7ES02Project ID: Cleburn Street well samplingProject Desc:
RLAB Approved Sample Analysis Results
Page 25 of 27
Analysis/ Analyte
Trichloroethene
Trichlorofluoromethane
1,1,2-Trichlorotrifluoroethane
Vinyl Chloride
m and/or p-Xylene
o-Xylene
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
Units 215-__ 216-__ 217-__ 218-__
5.0 U 5.0 U 5.0 U 5.0 U
5.0 U 5.0 U 5.0 U 5.0 U
5.0 U 5.0 U 5.0 U 5.0 U
5.0 U 5.0 U 5.0 U 5.0 U
10 U 10 U 10 U 10 U
5.0 U 5.0 U 5.0 U 5.0 U
4766ASR Number: 03/29/2010
MP7ES02Project ID: Cleburn Street well samplingProject Desc:
RLAB Approved Sample Analysis Results
Page 26 of 27
1 VOCs in Water by GC/MS
Analysis/ Analyte
Acetone
Benzene
Bromodichloromethane
Bromoform
Bromomethane
2-Butanone
Carbon Disulfide
Carbon Tetrachloride
Chlorobenzene
Chloroethane
Chloroform
Chloromethane
Cyclohexane
1,2-Dibromo-3-Chloropropane
Dibromochloromethane
1,2-Dibromoethane
1,2-Dichlorobenzene
1,3-Dichlorobenzene
1,4-Dichlorobenzene
Dichlorodifluoromethane
1,1-Dichloroethane
1,2-Dichloroethane
1,1-Dichloroethene
cis-1,2-Dichloroethene
trans-1,2-Dichloroethene
1,2-Dichloropropane
cis-1,3-Dichloropropene
trans-1,3-Dichloropropene
Ethyl Benzene
2-Hexanone
Isopropylbenzene
Methyl Acetate
Methyl tert-butyl ether
Methylcyclohexane
Methylene Chloride
4-Methyl-2-Pentanone
Naphthalene
Styrene
1,1,2,2-Tetrachloroethane
Tetrachloroethene
Toluene
1,2,3-Trichlorobenzene
1,2,4-Trichlorobenzene
1,1,1-Trichloroethane
1,1,2-Trichloroethane
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
Units 219-__ 220-__
180 150
5.0 U 5.0 U
5.2 5.0 U
5.0 U 5.0 U
5.0 U 5.0 U
25 99
5.0 U 5.0 U
42 5.0 U
5.0 U 5.0 U
5.0 U 5.0 U
130 5.0 U
5.0 U 5.0 U
5.0 U 5.0 U
5.0 U 5.0 U
5.0 U 5.0 U
5.0 U 5.0 U
5.0 U 5.0 U
5.0 U 5.0 U
5.0 U 5.0 U
10 U 10 U
5.0 U 5.0 U
5.0 U 5.0 U
5.0 U 5.0 U
5.0 U 5.0 U
5.0 U 5.0 U
5.0 U 5.0 U
5.0 U 5.0 U
5.0 U 5.0 U
5.0 U 5.0 U
5.0 U 5.0 U
5.0 U 5.0 U
5.0 U 5.0 U
10 U 10 U
5.0 U 5.0 U
5.0 U 5.0 U
5.0 U 5.0 U
10 U 10 U
5.0 U 5.0 U
5.0 U 5.0 U
5.0 U 5.0 U
5.0 U 5.0 U
5.0 U 5.0 U
5.0 U 5.0 U
35 5.0 U
5.0 U 5.0 U
4766ASR Number: 03/29/2010
MP7ES02Project ID: Cleburn Street well samplingProject Desc:
RLAB Approved Sample Analysis Results
Page 27 of 27
Analysis/ Analyte
Trichloroethene
Trichlorofluoromethane
1,1,2-Trichlorotrifluoroethane
Vinyl Chloride
m and/or p-Xylene
o-Xylene
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
Units 219-__ 220-__
5.0 U 5.0 U
5.0 U 5.0 U
5.0 U 5.0 U
5.0 U 5.0 U
10 U 10 U
5.0 U 5.0 U
4766ASR Number: 03/29/2010
MP7ES02Project ID: Cleburn Street well samplingProject Desc:
RLAB Approved Sample Analysis Results
4766
MP7ES02Project ID:
Cleburn Street well sampling
Mary PetersonSUPR/IANE
United States Environmental Protection AgencyRegion VII
901 N. 5th StreetKansas City, KS 66101
__/__/____
Data Disposition/Sample Release for ASR #:
Project Description:
Subject:
Kaye DollmannENSV/RLAB
I have received and reviewed the Transmittal of Sample Analysis Results for the above-referencedAnalytical Services Request(ASR) and have indicated my findings below by checking one of theboxes for Data Disposition.
I understand all samples will be disposed upon receipt of this form, unless samples are requestedto be held. If I do not return this form all samples will be disposed of on ___________________.
"RELEASED" - Read-only to all Region 7 employees and contractors that have R7LIMS"Customer" account. All Samples may be disposed of upon receipt of this form if not requested tobe held.
"Project Manager Accessible" - Available on the LAN in R7LIMS for my use only. All Samples maybe disposed of upon receipt of this form if not requested to be held.
"Archived" - THIS DATA IS OF A SENSITIVE NATURE. Any future reports must be requestedthrough the laboratory. All samples may be disposed of upon receipt of the form if not requestedto be held.
Date:
From:
To:
Hold Samples - I have determined that the samples need to be held until ______________, afterwhich time they will be disposed of in accordance with applicable regulations. The reason for the hold is:
Samples are associated with a legal proceeding.
Question/Concern with data - possible reanalysis requested.
Other:________________________________________________________________
MARCH 2010
Page 1 of 27
03/30/2010Date:
4818
MP7ES02
Cleburn Street well sampling
Mary PetersonSUPR/IANE
Transmittal of Sample Analysis Results for ASR #:
Project ID:
Project Description:
Michael F. Davis, ChiefChemical Analysis and Response Branch, Environmental Services Division
To:
Enclosed are the analytical data for the above-referenced Analytical Services Request (ASR) andProject. The Regional Laboratory has reviewed and verified the results in accordance with proceduresdescribed in our Quality Manual (QM). In addition to all of the analytical results, this transmittalcontains pertinent information that may have influenced the reported results and documents anydeviations from the established requirements of the QM.
Please contact us within 14 days of receipt of this package if you determine there is a need for anychanges. Please complete the enclosed Customer Satisfaction Survey and Data Disposition/SampleRelease memo for this ASR as soon as possible. The process of disposing of the samples for this ASRwill be initiated 30 days from the date of this transmittal unless an alternate release date is specifiedon the Data Disposition/Sample Release memo.
If you have any questions or concerns relating to this data package, contact our customer service lineat 913-551-5295.
Enclosures
cc: Analytical Data File.
United States Environmental Protection AgencyRegion 7
901 N. 5th StreetKansas City, KS 66101
Subject:
From:
Page 2 of 27
4818ASR Number: 03/30/2010
Mary Peterson SUPR/IANE 913-551-7882
MP7ES02
Cleburn Street well sampling
Grand Island Nebraska Superfund
CLEBURN STREET WELL - 1 HR MARTINIZING GWRESORATION
07ESSite ID: 02
Site Cleanup Support
2nd round of 1st Injection event.
Project Manager: Org: Phone:
Project ID:
Project Desc:
Location: State: Program:
Site Name: Site OU:
Purpose:
__ = Field SampleFB = Field BlankFD = Field Duplicate
QC Codes identify the type of sample for quality control purpose.
Degrees CelsiusNephelometric Turbidity UnitsStandard Units (pH)Milligrams per LiterMicrograms per LiterMicromhos per Centimeter
Specific units in which results arereported.
The identification of the analyte is acceptable; the reported value is anestimate.The presence or absence of the analyte can not be determined from the datadue to severe quality control problems. The data are rejected andconsidered unusable.The analyte was not detected at or above the reporting limit.The analyte was not detected at or above the reporting limit. The reportinglimit is an estimate.
Specific codes used in conjunction with data values to provide additional information on the quality of reported results, or used to explain the absence of a specific value.
Summary of Project Information
Explanation of Codes, Units and Qualifiers used on this report
Sample QC Codes: Units:
J
R
UUJ
=
=
==
Data Qualifiers:
= Values have been reviewed and found acceptable for use. (Blank)
Deg CNTUSU
mg/Lug/L
umhos/cm
======
2009073QAPP Number:
302DD2CGPRA PRC:
Page 3 of 27
1
2
2
4
5
6
7
8
9
10
11
12
12
14
15
16
17
17
19
20
21
22
23
26
27
28
29
SampleNo
__
__
FD
__
__
__
__
__
__
__
__
__
FD
__
__
__
__
FD
__
__
__
__
__
FB
FB
FB
FB
QCCode
Water
Water
Water
Water
Water
Water
Water
Water
Water
Water
Water
Water
Water
Water
Water
Water
Water
Water
Water
Water
Water
Water
Water
Water
Water
Water
Water
Matrix
IW-1
IW-2
IW-2/Field Duplicate of sample 2
IW-3
IW-4
IW-5
ERT-16
IW-6
IW-7
IW-8
IW-9
IW-10
IW-10/Field Duplicate of sample12DPE-2
DPE-1
MW-2B
MW-2A
MW-2A/Field Duplicate of sample17ERT-15
MW-12A
DPE-4
DPE-3
ERT-14
Preservative Blank sample
VOA Trip Blank sample 1
VOA Trip Blank sample 2
VOA Trip Blank sample 3
Location DescriptionExternal
Sample No
03/01/2010
03/01/2010
03/01/2010
03/01/2010
03/01/2010
03/02/2010
03/02/2010
03/02/2010
03/02/2010
03/02/2010
03/02/2010
03/03/2010
03/03/2010
03/03/2010
03/03/2010
03/03/2010
03/03/2010
03/03/2010
03/04/2010
03/04/2010
03/04/2010
03/04/2010
03/04/2010
03/01/2010
02/24/2010
02/24/2010
02/24/2010
Start Date
11:35
14:25
14:25
17:05
18:00
08:40
10:15
13:25
15:30
18:00
18:55
09:30
09:30
13:46
14:55
16:55
18:25
18:25
08:40
10:15
11:45
13:55
15:10
09:40
15:00
15:05
15:10
Start Time
03/03/2010
03/02/2010
03/01/2010
End Date
09:45
12:40
09:50
End Time
03/02/2010
03/02/2010
03/02/2010
03/03/2010
03/03/2010
03/03/2010
03/03/2010
03/03/2010
03/03/2010
03/04/2010
03/04/2010
03/04/2010
03/04/2010
03/04/2010
03/04/2010
03/05/2010
03/05/2010
03/05/2010
03/05/2010
03/05/2010
03/05/2010
03/05/2010
03/05/2010
03/02/2010
03/04/2010
03/03/2010
03/02/2010
ReceiptDate
4818 03/30/2010
MP7ES02Project ID: Cleburn Street well samplingProject Desc:
ASR Number: Sample Information Summary
-
-
-
-
-
-
-
-
-
-
-
-
-
-
-
-
-
-
-
-
-
-
-
-
-
-
-
Page 4 of 27
1
1
1
1
Alkalinity in Water by Titration
Anions in Water by Ion Chromatography
Conductivity by Field Measurement
Hardness in Water by Calculation
Region 7 EPA Laboratory - Kansas City, Ks.
Region 7 ESAT Contract Lab (In-House)
(Field Measurement)
Region 7 ESAT Contract Lab (In-House)
Lab:
Lab:
Lab:
Lab:
EPA Region 7 RLAB Method 3132.1E
Region 7 RLAB Method 3135.12A
Measurement of field parameter
EPA Region 7 RLAB Method 3122.3C
Method:
Method:
Method:
Method:
Dilutions were necessary in order to obtain valid results and prevent instrumentdamage due to matrix interferences for samples 1, 2, 2 FD, 4, 5, 6, 7, 8, 9, 10, 11, 12, 12FD, 14, 15, 17, 17 FD, 21, and 22 . This increased the reporting limits by a factor of 10000for these samples.
(N/A)
Comments:
Comments:
Comments:
1-__ 2-__ 2-FD 4-__ 5-__ 6-__ 7-__8-__ 9-__ 10-__ 11-__ 12-__ 12-FD 14-__15-__ 16-__ 17-__ 17-FD 19-__ 20-__ 21-__22-__ 23-__
1-__ 2-__ 2-FD 4-__ 5-__ 6-__ 7-__8-__ 9-__ 10-__ 11-__ 12-__ 12-FD 14-__15-__ 16-__ 17-__ 17-FD 19-__ 20-__ 21-__22-__ 23-__
1-__ 2-__ 2-FD 4-__ 5-__ 6-__ 7-__8-__ 9-__ 10-__ 11-__ 12-__ 12-FD 14-__15-__ 16-__ 17-__ 17-FD 19-__ 20-__ 21-__22-__ 23-__
1-__ 2-__ 2-FD 4-__ 5-__ 6-__ 7-__8-__ 9-__ 10-__ 11-__ 12-__ 12-FD 14-__15-__ 16-__ 17-__ 17-FD 19-__ 20-__ 21-__22-__ 23-__
Samples:
Samples:
Samples:
Samples:
4818ASR Number: 03/30/2010
MP7ES02Project ID: Cleburn Street well samplingProject Desc
RLAB Approved Analysis Comments
Analysis Comments About Results For This Analysis
Page 5 of 27
1
1
1
1
Metals in Water by ICP-AES
pH of Water by Field Measurement
TDS or Total Dissolved Solids
Temperature of Water by Field Measurement
Region 7 ESAT Contract Lab (In-House)
(Field Measurement)
Region 7 EPA Laboratory - Kansas City, Ks.
Lab:
Lab:
Lab:
EPA Region 7 RLAB Method 3122.3C
Measurement of field parameter
EPA Region 7 RLAB Method 3142.2B
Method:
Method:
Method:
Dilutions were necessary in order to obtain valid results due to matrix interferences forsamples 1, 2, 2FD, 4-12, 12FD, 13-15, 17, 17FD, 21, and 22. This increased the reportinglimits by a factor of 100 for these samples.
Nickel (102, 85-101) was J-coded in samples 17, 17FD, 20, and 19. Although the analytein question has been positively identified in the samples, the quantitation is an estimate (J-coded) due to high recovery of this analyte in the laboratory control sample, 951LCS. Theactual concentration for this analyte may be lower than the reported value.
(N/A)
(N/A)
Comments:
Comments:
Comments:
Comments:
1-__ 2-__ 2-FD 4-__ 5-__ 6-__ 7-__8-__ 9-__ 10-__ 11-__ 12-__ 12-FD 14-__15-__ 16-__ 17-__ 17-FD 19-__ 20-__ 21-__22-__ 23-__ 26-FB
1-__ 2-__ 2-FD 4-__ 5-__ 6-__ 7-__8-__ 9-__ 10-__ 11-__ 12-__ 12-FD 14-__15-__ 16-__ 17-__ 17-FD 19-__ 20-__ 21-__22-__ 23-__
1-__ 2-__ 2-FD 4-__ 5-__ 6-__ 7-__8-__ 9-__ 10-__ 11-__ 12-__ 12-FD 14-__15-__ 16-__ 17-__ 17-FD 19-__ 20-__ 21-__22-__ 23-__
Samples:
Samples:
Samples:
4818ASR Number: 03/30/2010
MP7ES02Project ID: Cleburn Street well samplingProject Desc
RLAB Approved Analysis Comments
Analysis Comments About Results For This Analysis
Page 6 of 27
1
1
Total Organic Carbon in Water
Turbidity of Water by Field Measurement
(Field Measurement)
RASP Contract Lab (Out-Source)
(Field Measurement)
Lab:
Lab:
Lab:
Measurement of field parameter
Similar to EPA SW846 Method 9060 or StandardMethods (20th Edtion) 5310 B, C,or D (see comments)
Measurement of field parameter
Method:
Method:
Method:
(N/A)
MS/MSD analysis was performed on samples 4818-1, 4818-9, 4818-10, & 4818-16 (due tomultiple sample shipments). The MS and/or MSD recoveries for sample 4818-1 (82% /74%), 4818-9 (11% / 5%), & 4818-10 (67% / 59%) were below the lower control limit of80%. Calculated RPD's and all LCS recoveries were within applicable control limits.TOCwas J-coded in samples 4818-1, 4818-9, & 4818-10. Although the analyte in question hasbeen positively identified in the samples, the quantitation is an estimate (J-coded) due tolow recovery of this analyte in the laboratory matrix spike. The actual concentration forthis analyte may be higher than the reported value.
A laboratory duplicate (LD) analysis was performed on sample 4818-10. The calculated %difference of 43% between 4818-10 & 4818-10LD was outside the control limit of 20%.TOC was J-coded in sample 4818-10. Although the analyte in question has been positivelyidentified in the sample, the quantitation is an estimate (J-coded) due to poor precisionobtained for this analyte in the laboratory duplicate sample.
(N/A)
Comments:
Comments:
Comments:
1-__ 2-__ 2-FD 4-__ 5-__ 6-__ 7-__8-__ 9-__ 10-__ 11-__ 12-__ 12-FD 14-__15-__ 16-__ 17-__ 17-FD 19-__ 20-__ 21-__22-__ 23-__
1-__ 2-__ 2-FD 4-__ 5-__ 6-__ 7-__8-__ 9-__ 10-__ 11-__ 12-__ 12-FD 14-__15-__ 16-__ 17-__ 17-FD 19-__ 20-__ 21-__22-__ 23-__ 26-FB
1-__ 2-__ 2-FD 4-__ 5-__ 6-__ 7-__8-__ 9-__ 10-__ 11-__ 12-__ 12-FD 14-__15-__ 16-__ 17-__ 17-FD 19-__ 20-__ 21-__22-__ 23-__
Samples:
Samples:
Samples:
4818ASR Number: 03/30/2010
MP7ES02Project ID: Cleburn Street well samplingProject Desc
RLAB Approved Analysis Comments
Analysis Comments About Results For This Analysis
Page 7 of 27
1 VOCs in Water by GC/MS
Region 7 ESAT Contract Lab (In-House)Lab:
EPA Region 7 RLAB Method 3230.1FMethod:
Nineteen of the samples contained potassium permanganate. These samples were dilutedto keep the column from being damaged. The resulting reporting limit for these sampleswas higher than the normal reporting limit. Dichlorodifluoromethane (+25.5%) was UJ-coded in samples 26-FB, 27-FB, 28-FB, 29-FB,16, 20, 19, 1, 2, 2-FD, 4, 5, 6, 7, 8, 9, and 10. This analyte was not found in the samplesat or above the reporting limit, however, the reporting limit is an estimate (UJ-coded) dueto the continuing calibration check not meeting accuracy specifications. The actualreporting limit for this analyte may be higher than the reported value. Styrene was reported with a N/A and a R-code since it was not recovered in the matrixspike or duplicate. The potassium permanganate in the diluted sample is probably whyStyrene did not recover. Styrene had unacceptable response in the laboratory matrix spikeindicating that it was not possible to obtain valid results for this analyte. Results of 'N/A'were reported with a R-code for samples 1. trans-1,2-Dichloroethene (3% & 2%, 82%-121%), cis-1,3-Dichloropropene (17% & 15%,82%-113%), trans-1,3-Dichloropropene (2% & 1%, 84%-117%), and Vinyl Chloride (12%& 10%, 77%-120%) were UJ coded in sample 1. These analytes were not found in thesample at or above the reporting limit, however, the reporting limit is an estimate (UJ-coded) due to low recovery of these analytes in the laboratory matrix spike. The actualreporting limit for these analytes may be higher than the reported value. The low recoveryis probably due to the potassium permanganate that was present in the diluted sample. trans-1,2-Dichloroethene (33RPD, 10PCL), cis-1,3-Dichloropropene (15RPD, 7.8PCL),trans-1,3-Dichloropropene (35RPD, 8.5PCL), Methyl tert-butyl ether (6.2RPD, 5..4PCL), andVinyl Chloride (20RPD, 13PCL) were UJ-coded in sample 1. These analytes were not foundin the sample at or above the reporting limit, however, the reporting limit is an estimate(UJ-coded) due to poor precision obtained for these analytes in the laboratory matrix spikeand matrix spike duplicate. The actual reporting limit for these analytes may be higherthan the reported value.
Comments:
1-__ 2-__ 2-FD 4-__ 5-__ 6-__ 7-__8-__ 9-__ 10-__ 11-__ 12-__ 12-FD 14-__15-__ 16-__ 17-__ 17-FD 19-__ 20-__ 21-__22-__ 23-__ 26-FB 27-FB 28-FB 29-FB
Samples:
4818ASR Number: 03/30/2010
MP7ES02Project ID: Cleburn Street well samplingProject Desc
RLAB Approved Analysis Comments
Analysis Comments About Results For This Analysis
Page 8 of 27
1
1
1
1
1
1
1
1
1
1
1
Alkalinity in Water by Titration
Anions in Water by Ion Chromatography
Conductivity by Field Measurement
Hardness in Water by Calculation
Metals in Water by ICP-AES
pH of Water by Field Measurement
TDS or Total Dissolved Solids
Temperature of Water by Field Measurement
Total Organic Carbon in Water
Turbidity of Water by Field Measurement
VOCs in Water by GC/MS
Analysis/ Analyte
Alkalinity, total
Sulfate
Conductivity
Hardness as CaCO3
Aluminum
Antimony
Arsenic
Barium
Beryllium
Cadmium
Calcium
Chromium
Cobalt
Copper
Iron
Lead
Magnesium
Manganese
Molybdenum
Nickel
Potassium
Selenium
Silver
Sodium
Thallium
Titanium
Vanadium
Zinc
pH
Solids, total dissolved
Temperature
Total Organic Carbon
Turbidity
Acetone
Benzene
mg/L
mg/L
umhos/cm
mg/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
mg/L
ug/L
ug/L
ug/L
ug/L
ug/L
mg/L
ug/L
ug/L
ug/L
mg/L
ug/L
ug/L
mg/L
ug/L
ug/L
ug/L
ug/L
SU
mg/L
Deg C
mg/L
NTU
ug/L
ug/L
Units 1-__ 2-__ 2-FD 4-__
218 202 202 259
10000 U 10000 U 10000 U 10000 U
3110 3960 3960 4590
1370 1320 U 1320 U 1320 U
5000 U 5000 U 5000 U 5000 U
5000 U 5000 U 5000 U 5000 U
2500 U 2500 U 2500 U 2500 U
1000 U 1000 U 1000 U 1000 U
300 U 300 U 300 U 300 U
300 U 300 U 300 U 300 U
218 200 U 200 U 200 U
1500 U 1500 U 1500 U 1500 U
1000 U 1000 U 1000 U 1000 U
500 U 500 U 500 U 500 U
5000 U 5000 U 5000 U 5000 U
5000 U 5000 U 5000 U 5000 U
200 U 200 U 200 U 200 U
364000 370000 361000 332000
1500 U 1500 U 1500 U 1500 U
2000 U 2000 U 2000 U 2000 U
1210 1280 1170 1140
5000 U 5000 U 5000 U 5000 U
2500 U 2500 U 2500 U 2500 U
500 U 500 U 500 U 500 U
5000 U 5000 U 5000 U 5000 U
2000 U 2000 U 2000 U 2000 U
1000 U 1000 U 1000 U 1000 U
2500 U 2500 U 2500 U 2500 U
7.26 7.26 7.26 7.56
6150 6450 6450 7060
11.72 11.74 11.74 12.03
1.27 J 1.89 1.71 1.63
1.6 4.2 4.2 9.63
25000 U 25000 U 25000 U 25000 U
25000 U 25000 U 25000 U 25000 U
4818ASR Number: 03/30/2010
MP7ES02Project ID: Cleburn Street well samplingProject Desc:
RLAB Approved Sample Analysis Results
Page 9 of 27
Analysis/ Analyte
Bromodichloromethane
Bromoform
Bromomethane
2-Butanone
Carbon Disulfide
Carbon Tetrachloride
Chlorobenzene
Chloroethane
Chloroform
Chloromethane
Cyclohexane
1,2-Dibromo-3-Chloropropane
Dibromochloromethane
1,2-Dibromoethane
1,2-Dichlorobenzene
1,3-Dichlorobenzene
1,4-Dichlorobenzene
Dichlorodifluoromethane
1,1-Dichloroethane
1,2-Dichloroethane
1,1-Dichloroethene
cis-1,2-Dichloroethene
trans-1,2-Dichloroethene
1,2-Dichloropropane
cis-1,3-Dichloropropene
trans-1,3-Dichloropropene
Ethyl Benzene
2-Hexanone
Isopropylbenzene
Methyl Acetate
Methyl tert-butyl ether
Methylcyclohexane
Methylene Chloride
4-Methyl-2-Pentanone
Naphthalene
Styrene
1,1,2,2-Tetrachloroethane
Tetrachloroethene
Toluene
1,2,3-Trichlorobenzene
1,2,4-Trichlorobenzene
1,1,1-Trichloroethane
1,1,2-Trichloroethane
Trichloroethene
Trichlorofluoromethane
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
Units 1-__ 2-__ 2-FD 4-__
25000 U 25000 U 25000 U 25000 U
25000 U 25000 U 25000 U 25000 U
25000 U 25000 U 25000 U 25000 U
25000 U 25000 U 25000 U 25000 U
25000 U 25000 U 25000 U 25000 U
25000 U 25000 U 25000 U 25000 U
25000 U 25000 U 25000 U 25000 U
25000 U 25000 U 25000 U 25000 U
25000 U 25000 U 25000 U 25000 U
25000 U 25000 U 25000 U 25000 U
25000 U 25000 U 25000 U 25000 U
25000 U 25000 U 25000 U 25000 U
25000 U 25000 U 25000 U 25000 U
25000 U 25000 U 25000 U 25000 U
25000 U 25000 U 25000 U 25000 U
25000 U 25000 U 25000 U 25000 U
25000 U 25000 U 25000 U 25000 U
25000 UJ 25000 UJ 25000 UJ 25000 UJ
25000 U 25000 U 25000 U 25000 U
25000 U 25000 U 25000 U 25000 U
25000 U 25000 U 25000 U 25000 U
25000 U 25000 U 25000 U 25000 U
25000 UJ 25000 U 25000 U 25000 U
25000 U 25000 U 25000 U 25000 U
25000 UJ 25000 U 25000 U 25000 U
25000 UJ 25000 U 25000 U 25000 U
25000 U 25000 U 25000 U 25000 U
25000 U 25000 U 25000 U 25000 U
25000 U 25000 U 25000 U 25000 U
25000 U 25000 U 25000 U 25000 U
50000 UJ 50000 U 50000 U 50000 U
25000 U 25000 U 25000 U 25000 U
25000 U 25000 U 25000 U 25000 U
25000 U 25000 U 25000 U 25000 U
50000 U 50000 U 50000 U 50000 U
N/A R 25000 U 25000 U 25000 U
25000 U 25000 U 25000 U 25000 U
25000 U 25000 U 25000 U 25000 U
25000 U 25000 U 25000 U 25000 U
25000 U 25000 U 25000 U 25000 U
25000 U 25000 U 25000 U 25000 U
25000 U 25000 U 25000 U 25000 U
25000 U 25000 U 25000 U 25000 U
25000 U 25000 U 25000 U 25000 U
25000 U 25000 U 25000 U 25000 U
4818ASR Number: 03/30/2010
MP7ES02Project ID: Cleburn Street well samplingProject Desc:
RLAB Approved Sample Analysis Results
Page 10 of 27
Analysis/ Analyte
1,1,2-Trichlorotrifluoroethane
Vinyl Chloride
m and/or p-Xylene
o-Xylene
ug/L
ug/L
ug/L
ug/L
Units 1-__ 2-__ 2-FD 4-__
25000 U 25000 U 25000 U 25000 U
25000 UJ 25000 U 25000 U 25000 U
50000 U 50000 U 50000 U 50000 U
25000 U 25000 U 25000 U 25000 U
4818ASR Number: 03/30/2010
MP7ES02Project ID: Cleburn Street well samplingProject Desc:
RLAB Approved Sample Analysis Results
Page 11 of 27
1
1
1
1
1
1
1
1
1
1
1
Alkalinity in Water by Titration
Anions in Water by Ion Chromatography
Conductivity by Field Measurement
Hardness in Water by Calculation
Metals in Water by ICP-AES
pH of Water by Field Measurement
TDS or Total Dissolved Solids
Temperature of Water by Field Measurement
Total Organic Carbon in Water
Turbidity of Water by Field Measurement
VOCs in Water by GC/MS
Analysis/ Analyte
Alkalinity, total
Sulfate
Conductivity
Hardness as CaCO3
Aluminum
Antimony
Arsenic
Barium
Beryllium
Cadmium
Calcium
Chromium
Cobalt
Copper
Iron
Lead
Magnesium
Manganese
Molybdenum
Nickel
Potassium
Selenium
Silver
Sodium
Thallium
Titanium
Vanadium
Zinc
pH
Solids, total dissolved
Temperature
Total Organic Carbon
Turbidity
Acetone
Benzene
mg/L
mg/L
umhos/cm
mg/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
mg/L
ug/L
ug/L
ug/L
ug/L
ug/L
mg/L
ug/L
ug/L
ug/L
mg/L
ug/L
ug/L
mg/L
ug/L
ug/L
ug/L
ug/L
SU
mg/L
Deg C
mg/L
NTU
ug/L
ug/L
Units 5-__ 6-__ 7-__ 8-__
289 139 240 156
10000 U 10000 U 10000 U 10000 U
5360 16.30 2470 6250
1320 U 1320 U 1910 2040
5000 U 5000 U 5000 U 5000 U
5000 U 5000 U 5000 U 5000 U
2500 U 2500 U 2500 U 2500 U
1000 U 1000 U 1000 U 1000 U
300 U 300 U 300 U 300 U
300 U 300 U 300 U 300 U
200 U 200 U 437 487
1500 U 1500 U 11000 1500 U
1000 U 1000 U 1000 U 1000 U
500 U 500 U 500 U 500 U
5000 U 5000 U 5000 U 5000 U
5000 U 5000 U 5000 U 5000 U
200 U 200 U 200 U 200 U
420000 349000 308000 402000
1500 U 1500 U 1500 U 1500 U
2000 U 2000 U 5310 2000 U
1590 773 344 664
5000 U 5000 U 5000 U 5000 U
2500 U 2500 U 2500 U 2500 U
500 U 500 U 500 U 500 U
5000 U 5000 U 5000 U 5000 U
2000 U 2000 U 2000 U 2000 U
1000 U 1000 U 1000 U 1000 U
2500 U 2500 U 2500 U 2500 U
7.33 6.01 5.80 5.82
8280 4730 6530 6840
11.83 11.97 11.64 12.00
1.54 1 U 1.94 1.21
3.4 56.4 2.9 2.1
25000 U 25000 U 25000 U 25000 U
25000 U 25000 U 25000 U 25000 U
4818ASR Number: 03/30/2010
MP7ES02Project ID: Cleburn Street well samplingProject Desc:
RLAB Approved Sample Analysis Results
Page 12 of 27
Analysis/ Analyte
Bromodichloromethane
Bromoform
Bromomethane
2-Butanone
Carbon Disulfide
Carbon Tetrachloride
Chlorobenzene
Chloroethane
Chloroform
Chloromethane
Cyclohexane
1,2-Dibromo-3-Chloropropane
Dibromochloromethane
1,2-Dibromoethane
1,2-Dichlorobenzene
1,3-Dichlorobenzene
1,4-Dichlorobenzene
Dichlorodifluoromethane
1,1-Dichloroethane
1,2-Dichloroethane
1,1-Dichloroethene
cis-1,2-Dichloroethene
trans-1,2-Dichloroethene
1,2-Dichloropropane
cis-1,3-Dichloropropene
trans-1,3-Dichloropropene
Ethyl Benzene
2-Hexanone
Isopropylbenzene
Methyl Acetate
Methyl tert-butyl ether
Methylcyclohexane
Methylene Chloride
4-Methyl-2-Pentanone
Naphthalene
Styrene
1,1,2,2-Tetrachloroethane
Tetrachloroethene
Toluene
1,2,3-Trichlorobenzene
1,2,4-Trichlorobenzene
1,1,1-Trichloroethane
1,1,2-Trichloroethane
Trichloroethene
Trichlorofluoromethane
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
Units 5-__ 6-__ 7-__ 8-__
25000 U 25000 U 25000 U 25000 U
25000 U 25000 U 25000 U 25000 U
25000 U 25000 U 25000 U 25000 U
25000 U 25000 U 25000 U 25000 U
25000 U 25000 U 25000 U 25000 U
25000 U 25000 U 25000 U 25000 U
25000 U 25000 U 25000 U 25000 U
25000 U 25000 U 25000 U 25000 U
25000 U 25000 U 25000 U 25000 U
25000 U 25000 U 25000 U 25000 U
25000 U 25000 U 25000 U 25000 U
25000 U 25000 U 25000 U 25000 U
25000 U 25000 U 25000 U 25000 U
25000 U 25000 U 25000 U 25000 U
25000 U 25000 U 25000 U 25000 U
25000 U 25000 U 25000 U 25000 U
25000 U 25000 U 25000 U 25000 U
25000 UJ 25000 UJ 25000 UJ 25000 UJ
25000 U 25000 U 25000 U 25000 U
25000 U 25000 U 25000 U 25000 U
25000 U 25000 U 25000 U 25000 U
25000 U 25000 U 25000 U 25000 U
25000 U 25000 U 25000 U 25000 U
25000 U 25000 U 25000 U 25000 U
25000 U 25000 U 25000 U 25000 U
25000 U 25000 U 25000 U 25000 U
25000 U 25000 U 25000 U 25000 U
25000 U 25000 U 25000 U 25000 U
25000 U 25000 U 25000 U 25000 U
25000 U 25000 U 25000 U 25000 U
50000 U 50000 U 50000 U 50000 U
25000 U 25000 U 25000 U 25000 U
25000 U 25000 U 25000 U 25000 U
25000 U 25000 U 25000 U 25000 U
50000 U 50000 U 50000 U 50000 U
25000 U 25000 U 25000 U 25000 U
25000 U 25000 U 25000 U 25000 U
25000 U 25000 U 25000 U 25000 U
25000 U 25000 U 25000 U 25000 U
25000 U 25000 U 25000 U 25000 U
25000 U 25000 U 25000 U 25000 U
25000 U 25000 U 25000 U 25000 U
25000 U 25000 U 25000 U 25000 U
25000 U 25000 U 25000 U 25000 U
25000 U 25000 U 25000 U 25000 U
4818ASR Number: 03/30/2010
MP7ES02Project ID: Cleburn Street well samplingProject Desc:
RLAB Approved Sample Analysis Results
Page 13 of 27
Analysis/ Analyte
1,1,2-Trichlorotrifluoroethane
Vinyl Chloride
m and/or p-Xylene
o-Xylene
ug/L
ug/L
ug/L
ug/L
Units 5-__ 6-__ 7-__ 8-__
25000 U 25000 U 25000 U 25000 U
25000 U 25000 U 25000 U 25000 U
50000 U 50000 U 50000 U 50000 U
25000 U 25000 U 25000 U 25000 U
4818ASR Number: 03/30/2010
MP7ES02Project ID: Cleburn Street well samplingProject Desc:
RLAB Approved Sample Analysis Results
Page 14 of 27
1
1
1
1
1
1
1
1
1
1
1
Alkalinity in Water by Titration
Anions in Water by Ion Chromatography
Conductivity by Field Measurement
Hardness in Water by Calculation
Metals in Water by ICP-AES
pH of Water by Field Measurement
TDS or Total Dissolved Solids
Temperature of Water by Field Measurement
Total Organic Carbon in Water
Turbidity of Water by Field Measurement
VOCs in Water by GC/MS
Analysis/ Analyte
Alkalinity, total
Sulfate
Conductivity
Hardness as CaCO3
Aluminum
Antimony
Arsenic
Barium
Beryllium
Cadmium
Calcium
Chromium
Cobalt
Copper
Iron
Lead
Magnesium
Manganese
Molybdenum
Nickel
Potassium
Selenium
Silver
Sodium
Thallium
Titanium
Vanadium
Zinc
pH
Solids, total dissolved
Temperature
Total Organic Carbon
Turbidity
Acetone
Benzene
mg/L
mg/L
umhos/cm
mg/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
mg/L
ug/L
ug/L
ug/L
ug/L
ug/L
mg/L
ug/L
ug/L
ug/L
mg/L
ug/L
ug/L
mg/L
ug/L
ug/L
ug/L
ug/L
SU
mg/L
Deg C
mg/L
NTU
ug/L
ug/L
Units 9-__ 10-__ 11-__ 12-__
2.00 U 271 42.4 192
10000 U 10000 U 10000 U 10000 U
7720 4300 8040 6240
1870 1320 U 2050 1320 U
40600 5000 U 9730 5000 U
5000 U 5000 U 5000 U 5000 U
2500 U 2500 U 2500 U 2500 U
1000 U 1000 U 1000 U 1000 U
300 U 300 U 300 U 300 U
300 U 300 U 300 U 300 U
419 200 U 492 200 U
1500 U 1500 U 1500 U 1500 U
1000 U 1000 U 1000 U 1000 U
500 U 500 U 500 U 500 U
5000 U 5000 U 5000 U 5000 U
5000 U 5000 U 5000 U 5000 U
200 U 200 U 200 U 200 U
344000 312000 269000 323000
1500 U 1500 U 1500 U 1500 U
2000 U 2000 U 2000 U 2000 U
928 865 904 1090
5000 U 5000 U 5000 U 5000 U
2500 U 2500 U 2500 U 2500 U
500 U 500 U 500 U 500 U
5000 U 5000 U 5000 U 5000 U
2000 U 2000 U 2000 U 2000 U
1000 U 1000 U 1000 U 1000 U
2500 U 2500 U 2500 U 2500 U
3.58 6.40 4.85 5.72
8340 3670 7390 5540
9.49 11.83 10.23 10.53
2.1 J 2.02 J 1.95 1.63
38.9 0.0 80.3 3.0
25000 U 13000 U 13000 U 25000 U
25000 U 13000 U 13000 U 25000 U
4818ASR Number: 03/30/2010
MP7ES02Project ID: Cleburn Street well samplingProject Desc:
RLAB Approved Sample Analysis Results
Page 15 of 27
Analysis/ Analyte
Bromodichloromethane
Bromoform
Bromomethane
2-Butanone
Carbon Disulfide
Carbon Tetrachloride
Chlorobenzene
Chloroethane
Chloroform
Chloromethane
Cyclohexane
1,2-Dibromo-3-Chloropropane
Dibromochloromethane
1,2-Dibromoethane
1,2-Dichlorobenzene
1,3-Dichlorobenzene
1,4-Dichlorobenzene
Dichlorodifluoromethane
1,1-Dichloroethane
1,2-Dichloroethane
1,1-Dichloroethene
cis-1,2-Dichloroethene
trans-1,2-Dichloroethene
1,2-Dichloropropane
cis-1,3-Dichloropropene
trans-1,3-Dichloropropene
Ethyl Benzene
2-Hexanone
Isopropylbenzene
Methyl Acetate
Methyl tert-butyl ether
Methylcyclohexane
Methylene Chloride
4-Methyl-2-Pentanone
Naphthalene
Styrene
1,1,2,2-Tetrachloroethane
Tetrachloroethene
Toluene
1,2,3-Trichlorobenzene
1,2,4-Trichlorobenzene
1,1,1-Trichloroethane
1,1,2-Trichloroethane
Trichloroethene
Trichlorofluoromethane
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
Units 9-__ 10-__ 11-__ 12-__
25000 U 13000 U 13000 U 25000 U
25000 U 13000 U 13000 U 25000 U
25000 U 13000 U 13000 U 25000 U
25000 U 13000 U 13000 U 25000 U
25000 U 13000 U 13000 U 25000 U
25000 U 13000 U 13000 U 25000 U
25000 U 13000 U 13000 U 25000 U
25000 U 13000 U 13000 U 25000 U
25000 U 13000 U 13000 U 25000 U
25000 U 13000 U 13000 U 25000 U
25000 U 13000 U 13000 U 25000 U
25000 U 13000 U 13000 U 25000 U
25000 U 13000 U 13000 U 25000 U
25000 U 13000 U 13000 U 25000 U
25000 U 13000 U 13000 U 25000 U
25000 U 13000 U 13000 U 25000 U
25000 U 13000 U 13000 U 25000 U
25000 UJ 13000 UJ 13000 U 25000 U
25000 U 13000 U 13000 U 25000 U
25000 U 13000 U 13000 U 25000 U
25000 U 13000 U 13000 U 25000 U
25000 U 13000 U 13000 U 25000 U
25000 U 13000 U 13000 U 25000 U
25000 U 13000 U 13000 U 25000 U
25000 U 13000 U 13000 U 25000 U
25000 U 13000 U 13000 U 25000 U
25000 U 13000 U 13000 U 25000 U
25000 U 13000 U 13000 U 25000 U
25000 U 13000 U 13000 U 25000 U
25000 U 13000 U 13000 U 25000 U
50000 U 25000 U 25000 U 50000 U
25000 U 13000 U 13000 U 25000 U
25000 U 13000 U 13000 U 25000 U
25000 U 13000 U 13000 U 25000 U
50000 U 25000 U 25000 U 50000 U
25000 U 13000 U 13000 U 25000 U
25000 U 13000 U 13000 U 25000 U
25000 U 13000 U 13000 U 25000 U
25000 U 13000 U 13000 U 25000 U
25000 U 13000 U 13000 U 25000 U
25000 U 13000 U 13000 U 25000 U
25000 U 13000 U 13000 U 25000 U
25000 U 13000 U 13000 U 25000 U
25000 U 13000 U 13000 U 25000 U
25000 U 13000 U 13000 U 25000 U
4818ASR Number: 03/30/2010
MP7ES02Project ID: Cleburn Street well samplingProject Desc:
RLAB Approved Sample Analysis Results
Page 16 of 27
Analysis/ Analyte
1,1,2-Trichlorotrifluoroethane
Vinyl Chloride
m and/or p-Xylene
o-Xylene
ug/L
ug/L
ug/L
ug/L
Units 9-__ 10-__ 11-__ 12-__
25000 U 13000 U 13000 U 25000 U
25000 U 13000 U 13000 U 25000 U
50000 U 25000 U 25000 U 50000 U
25000 U 13000 U 13000 U 25000 U
4818ASR Number: 03/30/2010
MP7ES02Project ID: Cleburn Street well samplingProject Desc:
RLAB Approved Sample Analysis Results
Page 17 of 27
1
1
1
1
1
1
1
1
1
1
1
Alkalinity in Water by Titration
Anions in Water by Ion Chromatography
Conductivity by Field Measurement
Hardness in Water by Calculation
Metals in Water by ICP-AES
pH of Water by Field Measurement
TDS or Total Dissolved Solids
Temperature of Water by Field Measurement
Total Organic Carbon in Water
Turbidity of Water by Field Measurement
VOCs in Water by GC/MS
Analysis/ Analyte
Alkalinity, total
Sulfate
Conductivity
Hardness as CaCO3
Aluminum
Antimony
Arsenic
Barium
Beryllium
Cadmium
Calcium
Chromium
Cobalt
Copper
Iron
Lead
Magnesium
Manganese
Molybdenum
Nickel
Potassium
Selenium
Silver
Sodium
Thallium
Titanium
Vanadium
Zinc
pH
Solids, total dissolved
Temperature
Total Organic Carbon
Turbidity
Acetone
Benzene
mg/L
mg/L
umhos/cm
mg/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
mg/L
ug/L
ug/L
ug/L
ug/L
ug/L
mg/L
ug/L
ug/L
ug/L
mg/L
ug/L
ug/L
mg/L
ug/L
ug/L
ug/L
ug/L
SU
mg/L
Deg C
mg/L
NTU
ug/L
ug/L
Units 12-FD 14-__ 15-__ 16-__
193 176 260 139
10000 U 10000 U 10000 U 30.4 J
6240 1970 3670 721
1320 U 1320 U 1320 U 185
5000 U 5000 U 5000 U 371
5000 U 5000 U 5000 U 50 U
2500 U 2500 U 2500 U 25 U
1000 U 1000 U 1000 U 269
300 U 300 U 300 U 3 U
300 U 300 U 300 U 3 U
200 U 200 U 200 U 61.2
1500 U 1500 U 1820 15 U
1000 U 1000 U 1000 U 10 U
500 U 500 U 500 U 5 U
5000 U 5000 U 5000 U 600
5000 U 5000 U 5000 U 50 U
200 U 200 U 200 U 7.90
303000 209000 237000 71
1500 U 1500 U 1500 U 15 U
2000 U 2000 U 2000 U 20 U
1030 352 644 11.6
5000 U 5000 U 5000 U 50 U
2500 U 2500 U 2500 U 25 U
500 U 500 U 500 U 51.7
5000 U 5000 U 5000 U 50 U
2000 U 2000 U 2000 U 20 U
1000 U 1000 U 1000 U 10 U
2500 U 2500 U 2500 U 54
5.72 7.29 6.97 7.10
5540 1580 3150 290
10.53 13.25 12.97 12.19
1.64 1.51 1.64 3.87
3.0 11.3 28.5 26.3
25000 U 13000 U 13000 U 5.0 U
25000 U 13000 U 13000 U 5.0 U
4818ASR Number: 03/30/2010
MP7ES02Project ID: Cleburn Street well samplingProject Desc:
RLAB Approved Sample Analysis Results
Page 18 of 27
Analysis/ Analyte
Bromodichloromethane
Bromoform
Bromomethane
2-Butanone
Carbon Disulfide
Carbon Tetrachloride
Chlorobenzene
Chloroethane
Chloroform
Chloromethane
Cyclohexane
1,2-Dibromo-3-Chloropropane
Dibromochloromethane
1,2-Dibromoethane
1,2-Dichlorobenzene
1,3-Dichlorobenzene
1,4-Dichlorobenzene
Dichlorodifluoromethane
1,1-Dichloroethane
1,2-Dichloroethane
1,1-Dichloroethene
cis-1,2-Dichloroethene
trans-1,2-Dichloroethene
1,2-Dichloropropane
cis-1,3-Dichloropropene
trans-1,3-Dichloropropene
Ethyl Benzene
2-Hexanone
Isopropylbenzene
Methyl Acetate
Methyl tert-butyl ether
Methylcyclohexane
Methylene Chloride
4-Methyl-2-Pentanone
Naphthalene
Styrene
1,1,2,2-Tetrachloroethane
Tetrachloroethene
Toluene
1,2,3-Trichlorobenzene
1,2,4-Trichlorobenzene
1,1,1-Trichloroethane
1,1,2-Trichloroethane
Trichloroethene
Trichlorofluoromethane
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
Units 12-FD 14-__ 15-__ 16-__
25000 U 13000 U 13000 U 5.0 U
25000 U 13000 U 13000 U 5.0 U
25000 U 13000 U 13000 U 5.0 U
25000 U 13000 U 13000 U 5.0 U
25000 U 13000 U 13000 U 5.0 U
25000 U 13000 U 13000 U 5.0 U
25000 U 13000 U 13000 U 5.0 U
25000 U 13000 U 13000 U 5.0 U
25000 U 13000 U 13000 U 5.0 U
25000 U 13000 U 13000 U 5.0 U
25000 U 13000 U 13000 U 5.0 U
25000 U 13000 U 13000 U 5.0 U
25000 U 13000 U 13000 U 5.0 U
25000 U 13000 U 13000 U 5.0 U
25000 U 13000 U 13000 U 5.0 U
25000 U 13000 U 13000 U 5.0 U
25000 U 13000 U 13000 U 5.0 U
25000 U 13000 U 13000 U 5.0 UJ
25000 U 13000 U 13000 U 5.0 U
25000 U 13000 U 13000 U 5.0 U
25000 U 13000 U 13000 U 5.0 U
25000 U 13000 U 13000 U 5.0 U
25000 U 13000 U 13000 U 5.0 U
25000 U 13000 U 13000 U 5.0 U
25000 U 13000 U 13000 U 5.0 U
25000 U 13000 U 13000 U 5.0 U
25000 U 13000 U 13000 U 5.0 U
25000 U 13000 U 13000 U 5.0 U
25000 U 13000 U 13000 U 5.0 U
25000 U 13000 U 13000 U 5.0 U
50000 U 25000 U 25000 U 10 U
25000 U 13000 U 13000 U 5.0 U
25000 U 13000 U 13000 U 5.0 U
25000 U 13000 U 13000 U 5.0 U
50000 U 25000 U 25000 U 10 U
25000 U 13000 U 13000 U 5.0 U
25000 U 13000 U 13000 U 5.0 U
25000 U 13000 U 13000 U 5.0 U
25000 U 13000 U 13000 U 5.0 U
25000 U 13000 U 13000 U 5.0 U
25000 U 13000 U 13000 U 5.0 U
25000 U 13000 U 13000 U 5.0 U
25000 U 13000 U 13000 U 5.0 U
25000 U 13000 U 13000 U 5.0 U
25000 U 13000 U 13000 U 5.0 U
4818ASR Number: 03/30/2010
MP7ES02Project ID: Cleburn Street well samplingProject Desc:
RLAB Approved Sample Analysis Results
Page 19 of 27
Analysis/ Analyte
1,1,2-Trichlorotrifluoroethane
Vinyl Chloride
m and/or p-Xylene
o-Xylene
ug/L
ug/L
ug/L
ug/L
Units 12-FD 14-__ 15-__ 16-__
25000 U 13000 U 13000 U 5.0 U
25000 U 13000 U 13000 U 5.0 U
50000 U 25000 U 25000 U 10 U
25000 U 13000 U 13000 U 5.0 U
4818ASR Number: 03/30/2010
MP7ES02Project ID: Cleburn Street well samplingProject Desc:
RLAB Approved Sample Analysis Results
Page 20 of 27
1
1
1
1
1
1
1
1
1
1
1
Alkalinity in Water by Titration
Anions in Water by Ion Chromatography
Conductivity by Field Measurement
Hardness in Water by Calculation
Metals in Water by ICP-AES
pH of Water by Field Measurement
TDS or Total Dissolved Solids
Temperature of Water by Field Measurement
Total Organic Carbon in Water
Turbidity of Water by Field Measurement
VOCs in Water by GC/MS
Analysis/ Analyte
Alkalinity, total
Sulfate
Conductivity
Hardness as CaCO3
Aluminum
Antimony
Arsenic
Barium
Beryllium
Cadmium
Calcium
Chromium
Cobalt
Copper
Iron
Lead
Magnesium
Manganese
Molybdenum
Nickel
Potassium
Selenium
Silver
Sodium
Thallium
Titanium
Vanadium
Zinc
pH
Solids, total dissolved
Temperature
Total Organic Carbon
Turbidity
Acetone
Benzene
mg/L
mg/L
umhos/cm
mg/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
mg/L
ug/L
ug/L
ug/L
ug/L
ug/L
mg/L
ug/L
ug/L
ug/L
mg/L
ug/L
ug/L
mg/L
ug/L
ug/L
ug/L
ug/L
SU
mg/L
Deg C
mg/L
NTU
ug/L
ug/L
Units 17-__ 17-FD 19-__ 20-__
147 148 89.9 132
10000 U 10000 U 162 114
2850 2850 1190 1300
1320 U 1400 361 291
5000 U 5000 U 50 U 657
5000 U 5000 U 50 U 50 U
2500 U 2500 U 25 U 25 U
1000 U 1000 U 86 255
300 U 300 U 3 U 3 U
300 U 300 U 3 U 3 U
200 U 231 103 85.5
10800 14500 177 15 U
1000 U 1000 U 10 U 10 U
500 U 500 U 5 U 5 U
7350 9120 50 U 728
5000 U 5000 U 50 U 50 U
200 U 200 U 25.3 18.8
174000 259000 6950 208
1500 U 1500 U 15 U 15 U
2410 J 3310 J 37 J 20 J
200 U 200 U 16.7 10.6
5000 U 5000 U 50 U 50 U
2500 U 2500 U 25 U 25 U
500 U 500 U 70.9 138
5000 U 5000 U 50 U 50 U
2000 U 2000 U 20 U 20 U
1000 U 1000 U 10 U 10 U
2500 U 2500 U 25 U 25 U
6.31 6.31 6.70 6.72
2190 2320 820 738
12.7 12.7 15.27 13.55
3.18 2.96 2.96 2.96
147.8 147.8 4.9 3.3
25000 U 25000 U 100 U 5.0 U
25000 U 25000 U 100 U 5.0 U
4818ASR Number: 03/30/2010
MP7ES02Project ID: Cleburn Street well samplingProject Desc:
RLAB Approved Sample Analysis Results
Page 21 of 27
Analysis/ Analyte
Bromodichloromethane
Bromoform
Bromomethane
2-Butanone
Carbon Disulfide
Carbon Tetrachloride
Chlorobenzene
Chloroethane
Chloroform
Chloromethane
Cyclohexane
1,2-Dibromo-3-Chloropropane
Dibromochloromethane
1,2-Dibromoethane
1,2-Dichlorobenzene
1,3-Dichlorobenzene
1,4-Dichlorobenzene
Dichlorodifluoromethane
1,1-Dichloroethane
1,2-Dichloroethane
1,1-Dichloroethene
cis-1,2-Dichloroethene
trans-1,2-Dichloroethene
1,2-Dichloropropane
cis-1,3-Dichloropropene
trans-1,3-Dichloropropene
Ethyl Benzene
2-Hexanone
Isopropylbenzene
Methyl Acetate
Methyl tert-butyl ether
Methylcyclohexane
Methylene Chloride
4-Methyl-2-Pentanone
Naphthalene
Styrene
1,1,2,2-Tetrachloroethane
Tetrachloroethene
Toluene
1,2,3-Trichlorobenzene
1,2,4-Trichlorobenzene
1,1,1-Trichloroethane
1,1,2-Trichloroethane
Trichloroethene
Trichlorofluoromethane
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
Units 17-__ 17-FD 19-__ 20-__
25000 U 25000 U 100 U 5.0 U
25000 U 25000 U 100 U 5.0 U
25000 U 25000 U 100 U 5.0 U
25000 U 25000 U 100 U 5.0 U
25000 U 25000 U 100 U 5.0 U
25000 U 25000 U 100 U 5.0 U
25000 U 25000 U 100 U 5.0 U
25000 U 25000 U 100 U 5.0 U
25000 U 25000 U 100 U 5.0 U
25000 U 25000 U 100 U 5.0 U
25000 U 25000 U 100 U 5.0 U
25000 U 25000 U 100 U 5.0 U
25000 U 25000 U 100 U 5.0 U
25000 U 25000 U 100 U 5.0 U
25000 U 25000 U 100 U 5.0 U
25000 U 25000 U 100 U 5.0 U
25000 U 25000 U 100 U 5.0 U
25000 U 25000 U 100 UJ 5.0 UJ
25000 U 25000 U 100 U 5.0 U
25000 U 25000 U 100 U 5.0 U
25000 U 25000 U 100 U 5.0 U
25000 U 25000 U 100 U 10
25000 U 25000 U 100 U 5.0 U
25000 U 25000 U 100 U 5.0 U
25000 U 25000 U 100 U 5.0 U
25000 U 25000 U 100 U 5.0 U
25000 U 25000 U 100 U 5.0 U
25000 U 25000 U 100 U 5.0 U
25000 U 25000 U 100 U 5.0 U
25000 U 25000 U 100 U 5.0 U
50000 U 50000 U 200 U 10 U
25000 U 25000 U 100 U 5.0 U
25000 U 25000 U 100 U 5.0 U
25000 U 25000 U 100 U 5.0 U
50000 U 50000 U 200 U 10 U
25000 U 25000 U 100 U 5.0 U
25000 U 25000 U 100 U 5.0 U
25000 U 25000 U 100 U 1700
25000 U 25000 U 100 U 5.0 U
25000 U 25000 U 100 U 5.0 U
25000 U 25000 U 100 U 5.0 U
25000 U 25000 U 100 U 5.0 U
25000 U 25000 U 100 U 5.0 U
25000 U 25000 U 100 U 150
25000 U 25000 U 100 U 5.0 U
4818ASR Number: 03/30/2010
MP7ES02Project ID: Cleburn Street well samplingProject Desc:
RLAB Approved Sample Analysis Results
Page 22 of 27
Analysis/ Analyte
1,1,2-Trichlorotrifluoroethane
Vinyl Chloride
m and/or p-Xylene
o-Xylene
ug/L
ug/L
ug/L
ug/L
Units 17-__ 17-FD 19-__ 20-__
25000 U 25000 U 100 U 5.0 U
25000 U 25000 U 100 U 5.0 U
50000 U 50000 U 200 U 10 U
25000 U 25000 U 100 U 5.0 U
4818ASR Number: 03/30/2010
MP7ES02Project ID: Cleburn Street well samplingProject Desc:
RLAB Approved Sample Analysis Results
Page 23 of 27
1
1
1
1
1
1
1
1
1
1
1
Alkalinity in Water by Titration
Anions in Water by Ion Chromatography
Conductivity by Field Measurement
Hardness in Water by Calculation
Metals in Water by ICP-AES
pH of Water by Field Measurement
TDS or Total Dissolved Solids
Temperature of Water by Field Measurement
Total Organic Carbon in Water
Turbidity of Water by Field Measurement
VOCs in Water by GC/MS
Analysis/ Analyte
Alkalinity, total
Sulfate
Conductivity
Hardness as CaCO3
Aluminum
Antimony
Arsenic
Barium
Beryllium
Cadmium
Calcium
Chromium
Cobalt
Copper
Iron
Lead
Magnesium
Manganese
Molybdenum
Nickel
Potassium
Selenium
Silver
Sodium
Thallium
Titanium
Vanadium
Zinc
pH
Solids, total dissolved
Temperature
Total Organic Carbon
Turbidity
Acetone
Benzene
mg/L
mg/L
umhos/cm
mg/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
mg/L
ug/L
ug/L
ug/L
ug/L
ug/L
mg/L
ug/L
ug/L
ug/L
mg/L
ug/L
ug/L
mg/L
ug/L
ug/L
ug/L
ug/L
SU
mg/L
Deg C
mg/L
NTU
ug/L
ug/L
Units 21-__ 22-__ 23-__ 26-FB
372 241 75.6
10000 U 10000 U 101
8080 4430 1020
1320 U 1320 U 293
5000 U 5000 U 50 U 50 U
5000 U 5000 U 50 U 50 U
2500 U 2500 U 25 U 25 U
1000 U 1000 U 186 10 U
300 U 300 U 3 U 3 U
300 U 300 U 3 U 3 U
200 U 200 U 83.4 2.00 U
1500 U 1500 15 U 15 U
1000 U 1000 U 10 U 10 U
500 U 500 U 5 U 5 U
5000 U 5000 U 63 50 U
5000 U 5000 U 50 U 50 U
200 U 200 U 20.7 2.00 U
296000 298000 24 5 U
1500 U 1500 U 15 U 15 U
2000 U 2000 U 142 20 U
1480 790 17.2 2.00 U
5000 U 5000 U 50 U 50 U
2500 U 2500 U 25 U 25 U
500 U 500 U 63.7 5.00 U
5000 U 5000 U 50 U 50 U
2000 U 2000 U 20 U 20 U
1000 U 1000 U 10 U 10 U
2500 U 2500 U 25 U 25 U
6.85 6.81 6.68
8960 4110 664
14.52 15.01 15.44
1.47 1.15 1.8 1 U
3.1 21.8 20.3
25000 U 25000 U 5.0 U 5.0 U
25000 U 25000 U 5.0 U 5.0 U
4818ASR Number: 03/30/2010
MP7ES02Project ID: Cleburn Street well samplingProject Desc:
RLAB Approved Sample Analysis Results
Page 24 of 27
Analysis/ Analyte
Bromodichloromethane
Bromoform
Bromomethane
2-Butanone
Carbon Disulfide
Carbon Tetrachloride
Chlorobenzene
Chloroethane
Chloroform
Chloromethane
Cyclohexane
1,2-Dibromo-3-Chloropropane
Dibromochloromethane
1,2-Dibromoethane
1,2-Dichlorobenzene
1,3-Dichlorobenzene
1,4-Dichlorobenzene
Dichlorodifluoromethane
1,1-Dichloroethane
1,2-Dichloroethane
1,1-Dichloroethene
cis-1,2-Dichloroethene
trans-1,2-Dichloroethene
1,2-Dichloropropane
cis-1,3-Dichloropropene
trans-1,3-Dichloropropene
Ethyl Benzene
2-Hexanone
Isopropylbenzene
Methyl Acetate
Methyl tert-butyl ether
Methylcyclohexane
Methylene Chloride
4-Methyl-2-Pentanone
Naphthalene
Styrene
1,1,2,2-Tetrachloroethane
Tetrachloroethene
Toluene
1,2,3-Trichlorobenzene
1,2,4-Trichlorobenzene
1,1,1-Trichloroethane
1,1,2-Trichloroethane
Trichloroethene
Trichlorofluoromethane
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
Units 21-__ 22-__ 23-__ 26-FB
25000 U 25000 U 5.0 U 5.0 U
25000 U 25000 U 5.0 U 5.0 U
25000 U 25000 U 5.0 U 5.0 U
25000 U 25000 U 5.0 U 5.0 U
25000 U 25000 U 5.0 U 5.0 U
25000 U 25000 U 5.0 U 5.0 U
25000 U 25000 U 5.0 U 5.0 U
25000 U 25000 U 5.0 U 5.0 U
25000 U 25000 U 5.0 U 5.0 U
25000 U 25000 U 5.0 U 5.0 U
25000 U 25000 U 5.0 U 5.0 U
25000 U 25000 U 5.0 U 5.0 U
25000 U 25000 U 5.0 U 5.0 U
25000 U 25000 U 5.0 U 5.0 U
25000 U 25000 U 5.0 U 5.0 U
25000 U 25000 U 5.0 U 5.0 U
25000 U 25000 U 5.0 U 5.0 U
25000 U 25000 U 5.0 U 5.0 UJ
25000 U 25000 U 5.0 U 5.0 U
25000 U 25000 U 5.0 U 5.0 U
25000 U 25000 U 5.0 U 5.0 U
25000 U 25000 U 5.0 U 5.0 U
25000 U 25000 U 5.0 U 5.0 U
25000 U 25000 U 5.0 U 5.0 U
25000 U 25000 U 5.0 U 5.0 U
25000 U 25000 U 5.0 U 5.0 U
25000 U 25000 U 5.0 U 5.0 U
25000 U 25000 U 5.0 U 5.0 U
25000 U 25000 U 5.0 U 5.0 U
25000 U 25000 U 5.0 U 5.0 U
50000 U 50000 U 10 U 10 U
25000 U 25000 U 5.0 U 5.0 U
25000 U 25000 U 5.0 U 5.0 U
25000 U 25000 U 5.0 U 5.0 U
50000 U 50000 U 10 U 10 U
25000 U 25000 U 5.0 U 5.0 U
25000 U 25000 U 5.0 U 5.0 U
25000 U 25000 U 11 5.0 U
25000 U 25000 U 5.0 U 5.0 U
25000 U 25000 U 5.0 U 5.0 U
25000 U 25000 U 5.0 U 5.0 U
25000 U 25000 U 5.0 U 5.0 U
25000 U 25000 U 5.0 U 5.0 U
25000 U 25000 U 5.0 U 5.0 U
25000 U 25000 U 5.0 U 5.0 U
4818ASR Number: 03/30/2010
MP7ES02Project ID: Cleburn Street well samplingProject Desc:
RLAB Approved Sample Analysis Results
Page 25 of 27
Analysis/ Analyte
1,1,2-Trichlorotrifluoroethane
Vinyl Chloride
m and/or p-Xylene
o-Xylene
ug/L
ug/L
ug/L
ug/L
Units 21-__ 22-__ 23-__ 26-FB
25000 U 25000 U 5.0 U 5.0 U
25000 U 25000 U 5.0 U 5.0 U
50000 U 50000 U 10 U 10 U
25000 U 25000 U 5.0 U 5.0 U
4818ASR Number: 03/30/2010
MP7ES02Project ID: Cleburn Street well samplingProject Desc:
RLAB Approved Sample Analysis Results
Page 26 of 27
1 VOCs in Water by GC/MS
Analysis/ Analyte
Acetone
Benzene
Bromodichloromethane
Bromoform
Bromomethane
2-Butanone
Carbon Disulfide
Carbon Tetrachloride
Chlorobenzene
Chloroethane
Chloroform
Chloromethane
Cyclohexane
1,2-Dibromo-3-Chloropropane
Dibromochloromethane
1,2-Dibromoethane
1,2-Dichlorobenzene
1,3-Dichlorobenzene
1,4-Dichlorobenzene
Dichlorodifluoromethane
1,1-Dichloroethane
1,2-Dichloroethane
1,1-Dichloroethene
cis-1,2-Dichloroethene
trans-1,2-Dichloroethene
1,2-Dichloropropane
cis-1,3-Dichloropropene
trans-1,3-Dichloropropene
Ethyl Benzene
2-Hexanone
Isopropylbenzene
Methyl Acetate
Methyl tert-butyl ether
Methylcyclohexane
Methylene Chloride
4-Methyl-2-Pentanone
Naphthalene
Styrene
1,1,2,2-Tetrachloroethane
Tetrachloroethene
Toluene
1,2,3-Trichlorobenzene
1,2,4-Trichlorobenzene
1,1,1-Trichloroethane
1,1,2-Trichloroethane
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
Units 27-FB 28-FB 29-FB
5.0 U 5.0 U 5.0 U
5.0 U 5.0 U 5.0 U
5.0 U 5.0 U 5.0 U
5.0 U 5.0 U 5.0 U
5.0 U 5.0 U 5.0 U
5.0 U 5.0 U 5.0 U
5.0 U 5.0 U 5.0 U
5.0 U 5.0 U 5.0 U
5.0 U 5.0 U 5.0 U
5.0 U 5.0 U 5.0 U
5.0 U 5.0 U 5.0 U
5.0 U 5.0 U 5.0 U
5.0 U 5.0 U 5.0 U
5.0 U 5.0 U 5.0 U
5.0 U 5.0 U 5.0 U
5.0 U 5.0 U 5.0 U
5.0 U 5.0 U 5.0 U
5.0 U 5.0 U 5.0 U
5.0 U 5.0 U 5.0 U
5.0 UJ 5.0 UJ 5.0 UJ
5.0 U 5.0 U 5.0 U
5.0 U 5.0 U 5.0 U
5.0 U 5.0 U 5.0 U
5.0 U 5.0 U 5.0 U
5.0 U 5.0 U 5.0 U
5.0 U 5.0 U 5.0 U
5.0 U 5.0 U 5.0 U
5.0 U 5.0 U 5.0 U
5.0 U 5.0 U 5.0 U
5.0 U 5.0 U 5.0 U
5.0 U 5.0 U 5.0 U
5.0 U 5.0 U 5.0 U
10 U 10 U 10 U
5.0 U 5.0 U 5.0 U
5.0 U 5.0 U 5.0 U
5.0 U 5.0 U 5.0 U
10 U 10 U 10 U
5.0 U 5.0 U 5.0 U
5.0 U 5.0 U 5.0 U
5.0 U 5.0 U 5.0 U
5.0 U 5.0 U 5.0 U
5.0 U 5.0 U 5.0 U
5.0 U 5.0 U 5.0 U
5.0 U 5.0 U 5.0 U
5.0 U 5.0 U 5.0 U
4818ASR Number: 03/30/2010
MP7ES02Project ID: Cleburn Street well samplingProject Desc:
RLAB Approved Sample Analysis Results
Page 27 of 27
Analysis/ Analyte
Trichloroethene
Trichlorofluoromethane
1,1,2-Trichlorotrifluoroethane
Vinyl Chloride
m and/or p-Xylene
o-Xylene
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
Units 27-FB 28-FB 29-FB
5.0 U 5.0 U 5.0 U
5.0 U 5.0 U 5.0 U
5.0 U 5.0 U 5.0 U
5.0 U 5.0 U 5.0 U
10 U 10 U 10 U
5.0 U 5.0 U 5.0 U
4818ASR Number: 03/30/2010
MP7ES02Project ID: Cleburn Street well samplingProject Desc:
RLAB Approved Sample Analysis Results
4818
MP7ES02Project ID:
Cleburn Street well sampling
Mary PetersonSUPR/IANE
United States Environmental Protection AgencyRegion VII
901 N. 5th StreetKansas City, KS 66101
__/__/____
Data Disposition/Sample Release for ASR #:
Project Description:
Subject:
Kaye DollmannENSV/RLAB
I have received and reviewed the Transmittal of Sample Analysis Results for the above-referencedAnalytical Services Request(ASR) and have indicated my findings below by checking one of theboxes for Data Disposition.
I understand all samples will be disposed upon receipt of this form, unless samples are requestedto be held. If I do not return this form all samples will be disposed of on ___________________.
"RELEASED" - Read-only to all Region 7 employees and contractors that have R7LIMS"Customer" account. All Samples may be disposed of upon receipt of this form if not requested tobe held.
"Project Manager Accessible" - Available on the LAN in R7LIMS for my use only. All Samples maybe disposed of upon receipt of this form if not requested to be held.
"Archived" - THIS DATA IS OF A SENSITIVE NATURE. Any future reports must be requestedthrough the laboratory. All samples may be disposed of upon receipt of the form if not requestedto be held.
Date:
From:
To:
Hold Samples - I have determined that the samples need to be held until ______________, afterwhich time they will be disposed of in accordance with applicable regulations. The reason for the hold is:
Samples are associated with a legal proceeding.
Question/Concern with data - possible reanalysis requested.
Other:________________________________________________________________
APRIL 2010
Page 1 of 21
05/14/2010Date:
4846
MP7ES02
Cleburn Street well sampling
Mary PetersonSUPR/IANE
Transmittal of Sample Analysis Results for ASR #:
Project ID:
Project Description:
Michael F. Davis, ChiefChemical Analysis and Response Branch, Environmental Services Division
To:
Enclosed are the analytical data for the above-referenced Analytical Services Request (ASR) andProject. The Regional Laboratory has reviewed and verified the results in accordance with proceduresdescribed in our Quality Manual (QM). In addition to all of the analytical results, this transmittalcontains pertinent information that may have influenced the reported results and documents anydeviations from the established requirements of the QM.
Please contact us within 14 days of receipt of this package if you determine there is a need for anychanges. Please complete the enclosed Customer Satisfaction Survey and Data Disposition/SampleRelease memo for this ASR as soon as possible. The process of disposing of the samples for this ASRwill be initiated 30 days from the date of this transmittal unless an alternate release date is specifiedon the Data Disposition/Sample Release memo.
If you have any questions or concerns relating to this data package, contact our customer service lineat 913-551-5295.
Enclosures
cc: Analytical Data File.
United States Environmental Protection AgencyRegion 7
901 N. 5th StreetKansas City, KS 66101
Subject:
From:
Page 2 of 21
4846ASR Number: 05/14/2010
Mary Peterson SUPR/IANE 913-551-7882
MP7ES02
Cleburn Street well sampling
Grand Island Nebraska Superfund
CLEBURN STREET WELL - 1 HR MARTINIZING GWRESORATION
07ESSite ID: 02
Site Cleanup Support
Injection sampling event.
Project Manager: Org: Phone:
Project ID:
Project Desc:
Location: State: Program:
Site Name: Site OU:
Purpose:
__ = Field SampleFB = Field BlankFD = Field Duplicate
QC Codes identify the type of sample for quality control purpose.
Milligrams per LiterMicrograms per Liter
Specific units in which results arereported.
The identification of the analyte is acceptable; the reported value is anestimate.The analyte was not detected at or above the reporting limit.The analyte was not detected at or above the reporting limit. The reportinglimit is an estimate.
Specific codes used in conjunction with data values to provide additional information on the quality of reported results, or used to explain the absence of a specific value.
Summary of Project Information
Explanation of Codes, Units and Qualifiers used on this report
Sample QC Codes: Units:
J
UUJ
=
==
Data Qualifiers:
= Values have been reviewed and found acceptable for use. (Blank)
mg/Lug/L
==
2009073QAPP Number:
302DD2CGPRA PRC:
Page 3 of 21
1
2
4
5
5
6
7
8
9
10
11
12
12
14
15
16
17
17
18
19
20
21
22
26
27
28
29
SampleNo
__
__
__
__
FD
__
__
__
__
__
__
__
FD
__
__
__
__
FD
__
__
__
__
__
FB
FB
FB
FB
QCCode
Water
Water
Water
Water
Water
Water
Water
Water
Water
Water
Water
Water
Water
Water
Water
Water
Water
Water
Water
Water
Water
Water
Water
Water
Water
Water
Water
Matrix
ERT-15
IW-1
IW-2
IW-3
IW-3/Field Duplicate of sample 5
IW-4
IW-5
IW-6
IW-7
ERT-16
IW-9
IW-8
IW-8/Field Duplicate of sample 12
IW-10
MW-2A
MW-2B
ERT-14
ERT-14/Field Duplicate of sample17MW-12A
DPE-4
DPE-3
DPE-1
DPE-2
Preservative Blank sample
Trip Blank
Trip Blank sample
VOA Trip Blank sample
Location DescriptionExternal
Sample No
04/05/2010
04/05/2010
04/05/2010
04/06/2010
04/06/2010
04/06/2010
04/06/2010
04/06/2010
04/06/2010
04/06/2010
04/07/2010
04/07/2010
04/07/2010
04/07/2010
04/07/2010
04/07/2010
04/05/2010
04/05/2010
04/07/2010
04/08/2010
04/08/2010
04/08/2010
04/08/2010
04/07/2010
03/31/2010
03/31/2010
03/31/2010
Start Date
14:45
16:40
17:50
08:50
08:50
10:10
11:30
13:10
15:55
18:55
09:40
11:00
11:00
12:20
13:40
14:55
13:10
13:10
17:50
10:25
11:40
15:40
16:45
08:00
15:05
15:10
15:15
Start Time
04/07/2010
04/06/2010
04/05/2010
End Date
08:20
08:10
14:55
End Time
04/06/2010
04/07/2010
04/07/2010
04/07/2010
04/07/2010
04/07/2010
04/07/2010
04/07/2010
04/07/2010
04/08/2010
04/08/2010
04/08/2010
04/08/2010
04/08/2010
04/08/2010
04/08/2010
04/06/2010
04/06/2010
04/09/2010
04/09/2010
04/09/2010
04/09/2010
04/09/2010
04/08/2010
04/08/2010
04/07/2010
04/06/2010
ReceiptDate
4846 05/14/2010
MP7ES02Project ID: Cleburn Street well samplingProject Desc:
ASR Number: Sample Information Summary
-
-
-
-
-
-
-
-
-
-
-
-
-
-
-
-
-
-
-
-
-
-
-
-
-
-
-
Page 4 of 21
1
1
1
1
Alkalinity in Water by Titration
Anions in Water by Ion Chromatography
Hardness in Water by Calculation
Metals in Water by ICP-AES
Region 7 ESAT Contract Lab (In-House)
Region 7 ESAT Contract Lab (In-House)
Region 7 ESAT Contract Lab (In-House)
Region 7 ESAT Contract Lab (In-House)
Lab:
Lab:
Lab:
Lab:
EPA Region 7 RLAB Method 3132.1E
Region 7 RLAB Method 3135.12A
EPA Region 7 RLAB Method 3122.3C
Method:
Method:
Method:
(N/A)
Dilutions were necessary in order to obtain valid results and to avoid instrumentdamage due to matrix interferences for samples 2, 4, 5, 5 FD, 6, 7, 8, 9, 10, 11, 12, 12 FD,14, 15, 19, 20, 21 , and 22. This increased the reporting limits by a factor of 10000 forthese samples.
Sulfate (134, 80-120) was J-coded in sample 18. Although the analyte in question hasbeen positively identified in the sample, the quantitation is an estimate (J-coded) due tohigh recovery of this analyte in the laboratory matrix spike duplicate. The actualconcentration for this analyte may be lower than the reported value.
Dilutions were necessary in order to obtain valid results due to matrix interferences forsamples 2-15 and 19-22. This increased the reporting limits by a factor of 100 for thesesamples.
Comments:
Comments:
Comments:
1-__ 2-__ 4-__ 5-__ 5-FD 6-__ 7-__8-__ 9-__ 10-__ 11-__ 12-__ 12-FD 14-__15-__ 16-__ 17-__ 17-FD 18-__ 19-__ 20-__21-__ 22-__
1-__ 2-__ 4-__ 5-__ 5-FD 6-__ 7-__8-__ 9-__ 10-__ 11-__ 12-__ 12-FD 14-__15-__ 16-__ 17-__ 17-FD 18-__ 19-__ 20-__21-__ 22-__
1-__ 2-__ 4-__ 5-__ 5-FD 6-__ 7-__8-__ 9-__ 10-__ 11-__ 12-__ 12-FD 14-__15-__ 16-__ 17-__ 17-FD 18-__ 19-__ 20-__21-__ 22-__ 26-FB
Samples:
Samples:
Samples:
4846ASR Number: 05/14/2010
MP7ES02Project ID: Cleburn Street well samplingProject Desc
RLAB Approved Analysis Comments
Analysis Comments About Results For This Analysis
Page 5 of 21
1
1
TDS or Total Dissolved Solids
Total Organic Carbon in Water
Region 7 EPA Laboratory - Kansas City, Ks.
RASP Contract Lab (Out-Source)
Lab:
Lab:
EPA Region 7 RLAB Method 3122.3C
EPA Region 7 RLAB Method 3142.2B
Similar to EPA SW846 Method 9060 or StandardMethods (20th Edtion) 5310 B, C,or D (see comments)
Method:
Method:
Method:
Dilutions were necessary in order to obtain valid results due to matrix interferences forsamples 2-15 and 19-22. This increased the reporting limits by a factor of 100 for thesesamples.
Total Dissolved Solids was J-coded in sample 17. Although the analyte in question hasbeen positively identified in the sample, the quantitation is an estimate (J-coded) due tolow recovery of this analyte in the laboratory matrix spike. The actual concentration forthis analyte may be higher than the reported value. (MS/MSD recoveries 82% & 83%, LAL90%)
Samples 4846-18 thru 4846-22 were shipped on 04/09/10 for arrival at the lab on04/10/10. Samples were not delivered until 04/12/10 which resulted in the coolertemperature being 8.4ºC at sample receipt by the laboratory. No data were qualified andthe analysis proceeded as requested.
Total Organic Carbon was J-coded in sample 4846-1. Although the analyte in question hasbeen positively identified in the sample, the quantitation is an estimate (J-coded) due tolow recovery of this analyte in the laboratory matrix spike. The actual concentration forthis analyte may be higher than the reported value.
Comments:
Comments:
Comments:
1-__ 2-__ 4-__ 5-__ 5-FD 6-__ 7-__8-__ 9-__ 10-__ 11-__ 12-__ 12-FD 14-__15-__ 16-__ 17-__ 17-FD 18-__ 19-__ 20-__21-__ 22-__ 26-FB
1-__ 2-__ 4-__ 5-__ 5-FD 6-__ 7-__8-__ 9-__ 10-__ 11-__ 12-__ 12-FD 14-__15-__ 16-__ 17-__ 17-FD 18-__ 19-__ 20-__21-__ 22-__
1-__ 2-__ 4-__ 5-__ 5-FD 6-__ 7-__8-__ 9-__ 10-__ 11-__ 12-__ 12-FD 14-__15-__ 16-__ 17-__ 17-FD 18-__ 19-__ 20-__21-__ 22-__ 26-FB
Samples:
Samples:
Samples:
4846ASR Number: 05/14/2010
MP7ES02Project ID: Cleburn Street well samplingProject Desc
RLAB Approved Analysis Comments
Analysis Comments About Results For This Analysis
Page 6 of 21
1 VOCs in Water by GC/MS
Region 7 EPA Laboratory - Kansas City, Ks.Lab:
EPA Region 7 RLAB Method 3230.1FMethod:
Total Organic Carbon was J-coded in sample 4846-1. Although the analyte in question hasbeen positively identified in the sample, the quantitation is an estimate (J-coded) due topoor precision obtained for this analyte in the laboratory duplicate sample.
Samples required dilution for high permanganate levels (purple color). Diluted sampleshad raised reporting limits. Samples were diluted as follows: 1: 50x2-14: 4000x15: 2000x16-18: no dilution19-22: 4000x26FB-29FB: no dilution
The dark purple color in the samples prevented the determination of pH, so preservationcould not be confirmed in the following samples: 2, 4, 5, 5FD, 6-12, 12FD, 14, 15, and 19-22. As these samples were analyzed within 7 days of collection no data were affected.
Sample 18 had Trichloroethene and Tetrachloroethene above the calibration range. Thesevalues have been J-coded, as dilutions could not be analyzed due to instrument problems.The value for Trichloroethene should be close to the true value, as it did not exceed thepredicted linear range of the curve (value: 290, Curve upper range: 200ug/L).Tetrachloroethene will be biased lower than the true value.
Dichlorodifluoromethane, Carbon Tetrachloride and Bromoform were UJ-coded in samples1, 2, 4, 5, 5FD, 6-11, 26FB, 27FB, 28FB and 29FB. These analytes were not found in thesamples at or above the reporting limit, however, the reporting limit is an estimate (UJ-coded) due to the continuing calibration check not meeting accuracy specifications, and lowrecovery in the laboratory control sample for Carbon Tetrachloride and Bromoform. Theactual reporting limit for these analytes may be higher than the reported value. Sample 1was also UJ-coded for Bromoform due to low recovery in the matrix spikes.
Dibromochloromethane was UJ-coded in samples 1, 2, 4, 5, 5FD, 6-11, 26FB, 27FB, 28FBand 29FB. This analyte was not found in the samples at or above the reporting limit,however, the reporting limit is an estimate (UJ-coded) due to low recovery of this analytein the laboratory control sample. The actual reporting limit for this analyte may be higherthan the reported value. Sample 1 was also UJ-coded for this analyte due to low recoveryin the matrix spikes.
1,2-Dibromoethane, 1,3-Dichlorobenzene, cis-1,2-Dichloroethene, trans-1,2-
Comments:
1-__ 2-__ 4-__ 5-__ 5-FD 6-__ 7-__8-__ 9-__ 10-__ 11-__ 12-__ 12-FD 14-__15-__ 16-__ 17-__ 17-FD 18-__ 19-__ 20-__21-__ 22-__ 26-FB 27-FB 28-FB 29-FB
Samples:
4846ASR Number: 05/14/2010
MP7ES02Project ID: Cleburn Street well samplingProject Desc
RLAB Approved Analysis Comments
Analysis Comments About Results For This Analysis
Page 7 of 21
Dichloroethene, cis-1,3-Dichloropropene, trans-1,3-Dichloropropene, Methylene Chloride,Styrene, and Vinyl Chloride were UJ-coded in sample 1. These analytes were not found inthe sample at or above the reporting limit, however, the reporting limit is an estimate (UJ-coded) due to low recovery of these analytes in the laboratory matrix spikes. The actualreporting limit for these analytes may be higher than the reported value. Trans-1,2-Dichloroethene, trans-1,3-Dichloropropene and Vinyl Chloride were also UJ-coded due topoor precision in the matrix spike and spike duplicate.
Bromomethane, Chloroethane, 1,3-Dichlorobenzene, and Methylene Chloride were UJ-coded in sample 16. These analytes were not found in the sample at or above thereporting limit, however, the reporting limit is an estimate (UJ-coded) due to low recoveryof these analytes in the laboratory matrix spike. The actual reporting limit for theseanalytes may be higher than the reported value.
Low recovery of Matrix Spikes in sample 1 may have been due to permanganate presencein the sample.
4846ASR Number: 05/14/2010
MP7ES02Project ID: Cleburn Street well samplingProject Desc
RLAB Approved Analysis Comments
Analysis Comments About Results For This Analysis
Page 8 of 21
1
1
1
1
1
1
1
Alkalinity in Water by Titration
Anions in Water by Ion Chromatography
Hardness in Water by Calculation
Metals in Water by ICP-AES
TDS or Total Dissolved Solids
Total Organic Carbon in Water
VOCs in Water by GC/MS
Analysis/ Analyte
Alkalinity, total
Sulfate
Hardness as CaCO3
Aluminum
Antimony
Arsenic
Barium
Beryllium
Cadmium
Calcium
Chromium
Cobalt
Copper
Iron
Lead
Magnesium
Manganese
Molybdenum
Nickel
Potassium
Selenium
Silver
Sodium
Thallium
Titanium
Vanadium
Zinc
Solids, total dissolved
Total Organic Carbon
Acetone
Benzene
Bromodichloromethane
Bromoform
Bromomethane
2-Butanone
Carbon Disulfide
Carbon Tetrachloride
Chlorobenzene
Chloroethane
mg/L
mg/L
mg/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
mg/L
ug/L
ug/L
ug/L
ug/L
ug/L
mg/L
ug/L
ug/L
ug/L
mg/L
ug/L
ug/L
mg/L
ug/L
ug/L
ug/L
ug/L
mg/L
mg/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
Units 1-__ 2-__ 4-__ 5-__
87.3 226 230 288
122 10000 U 10000 U 10000 U
262 1320 U 1320 U 1320 U
50 U 5000 U 5000 U 5000 U
50 U 5000 U 5000 U 5000 U
25 U 2500 U 2500 U 2500 U
86 1000 U 1000 U 1000 U
3 U 300 U 300 U 300 U
3 U 300 U 300 U 300 U
73.7 200 U 200 U 200 U
90 1500 U 1500 U 1500 U
10 U 1000 U 1000 U 1000 U
5 U 500 U 500 U 500 U
50 U 5000 U 5000 U 5000 U
50 U 5000 U 5000 U 5000 U
18.9 200 U 200 U 200 U
18900 354000 232000 331000
15 U 1500 U 1500 U 1500 U
20 U 2000 U 2000 U 2000 U
13.5 2670 2010 2440
50 U 5000 U 5000 U 5000 U
25 U 2500 U 2500 U 2500 U
57.9 500 U 500 U 500 U
50 U 5000 U 5000 U 5000 U
20 U 2000 U 2000 U 2000 U
10 U 1000 U 1000 U 1000 U
25 U 2500 U 2500 U 2500 U
493 15200 12900 12800
2.37 J 1.5 1.51 1.73
250 U 20000 U 20000 U 20000 U
250 U 20000 U 20000 U 20000 U
250 U 20000 U 20000 U 20000 U
250 UJ 20000 UJ 20000 UJ 20000 UJ
250 U 20000 U 20000 U 20000 U
250 U 20000 U 20000 U 20000 U
250 U 20000 U 20000 U 20000 U
250 UJ 20000 UJ 20000 UJ 20000 UJ
250 U 20000 U 20000 U 20000 U
250 UJ 20000 U 20000 U 20000 U
4846ASR Number: 05/14/2010
MP7ES02Project ID: Cleburn Street well samplingProject Desc:
RLAB Approved Sample Analysis Results
Page 9 of 21
Analysis/ Analyte
Chloroform
Chloromethane
Cyclohexane
1,2-Dibromo-3-Chloropropane
Dibromochloromethane
1,2-Dibromoethane
1,2-Dichlorobenzene
1,3-Dichlorobenzene
1,4-Dichlorobenzene
Dichlorodifluoromethane
1,1-Dichloroethane
1,2-Dichloroethane
1,1-Dichloroethene
cis-1,2-Dichloroethene
trans-1,2-Dichloroethene
1,2-Dichloropropane
cis-1,3-Dichloropropene
trans-1,3-Dichloropropene
Ethyl Benzene
2-Hexanone
Isopropylbenzene
Methyl Acetate
Methyl tert-butyl ether
Methylcyclohexane
Methylene Chloride
4-Methyl-2-Pentanone
Naphthalene
Styrene
1,1,2,2-Tetrachloroethane
Tetrachloroethene
Toluene
1,2,3-Trichlorobenzene
1,2,4-Trichlorobenzene
1,1,1-Trichloroethane
1,1,2-Trichloroethane
Trichloroethene
Trichlorofluoromethane
1,1,2-Trichlorotrifluoroethane
Vinyl Chloride
m and/or p-Xylene
o-Xylene
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
Units 1-__ 2-__ 4-__ 5-__
250 U 20000 U 20000 U 20000 U
250 U 20000 U 20000 U 20000 U
250 U 20000 U 20000 U 20000 U
250 U 20000 U 20000 U 20000 U
250 UJ 20000 UJ 20000 UJ 20000 UJ
250 UJ 20000 U 20000 U 20000 U
250 U 20000 U 20000 U 20000 U
250 UJ 20000 U 20000 U 20000 U
250 U 20000 U 20000 U 20000 U
250 UJ 20000 UJ 20000 UJ 20000 UJ
250 U 20000 U 20000 U 20000 U
250 U 20000 U 20000 U 20000 U
250 U 20000 U 20000 U 20000 U
250 UJ 20000 U 20000 U 20000 U
250 UJ 20000 U 20000 U 20000 U
250 U 20000 U 20000 U 20000 U
250 UJ 20000 U 20000 U 20000 U
250 UJ 20000 U 20000 U 20000 U
250 U 20000 U 20000 U 20000 U
250 U 20000 U 20000 U 20000 U
250 U 20000 U 20000 U 20000 U
250 U 20000 U 20000 U 20000 U
500 U 40000 U 40000 U 40000 U
250 U 20000 U 20000 U 20000 U
250 UJ 20000 U 20000 U 20000 U
250 U 20000 U 20000 U 20000 U
500 U 40000 U 40000 U 40000 U
250 UJ 20000 U 20000 U 20000 U
250 U 20000 U 20000 U 20000 U
250 U 20000 U 20000 U 20000 U
250 U 20000 U 20000 U 20000 U
250 U 20000 U 20000 U 20000 U
250 U 20000 U 20000 U 20000 U
250 U 20000 U 20000 U 20000 U
250 U 20000 U 20000 U 20000 U
250 U 20000 U 20000 U 20000 U
250 U 20000 U 20000 U 20000 U
250 U 20000 U 20000 U 20000 U
250 UJ 20000 U 20000 U 20000 U
500 U 40000 U 40000 U 40000 U
250 U 20000 U 20000 U 20000 U
4846ASR Number: 05/14/2010
MP7ES02Project ID: Cleburn Street well samplingProject Desc:
RLAB Approved Sample Analysis Results
Page 10 of 21
1
1
1
1
1
1
1
Alkalinity in Water by Titration
Anions in Water by Ion Chromatography
Hardness in Water by Calculation
Metals in Water by ICP-AES
TDS or Total Dissolved Solids
Total Organic Carbon in Water
VOCs in Water by GC/MS
Analysis/ Analyte
Alkalinity, total
Sulfate
Hardness as CaCO3
Aluminum
Antimony
Arsenic
Barium
Beryllium
Cadmium
Calcium
Chromium
Cobalt
Copper
Iron
Lead
Magnesium
Manganese
Molybdenum
Nickel
Potassium
Selenium
Silver
Sodium
Thallium
Titanium
Vanadium
Zinc
Solids, total dissolved
Total Organic Carbon
Acetone
Benzene
Bromodichloromethane
Bromoform
Bromomethane
2-Butanone
Carbon Disulfide
Carbon Tetrachloride
Chlorobenzene
Chloroethane
mg/L
mg/L
mg/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
mg/L
ug/L
ug/L
ug/L
ug/L
ug/L
mg/L
ug/L
ug/L
ug/L
mg/L
ug/L
ug/L
mg/L
ug/L
ug/L
ug/L
ug/L
mg/L
mg/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
Units 5-FD 6-__ 7-__ 8-__
285 329 299 202
10000 U 10000 U 10000 U 10000 U
1320 U 1320 U 1620 1600
5000 U 5000 U 5000 U 5000 U
5000 U 5000 U 5000 U 5000 U
2500 U 2500 U 2500 U 2500 U
1000 U 1000 U 1000 U 1000 U
300 U 300 U 300 U 300 U
300 U 300 U 300 U 300 U
200 U 200 U 318 310
1500 U 1500 U 1500 U 1500 U
1000 U 1000 U 1000 U 1000 U
500 U 500 U 500 U 500 U
5000 U 5000 U 5000 U 5000 U
5000 U 5000 U 5000 U 5000 U
200 U 200 U 200 U 200 U
393000 297000 387000 449000
1500 U 1500 U 1500 U 1500 U
2000 U 2000 U 2000 U 2000 U
2430 2420 2690 1660
5000 U 5000 U 5000 U 5000 U
2500 U 2500 U 2500 U 2500 U
500 U 500 U 500 U 500 U
5000 U 5000 U 5000 U 5000 U
2000 U 2000 U 2000 U 2000 U
1000 U 1000 U 1000 U 1000 U
2500 U 2500 U 2500 U 2500 U
12600 14000 14100 10100
1.69 1.68 2.29 1.96
20000 U 20000 U 20000 U 20000 U
20000 U 20000 U 20000 U 20000 U
20000 U 20000 U 20000 U 20000 U
20000 UJ 20000 UJ 20000 UJ 20000 UJ
20000 U 20000 U 20000 U 20000 U
20000 U 20000 U 20000 U 20000 U
20000 U 20000 U 20000 U 20000 U
20000 UJ 20000 UJ 20000 UJ 20000 UJ
20000 U 20000 U 20000 U 20000 U
20000 U 20000 U 20000 U 20000 U
4846ASR Number: 05/14/2010
MP7ES02Project ID: Cleburn Street well samplingProject Desc:
RLAB Approved Sample Analysis Results
Page 11 of 21
Analysis/ Analyte
Chloroform
Chloromethane
Cyclohexane
1,2-Dibromo-3-Chloropropane
Dibromochloromethane
1,2-Dibromoethane
1,2-Dichlorobenzene
1,3-Dichlorobenzene
1,4-Dichlorobenzene
Dichlorodifluoromethane
1,1-Dichloroethane
1,2-Dichloroethane
1,1-Dichloroethene
cis-1,2-Dichloroethene
trans-1,2-Dichloroethene
1,2-Dichloropropane
cis-1,3-Dichloropropene
trans-1,3-Dichloropropene
Ethyl Benzene
2-Hexanone
Isopropylbenzene
Methyl Acetate
Methyl tert-butyl ether
Methylcyclohexane
Methylene Chloride
4-Methyl-2-Pentanone
Naphthalene
Styrene
1,1,2,2-Tetrachloroethane
Tetrachloroethene
Toluene
1,2,3-Trichlorobenzene
1,2,4-Trichlorobenzene
1,1,1-Trichloroethane
1,1,2-Trichloroethane
Trichloroethene
Trichlorofluoromethane
1,1,2-Trichlorotrifluoroethane
Vinyl Chloride
m and/or p-Xylene
o-Xylene
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
Units 5-FD 6-__ 7-__ 8-__
20000 U 20000 U 20000 U 20000 U
20000 U 20000 U 20000 U 20000 U
20000 U 20000 U 20000 U 20000 U
20000 U 20000 U 20000 U 20000 U
20000 UJ 20000 UJ 20000 UJ 20000 UJ
20000 U 20000 U 20000 U 20000 U
20000 U 20000 U 20000 U 20000 U
20000 U 20000 U 20000 U 20000 U
20000 U 20000 U 20000 U 20000 U
20000 UJ 20000 UJ 20000 UJ 20000 UJ
20000 U 20000 U 20000 U 20000 U
20000 U 20000 U 20000 U 20000 U
20000 U 20000 U 20000 U 20000 U
20000 U 20000 U 20000 U 20000 U
20000 U 20000 U 20000 U 20000 U
20000 U 20000 U 20000 U 20000 U
20000 U 20000 U 20000 U 20000 U
20000 U 20000 U 20000 U 20000 U
20000 U 20000 U 20000 U 20000 U
20000 U 20000 U 20000 U 20000 U
20000 U 20000 U 20000 U 20000 U
20000 U 20000 U 20000 U 20000 U
40000 U 40000 U 40000 U 40000 U
20000 U 20000 U 20000 U 20000 U
20000 U 20000 U 20000 U 20000 U
20000 U 20000 U 20000 U 20000 U
40000 U 40000 U 40000 U 40000 U
20000 U 20000 U 20000 U 20000 U
20000 U 20000 U 20000 U 20000 U
20000 U 20000 U 20000 U 20000 U
20000 U 20000 U 20000 U 20000 U
20000 U 20000 U 20000 U 20000 U
20000 U 20000 U 20000 U 20000 U
20000 U 20000 U 20000 U 20000 U
20000 U 20000 U 20000 U 20000 U
20000 U 20000 U 20000 U 20000 U
20000 U 20000 U 20000 U 20000 U
20000 U 20000 U 20000 U 20000 U
20000 U 20000 U 20000 U 20000 U
40000 U 40000 U 40000 U 40000 U
20000 U 20000 U 20000 U 20000 U
4846ASR Number: 05/14/2010
MP7ES02Project ID: Cleburn Street well samplingProject Desc:
RLAB Approved Sample Analysis Results
Page 12 of 21
1
1
1
1
1
1
1
Alkalinity in Water by Titration
Anions in Water by Ion Chromatography
Hardness in Water by Calculation
Metals in Water by ICP-AES
TDS or Total Dissolved Solids
Total Organic Carbon in Water
VOCs in Water by GC/MS
Analysis/ Analyte
Alkalinity, total
Sulfate
Hardness as CaCO3
Aluminum
Antimony
Arsenic
Barium
Beryllium
Cadmium
Calcium
Chromium
Cobalt
Copper
Iron
Lead
Magnesium
Manganese
Molybdenum
Nickel
Potassium
Selenium
Silver
Sodium
Thallium
Titanium
Vanadium
Zinc
Solids, total dissolved
Total Organic Carbon
Acetone
Benzene
Bromodichloromethane
Bromoform
Bromomethane
2-Butanone
Carbon Disulfide
Carbon Tetrachloride
Chlorobenzene
Chloroethane
mg/L
mg/L
mg/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
mg/L
ug/L
ug/L
ug/L
ug/L
ug/L
mg/L
ug/L
ug/L
ug/L
mg/L
ug/L
ug/L
mg/L
ug/L
ug/L
ug/L
ug/L
mg/L
mg/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
Units 9-__ 10-__ 11-__ 12-__
2.00 U 267 309 260
10000 U 10000 U 10000 U 10000 U
1540 2240 1350 1320 U
36200 5000 U 5000 U 5000 U
5000 U 5000 U 5000 U 5000 U
2500 U 2500 U 2500 U 2500 U
1000 U 1000 U 1000 U 1000 U
300 U 300 U 300 U 300 U
300 U 300 U 300 U 300 U
287 569 212 200 U
1500 U 2730 1500 U 1500 U
1000 U 1000 U 1000 U 1000 U
500 U 500 U 500 U 500 U
5000 U 5000 U 5000 U 5000 U
5000 U 5000 U 5000 U 5000 U
200 U 200 U 200 U 200 U
451000 417000 391000 295000
1500 U 1500 U 1500 U 1500 U
2000 U 2400 2000 U 2000 U
2080 1190 2270 2460
5000 U 5000 U 5000 U 5000 U
2500 U 2500 U 2500 U 2500 U
500 U 500 U 500 U 500 U
5000 U 5000 U 5000 U 5000 U
2000 U 2000 U 2000 U 2000 U
1000 U 1000 U 1000 U 1000 U
2500 U 2500 U 2500 U 2500 U
11000 10800 11300 12100
2.1 3 U 3 U 3 U
20000 U 20000 U 20000 U 20000 U
20000 U 20000 U 20000 U 20000 U
20000 U 20000 U 20000 U 20000 U
20000 UJ 20000 UJ 20000 UJ 20000 U
20000 U 20000 U 20000 U 20000 U
20000 U 20000 U 20000 U 20000 U
20000 U 20000 U 20000 U 20000 U
20000 UJ 20000 UJ 20000 UJ 20000 U
20000 U 20000 U 20000 U 20000 U
20000 U 20000 U 20000 U 20000 U
4846ASR Number: 05/14/2010
MP7ES02Project ID: Cleburn Street well samplingProject Desc:
RLAB Approved Sample Analysis Results
Page 13 of 21
Analysis/ Analyte
Chloroform
Chloromethane
Cyclohexane
1,2-Dibromo-3-Chloropropane
Dibromochloromethane
1,2-Dibromoethane
1,2-Dichlorobenzene
1,3-Dichlorobenzene
1,4-Dichlorobenzene
Dichlorodifluoromethane
1,1-Dichloroethane
1,2-Dichloroethane
1,1-Dichloroethene
cis-1,2-Dichloroethene
trans-1,2-Dichloroethene
1,2-Dichloropropane
cis-1,3-Dichloropropene
trans-1,3-Dichloropropene
Ethyl Benzene
2-Hexanone
Isopropylbenzene
Methyl Acetate
Methyl tert-butyl ether
Methylcyclohexane
Methylene Chloride
4-Methyl-2-Pentanone
Naphthalene
Styrene
1,1,2,2-Tetrachloroethane
Tetrachloroethene
Toluene
1,2,3-Trichlorobenzene
1,2,4-Trichlorobenzene
1,1,1-Trichloroethane
1,1,2-Trichloroethane
Trichloroethene
Trichlorofluoromethane
1,1,2-Trichlorotrifluoroethane
Vinyl Chloride
m and/or p-Xylene
o-Xylene
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
Units 9-__ 10-__ 11-__ 12-__
20000 U 20000 U 20000 U 20000 U
20000 U 20000 U 20000 U 20000 U
20000 U 20000 U 20000 U 20000 U
20000 U 20000 U 20000 U 20000 U
20000 UJ 20000 UJ 20000 UJ 20000 U
20000 U 20000 U 20000 U 20000 U
20000 U 20000 U 20000 U 20000 U
20000 U 20000 U 20000 U 20000 U
20000 U 20000 U 20000 U 20000 U
20000 UJ 20000 UJ 20000 UJ 20000 U
20000 U 20000 U 20000 U 20000 U
20000 U 20000 U 20000 U 20000 U
20000 U 20000 U 20000 U 20000 U
20000 U 20000 U 20000 U 20000 U
20000 U 20000 U 20000 U 20000 U
20000 U 20000 U 20000 U 20000 U
20000 U 20000 U 20000 U 20000 U
20000 U 20000 U 20000 U 20000 U
20000 U 20000 U 20000 U 20000 U
20000 U 20000 U 20000 U 20000 U
20000 U 20000 U 20000 U 20000 U
20000 U 20000 U 20000 U 20000 U
40000 U 40000 U 40000 U 40000 U
20000 U 20000 U 20000 U 20000 U
20000 U 20000 U 20000 U 20000 U
20000 U 20000 U 20000 U 20000 U
40000 U 40000 U 40000 U 40000 U
20000 U 20000 U 20000 U 20000 U
20000 U 20000 U 20000 U 20000 U
20000 U 20000 U 20000 U 20000 U
20000 U 20000 U 20000 U 20000 U
20000 U 20000 U 20000 U 20000 U
20000 U 20000 U 20000 U 20000 U
20000 U 20000 U 20000 U 20000 U
20000 U 20000 U 20000 U 20000 U
20000 U 20000 U 20000 U 20000 U
20000 U 20000 U 20000 U 20000 U
20000 U 20000 U 20000 U 20000 U
20000 U 20000 U 20000 U 20000 U
40000 U 40000 U 40000 U 40000 U
20000 U 20000 U 20000 U 20000 U
4846ASR Number: 05/14/2010
MP7ES02Project ID: Cleburn Street well samplingProject Desc:
RLAB Approved Sample Analysis Results
Page 14 of 21
1
1
1
1
1
1
1
Alkalinity in Water by Titration
Anions in Water by Ion Chromatography
Hardness in Water by Calculation
Metals in Water by ICP-AES
TDS or Total Dissolved Solids
Total Organic Carbon in Water
VOCs in Water by GC/MS
Analysis/ Analyte
Alkalinity, total
Sulfate
Hardness as CaCO3
Aluminum
Antimony
Arsenic
Barium
Beryllium
Cadmium
Calcium
Chromium
Cobalt
Copper
Iron
Lead
Magnesium
Manganese
Molybdenum
Nickel
Potassium
Selenium
Silver
Sodium
Thallium
Titanium
Vanadium
Zinc
Solids, total dissolved
Total Organic Carbon
Acetone
Benzene
Bromodichloromethane
Bromoform
Bromomethane
2-Butanone
Carbon Disulfide
Carbon Tetrachloride
Chlorobenzene
Chloroethane
mg/L
mg/L
mg/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
mg/L
ug/L
ug/L
ug/L
ug/L
ug/L
mg/L
ug/L
ug/L
ug/L
mg/L
ug/L
ug/L
mg/L
ug/L
ug/L
ug/L
ug/L
mg/L
mg/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
Units 12-FD 14-__ 15-__ 16-__
263 249 233 144
10000 U 10000 U 10000 U 33.7
1320 U 1320 U 1580 200
5000 U 5000 U 5000 U 216
5000 U 5000 U 5000 U 50 U
2500 U 2500 U 2500 U 25 U
1000 U 1000 U 1000 U 358
300 U 300 U 300 U 3 U
300 U 300 U 300 U 3 U
200 U 200 U 302 63.6
1500 U 1500 U 11500 15 U
1000 U 1000 U 1000 U 10 U
500 U 500 U 500 U 5 U
5000 U 5000 U 5000 U 293
5000 U 5000 U 5000 U 50 U
200 U 200 U 200 U 9.91
262000 267000 325000 16
1500 U 1500 U 1500 U 15 U
2000 U 2000 U 2000 U 20 U
2350 2380 200 U 10.1
5000 U 5000 U 5000 U 50 U
2500 U 2500 U 2500 U 25 U
500 U 500 U 500 U 14.1
5000 U 5000 U 5000 U 50 U
2000 U 2000 U 2000 U 20 U
1000 U 1000 U 1000 U 10 U
2500 U 2500 U 2500 U 27
12600 11900 3160 322
3 U 3 U 3 U 1.15
20000 U 20000 U 10000 U 5.0 U
20000 U 20000 U 10000 U 5.0 U
20000 U 20000 U 10000 U 5.0 U
20000 U 20000 U 10000 U 5.0 U
20000 U 20000 U 10000 U 5.0 UJ
20000 U 20000 U 10000 U 5.0 U
20000 U 20000 U 10000 U 5.0 U
20000 U 20000 U 10000 U 5.0 U
20000 U 20000 U 10000 U 5.0 U
20000 U 20000 U 10000 U 5.0 UJ
4846ASR Number: 05/14/2010
MP7ES02Project ID: Cleburn Street well samplingProject Desc:
RLAB Approved Sample Analysis Results
Page 15 of 21
Analysis/ Analyte
Chloroform
Chloromethane
Cyclohexane
1,2-Dibromo-3-Chloropropane
Dibromochloromethane
1,2-Dibromoethane
1,2-Dichlorobenzene
1,3-Dichlorobenzene
1,4-Dichlorobenzene
Dichlorodifluoromethane
1,1-Dichloroethane
1,2-Dichloroethane
1,1-Dichloroethene
cis-1,2-Dichloroethene
trans-1,2-Dichloroethene
1,2-Dichloropropane
cis-1,3-Dichloropropene
trans-1,3-Dichloropropene
Ethyl Benzene
2-Hexanone
Isopropylbenzene
Methyl Acetate
Methyl tert-butyl ether
Methylcyclohexane
Methylene Chloride
4-Methyl-2-Pentanone
Naphthalene
Styrene
1,1,2,2-Tetrachloroethane
Tetrachloroethene
Toluene
1,2,3-Trichlorobenzene
1,2,4-Trichlorobenzene
1,1,1-Trichloroethane
1,1,2-Trichloroethane
Trichloroethene
Trichlorofluoromethane
1,1,2-Trichlorotrifluoroethane
Vinyl Chloride
m and/or p-Xylene
o-Xylene
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
Units 12-FD 14-__ 15-__ 16-__
20000 U 20000 U 10000 U 5.0 U
20000 U 20000 U 10000 U 5.0 U
20000 U 20000 U 10000 U 5.0 U
20000 U 20000 U 10000 U 5.0 U
20000 U 20000 U 10000 U 5.0 U
20000 U 20000 U 10000 U 5.0 U
20000 U 20000 U 10000 U 5.0 U
20000 U 20000 U 10000 U 5.0 UJ
20000 U 20000 U 10000 U 5.0 U
20000 U 20000 U 10000 U 5.0 U
20000 U 20000 U 10000 U 5.0 U
20000 U 20000 U 10000 U 5.0 U
20000 U 20000 U 10000 U 5.0 U
20000 U 20000 U 10000 U 5.0 U
20000 U 20000 U 10000 U 5.0 U
20000 U 20000 U 10000 U 5.0 U
20000 U 20000 U 10000 U 5.0 U
20000 U 20000 U 10000 U 5.0 U
20000 U 20000 U 10000 U 5.0 U
20000 U 20000 U 10000 U 5.0 U
20000 U 20000 U 10000 U 5.0 U
20000 U 20000 U 10000 U 5.0 U
40000 U 40000 U 20000 U 10 U
20000 U 20000 U 10000 U 5.0 U
20000 U 20000 U 10000 U 5.0 UJ
20000 U 20000 U 10000 U 5.0 U
40000 U 40000 U 20000 U 10 U
20000 U 20000 U 10000 U 5.0 U
20000 U 20000 U 10000 U 5.0 U
20000 U 20000 U 10000 U 5.0 U
20000 U 20000 U 10000 U 5.0 U
20000 U 20000 U 10000 U 5.0 U
20000 U 20000 U 10000 U 5.0 U
20000 U 20000 U 10000 U 5.0 U
20000 U 20000 U 10000 U 5.0 U
20000 U 20000 U 10000 U 5.0 U
20000 U 20000 U 10000 U 5.0 U
20000 U 20000 U 10000 U 5.0 U
20000 U 20000 U 10000 U 5.0 U
40000 U 40000 U 20000 U 10 U
20000 U 20000 U 10000 U 5.0 U
4846ASR Number: 05/14/2010
MP7ES02Project ID: Cleburn Street well samplingProject Desc:
RLAB Approved Sample Analysis Results
Page 16 of 21
1
1
1
1
1
1
1
Alkalinity in Water by Titration
Anions in Water by Ion Chromatography
Hardness in Water by Calculation
Metals in Water by ICP-AES
TDS or Total Dissolved Solids
Total Organic Carbon in Water
VOCs in Water by GC/MS
Analysis/ Analyte
Alkalinity, total
Sulfate
Hardness as CaCO3
Aluminum
Antimony
Arsenic
Barium
Beryllium
Cadmium
Calcium
Chromium
Cobalt
Copper
Iron
Lead
Magnesium
Manganese
Molybdenum
Nickel
Potassium
Selenium
Silver
Sodium
Thallium
Titanium
Vanadium
Zinc
Solids, total dissolved
Total Organic Carbon
Acetone
Benzene
Bromodichloromethane
Bromoform
Bromomethane
2-Butanone
Carbon Disulfide
Carbon Tetrachloride
Chlorobenzene
Chloroethane
mg/L
mg/L
mg/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
mg/L
ug/L
ug/L
ug/L
ug/L
ug/L
mg/L
ug/L
ug/L
ug/L
mg/L
ug/L
ug/L
mg/L
ug/L
ug/L
ug/L
ug/L
mg/L
mg/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
Units 17-__ 17-FD 18-__ 19-__
69.9 69.2 157 256
81.5 81.8 62.7 J 10000 U
245 228 213 1320 U
77 50 U 159 5000 U
50 U 50 U 50 U 5000 U
25 U 25 U 25 U 2500 U
162 145 192 1000 U
3 U 3 U 3 U 300 U
3 U 3 U 3 U 300 U
69.1 64.3 61.8 200 U
461 16 15 U 1500 U
10 U 10 U 10 U 1000 U
7 5 U 5 U 500 U
2350 123 167 5000 U
50 U 50 U 50 U 5000 U
17.6 16.3 14.3 200 U
6 5 45 287000
15 U 15 U 15 U 1500 U
41 33.1 20 U 2000 U
14.6 13.8 8.22 3730
50 U 50 U 50 U 5000 U
25 U 25 U 25 U 2500 U
55.1 50.6 91.5 500 U
50 U 50 U 50 U 5000 U
20 U 20 U 20 U 2000 U
10 U 10 U 10 U 1000 U
25 U 25 U 25 U 2500 U
553 J 525 500 20000
3 U 3 U 2.66 1 U
5.0 U 5.0 U 5.0 U 20000 U
5.0 U 5.0 U 5.0 U 20000 U
5.0 U 5.0 U 5.0 U 20000 U
5.0 U 5.0 U 5.0 U 20000 U
5.0 U 5.0 U 5.0 U 20000 U
5.0 U 5.0 U 5.0 U 20000 U
5.0 U 5.0 U 5.0 U 20000 U
5.0 U 5.0 U 5.0 U 20000 U
5.0 U 5.0 U 5.0 U 20000 U
5.0 U 5.0 U 5.0 U 20000 U
4846ASR Number: 05/14/2010
MP7ES02Project ID: Cleburn Street well samplingProject Desc:
RLAB Approved Sample Analysis Results
Page 17 of 21
Analysis/ Analyte
Chloroform
Chloromethane
Cyclohexane
1,2-Dibromo-3-Chloropropane
Dibromochloromethane
1,2-Dibromoethane
1,2-Dichlorobenzene
1,3-Dichlorobenzene
1,4-Dichlorobenzene
Dichlorodifluoromethane
1,1-Dichloroethane
1,2-Dichloroethane
1,1-Dichloroethene
cis-1,2-Dichloroethene
trans-1,2-Dichloroethene
1,2-Dichloropropane
cis-1,3-Dichloropropene
trans-1,3-Dichloropropene
Ethyl Benzene
2-Hexanone
Isopropylbenzene
Methyl Acetate
Methyl tert-butyl ether
Methylcyclohexane
Methylene Chloride
4-Methyl-2-Pentanone
Naphthalene
Styrene
1,1,2,2-Tetrachloroethane
Tetrachloroethene
Toluene
1,2,3-Trichlorobenzene
1,2,4-Trichlorobenzene
1,1,1-Trichloroethane
1,1,2-Trichloroethane
Trichloroethene
Trichlorofluoromethane
1,1,2-Trichlorotrifluoroethane
Vinyl Chloride
m and/or p-Xylene
o-Xylene
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
Units 17-__ 17-FD 18-__ 19-__
5.0 U 5.0 U 6.0 20000 U
5.0 U 5.0 U 5.0 U 20000 U
5.0 U 5.0 U 5.0 U 20000 U
5.0 U 5.0 U 5.0 U 20000 U
5.0 U 5.0 U 5.0 U 20000 U
5.0 U 5.0 U 5.0 U 20000 U
5.0 U 5.0 U 5.0 U 20000 U
5.0 U 5.0 U 5.0 U 20000 U
5.0 U 5.0 U 5.0 U 20000 U
5.0 U 5.0 U 5.0 U 20000 U
5.0 U 5.0 U 5.0 U 20000 U
5.0 U 5.0 U 5.0 U 20000 U
5.0 U 5.0 U 5.0 U 20000 U
5.0 U 5.0 U 10 20000 U
5.0 U 5.0 U 5.0 U 20000 U
5.0 U 5.0 U 5.0 U 20000 U
5.0 U 5.0 U 5.0 U 20000 U
5.0 U 5.0 U 5.0 U 20000 U
5.0 U 5.0 U 5.0 U 20000 U
5.0 U 5.0 U 5.0 U 20000 U
5.0 U 5.0 U 5.0 U 20000 U
5.0 U 5.0 U 5.0 U 20000 U
10 U 10 U 10 U 40000 U
5.0 U 5.0 U 5.0 U 20000 U
5.0 U 5.0 U 5.0 U 20000 U
5.0 U 5.0 U 5.0 U 20000 U
10 U 10 U 10 U 40000 U
5.0 U 5.0 U 5.0 U 20000 U
5.0 U 5.0 U 5.0 U 20000 U
7.8 7.0 3600 J 20000 U
5.0 U 5.0 U 5.0 U 20000 U
5.0 U 5.0 U 5.0 U 20000 U
5.0 U 5.0 U 5.0 U 20000 U
5.0 U 5.0 U 5.0 U 20000 U
5.0 U 5.0 U 5.0 U 20000 U
5.0 U 5.0 U 290 J 20000 U
5.0 U 5.0 U 5.0 U 20000 U
5.0 U 5.0 U 5.0 U 20000 U
5.0 U 5.0 U 5.0 U 20000 U
10 U 10 U 10 U 40000 U
5.0 U 5.0 U 5.3 20000 U
4846ASR Number: 05/14/2010
MP7ES02Project ID: Cleburn Street well samplingProject Desc:
RLAB Approved Sample Analysis Results
Page 18 of 21
1
1
1
1
1
1
1
Alkalinity in Water by Titration
Anions in Water by Ion Chromatography
Hardness in Water by Calculation
Metals in Water by ICP-AES
TDS or Total Dissolved Solids
Total Organic Carbon in Water
VOCs in Water by GC/MS
Analysis/ Analyte
Alkalinity, total
Sulfate
Hardness as CaCO3
Aluminum
Antimony
Arsenic
Barium
Beryllium
Cadmium
Calcium
Chromium
Cobalt
Copper
Iron
Lead
Magnesium
Manganese
Molybdenum
Nickel
Potassium
Selenium
Silver
Sodium
Thallium
Titanium
Vanadium
Zinc
Solids, total dissolved
Total Organic Carbon
Acetone
Benzene
Bromodichloromethane
Bromoform
Bromomethane
2-Butanone
Carbon Disulfide
Carbon Tetrachloride
Chlorobenzene
Chloroethane
mg/L
mg/L
mg/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
mg/L
ug/L
ug/L
ug/L
ug/L
ug/L
mg/L
ug/L
ug/L
ug/L
mg/L
ug/L
ug/L
mg/L
ug/L
ug/L
ug/L
ug/L
mg/L
mg/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
Units 20-__ 21-__ 22-__ 26-FB
245 221 204
10000 U 10000 U 10000 U
1320 U 1320 U 1320 U 13.2 U
5000 U 5000 U 5000 U 50 U
5000 U 5000 U 5000 U 50 U
2500 U 2500 U 2500 U 25 U
1000 U 1000 U 1000 U 10 U
300 U 300 U 300 U 3 U
300 U 300 U 300 U 3 U
200 U 200 U 200 U 2.00 U
1500 U 1500 U 1500 U 15 U
1000 U 1000 U 1000 U 10 U
500 U 500 U 500 U 5 U
5000 U 5000 U 5000 U 112
5000 U 5000 U 5000 U 50 U
200 U 200 U 200 U 2.00 U
378000 416000 544000 5 U
1500 U 1500 U 1500 U 15 U
2000 U 2000 U 2000 U 20 U
1770 1530 1370 2.00 U
5000 U 5000 U 5000 U 50 U
2500 U 2500 U 2500 U 25 U
500 U 500 U 500 U 5.00 U
5000 U 5000 U 5000 U 50 U
2000 U 2000 U 2000 U 20 U
1000 U 1000 U 1000 U 10 U
2500 U 2500 U 2500 U 25 U
9320 6620 6000
1 U 1.52 1 U 1 U
20000 U 20000 U 20000 U 5.0 U
20000 U 20000 U 20000 U 5.0 U
20000 U 20000 U 20000 U 5.0 U
20000 U 20000 U 20000 U 5.0 UJ
20000 U 20000 U 20000 U 5.0 U
20000 U 20000 U 20000 U 5.0 U
20000 U 20000 U 20000 U 5.0 U
20000 U 20000 U 20000 U 5.0 UJ
20000 U 20000 U 20000 U 5.0 U
20000 U 20000 U 20000 U 5.0 U
4846ASR Number: 05/14/2010
MP7ES02Project ID: Cleburn Street well samplingProject Desc:
RLAB Approved Sample Analysis Results
Page 19 of 21
Analysis/ Analyte
Chloroform
Chloromethane
Cyclohexane
1,2-Dibromo-3-Chloropropane
Dibromochloromethane
1,2-Dibromoethane
1,2-Dichlorobenzene
1,3-Dichlorobenzene
1,4-Dichlorobenzene
Dichlorodifluoromethane
1,1-Dichloroethane
1,2-Dichloroethane
1,1-Dichloroethene
cis-1,2-Dichloroethene
trans-1,2-Dichloroethene
1,2-Dichloropropane
cis-1,3-Dichloropropene
trans-1,3-Dichloropropene
Ethyl Benzene
2-Hexanone
Isopropylbenzene
Methyl Acetate
Methyl tert-butyl ether
Methylcyclohexane
Methylene Chloride
4-Methyl-2-Pentanone
Naphthalene
Styrene
1,1,2,2-Tetrachloroethane
Tetrachloroethene
Toluene
1,2,3-Trichlorobenzene
1,2,4-Trichlorobenzene
1,1,1-Trichloroethane
1,1,2-Trichloroethane
Trichloroethene
Trichlorofluoromethane
1,1,2-Trichlorotrifluoroethane
Vinyl Chloride
m and/or p-Xylene
o-Xylene
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
Units 20-__ 21-__ 22-__ 26-FB
20000 U 20000 U 20000 U 5.0 U
20000 U 20000 U 20000 U 5.0 U
20000 U 20000 U 20000 U 5.0 U
20000 U 20000 U 20000 U 5.0 U
20000 U 20000 U 20000 U 5.0 UJ
20000 U 20000 U 20000 U 5.0 U
20000 U 20000 U 20000 U 5.0 U
20000 U 20000 U 20000 U 5.0 U
20000 U 20000 U 20000 U 5.0 U
20000 U 20000 U 20000 U 5.0 UJ
20000 U 20000 U 20000 U 5.0 U
20000 U 20000 U 20000 U 5.0 U
20000 U 20000 U 20000 U 5.0 U
20000 U 20000 U 20000 U 5.0 U
20000 U 20000 U 20000 U 5.0 U
20000 U 20000 U 20000 U 5.0 U
20000 U 20000 U 20000 U 5.0 U
20000 U 20000 U 20000 U 5.0 U
20000 U 20000 U 20000 U 5.0 U
20000 U 20000 U 20000 U 5.0 U
20000 U 20000 U 20000 U 5.0 U
20000 U 20000 U 20000 U 5.0 U
40000 U 40000 U 40000 U 10 U
20000 U 20000 U 20000 U 5.0 U
20000 U 20000 U 20000 U 5.0 U
20000 U 20000 U 20000 U 5.0 U
40000 U 40000 U 40000 U 10 U
20000 U 20000 U 20000 U 5.0 U
20000 U 20000 U 20000 U 5.0 U
20000 U 20000 U 20000 U 5.0 U
20000 U 20000 U 20000 U 5.0 U
20000 U 20000 U 20000 U 5.0 U
20000 U 20000 U 20000 U 5.0 U
20000 U 20000 U 20000 U 5.0 U
20000 U 20000 U 20000 U 5.0 U
20000 U 20000 U 20000 U 5.0 U
20000 U 20000 U 20000 U 5.0 U
20000 U 20000 U 20000 U 5.0 U
20000 U 20000 U 20000 U 5.0 U
40000 U 40000 U 40000 U 10 U
20000 U 20000 U 20000 U 5.0 U
4846ASR Number: 05/14/2010
MP7ES02Project ID: Cleburn Street well samplingProject Desc:
RLAB Approved Sample Analysis Results
Page 20 of 21
1 VOCs in Water by GC/MS
Analysis/ Analyte
Acetone
Benzene
Bromodichloromethane
Bromoform
Bromomethane
2-Butanone
Carbon Disulfide
Carbon Tetrachloride
Chlorobenzene
Chloroethane
Chloroform
Chloromethane
Cyclohexane
1,2-Dibromo-3-Chloropropane
Dibromochloromethane
1,2-Dibromoethane
1,2-Dichlorobenzene
1,3-Dichlorobenzene
1,4-Dichlorobenzene
Dichlorodifluoromethane
1,1-Dichloroethane
1,2-Dichloroethane
1,1-Dichloroethene
cis-1,2-Dichloroethene
trans-1,2-Dichloroethene
1,2-Dichloropropane
cis-1,3-Dichloropropene
trans-1,3-Dichloropropene
Ethyl Benzene
2-Hexanone
Isopropylbenzene
Methyl Acetate
Methyl tert-butyl ether
Methylcyclohexane
Methylene Chloride
4-Methyl-2-Pentanone
Naphthalene
Styrene
1,1,2,2-Tetrachloroethane
Tetrachloroethene
Toluene
1,2,3-Trichlorobenzene
1,2,4-Trichlorobenzene
1,1,1-Trichloroethane
1,1,2-Trichloroethane
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
Units 27-FB 28-FB 29-FB
5.0 U 5.0 U 5.0 U
5.0 U 5.0 U 5.0 U
5.0 U 5.0 U 5.0 U
5.0 UJ 5.0 UJ 5.0 UJ
5.0 U 5.0 U 5.0 U
5.0 U 5.0 U 5.0 U
5.0 U 5.0 U 5.0 U
5.0 UJ 5.0 UJ 5.0 UJ
5.0 U 5.0 U 5.0 U
5.0 U 5.0 U 5.0 U
5.0 U 5.0 U 5.0 U
5.0 U 5.0 U 5.0 U
5.0 U 5.0 U 5.0 U
5.0 U 5.0 U 5.0 U
5.0 UJ 5.0 UJ 5.0 UJ
5.0 U 5.0 U 5.0 U
5.0 U 5.0 U 5.0 U
5.0 U 5.0 U 5.0 U
5.0 U 5.0 U 5.0 U
5.0 UJ 5.0 UJ 5.0 UJ
5.0 U 5.0 U 5.0 U
5.0 U 5.0 U 5.0 U
5.0 U 5.0 U 5.0 U
5.0 U 5.0 U 5.0 U
5.0 U 5.0 U 5.0 U
5.0 U 5.0 U 5.0 U
5.0 U 5.0 U 5.0 U
5.0 U 5.0 U 5.0 U
5.0 U 5.0 U 5.0 U
5.0 U 5.0 U 5.0 U
5.0 U 5.0 U 5.0 U
5.0 U 5.0 U 5.0 U
10 U 10 U 10 U
5.0 U 5.0 U 5.0 U
5.0 U 5.0 U 5.0 U
5.0 U 5.0 U 5.0 U
10 U 10 U 10 U
5.0 U 5.0 U 5.0 U
5.0 U 5.0 U 5.0 U
5.0 U 5.0 U 5.0 U
5.0 U 5.0 U 5.0 U
5.0 U 5.0 U 5.0 U
5.0 U 5.0 U 5.0 U
5.0 U 5.0 U 5.0 U
5.0 U 5.0 U 5.0 U
4846ASR Number: 05/14/2010
MP7ES02Project ID: Cleburn Street well samplingProject Desc:
RLAB Approved Sample Analysis Results
Page 21 of 21
Analysis/ Analyte
Trichloroethene
Trichlorofluoromethane
1,1,2-Trichlorotrifluoroethane
Vinyl Chloride
m and/or p-Xylene
o-Xylene
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
Units 27-FB 28-FB 29-FB
5.0 U 5.0 U 5.0 U
5.0 U 5.0 U 5.0 U
5.0 U 5.0 U 5.0 U
5.0 U 5.0 U 5.0 U
10 U 10 U 10 U
5.0 U 5.0 U 5.0 U
4846ASR Number: 05/14/2010
MP7ES02Project ID: Cleburn Street well samplingProject Desc:
RLAB Approved Sample Analysis Results
4846
MP7ES02Project ID:
Cleburn Street well sampling
Mary PetersonSUPR/IANE
United States Environmental Protection AgencyRegion VII
901 N. 5th StreetKansas City, KS 66101
__/__/____
Data Disposition/Sample Release for ASR #:
Project Description:
Subject:
Kaye DollmannENSV/RLAB
I have received and reviewed the Transmittal of Sample Analysis Results for the above-referencedAnalytical Services Request(ASR) and have indicated my findings below by checking one of theboxes for Data Disposition.
I understand all samples will be disposed upon receipt of this form, unless samples are requestedto be held. If I do not return this form all samples will be disposed of on ___________________.
"RELEASED" - Read-only to all Region 7 employees and contractors that have R7LIMS"Customer" account. All Samples may be disposed of upon receipt of this form if not requested tobe held.
"Project Manager Accessible" - Available on the LAN in R7LIMS for my use only. All Samples maybe disposed of upon receipt of this form if not requested to be held.
"Archived" - THIS DATA IS OF A SENSITIVE NATURE. Any future reports must be requestedthrough the laboratory. All samples may be disposed of upon receipt of the form if not requestedto be held.
Date:
From:
To:
Hold Samples - I have determined that the samples need to be held until ______________, afterwhich time they will be disposed of in accordance with applicable regulations. The reason for the hold is:
Samples are associated with a legal proceeding.
Question/Concern with data - possible reanalysis requested.
Other:________________________________________________________________
Page 1 of 17
05/21/2010Date:
4862
MP7ES02
Cleburn Street well sampling
Mary PetersonSUPR/IANE
Transmittal of Sample Analysis Results for ASR #:
Project ID:
Project Description:
Michael F. Davis, ChiefChemical Analysis and Response Branch, Environmental Services Division
To:
Enclosed are the analytical data for the above-referenced Analytical Services Request (ASR) andProject. The Regional Laboratory has reviewed and verified the results in accordance with proceduresdescribed in our Quality Manual (QM). In addition to all of the analytical results, this transmittalcontains pertinent information that may have influenced the reported results and documents anydeviations from the established requirements of the QM.
Please contact us within 14 days of receipt of this package if you determine there is a need for anychanges. Please complete the enclosed Customer Satisfaction Survey and Data Disposition/SampleRelease memo for this ASR as soon as possible. The process of disposing of the samples for this ASRwill be initiated 30 days from the date of this transmittal unless an alternate release date is specifiedon the Data Disposition/Sample Release memo.
If you have any questions or concerns relating to this data package, contact our customer service lineat 913-551-5295.
Enclosures
cc: Analytical Data File.
United States Environmental Protection AgencyRegion 7
901 N. 5th StreetKansas City, KS 66101
Subject:
From:
Page 2 of 17
4862ASR Number: 05/21/2010
Mary Peterson SUPR/IANE 913-551-7882
MP7ES02
Cleburn Street well sampling
Grand Island Nebraska Superfund
CLEBURN STREET WELL - 1 HR MARTINIZING GWRESORATION
07ESSite ID: 02
Site Cleanup Support
Injection sampling event (w/ASR #4846).
Samples collected using new preservative.
Project Manager: Org: Phone:
Project ID:
Project Desc:
Location: State: Program:
Site Name: Site OU:
Purpose:
__ = Field SampleFB = Field BlankFD = Field Duplicate
QC Codes identify the type of sample for quality control purpose.
Degrees CelsiusNephelometric Turbidity UnitsStandard Units (pH)Micrograms per LiterMicromhos per Centimeter
Specific units in which results arereported.
The identification of the analyte is acceptable; the reported value is anestimate.The analyte was not detected at or above the reporting limit.The analyte was not detected at or above the reporting limit. The reportinglimit is an estimate.
Specific codes used in conjunction with data values to provide additional information on the quality of reported results, or used to explain the absence of a specific value.
Summary of Project Information
Explanation of Codes, Units and Qualifiers used on this report
Sample QC Codes: Units:
J
UUJ
=
==
Data Qualifiers:
= Values have been reviewed and found acceptable for use. (Blank)
Deg CNTUSU
ug/Lumhos/cm
=====
2009073QAPP Number:
302DD2CGPRA PRC:
Page 3 of 17
101
102
104
105
105
106
107
108
109
110
111
112
112
114
115
119
120
121
122
126
129
SampleNo
__
__
__
__
FD
__
__
__
__
__
__
__
FD
__
__
__
__
__
__
FB
FB
QCCode
Water
Water
Water
Water
Water
Water
Water
Water
Water
Water
Water
Water
Water
Water
Water
Water
Water
Water
Water
Water
Water
Matrix
ERT-15
IW-1
IW-2
IW-3
IW-3
IW-4
IW-5
IW-6
IW-7
ERT-16
IW-9
IW-8
IW-8/Field Duplicate of sample112IW-10
MW-2A
DPE-4
DPE-3
DPE-1
DPE-2
Preservative Blank sample
Trip Blank sample
Location DescriptionExternal
Sample No
04/05/2010
04/05/2010
04/05/2010
04/05/2010
04/05/2010
04/06/2010
04/06/2010
04/06/2010
04/06/2010
04/06/2010
04/07/2010
04/07/2010
04/07/2010
04/07/2010
04/07/2010
04/08/2010
04/08/2010
04/08/2010
04/08/2010
04/07/2010
Start Date
14:45
16:40
17:50
08:50
08:50
10:10
11:30
13:10
15:55
18:55
09:40
11:00
11:00
12:20
13:40
10:25
11:40
15:40
16:45
08:00
Start Time
04/05/2010
End Date
15:00
End Time
04/06/2010
04/07/2010
04/07/2010
04/07/2010
04/07/2010
04/07/2010
04/07/2010
04/07/2010
04/07/2010
04/08/2010
04/08/2010
04/08/2010
04/08/2010
04/08/2010
04/08/2010
04/09/2010
04/09/2010
04/09/2010
04/09/2010
04/08/2010
04/06/2010
ReceiptDate
4862 05/21/2010
MP7ES02Project ID: Cleburn Street well samplingProject Desc:
ASR Number: Sample Information Summary
-
-
-
-
-
-
-
-
-
-
-
-
-
-
-
-
-
-
-
-
-
Page 4 of 17
1
1
1
1
1
Conductivity by Field Measurement
pH of Water by Field Measurement
Temperature of Water by Field Measurement
Turbidity of Water by Field Measurement
VOCs in Water by GC/MS
(Field Measurement)
(Field Measurement)
(Field Measurement)
(Field Measurement)
Region 7 EPA Laboratory - Kansas City, Ks.
Lab:
Lab:
Lab:
Lab:
Lab:
Measurement of field parameter
Measurement of field parameter
Measurement of field parameter
Measurement of field parameter
EPA Region 7 RLAB Method 3230.1F
Method:
Method:
Method:
Method:
Method:
(N/A)
(N/A)
(N/A)
(N/A)
Permanganate in the samples caused significant interference with the analysis, withInternal Standards and Surrogates having low response. This required coding for hits andnon-detects for several compounds. All coded hits for analyzed compounds are most likelylower than actual values. There is significant UJ-coding, indicating that the reporting limits
Comments:
Comments:
Comments:
Comments:
Comments:
101-__
101-__
101-__
101-__
101-__ 102-__ 104-__ 105-__ 105-FD 106-__ 107-__108-__ 109-__ 110-__ 111-__ 112-__ 112-FD 114-__115-__ 119-__ 120-__ 121-__ 122-__ 126-FB 129-FB
Samples:
Samples:
Samples:
Samples:
Samples:
4862ASR Number: 05/21/2010
MP7ES02Project ID: Cleburn Street well samplingProject Desc
RLAB Approved Analysis Comments
Analysis Comments About Results For This Analysis
Page 5 of 17
for the coded analytes are estimates and the actual reporting limits may be higher.
For the sake of brevity, it can be assumed that all codes not mentioned below are relatedto the permanganate interference, and no further explanatory comments will be posted inthe analysis report. Non-coded data meet all quality control requirements.
Samples 102-114 were diluted to reduce interference from precipitate in the sample vials.They have been reported at a dilution of 2x with a raised reporting limit .
Samples 107 and 110 required a 10x dilution for Carbon Tetrachloride.
Sample 109 was over the calibration range for Carbon Tetrachloride and Chloroform.Sample could not be rerun due to instrument issues. The values reported have been J-coded as they are estimates and may be biased low.
Acid preservation was buffered by the addition of Ascorbic acid. All samples were betweena pH of 2 and 4. The presence of the Ascorbic Acid has been shown to preserve theanalytes in the samples, as the presence of Permanganate, which was neutralized, wouldhave degraded the analytes of interest much more severely than the passage of time.
Samples 102, 104, 105, 105FD, 106-110 were analyzed past the 14-day holding times.This was not used to qualify data, as samples were within 4-14.5 hrs of the holding times.102 - 6.5hrs late104 - 4105 - 14105FD - 14.5106 - 14107 - 13.5108 - 12.5109 - 10110 - 8
Methylene Chloride was UJ-coded in samples 101, 126FB and 129FB. This analyte was notfound in the samples at or above the reporting limit, however, the reporting limit is anestimate (UJ-coded) due to low recovery of this analyte in the laboratory control sample.The actual reporting limit for this analyte may be higher than the reported value.
4862ASR Number: 05/21/2010
MP7ES02Project ID: Cleburn Street well samplingProject Desc
RLAB Approved Analysis Comments
Analysis Comments About Results For This Analysis
Page 6 of 17
1
1
1
1
1
Conductivity by Field Measurement
pH of Water by Field Measurement
Temperature of Water by Field Measurement
Turbidity of Water by Field Measurement
VOCs in Water by GC/MS
Analysis/ Analyte
Conductivity
pH
Temperature
Turbidity
Acetone
Benzene
Bromodichloromethane
Bromoform
Bromomethane
2-Butanone
Carbon Disulfide
Carbon Tetrachloride
Chlorobenzene
Chloroethane
Chloroform
Chloromethane
Cyclohexane
1,2-Dibromo-3-Chloropropane
Dibromochloromethane
1,2-Dibromoethane
1,2-Dichlorobenzene
1,3-Dichlorobenzene
1,4-Dichlorobenzene
Dichlorodifluoromethane
1,1-Dichloroethane
1,2-Dichloroethane
1,1-Dichloroethene
cis-1,2-Dichloroethene
trans-1,2-Dichloroethene
1,2-Dichloropropane
cis-1,3-Dichloropropene
trans-1,3-Dichloropropene
Ethyl Benzene
2-Hexanone
Isopropylbenzene
Methyl Acetate
Methyl tert-butyl ether
Methylcyclohexane
Methylene Chloride
4-Methyl-2-Pentanone
Naphthalene
umhos/cm
SU
Deg C
NTU
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
Units 101-__ 102-__ 104-__ 105-__
830
6.76
14.75
0.0
8.8 110 J 120 J 130 J
5.0 U 10 U 10 U 10 UJ
5.0 U 10 U 10 U 10 UJ
5.0 UJ 10 U 10 U 10 UJ
5.0 U 10 U 10 U 10 U
5.0 U 10 UJ 10 UJ 10 UJ
5.0 U 10 U 10 U 10 U
5.0 U 10 U 10 U 10 U
5.0 U 10 U 10 U 10 UJ
5.0 U 10 U 10 U 10 U
5.0 U 10 U 10 U 10 U
5.0 U 10 U 10 U 10 U
5.0 U 10 U 10 U 10 U
5.0 U 10 U 10 U 10 UJ
5.0 U 10 U 10 U 10 UJ
5.0 UJ 10 U 10 U 10 UJ
5.0 U 10 U 10 U 10 UJ
5.0 U 10 U 10 U 10 UJ
5.0 U 10 U 10 U 10 UJ
5.0 U 10 U 10 U 10 U
5.0 U 10 U 10 U 10 U
5.0 U 10 U 10 U 10 UJ
5.0 U 10 U 10 U 10 U
5.0 U 10 U 10 U 10 U
5.0 U 10 U 10 U 10 U
5.0 U 10 U 10 U 10 UJ
5.0 U 10 U 10 U 10 UJ
5.0 U 10 U 10 U 10 UJ
5.0 U 10 U 10 U 10 UJ
5.0 U 10 U 10 U 10 UJ
5.0 U 10 U 10 U 10 UJ
5.0 UJ 10 U 10 U 10 U
10 U 20 U 20 U 20 U
5.0 U 10 U 10 U 10 UJ
5.0 UJ 10 U 10 U 10 U
5.0 UJ 10 U 10 U 10 UJ
10 UJ 20 U 20 U 20 UJ
4862ASR Number: 05/21/2010
MP7ES02Project ID: Cleburn Street well samplingProject Desc:
RLAB Approved Sample Analysis Results
Page 7 of 17
Analysis/ Analyte
Styrene
1,1,2,2-Tetrachloroethane
Tetrachloroethene
Toluene
1,2,3-Trichlorobenzene
1,2,4-Trichlorobenzene
1,1,1-Trichloroethane
1,1,2-Trichloroethane
Trichloroethene
Trichlorofluoromethane
1,1,2-Trichlorotrifluoroethane
Vinyl Chloride
m and/or p-Xylene
o-Xylene
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
Units 101-__ 102-__ 104-__ 105-__
5.0 U 10 U 10 U 10 UJ
5.0 U 10 U 10 U 10 UJ
5.0 U 10 U 10 U 10 UJ
5.0 U 10 U 10 U 10 UJ
5.0 U 10 U 10 U 10 UJ
5.0 U 10 U 10 U 10 UJ
5.0 U 10 U 10 U 10 U
5.0 UJ 10 U 10 U 10 UJ
5.0 U 10 U 10 U 10 UJ
5.0 U 10 U 10 U 10 U
5.0 U 10 U 10 U 10 U
5.0 U 10 U 10 U 10 U
10 U 20 U 20 U 20 UJ
5.0 U 10 U 10 U 10 UJ
4862ASR Number: 05/21/2010
MP7ES02Project ID: Cleburn Street well samplingProject Desc:
RLAB Approved Sample Analysis Results
Page 8 of 17
1 VOCs in Water by GC/MS
Analysis/ Analyte
Acetone
Benzene
Bromodichloromethane
Bromoform
Bromomethane
2-Butanone
Carbon Disulfide
Carbon Tetrachloride
Chlorobenzene
Chloroethane
Chloroform
Chloromethane
Cyclohexane
1,2-Dibromo-3-Chloropropane
Dibromochloromethane
1,2-Dibromoethane
1,2-Dichlorobenzene
1,3-Dichlorobenzene
1,4-Dichlorobenzene
Dichlorodifluoromethane
1,1-Dichloroethane
1,2-Dichloroethane
1,1-Dichloroethene
cis-1,2-Dichloroethene
trans-1,2-Dichloroethene
1,2-Dichloropropane
cis-1,3-Dichloropropene
trans-1,3-Dichloropropene
Ethyl Benzene
2-Hexanone
Isopropylbenzene
Methyl Acetate
Methyl tert-butyl ether
Methylcyclohexane
Methylene Chloride
4-Methyl-2-Pentanone
Naphthalene
Styrene
1,1,2,2-Tetrachloroethane
Tetrachloroethene
Toluene
1,2,3-Trichlorobenzene
1,2,4-Trichlorobenzene
1,1,1-Trichloroethane
1,1,2-Trichloroethane
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
Units 105-FD 106-__ 107-__ 108-__
120 J 58 J 200 J 280 J
10 UJ 10 UJ 10 UJ 10 UJ
10 UJ 10 UJ 10 UJ 10 UJ
10 UJ 10 UJ 10 UJ 10 UJ
10 U 10 U 10 U 10 UJ
10 UJ 10 UJ 12 J 10 UJ
10 U 10 U 10 U 10 UJ
10 U 200 570 200 J
10 UJ 10 UJ 10 UJ 10 UJ
10 U 10 U 10 U 10 UJ
10 U 10 U 190 160 J
10 U 10 U 10 U 10 UJ
10 U 10 U 10 U 10 UJ
10 UJ 10 UJ 10 UJ 10 UJ
10 UJ 10 UJ 10 UJ 10 UJ
10 UJ 10 UJ 10 UJ 10 UJ
10 UJ 10 UJ 10 UJ 10 UJ
10 UJ 10 UJ 10 UJ 10 UJ
10 UJ 10 UJ 10 UJ 10 UJ
10 U 10 U 10 U 10 UJ
10 U 10 U 10 U 10 UJ
10 UJ 10 UJ 10 UJ 10 UJ
10 U 10 U 10 U 10 UJ
10 U 10 U 10 U 10 UJ
10 U 10 U 10 U 10 UJ
10 UJ 10 UJ 10 UJ 10 UJ
10 UJ 10 UJ 10 UJ 10 UJ
10 UJ 10 UJ 10 UJ 10 UJ
10 UJ 10 UJ 10 UJ 10 UJ
10 UJ 10 UJ 10 UJ 10 UJ
10 UJ 10 UJ 10 UJ 10 UJ
10 U 10 U 10 U 10 UJ
20 U 20 U 20 U 20 UJ
10 UJ 10 UJ 10 UJ 10 UJ
10 U 10 U 10 U 10 UJ
10 UJ 10 UJ 10 UJ 10 UJ
20 UJ 20 UJ 20 UJ 20 UJ
10 UJ 10 UJ 10 UJ 10 UJ
10 UJ 10 UJ 10 UJ 10 UJ
10 UJ 10 UJ 30 J 10 UJ
10 UJ 10 UJ 10 UJ 10 UJ
10 UJ 10 UJ 10 UJ 10 UJ
10 UJ 10 UJ 10 UJ 10 UJ
10 U 10 U 39 19 J
10 UJ 10 UJ 10 UJ 10 UJ
4862ASR Number: 05/21/2010
MP7ES02Project ID: Cleburn Street well samplingProject Desc:
RLAB Approved Sample Analysis Results
Page 9 of 17
Analysis/ Analyte
Trichloroethene
Trichlorofluoromethane
1,1,2-Trichlorotrifluoroethane
Vinyl Chloride
m and/or p-Xylene
o-Xylene
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
Units 105-FD 106-__ 107-__ 108-__
10 UJ 10 UJ 10 UJ 10 UJ
10 U 10 U 10 U 10 UJ
10 U 10 U 10 U 10 UJ
10 U 10 U 10 U 10 UJ
20 UJ 20 UJ 20 UJ 20 UJ
10 UJ 10 UJ 10 UJ 10 UJ
4862ASR Number: 05/21/2010
MP7ES02Project ID: Cleburn Street well samplingProject Desc:
RLAB Approved Sample Analysis Results
Page 10 of 17
1 VOCs in Water by GC/MS
Analysis/ Analyte
Acetone
Benzene
Bromodichloromethane
Bromoform
Bromomethane
2-Butanone
Carbon Disulfide
Carbon Tetrachloride
Chlorobenzene
Chloroethane
Chloroform
Chloromethane
Cyclohexane
1,2-Dibromo-3-Chloropropane
Dibromochloromethane
1,2-Dibromoethane
1,2-Dichlorobenzene
1,3-Dichlorobenzene
1,4-Dichlorobenzene
Dichlorodifluoromethane
1,1-Dichloroethane
1,2-Dichloroethane
1,1-Dichloroethene
cis-1,2-Dichloroethene
trans-1,2-Dichloroethene
1,2-Dichloropropane
cis-1,3-Dichloropropene
trans-1,3-Dichloropropene
Ethyl Benzene
2-Hexanone
Isopropylbenzene
Methyl Acetate
Methyl tert-butyl ether
Methylcyclohexane
Methylene Chloride
4-Methyl-2-Pentanone
Naphthalene
Styrene
1,1,2,2-Tetrachloroethane
Tetrachloroethene
Toluene
1,2,3-Trichlorobenzene
1,2,4-Trichlorobenzene
1,1,1-Trichloroethane
1,1,2-Trichloroethane
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
Units 109-__ 110-__ 111-__ 112-__
240 J 190 J 300 J 110 J
10 UJ 10 UJ 10 UJ 10 UJ
12 J 10 UJ 10 UJ 10 UJ
10 UJ 10 UJ 10 UJ 10 UJ
10 UJ 10 UJ 10 UJ 10 UJ
10 UJ 10 UJ 10 UJ 10 UJ
10 UJ 10 UJ 10 UJ 10 UJ
910 J 540 J 210 J 10 UJ
10 UJ 10 UJ 10 UJ 10 UJ
10 UJ 10 UJ 10 UJ 10 UJ
510 J 150 J 64 J 10 UJ
14 J 10 UJ 10 UJ 10 UJ
10 UJ 10 UJ 10 UJ 10 UJ
10 UJ 10 UJ 10 UJ 10 UJ
10 UJ 10 UJ 10 UJ 10 UJ
10 UJ 10 UJ 10 UJ 10 UJ
10 UJ 10 UJ 10 UJ 10 UJ
10 UJ 10 UJ 10 UJ 10 UJ
10 UJ 10 UJ 10 UJ 10 UJ
10 UJ 10 UJ 10 UJ 10 UJ
10 UJ 10 UJ 10 UJ 10 UJ
10 UJ 10 UJ 10 UJ 10 UJ
10 UJ 10 UJ 10 UJ 10 UJ
10 UJ 10 UJ 10 UJ 10 UJ
10 UJ 10 UJ 10 UJ 10 UJ
10 UJ 10 UJ 10 UJ 10 UJ
10 UJ 10 UJ 10 UJ 10 UJ
10 UJ 10 UJ 10 UJ 10 UJ
10 UJ 10 UJ 10 UJ 10 UJ
10 UJ 10 UJ 10 UJ 10 UJ
10 UJ 10 UJ 10 UJ 10 UJ
10 UJ 10 UJ 10 UJ 10 UJ
20 UJ 20 UJ 20 UJ 20 UJ
10 UJ 10 UJ 10 UJ 10 UJ
10 UJ 10 UJ 10 UJ 10 UJ
10 UJ 10 UJ 10 UJ 10 UJ
20 UJ 20 UJ 20 UJ 20 UJ
10 UJ 10 UJ 10 UJ 10 UJ
10 UJ 10 UJ 10 UJ 10 UJ
11 J 10 UJ 10 UJ 10 UJ
10 UJ 10 UJ 10 UJ 10 UJ
10 UJ 10 UJ 10 UJ 10 UJ
10 UJ 10 UJ 10 UJ 10 UJ
54 J 20 J 10 UJ 10 UJ
10 UJ 10 UJ 10 UJ 10 UJ
4862ASR Number: 05/21/2010
MP7ES02Project ID: Cleburn Street well samplingProject Desc:
RLAB Approved Sample Analysis Results
Page 11 of 17
Analysis/ Analyte
Trichloroethene
Trichlorofluoromethane
1,1,2-Trichlorotrifluoroethane
Vinyl Chloride
m and/or p-Xylene
o-Xylene
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
Units 109-__ 110-__ 111-__ 112-__
10 UJ 10 UJ 10 UJ 10 UJ
10 UJ 10 UJ 10 UJ 10 UJ
10 UJ 10 UJ 10 UJ 10 UJ
10 UJ 10 UJ 10 UJ 10 UJ
20 UJ 20 UJ 20 UJ 20 UJ
10 UJ 10 UJ 10 UJ 10 UJ
4862ASR Number: 05/21/2010
MP7ES02Project ID: Cleburn Street well samplingProject Desc:
RLAB Approved Sample Analysis Results
Page 12 of 17
1 VOCs in Water by GC/MS
Analysis/ Analyte
Acetone
Benzene
Bromodichloromethane
Bromoform
Bromomethane
2-Butanone
Carbon Disulfide
Carbon Tetrachloride
Chlorobenzene
Chloroethane
Chloroform
Chloromethane
Cyclohexane
1,2-Dibromo-3-Chloropropane
Dibromochloromethane
1,2-Dibromoethane
1,2-Dichlorobenzene
1,3-Dichlorobenzene
1,4-Dichlorobenzene
Dichlorodifluoromethane
1,1-Dichloroethane
1,2-Dichloroethane
1,1-Dichloroethene
cis-1,2-Dichloroethene
trans-1,2-Dichloroethene
1,2-Dichloropropane
cis-1,3-Dichloropropene
trans-1,3-Dichloropropene
Ethyl Benzene
2-Hexanone
Isopropylbenzene
Methyl Acetate
Methyl tert-butyl ether
Methylcyclohexane
Methylene Chloride
4-Methyl-2-Pentanone
Naphthalene
Styrene
1,1,2,2-Tetrachloroethane
Tetrachloroethene
Toluene
1,2,3-Trichlorobenzene
1,2,4-Trichlorobenzene
1,1,1-Trichloroethane
1,1,2-Trichloroethane
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
Units 112-FD 114-__ 115-__ 119-__
120 J 160 J 73 J 14 J
10 UJ 10 UJ 5.0 UJ 5.0 UJ
10 UJ 10 UJ 5.0 UJ 5.0 UJ
10 UJ 10 UJ 5.0 UJ 5.0 UJ
10 UJ 10 UJ 5.0 U 5.0 U
10 UJ 10 UJ 5.0 UJ 5.0 UJ
10 UJ 10 UJ 5.0 U 5.0 U
10 UJ 60 J 75 5.0 U
10 UJ 10 UJ 5.0 U 5.0 U
10 UJ 10 UJ 5.0 U 5.0 U
10 UJ 10 UJ 39 5.0 U
10 UJ 10 UJ 5.0 U 5.0 U
10 UJ 10 UJ 5.0 U 5.0 U
10 UJ 10 UJ 5.0 UJ 5.0 UJ
10 UJ 10 UJ 5.0 UJ 5.0 UJ
10 UJ 10 UJ 5.0 UJ 5.0 UJ
10 UJ 10 UJ 5.0 U 5.0 U
10 UJ 10 UJ 5.0 U 5.0 U
10 UJ 10 UJ 5.0 U 5.0 U
10 UJ 10 UJ 5.0 U 5.0 U
10 UJ 10 UJ 5.0 U 5.0 U
10 UJ 10 UJ 5.0 UJ 5.0 UJ
10 UJ 10 UJ 5.0 U 5.0 U
10 UJ 10 UJ 5.0 U 5.0 U
10 UJ 10 UJ 5.0 U 5.0 U
10 UJ 10 UJ 5.0 UJ 5.0 UJ
10 UJ 10 UJ 5.0 UJ 5.0 UJ
10 UJ 10 UJ 5.0 U 5.0 U
10 UJ 10 UJ 5.0 U 5.0 U
10 UJ 10 UJ 5.0 UJ 5.0 UJ
10 UJ 10 UJ 5.0 U 5.0 U
10 UJ 10 UJ 5.0 UJ 5.0 UJ
20 UJ 20 UJ 10 U 10 U
10 UJ 10 UJ 5.0 UJ 5.0 UJ
10 UJ 10 UJ 5.0 U 5.0 U
10 UJ 10 UJ 5.0 UJ 5.0 UJ
20 UJ 20 UJ 10 UJ 10 UJ
10 UJ 10 UJ 5.0 U 5.0 U
10 UJ 10 UJ 5.0 UJ 5.0 UJ
10 UJ 10 UJ 150 5.0 U
10 UJ 10 UJ 5.0 UJ 5.0 UJ
10 UJ 10 UJ 5.0 U 5.0 U
10 UJ 10 UJ 5.0 U 5.0 U
10 UJ 10 UJ 55 5.0 U
10 UJ 10 UJ 5.0 UJ 5.0 UJ
4862ASR Number: 05/21/2010
MP7ES02Project ID: Cleburn Street well samplingProject Desc:
RLAB Approved Sample Analysis Results
Page 13 of 17
Analysis/ Analyte
Trichloroethene
Trichlorofluoromethane
1,1,2-Trichlorotrifluoroethane
Vinyl Chloride
m and/or p-Xylene
o-Xylene
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
Units 112-FD 114-__ 115-__ 119-__
10 UJ 10 UJ 5.0 UJ 5.0 UJ
10 UJ 10 UJ 5.0 U 5.0 U
10 UJ 10 UJ 5.0 U 5.0 U
10 UJ 10 UJ 5.0 U 5.0 U
20 UJ 20 UJ 10 U 10 U
10 UJ 10 UJ 5.0 U 5.0 U
4862ASR Number: 05/21/2010
MP7ES02Project ID: Cleburn Street well samplingProject Desc:
RLAB Approved Sample Analysis Results
Page 14 of 17
1 VOCs in Water by GC/MS
Analysis/ Analyte
Acetone
Benzene
Bromodichloromethane
Bromoform
Bromomethane
2-Butanone
Carbon Disulfide
Carbon Tetrachloride
Chlorobenzene
Chloroethane
Chloroform
Chloromethane
Cyclohexane
1,2-Dibromo-3-Chloropropane
Dibromochloromethane
1,2-Dibromoethane
1,2-Dichlorobenzene
1,3-Dichlorobenzene
1,4-Dichlorobenzene
Dichlorodifluoromethane
1,1-Dichloroethane
1,2-Dichloroethane
1,1-Dichloroethene
cis-1,2-Dichloroethene
trans-1,2-Dichloroethene
1,2-Dichloropropane
cis-1,3-Dichloropropene
trans-1,3-Dichloropropene
Ethyl Benzene
2-Hexanone
Isopropylbenzene
Methyl Acetate
Methyl tert-butyl ether
Methylcyclohexane
Methylene Chloride
4-Methyl-2-Pentanone
Naphthalene
Styrene
1,1,2,2-Tetrachloroethane
Tetrachloroethene
Toluene
1,2,3-Trichlorobenzene
1,2,4-Trichlorobenzene
1,1,1-Trichloroethane
1,1,2-Trichloroethane
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
Units 120-__ 121-__ 122-__ 126-FB
34 J 24 J 9.5 J 5.0 U
5.0 UJ 5.0 UJ 5.0 UJ 5.0 U
5.0 UJ 5.0 UJ 5.0 UJ 5.0 U
5.0 UJ 5.0 UJ 5.0 UJ 5.0 U
5.0 U 5.0 U 5.0 U 5.0 U
5.0 UJ 5.0 UJ 5.0 UJ 5.0 U
5.0 U 5.0 U 5.0 U 5.0 U
98 44 5.0 U 5.0 U
5.0 U 5.0 U 5.0 U 5.0 U
5.0 U 5.0 U 5.0 U 5.0 U
45 55 5.0 U 5.0 U
5.0 U 5.0 U 5.0 U 5.0 U
5.0 U 5.0 U 5.0 U 5.0 U
5.0 UJ 5.0 UJ 5.0 UJ 5.0 U
5.0 UJ 5.0 UJ 5.0 UJ 5.0 U
5.0 UJ 5.0 UJ 5.0 UJ 5.0 U
5.0 U 5.0 U 5.0 U 5.0 U
5.0 U 5.0 U 5.0 U 5.0 U
5.0 U 5.0 U 5.0 U 5.0 U
5.0 U 5.0 U 5.0 U 5.0 U
5.0 U 5.0 U 5.0 U 5.0 U
5.0 UJ 5.0 UJ 5.0 UJ 5.0 U
5.0 U 5.0 U 5.0 U 5.0 U
5.0 U 5.0 U 5.0 U 5.0 U
5.0 U 5.0 U 5.0 U 5.0 U
5.0 UJ 5.0 UJ 5.0 UJ 5.0 U
5.0 UJ 5.0 UJ 5.0 UJ 5.0 U
5.0 U 5.0 U 5.0 U 5.0 U
5.0 U 5.0 U 5.0 U 5.0 U
5.0 UJ 5.0 UJ 5.0 UJ 5.0 U
5.0 U 5.0 U 5.0 U 5.0 U
5.0 UJ 5.0 UJ 5.0 UJ 5.0 U
10 U 10 U 10 U 10 U
5.0 UJ 5.0 UJ 5.0 UJ 5.0 U
5.0 U 5.0 U 5.0 U 5.0 UJ
5.0 UJ 5.0 UJ 5.0 UJ 5.0 U
10 UJ 10 UJ 10 UJ 10 U
5.0 U 5.0 U 5.0 U 5.0 U
5.0 UJ 5.0 UJ 5.0 UJ 5.0 U
55 180 5.0 U 5.0 U
5.0 UJ 5.0 UJ 5.0 UJ 5.0 U
5.0 U 5.0 U 5.0 U 5.0 U
5.0 U 5.0 U 5.0 U 5.0 U
16 5.0 U 5.0 U 5.0 U
5.0 UJ 5.0 UJ 5.0 UJ 5.0 U
4862ASR Number: 05/21/2010
MP7ES02Project ID: Cleburn Street well samplingProject Desc:
RLAB Approved Sample Analysis Results
Page 15 of 17
Analysis/ Analyte
Trichloroethene
Trichlorofluoromethane
1,1,2-Trichlorotrifluoroethane
Vinyl Chloride
m and/or p-Xylene
o-Xylene
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
Units 120-__ 121-__ 122-__ 126-FB
5.0 UJ 5.0 UJ 5.0 UJ 5.0 U
5.0 U 5.0 U 5.0 U 5.0 U
5.0 U 5.0 U 5.0 U 5.0 U
5.0 U 5.0 U 5.0 U 5.0 U
10 U 10 U 10 U 10 U
5.0 U 5.0 U 5.0 U 5.0 U
4862ASR Number: 05/21/2010
MP7ES02Project ID: Cleburn Street well samplingProject Desc:
RLAB Approved Sample Analysis Results
Page 16 of 17
1 VOCs in Water by GC/MS
Analysis/ Analyte
Acetone
Benzene
Bromodichloromethane
Bromoform
Bromomethane
2-Butanone
Carbon Disulfide
Carbon Tetrachloride
Chlorobenzene
Chloroethane
Chloroform
Chloromethane
Cyclohexane
1,2-Dibromo-3-Chloropropane
Dibromochloromethane
1,2-Dibromoethane
1,2-Dichlorobenzene
1,3-Dichlorobenzene
1,4-Dichlorobenzene
Dichlorodifluoromethane
1,1-Dichloroethane
1,2-Dichloroethane
1,1-Dichloroethene
cis-1,2-Dichloroethene
trans-1,2-Dichloroethene
1,2-Dichloropropane
cis-1,3-Dichloropropene
trans-1,3-Dichloropropene
Ethyl Benzene
2-Hexanone
Isopropylbenzene
Methyl Acetate
Methyl tert-butyl ether
Methylcyclohexane
Methylene Chloride
4-Methyl-2-Pentanone
Naphthalene
Styrene
1,1,2,2-Tetrachloroethane
Tetrachloroethene
Toluene
1,2,3-Trichlorobenzene
1,2,4-Trichlorobenzene
1,1,1-Trichloroethane
1,1,2-Trichloroethane
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
Units 129-FB
35
5.0 U
5.0 U
5.0 U
5.0 U
5.0 U
5.0 U
5.0 U
5.0 U
5.0 U
5.0 U
5.0 U
5.0 U
5.0 U
5.0 U
5.0 U
5.0 U
5.0 U
5.0 U
5.0 U
5.0 U
5.0 U
5.0 U
5.0 U
5.0 U
5.0 U
5.0 U
5.0 U
5.0 U
5.0 U
5.0 U
5.0 U
10 U
5.0 U
5.0 UJ
5.0 U
10 U
5.0 U
5.0 U
5.0 U
5.0 U
5.0 U
5.0 U
5.0 U
5.0 U
4862ASR Number: 05/21/2010
MP7ES02Project ID: Cleburn Street well samplingProject Desc:
RLAB Approved Sample Analysis Results
Page 17 of 17
Analysis/ Analyte
Trichloroethene
Trichlorofluoromethane
1,1,2-Trichlorotrifluoroethane
Vinyl Chloride
m and/or p-Xylene
o-Xylene
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
Units 129-FB
5.0 U
5.0 U
5.0 U
5.0 U
10 U
5.0 U
4862ASR Number: 05/21/2010
MP7ES02Project ID: Cleburn Street well samplingProject Desc:
RLAB Approved Sample Analysis Results
4862
MP7ES02Project ID:
Cleburn Street well sampling
Mary PetersonSUPR/IANE
United States Environmental Protection AgencyRegion VII
901 N. 5th StreetKansas City, KS 66101
__/__/____
Data Disposition/Sample Release for ASR #:
Project Description:
Subject:
Kaye DollmannENSV/RLAB
I have received and reviewed the Transmittal of Sample Analysis Results for the above-referencedAnalytical Services Request(ASR) and have indicated my findings below by checking one of theboxes for Data Disposition.
I understand all samples will be disposed upon receipt of this form, unless samples are requestedto be held. If I do not return this form all samples will be disposed of on ___________________.
"RELEASED" - Read-only to all Region 7 employees and contractors that have R7LIMS"Customer" account. All Samples may be disposed of upon receipt of this form if not requested tobe held.
"Project Manager Accessible" - Available on the LAN in R7LIMS for my use only. All Samples maybe disposed of upon receipt of this form if not requested to be held.
"Archived" - THIS DATA IS OF A SENSITIVE NATURE. Any future reports must be requestedthrough the laboratory. All samples may be disposed of upon receipt of the form if not requestedto be held.
Date:
From:
To:
Hold Samples - I have determined that the samples need to be held until ______________, afterwhich time they will be disposed of in accordance with applicable regulations. The reason for the hold is:
Samples are associated with a legal proceeding.
Question/Concern with data - possible reanalysis requested.
Other:________________________________________________________________
MAY 2010
Page 1 of 43
06/07/2010Date:
4889
MP7ES02
Cleburn Street well sampling
Mary PetersonSUPR/IANE
Transmittal of Sample Analysis Results for ASR #:
Project ID:
Project Description:
Michael F. Davis, ChiefChemical Analysis and Response Branch, Environmental Services Division
To:
Enclosed are the analytical data for the above-referenced Analytical Services Request (ASR) andProject. The Regional Laboratory has reviewed and verified the results in accordance with proceduresdescribed in our Quality Manual (QM). In addition to all of the analytical results, this transmittalcontains pertinent information that may have influenced the reported results and documents anydeviations from the established requirements of the QM.
Please contact us within 14 days of receipt of this package if you determine there is a need for anychanges. Please complete the enclosed Customer Satisfaction Survey and Data Disposition/SampleRelease memo for this ASR as soon as possible. The process of disposing of the samples for this ASRwill be initiated 30 days from the date of this transmittal unless an alternate release date is specifiedon the Data Disposition/Sample Release memo.
If you have any questions or concerns relating to this data package, contact our customer service lineat 913-551-5295.
Enclosures
cc: Analytical Data File.
United States Environmental Protection AgencyRegion 7
901 N. 5th StreetKansas City, KS 66101
Subject:
From:
Page 2 of 43
4889ASR Number: 06/07/2010
Mary Peterson SUPR/IANE 913-551-7882
MP7ES02
Cleburn Street well sampling
Grand Island Nebraska Superfund
CLEBURN STREET WELL - 1 HR MARTINIZING GWRESORATION
07ESSite ID: 02
Site Cleanup Support
May 3rd Quarterly and Post Injection monitoring sampling.
Project Manager: Org: Phone:
Project ID:
Project Desc:
Location: State: Program:
Site Name: Site OU:
Purpose:
__ = Field SampleFB = Field BlankFD = Field Duplicate
QC Codes identify the type of sample for quality control purpose.
Degrees CelsiusNephelometric Turbidity UnitsStandard Units (pH)Milligrams per LiterMicrograms per LiterMicromhos per Centimeter
Specific units in which results arereported.
The identification of the analyte is acceptable; the reported value is anestimate.The analyte was not detected at or above the reporting limit.The analyte was not detected at or above the reporting limit. The reportinglimit is an estimate.
Specific codes used in conjunction with data values to provide additional information on the quality of reported results, or used to explain the absence of a specific value.
Summary of Project Information
Explanation of Codes, Units and Qualifiers used on this report
Sample QC Codes: Units:
J
UUJ
=
==
Data Qualifiers:
= Values have been reviewed and found acceptable for use. (Blank)
Deg CNTUSU
mg/Lug/L
umhos/cm
======
2009073QAPP Number:
302DD2CGPRA PRC:
Page 3 of 43
1
2
3
4
4
5
6
7
8
9
10
10
11
12
13
14
15
16
17
18
19
20
20
24
25
26
27
28
29
29
30
31
32
33
33
34
35
36
37
38
39
40
40
SampleNo
__
__
__
__
FD
__
__
__
__
__
__
FD
__
__
__
__
__
__
__
__
__
__
FD
FB
__
__
__
__
__
FD
__
__
__
__
FD
__
__
__
__
__
__
__
FD
QCCode
Water
Water
Water
Water
Water
Water
Water
Water
Water
Water
Water
Water
Water
Water
Water
Water
Water
Water
Water
Water
Water
Water
Water
Water
Water
Water
Water
Water
Water
Water
Water
Water
Water
Water
Water
Water
Water
Water
Water
Water
Water
Water
Water
Matrix
ERT-15
IW-1
IW-2
IW-3
IW-3/Field Duplicate of sample 4
IW-4
IW-5
IW-6
IW-7
ERT-16
IW-8
IW-8/Field Duplicate of sample 10
IW-9
IW-10
MW-2A
DPT-3
DPE-1
DPE-2
MW-2B
DPE-4
MW-12A
ERT-14
ERT-14/Field Duplicate of sample20Preservative Blank sample
MW-13A
MW-105-BB
MW-8A
Cleburn Street Well
MW-8B
MW-8B/Field Duplicate of sample29MW-102-AA
MW-102-BB
MW-9A
MW-106-CC
MW-106-CC/Field Duplicate ofsample 33MW-106-BB
MW-104AA
MW-104-BB
MW-10B
MW-10A
MW-103-CC
MW-103-BB
MW-103-BB/Field Duplicate of
Location DescriptionExternal
Sample No
05/03/2010
05/04/2010
05/04/2010
05/04/2010
05/04/2010
05/04/2010
05/04/2010
05/04/2010
05/04/2010
05/05/2010
05/05/2010
05/05/2010
05/05/2010
05/05/2010
05/05/2010
05/05/2010
05/05/2010
05/06/2010
05/06/2010
05/06/2010
05/06/2010
05/06/2010
05/06/2010
05/04/2010
05/06/2010
05/07/2010
05/07/2010
05/07/2010
05/07/2010
05/07/2010
05/07/2010
05/07/2010
05/07/2010
05/07/2010
05/07/2010
05/08/2010
05/08/2010
05/08/2010
05/08/2010
05/08/2010
05/08/2010
05/08/2010
05/08/2010
Start Date
17:20
08:55
10:00
10:55
10:55
12:20
13:50
15:50
17:05
10:00
11:05
11:05
12:40
13:50
15:15
16:35
18:20
10:10
11:20
12:30
13:55
15:15
15:15
15:15
17:40
12:20
13:10
12:50
14:35
14:35
15:35
16:20
17:30
18:05
18:05
09:40
10:30
11:05
11:50
13:00
13:55
14:40
14:40
Start Time
End Date
End Time
05/05/2010
05/05/2010
05/05/2010
05/05/2010
05/05/2010
05/05/2010
05/05/2010
05/05/2010
05/06/2010
05/06/2010
05/06/2010
05/06/2010
05/06/2010
05/06/2010
05/06/2010
05/07/2010
05/07/2010
05/07/2010
05/07/2010
05/07/2010
05/07/2010
05/07/2010
05/07/2010
05/05/2010
05/10/2010
05/10/2010
05/10/2010
05/10/2010
05/10/2010
05/10/2010
05/10/2010
05/10/2010
05/10/2010
05/10/2010
05/10/2010
05/10/2010
05/10/2010
05/10/2010
05/10/2010
05/10/2010
05/10/2010
05/10/2010
05/10/2010
ReceiptDate
4889 06/07/2010
MP7ES02Project ID: Cleburn Street well samplingProject Desc:
ASR Number: Sample Information Summary
-
-
-
-
-
-
-
-
-
-
-
-
-
-
-
-
-
-
-
-
-
-
-
-
-
-
-
-
-
-
-
-
-
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-
-
-
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Page 4 of 43
41
42
43
44
45
46
47
52
53
54
SampleNo
__
__
__
__
__
__
__
FB
FB
FB
QCCode
Water
Water
Water
Water
Water
Water
Water
Water
Water
Water
Matrix
sample 40
MW-103-AA
MW-11B
MW-108-BB
MW-11A
MW-107-AA
MW-107-BB
MW-101-AA
Routine VOA Trip Blank sample 1
Routine VOA Trip Blank sample 2
Routine VOA Trip Blank sample 3
Location DescriptionExternal
Sample No
05/08/2010
05/08/2010
05/08/2010
05/08/2010
05/08/2010
05/08/2010
05/08/2010
04/29/2010
04/29/2010
04/29/2010
Start Date
15:15
16:05
16:45
17:20
18:00
18:35
19:15
06:51
06:52
06:50
Start Time
05/03/2010
05/06/2010
05/05/2010
End Date
17:20
08:45
08:45
End Time
05/10/2010
05/10/2010
05/10/2010
05/10/2010
05/10/2010
05/10/2010
05/10/2010
05/05/2010
05/07/2010
05/06/2010
ReceiptDate
4889 06/07/2010
MP7ES02Project ID: Cleburn Street well samplingProject Desc:
ASR Number: Sample Information Summary
-
-
-
-
-
-
-
-
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-
Page 5 of 43
1
1
1
1
Alkalinity in Water by Titration
Anions in Water by Ion Chromatography
Conductivity by Field Measurement
Hardness in Water by Calculation
Region 7 ESAT Contract Lab (In-House)
Region 7 ESAT Contract Lab (In-House)
(Field Measurement)
Lab:
Lab:
Lab:
EPA Region 7 RLAB Method 3132.1E
Region 7 RLAB Method 3135.12A
Measurement of field parameter
Method:
Method:
Method:
(N/A)
Dilutions were necessary in order to obtain valid results due to matrix interferences forsamples 2, 3, 4, 4 FD, 5, 6, 7, 8, 9, 10, 10 FD, 11, 12, 13, 14, 15, 16 and 18. Thisincreased the reporting limits by a factor of 10000 for these samples.
Sulfate (78, 80-120) was J-coded in sample 17. Although the analyte in question hasbeen positively identified in the sample, the quantitation is an estimate (J-coded) due tolow recovery of this analyte in the laboratory matrix spike. The actual concentration forthis analyte may be higher than the reported value.
(N/A)
Comments:
Comments:
Comments:
1-__ 2-__ 3-__ 4-__ 4-FD 5-__ 6-__7-__ 8-__ 9-__ 10-__ 10-FD 11-__ 12-__13-__ 14-__ 15-__ 16-__ 17-__ 18-__ 19-__20-__ 20-FD
1-__ 2-__ 3-__ 4-__ 4-FD 5-__ 6-__7-__ 8-__ 9-__ 10-__ 10-FD 11-__ 12-__13-__ 14-__ 15-__ 16-__ 17-__ 18-__ 19-__20-__ 20-FD
1-__ 2-__ 3-__ 4-__ 4-FD 5-__ 6-__7-__ 8-__ 9-__ 10-__ 10-FD 11-__ 12-__13-__ 14-__ 15-__ 16-__ 17-__ 18-__ 19-__20-__ 20-FD 25-__ 26-__ 27-__ 28-__ 29-__29-FD 30-__ 31-__ 32-__ 33-__ 33-FD 34-__35-__ 36-__ 37-__ 38-__ 39-__ 40-__ 40-FD41-__ 42-__ 43-__ 44-__ 45-__ 46-__ 47-__
Samples:
Samples:
Samples:
4889ASR Number: 06/07/2010
MP7ES02Project ID: Cleburn Street well samplingProject Desc
RLAB Approved Analysis Comments
Analysis Comments About Results For This Analysis
Page 6 of 43
1
1
1
Metals in Water by ICP-AES
pH of Water by Field Measurement
TDS or Total Dissolved Solids
Region 7 ESAT Contract Lab (In-House)
Region 7 ESAT Contract Lab (In-House)
(Field Measurement)
Region 7 EPA Laboratory - Kansas City, Ks.
Lab:
Lab:
Lab:
Lab:
EPA Region 7 RLAB Method 3122.3C
EPA Region 7 RLAB Method 3122.3C
Measurement of field parameter
EPA Region 7 RLAB Method 3142.2B
Method:
Method:
Method:
Method:
Dilutions were necessary in order to obtain valid results due to matrix interferences forsamples 2-6, 10, 10FD, 16, and 18. This increased the reporting limits by a factor of 100for these samples.
Dilutions were necessary in order to obtain valid results due to matrix interferences forsamples 2-16 and 18. This increased the reporting limits by a factor of 100 for thesesamples.
(N/A)
Comments:
Comments:
Comments:
1-__ 2-__ 3-__ 4-__ 4-FD 5-__ 6-__7-__ 8-__ 9-__ 10-__ 10-FD 11-__ 12-__13-__ 14-__ 15-__ 16-__ 17-__ 18-__ 19-__20-__ 20-FD
1-__ 2-__ 3-__ 4-__ 4-FD 5-__ 6-__7-__ 8-__ 9-__ 10-__ 10-FD 11-__ 12-__13-__ 14-__ 15-__ 16-__ 17-__ 18-__ 19-__20-__ 20-FD 24-FB
1-__ 2-__ 3-__ 4-__ 4-FD 5-__ 6-__7-__ 8-__ 9-__ 10-__ 10-FD 11-__ 12-__13-__ 14-__ 15-__ 16-__ 17-__ 18-__ 19-__20-__ 20-FD 25-__ 26-__ 27-__ 28-__ 29-__29-FD 30-__ 31-__ 32-__ 33-__ 33-FD 34-__35-__ 36-__ 37-__ 38-__ 39-__ 40-__ 40-FD41-__ 42-__ 43-__ 44-__ 45-__ 46-__ 47-__
1-__ 2-__ 3-__ 4-__ 4-FD 5-__ 6-__7-__ 8-__ 9-__ 10-__ 10-FD 11-__ 12-__
Samples:
Samples:
Samples:
Samples:
4889ASR Number: 06/07/2010
MP7ES02Project ID: Cleburn Street well samplingProject Desc
RLAB Approved Analysis Comments
Analysis Comments About Results For This Analysis
Page 7 of 43
1
1
1
Temperature of Water by Field Measurement
Turbidity of Water by Field Measurement
VOCs in Water by GC/MS
(Field Measurement)
(Field Measurement)
Region 7 ESAT Contract Lab (In-House)
Lab:
Lab:
Lab:
Measurement of field parameter
Measurement of field parameter
EPA Region 7 RLAB Method 3230.1F
Method:
Method:
Method:
(N/A)
(N/A)
Comments:
Comments:
Comments:
13-__ 14-__ 15-__ 16-__ 17-__ 18-__ 19-__20-__ 20-FD
1-__ 2-__ 3-__ 4-__ 4-FD 5-__ 6-__7-__ 8-__ 9-__ 10-__ 10-FD 11-__ 12-__13-__ 14-__ 15-__ 16-__ 17-__ 18-__ 19-__20-__ 20-FD 25-__ 26-__ 27-__ 28-__ 29-__29-FD 30-__ 31-__ 32-__ 33-__ 33-FD 34-__35-__ 36-__ 37-__ 38-__ 39-__ 40-__ 40-FD41-__ 42-__ 43-__ 44-__ 45-__ 46-__ 47-__
1-__ 2-__ 3-__ 4-__ 4-FD 5-__ 6-__7-__ 8-__ 9-__ 10-__ 10-FD 11-__ 12-__13-__ 14-__ 15-__ 16-__ 17-__ 18-__ 19-__20-__ 20-FD 25-__ 26-__ 27-__ 28-__ 29-__29-FD 30-__ 31-__ 32-__ 33-__ 33-FD 34-__35-__ 36-__ 37-__ 38-__ 39-__ 40-__ 40-FD41-__ 42-__ 43-__ 44-__ 45-__ 46-__ 47-__
1-__ 2-__ 3-__ 4-__ 4-FD 5-__ 6-__7-__ 8-__ 9-__ 10-__ 10-FD 11-__ 12-__13-__ 14-__ 15-__ 16-__ 17-__ 18-__ 19-__20-__ 20-FD 24-FB 25-__ 26-__ 27-__ 28-__29-__ 29-FD 30-__ 31-__ 32-__ 33-__ 33-FD34-__ 35-__ 36-__ 37-__ 38-__ 39-__ 40-__40-FD 41-__ 42-__ 43-__ 44-__ 45-__ 46-__
Samples:
Samples:
Samples:
Samples:
4889ASR Number: 06/07/2010
MP7ES02Project ID: Cleburn Street well samplingProject Desc
RLAB Approved Analysis Comments
Analysis Comments About Results For This Analysis
Page 8 of 43
Twenty of the samples contained potassium permanganate. These samples were diluted tokeep the column from being damaged. The resulting reporting limit for these samples washigher than the normal reporting limit. Dichlorodifluoromethane (+23.5%) was UJ-coded in samples 52-FB, 53-FB, 54-FB, 24-FB,39, 34, 35, 36, 37, 38, 40, 40-FD, 42, 43, 44, 45, 46, 47, 26, 27, 28, 29, and 29-FD. Thisanalyte was not found in the samples at or above the reporting limit, however, thereporting limit is an estimate (UJ-coded) due to the continuing calibration check notmeeting accuracy specifications. The actual reporting limit for this analyte may be higherthan the reported value. Methyl tert-butyl ether (+26.1%) was UJ-coded in samples 17, 41, 31, 32, 33, 33-FD, 19,20-FD, 25, 2, 3, 4, 4-FD, 5, 6, 7, 8, 9, 10, 10-FD, 11, 12, 13, and 14. This analyte was notfound in the samples at or above the reporting limit, however, the reporting limit is anestimate (UJ-coded) due to the continuing calibration check not meeting accuracyspecifications. The actual reporting limit for this analyte may be higher than the reportedvalue.
Naphthalene (-42.1%)was J-coded in sample 19. Although the analyte in question hasbeen positively identified in the samples, the quantitation is an estimate (J-coded) due tothe continuing calibration check not meeting accuracy specifications. The actualconcentration for this analyte may be lower than the reported value. Methyl tert-butyl ether (+26.5%) was UJ-coded in samples 20, 15, 16, 18, 30 and 1. Thisanalyte was not found in the samples at or above the reporting limit, however, thereporting limit is an estimate (UJ-coded) due to the continuing calibration check notmeeting accuracy specifications. The actual reporting limit for this analyte may be higherthan the reported value. Naphthalene (-38.8%) was J-coded in sample 19. Although the analyte in question hasbeen positively identified in the samples, the quantitation is an estimate (J-coded) due tothe continuing calibration check not meeting accuracy specifications. The actualconcentration for this analyte may be lower than the reported value. Methyl tert-butyl ether (74%, 82%-116%) was UJ-coded in samples 17, 41, 31, 32, 33,33-FD, 19, 20-FD, 25, 2, 3, 4, 4-FD, 5, 6, 7, 8, 9, 10, 10-FD, 11, 12, 13, and 14. Thisanalyte was not found in the samples at or above the reporting limit, however, thereporting limit is an estimate (UJ-coded) due to low recovery of this analyte in thelaboratory control sample. The actual reporting limit for this analyte may be higher thanthe reported value. Naphthalene (142%, 80%-123%) was J-coded in sample 19. Although the analyte inquestion has been positively identified in the samples, the quantitation is an estimate (J-coded) due to high recovery of this analyte in the laboratory control sample. The actualconcentration for this analyte may be lower than the reported value.
Comments:
47-__ 52-FB 53-FB 54-FB Samples:
4889ASR Number: 06/07/2010
MP7ES02Project ID: Cleburn Street well samplingProject Desc
RLAB Approved Analysis Comments
Analysis Comments About Results For This Analysis
Page 9 of 43
Methyl tert-butyl ether (73%, 82%-116%) was UJ-coded in samples 20, 15, 16, 18, 30 and1. This analyte was not found in the samples at or above the reporting limit, however, thereporting limit is an estimate (UJ-coded) due to low recovery of this analyte in thelaboratory control sample. The actual reporting limit for this analyte may be higher thanthe reported value. Methyl tert-butyl ether (71%, 75%-119%) was UJ-coded in sample 34. This analyte wasnot found in the sample at or above the reporting limit, however, the reporting limit is anestimate (UJ-coded) due to low recovery of this analyte in the laboratory matrix spike. Theactual reporting limit for this analyte may be higher than the reported value. Bromodichloromethane (6.4RPD, 6.1PCL) and 1,2-Dichloroethane (6.4RPD, 6.3PCL) wereUJ-coded in sample 17. These analytes were not found in the sample at or above thereporting limit, however, the reporting limit is an estimate (UJ-coded) due to poor precisionobtained for these analytes in the laboratory matrix spike and matrix spike duplicate. Theactual reporting limit for these analytes may be higher than the reported value.
4889ASR Number: 06/07/2010
MP7ES02Project ID: Cleburn Street well samplingProject Desc
RLAB Approved Analysis Comments
Analysis Comments About Results For This Analysis
Page 10 of 43
1
1
1
1
1
1
1
1
1
1
Alkalinity in Water by Titration
Anions in Water by Ion Chromatography
Conductivity by Field Measurement
Hardness in Water by Calculation
Metals in Water by ICP-AES
pH of Water by Field Measurement
TDS or Total Dissolved Solids
Temperature of Water by Field Measurement
Turbidity of Water by Field Measurement
VOCs in Water by GC/MS
Analysis/ Analyte
Alkalinity, total
Sulfate
Conductivity
Hardness as CaCO3
Aluminum
Antimony
Arsenic
Barium
Beryllium
Cadmium
Calcium
Chromium
Cobalt
Copper
Iron
Lead
Magnesium
Manganese
Molybdenum
Nickel
Potassium
Selenium
Silver
Sodium
Thallium
Titanium
Vanadium
Zinc
pH
Solids, total dissolved
Temperature
Turbidity
Acetone
Benzene
Bromodichloromethane
Bromoform
mg/L
mg/L
umhos/cm
mg/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
mg/L
ug/L
ug/L
ug/L
ug/L
ug/L
mg/L
ug/L
ug/L
ug/L
mg/L
ug/L
ug/L
mg/L
ug/L
ug/L
ug/L
ug/L
SU
mg/L
Deg C
NTU
ug/L
ug/L
ug/L
ug/L
Units 1-__ 2-__ 3-__ 4-__
85.5 210 225 256
125 10000 U 10000 U 10000 U
894 6990 6750 8100
279 1320 U 1320 U 1320 U
50 U 5000 U 5000 U 5000 U
50 U 5000 U 5000 U 5000 U
25 U 2500 U 2500 U 2500 U
81 1000 U 1000 U 1000 U
3 U 300 U 300 U 300 U
3 U 300 U 300 U 300 U
79.3 200 U 200 U 200 U
51 1500 U 1500 U 1500 U
10 U 1000 U 1000 U 1000 U
5 U 500 U 500 U 500 U
50 U 5000 U 5000 U 5000 U
50 U 5000 U 5000 U 5000 U
19.7 200 U 200 U 200 U
4410 393000 371000 316000
15 U 1500 U 1500 U 1500 U
20 U 2000 U 2000 U 2000 U
14.2 1660 1500 1820
50 U 5000 U 5000 U 5000 U
25 U 2500 U 2500 U 2500 U
64.9 500 U 500 U 500 U
50 U 5000 U 5000 U 5000 U
20 U 2000 U 2000 U 2000 U
10 U 1000 U 1000 U 1000 U
25 U 2500 U 2500 U 2500 U
6.78 7.52 7.32 7.55
440 8300 8030 10200
15.81 14.52 14.55 14.68
0.0 5.2 2.0 3.6
100 U 25000 U 25000 U 25000 U
100 U 25000 U 25000 U 25000 U
100 U 25000 U 25000 U 25000 U
100 U 25000 U 25000 U 25000 U
4889ASR Number: 06/07/2010
MP7ES02Project ID: Cleburn Street well samplingProject Desc:
RLAB Approved Sample Analysis Results
Page 11 of 43
Analysis/ Analyte
Bromomethane
2-Butanone
Carbon Disulfide
Carbon Tetrachloride
Chlorobenzene
Chloroethane
Chloroform
Chloromethane
Cyclohexane
1,2-Dibromo-3-Chloropropane
Dibromochloromethane
1,2-Dibromoethane
1,2-Dichlorobenzene
1,3-Dichlorobenzene
1,4-Dichlorobenzene
Dichlorodifluoromethane
1,1-Dichloroethane
1,2-Dichloroethane
1,1-Dichloroethene
cis-1,2-Dichloroethene
trans-1,2-Dichloroethene
1,2-Dichloropropane
cis-1,3-Dichloropropene
trans-1,3-Dichloropropene
Ethyl Benzene
2-Hexanone
Isopropylbenzene
Methyl Acetate
Methyl tert-butyl ether
Methylcyclohexane
Methylene Chloride
4-Methyl-2-Pentanone
Naphthalene
Styrene
1,1,2,2-Tetrachloroethane
Tetrachloroethene
Toluene
1,2,3-Trichlorobenzene
1,2,4-Trichlorobenzene
1,1,1-Trichloroethane
1,1,2-Trichloroethane
Trichloroethene
Trichlorofluoromethane
1,1,2-Trichlorotrifluoroethane
Vinyl Chloride
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
Units 1-__ 2-__ 3-__ 4-__
100 U 25000 U 25000 U 25000 U
100 U 25000 U 25000 U 25000 U
100 U 25000 U 25000 U 25000 U
100 U 25000 U 25000 U 25000 U
100 U 25000 U 25000 U 25000 U
100 U 25000 U 25000 U 25000 U
100 U 25000 U 25000 U 25000 U
100 U 25000 U 25000 U 25000 U
100 U 25000 U 25000 U 25000 U
100 U 25000 U 25000 U 25000 U
100 U 25000 U 25000 U 25000 U
100 U 25000 U 25000 U 25000 U
100 U 25000 U 25000 U 25000 U
100 U 25000 U 25000 U 25000 U
100 U 25000 U 25000 U 25000 U
100 U 25000 U 25000 U 25000 U
100 U 25000 U 25000 U 25000 U
100 U 25000 U 25000 U 25000 U
100 U 25000 U 25000 U 25000 U
100 U 25000 U 25000 U 25000 U
100 U 25000 U 25000 U 25000 U
100 U 25000 U 25000 U 25000 U
100 U 25000 U 25000 U 25000 U
100 U 25000 U 25000 U 25000 U
100 U 25000 U 25000 U 25000 U
100 U 25000 U 25000 U 25000 U
100 U 25000 U 25000 U 25000 U
100 U 25000 U 25000 U 25000 U
200 UJ 50000 UJ 50000 UJ 50000 UJ
100 U 25000 U 25000 U 25000 U
100 U 25000 U 25000 U 25000 U
100 U 25000 U 25000 U 25000 U
200 U 50000 U 50000 U 50000 U
100 U 25000 U 25000 U 25000 U
100 U 25000 U 25000 U 25000 U
100 U 25000 U 25000 U 25000 U
100 U 25000 U 25000 U 25000 U
100 U 25000 U 25000 U 25000 U
100 U 25000 U 25000 U 25000 U
100 U 25000 U 25000 U 25000 U
100 U 25000 U 25000 U 25000 U
100 U 25000 U 25000 U 25000 U
100 U 25000 U 25000 U 25000 U
100 U 25000 U 25000 U 25000 U
100 U 25000 U 25000 U 25000 U
4889ASR Number: 06/07/2010
MP7ES02Project ID: Cleburn Street well samplingProject Desc:
RLAB Approved Sample Analysis Results
Page 12 of 43
Analysis/ Analyte
m and/or p-Xylene
o-Xylene
ug/L
ug/L
Units 1-__ 2-__ 3-__ 4-__
200 U 50000 U 50000 U 50000 U
100 U 25000 U 25000 U 25000 U
4889ASR Number: 06/07/2010
MP7ES02Project ID: Cleburn Street well samplingProject Desc:
RLAB Approved Sample Analysis Results
Page 13 of 43
1
1
1
1
1
1
1
1
1
1
Alkalinity in Water by Titration
Anions in Water by Ion Chromatography
Conductivity by Field Measurement
Hardness in Water by Calculation
Metals in Water by ICP-AES
pH of Water by Field Measurement
TDS or Total Dissolved Solids
Temperature of Water by Field Measurement
Turbidity of Water by Field Measurement
VOCs in Water by GC/MS
Analysis/ Analyte
Alkalinity, total
Sulfate
Conductivity
Hardness as CaCO3
Aluminum
Antimony
Arsenic
Barium
Beryllium
Cadmium
Calcium
Chromium
Cobalt
Copper
Iron
Lead
Magnesium
Manganese
Molybdenum
Nickel
Potassium
Selenium
Silver
Sodium
Thallium
Titanium
Vanadium
Zinc
pH
Solids, total dissolved
Temperature
Turbidity
Acetone
Benzene
Bromodichloromethane
Bromoform
mg/L
mg/L
umhos/cm
mg/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
mg/L
ug/L
ug/L
ug/L
ug/L
ug/L
mg/L
ug/L
ug/L
ug/L
mg/L
ug/L
ug/L
mg/L
ug/L
ug/L
ug/L
ug/L
SU
mg/L
Deg C
NTU
ug/L
ug/L
ug/L
ug/L
Units 4-FD 5-__ 6-__ 7-__
259 317 138 203
10000 U 10000 U 10000 U 10000 U
8100 9210 8270 7680
1320 U 1320 U 1320 U 2190
5000 U 5000 U 5000 U 5000 U
5000 U 5000 U 5000 U 5000 U
2500 U 2500 U 2500 U 2500 U
1000 U 1000 U 1000 U 1000 U
300 U 300 U 300 U 300 U
300 U 300 U 300 U 300 U
200 U 200 U 200 U 547
1500 U 1500 U 1500 U 1500 U
1000 U 1000 U 1000 U 1000 U
500 U 500 U 500 U 500 U
5000 U 5000 U 5000 U 5000 U
5000 U 5000 U 5000 U 5000 U
200 U 200 U 200 U 200 U
354000 304000 305000 383000
1500 U 1500 U 1500 U 1500 U
2000 U 2000 U 2000 U 2000 U
1790 2200 1970 1170
5000 U 5000 U 5000 U 5000 U
2500 U 2500 U 2500 U 2500 U
500 U 500 U 500 U 500 U
5000 U 5000 U 5000 U 5000 U
2000 U 2000 U 2000 U 2000 U
1000 U 1000 U 1000 U 1000 U
2500 U 2500 U 2500 U 2500 U
7.55 6.57 6.03 5.67
9470 11900 9660 8210
14.68 4.60 14.23 21.05
3.6 1.6 2.2 3.1
25000 U 25000 U 25000 U 25000 U
25000 U 25000 U 25000 U 25000 U
25000 U 25000 U 25000 U 25000 U
25000 U 25000 U 25000 U 25000 U
4889ASR Number: 06/07/2010
MP7ES02Project ID: Cleburn Street well samplingProject Desc:
RLAB Approved Sample Analysis Results
Page 14 of 43
Analysis/ Analyte
Bromomethane
2-Butanone
Carbon Disulfide
Carbon Tetrachloride
Chlorobenzene
Chloroethane
Chloroform
Chloromethane
Cyclohexane
1,2-Dibromo-3-Chloropropane
Dibromochloromethane
1,2-Dibromoethane
1,2-Dichlorobenzene
1,3-Dichlorobenzene
1,4-Dichlorobenzene
Dichlorodifluoromethane
1,1-Dichloroethane
1,2-Dichloroethane
1,1-Dichloroethene
cis-1,2-Dichloroethene
trans-1,2-Dichloroethene
1,2-Dichloropropane
cis-1,3-Dichloropropene
trans-1,3-Dichloropropene
Ethyl Benzene
2-Hexanone
Isopropylbenzene
Methyl Acetate
Methyl tert-butyl ether
Methylcyclohexane
Methylene Chloride
4-Methyl-2-Pentanone
Naphthalene
Styrene
1,1,2,2-Tetrachloroethane
Tetrachloroethene
Toluene
1,2,3-Trichlorobenzene
1,2,4-Trichlorobenzene
1,1,1-Trichloroethane
1,1,2-Trichloroethane
Trichloroethene
Trichlorofluoromethane
1,1,2-Trichlorotrifluoroethane
Vinyl Chloride
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
Units 4-FD 5-__ 6-__ 7-__
25000 U 25000 U 25000 U 25000 U
25000 U 25000 U 25000 U 25000 U
25000 U 25000 U 25000 U 25000 U
25000 U 25000 U 25000 U 25000 U
25000 U 25000 U 25000 U 25000 U
25000 U 25000 U 25000 U 25000 U
25000 U 25000 U 25000 U 25000 U
25000 U 25000 U 25000 U 25000 U
25000 U 25000 U 25000 U 25000 U
25000 U 25000 U 25000 U 25000 U
25000 U 25000 U 25000 U 25000 U
25000 U 25000 U 25000 U 25000 U
25000 U 25000 U 25000 U 25000 U
25000 U 25000 U 25000 U 25000 U
25000 U 25000 U 25000 U 25000 U
25000 U 25000 U 25000 U 25000 U
25000 U 25000 U 25000 U 25000 U
25000 U 25000 U 25000 U 25000 U
25000 U 25000 U 25000 U 25000 U
25000 U 25000 U 25000 U 25000 U
25000 U 25000 U 25000 U 25000 U
25000 U 25000 U 25000 U 25000 U
25000 U 25000 U 25000 U 25000 U
25000 U 25000 U 25000 U 25000 U
25000 U 25000 U 25000 U 25000 U
25000 U 25000 U 25000 U 25000 U
25000 U 25000 U 25000 U 25000 U
25000 U 25000 U 25000 U 25000 U
50000 UJ 50000 UJ 50000 UJ 50000 UJ
25000 U 25000 U 25000 U 25000 U
25000 U 25000 U 25000 U 25000 U
25000 U 25000 U 25000 U 25000 U
50000 U 50000 U 50000 U 50000 U
25000 U 25000 U 25000 U 25000 U
25000 U 25000 U 25000 U 25000 U
25000 U 25000 U 25000 U 25000 U
25000 U 25000 U 25000 U 25000 U
25000 U 25000 U 25000 U 25000 U
25000 U 25000 U 25000 U 25000 U
25000 U 25000 U 25000 U 25000 U
25000 U 25000 U 25000 U 25000 U
25000 U 25000 U 25000 U 25000 U
25000 U 25000 U 25000 U 25000 U
25000 U 25000 U 25000 U 25000 U
25000 U 25000 U 25000 U 25000 U
4889ASR Number: 06/07/2010
MP7ES02Project ID: Cleburn Street well samplingProject Desc:
RLAB Approved Sample Analysis Results
Page 15 of 43
Analysis/ Analyte
m and/or p-Xylene
o-Xylene
ug/L
ug/L
Units 4-FD 5-__ 6-__ 7-__
50000 U 50000 U 50000 U 50000 U
25000 U 25000 U 25000 U 25000 U
4889ASR Number: 06/07/2010
MP7ES02Project ID: Cleburn Street well samplingProject Desc:
RLAB Approved Sample Analysis Results
Page 16 of 43
1
1
1
1
1
1
1
1
1
1
Alkalinity in Water by Titration
Anions in Water by Ion Chromatography
Conductivity by Field Measurement
Hardness in Water by Calculation
Metals in Water by ICP-AES
pH of Water by Field Measurement
TDS or Total Dissolved Solids
Temperature of Water by Field Measurement
Turbidity of Water by Field Measurement
VOCs in Water by GC/MS
Analysis/ Analyte
Alkalinity, total
Sulfate
Conductivity
Hardness as CaCO3
Aluminum
Antimony
Arsenic
Barium
Beryllium
Cadmium
Calcium
Chromium
Cobalt
Copper
Iron
Lead
Magnesium
Manganese
Molybdenum
Nickel
Potassium
Selenium
Silver
Sodium
Thallium
Titanium
Vanadium
Zinc
pH
Solids, total dissolved
Temperature
Turbidity
Acetone
Benzene
Bromodichloromethane
Bromoform
mg/L
mg/L
umhos/cm
mg/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
mg/L
ug/L
ug/L
ug/L
ug/L
ug/L
mg/L
ug/L
ug/L
ug/L
mg/L
ug/L
ug/L
mg/L
ug/L
ug/L
ug/L
ug/L
SU
mg/L
Deg C
NTU
ug/L
ug/L
ug/L
ug/L
Units 8-__ 9-__ 10-__ 10-FD
2.00 U 233 273 271
10000 U 10000 U 10000 U 10000 U
10400 8810 5960 5960
1620 1770 1320 U 1320 U
43100 5000 U 5000 U 5000 U
5000 U 5000 U 5000 U 5000 U
2500 U 2500 U 2500 U 2500 U
1000 U 1000 U 1000 U 1000 U
300 U 300 U 300 U 300 U
300 U 300 U 300 U 300 U
319 379 200 U 200 U
1500 U 2070 1500 U 1500 U
1000 U 1000 U 1000 U 1000 U
500 U 500 U 500 U 500 U
5000 U 5000 U 5000 U 5000 U
5000 U 5000 U 5000 U 5000 U
200 U 200 U 200 U 200 U
417000 200000 265000 349000
1500 U 1500 U 1500 U 1500 U
2000 U 2650 2000 U 2000 U
1740 889 1160 1440
5000 U 5000 U 5000 U 5000 U
2500 U 2500 U 2500 U 2500 U
500 U 500 U 500 U 500 U
5000 U 5000 U 5000 U 5000 U
2000 U 2000 U 2000 U 2000 U
1000 U 1000 U 1000 U 1000 U
2500 U 2500 U 2500 U 2500 U
2.45 609 6.82 6.82
9900 10300 6080 6620
17.81 21.84 15.66 15.66
134 17.3 0.0 0.0
25000 U 25000 U 25000 U 25000 U
25000 U 25000 U 25000 U 25000 U
25000 U 25000 U 25000 U 25000 U
25000 U 25000 U 25000 U 25000 U
4889ASR Number: 06/07/2010
MP7ES02Project ID: Cleburn Street well samplingProject Desc:
RLAB Approved Sample Analysis Results
Page 17 of 43
Analysis/ Analyte
Bromomethane
2-Butanone
Carbon Disulfide
Carbon Tetrachloride
Chlorobenzene
Chloroethane
Chloroform
Chloromethane
Cyclohexane
1,2-Dibromo-3-Chloropropane
Dibromochloromethane
1,2-Dibromoethane
1,2-Dichlorobenzene
1,3-Dichlorobenzene
1,4-Dichlorobenzene
Dichlorodifluoromethane
1,1-Dichloroethane
1,2-Dichloroethane
1,1-Dichloroethene
cis-1,2-Dichloroethene
trans-1,2-Dichloroethene
1,2-Dichloropropane
cis-1,3-Dichloropropene
trans-1,3-Dichloropropene
Ethyl Benzene
2-Hexanone
Isopropylbenzene
Methyl Acetate
Methyl tert-butyl ether
Methylcyclohexane
Methylene Chloride
4-Methyl-2-Pentanone
Naphthalene
Styrene
1,1,2,2-Tetrachloroethane
Tetrachloroethene
Toluene
1,2,3-Trichlorobenzene
1,2,4-Trichlorobenzene
1,1,1-Trichloroethane
1,1,2-Trichloroethane
Trichloroethene
Trichlorofluoromethane
1,1,2-Trichlorotrifluoroethane
Vinyl Chloride
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
Units 8-__ 9-__ 10-__ 10-FD
25000 U 25000 U 25000 U 25000 U
25000 U 25000 U 25000 U 25000 U
25000 U 25000 U 25000 U 25000 U
25000 U 25000 U 25000 U 25000 U
25000 U 25000 U 25000 U 25000 U
25000 U 25000 U 25000 U 25000 U
25000 U 25000 U 25000 U 25000 U
25000 U 25000 U 25000 U 25000 U
25000 U 25000 U 25000 U 25000 U
25000 U 25000 U 25000 U 25000 U
25000 U 25000 U 25000 U 25000 U
25000 U 25000 U 25000 U 25000 U
25000 U 25000 U 25000 U 25000 U
25000 U 25000 U 25000 U 25000 U
25000 U 25000 U 25000 U 25000 U
25000 U 25000 U 25000 U 25000 U
25000 U 25000 U 25000 U 25000 U
25000 U 25000 U 25000 U 25000 U
25000 U 25000 U 25000 U 25000 U
25000 U 25000 U 25000 U 25000 U
25000 U 25000 U 25000 U 25000 U
25000 U 25000 U 25000 U 25000 U
25000 U 25000 U 25000 U 25000 U
25000 U 25000 U 25000 U 25000 U
25000 U 25000 U 25000 U 25000 U
25000 U 25000 U 25000 U 25000 U
25000 U 25000 U 25000 U 25000 U
25000 U 25000 U 25000 U 25000 U
50000 UJ 50000 UJ 50000 UJ 50000 UJ
25000 U 25000 U 25000 U 25000 U
25000 U 25000 U 25000 U 25000 U
25000 U 25000 U 25000 U 25000 U
50000 U 50000 U 50000 U 50000 U
25000 U 25000 U 25000 U 25000 U
25000 U 25000 U 25000 U 25000 U
25000 U 25000 U 25000 U 25000 U
25000 U 25000 U 25000 U 25000 U
25000 U 25000 U 25000 U 25000 U
25000 U 25000 U 25000 U 25000 U
25000 U 25000 U 25000 U 25000 U
25000 U 25000 U 25000 U 25000 U
25000 U 25000 U 25000 U 25000 U
25000 U 25000 U 25000 U 25000 U
25000 U 25000 U 25000 U 25000 U
25000 U 25000 U 25000 U 25000 U
4889ASR Number: 06/07/2010
MP7ES02Project ID: Cleburn Street well samplingProject Desc:
RLAB Approved Sample Analysis Results
Page 18 of 43
Analysis/ Analyte
m and/or p-Xylene
o-Xylene
ug/L
ug/L
Units 8-__ 9-__ 10-__ 10-FD
50000 U 50000 U 50000 U 50000 U
25000 U 25000 U 25000 U 25000 U
4889ASR Number: 06/07/2010
MP7ES02Project ID: Cleburn Street well samplingProject Desc:
RLAB Approved Sample Analysis Results
Page 19 of 43
1
1
1
1
1
1
1
1
1
1
Alkalinity in Water by Titration
Anions in Water by Ion Chromatography
Conductivity by Field Measurement
Hardness in Water by Calculation
Metals in Water by ICP-AES
pH of Water by Field Measurement
TDS or Total Dissolved Solids
Temperature of Water by Field Measurement
Turbidity of Water by Field Measurement
VOCs in Water by GC/MS
Analysis/ Analyte
Alkalinity, total
Sulfate
Conductivity
Hardness as CaCO3
Aluminum
Antimony
Arsenic
Barium
Beryllium
Cadmium
Calcium
Chromium
Cobalt
Copper
Iron
Lead
Magnesium
Manganese
Molybdenum
Nickel
Potassium
Selenium
Silver
Sodium
Thallium
Titanium
Vanadium
Zinc
pH
Solids, total dissolved
Temperature
Turbidity
Acetone
Benzene
Bromodichloromethane
Bromoform
mg/L
mg/L
umhos/cm
mg/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
mg/L
ug/L
ug/L
ug/L
ug/L
ug/L
mg/L
ug/L
ug/L
ug/L
mg/L
ug/L
ug/L
mg/L
ug/L
ug/L
ug/L
ug/L
SU
mg/L
Deg C
NTU
ug/L
ug/L
ug/L
ug/L
Units 11-__ 12-__ 13-__ 14-__
166 288 272 347
10000 U 10000 U 10000 U 10000 U
10,000 9020 3910 7890
2040 1370 1670 1870
5000 U 5000 U 5000 U 5000 U
5000 U 5000 U 5000 U 5000 U
2500 U 2500 U 2500 U 2500 U
1000 U 1000 U 1000 U 1000 U
300 U 300 U 300 U 300 U
300 U 300 U 300 U 300 U
486 220 338 421
1500 U 1500 U 7030 1500 U
1000 U 1000 U 1000 U 1000 U
500 U 500 U 500 U 500 U
5000 U 5000 U 5000 U 5000 U
5000 U 5000 U 5000 U 5000 U
200 U 200 U 200 U 200 U
314000 355000 265000 341000
1500 U 1500 U 1500 U 1500 U
2000 U 2000 U 2000 U 2000 U
1600 1850 208 1150
5000 U 5000 U 5000 U 5000 U
2500 U 2500 U 2500 U 2500 U
500 U 500 U 500 U 500 U
5000 U 5000 U 5000 U 5000 U
2000 U 2000 U 2000 U 2000 U
1000 U 1000 U 1000 U 1000 U
2500 U 2500 U 2500 U 2500 U
5.88 6.67 6.77 6.96
10500 10600 3690 8870
16.55 15.09 14.65 15.14
39.5 0.1 11.9 41.1
25000 U 25000 U 25000 U 25000 U
25000 U 25000 U 25000 U 25000 U
25000 U 25000 U 25000 U 25000 U
25000 U 25000 U 25000 U 25000 U
4889ASR Number: 06/07/2010
MP7ES02Project ID: Cleburn Street well samplingProject Desc:
RLAB Approved Sample Analysis Results
Page 20 of 43
Analysis/ Analyte
Bromomethane
2-Butanone
Carbon Disulfide
Carbon Tetrachloride
Chlorobenzene
Chloroethane
Chloroform
Chloromethane
Cyclohexane
1,2-Dibromo-3-Chloropropane
Dibromochloromethane
1,2-Dibromoethane
1,2-Dichlorobenzene
1,3-Dichlorobenzene
1,4-Dichlorobenzene
Dichlorodifluoromethane
1,1-Dichloroethane
1,2-Dichloroethane
1,1-Dichloroethene
cis-1,2-Dichloroethene
trans-1,2-Dichloroethene
1,2-Dichloropropane
cis-1,3-Dichloropropene
trans-1,3-Dichloropropene
Ethyl Benzene
2-Hexanone
Isopropylbenzene
Methyl Acetate
Methyl tert-butyl ether
Methylcyclohexane
Methylene Chloride
4-Methyl-2-Pentanone
Naphthalene
Styrene
1,1,2,2-Tetrachloroethane
Tetrachloroethene
Toluene
1,2,3-Trichlorobenzene
1,2,4-Trichlorobenzene
1,1,1-Trichloroethane
1,1,2-Trichloroethane
Trichloroethene
Trichlorofluoromethane
1,1,2-Trichlorotrifluoroethane
Vinyl Chloride
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
Units 11-__ 12-__ 13-__ 14-__
25000 U 25000 U 25000 U 25000 U
25000 U 25000 U 25000 U 25000 U
25000 U 25000 U 25000 U 25000 U
25000 U 25000 U 25000 U 25000 U
25000 U 25000 U 25000 U 25000 U
25000 U 25000 U 25000 U 25000 U
25000 U 25000 U 25000 U 25000 U
25000 U 25000 U 25000 U 25000 U
25000 U 25000 U 25000 U 25000 U
25000 U 25000 U 25000 U 25000 U
25000 U 25000 U 25000 U 25000 U
25000 U 25000 U 25000 U 25000 U
25000 U 25000 U 25000 U 25000 U
25000 U 25000 U 25000 U 25000 U
25000 U 25000 U 25000 U 25000 U
25000 U 25000 U 25000 U 25000 U
25000 U 25000 U 25000 U 25000 U
25000 U 25000 U 25000 U 25000 U
25000 U 25000 U 25000 U 25000 U
25000 U 25000 U 25000 U 25000 U
25000 U 25000 U 25000 U 25000 U
25000 U 25000 U 25000 U 25000 U
25000 U 25000 U 25000 U 25000 U
25000 U 25000 U 25000 U 25000 U
25000 U 25000 U 25000 U 25000 U
25000 U 25000 U 25000 U 25000 U
25000 U 25000 U 25000 U 25000 U
25000 U 25000 U 25000 U 25000 U
50000 UJ 50000 UJ 50000 UJ 50000 UJ
25000 U 25000 U 25000 U 25000 U
25000 U 25000 U 25000 U 25000 U
25000 U 25000 U 25000 U 25000 U
50000 U 50000 U 50000 U 50000 U
25000 U 25000 U 25000 U 25000 U
25000 U 25000 U 25000 U 25000 U
25000 U 25000 U 25000 U 25000 U
25000 U 25000 U 25000 U 25000 U
25000 U 25000 U 25000 U 25000 U
25000 U 25000 U 25000 U 25000 U
25000 U 25000 U 25000 U 25000 U
25000 U 25000 U 25000 U 25000 U
25000 U 25000 U 25000 U 25000 U
25000 U 25000 U 25000 U 25000 U
25000 U 25000 U 25000 U 25000 U
25000 U 25000 U 25000 U 25000 U
4889ASR Number: 06/07/2010
MP7ES02Project ID: Cleburn Street well samplingProject Desc:
RLAB Approved Sample Analysis Results
Page 21 of 43
Analysis/ Analyte
m and/or p-Xylene
o-Xylene
ug/L
ug/L
Units 11-__ 12-__ 13-__ 14-__
50000 U 50000 U 50000 U 50000 U
25000 U 25000 U 25000 U 25000 U
4889ASR Number: 06/07/2010
MP7ES02Project ID: Cleburn Street well samplingProject Desc:
RLAB Approved Sample Analysis Results
Page 22 of 43
1
1
1
1
1
1
1
1
1
1
Alkalinity in Water by Titration
Anions in Water by Ion Chromatography
Conductivity by Field Measurement
Hardness in Water by Calculation
Metals in Water by ICP-AES
pH of Water by Field Measurement
TDS or Total Dissolved Solids
Temperature of Water by Field Measurement
Turbidity of Water by Field Measurement
VOCs in Water by GC/MS
Analysis/ Analyte
Alkalinity, total
Sulfate
Conductivity
Hardness as CaCO3
Aluminum
Antimony
Arsenic
Barium
Beryllium
Cadmium
Calcium
Chromium
Cobalt
Copper
Iron
Lead
Magnesium
Manganese
Molybdenum
Nickel
Potassium
Selenium
Silver
Sodium
Thallium
Titanium
Vanadium
Zinc
pH
Solids, total dissolved
Temperature
Turbidity
Acetone
Benzene
Bromodichloromethane
Bromoform
mg/L
mg/L
umhos/cm
mg/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
mg/L
ug/L
ug/L
ug/L
ug/L
ug/L
mg/L
ug/L
ug/L
ug/L
mg/L
ug/L
ug/L
mg/L
ug/L
ug/L
ug/L
ug/L
SU
mg/L
Deg C
NTU
ug/L
ug/L
ug/L
ug/L
Units 15-__ 16-__ 17-__ 18-__
476 216 142 566
10000 U 10000 U 33.3 10000 U
7090 5110 503 7020
1650 1320 U 206 1320 U
5000 U 5000 U 50 U 5000 U
5000 U 5000 U 50 U 5000 U
2500 U 2500 U 25 U 2500 U
1000 U 1000 U 359 1000 U
300 U 300 U 3 U 300 U
300 U 300 U 3 U 300 U
332 200 U 66.1 200 U
5430 1500 U 15 U 1500 U
1000 U 1000 U 10 U 1000 U
500 U 500 U 5 U 500 U
5000 U 5000 U 95 5000 U
5000 U 5000 U 50 U 5000 U
200 U 200 U 9.95 200 U
319000 367000 10 321000
1500 U 1500 U 15 U 1500 U
2000 U 2000 U 20 U 2000 U
1470 1170 9.69 1720
5000 U 5000 U 50 U 5000 U
2500 U 2500 U 25 U 2500 U
500 U 500 U 12.3 500 U
5000 U 5000 U 50 U 5000 U
2000 U 2000 U 20 U 2000 U
1000 U 1000 U 10 U 1000 U
2500 U 2500 U 25 U 2500 U
6.94 8.17 7.11 9.17
6310 6160 323 8280
15.62 14.22 14.29 13.96
113 13.5 0.0 22.4
25000 U 25000 U 5.0 U 25000 U
25000 U 25000 U 5.0 U 25000 U
25000 U 25000 U 5.0 UJ 25000 U
25000 U 25000 U 5.0 U 25000 U
4889ASR Number: 06/07/2010
MP7ES02Project ID: Cleburn Street well samplingProject Desc:
RLAB Approved Sample Analysis Results
Page 23 of 43
Analysis/ Analyte
Bromomethane
2-Butanone
Carbon Disulfide
Carbon Tetrachloride
Chlorobenzene
Chloroethane
Chloroform
Chloromethane
Cyclohexane
1,2-Dibromo-3-Chloropropane
Dibromochloromethane
1,2-Dibromoethane
1,2-Dichlorobenzene
1,3-Dichlorobenzene
1,4-Dichlorobenzene
Dichlorodifluoromethane
1,1-Dichloroethane
1,2-Dichloroethane
1,1-Dichloroethene
cis-1,2-Dichloroethene
trans-1,2-Dichloroethene
1,2-Dichloropropane
cis-1,3-Dichloropropene
trans-1,3-Dichloropropene
Ethyl Benzene
2-Hexanone
Isopropylbenzene
Methyl Acetate
Methyl tert-butyl ether
Methylcyclohexane
Methylene Chloride
4-Methyl-2-Pentanone
Naphthalene
Styrene
1,1,2,2-Tetrachloroethane
Tetrachloroethene
Toluene
1,2,3-Trichlorobenzene
1,2,4-Trichlorobenzene
1,1,1-Trichloroethane
1,1,2-Trichloroethane
Trichloroethene
Trichlorofluoromethane
1,1,2-Trichlorotrifluoroethane
Vinyl Chloride
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
Units 15-__ 16-__ 17-__ 18-__
25000 U 25000 U 5.0 U 25000 U
25000 U 25000 U 5.0 U 25000 U
25000 U 25000 U 5.0 U 25000 U
25000 U 25000 U 5.0 U 25000 U
25000 U 25000 U 5.0 U 25000 U
25000 U 25000 U 5.0 U 25000 U
25000 U 25000 U 5.0 U 25000 U
25000 U 25000 U 5.0 U 25000 U
25000 U 25000 U 5.0 U 25000 U
25000 U 25000 U 5.0 U 25000 U
25000 U 25000 U 5.0 U 25000 U
25000 U 25000 U 5.0 U 25000 U
25000 U 25000 U 5.0 U 25000 U
25000 U 25000 U 5.0 U 25000 U
25000 U 25000 U 5.0 U 25000 U
25000 U 25000 U 5.0 U 25000 U
25000 U 25000 U 5.0 U 25000 U
25000 U 25000 U 5.0 UJ 25000 U
25000 U 25000 U 5.0 U 25000 U
25000 U 25000 U 5.0 U 25000 U
25000 U 25000 U 5.0 U 25000 U
25000 U 25000 U 5.0 U 25000 U
25000 U 25000 U 5.0 U 25000 U
25000 U 25000 U 5.0 U 25000 U
25000 U 25000 U 5.0 U 25000 U
25000 U 25000 U 5.0 U 25000 U
25000 U 25000 U 5.0 U 25000 U
25000 U 25000 U 5.0 U 25000 U
50000 UJ 50000 UJ 10 UJ 50000 UJ
25000 U 25000 U 5.0 U 25000 U
25000 U 25000 U 5.0 U 25000 U
25000 U 25000 U 5.0 U 25000 U
50000 U 50000 U 10 U 50000 U
25000 U 25000 U 5.0 U 25000 U
25000 U 25000 U 5.0 U 25000 U
25000 U 25000 U 5.0 U 25000 U
25000 U 25000 U 5.0 U 25000 U
25000 U 25000 U 5.0 U 25000 U
25000 U 25000 U 5.0 U 25000 U
25000 U 25000 U 5.0 U 25000 U
25000 U 25000 U 5.0 U 25000 U
25000 U 25000 U 5.0 U 25000 U
25000 U 25000 U 5.0 U 25000 U
25000 U 25000 U 5.0 U 25000 U
25000 U 25000 U 5.0 U 25000 U
4889ASR Number: 06/07/2010
MP7ES02Project ID: Cleburn Street well samplingProject Desc:
RLAB Approved Sample Analysis Results
Page 24 of 43
Analysis/ Analyte
m and/or p-Xylene
o-Xylene
ug/L
ug/L
Units 15-__ 16-__ 17-__ 18-__
50000 U 50000 U 10 U 50000 U
25000 U 25000 U 5.0 U 25000 U
4889ASR Number: 06/07/2010
MP7ES02Project ID: Cleburn Street well samplingProject Desc:
RLAB Approved Sample Analysis Results
Page 25 of 43
1
1
1
1
1
1
1
1
1
1
Alkalinity in Water by Titration
Anions in Water by Ion Chromatography
Conductivity by Field Measurement
Hardness in Water by Calculation
Metals in Water by ICP-AES
pH of Water by Field Measurement
TDS or Total Dissolved Solids
Temperature of Water by Field Measurement
Turbidity of Water by Field Measurement
VOCs in Water by GC/MS
Analysis/ Analyte
Alkalinity, total
Sulfate
Conductivity
Hardness as CaCO3
Aluminum
Antimony
Arsenic
Barium
Beryllium
Cadmium
Calcium
Chromium
Cobalt
Copper
Iron
Lead
Magnesium
Manganese
Molybdenum
Nickel
Potassium
Selenium
Silver
Sodium
Thallium
Titanium
Vanadium
Zinc
pH
Solids, total dissolved
Temperature
Turbidity
Acetone
Benzene
Bromodichloromethane
Bromoform
mg/L
mg/L
umhos/cm
mg/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
mg/L
ug/L
ug/L
ug/L
ug/L
ug/L
mg/L
ug/L
ug/L
ug/L
mg/L
ug/L
ug/L
mg/L
ug/L
ug/L
ug/L
ug/L
SU
mg/L
Deg C
NTU
ug/L
ug/L
ug/L
ug/L
Units 19-__ 20-__ 20-FD 24-FB
140 78.2 77.7
67.2 92.8 106
937 971 971
251 293 285
519 50 U 50 U 50 U
50 U 50 U 50 U 50 U
25 U 25 U 25 U 25 U
223 170 166 10 U
3 U 3 U 3 U 3 U
3 U 3 U 3 U 3 U
73.9 83.4 81.8 2.00 U
15 U 15 U 15 U 15 U
10 U 10 U 10 U 10 U
5 U 5 U 5 U 5 U
477 50 U 50 U 50 U
50 U 50 U 50 U 50 U
16.2 20.6 19.7 2.00 U
184 9 5 U 5 U
15 U 15 U 15 U 15 U
20 U 27 25 20 U
8.45 16.8 16.4 2.00 U
50 U 50 U 50 U 50 U
25 U 25 U 25 U 25 U
90.4 69.8 66.1 5.00 U
50 U 50 U 50 U 50 U
20 U 20 U 20 U 20 U
10 U 10 U 10 U 10 U
25 U 25 U 25 U 25 U
6.90 7.01 7.01
584 680 680
14.54 15.38 15.38
0.0 0.0 0.0
5.0 U 5.0 U 5.0 U 5.0 U
5.0 U 5.0 U 5.0 U 5.0 U
5.0 U 5.0 U 5.0 U 5.0 U
5.0 U 5.0 U 5.0 U 5.0 U
4889ASR Number: 06/07/2010
MP7ES02Project ID: Cleburn Street well samplingProject Desc:
RLAB Approved Sample Analysis Results
Page 26 of 43
Analysis/ Analyte
Bromomethane
2-Butanone
Carbon Disulfide
Carbon Tetrachloride
Chlorobenzene
Chloroethane
Chloroform
Chloromethane
Cyclohexane
1,2-Dibromo-3-Chloropropane
Dibromochloromethane
1,2-Dibromoethane
1,2-Dichlorobenzene
1,3-Dichlorobenzene
1,4-Dichlorobenzene
Dichlorodifluoromethane
1,1-Dichloroethane
1,2-Dichloroethane
1,1-Dichloroethene
cis-1,2-Dichloroethene
trans-1,2-Dichloroethene
1,2-Dichloropropane
cis-1,3-Dichloropropene
trans-1,3-Dichloropropene
Ethyl Benzene
2-Hexanone
Isopropylbenzene
Methyl Acetate
Methyl tert-butyl ether
Methylcyclohexane
Methylene Chloride
4-Methyl-2-Pentanone
Naphthalene
Styrene
1,1,2,2-Tetrachloroethane
Tetrachloroethene
Toluene
1,2,3-Trichlorobenzene
1,2,4-Trichlorobenzene
1,1,1-Trichloroethane
1,1,2-Trichloroethane
Trichloroethene
Trichlorofluoromethane
1,1,2-Trichlorotrifluoroethane
Vinyl Chloride
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
Units 19-__ 20-__ 20-FD 24-FB
5.0 U 5.0 U 5.0 U 5.0 U
5.0 U 5.0 U 5.0 U 5.0 U
5.0 U 5.0 U 5.0 U 5.0 U
5.0 U 5.0 U 5.0 U 5.0 U
5.0 U 5.0 U 5.0 U 5.0 U
5.0 U 5.0 U 5.0 U 5.0 U
5.0 U 5.0 U 5.0 U 5.0 U
5.0 U 5.0 U 5.0 U 5.0 U
6.1 5.0 U 5.0 U 5.0 U
5.0 U 5.0 U 5.0 U 5.0 U
5.0 U 5.0 U 5.0 U 5.0 U
5.0 U 5.0 U 5.0 U 5.0 U
5.0 U 5.0 U 5.0 U 5.0 U
5.0 U 5.0 U 5.0 U 5.0 U
5.0 U 5.0 U 5.0 U 5.0 U
5.0 U 5.0 U 5.0 U 5.0 UJ
5.0 U 5.0 U 5.0 U 5.0 U
5.0 U 5.0 U 5.0 U 5.0 U
5.0 U 5.0 U 5.0 U 5.0 U
12 5.0 U 5.0 U 5.0 U
5.0 U 5.0 U 5.0 U 5.0 U
5.0 U 5.0 U 5.0 U 5.0 U
5.0 U 5.0 U 5.0 U 5.0 U
5.0 U 5.0 U 5.0 U 5.0 U
5.0 U 5.0 U 5.0 U 5.0 U
5.0 U 5.0 U 5.0 U 5.0 U
5.0 U 5.0 U 5.0 U 5.0 U
5.0 U 5.0 U 5.0 U 5.0 U
10 UJ 10 UJ 10 UJ 10 U
5.0 U 5.0 U 5.0 U 5.0 U
5.0 U 5.0 U 5.0 U 5.0 U
5.0 U 5.0 U 5.0 U 5.0 U
12 J 10 U 10 U 10 U
5.0 U 5.0 U 5.0 U 5.0 U
5.0 U 5.0 U 5.0 U 5.0 U
4100 11 11 5.0 U
5.3 5.0 U 5.0 U 5.0 U
5.0 U 5.0 U 5.0 U 5.0 U
5.0 U 5.0 U 5.0 U 5.0 U
5.0 U 5.0 U 5.0 U 5.0 U
5.0 U 5.0 U 5.0 U 5.0 U
280 5.0 U 5.0 U 5.0 U
5.0 U 5.0 U 5.0 U 5.0 U
5.0 U 5.0 U 5.0 U 5.0 U
5.0 U 5.0 U 5.0 U 5.0 U
4889ASR Number: 06/07/2010
MP7ES02Project ID: Cleburn Street well samplingProject Desc:
RLAB Approved Sample Analysis Results
Page 27 of 43
Analysis/ Analyte
m and/or p-Xylene
o-Xylene
ug/L
ug/L
Units 19-__ 20-__ 20-FD 24-FB
23 10 U 10 U 10 U
9.0 5.0 U 5.0 U 5.0 U
4889ASR Number: 06/07/2010
MP7ES02Project ID: Cleburn Street well samplingProject Desc:
RLAB Approved Sample Analysis Results
Page 28 of 43
1
1
1
1
1
Conductivity by Field Measurement
pH of Water by Field Measurement
Temperature of Water by Field Measurement
Turbidity of Water by Field Measurement
VOCs in Water by GC/MS
Analysis/ Analyte
Conductivity
pH
Temperature
Turbidity
Acetone
Benzene
Bromodichloromethane
Bromoform
Bromomethane
2-Butanone
Carbon Disulfide
Carbon Tetrachloride
Chlorobenzene
Chloroethane
Chloroform
Chloromethane
Cyclohexane
1,2-Dibromo-3-Chloropropane
Dibromochloromethane
1,2-Dibromoethane
1,2-Dichlorobenzene
1,3-Dichlorobenzene
1,4-Dichlorobenzene
Dichlorodifluoromethane
1,1-Dichloroethane
1,2-Dichloroethane
1,1-Dichloroethene
cis-1,2-Dichloroethene
trans-1,2-Dichloroethene
1,2-Dichloropropane
cis-1,3-Dichloropropene
trans-1,3-Dichloropropene
Ethyl Benzene
2-Hexanone
Isopropylbenzene
Methyl Acetate
Methyl tert-butyl ether
Methylcyclohexane
Methylene Chloride
4-Methyl-2-Pentanone
Naphthalene
umhos/cm
SU
Deg C
NTU
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
Units 25-__ 26-__ 27-__ 28-__
749 818 1140 619
7.28 6.94 6.62 5.56
14.54 14.51 14.17 14.86
0.0 0.0 0.0 416
5.0 U 5.0 U 5.0 U 5.0 U
5.0 U 5.0 U 5.0 U 5.0 U
5.0 U 5.0 U 5.0 U 5.0 U
5.0 U 5.0 U 5.0 U 5.0 U
5.0 U 5.0 U 5.0 U 5.0 U
5.0 U 5.0 U 5.0 U 5.0 U
5.0 U 5.0 U 5.0 U 5.0 U
5.0 U 5.0 U 5.0 U 5.0 U
5.0 U 5.0 U 5.0 U 5.0 U
5.0 U 5.0 U 5.0 U 5.0 U
5.0 U 5.0 U 5.0 U 5.0 U
5.0 U 5.0 U 5.0 U 5.0 U
5.0 U 5.0 U 5.0 U 5.0 U
5.0 U 5.0 U 5.0 U 5.0 U
5.0 U 5.0 U 5.0 U 5.0 U
5.0 U 5.0 U 5.0 U 5.0 U
5.0 U 5.0 U 5.0 U 5.0 U
5.0 U 5.0 U 5.0 U 5.0 U
5.0 U 5.0 U 5.0 U 5.0 U
5.0 U 5.0 UJ 5.0 UJ 5.0 UJ
5.0 U 5.0 U 5.0 U 5.0 U
5.0 U 5.0 U 5.0 U 5.0 U
5.0 U 5.0 U 5.0 U 5.0 U
5.0 U 5.0 U 5.0 U 5.0 U
5.0 U 5.0 U 5.0 U 5.0 U
5.0 U 5.0 U 5.0 U 5.0 U
5.0 U 5.0 U 5.0 U 5.0 U
5.0 U 5.0 U 5.0 U 5.0 U
5.0 U 5.0 U 5.0 U 5.0 U
5.0 U 5.0 U 5.0 U 5.0 U
5.0 U 5.0 U 5.0 U 5.0 U
5.0 U 5.0 U 5.0 U 5.0 U
10 UJ 10 U 10 U 10 U
5.0 U 5.0 U 5.0 U 5.0 U
5.0 U 5.0 U 5.0 U 5.0 U
5.0 U 5.0 U 5.0 U 5.0 U
10 U 10 U 10 U 10 U
4889ASR Number: 06/07/2010
MP7ES02Project ID: Cleburn Street well samplingProject Desc:
RLAB Approved Sample Analysis Results
Page 29 of 43
Analysis/ Analyte
Styrene
1,1,2,2-Tetrachloroethane
Tetrachloroethene
Toluene
1,2,3-Trichlorobenzene
1,2,4-Trichlorobenzene
1,1,1-Trichloroethane
1,1,2-Trichloroethane
Trichloroethene
Trichlorofluoromethane
1,1,2-Trichlorotrifluoroethane
Vinyl Chloride
m and/or p-Xylene
o-Xylene
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
Units 25-__ 26-__ 27-__ 28-__
5.0 U 5.0 U 5.0 U 5.0 U
5.0 U 5.0 U 5.0 U 5.0 U
5.0 U 5.0 U 5.0 U 5.0 U
5.0 U 5.0 U 5.0 U 5.0 U
5.0 U 5.0 U 5.0 U 5.0 U
5.0 U 5.0 U 5.0 U 5.0 U
5.0 U 5.0 U 5.0 U 5.0 U
5.0 U 5.0 U 5.0 U 5.0 U
5.0 U 5.0 U 5.0 U 5.0 U
5.0 U 5.0 U 5.0 U 5.0 U
5.0 U 5.0 U 5.0 U 5.0 U
5.0 U 5.0 U 5.0 U 5.0 U
10 U 10 U 10 U 10 U
5.0 U 5.0 U 5.0 U 5.0 U
4889ASR Number: 06/07/2010
MP7ES02Project ID: Cleburn Street well samplingProject Desc:
RLAB Approved Sample Analysis Results
Page 30 of 43
1
1
1
1
1
Conductivity by Field Measurement
pH of Water by Field Measurement
Temperature of Water by Field Measurement
Turbidity of Water by Field Measurement
VOCs in Water by GC/MS
Analysis/ Analyte
Conductivity
pH
Temperature
Turbidity
Acetone
Benzene
Bromodichloromethane
Bromoform
Bromomethane
2-Butanone
Carbon Disulfide
Carbon Tetrachloride
Chlorobenzene
Chloroethane
Chloroform
Chloromethane
Cyclohexane
1,2-Dibromo-3-Chloropropane
Dibromochloromethane
1,2-Dibromoethane
1,2-Dichlorobenzene
1,3-Dichlorobenzene
1,4-Dichlorobenzene
Dichlorodifluoromethane
1,1-Dichloroethane
1,2-Dichloroethane
1,1-Dichloroethene
cis-1,2-Dichloroethene
trans-1,2-Dichloroethene
1,2-Dichloropropane
cis-1,3-Dichloropropene
trans-1,3-Dichloropropene
Ethyl Benzene
2-Hexanone
Isopropylbenzene
Methyl Acetate
Methyl tert-butyl ether
Methylcyclohexane
Methylene Chloride
4-Methyl-2-Pentanone
Naphthalene
umhos/cm
SU
Deg C
NTU
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
Units 29-__ 29-FD 30-__ 31-__
505 505 2380 844
6.95 6.95 7.00 6.72
14.61 14.61 16.03 14.67
0.0 0.0 0.0 0.0
5.0 U 5.0 U 25000 U 5.0 U
5.0 U 5.0 U 25000 U 5.0 U
5.0 U 5.0 U 25000 U 5.0 U
5.0 U 5.0 U 25000 U 5.0 U
5.0 U 5.0 U 25000 U 5.0 U
5.0 U 5.0 U 25000 U 5.0 U
5.0 U 5.0 U 25000 U 5.0 U
5.0 U 5.0 U 25000 U 5.0 U
5.0 U 5.0 U 25000 U 5.0 U
5.0 U 5.0 U 25000 U 5.0 U
5.0 U 5.0 U 25000 U 5.0 U
5.0 U 5.0 U 25000 U 5.0 U
5.0 U 5.0 U 25000 U 5.0 U
5.0 U 5.0 U 25000 U 5.0 U
5.0 U 5.0 U 25000 U 5.0 U
5.0 U 5.0 U 25000 U 5.0 U
5.0 U 5.0 U 25000 U 5.0 U
5.0 U 5.0 U 25000 U 5.0 U
5.0 U 5.0 U 25000 U 5.0 U
5.0 UJ 5.0 UJ 25000 U 5.0 U
5.0 U 5.0 U 25000 U 5.0 U
5.0 U 5.0 U 25000 U 5.0 U
5.0 U 5.0 U 25000 U 5.0 U
5.0 U 5.0 U 25000 U 5.0 U
5.0 U 5.0 U 25000 U 5.0 U
5.0 U 5.0 U 25000 U 5.0 U
5.0 U 5.0 U 25000 U 5.0 U
5.0 U 5.0 U 25000 U 5.0 U
5.0 U 5.0 U 25000 U 5.0 U
5.0 U 5.0 U 25000 U 5.0 U
5.0 U 5.0 U 25000 U 5.0 U
5.0 U 5.0 U 25000 U 5.0 U
10 U 10 U 50000 UJ 10 UJ
5.0 U 5.0 U 25000 U 5.0 U
5.0 U 5.0 U 25000 U 5.0 U
5.0 U 5.0 U 25000 U 5.0 U
10 U 10 U 50000 U 10 U
4889ASR Number: 06/07/2010
MP7ES02Project ID: Cleburn Street well samplingProject Desc:
RLAB Approved Sample Analysis Results
Page 31 of 43
Analysis/ Analyte
Styrene
1,1,2,2-Tetrachloroethane
Tetrachloroethene
Toluene
1,2,3-Trichlorobenzene
1,2,4-Trichlorobenzene
1,1,1-Trichloroethane
1,1,2-Trichloroethane
Trichloroethene
Trichlorofluoromethane
1,1,2-Trichlorotrifluoroethane
Vinyl Chloride
m and/or p-Xylene
o-Xylene
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
Units 29-__ 29-FD 30-__ 31-__
5.0 U 5.0 U 25000 U 5.0 U
5.0 U 5.0 U 25000 U 5.0 U
5.0 U 5.0 U 25000 U 5.0 U
5.0 U 5.0 U 25000 U 5.0 U
5.0 U 5.0 U 25000 U 5.0 U
5.0 U 5.0 U 25000 U 5.0 U
5.0 U 5.0 U 25000 U 5.0 U
5.0 U 5.0 U 25000 U 5.0 U
5.0 U 5.0 U 25000 U 5.0 U
5.0 U 5.0 U 25000 U 5.0 U
5.0 U 5.0 U 25000 U 5.0 U
5.0 U 5.0 U 25000 U 5.0 U
10 U 10 U 50000 U 10 U
5.0 U 5.0 U 25000 U 5.0 U
4889ASR Number: 06/07/2010
MP7ES02Project ID: Cleburn Street well samplingProject Desc:
RLAB Approved Sample Analysis Results
Page 32 of 43
1
1
1
1
1
Conductivity by Field Measurement
pH of Water by Field Measurement
Temperature of Water by Field Measurement
Turbidity of Water by Field Measurement
VOCs in Water by GC/MS
Analysis/ Analyte
Conductivity
pH
Temperature
Turbidity
Acetone
Benzene
Bromodichloromethane
Bromoform
Bromomethane
2-Butanone
Carbon Disulfide
Carbon Tetrachloride
Chlorobenzene
Chloroethane
Chloroform
Chloromethane
Cyclohexane
1,2-Dibromo-3-Chloropropane
Dibromochloromethane
1,2-Dibromoethane
1,2-Dichlorobenzene
1,3-Dichlorobenzene
1,4-Dichlorobenzene
Dichlorodifluoromethane
1,1-Dichloroethane
1,2-Dichloroethane
1,1-Dichloroethene
cis-1,2-Dichloroethene
trans-1,2-Dichloroethene
1,2-Dichloropropane
cis-1,3-Dichloropropene
trans-1,3-Dichloropropene
Ethyl Benzene
2-Hexanone
Isopropylbenzene
Methyl Acetate
Methyl tert-butyl ether
Methylcyclohexane
Methylene Chloride
4-Methyl-2-Pentanone
Naphthalene
umhos/cm
SU
Deg C
NTU
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
Units 32-__ 33-__ 33-FD 34-__
517 515 515 785
6.53 6.98 6.98 6.47
14.37 14.97 14.97 14.41
0.0 0.0 0.0 0.0
5.0 U 5.0 U 5.0 U 5.0 U
5.0 U 5.0 U 5.0 U 5.0 U
5.0 U 5.0 U 5.0 U 5.0 U
5.0 U 5.0 U 5.0 U 5.0 U
5.0 U 5.0 U 5.0 U 5.0 U
5.0 U 5.0 U 5.0 U 5.0 U
5.0 U 5.0 U 5.0 U 5.0 U
5.0 U 5.0 U 5.0 U 5.0 U
5.0 U 5.0 U 5.0 U 5.0 U
5.0 U 5.0 U 5.0 U 5.0 U
5.0 U 5.0 U 5.0 U 5.0 U
5.0 U 5.0 U 5.0 U 5.0 U
5.0 U 5.0 U 5.0 U 5.0 U
5.0 U 5.0 U 5.0 U 5.0 U
5.0 U 5.0 U 5.0 U 5.0 U
5.0 U 5.0 U 5.0 U 5.0 U
5.0 U 5.0 U 5.0 U 5.0 U
5.0 U 5.0 U 5.0 U 5.0 U
5.0 U 5.0 U 5.0 U 5.0 U
5.0 U 5.0 U 5.0 U 5.0 UJ
5.0 U 5.0 U 5.0 U 5.0 U
5.0 U 5.0 U 5.0 U 5.0 U
5.0 U 5.0 U 5.0 U 5.0 U
5.0 U 5.0 U 5.0 U 5.0 U
5.0 U 5.0 U 5.0 U 5.0 U
5.0 U 5.0 U 5.0 U 5.0 U
5.0 U 5.0 U 5.0 U 5.0 U
5.0 U 5.0 U 5.0 U 5.0 U
5.0 U 5.0 U 5.0 U 5.0 U
5.0 U 5.0 U 5.0 U 5.0 U
5.0 U 5.0 U 5.0 U 5.0 U
5.0 U 5.0 U 5.0 U 5.0 U
10 UJ 10 UJ 10 UJ 10 UJ
5.0 U 5.0 U 5.0 U 5.0 U
5.0 U 5.0 U 5.0 U 5.0 U
5.0 U 5.0 U 5.0 U 5.0 U
10 U 10 U 10 U 10 U
4889ASR Number: 06/07/2010
MP7ES02Project ID: Cleburn Street well samplingProject Desc:
RLAB Approved Sample Analysis Results
Page 33 of 43
Analysis/ Analyte
Styrene
1,1,2,2-Tetrachloroethane
Tetrachloroethene
Toluene
1,2,3-Trichlorobenzene
1,2,4-Trichlorobenzene
1,1,1-Trichloroethane
1,1,2-Trichloroethane
Trichloroethene
Trichlorofluoromethane
1,1,2-Trichlorotrifluoroethane
Vinyl Chloride
m and/or p-Xylene
o-Xylene
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
Units 32-__ 33-__ 33-FD 34-__
5.0 U 5.0 U 5.0 U 5.0 U
5.0 U 5.0 U 5.0 U 5.0 U
5.0 U 5.0 U 5.0 U 5.0 U
5.0 U 5.0 U 5.0 U 5.0 U
5.0 U 5.0 U 5.0 U 5.0 U
5.0 U 5.0 U 5.0 U 5.0 U
5.0 U 5.0 U 5.0 U 5.0 U
5.0 U 5.0 U 5.0 U 5.0 U
5.0 U 5.0 U 5.0 U 5.0 U
5.0 U 5.0 U 5.0 U 5.0 U
5.0 U 5.0 U 5.0 U 5.0 U
5.0 U 5.0 U 5.0 U 5.0 U
10 U 10 U 10 U 10 U
5.0 U 5.0 U 5.0 U 5.0 U
4889ASR Number: 06/07/2010
MP7ES02Project ID: Cleburn Street well samplingProject Desc:
RLAB Approved Sample Analysis Results
Page 34 of 43
1
1
1
1
1
Conductivity by Field Measurement
pH of Water by Field Measurement
Temperature of Water by Field Measurement
Turbidity of Water by Field Measurement
VOCs in Water by GC/MS
Analysis/ Analyte
Conductivity
pH
Temperature
Turbidity
Acetone
Benzene
Bromodichloromethane
Bromoform
Bromomethane
2-Butanone
Carbon Disulfide
Carbon Tetrachloride
Chlorobenzene
Chloroethane
Chloroform
Chloromethane
Cyclohexane
1,2-Dibromo-3-Chloropropane
Dibromochloromethane
1,2-Dibromoethane
1,2-Dichlorobenzene
1,3-Dichlorobenzene
1,4-Dichlorobenzene
Dichlorodifluoromethane
1,1-Dichloroethane
1,2-Dichloroethane
1,1-Dichloroethene
cis-1,2-Dichloroethene
trans-1,2-Dichloroethene
1,2-Dichloropropane
cis-1,3-Dichloropropene
trans-1,3-Dichloropropene
Ethyl Benzene
2-Hexanone
Isopropylbenzene
Methyl Acetate
Methyl tert-butyl ether
Methylcyclohexane
Methylene Chloride
4-Methyl-2-Pentanone
Naphthalene
umhos/cm
SU
Deg C
NTU
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
Units 35-__ 36-__ 37-__ 38-__
1610 793 552 488
6.92 6.91 7.03 6.78
14.84 15.71 14.53 15.79
40.1 41.6 34.9 0.0
5.0 U 5.0 U 5.0 U 5.0 U
5.0 U 5.0 U 5.0 U 5.0 U
5.0 U 5.0 U 5.0 U 5.0 U
5.0 U 5.0 U 5.0 U 5.0 U
5.0 U 5.0 U 5.0 U 5.0 U
5.0 U 5.0 U 5.0 U 5.0 U
5.0 U 5.0 U 5.0 U 5.0 U
5.0 U 5.0 U 5.0 U 5.0 U
5.0 U 5.0 U 5.0 U 5.0 U
5.0 U 5.0 U 5.0 U 5.0 U
5.0 U 5.0 U 5.0 U 5.0 U
5.0 U 5.0 U 5.0 U 5.0 U
5.0 U 5.0 U 5.0 U 5.0 U
5.0 U 5.0 U 5.0 U 5.0 U
5.0 U 5.0 U 5.0 U 5.0 U
5.0 U 5.0 U 5.0 U 5.0 U
5.0 U 5.0 U 5.0 U 5.0 U
5.0 U 5.0 U 5.0 U 5.0 U
5.0 U 5.0 U 5.0 U 5.0 U
5.0 UJ 5.0 UJ 5.0 UJ 5.0 UJ
5.0 U 5.0 U 5.0 U 5.0 U
5.0 U 5.0 U 5.0 U 5.0 U
5.0 U 5.0 U 5.0 U 5.0 U
5.0 U 5.0 U 5.0 U 5.0 U
5.0 U 5.0 U 5.0 U 5.0 U
5.0 U 5.0 U 5.0 U 5.0 U
5.0 U 5.0 U 5.0 U 5.0 U
5.0 U 5.0 U 5.0 U 5.0 U
5.0 U 5.0 U 5.0 U 5.0 U
5.0 U 5.0 U 5.0 U 5.0 U
5.0 U 5.0 U 5.0 U 5.0 U
5.0 U 5.0 U 5.0 U 5.0 U
10 U 10 U 10 U 10 U
5.0 U 5.0 U 5.0 U 5.0 U
5.0 U 5.0 U 5.0 U 5.0 U
5.0 U 5.0 U 5.0 U 5.0 U
10 U 10 U 10 U 10 U
4889ASR Number: 06/07/2010
MP7ES02Project ID: Cleburn Street well samplingProject Desc:
RLAB Approved Sample Analysis Results
Page 35 of 43
Analysis/ Analyte
Styrene
1,1,2,2-Tetrachloroethane
Tetrachloroethene
Toluene
1,2,3-Trichlorobenzene
1,2,4-Trichlorobenzene
1,1,1-Trichloroethane
1,1,2-Trichloroethane
Trichloroethene
Trichlorofluoromethane
1,1,2-Trichlorotrifluoroethane
Vinyl Chloride
m and/or p-Xylene
o-Xylene
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
Units 35-__ 36-__ 37-__ 38-__
5.0 U 5.0 U 5.0 U 5.0 U
5.0 U 5.0 U 5.0 U 5.0 U
5.0 U 5.0 U 5.0 U 5.0 U
5.0 U 5.0 U 5.0 U 5.0 U
5.0 U 5.0 U 5.0 U 5.0 U
5.0 U 5.0 U 5.0 U 5.0 U
5.0 U 5.0 U 5.0 U 5.0 U
5.0 U 5.0 U 5.0 U 5.0 U
5.0 U 5.0 U 5.0 U 5.0 U
5.0 U 5.0 U 5.0 U 5.0 U
5.0 U 5.0 U 5.0 U 5.0 U
5.0 U 5.0 U 5.0 U 5.0 U
10 U 10 U 10 U 10 U
5.0 U 5.0 U 5.0 U 5.0 U
4889ASR Number: 06/07/2010
MP7ES02Project ID: Cleburn Street well samplingProject Desc:
RLAB Approved Sample Analysis Results
Page 36 of 43
1
1
1
1
1
Conductivity by Field Measurement
pH of Water by Field Measurement
Temperature of Water by Field Measurement
Turbidity of Water by Field Measurement
VOCs in Water by GC/MS
Analysis/ Analyte
Conductivity
pH
Temperature
Turbidity
Acetone
Benzene
Bromodichloromethane
Bromoform
Bromomethane
2-Butanone
Carbon Disulfide
Carbon Tetrachloride
Chlorobenzene
Chloroethane
Chloroform
Chloromethane
Cyclohexane
1,2-Dibromo-3-Chloropropane
Dibromochloromethane
1,2-Dibromoethane
1,2-Dichlorobenzene
1,3-Dichlorobenzene
1,4-Dichlorobenzene
Dichlorodifluoromethane
1,1-Dichloroethane
1,2-Dichloroethane
1,1-Dichloroethene
cis-1,2-Dichloroethene
trans-1,2-Dichloroethene
1,2-Dichloropropane
cis-1,3-Dichloropropene
trans-1,3-Dichloropropene
Ethyl Benzene
2-Hexanone
Isopropylbenzene
Methyl Acetate
Methyl tert-butyl ether
Methylcyclohexane
Methylene Chloride
4-Methyl-2-Pentanone
Naphthalene
umhos/cm
SU
Deg C
NTU
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
Units 39-__ 40-__ 40-FD 41-__
552 821 821 953
6.98 6.84 6.84 6.87
16.24 16.59 16.59 16.13
33.5 51.7 51.7 0.0
5.0 U 5.0 U 5.0 U 5.0 U
5.0 U 5.0 U 5.0 U 5.0 U
5.0 U 5.0 U 5.0 U 5.0 U
5.0 U 5.0 U 5.0 U 5.0 U
5.0 U 5.0 U 5.0 U 5.0 U
5.0 U 5.0 U 5.0 U 5.0 U
5.0 U 5.0 U 5.0 U 5.0 U
5.0 U 5.0 U 5.0 U 5.0 U
5.0 U 5.0 U 5.0 U 5.0 U
5.0 U 5.0 U 5.0 U 5.0 U
5.0 U 5.0 U 5.0 U 5.0 U
5.0 U 5.0 U 5.0 U 5.0 U
5.0 U 5.0 U 5.0 U 5.0 U
5.0 U 5.0 U 5.0 U 5.0 U
5.0 U 5.0 U 5.0 U 5.0 U
5.0 U 5.0 U 5.0 U 5.0 U
5.0 U 5.0 U 5.0 U 5.0 U
5.0 U 5.0 U 5.0 U 5.0 U
5.0 U 5.0 U 5.0 U 5.0 U
5.0 UJ 5.0 UJ 5.0 UJ 5.0 U
5.0 U 5.0 U 5.0 U 5.0 U
5.0 U 5.0 U 5.0 U 5.0 U
5.0 U 5.0 U 5.0 U 5.0 U
5.0 U 5.0 U 5.0 U 5.0 U
5.0 U 5.0 U 5.0 U 5.0 U
5.0 U 5.0 U 5.0 U 5.0 U
5.0 U 5.0 U 5.0 U 5.0 U
5.0 U 5.0 U 5.0 U 5.0 U
5.0 U 5.0 U 5.0 U 5.0 U
5.0 U 5.0 U 5.0 U 5.0 U
5.0 U 5.0 U 5.0 U 5.0 U
5.0 U 5.0 U 5.0 U 5.0 U
10 U 10 U 10 U 10 UJ
5.0 U 5.0 U 5.0 U 5.0 U
5.0 U 5.0 U 5.0 U 5.0 U
5.0 U 5.0 U 5.0 U 5.0 U
10 U 10 U 10 U 10 U
4889ASR Number: 06/07/2010
MP7ES02Project ID: Cleburn Street well samplingProject Desc:
RLAB Approved Sample Analysis Results
Page 37 of 43
Analysis/ Analyte
Styrene
1,1,2,2-Tetrachloroethane
Tetrachloroethene
Toluene
1,2,3-Trichlorobenzene
1,2,4-Trichlorobenzene
1,1,1-Trichloroethane
1,1,2-Trichloroethane
Trichloroethene
Trichlorofluoromethane
1,1,2-Trichlorotrifluoroethane
Vinyl Chloride
m and/or p-Xylene
o-Xylene
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
Units 39-__ 40-__ 40-FD 41-__
5.0 U 5.0 U 5.0 U 5.0 U
5.0 U 5.0 U 5.0 U 5.0 U
5.0 U 5.0 U 5.0 U 5.0 U
5.0 U 5.0 U 5.0 U 5.0 U
5.0 U 5.0 U 5.0 U 5.0 U
5.0 U 5.0 U 5.0 U 5.0 U
5.0 U 5.0 U 5.0 U 5.0 U
5.0 U 5.0 U 5.0 U 5.0 U
5.0 U 5.0 U 5.0 U 5.0 U
5.0 U 5.0 U 5.0 U 5.0 U
5.0 U 5.0 U 5.0 U 5.0 U
5.0 U 5.0 U 5.0 U 5.0 U
10 U 10 U 10 U 10 U
5.0 U 5.0 U 5.0 U 5.0 U
4889ASR Number: 06/07/2010
MP7ES02Project ID: Cleburn Street well samplingProject Desc:
RLAB Approved Sample Analysis Results
Page 38 of 43
1
1
1
1
1
Conductivity by Field Measurement
pH of Water by Field Measurement
Temperature of Water by Field Measurement
Turbidity of Water by Field Measurement
VOCs in Water by GC/MS
Analysis/ Analyte
Conductivity
pH
Temperature
Turbidity
Acetone
Benzene
Bromodichloromethane
Bromoform
Bromomethane
2-Butanone
Carbon Disulfide
Carbon Tetrachloride
Chlorobenzene
Chloroethane
Chloroform
Chloromethane
Cyclohexane
1,2-Dibromo-3-Chloropropane
Dibromochloromethane
1,2-Dibromoethane
1,2-Dichlorobenzene
1,3-Dichlorobenzene
1,4-Dichlorobenzene
Dichlorodifluoromethane
1,1-Dichloroethane
1,2-Dichloroethane
1,1-Dichloroethene
cis-1,2-Dichloroethene
trans-1,2-Dichloroethene
1,2-Dichloropropane
cis-1,3-Dichloropropene
trans-1,3-Dichloropropene
Ethyl Benzene
2-Hexanone
Isopropylbenzene
Methyl Acetate
Methyl tert-butyl ether
Methylcyclohexane
Methylene Chloride
4-Methyl-2-Pentanone
Naphthalene
umhos/cm
SU
Deg C
NTU
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
Units 42-__ 43-__ 44-__ 45-__
389 772 925 1830
7.44 6.79 7.30 7.03
16.46 16.63 13.76 15.30
1.1 37.9 5.9 0.0
5.0 U 5.0 U 5.0 U 5.0 U
5.0 U 5.0 U 5.0 U 5.0 U
5.0 U 5.0 U 5.0 U 5.0 U
5.0 U 5.0 U 5.0 U 5.0 U
5.0 U 5.0 U 5.0 U 5.0 U
5.0 U 5.0 U 5.0 U 5.0 U
5.0 U 5.0 U 5.0 U 5.0 U
5.0 U 5.0 U 5.0 U 5.0 U
5.0 U 5.0 U 5.0 U 5.0 U
5.0 U 5.0 U 5.0 U 5.0 U
5.0 U 5.0 U 5.0 U 5.0 U
5.0 U 5.0 U 5.0 U 5.0 U
5.0 U 5.0 U 5.0 U 5.0 U
5.0 U 5.0 U 5.0 U 5.0 U
5.0 U 5.0 U 5.0 U 5.0 U
5.0 U 5.0 U 5.0 U 5.0 U
5.0 U 5.0 U 5.0 U 5.0 U
5.0 U 5.0 U 5.0 U 5.0 U
5.0 U 5.0 U 5.0 U 5.0 U
5.0 UJ 5.0 UJ 5.0 UJ 5.0 UJ
5.0 U 5.0 U 5.0 U 5.0 U
5.0 U 5.0 U 5.0 U 5.0 U
5.0 U 5.0 U 5.0 U 5.0 U
5.0 U 5.0 U 5.0 U 5.0 U
5.0 U 5.0 U 5.0 U 5.0 U
5.0 U 5.0 U 5.0 U 5.0 U
5.0 U 5.0 U 5.0 U 5.0 U
5.0 U 5.0 U 5.0 U 5.0 U
5.0 U 5.0 U 5.0 U 5.0 U
5.0 U 5.0 U 5.0 U 5.0 U
5.0 U 5.0 U 5.0 U 5.0 U
5.0 U 5.0 U 5.0 U 5.0 U
10 U 10 U 10 U 10 U
5.0 U 5.0 U 5.0 U 5.0 U
5.0 U 5.0 U 5.0 U 5.0 U
5.0 U 5.0 U 5.0 U 5.0 U
10 U 10 U 10 U 10 U
4889ASR Number: 06/07/2010
MP7ES02Project ID: Cleburn Street well samplingProject Desc:
RLAB Approved Sample Analysis Results
Page 39 of 43
Analysis/ Analyte
Styrene
1,1,2,2-Tetrachloroethane
Tetrachloroethene
Toluene
1,2,3-Trichlorobenzene
1,2,4-Trichlorobenzene
1,1,1-Trichloroethane
1,1,2-Trichloroethane
Trichloroethene
Trichlorofluoromethane
1,1,2-Trichlorotrifluoroethane
Vinyl Chloride
m and/or p-Xylene
o-Xylene
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
Units 42-__ 43-__ 44-__ 45-__
5.0 U 5.0 U 5.0 U 5.0 U
5.0 U 5.0 U 5.0 U 5.0 U
5.0 U 5.0 U 5.0 U 5.0 U
5.0 U 5.0 U 5.0 U 5.0 U
5.0 U 5.0 U 5.0 U 5.0 U
5.0 U 5.0 U 5.0 U 5.0 U
5.0 U 5.0 U 5.0 U 5.0 U
5.0 U 5.0 U 5.0 U 5.0 U
5.0 U 5.0 U 5.0 U 5.0 U
5.0 U 5.0 U 5.0 U 5.0 U
5.0 U 5.0 U 5.0 U 5.0 U
5.0 U 5.0 U 5.0 U 5.0 U
10 U 10 U 10 U 10 U
5.0 U 5.0 U 5.0 U 5.0 U
4889ASR Number: 06/07/2010
MP7ES02Project ID: Cleburn Street well samplingProject Desc:
RLAB Approved Sample Analysis Results
Page 40 of 43
1
1
1
1
1
Conductivity by Field Measurement
pH of Water by Field Measurement
Temperature of Water by Field Measurement
Turbidity of Water by Field Measurement
VOCs in Water by GC/MS
Analysis/ Analyte
Conductivity
pH
Temperature
Turbidity
Acetone
Benzene
Bromodichloromethane
Bromoform
Bromomethane
2-Butanone
Carbon Disulfide
Carbon Tetrachloride
Chlorobenzene
Chloroethane
Chloroform
Chloromethane
Cyclohexane
1,2-Dibromo-3-Chloropropane
Dibromochloromethane
1,2-Dibromoethane
1,2-Dichlorobenzene
1,3-Dichlorobenzene
1,4-Dichlorobenzene
Dichlorodifluoromethane
1,1-Dichloroethane
1,2-Dichloroethane
1,1-Dichloroethene
cis-1,2-Dichloroethene
trans-1,2-Dichloroethene
1,2-Dichloropropane
cis-1,3-Dichloropropene
trans-1,3-Dichloropropene
Ethyl Benzene
2-Hexanone
Isopropylbenzene
Methyl Acetate
Methyl tert-butyl ether
Methylcyclohexane
Methylene Chloride
4-Methyl-2-Pentanone
Naphthalene
umhos/cm
SU
Deg C
NTU
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
Units 46-__ 47-__ 52-FB 53-FB
953 824
6.77 6.75
15.5 14.37
4.0 0.0
5.0 U 5.0 U 5.0 U 5.0 U
5.0 U 5.0 U 5.0 U 5.0 U
5.0 U 5.0 U 5.0 U 5.0 U
5.0 U 5.0 U 5.0 U 5.0 U
5.0 U 5.0 U 5.0 U 5.0 U
5.0 U 5.0 U 5.0 U 5.0 U
5.0 U 5.0 U 5.0 U 5.0 U
5.0 U 5.0 U 5.0 U 5.0 U
5.0 U 5.0 U 5.0 U 5.0 U
5.0 U 5.0 U 5.0 U 5.0 U
5.0 U 5.0 U 5.0 U 5.0 U
5.0 U 5.0 U 5.0 U 5.0 U
5.0 U 5.0 U 5.0 U 5.0 U
5.0 U 5.0 U 5.0 U 5.0 U
5.0 U 5.0 U 5.0 U 5.0 U
5.0 U 5.0 U 5.0 U 5.0 U
5.0 U 5.0 U 5.0 U 5.0 U
5.0 U 5.0 U 5.0 U 5.0 U
5.0 U 5.0 U 5.0 U 5.0 U
5.0 UJ 5.0 UJ 5.0 UJ 5.0 UJ
5.0 U 5.0 U 5.0 U 5.0 U
5.0 U 5.0 U 5.0 U 5.0 U
5.0 U 5.0 U 5.0 U 5.0 U
5.0 U 5.0 U 5.0 U 5.0 U
5.0 U 5.0 U 5.0 U 5.0 U
5.0 U 5.0 U 5.0 U 5.0 U
5.0 U 5.0 U 5.0 U 5.0 U
5.0 U 5.0 U 5.0 U 5.0 U
5.0 U 5.0 U 5.0 U 5.0 U
5.0 U 5.0 U 5.0 U 5.0 U
5.0 U 5.0 U 5.0 U 5.0 U
5.0 U 5.0 U 5.0 U 5.0 U
10 U 10 U 10 U 10 U
5.0 U 5.0 U 5.0 U 5.0 U
5.0 U 5.0 U 5.0 U 5.0 U
5.0 U 5.0 U 5.0 U 5.0 U
10 U 10 U 10 U 10 U
4889ASR Number: 06/07/2010
MP7ES02Project ID: Cleburn Street well samplingProject Desc:
RLAB Approved Sample Analysis Results
Page 41 of 43
Analysis/ Analyte
Styrene
1,1,2,2-Tetrachloroethane
Tetrachloroethene
Toluene
1,2,3-Trichlorobenzene
1,2,4-Trichlorobenzene
1,1,1-Trichloroethane
1,1,2-Trichloroethane
Trichloroethene
Trichlorofluoromethane
1,1,2-Trichlorotrifluoroethane
Vinyl Chloride
m and/or p-Xylene
o-Xylene
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
Units 46-__ 47-__ 52-FB 53-FB
5.0 U 5.0 U 5.0 U 5.0 U
5.0 U 5.0 U 5.0 U 5.0 U
15 5.0 U 5.0 U 5.0 U
5.0 U 5.0 U 5.0 U 5.0 U
5.0 U 5.0 U 5.0 U 5.0 U
5.0 U 5.0 U 5.0 U 5.0 U
5.0 U 5.0 U 5.0 U 5.0 U
5.0 U 5.0 U 5.0 U 5.0 U
5.0 U 5.0 U 5.0 U 5.0 U
5.0 U 5.0 U 5.0 U 5.0 U
5.0 U 5.0 U 5.0 U 5.0 U
5.0 U 5.0 U 5.0 U 5.0 U
10 U 10 U 10 U 10 U
5.0 U 5.0 U 5.0 U 5.0 U
4889ASR Number: 06/07/2010
MP7ES02Project ID: Cleburn Street well samplingProject Desc:
RLAB Approved Sample Analysis Results
Page 42 of 43
1 VOCs in Water by GC/MS
Analysis/ Analyte
Acetone
Benzene
Bromodichloromethane
Bromoform
Bromomethane
2-Butanone
Carbon Disulfide
Carbon Tetrachloride
Chlorobenzene
Chloroethane
Chloroform
Chloromethane
Cyclohexane
1,2-Dibromo-3-Chloropropane
Dibromochloromethane
1,2-Dibromoethane
1,2-Dichlorobenzene
1,3-Dichlorobenzene
1,4-Dichlorobenzene
Dichlorodifluoromethane
1,1-Dichloroethane
1,2-Dichloroethane
1,1-Dichloroethene
cis-1,2-Dichloroethene
trans-1,2-Dichloroethene
1,2-Dichloropropane
cis-1,3-Dichloropropene
trans-1,3-Dichloropropene
Ethyl Benzene
2-Hexanone
Isopropylbenzene
Methyl Acetate
Methyl tert-butyl ether
Methylcyclohexane
Methylene Chloride
4-Methyl-2-Pentanone
Naphthalene
Styrene
1,1,2,2-Tetrachloroethane
Tetrachloroethene
Toluene
1,2,3-Trichlorobenzene
1,2,4-Trichlorobenzene
1,1,1-Trichloroethane
1,1,2-Trichloroethane
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
Units 54-FB
5.0 U
5.0 U
5.0 U
5.0 U
5.0 U
5.0 U
5.0 U
5.0 U
5.0 U
5.0 U
5.0 U
5.0 U
5.0 U
5.0 U
5.0 U
5.0 U
5.0 U
5.0 U
5.0 U
5.0 UJ
5.0 U
5.0 U
5.0 U
5.0 U
5.0 U
5.0 U
5.0 U
5.0 U
5.0 U
5.0 U
5.0 U
5.0 U
10 U
5.0 U
5.0 U
5.0 U
10 U
5.0 U
5.0 U
5.0 U
5.0 U
5.0 U
5.0 U
5.0 U
5.0 U
4889ASR Number: 06/07/2010
MP7ES02Project ID: Cleburn Street well samplingProject Desc:
RLAB Approved Sample Analysis Results
Page 43 of 43
Analysis/ Analyte
Trichloroethene
Trichlorofluoromethane
1,1,2-Trichlorotrifluoroethane
Vinyl Chloride
m and/or p-Xylene
o-Xylene
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
Units 54-FB
5.0 U
5.0 U
5.0 U
5.0 U
10 U
5.0 U
4889ASR Number: 06/07/2010
MP7ES02Project ID: Cleburn Street well samplingProject Desc:
RLAB Approved Sample Analysis Results
4889
MP7ES02Project ID:
Cleburn Street well sampling
Mary PetersonSUPR/IANE
United States Environmental Protection AgencyRegion VII
901 N. 5th StreetKansas City, KS 66101
__/__/____
Data Disposition/Sample Release for ASR #:
Project Description:
Subject:
Kaye DollmannENSV/RLAB
I have received and reviewed the Transmittal of Sample Analysis Results for the above-referencedAnalytical Services Request(ASR) and have indicated my findings below by checking one of theboxes for Data Disposition.
I understand all samples will be disposed upon receipt of this form, unless samples are requestedto be held. If I do not return this form all samples will be disposed of on ___________________.
"RELEASED" - Read-only to all Region 7 employees and contractors that have R7LIMS"Customer" account. All Samples may be disposed of upon receipt of this form if not requested tobe held.
"Project Manager Accessible" - Available on the LAN in R7LIMS for my use only. All Samples maybe disposed of upon receipt of this form if not requested to be held.
"Archived" - THIS DATA IS OF A SENSITIVE NATURE. Any future reports must be requestedthrough the laboratory. All samples may be disposed of upon receipt of the form if not requestedto be held.
Date:
From:
To:
Hold Samples - I have determined that the samples need to be held until ______________, afterwhich time they will be disposed of in accordance with applicable regulations. The reason for the hold is:
Samples are associated with a legal proceeding.
Question/Concern with data - possible reanalysis requested.
Other:________________________________________________________________
JULY 2010
Page 1 of 17
06/07/2010Date:
4890
MP7ES02
Cleburn Street well sampling
Mary PetersonSUPR/IANE
Transmittal of Sample Analysis Results for ASR #:
Project ID:
Project Description:
Michael F. Davis, ChiefChemical Analysis and Response Branch, Environmental Services Division
To:
Enclosed are the analytical data for the above-referenced Analytical Services Request (ASR) andProject. The Regional Laboratory has reviewed and verified the results in accordance with proceduresdescribed in our Quality Manual (QM). In addition to all of the analytical results, this transmittalcontains pertinent information that may have influenced the reported results and documents anydeviations from the established requirements of the QM.
Please contact us within 14 days of receipt of this package if you determine there is a need for anychanges. Please complete the enclosed Customer Satisfaction Survey and Data Disposition/SampleRelease memo for this ASR as soon as possible. The process of disposing of the samples for this ASRwill be initiated 30 days from the date of this transmittal unless an alternate release date is specifiedon the Data Disposition/Sample Release memo.
If you have any questions or concerns relating to this data package, contact our customer service lineat 913-551-5295.
Enclosures
cc: Analytical Data File.
United States Environmental Protection AgencyRegion 7
901 N. 5th StreetKansas City, KS 66101
Subject:
From:
Page 2 of 17
4890ASR Number: 06/07/2010
Mary Peterson SUPR/IANE 913-551-7882
MP7ES02
Cleburn Street well sampling
Grand Island Nebraska Superfund
CLEBURN STREET WELL - 1 HR MARTINIZING GWRESORATION
07ESSite ID: 02
Site Cleanup Support
This EPA research/ascorbic acid ASR is in conjunction with ASR #4889.
VOA samples with permanganate will be preserved with ascorbic acid under this ASR. We are currently developing the protocol to use the new preservative.
Project Manager: Org: Phone:
Project ID:
Project Desc:
Location: State: Program:
Site Name: Site OU:
Purpose:
__ = Field SampleFB = Field BlankFD = Field Duplicate
QC Codes identify the type of sample for quality control purpose.
Degrees CelsiusNephelometric Turbidity UnitsStandard Units (pH)Micrograms per LiterMicromhos per Centimeter
Specific units in which results arereported.
The identification of the analyte is acceptable; the reported value is anestimate.Parameter not analyzed.The analyte was not detected at or above the reporting limit.The analyte was not detected at or above the reporting limit. The reportinglimit is an estimate.
Specific codes used in conjunction with data values to provide additional information on the quality of reported results, or used to explain the absence of a specific value.
Summary of Project Information
Explanation of Codes, Units and Qualifiers used on this report
Sample QC Codes: Units:
J
OU
UJ
=
===
Data Qualifiers:
= Values have been reviewed and found acceptable for use. (Blank)
Deg CNTUSU
ug/Lumhos/cm
=====
2009073QAPP Number:
302DD2CGPRA PRC:
Page 3 of 17
101
102
103
104
104
105
106
107
108
109
110
110
111
112
113
114
115
116
118
124
130
152
SampleNo
__
__
__
__
FD
__
__
__
__
__
__
FD
__
__
__
__
__
__
__
FB
__
FB
QCCode
Water
Water
Water
Water
Water
Water
Water
Water
Water
Water
Water
Water
Water
Water
Water
Water
Water
Water
Water
Water
Water
Water
Matrix
ERT-15
IW-1
IW-2
IW-3
IW-3/Field Duplicate of sample104IW-4
IW-5
IW-6
IW-7
ERT-16
IW-8
IW-8/Field Duplicate of sample110IW-9
IW-10
MW-2A
DPT-3
DPE-1
DPE-2
DPE-4
Preservative Blank sample
MW-102-AA
Trip Blank #1
Location DescriptionExternal
Sample No
05/03/2010
05/04/2010
05/04/2010
05/04/2010
05/04/2010
05/04/2010
05/04/2010
05/04/2010
05/04/2010
05/05/2010
05/05/2010
05/05/2010
05/05/2010
05/05/2010
05/05/2010
05/05/2010
05/05/2010
05/06/2010
05/06/2010
05/04/2010
05/07/2010
04/20/2010
Start Date
17:20
08:55
10:00
10:55
10:55
12:20
13:50
15:50
17:05
10:00
11:05
11:05
12:40
13:50
15:15
16:35
18:20
10:10
12:30
15:25
15:35
Start Time
05/03/2010
End Date
17:15
End Time
05/05/2010
05/05/2010
05/05/2010
05/05/2010
05/05/2010
05/05/2010
05/05/2010
05/05/2010
05/06/2010
05/06/2010
05/06/2010
05/06/2010
05/06/2010
05/06/2010
05/06/2010
05/07/2010
05/07/2010
05/07/2010
05/07/2010
05/05/2010
05/10/2010
05/05/2010
ReceiptDate
4890 06/07/2010
MP7ES02Project ID: Cleburn Street well samplingProject Desc:
ASR Number: Sample Information Summary
-
-
-
-
-
-
-
-
-
-
-
-
-
-
-
-
-
-
-
-
-
-
Page 4 of 17
1
1
1
1
1
Conductivity by Field Measurement
pH of Water by Field Measurement
Temperature of Water by Field Measurement
Turbidity of Water by Field Measurement
VOCs in Water by GC/MS
(Field Measurement)
(Field Measurement)
(Field Measurement)
(Field Measurement)
Region 7 EPA Laboratory - Kansas City, Ks.
Lab:
Lab:
Lab:
Lab:
Lab:
Measurement of field parameter
Measurement of field parameter
Measurement of field parameter
Measurement of field parameter
EPA Region 7 RLAB Method 3230.1F
Method:
Method:
Method:
Method:
Method:
(N/A)
(N/A)
(N/A)
(N/A)
Comments:
Comments:
Comments:
Comments:
101-__ 102-__ 103-__ 104-__ 104-FD 105-__ 106-__107-__ 108-__ 109-__ 110-__ 110-FD 111-__ 112-__113-__ 114-__ 115-__ 116-__ 118-__ 130-__
101-__ 102-__ 103-__ 104-__ 104-FD 105-__ 106-__107-__ 108-__ 109-__ 110-__ 110-FD 111-__ 112-__113-__ 114-__ 115-__ 116-__ 118-__ 130-__
101-__ 102-__ 103-__ 104-__ 104-FD 105-__ 106-__107-__ 108-__ 109-__ 110-__ 110-FD 111-__ 112-__113-__ 114-__ 115-__ 116-__ 118-__ 130-__
101-__ 102-__ 103-__ 104-__ 104-FD 105-__ 106-__107-__ 108-__ 109-__ 110-__ 110-FD 111-__ 112-__113-__ 114-__ 115-__ 116-__ 118-__ 130-__
Samples:
Samples:
Samples:
Samples:
4890ASR Number: 06/07/2010
MP7ES02Project ID: Cleburn Street well samplingProject Desc
RLAB Approved Analysis Comments
Analysis Comments About Results For This Analysis
Page 5 of 17
21 Actual samples were analyzed with this ASR. There was insufficient sample volume torun a 2nd set of spikes, as required by the method. The Matrix Spike and Spike Duplicateanalyzed met criteria, as did the Field Duplicate, indicating data quality was acceptable.
Samples 101 (19hrs past), 102-108 (1 - 5.5hrs past) and 124FB (32hrs past) wereanalyzed past the 14-day holding times, due to instrument issues causing delay. Sample101 had good Spike and Spike Duplicate data, and as other times were close, samples 101-108 were not coded. Sample 124FB has been UJ-coded for all analytes except Acetone,which was J-coded.
Sample 152FB had no data to report, as the sample was lost during 2 failed sample runs,due to instrument malfunction.
All samples, except 124FB, were diluted to reduce interference from precipitate in thesample vials. They have been reported at a dilution of 2X with a raised reporting limit.
Samples 107, 108, 109, 111, and 112 required dilution for Acetone. Samples 108 and 109required dilution for Carbon Tetrachloride. Sample 108 required dilution for Chloroform.Sample 111 required dilution for Tetrachloroethene.
Acid preservation was buffered by the addition of Ascorbic acid. All samples were betweena pH of 2 and 4. The presence of the Ascorbic Acid has been shown to preserve theanalytes in the samples, so no data were coded.
1,2-Dichloropropane (87%, LCL: 89%), 1,2-Dibromoethane (85%, LCL: 87%), and EthylBenzene (89%, LCL: 90%) were UJ-coded in samples 112-116, 118 and 130. Theseanalytes were not found in the samples at or above the reporting limit, however, thereporting limit is an estimate (UJ-coded) due to low recovery of these analytes in thelaboratory control sample. The actual reporting limit for this analyte may be higher thanthe reported value. Sample 124FB was already coded for holding time, so no furthercoding was required for these analytes.
Chloroethane (83%, LCL: 84%), 1,2-Dibromoethane (89%, LCL: 90%) and 1,3-Dichlorobenzene (89%, LCL: 91%) were UJ-coded in sample 101. These analytes were notfound in the sample at or above the reporting limit, however, the reporting limit is anestimate (UJ-coded) due to low recovery of these analytes in the laboratory matrix spikeand/or spike duplicate. The actual reporting limit for these analytes may be higher thanthe reported value.
Comments:
101-__ 102-__ 103-__ 104-__ 104-FD 105-__ 106-__107-__ 108-__ 109-__ 110-__ 110-FD 111-__ 112-__113-__ 114-__ 115-__ 116-__ 118-__ 124-FB 130-__152-FB
Samples:
4890ASR Number: 06/07/2010
MP7ES02Project ID: Cleburn Street well samplingProject Desc
RLAB Approved Analysis Comments
Analysis Comments About Results For This Analysis
Page 6 of 17
1
1
1
1
1
Conductivity by Field Measurement
pH of Water by Field Measurement
Temperature of Water by Field Measurement
Turbidity of Water by Field Measurement
VOCs in Water by GC/MS
Analysis/ Analyte
Conductivity
pH
Temperature
Turbidity
Acetone
Benzene
Bromodichloromethane
Bromoform
Bromomethane
2-Butanone
Carbon Disulfide
Carbon Tetrachloride
Chlorobenzene
Chloroethane
Chloroform
Chloromethane
Cyclohexane
1,2-Dibromo-3-Chloropropane
Dibromochloromethane
1,2-Dibromoethane
1,2-Dichlorobenzene
1,3-Dichlorobenzene
1,4-Dichlorobenzene
Dichlorodifluoromethane
1,1-Dichloroethane
1,2-Dichloroethane
1,1-Dichloroethene
cis-1,2-Dichloroethene
trans-1,2-Dichloroethene
1,2-Dichloropropane
cis-1,3-Dichloropropene
trans-1,3-Dichloropropene
Ethyl Benzene
2-Hexanone
Isopropylbenzene
Methyl Acetate
Methyl tert-butyl ether
Methylcyclohexane
Methylene Chloride
4-Methyl-2-Pentanone
Naphthalene
umhos/cm
SU
Deg C
NTU
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
Units 101-__ 102-__ 103-__ 104-__
894 6990 6750 8100
6.78 7.52 7.32 7.55
15.81 14.52 14.55 14.68
0.0 5.2 2.0 3.6
16 230 300 210
10 U 10 U 10 U 10 U
10 U 10 U 10 U 10 U
10 U 10 U 10 U 10 U
10 U 10 U 10 U 10 U
10 U 10 U 10 U 22
10 U 10 U 10 U 10 U
10 U 10 U 10 U 10 U
10 U 10 U 10 U 10 U
10 UJ 10 U 10 U 10 U
10 U 10 U 10 U 10 U
10 U 10 U 10 U 10 U
10 U 10 U 10 U 10 U
10 U 10 U 10 U 10 U
10 U 10 U 10 U 10 U
10 UJ 10 U 10 U 10 U
10 U 10 U 10 U 10 U
10 UJ 10 U 10 U 10 U
10 U 10 U 10 U 10 U
10 U 10 U 10 U 10 U
10 U 10 U 10 U 10 U
10 U 10 U 10 U 10 U
10 U 10 U 10 U 10 U
10 U 10 U 10 U 10 U
10 U 10 U 10 U 10 U
10 U 10 U 10 U 10 U
10 U 10 U 10 U 10 U
10 U 10 U 10 U 10 U
10 U 10 U 10 U 10 U
10 U 10 U 10 U 10 U
10 U 10 U 10 U 10 U
10 U 10 U 10 U 10 U
20 U 20 U 20 U 20 U
10 U 10 U 10 U 10 U
10 U 10 U 10 U 10 U
10 U 10 U 10 U 10 U
20 U 20 U 20 U 20 U
4890ASR Number: 06/07/2010
MP7ES02Project ID: Cleburn Street well samplingProject Desc:
RLAB Approved Sample Analysis Results
Page 7 of 17
Analysis/ Analyte
Styrene
1,1,2,2-Tetrachloroethane
Tetrachloroethene
Toluene
1,2,3-Trichlorobenzene
1,2,4-Trichlorobenzene
1,1,1-Trichloroethane
1,1,2-Trichloroethane
Trichloroethene
Trichlorofluoromethane
1,1,2-Trichlorotrifluoroethane
Vinyl Chloride
m and/or p-Xylene
o-Xylene
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
Units 101-__ 102-__ 103-__ 104-__
10 U 10 U 10 U 10 U
10 U 10 U 10 U 10 U
10 U 10 U 10 U 10 U
10 U 10 U 10 U 10 U
10 U 10 U 10 U 10 U
10 U 10 U 10 U 10 U
10 U 10 U 10 U 10 U
10 U 10 U 10 U 10 U
10 U 10 U 10 U 10 U
10 U 10 U 10 U 10 U
10 U 10 U 10 U 10 U
10 U 10 U 10 U 10 U
20 U 20 U 20 U 20 U
10 U 10 U 10 U 10 U
4890ASR Number: 06/07/2010
MP7ES02Project ID: Cleburn Street well samplingProject Desc:
RLAB Approved Sample Analysis Results
Page 8 of 17
1
1
1
1
1
Conductivity by Field Measurement
pH of Water by Field Measurement
Temperature of Water by Field Measurement
Turbidity of Water by Field Measurement
VOCs in Water by GC/MS
Analysis/ Analyte
Conductivity
pH
Temperature
Turbidity
Acetone
Benzene
Bromodichloromethane
Bromoform
Bromomethane
2-Butanone
Carbon Disulfide
Carbon Tetrachloride
Chlorobenzene
Chloroethane
Chloroform
Chloromethane
Cyclohexane
1,2-Dibromo-3-Chloropropane
Dibromochloromethane
1,2-Dibromoethane
1,2-Dichlorobenzene
1,3-Dichlorobenzene
1,4-Dichlorobenzene
Dichlorodifluoromethane
1,1-Dichloroethane
1,2-Dichloroethane
1,1-Dichloroethene
cis-1,2-Dichloroethene
trans-1,2-Dichloroethene
1,2-Dichloropropane
cis-1,3-Dichloropropene
trans-1,3-Dichloropropene
Ethyl Benzene
2-Hexanone
Isopropylbenzene
Methyl Acetate
Methyl tert-butyl ether
Methylcyclohexane
Methylene Chloride
4-Methyl-2-Pentanone
Naphthalene
umhos/cm
SU
Deg C
NTU
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
Units 104-FD 105-__ 106-__ 107-__
8100 9210 8270 7680
7.55 6.57 6.03 5.67
14.68 4.60 14.23 21.05
3.6 1.6 2.2 3.1
200 230 100 850
10 U 10 U 10 U 10 U
10 U 10 U 10 U 10.
10 U 10 U 10 U 10 U
10 U 10 U 10 U 10 U
22 10 U 10 U 24
10 U 10 U 10 U 10 U
10 U 110 83 160
10 U 10 U 10 U 10 U
10 U 10 U 10 U 10 U
10 U 10 U 54 170
10 U 10 U 10 U 10 U
10 U 10 U 10 U 10 U
10 U 10 U 10 U 10 U
10 U 10 U 10 U 10 U
10 U 10 U 10 U 10 U
10 U 10 U 10 U 10 U
10 U 10 U 10 U 10 U
10 U 10 U 10 U 10 U
10 U 10 U 10 U 10 U
10 U 10 U 10 U 10 U
10 U 10 U 10 U 10 U
10 U 10 U 10 U 10 U
10 U 10 U 10 U 10 U
10 U 10 U 10 U 10 U
10 U 10 U 10 U 10 U
10 U 10 U 10 U 10 U
10 U 10 U 10 U 10 U
10 U 10 U 10 U 10 U
10 U 10 U 10 U 10 U
10 U 10 U 10 U 10 U
10 U 10 U 10 U 10 U
20 U 20 U 20 U 20 U
10 U 10 U 10 U 10 U
10 U 10 U 10 U 10 U
10 U 10 U 10 U 10 U
20 U 20 U 20 U 20 U
4890ASR Number: 06/07/2010
MP7ES02Project ID: Cleburn Street well samplingProject Desc:
RLAB Approved Sample Analysis Results
Page 9 of 17
Analysis/ Analyte
Styrene
1,1,2,2-Tetrachloroethane
Tetrachloroethene
Toluene
1,2,3-Trichlorobenzene
1,2,4-Trichlorobenzene
1,1,1-Trichloroethane
1,1,2-Trichloroethane
Trichloroethene
Trichlorofluoromethane
1,1,2-Trichlorotrifluoroethane
Vinyl Chloride
m and/or p-Xylene
o-Xylene
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
Units 104-FD 105-__ 106-__ 107-__
10 U 10 U 10 U 10 U
10 U 10 U 10 U 10 U
10 U 10 U 370 10 U
10 U 10 U 10 U 10 U
10 U 10 U 10 U 10 U
10 U 10 U 10 U 10 U
10 U 10 U 10 U 13
10 U 10 U 10 U 10 U
10 U 10 U 10 U 10 U
10 U 10 U 10 U 10 U
10 U 10 U 10 U 10 U
10 U 10 U 10 U 10 U
20 U 20 U 20 U 20 U
10 U 10 U 10 U 10 U
4890ASR Number: 06/07/2010
MP7ES02Project ID: Cleburn Street well samplingProject Desc:
RLAB Approved Sample Analysis Results
Page 10 of 17
1
1
1
1
1
Conductivity by Field Measurement
pH of Water by Field Measurement
Temperature of Water by Field Measurement
Turbidity of Water by Field Measurement
VOCs in Water by GC/MS
Analysis/ Analyte
Conductivity
pH
Temperature
Turbidity
Acetone
Benzene
Bromodichloromethane
Bromoform
Bromomethane
2-Butanone
Carbon Disulfide
Carbon Tetrachloride
Chlorobenzene
Chloroethane
Chloroform
Chloromethane
Cyclohexane
1,2-Dibromo-3-Chloropropane
Dibromochloromethane
1,2-Dibromoethane
1,2-Dichlorobenzene
1,3-Dichlorobenzene
1,4-Dichlorobenzene
Dichlorodifluoromethane
1,1-Dichloroethane
1,2-Dichloroethane
1,1-Dichloroethene
cis-1,2-Dichloroethene
trans-1,2-Dichloroethene
1,2-Dichloropropane
cis-1,3-Dichloropropene
trans-1,3-Dichloropropene
Ethyl Benzene
2-Hexanone
Isopropylbenzene
Methyl Acetate
Methyl tert-butyl ether
Methylcyclohexane
Methylene Chloride
4-Methyl-2-Pentanone
Naphthalene
umhos/cm
SU
Deg C
NTU
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
Units 108-__ 109-__ 110-__ 110-FD
10400 8810 5960 5960
2.45 609 6.82 6.82
17.81 21.84 15.66 15.66
134 17.3 0.0 0.0
580 510 270 290
10 U 10 U 10 U 10 U
15 10 U 10 U 10 U
10 U 10 U 10 U 10 U
10 U 10 U 10 U 10 U
31 10 U 16 16
10 U 10 U 10 U 10 U
610 380 69 69
10 U 10 U 10 U 10 U
10 U 10 U 10 U 10 U
390 200 14 15
10 U 10 U 10 U 10 U
10 U 10 U 10 U 10 U
10 U 10 U 10 U 10 U
10 U 10 U 10 U 10 U
10 U 10 U 10 U 10 U
10 U 10 U 10 U 10 U
10 U 10 U 10 U 10 U
10 U 10 U 10 U 10 U
10 U 10 U 10 U 10 U
10 U 10 U 10 U 10 U
10 U 10 U 10 U 10 U
10 U 10 U 10 U 10 U
10 U 10 U 10 U 10 U
10 U 10 U 10 U 10 U
10 U 10 U 10 U 10 U
10 U 10 U 10 U 10 U
10 U 10 U 10 U 10 U
10 U 10 U 10 U 10 U
10 U 10 U 10 U 10 U
10 U 10 U 10 U 10 U
10 U 10 U 10 U 10 U
20 U 20 U 20 U 20 U
10 U 10 U 10 U 10 U
10 U 10 U 10 U 10 U
10 U 10 U 10 U 10 U
20 U 20 U 20 U 20 U
4890ASR Number: 06/07/2010
MP7ES02Project ID: Cleburn Street well samplingProject Desc:
RLAB Approved Sample Analysis Results
Page 11 of 17
Analysis/ Analyte
Styrene
1,1,2,2-Tetrachloroethane
Tetrachloroethene
Toluene
1,2,3-Trichlorobenzene
1,2,4-Trichlorobenzene
1,1,1-Trichloroethane
1,1,2-Trichloroethane
Trichloroethene
Trichlorofluoromethane
1,1,2-Trichlorotrifluoroethane
Vinyl Chloride
m and/or p-Xylene
o-Xylene
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
Units 108-__ 109-__ 110-__ 110-FD
10 U 10 U 10 U 10 U
10 U 10 U 10 U 10 U
17 34 10. 10 U
10 U 10 U 10 U 10 U
10 U 10 U 10 U 10 U
10 U 10 U 10 U 10 U
35 12 10 U 10 U
10 U 10 U 10 U 10 U
10 U 10 U 10 U 10 U
10 U 10 U 10 U 10 U
10 U 10 U 10 U 10 U
10 U 10 U 10 U 10 U
20 U 20 U 20 U 20 U
10 U 10 U 10 U 10 U
4890ASR Number: 06/07/2010
MP7ES02Project ID: Cleburn Street well samplingProject Desc:
RLAB Approved Sample Analysis Results
Page 12 of 17
1
1
1
1
1
Conductivity by Field Measurement
pH of Water by Field Measurement
Temperature of Water by Field Measurement
Turbidity of Water by Field Measurement
VOCs in Water by GC/MS
Analysis/ Analyte
Conductivity
pH
Temperature
Turbidity
Acetone
Benzene
Bromodichloromethane
Bromoform
Bromomethane
2-Butanone
Carbon Disulfide
Carbon Tetrachloride
Chlorobenzene
Chloroethane
Chloroform
Chloromethane
Cyclohexane
1,2-Dibromo-3-Chloropropane
Dibromochloromethane
1,2-Dibromoethane
1,2-Dichlorobenzene
1,3-Dichlorobenzene
1,4-Dichlorobenzene
Dichlorodifluoromethane
1,1-Dichloroethane
1,2-Dichloroethane
1,1-Dichloroethene
cis-1,2-Dichloroethene
trans-1,2-Dichloroethene
1,2-Dichloropropane
cis-1,3-Dichloropropene
trans-1,3-Dichloropropene
Ethyl Benzene
2-Hexanone
Isopropylbenzene
Methyl Acetate
Methyl tert-butyl ether
Methylcyclohexane
Methylene Chloride
4-Methyl-2-Pentanone
Naphthalene
umhos/cm
SU
Deg C
NTU
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
Units 111-__ 112-__ 113-__ 114-__
10,000 9020 3910 7890
5.88 6.67 6.77 2.80
16.55 15.09 14.65 15.14
39.5 0.1 11.9 41.1
790 600 330 230
10 U 10 U 10 U 10 U
12 10 U 10 U 10 U
10 U 10 U 10 U 10 U
10 U 10 U 10 U 10 U
28 10 U 10 U 10 U
10 U 10 U 10 U 10 U
210 94 33 98
10 U 10 U 10 U 10 U
10 U 10 U 10 U 10 U
240 130 26 100
10 U 10 U 10 U 10 U
10 U 10 U 10 U 10 U
10 U 10 U 10 U 10 U
10 U 10 U 10 U 10 U
10 U 10 UJ 10 UJ 10 UJ
20 10 U 10 U 10 U
10 U 10 U 10 U 10 U
10 U 10 U 10 U 10 U
10 U 10 U 10 U 10 U
10 U 10 U 10 U 10 U
10 U 10 U 10 U 10 U
10 U 10 U 10 U 10 U
10 U 10 U 10 U 10 U
10 U 10 U 10 U 10 U
10 U 10 UJ 10 UJ 10 UJ
10 U 10 U 10 U 10 U
10 U 10 U 10 U 10 U
10 U 10 UJ 10 UJ 10 UJ
10 U 10 U 10 U 10 U
10 U 10 U 10 U 10 U
10 U 10 U 10 U 10 U
20 U 20 U 20 U 20 U
10 U 10 U 10 U 10 U
10 U 10 U 10 U 10 U
10 U 10 U 10 U 10 U
20 U 20 U 20 U 20 U
4890ASR Number: 06/07/2010
MP7ES02Project ID: Cleburn Street well samplingProject Desc:
RLAB Approved Sample Analysis Results
Page 13 of 17
Analysis/ Analyte
Styrene
1,1,2,2-Tetrachloroethane
Tetrachloroethene
Toluene
1,2,3-Trichlorobenzene
1,2,4-Trichlorobenzene
1,1,1-Trichloroethane
1,1,2-Trichloroethane
Trichloroethene
Trichlorofluoromethane
1,1,2-Trichlorotrifluoroethane
Vinyl Chloride
m and/or p-Xylene
o-Xylene
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
Units 111-__ 112-__ 113-__ 114-__
10 U 10 U 10 U 10 U
10 U 10 U 10 U 10 U
600 10 U 10 U 10 U
10 U 10 U 10 U 10 U
10 U 10 U 10 U 10 U
10 U 10 U 10 U 10 U
35 20 42 24
10 U 10 U 10 U 10 U
10 U 10 U 10 U 10 U
10 U 10 U 10 U 10 U
10 U 10 U 10 U 10 U
10 U 10 U 10 U 10 U
20 U 20 U 20 U 20 U
10 U 10 U 10 U 10 U
4890ASR Number: 06/07/2010
MP7ES02Project ID: Cleburn Street well samplingProject Desc:
RLAB Approved Sample Analysis Results
Page 14 of 17
1
1
1
1
1
Conductivity by Field Measurement
pH of Water by Field Measurement
Temperature of Water by Field Measurement
Turbidity of Water by Field Measurement
VOCs in Water by GC/MS
Analysis/ Analyte
Conductivity
pH
Temperature
Turbidity
Acetone
Benzene
Bromodichloromethane
Bromoform
Bromomethane
2-Butanone
Carbon Disulfide
Carbon Tetrachloride
Chlorobenzene
Chloroethane
Chloroform
Chloromethane
Cyclohexane
1,2-Dibromo-3-Chloropropane
Dibromochloromethane
1,2-Dibromoethane
1,2-Dichlorobenzene
1,3-Dichlorobenzene
1,4-Dichlorobenzene
Dichlorodifluoromethane
1,1-Dichloroethane
1,2-Dichloroethane
1,1-Dichloroethene
cis-1,2-Dichloroethene
trans-1,2-Dichloroethene
1,2-Dichloropropane
cis-1,3-Dichloropropene
trans-1,3-Dichloropropene
Ethyl Benzene
2-Hexanone
Isopropylbenzene
Methyl Acetate
Methyl tert-butyl ether
Methylcyclohexane
Methylene Chloride
4-Methyl-2-Pentanone
Naphthalene
umhos/cm
SU
Deg C
NTU
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
Units 115-__ 116-__ 118-__ 124-FB
7090 5110 7020
6.94 8.17 9.17
15.62 14.22 13.96
113 13.5 22.4
260 47 42 6.2 J
10 U 10 U 10 U 5.0 UJ
10 U 10 U 10 U 5.0 UJ
10 U 10 U 10 U 5.0 UJ
10 U 10 U 10 U 5.0 UJ
10 U 10 U 10 U 5.0 UJ
10 U 10 U 10 U 5.0 UJ
140 10 U 240 5.0 UJ
10 U 10 U 10 U 5.0 UJ
10 U 10 U 10 U 5.0 UJ
260 10 U 26 5.0 UJ
10 U 10 U 10 U 5.0 UJ
10 U 10 U 10 U 5.0 UJ
10 U 10 U 10 U 5.0 UJ
10 U 10 U 10 U 5.0 UJ
10 UJ 10 UJ 10 UJ 5.0 UJ
10 U 10 U 10 U 5.0 UJ
10 U 10 U 10 U 5.0 UJ
10 U 10 U 10 U 5.0 UJ
10 U 10 U 10 U 5.0 UJ
10 U 10 U 10 U 5.0 UJ
10 U 10 U 10 U 5.0 UJ
10 U 10 U 10 U 5.0 UJ
10 U 10 U 10 U 5.0 UJ
10 U 10 U 10 U 5.0 UJ
10 UJ 10 UJ 10 UJ 5.0 UJ
10 U 10 U 10 U 5.0 UJ
10 U 10 U 10 U 5.0 UJ
10 UJ 10 UJ 10 UJ 5.0 UJ
10 U 10 U 10 U 5.0 UJ
10 U 10 U 10 U 5.0 UJ
10 U 10 U 10 U 5.0 UJ
20 U 20 U 20 U 10 UJ
10 U 10 U 10 U 5.0 UJ
10 U 10 U 10 U 5.0 UJ
10 U 10 U 10 U 5.0 UJ
20 U 20 U 20 U 10 UJ
4890ASR Number: 06/07/2010
MP7ES02Project ID: Cleburn Street well samplingProject Desc:
RLAB Approved Sample Analysis Results
Page 15 of 17
Analysis/ Analyte
Styrene
1,1,2,2-Tetrachloroethane
Tetrachloroethene
Toluene
1,2,3-Trichlorobenzene
1,2,4-Trichlorobenzene
1,1,1-Trichloroethane
1,1,2-Trichloroethane
Trichloroethene
Trichlorofluoromethane
1,1,2-Trichlorotrifluoroethane
Vinyl Chloride
m and/or p-Xylene
o-Xylene
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
Units 115-__ 116-__ 118-__ 124-FB
10 U 10 U 10 U 5.0 UJ
10 U 10 U 10 U 5.0 UJ
10 U 10 U 10 U 5.0 UJ
10 U 10 U 10 U 5.0 UJ
10 U 10 U 10 U 5.0 UJ
10 U 10 U 10 U 5.0 UJ
10 U 10 U 11 5.0 UJ
10 U 10 U 10 U 5.0 UJ
10 U 10 U 10 U 5.0 UJ
10 U 10 U 10 U 5.0 UJ
10 U 10 U 10 U 5.0 UJ
10 U 10 U 10 U 5.0 UJ
20 U 20 U 20 U 10 UJ
10 U 10 U 10 U 5.0 UJ
4890ASR Number: 06/07/2010
MP7ES02Project ID: Cleburn Street well samplingProject Desc:
RLAB Approved Sample Analysis Results
Page 16 of 17
1
1
1
1
1
Conductivity by Field Measurement
pH of Water by Field Measurement
Temperature of Water by Field Measurement
Turbidity of Water by Field Measurement
VOCs in Water by GC/MS
Analysis/ Analyte
Conductivity
pH
Temperature
Turbidity
Acetone
Benzene
Bromodichloromethane
Bromoform
Bromomethane
2-Butanone
Carbon Disulfide
Carbon Tetrachloride
Chlorobenzene
Chloroethane
Chloroform
Chloromethane
Cyclohexane
1,2-Dibromo-3-Chloropropane
Dibromochloromethane
1,2-Dibromoethane
1,2-Dichlorobenzene
1,3-Dichlorobenzene
1,4-Dichlorobenzene
Dichlorodifluoromethane
1,1-Dichloroethane
1,2-Dichloroethane
1,1-Dichloroethene
cis-1,2-Dichloroethene
trans-1,2-Dichloroethene
1,2-Dichloropropane
cis-1,3-Dichloropropene
trans-1,3-Dichloropropene
Ethyl Benzene
2-Hexanone
Isopropylbenzene
Methyl Acetate
Methyl tert-butyl ether
Methylcyclohexane
Methylene Chloride
4-Methyl-2-Pentanone
Naphthalene
umhos/cm
SU
Deg C
NTU
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
Units 130-__ 152-FB
2380
7.00
16.03
0.0
45 N/A O
10 U N/A O
10 U N/A O
10 U N/A O
10 U N/A O
10 U N/A O
10 U N/A O
10 U N/A O
10 U N/A O
10 U N/A O
10 U N/A O
10 U N/A O
10 U N/A O
10 U N/A O
10 U N/A O
10 UJ N/A O
10 U N/A O
10 U N/A O
10 U N/A O
10 U N/A O
10 U N/A O
10 U N/A O
10 U N/A O
10 U N/A O
10 U N/A O
10 UJ N/A O
10 U N/A O
10 U N/A O
10 UJ N/A O
10 U N/A O
10 U N/A O
10 U N/A O
20 U N/A O
10 U N/A O
10 U N/A O
10 U N/A O
20 U N/A O
4890ASR Number: 06/07/2010
MP7ES02Project ID: Cleburn Street well samplingProject Desc:
RLAB Approved Sample Analysis Results
Page 17 of 17
Analysis/ Analyte
Styrene
1,1,2,2-Tetrachloroethane
Tetrachloroethene
Toluene
1,2,3-Trichlorobenzene
1,2,4-Trichlorobenzene
1,1,1-Trichloroethane
1,1,2-Trichloroethane
Trichloroethene
Trichlorofluoromethane
1,1,2-Trichlorotrifluoroethane
Vinyl Chloride
m and/or p-Xylene
o-Xylene
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
Units 130-__ 152-FB
10 U N/A O
10 U N/A O
10 U N/A O
10 U N/A O
10 U N/A O
10 U N/A O
10 U N/A O
10 U N/A O
10 U N/A O
10 U N/A O
10 U N/A O
10 U N/A O
20 U N/A O
10 U N/A O
4890ASR Number: 06/07/2010
MP7ES02Project ID: Cleburn Street well samplingProject Desc:
RLAB Approved Sample Analysis Results
4890
MP7ES02Project ID:
Cleburn Street well sampling
Mary PetersonSUPR/IANE
United States Environmental Protection AgencyRegion VII
901 N. 5th StreetKansas City, KS 66101
__/__/____
Data Disposition/Sample Release for ASR #:
Project Description:
Subject:
Kaye DollmannENSV/RLAB
I have received and reviewed the Transmittal of Sample Analysis Results for the above-referencedAnalytical Services Request(ASR) and have indicated my findings below by checking one of theboxes for Data Disposition.
I understand all samples will be disposed upon receipt of this form, unless samples are requestedto be held. If I do not return this form all samples will be disposed of on ___________________.
"RELEASED" - Read-only to all Region 7 employees and contractors that have R7LIMS"Customer" account. All Samples may be disposed of upon receipt of this form if not requested tobe held.
"Project Manager Accessible" - Available on the LAN in R7LIMS for my use only. All Samples maybe disposed of upon receipt of this form if not requested to be held.
"Archived" - THIS DATA IS OF A SENSITIVE NATURE. Any future reports must be requestedthrough the laboratory. All samples may be disposed of upon receipt of the form if not requestedto be held.
Date:
From:
To:
Hold Samples - I have determined that the samples need to be held until ______________, afterwhich time they will be disposed of in accordance with applicable regulations. The reason for the hold is:
Samples are associated with a legal proceeding.
Question/Concern with data - possible reanalysis requested.
Other:________________________________________________________________
JULY 2010
Page 1 of 36
09/16/2010Date:
4981
MP7ES02
Cleburn Street well sampling
Mary PetersonSUPR/IANE
Transmittal of Sample Analysis Results for ASR #:
Project ID:
Project Description:
Michael F. Davis, ChiefChemical Analysis and Response Branch, Environmental Services Division
To:
Enclosed are the analytical data for the above-referenced Analytical Services Request (ASR) andProject. The Regional Laboratory has reviewed and verified the results in accordance with proceduresdescribed in our Quality Manual (QM). In addition to all of the analytical results, this transmittalcontains pertinent information that may have influenced the reported results and documents anydeviations from the established requirements of the QM.
Please contact us within 14 days of receipt of this package if you determine there is a need for anychanges. Please complete the enclosed Customer Satisfaction Survey and Data Disposition/SampleRelease memo for this ASR as soon as possible. The process of disposing of the samples for this ASRwill be initiated 30 days from the date of this transmittal unless an alternate release date is specifiedon the Data Disposition/Sample Release memo.
If you have any questions or concerns relating to this data package, contact our customer service lineat 913-551-5295.
Enclosures
cc: Analytical Data File.
United States Environmental Protection AgencyRegion 7
901 N. 5th StreetKansas City, KS 66101
Subject:
From:
Page 2 of 36
4981ASR Number: 09/16/2010
Mary Peterson SUPR/IANE 913-551-7882
MP7ES02
Cleburn Street well sampling
Grand Island Nebraska Superfund
CLEBURN STREET WELL - 1 HR MARTINIZING GWRESORATION
07ESSite ID: 02
Site Cleanup Support
Quarterly and Post Injection monitoring sampling.
Project Manager: Org: Phone:
Project ID:
Project Desc:
Location: State: Program:
Site Name: Site OU:
Purpose:
__ = Field SampleFB = Field BlankFD = Field Duplicate
QC Codes identify the type of sample for quality control purpose.
Milligrams per LiterMicrograms per Liter
Specific units in which results arereported.
The identification of the analyte is acceptable; the reported value is anestimate.The analyte was not detected at or above the reporting limit.The analyte was not detected at or above the reporting limit. The reportinglimit is an estimate.
Specific codes used in conjunction with data values to provide additional information on the quality of reported results, or used to explain the absence of a specific value.
Summary of Project Information
Explanation of Codes, Units and Qualifiers used on this report
Sample QC Codes: Units:
J
UUJ
=
==
Data Qualifiers:
= Values have been reviewed and found acceptable for use. (Blank)
mg/Lug/L
==
2009073QAPP Number:
302DD2CGPRA PRC:
Page 3 of 36
1
2
3
4
4
5
6
7
8
9
10
10
11
12
13
14
15
16
17
18
19
22
22
24
25
26
27
28
29
30
31
32
32
34
35
35
37
38
39
40
41
42
43
SampleNo
__
__
__
__
FD
__
__
__
__
__
__
FD
__
__
__
__
__
__
__
__
__
__
FD
FB
__
__
__
__
__
__
__
__
FD
__
__
FD
__
__
__
__
__
__
__
QCCode
Water
Water
Water
Water
Water
Water
Water
Water
Water
Water
Water
Water
Water
Water
Water
Water
Water
Water
Water
Water
Water
Water
Water
Water
Water
Water
Water
Water
Water
Water
Water
Water
Water
Water
Water
Water
Water
Water
Water
Water
Water
Water
Water
Matrix
ERT-14
ERT-15
IW-2
IW-1
IW-1/Field Duplicate of sample 4
IW-4
IW-5
IW-6
IW-7
IW-9
IW-3
IW-3/Field Duplicate of sample 10
IW-10
ERT-16
DPE-1
DPE-2
DPE-3
DPE-4
MW-2A
MW-2B
MW-12A
IW-8
IW-8/Field Duplicate of sample 22
Preservative Blank
MW-13A
MW-102-AA
MW-102-BB
Cleburn Street well
MW-107-BB
MW-107-BB
MW-11-A
MW-108-BB
MW-108-BB/Field Duplicate ofsample 32MW-11-B
MW-8B
MW-8B/Field Duplicate of sample35MW-8A
MW-105-BB
MW-10A
MW-10B
MW-103-CC
MW-103-BB
MW-103-AA
Location DescriptionExternal
Sample No
07/26/2010
07/26/2010
07/27/2010
07/27/2010
07/27/2010
07/27/2010
07/27/2010
07/27/2010
07/27/2010
07/28/2010
07/27/2010
07/27/2010
07/28/2010
07/28/2010
07/28/2010
07/29/2010
07/29/2010
07/29/2010
07/29/2010
07/29/2010
07/29/2010
07/28/2010
07/28/2010
07/26/2010
07/30/2010
07/30/2010
07/30/2010
07/30/2010
07/30/2010
07/30/2010
07/30/2010
07/30/2010
07/30/2010
07/30/2010
07/31/2010
07/31/2010
07/31/2010
07/31/2010
07/31/2010
07/31/2010
08/01/2010
08/01/2010
08/01/2010
Start Date
14:45
16:25
10:40
09:20
09:20
13:00
14:25
15:25
18:35
12:45
11:40
11:40
14:40
16:20
17:55
09:10
10:35
12:00
13:45
14:40
15:30
10:15
10:15
12:05
08:40
10:15
11:05
13:00
13:30
14:05
15:00
15:50
15:50
16:50
13:45
13:45
14:30
15:20
16:45
17:45
09:30
10:15
10:50
Start Time
End Date
End Time
07/27/2010
07/27/2010
07/28/2010
07/28/2010
07/28/2010
07/28/2010
07/28/2010
07/28/2010
07/29/2010
07/29/2010
07/28/2010
07/28/2010
07/29/2010
07/29/2010
07/30/2010
07/30/2010
07/30/2010
07/30/2010
07/30/2010
07/30/2010
07/30/2010
07/29/2010
07/29/2010
07/27/2010
08/03/2010
08/03/2010
08/03/2010
08/03/2010
08/03/2010
08/03/2010
08/03/2010
08/03/2010
08/03/2010
08/03/2010
08/03/2010
08/03/2010
08/03/2010
08/03/2010
08/03/2010
08/03/2010
08/03/2010
08/03/2010
08/03/2010
ReceiptDate
4981 09/16/2010
MP7ES02Project ID: Cleburn Street well samplingProject Desc:
ASR Number: Sample Information Summary
-
-
-
-
-
-
-
-
-
-
-
-
-
-
-
-
-
-
-
-
-
-
-
-
-
-
-
-
-
-
-
-
-
-
-
-
-
-
-
-
-
-
-
Page 4 of 36
44
45
45
47
48
49
50
53
54
55
SampleNo
__
__
FD
__
__
__
__
FB
FB
FB
QCCode
Water
Water
Water
Water
Water
Water
Water
Water
Water
Water
Matrix
MW-101-AA
MW-106-CC
MW-106-CC/Field Duplicate ofsample 45MW-106-BB
MW-9A
MW-104-AA
MW-104-BB
VOA Trip Blank sample 1
VOA Trip Blank sample 2
VOA Trip Blank sample 3
Location DescriptionExternal
Sample No
08/01/2010
08/01/2010
08/01/2010
08/01/2010
08/01/2010
08/02/2010
08/02/2010
07/21/2010
07/21/2010
07/21/2010
Start Date
11:40
15:20
15:20
16:30
17:40
09:05
09:50
16:04
16:03
16:03
Start Time
07/26/2010
07/27/2010
07/28/2010
End Date
11:30
09:30
08:30
End Time
08/03/2010
08/03/2010
08/03/2010
08/03/2010
08/03/2010
08/03/2010
08/03/2010
07/27/2010
07/28/2010
07/29/2010
ReceiptDate
4981 09/16/2010
MP7ES02Project ID: Cleburn Street well samplingProject Desc:
ASR Number: Sample Information Summary
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-
-
-
-
-
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Page 5 of 36
1
1
1
1
Alkalinity in Water by Titration
Anions in Water by Ion Chromatography
Hardness in Water by Calculation
Metals in Water by ICP-AES
Region 7 ESAT Contract Lab (In-House)
Region 7 ESAT Contract Lab (In-House)
Region 7 ESAT Contract Lab (In-House)
Region 7 ESAT Contract Lab (In-House)
Lab:
Lab:
Lab:
Lab:
EPA Region 7 RLAB Method 3132.1E
Region 7 RLAB Method 3135.12A
EPA Region 7 RLAB Method 3122.3D
EPA Region 7 RLAB Method 3122.3D
Method:
Method:
Method:
Method:
(N/A)
Dilutions were necessary in order to obtain valid results due to matrix interferences forsamples 3, 4, 4 FD, 5, 6, 7, 8, 9, 10, 10 FD, 11, 12, 13, 14, 15, 16, 17, 22, 22 FD . Thisincreased the reporting limits by a factor of 10000 for these samples.
Sulfate (131, 80-120) was J-coded in sample 18. Although the analyte in question hasbeen positively identified in the sample, the quantitation is an estimate (J-coded) due tohigh recovery of this analyte in the laboratory matrix spike. The actual concentration forthis analyte may be lower than the reported value.
Comments:
Comments:
Comments:
1-__ 2-__ 3-__ 4-__ 4-FD 5-__ 6-__7-__ 8-__ 9-__ 10-__ 10-FD 11-__ 12-__13-__ 14-__ 15-__ 16-__ 17-__ 18-__ 19-__22-__ 22-FD
1-__ 2-__ 3-__ 4-__ 4-FD 5-__ 6-__7-__ 8-__ 9-__ 10-__ 10-FD 11-__ 12-__13-__ 14-__ 15-__ 16-__ 17-__ 18-__ 19-__22-__ 22-FD
1-__ 2-__ 3-__ 4-__ 4-FD 5-__ 6-__7-__ 8-__ 9-__ 10-__ 10-FD 11-__ 12-__13-__ 14-__ 15-__ 16-__ 17-__ 18-__ 19-__22-__ 22-FD 24-FB
Samples:
Samples:
Samples:
4981ASR Number: 09/16/2010
MP7ES02Project ID: Cleburn Street well samplingProject Desc
RLAB Approved Analysis Comments
Analysis Comments About Results For This Analysis
Page 6 of 36
1
1
TDS or Total Dissolved Solids
VOCs in Water by GC/MS
Region 7 ESAT Contract Lab (In-House)
Region 7 ESAT Contract Lab (In-House)
Lab:
Lab:
EPA Region 7 RLAB Method 3142.2C
EPA Region 7 RLAB Method 3230.1F
Method:
Method:
Dilutions were necessary in order to obtain valid results due to matrix interferences. Thereporting limits were elevated (100 times) due to dilutions in samples 2, 3, 4, 4FD, 6, 9,12, 13, 14, 16, 17, 18.
Dilutions were necessary in order to obtain valid results due to matrix interferences. Thereporting limits were elevated 1000 times due to dilutions in samples 5, 7, 8, 10, 10FD, 11,15, 22, 22FD.
Arsenic (8.0,5.0) was UJ-coded in sample 19. This analyte was not found in the sample ator above the reporting limit, however, the reporting limit is an estimate (UJ-coded) due topoor precision obtained for this analyte in the laboratory matrix spike and matrix spikeduplicate. The actual reporting limit for this analyte may be higher than the reportedvalue.
Thallium (6.4,5.0) was UJ-coded in sample 19. This analyte was not found in the sampleat or above the reporting limit, however, the reporting limit is an estimate (UJ-coded) dueto poor precision obtained for this analyte in the laboratory matrix spike and matrix spikeduplicate. The actual reporting limit for this analyte may be higher than the reportedvalue.
Comments:
Comments:
1-__ 2-__ 3-__ 4-__ 4-FD 5-__ 6-__7-__ 8-__ 9-__ 10-__ 10-FD 11-__ 12-__13-__ 14-__ 15-__ 16-__ 17-__ 18-__ 19-__22-__ 22-FD 24-FB
1-__ 2-__ 3-__ 4-__ 4-FD 5-__ 6-__7-__ 8-__ 9-__ 10-__ 10-FD 11-__ 12-__13-__ 14-__ 15-__ 16-__ 17-__ 18-__ 19-__22-__ 22-FD
1-__ 2-__ 3-__ 4-__ 4-FD 5-__ 6-__7-__ 8-__ 9-__ 10-__ 10-FD 11-__ 12-__13-__ 14-__ 15-__ 16-__ 17-__ 18-__ 19-__22-__ 22-FD 24-FB 25-__ 26-__ 27-__ 28-__29-__ 30-__ 31-__ 32-__ 32-FD 34-__ 35-__
Samples:
Samples:
Samples:
4981ASR Number: 09/16/2010
MP7ES02Project ID: Cleburn Street well samplingProject Desc
RLAB Approved Analysis Comments
Analysis Comments About Results For This Analysis
Page 7 of 36
Twenty of the samples contained potassium permanganate. These samples were diluted tokeep the column from being damaged. The resulting reporting limit for these samples were500 to 5000 times higher than the normal reporting limit.
Acetone (+39.2%), 2-Butanone (+30.3%), Carbon Tetrachloride (+20.8%), and 2-Hexanone (+20.6%) were UJ-coded in samples 24-FB, 53-FB, 2, 54-FB, 55-FB, 1, 18, 25,27, 28, 29, 30, 31, 32, 32-FD, 34, 35, 35-FD, 37, 38, 39, 40, 42, and 43. These analyteswere not found in the samples at or above the reporting limit, however, the reporting limitis an estimate (UJ-coded) due to the continuing calibration check not meeting accuracyspecifications. The actual reporting limit for these analytes may be higher than thereported value.
1,1,2-Trichlorotrifluoroethane (+23.5%), Cyclohexane (+27.5%), and Carbon Tetrachloride(+37.2%) were UJ-coded in samples 41, 44, 45, 45-FD, 47, 48, 49, 50, 19, 3, 4, 4-FD, 5,6, 7, 8, 9, 10, 10-FD, 11, 12, 13, 14, 15, and 17. These analytes were not found in thesamples at or above the reporting limit, however, the reporting limit is an estimate (UJ-coded) due to the continuing calibration check not meeting accuracy specifications. Theactual reporting limit for these analytes may be higher than the reported value.
1,1,2-Trichlorotrifluoroethane (+23.3%), 2-Butanone (+26.0%), 1,1,1-Trichloroethane(+22.4%), Cyclohexane (+26.1%), Carbon Tetrachloride (+40.7%), cis-1,3-Dichloropropene (+23.2%), trans-1,3-Dichloropropene (+26.8%), 2-Hexanone (+27.6%),1,2-Dibromoethane (+31.4%), and Bromoform (+21.5%) were UJ-coded in samples 16,22, 22-FD, and 26. These analytes were not found in the samples at or above thereporting limit, however, the reporting limit is an estimate (UJ-coded) due to thecontinuing calibration check not meeting accuracy specifications. The actual reporting limitfor these analytes may be higher than the reported value.
Carbon Tetrachloride (79%, 84%-119%) was UJ-coded in samples 24-FB, 53-FB, 2, 54-FB,55-FB, 1, 18, 25, 27, 28, 29, 30, 31, 32, 32-FD, 34, 35, 35-FD, 37, 38, 39, 40, 42, and 43. This analyte was not found in the samples at or above the reporting limit, however, thereporting limit is an estimate (UJ-coded) due to low recovery of this analyte in thelaboratory control sample. The actual reporting limit for this analyte may be higher thanthe reported value.
1,1,1-Trichloroethane (81%, 84%-119%), Carbon Tetrachloride (63%, 84%-119%), cis-1,3-Dichloropropene (84%, 85%-120%), and 1,2-Dibromoethane (81%, 87%-114%) wereUJ-coded in samples 41, 44, 45, 45-FD, 47, 48, 49, 50, 19, 3, 4, 4-FD, 5, 6, 7, 8, 9, 10,10-FD, 11, 12, 13, 14, 15, and 17. These analytes were not found in the samples at orabove the reporting limit, however, the reporting limit is an estimate (UJ-coded) due to lowrecovery of these analytes in the laboratory control sample. The actual reporting limit forthese analytes may be higher than the reported value.
1,1-Dichloroethane (83%, 86%-114%), 1,1,1-Trichloroethane (78%, 84%-119%), Carbon
Comments:
35-FD 37-__ 38-__ 39-__ 40-__ 41-__ 42-__43-__ 44-__ 45-__ 45-FD 47-__ 48-__ 49-__50-__ 53-FB 54-FB 55-FB
Samples:
4981ASR Number: 09/16/2010
MP7ES02Project ID: Cleburn Street well samplingProject Desc
RLAB Approved Analysis Comments
Analysis Comments About Results For This Analysis
Page 8 of 36
Tetrachloride (59%, 84%-119%), 1,2-Dichloropropane (87%, 89%-108%), cis-1,3-Dichloropropene (77%, 85%-120%), trans-1,3-Dichloropropene (73%, 78%-129%),Dibromochloromethane (84%, 86%-119%), 1,2-Dibromoethane (69%, 87%-114%), andBromoform (78%, 83%-119%) were UJ-coded in samples 16, 22, 22-FD, and 26. Theseanalytes were not found in the samples at or above the reporting limit, however, thereporting limit is an estimate (UJ-coded) due to low recovery of these analytes in thelaboratory control sample. The actual reporting limit for these analytes may be higher thanthe reported value.
1,2-Dibromoethane (86% & 87%, 90%-114%), 1,2-Dichlorobenzene (86%, 88%-116%),1,3-Dichlorobenzene (89% & 86%, 91%-115%), 1,4-Dichlorobenzene (88% & 87%, 89%-116%), and Styrene (16% & 16%, 83%-121%) were UJ-coded in sample 2. Theseanalytes were not found in the sample at or above the reporting limit, however, thereporting limit is an estimate (UJ-coded) due to low recovery of these analytes in thelaboratory matrix spike. The actual reporting limit for these analytes may be higher thanthe reported value.
Bromoform (74% & 75%, 77%-122%), Carbon Tetrachloride (60% & 62%, 78%-129%),Cyclohexane (69% & 71%, 76%-124%), Dibromochloromethane (84% & 85%, 86%-118%), 1,2-Dibromoethane (72% & 72%, 90%-114%), cis-1,3-Dichloropropene (80% &78%, 82%-113%), trans-1,3-Dichloropropene (78% & 75%, 84%-117%), 1,1,1-Trichloroethane (78%, 81%-126%), and 1,1,2-Trichlorotrifluoroethane (72%, 73%-125%)were UJ-coded in sample 41. These analytes were not found in the sample at or above thereporting limit, however, the reporting limit is an estimate (UJ-coded) due to low recoveryof these analytes in the laboratory matrix spike. The actual reporting limit for theseanalytes may be higher than the reported value.
Bromoform (68%, 77%-122%), Carbon Tetrachloride (61%, 78%-129%),Dibromochloromethane (81%, 86%-118%), 1,2-Dibromoethane (63%, 90%-114%), cis-1,3-Dichloropropene (74%, 82%-113%), trans-1,3-Dichloropropene (71%, 84%-117%),and 4-Methyl-2-Pentanone (72%, 79%-125%) were UJ-coded in sample 44. Theseanalytes were not found in the sample at or above the reporting limit, however, thereporting limit is an estimate (UJ-coded) due to low recovery of these analytes in thelaboratory matrix spike. The actual reporting limit for these analytes may be higher thanthe reported value.
1,3-Dichlorobenzene (8.4RPD, 7.9 PCL) and o-Xylene (8.7RPD, 8.3PCL) were UJ-coded insample 41. These analytes were not found in the sample at or above the reporting limit,however, the reporting limit is an estimate (UJ-coded) due to poor precision obtained forthese analytes in the laboratory matrix spike and matrix spike duplicate. The actualreporting limit for these analytes may be higher than the reported value.
4981ASR Number: 09/16/2010
MP7ES02Project ID: Cleburn Street well samplingProject Desc
RLAB Approved Analysis Comments
Analysis Comments About Results For This Analysis
Page 9 of 36
1
1
1
1
1
1
Alkalinity in Water by Titration
Anions in Water by Ion Chromatography
Hardness in Water by Calculation
Metals in Water by ICP-AES
TDS or Total Dissolved Solids
VOCs in Water by GC/MS
Analysis/ Analyte
Alkalinity, total
Sulfate
Hardness as CaCO3
Aluminum
Antimony
Arsenic
Barium
Beryllium
Cadmium
Calcium
Chromium
Cobalt
Copper
Iron
Lead
Magnesium
Manganese
Molybdenum
Nickel
Potassium
Selenium
Silver
Sodium
Thallium
Titanium
Vanadium
Zinc
Solids, total dissolved
Acetone
Benzene
Bromodichloromethane
Bromoform
Bromomethane
2-Butanone
Carbon Disulfide
Carbon Tetrachloride
Chlorobenzene
Chloroethane
Chloroform
Chloromethane
mg/L
mg/L
mg/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
mg/L
ug/L
ug/L
ug/L
ug/L
ug/L
mg/L
ug/L
ug/L
ug/L
mg/L
ug/L
ug/L
mg/L
ug/L
ug/L
ug/L
ug/L
mg/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
Units 1-__ 2-__ 3-__ 4-__
57.5 51.2 194 188
45.3 55.3 10000 U 10000 U
111 1300 U 1300 U 1300 U
54 5000 U 5000 U 5000 U
50 U 5000 U 5000 U 5000 U
25 U 2500 U 2500 U 2500 U
101 1000 U 1000 U 1000 U
3 U 300 U 300 U 300 U
3 U 300 U 300 U 300 U
31.9 200 U 200 U 200 U
15 1500 U 1500 U 1500 U
10 U 1000 U 1000 U 1000 U
5 U 500 U 500 U 500 U
128 5000 U 5000 U 5000 U
50 U 5000 U 5000 U 5000 U
7.60 200 U 200 U 200 U
5 U 500 U 321000 351000
15 U 1500 U 1500 U 1500 U
20 U 2000 U 2000 U 2000 U
10.1 200 U 642 736
50 U 5000 U 5000 U 5000 U
25 U 2500 U 2500 U 2500 U
31.8 500 U 500 U 500 U
50 U 5000 U 5000 U 5000 U
20 U 2000 U 2000 U 2000 U
10 U 1000 U 1000 U 1000 U
25 U 2500 U 2500 U 4500
271 313 2830 736
5.0 UJ 5.0 UJ 5000 U 5000 U
5.0 U 5.0 U 5000 U 5000 U
5.0 U 5.0 U 5000 U 5000 U
5.0 U 5.0 U 5000 U 5000 U
5.0 U 5.0 U 5000 U 5000 U
5.0 UJ 5.0 UJ 5000 U 5000 U
5.0 U 5.0 U 5000 U 5000 U
5.0 UJ 5.0 UJ 5000 UJ 5000 UJ
5.0 U 5.0 U 5000 U 5000 U
5.0 U 5.0 U 5000 U 5000 U
5.0 U 5.0 U 5000 U 5000 U
5.0 U 5.0 U 5000 U 5000 U
4981ASR Number: 09/16/2010
MP7ES02Project ID: Cleburn Street well samplingProject Desc:
RLAB Approved Sample Analysis Results
Page 10 of 36
Analysis/ Analyte
Cyclohexane
1,2-Dibromo-3-Chloropropane
Dibromochloromethane
1,2-Dibromoethane
1,2-Dichlorobenzene
1,3-Dichlorobenzene
1,4-Dichlorobenzene
Dichlorodifluoromethane
1,1-Dichloroethane
1,2-Dichloroethane
1,1-Dichloroethene
cis-1,2-Dichloroethene
trans-1,2-Dichloroethene
1,2-Dichloropropane
cis-1,3-Dichloropropene
trans-1,3-Dichloropropene
Ethyl Benzene
2-Hexanone
Isopropylbenzene
Methyl Acetate
Methyl tert-butyl ether
Methylcyclohexane
Methylene Chloride
4-Methyl-2-Pentanone
Naphthalene
Styrene
1,1,2,2-Tetrachloroethane
Tetrachloroethene
Toluene
1,2,3-Trichlorobenzene
1,2,4-Trichlorobenzene
1,1,1-Trichloroethane
1,1,2-Trichloroethane
Trichloroethene
Trichlorofluoromethane
1,1,2-Trichlorotrifluoroethane
Vinyl Chloride
m and/or p-Xylene
o-Xylene
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
Units 1-__ 2-__ 3-__ 4-__
5.0 U 5.0 U 5000 UJ 5000 UJ
5.0 U 5.0 U 5000 U 5000 U
5.0 U 5.0 U 5000 U 5000 U
5.0 U 5.0 UJ 5000 UJ 5000 UJ
5.0 U 5.0 UJ 5000 U 5000 U
5.0 U 5.0 UJ 5000 U 5000 U
5.0 U 5.0 UJ 5000 U 5000 U
5.0 U 5.0 U 5000 U 5000 U
5.0 U 5.0 U 5000 U 5000 U
5.0 U 5.0 U 5000 U 5000 U
5.0 U 5.0 U 5000 U 5000 U
5.0 U 5.0 U 5000 U 5000 U
5.0 U 5.0 U 5000 U 5000 U
5.0 U 5.0 U 5000 U 5000 U
5.0 U 5.0 U 5000 UJ 5000 UJ
5.0 U 5.0 U 5000 U 5000 U
5.0 U 5.0 U 5000 U 5000 U
5.0 UJ 5.0 UJ 5000 U 5000 U
5.0 U 5.0 U 5000 U 5000 U
5.0 U 5.0 U 5000 U 5000 U
10 U 10 U 10000 U 10000 U
5.0 U 5.0 U 5000 U 5000 U
5.0 U 5.0 U 5000 U 5000 U
5.0 U 5.0 U 5000 U 5000 U
10 U 10 U 10000 U 10000 U
5.0 U 5.0 UJ 5000 U 5000 U
5.0 U 5.0 U 5000 U 5000 U
5.0 U 5.0 U 5000 U 5000 U
5.0 U 5.0 U 5000 U 5000 U
5.0 U 5.0 U 5000 U 5000 U
5.0 U 5.0 U 5000 U 5000 U
5.0 U 5.0 U 5000 UJ 5000 UJ
5.0 U 5.0 U 5000 U 5000 U
5.0 U 5.0 U 5000 U 5000 U
5.0 U 5.0 U 5000 U 5000 U
5.0 U 5.0 U 5000 UJ 5000 UJ
5.0 U 5.0 U 5000 U 5000 U
10 U 10 U 10000 U 10000 U
5.0 U 5.0 U 5000 U 5000 U
4981ASR Number: 09/16/2010
MP7ES02Project ID: Cleburn Street well samplingProject Desc:
RLAB Approved Sample Analysis Results
Page 11 of 36
1
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1
1
1
1
Alkalinity in Water by Titration
Anions in Water by Ion Chromatography
Hardness in Water by Calculation
Metals in Water by ICP-AES
TDS or Total Dissolved Solids
VOCs in Water by GC/MS
Analysis/ Analyte
Alkalinity, total
Sulfate
Hardness as CaCO3
Aluminum
Antimony
Arsenic
Barium
Beryllium
Cadmium
Calcium
Chromium
Cobalt
Copper
Iron
Lead
Magnesium
Manganese
Molybdenum
Nickel
Potassium
Selenium
Silver
Sodium
Thallium
Titanium
Vanadium
Zinc
Solids, total dissolved
Acetone
Benzene
Bromodichloromethane
Bromoform
Bromomethane
2-Butanone
Carbon Disulfide
Carbon Tetrachloride
Chlorobenzene
Chloroethane
Chloroform
Chloromethane
mg/L
mg/L
mg/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
mg/L
ug/L
ug/L
ug/L
ug/L
ug/L
mg/L
ug/L
ug/L
ug/L
mg/L
ug/L
ug/L
mg/L
ug/L
ug/L
ug/L
ug/L
mg/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
Units 4-FD 5-__ 6-__ 7-__
188 239 208 227
10000 U 10000 U 10000 U 10000 U
1300 U 13000 U 1300 U 13000 U
5000 U 50000 U 5000 U 50000 U
5000 U 50000 U 5000 U 50000 U
2500 U 25000 U 2500 U 25000 U
1000 U 10000 U 1000 U 10000 U
300 U 3000 U 300 U 3000 U
300 U 3000 U 300 U 3000 U
200 U 2000 U 200 U 2000 U
1500 U 15000 U 1500 U 15000 U
1000 U 10000 U 1000 U 10000 U
500 U 5000 U 500 U 5000 U
5000 U 50000 U 5000 U 50000 U
5000 U 50000 U 5000 U 50000 U
200 U 2000 U 200 U 2000 U
282000 371000 214000 420000
1500 U 15000 U 1500 U 15000 U
2000 U 20000 U 2000 U 20000 U
598 2000 U 608 2000 U
5000 U 50000 U 5000 U 50000 U
2500 U 25000 U 2500 U 25000 U
500 U 5000 U 500 U 5000 U
5000 U 50000 U 5000 U 50000 U
2000 U 20000 U 2000 U 20000 U
1000 U 10000 U 1000 U 10000 U
2500 U 25000 U 2500 U 25000 U
2390 6440 2250 7450
5000 U 25000 U 5000 U 25000 U
5000 U 25000 U 5000 U 25000 U
5000 U 25000 U 5000 U 25000 U
5000 U 25000 U 5000 U 25000 U
5000 U 25000 U 5000 U 25000 U
5000 U 25000 U 5000 U 25000 U
5000 U 25000 U 5000 U 25000 U
5000 UJ 25000 UJ 5000 UJ 25000 UJ
5000 U 25000 U 5000 U 25000 U
5000 U 25000 U 5000 U 25000 U
5000 U 25000 U 5000 U 25000 U
5000 U 25000 U 5000 U 25000 U
4981ASR Number: 09/16/2010
MP7ES02Project ID: Cleburn Street well samplingProject Desc:
RLAB Approved Sample Analysis Results
Page 12 of 36
Analysis/ Analyte
Cyclohexane
1,2-Dibromo-3-Chloropropane
Dibromochloromethane
1,2-Dibromoethane
1,2-Dichlorobenzene
1,3-Dichlorobenzene
1,4-Dichlorobenzene
Dichlorodifluoromethane
1,1-Dichloroethane
1,2-Dichloroethane
1,1-Dichloroethene
cis-1,2-Dichloroethene
trans-1,2-Dichloroethene
1,2-Dichloropropane
cis-1,3-Dichloropropene
trans-1,3-Dichloropropene
Ethyl Benzene
2-Hexanone
Isopropylbenzene
Methyl Acetate
Methyl tert-butyl ether
Methylcyclohexane
Methylene Chloride
4-Methyl-2-Pentanone
Naphthalene
Styrene
1,1,2,2-Tetrachloroethane
Tetrachloroethene
Toluene
1,2,3-Trichlorobenzene
1,2,4-Trichlorobenzene
1,1,1-Trichloroethane
1,1,2-Trichloroethane
Trichloroethene
Trichlorofluoromethane
1,1,2-Trichlorotrifluoroethane
Vinyl Chloride
m and/or p-Xylene
o-Xylene
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
Units 4-FD 5-__ 6-__ 7-__
5000 UJ 25000 UJ 5000 UJ 25000 UJ
5000 U 25000 U 5000 U 25000 U
5000 U 25000 U 5000 U 25000 U
5000 UJ 25000 UJ 5000 UJ 25000 UJ
5000 U 25000 U 5000 U 25000 U
5000 U 25000 U 5000 U 25000 U
5000 U 25000 U 5000 U 25000 U
5000 U 25000 U 5000 U 25000 U
5000 U 25000 U 5000 U 25000 U
5000 U 25000 U 5000 U 25000 U
5000 U 25000 U 5000 U 25000 U
5000 U 25000 U 5000 U 25000 U
5000 U 25000 U 5000 U 25000 U
5000 U 25000 U 5000 U 25000 U
5000 UJ 25000 UJ 5000 UJ 25000 UJ
5000 U 25000 U 5000 U 25000 U
5000 U 25000 U 5000 U 25000 U
5000 U 25000 U 5000 U 25000 U
5000 U 25000 U 5000 U 25000 U
5000 U 25000 U 5000 U 25000 U
10000 U 50000 U 10000 U 50000 U
5000 U 25000 U 5000 U 25000 U
5000 U 25000 U 5000 U 25000 U
5000 U 25000 U 5000 U 25000 U
10000 U 50000 U 10000 U 50000 U
5000 U 25000 U 5000 U 25000 U
5000 U 25000 U 5000 U 25000 U
5000 U 25000 U 5000 U 25000 U
5000 U 25000 U 5000 U 25000 U
5000 U 25000 U 5000 U 25000 U
5000 U 25000 U 5000 U 25000 U
5000 UJ 25000 UJ 5000 UJ 25000 UJ
5000 U 25000 U 5000 U 25000 U
5000 U 25000 U 5000 U 25000 U
5000 U 25000 U 5000 U 25000 U
5000 UJ 25000 UJ 5000 UJ 25000 UJ
5000 U 25000 U 5000 U 25000 U
10000 U 50000 U 10000 U 50000 U
5000 U 25000 U 5000 U 25000 U
4981ASR Number: 09/16/2010
MP7ES02Project ID: Cleburn Street well samplingProject Desc:
RLAB Approved Sample Analysis Results
Page 13 of 36
1
1
1
1
1
1
Alkalinity in Water by Titration
Anions in Water by Ion Chromatography
Hardness in Water by Calculation
Metals in Water by ICP-AES
TDS or Total Dissolved Solids
VOCs in Water by GC/MS
Analysis/ Analyte
Alkalinity, total
Sulfate
Hardness as CaCO3
Aluminum
Antimony
Arsenic
Barium
Beryllium
Cadmium
Calcium
Chromium
Cobalt
Copper
Iron
Lead
Magnesium
Manganese
Molybdenum
Nickel
Potassium
Selenium
Silver
Sodium
Thallium
Titanium
Vanadium
Zinc
Solids, total dissolved
Acetone
Benzene
Bromodichloromethane
Bromoform
Bromomethane
2-Butanone
Carbon Disulfide
Carbon Tetrachloride
Chlorobenzene
Chloroethane
Chloroform
Chloromethane
mg/L
mg/L
mg/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
mg/L
ug/L
ug/L
ug/L
ug/L
ug/L
mg/L
ug/L
ug/L
ug/L
mg/L
ug/L
ug/L
mg/L
ug/L
ug/L
ug/L
ug/L
mg/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
Units 8-__ 9-__ 10-__ 10-FD
2.00 U 13.8 248 248
10000 U 10000 U 10000 U 10000 U
13000 U 1400 13000 U 13000 U
58100 8920 50000 U 50000 U
50000 U 5000 U 50000 U 50000 U
25000 U 2500 U 25000 U 25000 U
10000 U 1000 U 10000 U 10000 U
3000 U 300 U 3000 U 3000 U
3000 U 300 U 3000 U 3000 U
2000 U 238 2000 U 2000 U
15000 U 1500 U 15000 U 15000 U
10000 U 1000 U 10000 U 10000 U
5000 U 500 U 5000 U 5000 U
50000 U 5000 U 50000 U 50000 U
50000 U 5000 U 50000 U 50000 U
2000 U 200 U 2000 U 2000 U
398000 254000 397000 398000
15000 U 1500 U 15000 U 15000 U
20000 U 2000 U 20000 U 20000 U
2000 U 489 2000 U 2000 U
50000 U 5000 U 50000 U 50000 U
25000 U 2500 U 25000 U 25000 U
5000 U 500 U 5000 U 5000 U
50000 U 5000 U 50000 U 50000 U
20000 U 2000 U 20000 U 20000 U
10000 U 1000 U 10000 U 10000 U
25000 U 2500 U 25000 U 25000 U
7920 4210 4840 4820
25000 U 5000 U 25000 U 25000 U
25000 U 5000 U 25000 U 25000 U
25000 U 5000 U 25000 U 25000 U
25000 U 5000 U 25000 U 25000 U
25000 U 5000 U 25000 U 25000 U
25000 U 5000 U 25000 U 25000 U
25000 U 5000 U 25000 U 25000 U
25000 UJ 5000 UJ 25000 UJ 25000 UJ
25000 U 5000 U 25000 U 25000 U
25000 U 5000 U 25000 U 25000 U
25000 U 5000 U 25000 U 25000 U
25000 U 5000 U 25000 U 25000 U
4981ASR Number: 09/16/2010
MP7ES02Project ID: Cleburn Street well samplingProject Desc:
RLAB Approved Sample Analysis Results
Page 14 of 36
Analysis/ Analyte
Cyclohexane
1,2-Dibromo-3-Chloropropane
Dibromochloromethane
1,2-Dibromoethane
1,2-Dichlorobenzene
1,3-Dichlorobenzene
1,4-Dichlorobenzene
Dichlorodifluoromethane
1,1-Dichloroethane
1,2-Dichloroethane
1,1-Dichloroethene
cis-1,2-Dichloroethene
trans-1,2-Dichloroethene
1,2-Dichloropropane
cis-1,3-Dichloropropene
trans-1,3-Dichloropropene
Ethyl Benzene
2-Hexanone
Isopropylbenzene
Methyl Acetate
Methyl tert-butyl ether
Methylcyclohexane
Methylene Chloride
4-Methyl-2-Pentanone
Naphthalene
Styrene
1,1,2,2-Tetrachloroethane
Tetrachloroethene
Toluene
1,2,3-Trichlorobenzene
1,2,4-Trichlorobenzene
1,1,1-Trichloroethane
1,1,2-Trichloroethane
Trichloroethene
Trichlorofluoromethane
1,1,2-Trichlorotrifluoroethane
Vinyl Chloride
m and/or p-Xylene
o-Xylene
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
Units 8-__ 9-__ 10-__ 10-FD
25000 UJ 5000 UJ 25000 UJ 25000 UJ
25000 U 5000 U 25000 U 25000 U
25000 U 5000 U 25000 U 25000 U
25000 UJ 5000 UJ 25000 UJ 25000 UJ
25000 U 5000 U 25000 U 25000 U
25000 U 5000 U 25000 U 25000 U
25000 U 5000 U 25000 U 25000 U
25000 U 5000 U 25000 U 25000 U
25000 U 5000 U 25000 U 25000 U
25000 U 5000 U 25000 U 25000 U
25000 U 5000 U 25000 U 25000 U
25000 U 5000 U 25000 U 25000 U
25000 U 5000 U 25000 U 25000 U
25000 U 5000 U 25000 U 25000 U
25000 UJ 5000 UJ 25000 UJ 25000 UJ
25000 U 5000 U 25000 U 25000 U
25000 U 5000 U 25000 U 25000 U
25000 U 5000 U 25000 U 25000 U
25000 U 5000 U 25000 U 25000 U
25000 U 5000 U 25000 U 25000 U
50000 U 10000 U 50000 U 50000 U
25000 U 5000 U 25000 U 25000 U
25000 U 5000 U 25000 U 25000 U
25000 U 5000 U 25000 U 25000 U
50000 U 10000 U 50000 U 50000 U
25000 U 5000 U 25000 U 25000 U
25000 U 5000 U 25000 U 25000 U
25000 U 5000 U 25000 U 25000 U
25000 U 5000 U 25000 U 25000 U
25000 U 5000 U 25000 U 25000 U
25000 U 5000 U 25000 U 25000 U
25000 UJ 5000 UJ 25000 UJ 25000 UJ
25000 U 5000 U 25000 U 25000 U
25000 U 5000 U 25000 U 25000 U
25000 U 5000 U 25000 U 25000 U
25000 UJ 5000 UJ 25000 UJ 25000 UJ
25000 U 5000 U 25000 U 25000 U
50000 U 10000 U 50000 U 50000 U
25000 U 5000 U 25000 U 25000 U
4981ASR Number: 09/16/2010
MP7ES02Project ID: Cleburn Street well samplingProject Desc:
RLAB Approved Sample Analysis Results
Page 15 of 36
1
1
1
1
1
1
Alkalinity in Water by Titration
Anions in Water by Ion Chromatography
Hardness in Water by Calculation
Metals in Water by ICP-AES
TDS or Total Dissolved Solids
VOCs in Water by GC/MS
Analysis/ Analyte
Alkalinity, total
Sulfate
Hardness as CaCO3
Aluminum
Antimony
Arsenic
Barium
Beryllium
Cadmium
Calcium
Chromium
Cobalt
Copper
Iron
Lead
Magnesium
Manganese
Molybdenum
Nickel
Potassium
Selenium
Silver
Sodium
Thallium
Titanium
Vanadium
Zinc
Solids, total dissolved
Acetone
Benzene
Bromodichloromethane
Bromoform
Bromomethane
2-Butanone
Carbon Disulfide
Carbon Tetrachloride
Chlorobenzene
Chloroethane
Chloroform
Chloromethane
mg/L
mg/L
mg/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
mg/L
ug/L
ug/L
ug/L
ug/L
ug/L
mg/L
ug/L
ug/L
ug/L
mg/L
ug/L
ug/L
mg/L
ug/L
ug/L
ug/L
ug/L
mg/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
Units 11-__ 12-__ 13-__ 14-__
164 213 367 241
10000 U 10000 U 10000 U 10000 U
13000 U 1300 U 1500 1300 U
50000 U 6520 5000 U 5000 U
50000 U 5000 U 5000 U 5000 U
25000 U 2500 U 2500 U 2500 U
10000 U 1000 U 1000 U 1000 U
3000 U 300 U 300 U 300 U
3000 U 300 U 300 U 300 U
2000 U 200 U 281 200 U
15000 U 4030 4150 1500 U
10000 U 1000 U 1000 U 1000 U
5000 U 500 U 500 U 500 U
50000 U 5000 U 5000 U 5000 U
50000 U 5000 U 5000 U 5000 U
2000 U 200 U 200 U 200 U
365000 339000 337000 32400
15000 U 1500 U 1500 U 1500 U
20000 U 2920 2000 U 2000 U
2000 U 962 778 200 U
50000 U 5000 U 5000 U 5000 U
25000 U 2500 U 2500 U 2500 U
5000 U 500 U 500 U 500 U
50000 U 5000 U 5000 U 5000 U
20000 U 2000 U 2000 U 2000 U
10000 U 1000 U 1000 U 1000 U
25000 U 2500 U 2500 U 2500 U
5500 4260 4420 2890
5000 U 5000 U 5000 U 5000 U
5000 U 5000 U 5000 U 5000 U
5000 U 5000 U 5000 U 5000 U
5000 U 5000 U 5000 U 5000 U
5000 U 5000 U 5000 U 5000 U
5000 U 5000 U 5000 U 5000 U
5000 U 5000 U 5000 U 5000 U
5000 UJ 5000 UJ 5000 UJ 5000 UJ
5000 U 5000 U 5000 U 5000 U
5000 U 5000 U 5000 U 5000 U
5000 U 5000 U 5000 U 5000 U
5000 U 5000 U 5000 U 5000 U
4981ASR Number: 09/16/2010
MP7ES02Project ID: Cleburn Street well samplingProject Desc:
RLAB Approved Sample Analysis Results
Page 16 of 36
Analysis/ Analyte
Cyclohexane
1,2-Dibromo-3-Chloropropane
Dibromochloromethane
1,2-Dibromoethane
1,2-Dichlorobenzene
1,3-Dichlorobenzene
1,4-Dichlorobenzene
Dichlorodifluoromethane
1,1-Dichloroethane
1,2-Dichloroethane
1,1-Dichloroethene
cis-1,2-Dichloroethene
trans-1,2-Dichloroethene
1,2-Dichloropropane
cis-1,3-Dichloropropene
trans-1,3-Dichloropropene
Ethyl Benzene
2-Hexanone
Isopropylbenzene
Methyl Acetate
Methyl tert-butyl ether
Methylcyclohexane
Methylene Chloride
4-Methyl-2-Pentanone
Naphthalene
Styrene
1,1,2,2-Tetrachloroethane
Tetrachloroethene
Toluene
1,2,3-Trichlorobenzene
1,2,4-Trichlorobenzene
1,1,1-Trichloroethane
1,1,2-Trichloroethane
Trichloroethene
Trichlorofluoromethane
1,1,2-Trichlorotrifluoroethane
Vinyl Chloride
m and/or p-Xylene
o-Xylene
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
Units 11-__ 12-__ 13-__ 14-__
5000 UJ 5000 UJ 5000 UJ 5000 UJ
5000 U 5000 U 5000 U 5000 U
5000 U 5000 U 5000 U 5000 U
5000 UJ 5000 UJ 5000 UJ 5000 UJ
5000 U 5000 U 5000 U 5000 U
5000 U 5000 U 5000 U 5000 U
5000 U 5000 U 5000 U 5000 U
5000 U 5000 U 5000 U 5000 U
5000 U 5000 U 5000 U 5000 U
5000 U 5000 U 5000 U 5000 U
5000 U 5000 U 5000 U 5000 U
5000 U 5000 U 5000 U 5000 U
5000 U 5000 U 5000 U 5000 U
5000 U 5000 U 5000 U 5000 U
5000 UJ 5000 UJ 5000 UJ 5000 UJ
5000 U 5000 U 5000 U 5000 U
5000 U 5000 U 5000 U 5000 U
5000 U 5000 U 5000 U 5000 U
5000 U 5000 U 5000 U 5000 U
5000 U 5000 U 5000 U 5000 U
10000 U 10000 U 10000 U 10000 U
5000 U 5000 U 5000 U 5000 U
5000 U 5000 U 5000 U 5000 U
5000 U 5000 U 5000 U 5000 U
10000 U 10000 U 10000 U 10000 U
5000 U 5000 U 5000 U 5000 U
5000 U 5000 U 5000 U 5000 U
5000 U 5000 U 5000 U 5000 U
5000 U 5000 U 5000 U 5000 U
5000 U 5000 U 5000 U 5000 U
5000 U 5000 U 5000 U 5000 U
5000 UJ 5000 UJ 5000 UJ 5000 UJ
5000 U 5000 U 5000 U 5000 U
5000 U 5000 U 5000 U 5000 U
5000 U 5000 U 5000 U 5000 U
5000 UJ 5000 UJ 5000 UJ 5000 UJ
5000 U 5000 U 5000 U 5000 U
10000 U 10000 U 10000 U 10000 U
5000 U 5000 U 5000 U 5000 U
4981ASR Number: 09/16/2010
MP7ES02Project ID: Cleburn Street well samplingProject Desc:
RLAB Approved Sample Analysis Results
Page 17 of 36
1
1
1
1
1
1
Alkalinity in Water by Titration
Anions in Water by Ion Chromatography
Hardness in Water by Calculation
Metals in Water by ICP-AES
TDS or Total Dissolved Solids
VOCs in Water by GC/MS
Analysis/ Analyte
Alkalinity, total
Sulfate
Hardness as CaCO3
Aluminum
Antimony
Arsenic
Barium
Beryllium
Cadmium
Calcium
Chromium
Cobalt
Copper
Iron
Lead
Magnesium
Manganese
Molybdenum
Nickel
Potassium
Selenium
Silver
Sodium
Thallium
Titanium
Vanadium
Zinc
Solids, total dissolved
Acetone
Benzene
Bromodichloromethane
Bromoform
Bromomethane
2-Butanone
Carbon Disulfide
Carbon Tetrachloride
Chlorobenzene
Chloroethane
Chloroform
Chloromethane
mg/L
mg/L
mg/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
mg/L
ug/L
ug/L
ug/L
ug/L
ug/L
mg/L
ug/L
ug/L
ug/L
mg/L
ug/L
ug/L
mg/L
ug/L
ug/L
ug/L
ug/L
mg/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
Units 15-__ 16-__ 17-__ 18-__
398 692 262 146
10000 U 10000 U 10000 U 35.3 J
13000 U 1300 U 2000 1300 U
50000 U 5000 U 5000 U 5000 U
50000 U 5000 U 5000 U 5000 U
25000 U 2500 U 2500 U 2500 U
10000 U 1000 U 1000 U 1000 U
3000 U 300 U 300 U 300 U
3000 U 300 U 300 U 300 U
2000 U 200 U 461 200 U
15000 U 1500 U 8900 1500 U
10000 U 1000 U 1000 U 1000 U
5000 U 500 U 500 U 500 U
50000 U 5000 U 5000 U 5000 U
50000 U 5000 U 5000 U 5000 U
2000 U 200 U 200 U 200 U
351000 350000 294000 500 U
15000 U 1500 U 1500 U 1500 U
20000 U 2000 U 3870 2000 U
2000 U 1290 200 U 200 U
50000 U 5000 U 5000 U 5000 U
25000 U 2500 U 2500 U 2500 U
5000 U 500 U 500 U 500 U
50000 U 5000 U 5000 U 5000 U
20000 U 2000 U 2000 U 2000 U
10000 U 1000 U 1000 U 1000 U
25000 U 2500 U 2500 U 2500 U
6350 4970 3910 358
5000 U 5000 U 5000 U 5.0 UJ
5000 U 5000 U 5000 U 5.0 U
5000 U 5000 U 5000 U 5.0 U
5000 U 5000 UJ 5000 U 5.0 U
5000 U 5000 U 5000 U 5.0 U
5000 U 5000 UJ 5000 U 5.0 UJ
5000 U 5000 U 5000 U 5.0 U
5000 UJ 5000 UJ 5000 UJ 5.0 UJ
5000 U 5000 U 5000 U 5.0 U
5000 U 5000 U 5000 U 5.0 U
5000 U 5000 U 5000 U 5.0 U
5000 U 5000 U 5000 U 5.0 U
4981ASR Number: 09/16/2010
MP7ES02Project ID: Cleburn Street well samplingProject Desc:
RLAB Approved Sample Analysis Results
Page 18 of 36
Analysis/ Analyte
Cyclohexane
1,2-Dibromo-3-Chloropropane
Dibromochloromethane
1,2-Dibromoethane
1,2-Dichlorobenzene
1,3-Dichlorobenzene
1,4-Dichlorobenzene
Dichlorodifluoromethane
1,1-Dichloroethane
1,2-Dichloroethane
1,1-Dichloroethene
cis-1,2-Dichloroethene
trans-1,2-Dichloroethene
1,2-Dichloropropane
cis-1,3-Dichloropropene
trans-1,3-Dichloropropene
Ethyl Benzene
2-Hexanone
Isopropylbenzene
Methyl Acetate
Methyl tert-butyl ether
Methylcyclohexane
Methylene Chloride
4-Methyl-2-Pentanone
Naphthalene
Styrene
1,1,2,2-Tetrachloroethane
Tetrachloroethene
Toluene
1,2,3-Trichlorobenzene
1,2,4-Trichlorobenzene
1,1,1-Trichloroethane
1,1,2-Trichloroethane
Trichloroethene
Trichlorofluoromethane
1,1,2-Trichlorotrifluoroethane
Vinyl Chloride
m and/or p-Xylene
o-Xylene
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
Units 15-__ 16-__ 17-__ 18-__
5000 UJ 5000 UJ 5000 UJ 5.0 U
5000 U 5000 U 5000 U 5.0 U
5000 U 5000 UJ 5000 U 5.0 U
5000 UJ 5000 UJ 5000 UJ 5.0 U
5000 U 5000 U 5000 U 5.0 U
5000 U 5000 U 5000 U 5.0 U
5000 U 5000 U 5000 U 5.0 U
5000 U 5000 U 5000 U 5.0 U
5000 U 5000 UJ 5000 U 5.0 U
5000 U 5000 U 5000 U 5.0 U
5000 U 5000 U 5000 U 5.0 U
5000 U 5000 U 5000 U 5.0 U
5000 U 5000 U 5000 U 5.0 U
5000 U 5000 UJ 5000 U 5.0 U
5000 UJ 5000 UJ 5000 UJ 5.0 U
5000 U 5000 UJ 5000 U 5.0 U
5000 U 5000 U 5000 U 5.0 U
5000 U 5000 UJ 5000 U 5.0 UJ
5000 U 5000 U 5000 U 5.0 U
5000 U 5000 U 5000 U 5.0 U
10000 U 10000 U 10000 U 10 U
5000 U 5000 U 5000 U 5.0 U
5000 U 5000 U 5000 U 5.0 U
5000 U 5000 U 5000 U 5.0 U
10000 U 10000 U 10000 U 10 U
5000 U 5000 U 5000 U 5.0 U
5000 U 5000 U 5000 U 5.0 U
5000 U 5000 U 5000 U 5.0 U
5000 U 5000 U 5000 U 5.0 U
5000 U 5000 U 5000 U 5.0 U
5000 U 5000 U 5000 U 5.0 U
5000 UJ 5000 UJ 5000 UJ 5.0 U
5000 U 5000 U 5000 U 5.0 U
5000 U 5000 U 5000 U 5.0 U
5000 U 5000 U 5000 U 5.0 U
5000 UJ 5000 UJ 5000 UJ 5.0 U
5000 U 5000 U 5000 U 5.0 U
10000 U 10000 U 10000 U 10 U
5000 U 5000 U 5000 U 5.0 U
4981ASR Number: 09/16/2010
MP7ES02Project ID: Cleburn Street well samplingProject Desc:
RLAB Approved Sample Analysis Results
Page 19 of 36
1
1
1
1
1
1
Alkalinity in Water by Titration
Anions in Water by Ion Chromatography
Hardness in Water by Calculation
Metals in Water by ICP-AES
TDS or Total Dissolved Solids
VOCs in Water by GC/MS
Analysis/ Analyte
Alkalinity, total
Sulfate
Hardness as CaCO3
Aluminum
Antimony
Arsenic
Barium
Beryllium
Cadmium
Calcium
Chromium
Cobalt
Copper
Iron
Lead
Magnesium
Manganese
Molybdenum
Nickel
Potassium
Selenium
Silver
Sodium
Thallium
Titanium
Vanadium
Zinc
Solids, total dissolved
Acetone
Benzene
Bromodichloromethane
Bromoform
Bromomethane
2-Butanone
Carbon Disulfide
Carbon Tetrachloride
Chlorobenzene
Chloroethane
Chloroform
Chloromethane
mg/L
mg/L
mg/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
mg/L
ug/L
ug/L
ug/L
ug/L
ug/L
mg/L
ug/L
ug/L
ug/L
mg/L
ug/L
ug/L
mg/L
ug/L
ug/L
ug/L
ug/L
mg/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
Units 19-__ 22-__ 22-FD 24-FB
93.0 127 126
42.5 10000 U 10000 U
171 13000 U 13000 U 13 U
50 U 50000 U 50000 U 50 U
50 U 50000 U 50000 U 50 U
25 UJ 25000 U 25000 U 25 U
160 10000 U 10000 U 10 U
3 U 3000 U 3000 U 3 U
3 U 3860 3000 U 3 U
51.8 2000 U 2000 U 2.00 U
15 U 15000 U 15000 U 15 U
10 U 10000 U 10000 U 10 U
5 U 5000 U 5000 U 5 U
56 50000 U 50000 U 50 U
50 U 50000 U 50000 U 50 U
10.1 2000 U 2000 U 2.00 U
91 355000 353000 5 U
15 U 15000 U 15000 U 15 U
20 U 20000 U 20000 U 20 U
7.06 2000 U 2000 U 2.00 U
50 U 50000 U 50000 U 50 U
25 U 25000 U 25000 U 25 U
72.3 5000 U 5000 U 5.00 U
50 UJ 50000 U 50000 U 50 U
20 U 20000 U 20000 U 20 U
10 U 10000 U 10000 U 10 U
25 U 25000 U 25000 U 25 U
484 3830 2300
5.0 U 5000 U 5000 U 5.0 UJ
5.0 U 5000 U 5000 U 5.0 U
5.0 U 5000 U 5000 U 5.0 U
5.0 U 5000 UJ 5000 UJ 5.0 U
5.0 U 5000 U 5000 U 5.0 U
5.0 U 5000 UJ 5000 UJ 5.0 UJ
5.0 U 5000 U 5000 U 5.0 U
5.0 UJ 5000 UJ 5000 UJ 5.0 UJ
5.0 U 5000 U 5000 U 5.0 U
5.0 U 5000 U 5000 U 5.0 U
5.0 U 5000 U 5000 U 5.0 U
5.0 U 5000 U 5000 U 5.0 U
4981ASR Number: 09/16/2010
MP7ES02Project ID: Cleburn Street well samplingProject Desc:
RLAB Approved Sample Analysis Results
Page 20 of 36
Analysis/ Analyte
Cyclohexane
1,2-Dibromo-3-Chloropropane
Dibromochloromethane
1,2-Dibromoethane
1,2-Dichlorobenzene
1,3-Dichlorobenzene
1,4-Dichlorobenzene
Dichlorodifluoromethane
1,1-Dichloroethane
1,2-Dichloroethane
1,1-Dichloroethene
cis-1,2-Dichloroethene
trans-1,2-Dichloroethene
1,2-Dichloropropane
cis-1,3-Dichloropropene
trans-1,3-Dichloropropene
Ethyl Benzene
2-Hexanone
Isopropylbenzene
Methyl Acetate
Methyl tert-butyl ether
Methylcyclohexane
Methylene Chloride
4-Methyl-2-Pentanone
Naphthalene
Styrene
1,1,2,2-Tetrachloroethane
Tetrachloroethene
Toluene
1,2,3-Trichlorobenzene
1,2,4-Trichlorobenzene
1,1,1-Trichloroethane
1,1,2-Trichloroethane
Trichloroethene
Trichlorofluoromethane
1,1,2-Trichlorotrifluoroethane
Vinyl Chloride
m and/or p-Xylene
o-Xylene
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
Units 19-__ 22-__ 22-FD 24-FB
5.0 UJ 5000 UJ 5000 UJ 5.0 U
5.0 U 5000 U 5000 U 5.0 U
5.0 U 5000 UJ 5000 UJ 5.0 U
5.0 UJ 5000 UJ 5000 UJ 5.0 U
5.0 U 5000 U 5000 U 5.0 U
5.0 U 5000 U 5000 U 5.0 U
5.0 U 5000 U 5000 U 5.0 U
5.0 U 5000 U 5000 U 5.0 U
5.0 U 5000 UJ 5000 UJ 5.0 U
5.0 U 5000 U 5000 U 5.0 U
5.0 U 5000 U 5000 U 5.0 U
5.0 U 5000 U 5000 U 5.0 U
5.0 U 5000 U 5000 U 5.0 U
5.0 U 5000 UJ 5000 UJ 5.0 U
5.0 UJ 5000 UJ 5000 UJ 5.0 U
5.0 U 5000 UJ 5000 UJ 5.0 U
5.0 U 5000 U 5000 U 5.0 U
5.0 U 5000 UJ 5000 UJ 5.0 UJ
5.0 U 5000 U 5000 U 5.0 U
5.0 U 5000 U 5000 U 5.0 U
10 U 10000 U 10000 U 10 U
5.0 U 5000 U 5000 U 5.0 U
5.0 U 5000 U 5000 U 5.0 U
5.0 U 5000 U 5000 U 5.0 U
10 U 10000 U 10000 U 10 U
5.0 U 5000 U 5000 U 5.0 U
5.0 U 5000 U 5000 U 5.0 U
2100 5000 U 5000 U 5.0 U
5.0 U 5000 U 5000 U 5.0 U
5.0 U 5000 U 5000 U 5.0 U
5.0 U 5000 U 5000 U 5.0 U
5.0 UJ 5000 UJ 5000 UJ 5.0 U
5.0 U 5000 U 5000 U 5.0 U
370 5000 U 5000 U 5.0 U
5.0 U 5000 U 5000 U 5.0 U
5.0 UJ 5000 UJ 5000 UJ 5.0 U
5.0 U 5000 U 5000 U 5.0 U
10 U 10000 U 10000 U 10 U
5.0 U 5000 U 5000 U 5.0 U
4981ASR Number: 09/16/2010
MP7ES02Project ID: Cleburn Street well samplingProject Desc:
RLAB Approved Sample Analysis Results
Page 21 of 36
1 VOCs in Water by GC/MS
Analysis/ Analyte
Acetone
Benzene
Bromodichloromethane
Bromoform
Bromomethane
2-Butanone
Carbon Disulfide
Carbon Tetrachloride
Chlorobenzene
Chloroethane
Chloroform
Chloromethane
Cyclohexane
1,2-Dibromo-3-Chloropropane
Dibromochloromethane
1,2-Dibromoethane
1,2-Dichlorobenzene
1,3-Dichlorobenzene
1,4-Dichlorobenzene
Dichlorodifluoromethane
1,1-Dichloroethane
1,2-Dichloroethane
1,1-Dichloroethene
cis-1,2-Dichloroethene
trans-1,2-Dichloroethene
1,2-Dichloropropane
cis-1,3-Dichloropropene
trans-1,3-Dichloropropene
Ethyl Benzene
2-Hexanone
Isopropylbenzene
Methyl Acetate
Methyl tert-butyl ether
Methylcyclohexane
Methylene Chloride
4-Methyl-2-Pentanone
Naphthalene
Styrene
1,1,2,2-Tetrachloroethane
Tetrachloroethene
Toluene
1,2,3-Trichlorobenzene
1,2,4-Trichlorobenzene
1,1,1-Trichloroethane
1,1,2-Trichloroethane
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
Units 25-__ 26-__ 27-__ 28-__
5.0 UJ 2500 U 5.0 UJ 5.0 UJ
5.0 U 2500 U 5.0 U 5.0 U
5.0 U 2500 U 5.0 U 5.0 U
5.0 U 2500 UJ 5.0 U 5.0 U
5.0 U 2500 U 5.0 U 5.0 U
5.0 UJ 2500 UJ 5.0 UJ 5.0 UJ
5.0 U 2500 U 5.0 U 5.0 U
5.0 UJ 2500 UJ 5.0 UJ 5.0 UJ
5.0 U 2500 U 5.0 U 5.0 U
5.0 U 2500 U 5.0 U 5.0 U
5.0 U 2500 U 5.0 U 5.0 U
5.0 U 2500 U 5.0 U 5.0 U
5.0 U 2500 UJ 5.0 U 5.0 U
5.0 U 2500 U 5.0 U 5.0 U
5.0 U 2500 UJ 5.0 U 5.0 U
5.0 U 2500 UJ 5.0 U 5.0 U
5.0 U 2500 U 5.0 U 5.0 U
5.0 U 2500 U 5.0 U 5.0 U
5.0 U 2500 U 5.0 U 5.0 U
5.0 U 2500 U 5.0 U 5.0 U
5.0 U 2500 UJ 5.0 U 5.0 U
5.0 U 2500 U 5.0 U 5.0 U
5.0 U 2500 U 5.0 U 5.0 U
5.0 U 2500 U 5.0 U 5.0 U
5.0 U 2500 U 5.0 U 5.0 U
5.0 U 2500 UJ 5.0 U 5.0 U
5.0 U 2500 UJ 5.0 U 5.0 U
5.0 U 2500 UJ 5.0 U 5.0 U
5.0 U 2500 U 5.0 U 5.0 U
5.0 UJ 2500 UJ 5.0 UJ 5.0 UJ
5.0 U 2500 U 5.0 U 5.0 U
5.0 U 2500 U 5.0 U 5.0 U
10 U 5000 U 10 U 10 U
5.0 U 2500 U 5.0 U 5.0 U
5.0 U 2500 U 5.0 U 5.0 U
5.0 U 2500 U 5.0 U 5.0 U
10 U 5000 U 10 U 10 U
5.0 U 2500 U 5.0 U 5.0 U
5.0 U 2500 U 5.0 U 5.0 U
5.0 U 2500 U 5.0 U 5.0 U
5.0 U 2500 U 5.0 U 5.0 U
5.0 U 2500 U 5.0 U 5.0 U
5.0 U 2500 U 5.0 U 5.0 U
5.0 U 2500 UJ 5.0 U 5.0 U
5.0 U 2500 U 5.0 U 5.0 U
4981ASR Number: 09/16/2010
MP7ES02Project ID: Cleburn Street well samplingProject Desc:
RLAB Approved Sample Analysis Results
Page 22 of 36
Analysis/ Analyte
Trichloroethene
Trichlorofluoromethane
1,1,2-Trichlorotrifluoroethane
Vinyl Chloride
m and/or p-Xylene
o-Xylene
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
Units 25-__ 26-__ 27-__ 28-__
5.0 U 2500 U 5.0 U 5.0 U
5.0 U 2500 U 5.0 U 5.0 U
5.0 U 2500 UJ 5.0 U 5.0 U
5.0 U 2500 U 5.0 U 5.0 U
10 U 5000 U 10 U 10 U
5.0 U 2500 U 5.0 U 5.0 U
4981ASR Number: 09/16/2010
MP7ES02Project ID: Cleburn Street well samplingProject Desc:
RLAB Approved Sample Analysis Results
Page 23 of 36
1 VOCs in Water by GC/MS
Analysis/ Analyte
Acetone
Benzene
Bromodichloromethane
Bromoform
Bromomethane
2-Butanone
Carbon Disulfide
Carbon Tetrachloride
Chlorobenzene
Chloroethane
Chloroform
Chloromethane
Cyclohexane
1,2-Dibromo-3-Chloropropane
Dibromochloromethane
1,2-Dibromoethane
1,2-Dichlorobenzene
1,3-Dichlorobenzene
1,4-Dichlorobenzene
Dichlorodifluoromethane
1,1-Dichloroethane
1,2-Dichloroethane
1,1-Dichloroethene
cis-1,2-Dichloroethene
trans-1,2-Dichloroethene
1,2-Dichloropropane
cis-1,3-Dichloropropene
trans-1,3-Dichloropropene
Ethyl Benzene
2-Hexanone
Isopropylbenzene
Methyl Acetate
Methyl tert-butyl ether
Methylcyclohexane
Methylene Chloride
4-Methyl-2-Pentanone
Naphthalene
Styrene
1,1,2,2-Tetrachloroethane
Tetrachloroethene
Toluene
1,2,3-Trichlorobenzene
1,2,4-Trichlorobenzene
1,1,1-Trichloroethane
1,1,2-Trichloroethane
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
Units 29-__ 30-__ 31-__ 32-__
5.0 UJ 5.0 UJ 5.0 UJ 5.0 UJ
5.0 U 5.0 U 5.0 U 5.0 U
5.0 U 5.0 U 5.0 U 5.0 U
5.0 U 5.0 U 5.0 U 5.0 U
5.0 U 5.0 U 5.0 U 5.0 U
5.0 UJ 5.0 UJ 5.0 UJ 5.0 UJ
5.0 U 5.0 U 5.0 U 5.0 U
5.0 UJ 5.0 UJ 5.0 UJ 5.0 UJ
5.0 U 5.0 U 5.0 U 5.0 U
5.0 U 5.0 U 5.0 U 5.0 U
5.0 U 5.0 U 5.0 U 5.0 U
5.0 U 5.0 U 5.0 U 5.0 U
5.0 U 5.0 U 5.0 U 5.0 U
5.0 U 5.0 U 5.0 U 5.0 U
5.0 U 5.0 U 5.0 U 5.0 U
5.0 U 5.0 U 5.0 U 5.0 U
5.0 U 5.0 U 5.0 U 5.0 U
5.0 U 5.0 U 5.0 U 5.0 U
5.0 U 5.0 U 5.0 U 5.0 U
5.0 U 5.0 U 5.0 U 5.0 U
5.0 U 5.0 U 5.0 U 5.0 U
5.0 U 5.0 U 5.0 U 5.0 U
5.0 U 5.0 U 5.0 U 5.0 U
5.0 U 5.0 U 5.0 U 5.0 U
5.0 U 5.0 U 5.0 U 5.0 U
5.0 U 5.0 U 5.0 U 5.0 U
5.0 U 5.0 U 5.0 U 5.0 U
5.0 U 5.0 U 5.0 U 5.0 U
5.0 U 5.0 U 5.0 U 5.0 U
5.0 UJ 5.0 UJ 5.0 UJ 5.0 UJ
5.0 U 5.0 U 5.0 U 5.0 U
5.0 U 5.0 U 5.0 U 5.0 U
10 U 10 U 10 U 10 U
5.0 U 5.0 U 5.0 U 5.0 U
5.0 U 5.0 U 5.0 U 5.0 U
5.0 U 5.0 U 5.0 U 5.0 U
10 U 10 U 10 U 10 U
5.0 U 5.0 U 5.0 U 5.0 U
5.0 U 5.0 U 5.0 U 5.0 U
16 5.0 U 5.0 U 5.0 U
5.0 U 5.0 U 5.0 U 5.0 U
5.0 U 5.0 U 5.0 U 5.0 U
5.0 U 5.0 U 5.0 U 5.0 U
5.0 U 5.0 U 5.0 U 5.0 U
5.0 U 5.0 U 5.0 U 5.0 U
4981ASR Number: 09/16/2010
MP7ES02Project ID: Cleburn Street well samplingProject Desc:
RLAB Approved Sample Analysis Results
Page 24 of 36
Analysis/ Analyte
Trichloroethene
Trichlorofluoromethane
1,1,2-Trichlorotrifluoroethane
Vinyl Chloride
m and/or p-Xylene
o-Xylene
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
Units 29-__ 30-__ 31-__ 32-__
5.0 U 5.0 U 5.0 U 5.0 U
5.0 U 5.0 U 5.0 U 5.0 U
5.0 U 5.0 U 5.0 U 5.0 U
5.0 U 5.0 U 5.0 U 5.0 U
10 U 10 U 10 U 10 U
5.0 U 5.0 U 5.0 U 5.0 U
4981ASR Number: 09/16/2010
MP7ES02Project ID: Cleburn Street well samplingProject Desc:
RLAB Approved Sample Analysis Results
Page 25 of 36
1 VOCs in Water by GC/MS
Analysis/ Analyte
Acetone
Benzene
Bromodichloromethane
Bromoform
Bromomethane
2-Butanone
Carbon Disulfide
Carbon Tetrachloride
Chlorobenzene
Chloroethane
Chloroform
Chloromethane
Cyclohexane
1,2-Dibromo-3-Chloropropane
Dibromochloromethane
1,2-Dibromoethane
1,2-Dichlorobenzene
1,3-Dichlorobenzene
1,4-Dichlorobenzene
Dichlorodifluoromethane
1,1-Dichloroethane
1,2-Dichloroethane
1,1-Dichloroethene
cis-1,2-Dichloroethene
trans-1,2-Dichloroethene
1,2-Dichloropropane
cis-1,3-Dichloropropene
trans-1,3-Dichloropropene
Ethyl Benzene
2-Hexanone
Isopropylbenzene
Methyl Acetate
Methyl tert-butyl ether
Methylcyclohexane
Methylene Chloride
4-Methyl-2-Pentanone
Naphthalene
Styrene
1,1,2,2-Tetrachloroethane
Tetrachloroethene
Toluene
1,2,3-Trichlorobenzene
1,2,4-Trichlorobenzene
1,1,1-Trichloroethane
1,1,2-Trichloroethane
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
Units 32-FD 34-__ 35-__ 35-FD
5.0 UJ 5.0 UJ 5.0 UJ 5.0 UJ
5.0 U 5.0 U 5.0 U 5.0 U
5.0 U 5.0 U 5.0 U 5.0 U
5.0 U 5.0 U 5.0 U 5.0 U
5.0 U 5.0 U 5.0 U 5.0 U
5.0 UJ 5.0 UJ 5.0 UJ 5.0 UJ
5.0 U 5.0 U 5.0 U 5.0 U
5.0 UJ 5.0 UJ 5.0 UJ 5.0 UJ
5.0 U 5.0 U 5.0 U 5.0 U
5.0 U 5.0 U 5.0 U 5.0 U
5.0 U 5.0 U 5.0 U 5.0 U
5.0 U 5.0 U 5.0 U 5.0 U
5.0 U 5.0 U 5.0 U 5.0 U
5.0 U 5.0 U 5.0 U 5.0 U
5.0 U 5.0 U 5.0 U 5.0 U
5.0 U 5.0 U 5.0 U 5.0 U
5.0 U 5.0 U 5.0 U 5.0 U
5.0 U 5.0 U 5.0 U 5.0 U
5.0 U 5.0 U 5.0 U 5.0 U
5.0 U 5.0 U 5.0 U 5.0 U
5.0 U 5.0 U 5.0 U 5.0 U
5.0 U 5.0 U 5.0 U 5.0 U
5.0 U 5.0 U 5.0 U 5.0 U
5.0 U 5.0 U 5.0 U 5.0 U
5.0 U 5.0 U 5.0 U 5.0 U
5.0 U 5.0 U 5.0 U 5.0 U
5.0 U 5.0 U 5.0 U 5.0 U
5.0 U 5.0 U 5.0 U 5.0 U
5.0 U 5.0 U 5.0 U 5.0 U
5.0 UJ 5.0 UJ 5.0 UJ 5.0 UJ
5.0 U 5.0 U 5.0 U 5.0 U
5.0 U 5.0 U 5.0 U 5.0 U
10 U 10 U 10 U 10 U
5.0 U 5.0 U 5.0 U 5.0 U
5.0 U 5.0 U 5.0 U 5.0 U
5.0 U 5.0 U 5.0 U 5.0 U
10 U 10 U 10 U 10 U
5.0 U 5.0 U 5.0 U 5.0 U
5.0 U 5.0 U 5.0 U 5.0 U
5.0 U 5.0 U 5.0 U 5.0 U
5.0 U 5.0 U 5.0 U 5.0 U
5.0 U 5.0 U 5.0 U 5.0 U
5.0 U 5.0 U 5.0 U 5.0 U
5.0 U 5.0 U 5.0 U 5.0 U
5.0 U 5.0 U 5.0 U 5.0 U
4981ASR Number: 09/16/2010
MP7ES02Project ID: Cleburn Street well samplingProject Desc:
RLAB Approved Sample Analysis Results
Page 26 of 36
Analysis/ Analyte
Trichloroethene
Trichlorofluoromethane
1,1,2-Trichlorotrifluoroethane
Vinyl Chloride
m and/or p-Xylene
o-Xylene
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
Units 32-FD 34-__ 35-__ 35-FD
5.0 U 5.0 U 5.0 U 5.0 U
5.0 U 5.0 U 5.0 U 5.0 U
5.0 U 5.0 U 5.0 U 5.0 U
5.0 U 5.0 U 5.0 U 5.0 U
10 U 10 U 10 U 10 U
5.0 U 5.0 U 5.0 U 5.0 U
4981ASR Number: 09/16/2010
MP7ES02Project ID: Cleburn Street well samplingProject Desc:
RLAB Approved Sample Analysis Results
Page 27 of 36
1 VOCs in Water by GC/MS
Analysis/ Analyte
Acetone
Benzene
Bromodichloromethane
Bromoform
Bromomethane
2-Butanone
Carbon Disulfide
Carbon Tetrachloride
Chlorobenzene
Chloroethane
Chloroform
Chloromethane
Cyclohexane
1,2-Dibromo-3-Chloropropane
Dibromochloromethane
1,2-Dibromoethane
1,2-Dichlorobenzene
1,3-Dichlorobenzene
1,4-Dichlorobenzene
Dichlorodifluoromethane
1,1-Dichloroethane
1,2-Dichloroethane
1,1-Dichloroethene
cis-1,2-Dichloroethene
trans-1,2-Dichloroethene
1,2-Dichloropropane
cis-1,3-Dichloropropene
trans-1,3-Dichloropropene
Ethyl Benzene
2-Hexanone
Isopropylbenzene
Methyl Acetate
Methyl tert-butyl ether
Methylcyclohexane
Methylene Chloride
4-Methyl-2-Pentanone
Naphthalene
Styrene
1,1,2,2-Tetrachloroethane
Tetrachloroethene
Toluene
1,2,3-Trichlorobenzene
1,2,4-Trichlorobenzene
1,1,1-Trichloroethane
1,1,2-Trichloroethane
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
Units 37-__ 38-__ 39-__ 40-__
5.0 UJ 5.0 UJ 5.0 UJ 5.0 UJ
5.0 U 5.0 U 5.0 U 5.0 U
5.0 U 5.0 U 5.0 U 5.0 U
5.0 U 5.0 U 5.0 U 5.0 U
5.0 U 5.0 U 5.0 U 5.0 U
5.0 UJ 5.0 UJ 5.0 UJ 5.0 UJ
5.0 U 5.0 U 5.0 U 5.0 U
5.0 UJ 5.0 UJ 5.0 UJ 5.0 UJ
5.0 U 5.0 U 5.0 U 5.0 U
5.0 U 5.0 U 5.0 U 5.0 U
5.0 U 5.0 U 5.0 U 5.0 U
5.0 U 5.0 U 5.0 U 5.0 U
5.0 U 5.0 U 5.0 U 5.0 U
5.0 U 5.0 U 5.0 U 5.0 U
5.0 U 5.0 U 5.0 U 5.0 U
5.0 U 5.0 U 5.0 U 5.0 U
5.0 U 5.0 U 5.0 U 5.0 U
5.0 U 5.0 U 5.0 U 5.0 U
5.0 U 5.0 U 5.0 U 5.0 U
5.0 U 5.0 U 5.0 U 5.0 U
5.0 U 5.0 U 5.0 U 5.0 U
5.0 U 5.0 U 5.0 U 5.0 U
5.0 U 5.0 U 5.0 U 5.0 U
5.0 U 5.0 U 5.0 U 5.0 U
5.0 U 5.0 U 5.0 U 5.0 U
5.0 U 5.0 U 5.0 U 5.0 U
5.0 U 5.0 U 5.0 U 5.0 U
5.0 U 5.0 U 5.0 U 5.0 U
5.0 U 5.0 U 5.0 U 5.0 U
5.0 UJ 5.0 UJ 5.0 UJ 5.0 UJ
5.0 U 5.0 U 5.0 U 5.0 U
5.0 U 5.0 U 5.0 U 5.0 U
10 U 10 U 10 U 10 U
5.0 U 5.0 U 5.0 U 5.0 U
5.0 U 5.0 U 5.0 U 5.0 U
5.0 U 5.0 U 5.0 U 5.0 U
10 U 10 U 10 U 10 U
5.0 U 5.0 U 5.0 U 5.0 U
5.0 U 5.0 U 5.0 U 5.0 U
5.0 U 5.0 U 5.0 U 5.0 U
5.0 U 5.0 U 5.0 U 5.0 U
5.0 U 5.0 U 5.0 U 5.0 U
5.0 U 5.0 U 5.0 U 5.0 U
5.0 U 5.0 U 5.0 U 5.0 U
5.0 U 5.0 U 5.0 U 5.0 U
4981ASR Number: 09/16/2010
MP7ES02Project ID: Cleburn Street well samplingProject Desc:
RLAB Approved Sample Analysis Results
Page 28 of 36
Analysis/ Analyte
Trichloroethene
Trichlorofluoromethane
1,1,2-Trichlorotrifluoroethane
Vinyl Chloride
m and/or p-Xylene
o-Xylene
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
Units 37-__ 38-__ 39-__ 40-__
5.0 U 5.0 U 5.0 U 5.0 U
5.0 U 5.0 U 5.0 U 5.0 U
5.0 U 5.0 U 5.0 U 5.0 U
5.0 U 5.0 U 5.0 U 5.0 U
10 U 10 U 10 U 10 U
5.0 U 5.0 U 5.0 U 5.0 U
4981ASR Number: 09/16/2010
MP7ES02Project ID: Cleburn Street well samplingProject Desc:
RLAB Approved Sample Analysis Results
Page 29 of 36
1 VOCs in Water by GC/MS
Analysis/ Analyte
Acetone
Benzene
Bromodichloromethane
Bromoform
Bromomethane
2-Butanone
Carbon Disulfide
Carbon Tetrachloride
Chlorobenzene
Chloroethane
Chloroform
Chloromethane
Cyclohexane
1,2-Dibromo-3-Chloropropane
Dibromochloromethane
1,2-Dibromoethane
1,2-Dichlorobenzene
1,3-Dichlorobenzene
1,4-Dichlorobenzene
Dichlorodifluoromethane
1,1-Dichloroethane
1,2-Dichloroethane
1,1-Dichloroethene
cis-1,2-Dichloroethene
trans-1,2-Dichloroethene
1,2-Dichloropropane
cis-1,3-Dichloropropene
trans-1,3-Dichloropropene
Ethyl Benzene
2-Hexanone
Isopropylbenzene
Methyl Acetate
Methyl tert-butyl ether
Methylcyclohexane
Methylene Chloride
4-Methyl-2-Pentanone
Naphthalene
Styrene
1,1,2,2-Tetrachloroethane
Tetrachloroethene
Toluene
1,2,3-Trichlorobenzene
1,2,4-Trichlorobenzene
1,1,1-Trichloroethane
1,1,2-Trichloroethane
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
Units 41-__ 42-__ 43-__ 44-__
5.0 U 5.0 UJ 5.0 UJ 5.0 U
5.0 U 5.0 U 5.0 U 5.0 U
5.0 U 5.0 U 5.0 U 5.0 U
5.0 UJ 5.0 U 5.0 U 5.0 UJ
5.0 U 5.0 U 5.0 U 5.0 U
5.0 U 5.0 UJ 5.0 UJ 5.0 U
5.0 U 5.0 U 5.0 U 5.0 U
5.0 UJ 5.0 UJ 5.0 UJ 5.0 UJ
5.0 U 5.0 U 5.0 U 5.0 U
5.0 U 5.0 U 5.0 U 5.0 U
5.0 U 5.0 U 5.0 U 5.0 U
5.0 U 5.0 U 5.0 U 5.0 U
5.0 UJ 5.0 U 5.0 U 5.0 UJ
5.0 U 5.0 U 5.0 U 5.0 U
5.0 UJ 5.0 U 5.0 U 5.0 UJ
5.0 UJ 5.0 U 5.0 U 5.0 UJ
5.0 U 5.0 U 5.0 U 5.0 U
5.0 UJ 5.0 U 5.0 U 5.0 U
5.0 U 5.0 U 5.0 U 5.0 U
5.0 U 5.0 U 5.0 U 5.0 U
5.0 U 5.0 U 5.0 U 5.0 U
5.0 U 5.0 U 5.0 U 5.0 U
5.0 U 5.0 U 5.0 U 5.0 U
5.0 U 5.0 U 5.0 U 5.0 U
5.0 U 5.0 U 5.0 U 5.0 U
5.0 U 5.0 U 5.0 U 5.0 U
5.0 UJ 5.0 U 5.0 U 5.0 UJ
5.0 UJ 5.0 U 5.0 U 5.0 UJ
5.0 U 5.0 U 5.0 U 5.0 U
5.0 U 5.0 UJ 5.0 UJ 5.0 U
5.0 U 5.0 U 5.0 U 5.0 U
5.0 U 5.0 U 5.0 U 5.0 U
10 U 10 U 10 U 10 U
5.0 U 5.0 U 5.0 U 5.0 U
5.0 U 5.0 U 5.0 U 5.0 U
5.0 U 5.0 U 5.0 U 5.0 UJ
10 U 10 U 10 U 10 U
5.0 U 5.0 U 5.0 U 5.0 U
5.0 U 5.0 U 5.0 U 5.0 U
5.0 U 5.0 U 5.0 U 5.0 U
5.0 U 5.0 U 5.0 U 5.0 U
5.0 U 5.0 U 5.0 U 5.0 U
5.0 U 5.0 U 5.0 U 5.0 U
5.0 UJ 5.0 U 5.0 U 5.0 UJ
5.0 UJ 5.0 U 5.0 U 5.0 U
4981ASR Number: 09/16/2010
MP7ES02Project ID: Cleburn Street well samplingProject Desc:
RLAB Approved Sample Analysis Results
Page 30 of 36
Analysis/ Analyte
Trichloroethene
Trichlorofluoromethane
1,1,2-Trichlorotrifluoroethane
Vinyl Chloride
m and/or p-Xylene
o-Xylene
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
Units 41-__ 42-__ 43-__ 44-__
5.0 U 5.0 U 5.0 U 5.0 U
5.0 U 5.0 U 5.0 U 5.0 U
5.0 UJ 5.0 U 5.0 U 5.0 UJ
5.0 U 5.0 U 5.0 U 5.0 U
10 U 10 U 10 U 10 U
5.0 UJ 5.0 U 5.0 U 5.0 U
4981ASR Number: 09/16/2010
MP7ES02Project ID: Cleburn Street well samplingProject Desc:
RLAB Approved Sample Analysis Results
Page 31 of 36
1 VOCs in Water by GC/MS
Analysis/ Analyte
Acetone
Benzene
Bromodichloromethane
Bromoform
Bromomethane
2-Butanone
Carbon Disulfide
Carbon Tetrachloride
Chlorobenzene
Chloroethane
Chloroform
Chloromethane
Cyclohexane
1,2-Dibromo-3-Chloropropane
Dibromochloromethane
1,2-Dibromoethane
1,2-Dichlorobenzene
1,3-Dichlorobenzene
1,4-Dichlorobenzene
Dichlorodifluoromethane
1,1-Dichloroethane
1,2-Dichloroethane
1,1-Dichloroethene
cis-1,2-Dichloroethene
trans-1,2-Dichloroethene
1,2-Dichloropropane
cis-1,3-Dichloropropene
trans-1,3-Dichloropropene
Ethyl Benzene
2-Hexanone
Isopropylbenzene
Methyl Acetate
Methyl tert-butyl ether
Methylcyclohexane
Methylene Chloride
4-Methyl-2-Pentanone
Naphthalene
Styrene
1,1,2,2-Tetrachloroethane
Tetrachloroethene
Toluene
1,2,3-Trichlorobenzene
1,2,4-Trichlorobenzene
1,1,1-Trichloroethane
1,1,2-Trichloroethane
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
Units 45-__ 45-FD 47-__ 48-__
5.0 U 5.0 U 5.0 U 5.0 U
5.0 U 5.0 U 5.0 U 5.0 U
5.0 U 5.0 U 5.0 U 5.0 U
5.0 U 5.0 U 5.0 U 5.0 U
5.0 U 5.0 U 5.0 U 5.0 U
5.0 U 5.0 U 5.0 U 5.0 U
5.0 U 5.0 U 5.0 U 5.0 U
5.0 UJ 5.0 UJ 5.0 UJ 5.0 UJ
5.0 U 5.0 U 5.0 U 5.0 U
5.0 U 5.0 U 5.0 U 5.0 U
5.0 U 5.0 U 5.0 U 5.0 U
5.0 U 5.0 U 5.0 U 5.0 U
5.0 UJ 5.0 UJ 5.0 UJ 5.0 UJ
5.0 U 5.0 U 5.0 U 5.0 U
5.0 U 5.0 U 5.0 U 5.0 U
5.0 UJ 5.0 UJ 5.0 UJ 5.0 UJ
5.0 U 5.0 U 5.0 U 5.0 U
5.0 U 5.0 U 5.0 U 5.0 U
5.0 U 5.0 U 5.0 U 5.0 U
5.0 U 5.0 U 5.0 U 5.0 U
5.0 U 5.0 U 5.0 U 5.0 U
5.0 U 5.0 U 5.0 U 5.0 U
5.0 U 5.0 U 5.0 U 5.0 U
5.0 U 5.0 U 5.0 U 5.0 U
5.0 U 5.0 U 5.0 U 5.0 U
5.0 U 5.0 U 5.0 U 5.0 U
5.0 UJ 5.0 UJ 5.0 UJ 5.0 UJ
5.0 U 5.0 U 5.0 U 5.0 U
5.0 U 5.0 U 5.0 U 5.0 U
5.0 U 5.0 U 5.0 U 5.0 U
5.0 U 5.0 U 5.0 U 5.0 U
5.0 U 5.0 U 5.0 U 5.0 U
10 U 10 U 10 U 10 U
5.0 U 5.0 U 5.0 U 5.0 U
5.0 U 5.0 U 5.0 U 5.0 U
5.0 U 5.0 U 5.0 U 5.0 U
10 U 10 U 10 U 10 U
5.0 U 5.0 U 5.0 U 5.0 U
5.0 U 5.0 U 5.0 U 5.0 U
5.0 U 5.0 U 5.0 U 5.0 U
5.0 U 5.0 U 5.0 U 5.0 U
5.0 U 5.0 U 5.0 U 5.0 U
5.0 U 5.0 U 5.0 U 5.0 U
5.0 UJ 5.0 UJ 5.0 UJ 5.0 UJ
5.0 U 5.0 U 5.0 U 5.0 U
4981ASR Number: 09/16/2010
MP7ES02Project ID: Cleburn Street well samplingProject Desc:
RLAB Approved Sample Analysis Results
Page 32 of 36
Analysis/ Analyte
Trichloroethene
Trichlorofluoromethane
1,1,2-Trichlorotrifluoroethane
Vinyl Chloride
m and/or p-Xylene
o-Xylene
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
Units 45-__ 45-FD 47-__ 48-__
5.0 U 5.0 U 5.0 U 5.0 U
5.0 U 5.0 U 5.0 U 5.0 U
5.0 UJ 5.0 UJ 5.0 UJ 5.0 UJ
5.0 U 5.0 U 5.0 U 5.0 U
10 U 10 U 10 U 10 U
5.0 U 5.0 U 5.0 U 5.0 U
4981ASR Number: 09/16/2010
MP7ES02Project ID: Cleburn Street well samplingProject Desc:
RLAB Approved Sample Analysis Results
Page 33 of 36
1 VOCs in Water by GC/MS
Analysis/ Analyte
Acetone
Benzene
Bromodichloromethane
Bromoform
Bromomethane
2-Butanone
Carbon Disulfide
Carbon Tetrachloride
Chlorobenzene
Chloroethane
Chloroform
Chloromethane
Cyclohexane
1,2-Dibromo-3-Chloropropane
Dibromochloromethane
1,2-Dibromoethane
1,2-Dichlorobenzene
1,3-Dichlorobenzene
1,4-Dichlorobenzene
Dichlorodifluoromethane
1,1-Dichloroethane
1,2-Dichloroethane
1,1-Dichloroethene
cis-1,2-Dichloroethene
trans-1,2-Dichloroethene
1,2-Dichloropropane
cis-1,3-Dichloropropene
trans-1,3-Dichloropropene
Ethyl Benzene
2-Hexanone
Isopropylbenzene
Methyl Acetate
Methyl tert-butyl ether
Methylcyclohexane
Methylene Chloride
4-Methyl-2-Pentanone
Naphthalene
Styrene
1,1,2,2-Tetrachloroethane
Tetrachloroethene
Toluene
1,2,3-Trichlorobenzene
1,2,4-Trichlorobenzene
1,1,1-Trichloroethane
1,1,2-Trichloroethane
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
Units 49-__ 50-__ 53-FB 54-FB
5.0 U 5.0 U 5.0 UJ 5.0 UJ
5.0 U 5.0 U 5.0 U 5.0 U
5.0 U 5.0 U 5.0 U 5.0 U
5.0 U 5.0 U 5.0 U 5.0 U
5.0 U 5.0 U 5.0 U 5.0 U
5.0 U 5.0 U 5.0 UJ 5.0 UJ
5.0 U 5.0 U 5.0 U 5.0 U
5.0 UJ 5.0 UJ 5.0 UJ 5.0 UJ
5.0 U 5.0 U 5.0 U 5.0 U
5.0 U 5.0 U 5.0 U 5.0 U
5.0 U 5.0 U 5.0 U 5.0 U
5.0 U 5.0 U 5.0 U 5.0 U
5.0 UJ 5.0 UJ 5.0 U 5.0 U
5.0 U 5.0 U 5.0 U 5.0 U
5.0 U 5.0 U 5.0 U 5.0 U
5.0 UJ 5.0 UJ 5.0 U 5.0 U
5.0 U 5.0 U 5.0 U 5.0 U
5.0 U 5.0 U 5.0 U 5.0 U
5.0 U 5.0 U 5.0 U 5.0 U
5.0 U 5.0 U 5.0 U 5.0 U
5.0 U 5.0 U 5.0 U 5.0 U
5.0 U 5.0 U 5.0 U 5.0 U
5.0 U 5.0 U 5.0 U 5.0 U
5.0 U 5.0 U 5.0 U 5.0 U
5.0 U 5.0 U 5.0 U 5.0 U
5.0 U 5.0 U 5.0 U 5.0 U
5.0 UJ 5.0 UJ 5.0 U 5.0 U
5.0 U 5.0 U 5.0 U 5.0 U
5.0 U 5.0 U 5.0 U 5.0 U
5.0 U 5.0 U 5.0 UJ 5.0 UJ
5.0 U 5.0 U 5.0 U 5.0 U
5.0 U 5.0 U 5.0 U 5.0 U
10 U 10 U 10 U 10 U
5.0 U 5.0 U 5.0 U 5.0 U
5.0 U 5.0 U 5.0 U 5.0 U
5.0 U 5.0 U 5.0 U 5.0 U
10 U 10 U 10 U 10 U
5.0 U 5.0 U 5.0 U 5.0 U
5.0 U 5.0 U 5.0 U 5.0 U
5.6 5.0 U 5.0 U 5.0 U
5.0 U 5.0 U 5.0 U 5.0 U
5.0 U 5.0 U 5.0 U 5.0 U
5.0 U 5.0 U 5.0 U 5.0 U
5.0 UJ 5.0 UJ 5.0 U 5.0 U
5.0 U 5.0 U 5.0 U 5.0 U
4981ASR Number: 09/16/2010
MP7ES02Project ID: Cleburn Street well samplingProject Desc:
RLAB Approved Sample Analysis Results
Page 34 of 36
Analysis/ Analyte
Trichloroethene
Trichlorofluoromethane
1,1,2-Trichlorotrifluoroethane
Vinyl Chloride
m and/or p-Xylene
o-Xylene
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
Units 49-__ 50-__ 53-FB 54-FB
5.0 U 5.0 U 5.0 U 5.0 U
5.0 U 5.0 U 5.0 U 5.0 U
5.0 UJ 5.0 UJ 5.0 U 5.0 U
5.0 U 5.0 U 5.0 U 5.0 U
10 U 10 U 10 U 10 U
5.0 U 5.0 U 5.0 U 5.0 U
4981ASR Number: 09/16/2010
MP7ES02Project ID: Cleburn Street well samplingProject Desc:
RLAB Approved Sample Analysis Results
Page 35 of 36
1 VOCs in Water by GC/MS
Analysis/ Analyte
Acetone
Benzene
Bromodichloromethane
Bromoform
Bromomethane
2-Butanone
Carbon Disulfide
Carbon Tetrachloride
Chlorobenzene
Chloroethane
Chloroform
Chloromethane
Cyclohexane
1,2-Dibromo-3-Chloropropane
Dibromochloromethane
1,2-Dibromoethane
1,2-Dichlorobenzene
1,3-Dichlorobenzene
1,4-Dichlorobenzene
Dichlorodifluoromethane
1,1-Dichloroethane
1,2-Dichloroethane
1,1-Dichloroethene
cis-1,2-Dichloroethene
trans-1,2-Dichloroethene
1,2-Dichloropropane
cis-1,3-Dichloropropene
trans-1,3-Dichloropropene
Ethyl Benzene
2-Hexanone
Isopropylbenzene
Methyl Acetate
Methyl tert-butyl ether
Methylcyclohexane
Methylene Chloride
4-Methyl-2-Pentanone
Naphthalene
Styrene
1,1,2,2-Tetrachloroethane
Tetrachloroethene
Toluene
1,2,3-Trichlorobenzene
1,2,4-Trichlorobenzene
1,1,1-Trichloroethane
1,1,2-Trichloroethane
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
Units 55-FB
5.0 UJ
5.0 U
5.0 U
5.0 U
5.0 U
5.0 UJ
5.0 U
5.0 UJ
5.0 U
5.0 U
5.0 U
5.0 U
5.0 U
5.0 U
5.0 U
5.0 U
5.0 U
5.0 U
5.0 U
5.0 U
5.0 U
5.0 U
5.0 U
5.0 U
5.0 U
5.0 U
5.0 U
5.0 U
5.0 U
5.0 UJ
5.0 U
5.0 U
10 U
5.0 U
5.0 U
5.0 U
10 U
5.0 U
5.0 U
5.0 U
5.0 U
5.0 U
5.0 U
5.0 U
5.0 U
4981ASR Number: 09/16/2010
MP7ES02Project ID: Cleburn Street well samplingProject Desc:
RLAB Approved Sample Analysis Results
Page 36 of 36
Analysis/ Analyte
Trichloroethene
Trichlorofluoromethane
1,1,2-Trichlorotrifluoroethane
Vinyl Chloride
m and/or p-Xylene
o-Xylene
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
Units 55-FB
5.0 U
5.0 U
5.0 U
5.0 U
10 U
5.0 U
4981ASR Number: 09/16/2010
MP7ES02Project ID: Cleburn Street well samplingProject Desc:
RLAB Approved Sample Analysis Results
4981
MP7ES02Project ID:
Cleburn Street well sampling
Mary PetersonSUPR/IANE
United States Environmental Protection AgencyRegion VII
901 N. 5th StreetKansas City, KS 66101
__/__/____
Data Disposition/Sample Release for ASR #:
Project Description:
Subject:
Kaye DollmannENSV/RLAB
I have received and reviewed the Transmittal of Sample Analysis Results for the above-referencedAnalytical Services Request(ASR) and have indicated my findings below by checking one of theboxes for Data Disposition.
I understand all samples will be disposed upon receipt of this form, unless samples are requestedto be held. If I do not return this form all samples will be disposed of on ___________________.
"RELEASED" - Read-only to all Region 7 employees and contractors that have R7LIMS"Customer" account. All Samples may be disposed of upon receipt of this form if not requested tobe held.
"Project Manager Accessible" - Available on the LAN in R7LIMS for my use only. All Samples maybe disposed of upon receipt of this form if not requested to be held.
"Archived" - THIS DATA IS OF A SENSITIVE NATURE. Any future reports must be requestedthrough the laboratory. All samples may be disposed of upon receipt of the form if not requestedto be held.
Date:
From:
To:
Hold Samples - I have determined that the samples need to be held until ______________, afterwhich time they will be disposed of in accordance with applicable regulations. The reason for the hold is:
Samples are associated with a legal proceeding.
Question/Concern with data - possible reanalysis requested.
Other:________________________________________________________________
Page 1 of 18
09/07/2010Date:
4982
MP7ES02
Cleburn Street well sampling
Mary PetersonSUPR/IANE
Transmittal of Sample Analysis Results for ASR #:
Project ID:
Project Description:
Michael F. Davis, ChiefChemical Analysis and Response Branch, Environmental Services Division
To:
Enclosed are the analytical data for the above-referenced Analytical Services Request (ASR) andProject. The Regional Laboratory has reviewed and verified the results in accordance with proceduresdescribed in our Quality Manual (QM). In addition to all of the analytical results, this transmittalcontains pertinent information that may have influenced the reported results and documents anydeviations from the established requirements of the QM.
Please contact us within 14 days of receipt of this package if you determine there is a need for anychanges. Please complete the enclosed Customer Satisfaction Survey and Data Disposition/SampleRelease memo for this ASR as soon as possible. The process of disposing of the samples for this ASRwill be initiated 30 days from the date of this transmittal unless an alternate release date is specifiedon the Data Disposition/Sample Release memo.
If you have any questions or concerns relating to this data package, contact our customer service lineat 913-551-5295.
Enclosures
cc: Analytical Data File.
United States Environmental Protection AgencyRegion 7
901 N. 5th StreetKansas City, KS 66101
Subject:
From:
Page 2 of 18
4982ASR Number: 09/07/2010
Mary Peterson SUPR/IANE 913-551-7882
MP7ES02
Cleburn Street well sampling
Grand Island Nebraska Superfund
CLEBURN STREET WELL - 1 HR MARTINIZING GWRESORATION
07ESSite ID: 02
Site Cleanup Support
This EPA research/ascorbic acid ASR is in conjunction with ASR #4981.
VOA samples with permanganate will be preserved with ascorbic acid under this ASR. CARB and SUPR are currently developing the protocol to use the new preservative.
Project Manager: Org: Phone:
Project ID:
Project Desc:
Location: State: Program:
Site Name: Site OU:
Purpose:
__ = Field SampleFB = Field BlankFD = Field Duplicate
QC Codes identify the type of sample for quality control purpose.
Micrograms per Liter
Specific units in which results arereported.
The identification of the analyte is acceptable; the reported value is anestimate.The analyte was not detected at or above the reporting limit.The analyte was not detected at or above the reporting limit. The reportinglimit is an estimate.
Specific codes used in conjunction with data values to provide additional information on the quality of reported results, or used to explain the absence of a specific value.
Summary of Project Information
Explanation of Codes, Units and Qualifiers used on this report
Sample QC Codes: Units:
J
UUJ
=
==
Data Qualifiers:
= Values have been reviewed and found acceptable for use. (Blank)
ug/L =
2009073QAPP Number:
302DD2CGPRA PRC:
Page 3 of 18
102
103
104
104
105
106
107
108
109
110
110
111
112
113
114
115
116
117
122
122
124
126
153
SampleNo
__
__
__
FD
__
__
__
__
__
__
FD
__
__
__
__
__
__
__
__
FD
FB
__
FB
QCCode
Water
Water
Water
Water
Water
Water
Water
Water
Water
Water
Water
Water
Water
Water
Water
Water
Water
Water
Water
Water
Water
Water
Water
Matrix
ERT-15
IW-2
IW-1
IW-1/Field Duplicate of sample104IW-4
IW-5
IW-6
IW-7
IW-9
IW-3
IW-3
IW-10
ERT-16
DPE-1
DPE-2
DPE-3
DPE-4
MW-2A
IW-8
IW-8/Field Duplicate of sample122Preservative Blank prepared byHGL w/EPA DI waterMW-102-AA
Method Blank Trip Blank sampleprepared by EPA
Location DescriptionExternal
Sample No
07/26/2010
07/27/2010
07/27/2010
07/27/2010
07/27/2010
07/27/2010
07/27/2010
07/27/2010
07/28/2010
07/27/2010
07/27/2010
07/28/2010
07/28/2010
07/28/2010
07/29/2010
07/29/2010
07/29/2010
07/29/2010
07/28/2010
07/28/2010
07/26/2010
07/30/2010
07/26/2010
Start Date
16:25
10:40
09:20
09:20
13:00
14:25
15:25
18:35
12:45
11:40
11:40
14:40
16:20
17:55
09:10
10:35
12:00
13:45
10:15
10:15
12:15
10:15
12:00
Start Time
End Date
End Time
07/27/2010
07/28/2010
07/28/2010
07/28/2010
07/28/2010
07/28/2010
07/28/2010
07/29/2010
07/29/2010
07/28/2010
07/28/2010
07/29/2010
07/29/2010
07/30/2010
07/30/2010
07/30/2010
07/30/2010
07/30/2010
07/29/2010
07/29/2010
07/27/2010
08/03/2010
07/27/2010
ReceiptDate
4982 09/07/2010
MP7ES02Project ID: Cleburn Street well samplingProject Desc:
ASR Number: Sample Information Summary
-
-
-
-
-
-
-
-
-
-
-
-
-
-
-
-
-
-
-
-
-
-
-
Page 4 of 18
1 VOCs in Water by GC/MS
Region 7 EPA Laboratory - Kansas City, Ks.Lab:
EPA Region 7 RLAB Method 3230.1FMethod:
Permanganate and/or Ascorbic Acid in the samples caused significant interference with theanalysis, with Internal Standards and Surrogates having lowered response. This requiredseveral dilutions to analyze the samples. Many samples could not be rerun due to lack ofsample volume, and have been reported with the lowest reporting limit available.
Samples 104FD, 105-109, 111-115, 122, 122FD, 124FB and 153FB were diluted to reduceinterference from Ascorbic Acid in the sample vials. They have been reported at a dilutionof 4X with a raised reporting limit.
Samples 110, 110FD, 116 and 126 were diluted to reduce interference from Ascorbic Acidin the sample vials. They have been reported at a dilution of 10X with a raised reportinglimit.
Samples 117 was diluted to reduce interference from Ascorbic Acid in the sample vial andto capture the high Tetrachloroethene value. It has been reported at a dilution of 20X witha raised reporting limit.
Sample 103 required a 10x dilution for Tetrachloroethene.
Sample 106 required a 500X dilution for Tetrachloroethene.
Samples 112 required a 20X dilution for Tetrachloroethene.
Samples 122 and 122FD required a 100X dilution for Tetrachloroethene.
Carbon Tetrachloride was over the calibration range in sample 108. This compound hasbeen J-coded to indicate that it is an estimate. The value calculated is within the expectedlinear range of the curve, so data should be usable for its intended purpose.
Tetrachloroethene was over the calibration range in samples 109 and 111. This compoundhas been J-coded to indicate that it is an estimate, and may be higher than the reportedvalues.
Due to permanganate/ascorbic acid issues, and repeated analyses, there was not sufficientsample volume to perform the required matrix spikes and spike duplicates. One matrixspike was performed, and one lab duplicate was reported.
Acid preservation was buffered by the addition of Ascorbic acid. Almost all samples werebetween a pH of 2 and 4. The presence of the Ascorbic Acid has been shown to preserve
Comments:
102-__ 103-__ 104-__ 104-FD 105-__ 106-__ 107-__108-__ 109-__ 110-__ 110-FD 111-__ 112-__ 113-__114-__ 115-__ 116-__ 117-__ 122-__ 122-FD 124-FB126-__ 153-FB
Samples:
4982ASR Number: 09/07/2010
MP7ES02Project ID: Cleburn Street well samplingProject Desc
RLAB Approved Analysis Comments
Analysis Comments About Results For This Analysis
Page 5 of 18
the analytes in the samples better than the addition of acid alone, as the presence ofpermanganate tends to have a negative effect on the analytes of interest.
Methyl Acetate was UJ-coded in samples 102, 103, 104 110FD, 108, 109, 111, 112, 113,114, 115, 122, 122FD, 124FB, 153FB. This analyte was not found in the samples at orabove the reporting limit, however, the reporting limit is an estimate (UJ-coded) due to thecontinuing calibration check not meeting accuracy specifications. The actual reporting limitfor this analyte may be higher than the reported value.
Dichlorodifluoromethane, Chloromethane, Chloroethane and Cyclohexane were UJ-coded insamples 102, 103 and 104. These analytes were not found in the samples at or above thereporting limit, however, the reporting limit is an estimate (UJ-coded) due to thecontinuing calibration check not meeting accuracy specifications. The actual reporting limitfor these analytes may be higher than the reported value.
Acetone was J-coded in samples 102, 103, 104, 110FD, 108, 109, 111, 112, 113, 114, 115,122, 122FD and 153FB, and UJ-coded in 124FB. The reporting limit, or quantitation is anestimate (J-coded, UJ-coded for 124FB) due to the continuing calibration check not meetingaccuracy specifications. The actual concentration for this analyte may be different than thereported values. Acetone also had poor precision in samples 103 and 103LD.
2-Butanone and 2-Hexanone were UJ-coded in samples 110FD, 108, 109, 111, 112, 113,114, 115, 122, 122FD, 124FB and 153FB. Theses analytes were not found in the samplesat or above the reporting limit, however, the reporting limit is an estimate (UJ-coded) dueto the continuing calibration check not meeting accuracy specifications. The actualreporting limit for these analytes may be higher than the reported value.
Benzene and 1,2-Dichloropropane were UJ-coded in samples 102, 103, 104. Theseanalytes was not found in the samples at or above the reporting limit, however, thereporting limit is an estimate (UJ-coded) due to low recovery of these analytes in thelaboratory control sample. The actual reporting limit for these analytes may be higher thanthe reported value.
Bromoform, 1,2-Dibromo-3-Chloropropane, Dibromochloromethane, 1,2-Dibromoethane,trans-1,3-Dichloropropene, 2-Hexanone, 4-Methyl-2-Pentanone, Naphthalene, 1,1,2,2-Tetrachloroethane, 1,2,3-Trichlorobenzene and 1,1,2-Trichloroethane were UJ-coded insample 102. These analytes were not found in the sample at or above the reporting limit,however, the reporting limit is an estimate (UJ-coded) due to low recovery of this analytein the laboratory matrix spike, most likely due to the presence of Permanganate. Theactual reporting limit for this analyte may be higher than the reported value.
Sample 104 had all analytes associated with the internal standards Bromochloromethaneand Chlorobenzene-D5, and the surrogate 4-Bromofluorobenzene UJ-coded due to lowrecovery in the sample. These analytes include: Dichlorodifluoromethane, Chloromethane,Vinyl Chloride, Bromomethane, Chloroethane, Trichlorfluoromethane, 1,1,2-Trichlorotrifluoroethane, Methylene Chloride, Carbon Disulfide, 1,1-Dichloroethene, MethylAcetate, Methyl tert-butyl Ether, 1,1-Dichloroethane, trans-1,2-Dichloroethene, Chloroform,cis-1,2-Dichloroethene, 1,1,1-Trichloroethane, Carbon tetrachloride, 2-Butanone,Cyclohexane, 1,2-Dibromoethane, 1,3-Dichlorobenzene, 1,2-Dichlorobenzene,
4982ASR Number: 09/07/2010
MP7ES02Project ID: Cleburn Street well samplingProject Desc
RLAB Approved Analysis Comments
Analysis Comments About Results For This Analysis
Page 6 of 18
Isopropylbenzene, Dibromochloromethane, 1,1,2,2,-Tetrachloroethane, Chlorobenzene,Ethyl Benzene, Styrene, m- and/or p-Xylene, 1,2,3-Trichlorobenzene, 1,2,4-Trichlorobenzene, o-Xylene, Bromoform, 1,4-Dichlorobenzene, Naphthalene, trans-1,3-Dichloropropene, 2-Hexanone, 1,1,2-Trichloroethane, and 1,2-Dibromo-3-Chloropropane.Acetone and Tetrachloroethene were J-coded.
In sample 115, the compounds associated with the Internal StandardBromochloromethane: Dichlorodifluoromethane, Vinyl Chloride, Bromomethane,Chloroethane, Chloromethane, Trichlorfluoromethane, 1,1,2-Trichlorotrifluoroethane,Methylene Chloride, , Carbon Disulfide, 1,1-Dichloroethene, Methyl Acetate, Methyl tert-butyl Ether, 1,1-Dichloroethane, trans-1,2-dichloroethene, , cis-1,2-Dichloroethene, 2-Butanone, and Cyclohexane, were UJ-coded in this sample, while Chloroform, Acetone,1,1,1-Trichloroethane and Carbon tetrachloride were J-coded, due to low area response.
4982ASR Number: 09/07/2010
MP7ES02Project ID: Cleburn Street well samplingProject Desc
RLAB Approved Analysis Comments
Analysis Comments About Results For This Analysis
Page 7 of 18
1 VOCs in Water by GC/MS
Analysis/ Analyte
Acetone
Benzene
Bromodichloromethane
Bromoform
Bromomethane
2-Butanone
Carbon Disulfide
Carbon Tetrachloride
Chlorobenzene
Chloroethane
Chloroform
Chloromethane
Cyclohexane
1,2-Dibromo-3-Chloropropane
Dibromochloromethane
1,2-Dibromoethane
1,2-Dichlorobenzene
1,3-Dichlorobenzene
1,4-Dichlorobenzene
Dichlorodifluoromethane
1,1-Dichloroethane
1,2-Dichloroethane
1,1-Dichloroethene
cis-1,2-Dichloroethene
trans-1,2-Dichloroethene
1,2-Dichloropropane
cis-1,3-Dichloropropene
trans-1,3-Dichloropropene
Ethyl Benzene
2-Hexanone
Isopropylbenzene
Methyl Acetate
Methyl tert-butyl ether
Methylcyclohexane
Methylene Chloride
4-Methyl-2-Pentanone
Naphthalene
Styrene
1,1,2,2-Tetrachloroethane
Tetrachloroethene
Toluene
1,2,3-Trichlorobenzene
1,2,4-Trichlorobenzene
1,1,1-Trichloroethane
1,1,2-Trichloroethane
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
Units 102-__ 103-__ 104-__ 104-FD
9.0 J 39 J 15 J 32
5.0 UJ 5.0 UJ 5.0 UJ 20 U
5.0 U 5.0 U 5.0 U 20 U
5.0 UJ 5.0 U 5.0 UJ 20 U
5.0 U 5.0 U 5.0 UJ 20 U
5.0 U 5.0 U 5.0 UJ 20 U
5.0 U 5.0 U 5.0 UJ 20 U
5.0 U 5.0 U 5.0 UJ 20 U
5.0 U 5.0 U 5.0 UJ 20 U
5.0 UJ 5.0 UJ 5.0 UJ 20 U
5.0 U 5.0 U 5.0 UJ 20 U
5.0 UJ 5.0 UJ 5.0 UJ 20 U
5.0 UJ 5.0 UJ 5.0 UJ 20 U
5.0 UJ 5.0 U 5.0 UJ 20 U
5.0 UJ 5.0 U 5.0 UJ 20 U
5.0 UJ 5.0 U 5.0 UJ 20 U
5.0 U 5.0 U 5.0 UJ 20 U
5.0 U 5.0 U 5.0 UJ 20 U
5.0 U 5.0 U 5.0 UJ 20 U
5.0 UJ 5.0 UJ 5.0 UJ 20 U
5.0 U 5.0 U 5.0 UJ 20 U
5.0 U 5.0 U 5.0 U 20 U
5.0 U 5.0 U 5.0 UJ 20 U
5.0 U 5.0 U 5.0 UJ 20 U
5.0 U 5.0 U 5.0 UJ 20 U
5.0 UJ 5.0 UJ 5.0 UJ 20 U
5.0 U 5.0 U 5.0 U 20 U
5.0 UJ 5.0 U 5.0 UJ 20 U
5.0 U 5.0 U 5.0 UJ 20 U
5.0 UJ 5.0 U 5.0 UJ 20 U
5.0 U 5.0 U 5.0 UJ 20 U
5.0 UJ 5.0 UJ 5.0 UJ 20 U
10 U 10 U 10 UJ 40 U
5.0 U 5.0 U 5.0 U 20 U
5.0 U 5.0 U 5.0 UJ 20 U
5.0 UJ 5.0 U 5.0 U 20 U
10 UJ 10 U 10 UJ 40 U
5.0 U 5.0 U 5.0 UJ 20 U
5.0 UJ 5.0 U 5.0 UJ 20 U
5.0 U 690 7.8 J 20 U
5.0 U 5.0 U 5.0 U 20 U
5.0 UJ 5.0 U 5.0 UJ 20 U
5.0 U 5.0 U 5.0 UJ 20 U
5.0 U 5.0 U 5.0 UJ 20 U
5.0 UJ 5.0 U 5.0 UJ 20 U
4982ASR Number: 09/07/2010
MP7ES02Project ID: Cleburn Street well samplingProject Desc:
RLAB Approved Sample Analysis Results
Page 8 of 18
Analysis/ Analyte
Trichloroethene
Trichlorofluoromethane
1,1,2-Trichlorotrifluoroethane
Vinyl Chloride
m and/or p-Xylene
o-Xylene
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
Units 102-__ 103-__ 104-__ 104-FD
5.0 U 5.0 U 5.0 U 20 U
5.0 U 5.0 U 5.0 UJ 20 U
5.0 U 5.0 U 5.0 UJ 20 U
5.0 U 5.0 U 5.0 UJ 20 U
10 U 10 U 10 UJ 40 U
5.0 U 5.0 U 5.0 UJ 20 U
4982ASR Number: 09/07/2010
MP7ES02Project ID: Cleburn Street well samplingProject Desc:
RLAB Approved Sample Analysis Results
Page 9 of 18
1 VOCs in Water by GC/MS
Analysis/ Analyte
Acetone
Benzene
Bromodichloromethane
Bromoform
Bromomethane
2-Butanone
Carbon Disulfide
Carbon Tetrachloride
Chlorobenzene
Chloroethane
Chloroform
Chloromethane
Cyclohexane
1,2-Dibromo-3-Chloropropane
Dibromochloromethane
1,2-Dibromoethane
1,2-Dichlorobenzene
1,3-Dichlorobenzene
1,4-Dichlorobenzene
Dichlorodifluoromethane
1,1-Dichloroethane
1,2-Dichloroethane
1,1-Dichloroethene
cis-1,2-Dichloroethene
trans-1,2-Dichloroethene
1,2-Dichloropropane
cis-1,3-Dichloropropene
trans-1,3-Dichloropropene
Ethyl Benzene
2-Hexanone
Isopropylbenzene
Methyl Acetate
Methyl tert-butyl ether
Methylcyclohexane
Methylene Chloride
4-Methyl-2-Pentanone
Naphthalene
Styrene
1,1,2,2-Tetrachloroethane
Tetrachloroethene
Toluene
1,2,3-Trichlorobenzene
1,2,4-Trichlorobenzene
1,1,1-Trichloroethane
1,1,2-Trichloroethane
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
Units 105-__ 106-__ 107-__ 108-__
70 34 490 200 J
20 U 20 U 20 U 20 U
20 U 20 U 20 U 20 U
20 U 20 U 20 U 20 U
20 U 20 U 20 U 20 U
20 U 20 U 20 U 20 UJ
20 U 20 U 20 U 20 U
20 U 40 180 760 J
20 U 20 U 20 U 20 U
20 U 20 U 20 U 20 U
20 U 20 U 170 270
20 U 20 U 20 U 20 U
20 U 20 U 20 U 20 U
20 U 20 U 20 U 20 U
20 U 20 U 20 U 20 U
20 U 20 U 20 U 20 U
20 U 20 U 20 U 20 U
20 U 20 U 20 U 20 U
20 U 20 U 20 U 20 U
20 U 20 U 20 U 20 U
20 U 20 U 20 U 20 U
20 U 20 U 20 U 20 U
20 U 20 U 20 U 20 U
20 U 20 U 20 U 20 U
20 U 20 U 20 U 20 U
20 U 20 U 20 U 20 U
20 U 20 U 20 U 20 U
20 U 20 U 20 U 20 U
20 U 20 U 20 U 20 U
20 U 20 U 20 U 20 UJ
20 U 20 U 20 U 20 U
20 U 20 U 20 U 20 UJ
40 U 40 U 40 U 40 U
20 U 20 U 20 U 20 U
20 U 20 U 20 U 20 U
20 U 20 U 20 U 20 U
40 U 40 U 40 U 40 U
20 U 20 U 20 U 20 U
20 U 20 U 20 U 20 U
20 U 33000 43 29
20 U 20 U 20 U 20 U
20 U 20 U 20 U 20 U
20 U 20 U 20 U 20 U
20 U 20 U 20 U 35
20 U 20 U 20 U 20 U
4982ASR Number: 09/07/2010
MP7ES02Project ID: Cleburn Street well samplingProject Desc:
RLAB Approved Sample Analysis Results
Page 10 of 18
Analysis/ Analyte
Trichloroethene
Trichlorofluoromethane
1,1,2-Trichlorotrifluoroethane
Vinyl Chloride
m and/or p-Xylene
o-Xylene
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
Units 105-__ 106-__ 107-__ 108-__
20 U 20 U 20 U 20 U
20 U 20 U 20 U 20 U
20 U 20 U 20 U 20 U
20 U 20 U 20 U 20 U
40 U 40 U 40 U 40 U
20 U 20 U 20 U 20 U
4982ASR Number: 09/07/2010
MP7ES02Project ID: Cleburn Street well samplingProject Desc:
RLAB Approved Sample Analysis Results
Page 11 of 18
1 VOCs in Water by GC/MS
Analysis/ Analyte
Acetone
Benzene
Bromodichloromethane
Bromoform
Bromomethane
2-Butanone
Carbon Disulfide
Carbon Tetrachloride
Chlorobenzene
Chloroethane
Chloroform
Chloromethane
Cyclohexane
1,2-Dibromo-3-Chloropropane
Dibromochloromethane
1,2-Dibromoethane
1,2-Dichlorobenzene
1,3-Dichlorobenzene
1,4-Dichlorobenzene
Dichlorodifluoromethane
1,1-Dichloroethane
1,2-Dichloroethane
1,1-Dichloroethene
cis-1,2-Dichloroethene
trans-1,2-Dichloroethene
1,2-Dichloropropane
cis-1,3-Dichloropropene
trans-1,3-Dichloropropene
Ethyl Benzene
2-Hexanone
Isopropylbenzene
Methyl Acetate
Methyl tert-butyl ether
Methylcyclohexane
Methylene Chloride
4-Methyl-2-Pentanone
Naphthalene
Styrene
1,1,2,2-Tetrachloroethane
Tetrachloroethene
Toluene
1,2,3-Trichlorobenzene
1,2,4-Trichlorobenzene
1,1,1-Trichloroethane
1,1,2-Trichloroethane
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
Units 109-__ 110-__ 110-FD 111-__
88 J 63 64 J 120 J
20 U 50 U 50 U 20 U
20 U 50 U 50 U 20 U
20 U 50 U 50 U 20 U
20 U 50 U 50 U 20 U
20 UJ 50 U 50 UJ 20 UJ
20 U 50 U 50 U 20 U
240 50 U 50 U 96
20 U 50 U 50 U 20 U
20 U 50 U 50 U 20 U
180 50 U 50 U 110
20 U 50 U 50 U 20 U
20 U 50 U 50 U 20 U
20 U 50 U 50 U 20 U
20 U 50 U 50 U 20 U
20 U 50 U 50 U 20 U
20 U 50 U 50 U 20 U
20 U 50 U 50 U 20 U
20 U 50 U 50 U 20 U
20 U 50 U 50 U 20 U
20 U 50 U 50 U 20 U
20 U 50 U 50 U 20 U
20 U 50 U 50 U 20 U
20 U 50 U 50 U 20 U
20 U 50 U 50 U 20 U
20 U 50 U 50 U 20 U
20 U 50 U 50 U 20 U
20 U 50 U 50 U 20 U
20 U 50 U 50 U 20 U
20 UJ 50 U 50 UJ 20 UJ
20 U 50 U 50 U 20 U
20 UJ 50 U 50 UJ 20 UJ
40 U 100 U 100 U 40 U
20 U 50 U 50 U 20 U
20 U 50 U 50 U 20 U
20 U 50 U 50 U 20 U
40 U 100 U 100 U 40 U
20 U 50 U 50 U 20 U
20 U 50 U 50 U 20 U
7500 J 95 110 3200 J
20 U 50 U 50 U 20 U
20 U 50 U 50 U 20 U
20 U 50 U 50 U 20 U
64 50 U 50 U 26
20 U 50 U 50 U 20 U
4982ASR Number: 09/07/2010
MP7ES02Project ID: Cleburn Street well samplingProject Desc:
RLAB Approved Sample Analysis Results
Page 12 of 18
Analysis/ Analyte
Trichloroethene
Trichlorofluoromethane
1,1,2-Trichlorotrifluoroethane
Vinyl Chloride
m and/or p-Xylene
o-Xylene
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
Units 109-__ 110-__ 110-FD 111-__
20 U 50 U 50 U 20 U
20 U 50 U 50 U 20 U
20 U 50 U 50 U 20 U
20 U 50 U 50 U 20 U
40 U 100 U 100 U 40 U
20 U 50 U 50 U 20 U
4982ASR Number: 09/07/2010
MP7ES02Project ID: Cleburn Street well samplingProject Desc:
RLAB Approved Sample Analysis Results
Page 13 of 18
1 VOCs in Water by GC/MS
Analysis/ Analyte
Acetone
Benzene
Bromodichloromethane
Bromoform
Bromomethane
2-Butanone
Carbon Disulfide
Carbon Tetrachloride
Chlorobenzene
Chloroethane
Chloroform
Chloromethane
Cyclohexane
1,2-Dibromo-3-Chloropropane
Dibromochloromethane
1,2-Dibromoethane
1,2-Dichlorobenzene
1,3-Dichlorobenzene
1,4-Dichlorobenzene
Dichlorodifluoromethane
1,1-Dichloroethane
1,2-Dichloroethane
1,1-Dichloroethene
cis-1,2-Dichloroethene
trans-1,2-Dichloroethene
1,2-Dichloropropane
cis-1,3-Dichloropropene
trans-1,3-Dichloropropene
Ethyl Benzene
2-Hexanone
Isopropylbenzene
Methyl Acetate
Methyl tert-butyl ether
Methylcyclohexane
Methylene Chloride
4-Methyl-2-Pentanone
Naphthalene
Styrene
1,1,2,2-Tetrachloroethane
Tetrachloroethene
Toluene
1,2,3-Trichlorobenzene
1,2,4-Trichlorobenzene
1,1,1-Trichloroethane
1,1,2-Trichloroethane
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
Units 112-__ 113-__ 114-__ 115-__
100 J 84 J 31 J 67 J
20 U 20 U 20 U 20 U
20 U 20 U 20 U 20 U
20 U 20 U 20 U 20 U
20 U 20 U 20 U 20 UJ
20 UJ 20 UJ 20 UJ 20 UJ
20 U 20 U 20 U 20 UJ
1200 140 20 U 270 J
20 U 20 U 20 U 20 U
20 U 20 U 20 U 20 UJ
390 420 20 U 410 J
20 U 20 U 20 U 20 UJ
20 U 20 U 20 U 20 UJ
20 U 20 U 20 U 20 U
20 U 20 U 20 U 20 U
20 U 20 U 20 U 20 U
20 U 20 U 20 U 20 U
20 U 20 U 20 U 20 U
20 U 20 U 20 U 20 U
20 U 20 U 20 U 20 UJ
20 U 20 U 20 U 20 UJ
20 U 20 U 20 U 20 U
20 U 20 U 20 U 20 UJ
20 U 20 U 20 U 20 UJ
20 U 20 U 20 U 20 UJ
20 U 20 U 20 U 20 U
20 U 20 U 20 U 20 U
20 U 20 U 20 U 20 U
20 U 20 U 20 U 20 U
20 UJ 20 UJ 20 UJ 20 UJ
20 U 20 U 20 U 20 U
20 UJ 20 UJ 20 UJ 20 UJ
40 U 40 U 40 U 40 UJ
20 U 20 U 20 U 20 U
20 U 20 U 20 U 20 UJ
20 U 20 U 20 U 20 U
40 U 40 U 40 U 40 U
20 U 20 U 20 U 20 U
20 U 20 U 20 U 20 U
2000 37 20 20 U
20 U 20 U 20 U 20 U
20 U 20 U 20 U 20 U
20 U 20 U 20 U 20 U
39 20 U 20 U 94 J
20 U 20 U 20 U 20 U
4982ASR Number: 09/07/2010
MP7ES02Project ID: Cleburn Street well samplingProject Desc:
RLAB Approved Sample Analysis Results
Page 14 of 18
Analysis/ Analyte
Trichloroethene
Trichlorofluoromethane
1,1,2-Trichlorotrifluoroethane
Vinyl Chloride
m and/or p-Xylene
o-Xylene
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
Units 112-__ 113-__ 114-__ 115-__
20 U 20 U 20 U 20 U
20 U 20 U 20 U 20 UJ
20 U 20 U 20 U 20 UJ
20 U 20 U 20 U 20 UJ
40 U 40 U 40 U 40 U
20 U 20 U 20 U 20 U
4982ASR Number: 09/07/2010
MP7ES02Project ID: Cleburn Street well samplingProject Desc:
RLAB Approved Sample Analysis Results
Page 15 of 18
1 VOCs in Water by GC/MS
Analysis/ Analyte
Acetone
Benzene
Bromodichloromethane
Bromoform
Bromomethane
2-Butanone
Carbon Disulfide
Carbon Tetrachloride
Chlorobenzene
Chloroethane
Chloroform
Chloromethane
Cyclohexane
1,2-Dibromo-3-Chloropropane
Dibromochloromethane
1,2-Dibromoethane
1,2-Dichlorobenzene
1,3-Dichlorobenzene
1,4-Dichlorobenzene
Dichlorodifluoromethane
1,1-Dichloroethane
1,2-Dichloroethane
1,1-Dichloroethene
cis-1,2-Dichloroethene
trans-1,2-Dichloroethene
1,2-Dichloropropane
cis-1,3-Dichloropropene
trans-1,3-Dichloropropene
Ethyl Benzene
2-Hexanone
Isopropylbenzene
Methyl Acetate
Methyl tert-butyl ether
Methylcyclohexane
Methylene Chloride
4-Methyl-2-Pentanone
Naphthalene
Styrene
1,1,2,2-Tetrachloroethane
Tetrachloroethene
Toluene
1,2,3-Trichlorobenzene
1,2,4-Trichlorobenzene
1,1,1-Trichloroethane
1,1,2-Trichloroethane
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
Units 116-__ 117-__ 122-__ 122-FD
60 200 52 J 53 J
50 U 100 U 20 U 20 U
50 U 100 U 20 U 20 U
50 U 100 U 20 U 20 U
50 U 100 U 20 U 20 U
50 U 100 U 20 UJ 20 UJ
50 U 100 U 20 U 20 U
250 100 U 320 320
50 U 100 U 20 U 20 U
50 U 100 U 20 U 20 U
50 U 100 71 72
50 U 100 U 20 U 20 U
50 U 100 U 20 U 20 U
50 U 100 U 20 U 20 U
50 U 100 U 20 U 20 U
50 U 100 U 20 U 20 U
50 U 100 U 20 U 20 U
50 U 100 U 20 U 20 U
50 U 100 U 20 U 20 U
50 U 100 U 20 U 20 U
50 U 100 U 20 U 20 U
50 U 100 U 20 U 20 U
50 U 100 U 20 U 20 U
50 U 100 U 20 U 20 U
50 U 100 U 20 U 20 U
50 U 100 U 20 U 20 U
50 U 100 U 20 U 20 U
50 U 100 U 20 U 20 U
50 U 100 U 20 U 20 U
50 U 100 U 20 UJ 20 UJ
50 U 100 U 20 U 20 U
50 U 100 U 20 UJ 20 UJ
100 U 200 U 40 U 40 U
50 U 100 U 20 U 20 U
50 U 100 U 20 U 20 U
50 U 100 U 20 U 20 U
100 U 200 U 40 U 40 U
50 U 100 U 20 U 20 U
50 U 100 U 20 U 20 U
50 U 1600 6000 6000
50 U 100 U 20 U 20 U
50 U 100 U 20 U 20 U
50 U 100 U 20 U 20 U
50 U 100 U 20 U 20 U
50 U 100 U 20 U 20 U
4982ASR Number: 09/07/2010
MP7ES02Project ID: Cleburn Street well samplingProject Desc:
RLAB Approved Sample Analysis Results
Page 16 of 18
Analysis/ Analyte
Trichloroethene
Trichlorofluoromethane
1,1,2-Trichlorotrifluoroethane
Vinyl Chloride
m and/or p-Xylene
o-Xylene
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
Units 116-__ 117-__ 122-__ 122-FD
50 U 100 U 20 U 20 U
50 U 100 U 20 U 20 U
50 U 100 U 20 U 20 U
50 U 100 U 20 U 20 U
100 U 200 U 40 U 40 U
50 U 100 U 20 U 20 U
4982ASR Number: 09/07/2010
MP7ES02Project ID: Cleburn Street well samplingProject Desc:
RLAB Approved Sample Analysis Results
Page 17 of 18
1 VOCs in Water by GC/MS
Analysis/ Analyte
Acetone
Benzene
Bromodichloromethane
Bromoform
Bromomethane
2-Butanone
Carbon Disulfide
Carbon Tetrachloride
Chlorobenzene
Chloroethane
Chloroform
Chloromethane
Cyclohexane
1,2-Dibromo-3-Chloropropane
Dibromochloromethane
1,2-Dibromoethane
1,2-Dichlorobenzene
1,3-Dichlorobenzene
1,4-Dichlorobenzene
Dichlorodifluoromethane
1,1-Dichloroethane
1,2-Dichloroethane
1,1-Dichloroethene
cis-1,2-Dichloroethene
trans-1,2-Dichloroethene
1,2-Dichloropropane
cis-1,3-Dichloropropene
trans-1,3-Dichloropropene
Ethyl Benzene
2-Hexanone
Isopropylbenzene
Methyl Acetate
Methyl tert-butyl ether
Methylcyclohexane
Methylene Chloride
4-Methyl-2-Pentanone
Naphthalene
Styrene
1,1,2,2-Tetrachloroethane
Tetrachloroethene
Toluene
1,2,3-Trichlorobenzene
1,2,4-Trichlorobenzene
1,1,1-Trichloroethane
1,1,2-Trichloroethane
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
Units 124-FB 126-__ 153-FB
20 UJ 50 U 43 J
20 U 50 U 20 U
20 U 50 U 20 U
20 U 50 U 20 U
20 U 50 U 20 U
20 UJ 50 U 20 UJ
20 U 50 U 20 U
20 U 50 U 20 U
20 U 50 U 20 U
20 U 50 U 20 U
20 U 50 U 20 U
20 U 50 U 20 U
20 U 50 U 20 U
20 U 50 U 20 U
20 U 50 U 20 U
20 U 50 U 20 U
20 U 50 U 20 U
20 U 50 U 20 U
20 U 50 U 20 U
20 U 50 U 20 U
20 U 50 U 20 U
20 U 50 U 20 U
20 U 50 U 20 U
20 U 50 U 20 U
20 U 50 U 20 U
20 U 50 U 20 U
20 U 50 U 20 U
20 U 50 U 20 U
20 U 50 U 20 U
20 UJ 50 U 20 UJ
20 U 50 U 20 U
20 UJ 50 U 20 UJ
40 U 100 U 40 U
20 U 50 U 20 U
20 U 50 U 20 U
20 U 50 U 20 U
40 U 100 U 40 U
20 U 50 U 20 U
20 U 50 U 20 U
88 50 U 20 U
20 U 50 U 20 U
20 U 50 U 20 U
20 U 50 U 20 U
20 U 50 U 20 U
20 U 50 U 20 U
4982ASR Number: 09/07/2010
MP7ES02Project ID: Cleburn Street well samplingProject Desc:
RLAB Approved Sample Analysis Results
Page 18 of 18
Analysis/ Analyte
Trichloroethene
Trichlorofluoromethane
1,1,2-Trichlorotrifluoroethane
Vinyl Chloride
m and/or p-Xylene
o-Xylene
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
Units 124-FB 126-__ 153-FB
20 U 50 U 20 U
20 U 50 U 20 U
20 U 50 U 20 U
20 U 50 U 20 U
40 U 100 U 40 U
20 U 50 U 20 U
4982ASR Number: 09/07/2010
MP7ES02Project ID: Cleburn Street well samplingProject Desc:
RLAB Approved Sample Analysis Results
4982
MP7ES02Project ID:
Cleburn Street well sampling
Mary PetersonSUPR/IANE
United States Environmental Protection AgencyRegion VII
901 N. 5th StreetKansas City, KS 66101
__/__/____
Data Disposition/Sample Release for ASR #:
Project Description:
Subject:
Kaye DollmannENSV/RLAB
I have received and reviewed the Transmittal of Sample Analysis Results for the above-referencedAnalytical Services Request(ASR) and have indicated my findings below by checking one of theboxes for Data Disposition.
I understand all samples will be disposed upon receipt of this form, unless samples are requestedto be held. If I do not return this form all samples will be disposed of on ___________________.
"RELEASED" - Read-only to all Region 7 employees and contractors that have R7LIMS"Customer" account. All Samples may be disposed of upon receipt of this form if not requested tobe held.
"Project Manager Accessible" - Available on the LAN in R7LIMS for my use only. All Samples maybe disposed of upon receipt of this form if not requested to be held.
"Archived" - THIS DATA IS OF A SENSITIVE NATURE. Any future reports must be requestedthrough the laboratory. All samples may be disposed of upon receipt of the form if not requestedto be held.
Date:
From:
To:
Hold Samples - I have determined that the samples need to be held until ______________, afterwhich time they will be disposed of in accordance with applicable regulations. The reason for the hold is:
Samples are associated with a legal proceeding.
Question/Concern with data - possible reanalysis requested.
Other:________________________________________________________________