dost-x rstl brochure of testing and calibration services

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Page 1: DOST-X RSTL Brochure of Testing and Calibration Services
Page 2: DOST-X RSTL Brochure of Testing and Calibration Services

REGIONAL STANDARDS AND TESTING LABORATORIES DEPARTMENT OF SCIENCE AND TECHNOLOGY

Region X

BUSINESS PROCESS (Chemical and Microbiological Testing Laboratories)

1. Customer (person submitting a sample) registers at the guard house. 2. Customer proceeds to RSTL office at the second floor of the building

and upon instruction of the guard on duty. 3. Sample Receiving Officer (SRO) checks if the sample to be submitted

is valid and if a sterile sampling bottle is required.

If the sample is valid: 1. If sample is valid and sterile bottle is not required, customer gives

information to the SRO for the Test Request Form (TRF). 2. Upon completion of TRF, customer pays total cost of fees to the

Cashier in the first floor and claims Official Receipt (OR) of payment. 3. Customer comes back to the RSTL office, shows the OR and gets

duplicate copy of the TRF. 4. Customer claims Report of Analysis on the date due stated in the TRF.

Reports of analysis are issued only to the person who submitted the sample or to an authorized representative.

If a sterile bottle is required: 1. Customer gives information for the TRF upon instruction of SRO. 2. Customer pays to the Cashier at the 1st floor the partial payment of

P600 for drinking water samples or P500 for environmental samples and gets OR of payment.

3. Customer goes back to the RSTL office, shows OR and claims sterile sampling bottle and gets instructions on sampling schedule, sampling procedure, and handling of samples.

4. Customer comes back to the RSTL to submit valid samples.

If sample is invalid: Customer gets instructions on submission of valid samples and comes back on the scheduled date.

Note: The customer replaces loss, breakage, or damage to borrowed sampling bottles.

1

Page 3: DOST-X RSTL Brochure of Testing and Calibration Services

REGIONAL STANDARDS AND TESTING LABORATORIES DEPARTMENT OF SCIENCE AND TECHNOLOGY

Region X

SAMPLE TEST TEST METHOD

Food/Feed Products

& Raw Materials Ash Gravimetric 294.00

Calcium Flame AAS 1008.00

Fat, Crude or Ether Solvent Extraction 564.00

Extract

Fat, Total Hydrolysis and Solvent 850.00

Extraction

Fiber, Crude Weende 948.00

Fiber, Total Dietary Enzymatic/Gravimetric 5000.00

Iron Flame AAS 1008.00

Manganese Flame AAS 1008.00

Mercury Thermal Decomposition, 1008.00

Amalgamation, AAS

Moisture Content Air/Vacuum Oven 202.00

Nitrite Colorimetric 800.00

Phosphorus Dry Ashing, Molybdate 680.00

Colorimetric

Potassium Dry Ashing, Flame 680.00

Photometric

Protein, Crude Automated Kjeldahl 454.00

Vitamin C (Juices) Titration 1155.00

Sodium Flame AAS 1008.00

Sugar, Total Lane-Eynon Constant 454.00

Volume Volumetric

Titrable Acidity (Liquids) Titration 278.00

Water Activity Dew Point 118.00

(Minimum sample

required is 250 grams)

CHEMICAL TESTING LABORATORY

2

FEE (PhP)

Page 4: DOST-X RSTL Brochure of Testing and Calibration Services

Water and

Wastewater

(Minimum sample

required is one liter (1 L)

per test. Please confirm

with RSTL-X on the total

volume required if more

than one test is

requested)

Alkalinity, total Titration 312.00

5-day Biochemical Azide Modification 1008.00

Oxygen Demand (Dilution Technique)

Cadmium Flame AAS 1008.00

Calcium Flame AAS 1008.00

Chloride Titration, Argentometric 454.00

Chemical Oxygen Closed Reflux 960.00

Demand Colorimetric

Color (Hazen) Photometric, 100.00

Merck Spectroquant

REGIONAL STANDARDS AND TESTING LABORATORIES DEPARTMENT OF SCIENCE AND TECHNOLOGY

Region X

SAMPLE TEST TEST METHOD

CHEMICAL TESTING LABORATORY

Copper Flame AAS 1008.00

Dissolved Oxygen Azide Modification 336.00

Iron Flame AAS 1008.00

Lead Flame AAS 1008.00

Magnesium Flame AAS 1008.00

Manganese Flame AAS 1008.00

Mercury Flameless AAS 1008.00

Cold Vapor Technique

Thermal Decomposition, 1008.00

Amalgamation, AAS

Nitrate Photometric, 336.00

Merck Spectroquant

pH Glass Electrode 118.00

Phosphorus Stannous Chloride 680.00

Colorimetric

Potassium Flame Photometric 680.00

3

FEE (PhP)

Page 5: DOST-X RSTL Brochure of Testing and Calibration Services

REGIONAL STANDARDS AND TESTING LABORATORIES DEPARTMENT OF SCIENCE AND TECHNOLOGY

Region X

SAMPLE TEST TEST METHOD

CHEMICAL TESTING LABORATORY

Settleable Solids Volumetric 202.00

Sodium Flame AAS 1008.00

Sulfate Photometric, 336.00

Merck Spectroquant

Total Dissolved Solids Gravimetric 437.00

Total Hardness Titration, EDTA 320.00

Complexometric

Total Solids Gravimetric 445.00

Total Suspended Solids Gravimetric 480.00

Turbidity Photometric, 202.00

Merck Spectroquant

Zinc Flame AAS 1008.00

Salinity Salinometer 118.00

Fertilizer, Plant

Tissue, and other

Related Materials

Ash Gravimetric 294.00

Calcium Flame AAS 1008.00

Calcium Carbonate Titration 454.00

Equivalent

Lead Flame AAS 1008.00

Manganese Flame AAS 1008.00

Mercury Thermal Decomposition, 1008.00

Amalgamation, AAS

Moisture Content Air/Vacuum Oven 202.00

Dry Matter Content Air Oven 202.00

Nitrogen Kjeldahl 454.00

Sodium Flame AAS 1008.00

(Minimum sample

required is 250 grams,

dried and pulverized)

4

FEE (PhP)

Page 6: DOST-X RSTL Brochure of Testing and Calibration Services

Organic Matter Wakley Black 361.00

pH Glass Electrode 118.00

Phosphorus, total Dry Ashing, 680.00

Vanadomolybdate

Colorimetric

Potassium, total Dry Ashing, Flame 680.00

Photometric

Zinc Flame AAS 1008.00

REGIONAL STANDARDS AND TESTING LABORATORIES DEPARTMENT OF SCIENCE AND TECHNOLOGY

Region X

SAMPLE TEST TEST METHOD

CHEMICAL TESTING LABORATORY

Limestone

(Hydrated /

Quicklime)

(Minimum sample

required is 250 grams,

dried and pulverized)

Neutralizing Value Titration 320.00

5

FEE (PhP)

Mercury Thermal Decomposition, 1008.00

Amalgamation, AAS

Phosphorus, available Extraction, Stannous 420.00

(for soil) Chloride Colorimetric

Potassium, available Extraction, Flame 420.00

(for soil) Photometric

Sediments/Soil/

Sludge

(Minimum sample

required is 250 grams,

dried and pulverized)

Page 7: DOST-X RSTL Brochure of Testing and Calibration Services

REGIONAL STANDARDS AND TESTING LABORATORIES DEPARTMENT OF SCIENCE AND TECHNOLOGY

Region X

Food/Feed Products

& Raw Materials

Aerobic Plate Count, Pour Plate 420.00

cfu/g or mL

Coliforms, Multiple Tube 420.00

MPN/g or mL Fermentation Technique

Fecal Coliform, Multiple Tube 420.00

MPN/g or mL Fermentation Technique

E. coli Enumeration, Multiple Tube 648.00

MPN/g or mL Fermentation Technique

Coliforms, Pour Plate - VRBA 800.00

cfu/g or mL

Yeast and Mold Count, Pour Plate 420.00

cfu/g or mL

Spread Plate 420.00

Non-typhi Salmonella Presence/Absence 1008.00

spp. Detection (Rapid Test)

(Detected or Not Detected

/25 g or mL sample)

Staphylococcus aureus Spread Plate 1008.00

Enumeration,

cfu/g or mL

Vibrio parahaemolyticus Chromogenic Plates 500.00

Enumeration, cfu/g or mL (Rapid Test)

(for Seafoods)

Enterobacteriaceae, Chromogenic Plates 648.00

cfu/g or mL (Rapid Test)

Escherichia coli Chromogenic Plates 648.00

Enumeration, cfu/g or mL (Rapid Test)

(Minimum sample

required is six (6) packs

of unopened original

retail package, with total

weight of not less than

250 g or mL)

SAMPLE TEST TEST METHOD

MICROBIOLOGICAL TESTING LABORATORY

6

FEE (PhP)

Page 8: DOST-X RSTL Brochure of Testing and Calibration Services

REGIONAL STANDARDS AND TESTING LABORATORIES DEPARTMENT OF SCIENCE AND TECHNOLOGY

Region X

SAMPLE TEST TEST METHOD

MICROBIOLOGICAL TESTING LABORATORY

Salmonella spp. Chromogenic Plates 1008.00

Detection (Rapid Test)

Coliforms, Chromogenic Plates 420.00

cfu/g or mL (Rapid Test)

Aerobic Plate Count, Chromogenic Plates 420.00

cfu/g or mL (Rapid Test)

Yeast and Mold Count, Chromogenic Plates 420.00

cfu/g or mL (Rapid Test)

Staphylococcus aureus Chromogenic Plates 1008.00

Enumeration, cfu/g or mL (Rapid Test)

Commercial Sterility Presence/Absence 1008.00

(for low acid foods)

7

FEE (PhP)

Aerobic Plate Count, Pour Plate 420.00

cfu/cm2 Spread Plate 420.00

Bioburden Samples

Association of Official Analytical Chemists

Bacteriological Analytical Manual (BAM) Online

Collins & Lyne’s Microbiological Methods

Compendium of Analytical Method

Hyserve Manual

Merck Manual

National Standard Methods Health Protection Agency, UK

Standard References

Page 9: DOST-X RSTL Brochure of Testing and Calibration Services

REGIONAL STANDARDS AND TESTING LABORATORIES DEPARTMENT OF SCIENCE AND TECHNOLOGY

Region X

Heterotrophic Plate Pour Plate 420.00

Count, cfu/mL

Coliforms, Multiple Tube 420.00

MPN/100 mL, Fermentation Technique

drinking water

Fecal Coliform, Multiple Tube 420.00

MPN/100 mL, Fermentation Technique

drinking water

Coliform Count, MPN/ Multiple Tube 500.00

100 mL, environmental Fermentation Technique

water, 3 dilutions

Fecal Coliform, MPN/ Multiple Tube 500.00

100 mL, environmental Fermentation Technique

water, 3 dilutions

Escherichia coli Multiple Tube 648.00

Enumeration, Fermentation Technique

MPN/100 mL

Pseudomonas Multiple Tube 600.00

aeruginosa, Fermentation Technique

MPN/100 mL

Coliforms, Membrane Filtration 420.00

cfu/100 mL Technique

Heterotrophic Plate Chromogenic Plates 420.00

Count, cfu/mL (Rapid Test)

Coliforms, Chromogenic Plates 420.00

cfu/mL (Rapid Test)

Escherichia coli, Chromogenic Plates 648.00

Enumeration, cfu/mL (Rapid Test)

Water and

Wastewater

(Minimum sample

required is one (1)

unopened original retail

package of bottled

water or 250 mL in

provided sterile

sampling containers,

bottle or bag)

SAMPLE TEST TEST METHOD FEE (PhP)

MICROBIOLOGICAL TESTING LABORATORY

8

Hyserve Manual

Standard Methods for the Examination of Water and Wastewater

Standard References

Page 10: DOST-X RSTL Brochure of Testing and Calibration Services

REGIONAL STANDARDS AND TESTING LABORATORIES DEPARTMENT OF SCIENCE AND TECHNOLOGY

Region X

Alcohol Content Pycnometer 118.00

Free Fatty Acid Titration 278.00

Moisture Content Thermogravimetric/ 202.00

Vacuum Oven

Moisture Content, Critical Thermogravimetric 2828.00

Moisture Sorption Isotherm Gravimetric 5050.00

Nutrition Facts Gravimetric 1500.00

Computation (computation only)

Nutrition Facts Analysis Gravimetric 4308.00

with Computation

(with reports of chemical analysis for the following

parameters: moisture, total fat, protein, ash, and sodium)

pH Glass Electrode 118.00

Titrable Acidity Titration 278.00

Total Solids Gravimetric 445.00

Total Soluble Solids (Brix) Refractometer 118.00

Sensory Evaluation Panel 500.00

Specific Gravity Pycnometer 118.00

Water Activity Dew Point 118.00

Film Permeability Test Gravimetric 1414.00

(for PE Food Packaging)

Food Products

SAMPLE TEST TEST METHOD

ACCELERATED SHELF-LIFE EVALUATION LABORATORY

9

FEE (PhP)

Food Packaging

* Fee for Shelf-Life Evaluation will depend on the type of food deterioration.

Physical, chemical and microbiological parameters will be selected after the

type of food deterioration has been identified through Preliminary Evaluation.

(Minimum sample

required is six (6) packs

of unopened original

retail package, with total

weight of not less than

250 g)

Page 11: DOST-X RSTL Brochure of Testing and Calibration Services

REGIONAL STANDARDS AND TESTING LABORATORIES DEPARTMENT OF SCIENCE AND TECHNOLOGY

Region X

EQUIPMENT / SAMPLE TEST/CAPACITY

Volume Calibration

Gravimetric Method (5-10-20 liters) 250.00

Volumetric Method (5-10-20 liters) 150.00

Volumetric Method 100 liters 300.00

250-500 liters 500.00

1,000 liters and above 1500.00

Volumetric Method 10,000 liters 600.00

12,000 liters 750.00

13,000 liters 800.00

14,000 liters 850.00

16,000 liters 1000.00

18,000 liters 1100.00

20,000 liters 1200.00

22,000 liters 1350.00

24,000 liters 1450.00

30,000 liters 1800.00

Calibrating Bucket

REGIONAL METROLOGY LABORATORY

Proving Bucket

Tank Truck / Lorry

10

FEE (PhP)

Volumetric Method 2,000 liters 1500.00

Per additional liter 0.10

Other Type Tank

Page 12: DOST-X RSTL Brochure of Testing and Calibration Services

REGIONAL STANDARDS AND TESTING LABORATORIES DEPARTMENT OF SCIENCE AND TECHNOLOGY

Region X

EQUIPMENT / SAMPLE TEST/CAPACITY

REGIONAL METROLOGY LABORATORY

Class M 1-5 kg 100.00

10-25 kg 200.00

50 kg 500.00

500 kg 1000.00

Per Additional 100 g 200.00

Class F 1g – 1 kg 200.00

Class M 1 mg – 500 g 100.00/pc

Class F 1 mg – 500 g 200.00/pc

Spring Scale (dial) 10-20 kg 100.00

60-100 kg 200.00

250 kg, 1st 4 points 400.00

per additional point 100.00

500 kg, 1st 4 points 500.00

per additional point 200.00

Platform Balance 1st 4 points 500.00

per additional point 200.00

Triple Beam Balance 1st 9 points 1000.00

per additional point 200.00

0-10 kg, 1st 4 points 250.00

per additional point 100.00

20-60 kg, 1st 4 points 250.00

per additional point 100.00

100-500 kg, 1st 4 points 500.00

per additional point 200.00

Above 500 kg, 1st 4 points 1000.00

per additional point 200.00

Up to 8 points 1500.00

2500.00

linearity of aggragate and 1500.00

cement bin

Up to 1,000 kg 1250.00

Above 1,000 kg 2000.00

Mass Calibration

TEST WEIGHT

SCALE AND BALANCE

Mechanical

Electronic

11

Set of Weights

Analytical / High Accuracy

Truck Scale

Batching Plant

Batch Weigher

FEE (PhP)

Page 13: DOST-X RSTL Brochure of Testing and Calibration Services

REGIONAL STANDARDS AND TESTING LABORATORIES DEPARTMENT OF SCIENCE AND TECHNOLOGY

Region X

1st 4 points 1000.00

per additional point 200.00

1st 4 points 1000.00

per additional point 200.00

1st 4 points 1000.00

per additional point 200.00

1st 4 points 1500.00

per additional point 200.00

1st 4 points 1500.00

per additional point 200.00

Pressure Calibration

Pressure Gauge

Test Gauge

Temperature Calibration

Digital Thermometer

Thermocouple Probe/Wire

Oven/Freezer

Glass/Filled/Bimetallic Thermometer

Water Bath

EQUIPMENT / SAMPLE TEST/CAPACITY

REGIONAL METROLOGY LABORATORY

12

Up to 500 psi 300.00

Above 500 psi 400.00

Above 1,000 psi 500.00

Above 2,000 psi 1000.00

(note: all up to 4 points)

1800.00

FEE (PhP)

Page 14: DOST-X RSTL Brochure of Testing and Calibration Services

REGIONAL STANDARDS AND TESTING LABORATORIES DEPARTMENT OF SCIENCE AND TECHNOLOGY

Region X

AWARDS, ACCREDITATIONS, RECOGNITIONS,

PNS ISO/IEC 17025:2005 ACCREDITED

for Chemical and Microbiological Testing

Awarded the Plaque of Recognition from

DOST Central Office for being the FIRST

DOST RSTL to be accredited by the

Philippine Accreditation Office (PAO) in

the field of Chemical Testing and for

maintaining its accreditation for more

than 5 years

ACCREDITED by the Department of Health-Bureau of

Health Facilities and Services (DOH-BHFS) for Drinking

Water Physical, Chemical and Microbiological Analyses

Recognized by the Philippine Food and

Drug Administration (FDA) for Food

Testing

Registered at the Department of Environment and

Natural Resources-Environmental Management Bureau

(DENR-EMB) as a Hazardous Waste Generator

Licensed by the Philippine Drug

Enforcement Agency (PDEA) to

Handle Controlled Precursors and

Essential Chemicals

Laboratory Accreditation from the Department of

Agriculture-Bureau of Animal Industry for Feeds

Testing in 1999

REGISTRATIONS and LICENSES

Environmental Laboratory Accreditation

from the Department of Environment and

Natural Resources - Environmental

Management Bureau (DENR-EMB) in 2000

13

Special Permit from the Philippine National Police

(PNP) to Possess and Move Explosives/Explosive

Ingredients

Page 15: DOST-X RSTL Brochure of Testing and Calibration Services

REGIONAL STANDARDS AND TESTING LABORATORIES DEPARTMENT OF SCIENCE AND TECHNOLOGY

Region X

BUSINESS PROCESS (Regional Metrology Laboratory)

1. Customer (person submitting an item) registers at the guard house. 2. Customer proceeds to RML Office upon instruction of the guard on

duty. 3. Receiving officer checks if the request is an on-site or in-house

calibration.

If On-Site: 1. Customer writes letter requesting for on site calibration schedule. 2. Customer returns to RML to accompany staff to On-Site Location on

their scheduled date. 3. If an item(s) from RML needs to be borrowed, customer fills up item

borrowers slip. 4. The customer then proceeds to the Work Request Form procedure.

If In-House: 1. The receiving officer checks if the item is valid for calibration. 2. If the item is not valid, the customer requests instructions for item

validity. 3. If the item is valid, the customer proceeds to the Work Request Form

procedure.

Work Request Form Procedure: 1. Customer and Item Receiving Officer fill up the Work Request Form

(WRF). 2. Customer pays total cost of fees to the Cashier, and claims the Official

Receipt (OR). 3. Customer comes back to Receiving Officer, and shows OR. 4. Customer returns borrowed items (if applicable) after calibration has

been conducted. 5. Customer claims Certificate of Calibration and items on due date (An

authorized representative may claim the certificate of calibration).

14

Page 16: DOST-X RSTL Brochure of Testing and Calibration Services

Department of Science and Technology-X Mayor Jesus V. Seriña Street, Carmen

9000 Cagayan de Oro City

DOST-X VICINITY MAP

Golden Village

Pop Com

DOST-X

City Hospital

Mt. Carmel Church

City Hall

Cathedral

Ysalina Bridge

The Regional Standards and Testing Laboratories Region X

is now on

and

LIKE the Fan Page!

View the testing and calibration services offered by RSTL and you

may also post your inquiries, comments, complaints or

suggestions.

Booking of schedules for submission of samples for

analysis is still done through phone call or personally

at RSTL-X office.

St. Mary’s

Academy

Search the “DOST Regional Standards and Testing Laboratories Region X”,

Pictures and Layouts by ARCDablio Revised 01-04-13