deutsche akkreditierungsstelle gmbh annex to ... - aso-skz.deannex to the accreditation certificate...

This document is a translation. The definitive version is the original German annex to the accreditation certificate. 1/24

Deutsche Akkreditierungsstelle GmbH

Annex to the Accreditation Certificate D-PL-19761-01-00 according to DIN EN ISO/IEC 17025:2005 Period of validity: 17.12.2014 to 16.12.2019 Date of issue: 17.12.2014

Holder of certificate:

Mainsite GmbH & Co. KG, Analytik Service Obernburg Industrie Center Obernburg, 63784 Obernburg, Germany Tests in the fields:

physical, physico-chemical and chemical analysis of chemical products such as organic and inorganic chemicals, fibres, textile fabrics, dyes, oils, fats, waxes, resins, emulsifiers, additives, tensides, polymers, ceramics, metals, wood, glass, plastic films, rubber, lacquers, dispersions, polymers and plastic additives; physical, physico-chemical and chemical analysis of water; mechanical-technological and physical tests of semi-finished products, pre-products, parts and polymeric materials; selected acoustical measurements of noise at the workplace; expert module water Abbreviations used: see pages 22 ff. Within the given testing field marked with */**, the testing laboratory is permitted, without being required to inform and obtain prior approval from DAkkS, the following:

*) the free choice of standard or equivalent testing methods. **) the modification, development and refinement of testing methods.

The listed testing methods are exemplary. The testing laboratory maintains a current list of all testing methods within the flexible scope of accreditation. Within the scope of accreditation marked with ***, the testing laboratory is permitted, without being required to inform and obtain prior approval from DAkkS, to use standard testing methods listed here with different issue dates.

Annex to the accreditation certificate D-PL-19761-01-00

Period of validity: 17.12.2014 to 16.12.2019 - Translation - 2/24 Date of issue: 17.12.2014

1 Physical, physico-chemical and chemical analysis of chemical products, components and contaminants in raw materials, intermediate products and finished products

1.1 Analysis and identification of organic compounds in the liquid phase by NMR spectroscopy ** SP/n/001.04 2014-09

Identification and quantification of single component organic monomers and polymers in pure substances and mixtures by recording of a standard 1H-NMR spectrum

SP/n/002.04 2014-09

Identification of single component organic monomers and polymers in pure substances and mixtures by recording of a 13C-NMR spectrum

SP/n/010.01 1996-10

Determination of chain length in linear alkyl compounds

SP/n/011.02 2002-07

Determination of the ethylene oxide to propylene oxide ratio in ethoxylates/propoxylates by 1H-NMR

SP/n/014.02 2011-02

Determination of DMpT and MMA in MMA monomer

SP/n/016.02 2012-07

Incoming goods control for polyamidoamine epichlorohydrin resin by 1H-NMR

1.2 Analysis, identification and determination of primary and secondary products by UV-VIS/fluorescence spectroscopy ** VDA 275 1994-07

Moulded composites and fleeces for vehicles - Determination of formaldehyde release - Test procedure called modified flask method

SP/u/032.03 2008-08

UV-VIS spectroscopic determination of chlorophyll in MMA monomer

CL/p/002.03 2014-02

Photometric determination of carboxyl end groups (CEG) in polyester (PET)

CL/p/011.02 2010-12

Photometric determination of TiO2 in deep matt viscose and deep matt yarn



1.3 Analysis and identification of organic and inorganic compounds in solid and dissolved form by IR/Raman spectroscopy **

SP/i/002.05 2012-05

FTIR spectroscopic identity testing of PES/SPES

SP/i/006.04 2014-08

Determination of the IR characteristic of test specimens or sample material for the purpose of material identification, material comparison, failure analysis, technical problem solution or solution of other analytical problems

SP/i/025.02 2012-05

FTIR spectroscopic identity testing of gentamicin sulphate and clindamycin hydrochloride

SP/r/002.03 2012-07

Raman spectroscopic determination of sulfonation degree in SPES

CL/i/004.01 2011-09

Execution of NIR measurements for the identification of parent oils for preparations

1.4 Gas chromatographic analysis for the determination of organic compounds in liquids,

gases and polymers with standard detectors (FID) ** CH/g/019.01 2004-03

Control of acetone purity

VDA 277 1995-01

Non-metallic materials of the vehicle interior - Determination of the emission of organic compounds

CL/g/008.01 2012-04

Diethylene glycol in ethylene glycol - Gas chromatographic trace determination

CL/g/009.01 2013-10

Benzene and high boiling point components in carbon disulphide - Gas chromatographic trace determination

1.5 Gas chromatographic analysis for the determination of organic compounds in liquids,

gases and polymers by mass spectrometric detection ** CH/g/018.03 2000-08

Determination of carbon disulphide by thermodesorption/GC-MS

VDA 278 2011-10

Thermal desorption analysis of organic emissions for the characterisation of non-metallic materials for automobiles



1.6 Liquid chromatographic analysis for the determination of ingredients and components in solutions by HPLC and standard detection (UV, RI, DAD detection) **

CH/h/019.02 2013-10

Determination of hydroquinone in MMA

CH/h/020.01 2014-01

Determination of DmPT in MMA

ISO 15033 2007-03

Plastics - Determination of caprolactam and its cyclic and linear oligomers by HPLC

1.7 Liquid chromatographic analysis for the determination of molecular weight distributions

in polymer solutions by SEC ** PA/s/001.03 2000-06

Determination of molecular weight distributions of polymers by size exclusion chromatography (SEC)

PA/s/002.02 1995-06

SEC of coatings, resins and polyesters in THF

1.8 Titrimetric methods for the determination of active ingredient contents and

contaminants in raw materials, intermediate products and final products by potentiometry **

CL/t/001.01 2004-12

Determination of piperazine hexahydrate by the potentiometric determination of basic nitrogen (raw materials)

CL/t/024.01 2007-03

Potentiometric determination of total alkaline content in caustic soda lye

PA/d/026.03 2009-04

Determination of free sulphuric acid in sulfonated polyethersulfone (PES)

1.9 Titrimetric methods for the determination of active ingredient contents and

contaminants in raw materials, intermediate products and final products by visual endpoint determination **

CL/t/010.01 2004-12

Determination of hemicellulose in lye immersions



CL/t/011.02 2008-06

Determination of hydrogen sulphide and carbon disulphide in the spinning bath

CL/t/014.01 2004-12

Determination of gamma number (carbon dioxide method)

1.10 Determination of the physical parameter particle measurement by laser diffraction in

dispersions ** PA/p/025.02 2007-10

Particle measurements in liquids, aqueous media for medical applications and solids

EM/p/003.02 2009-10

Particle size measurement of PMMA samples

1.11 Refractometric determination of the physical parameter refractive index of liquids ** PA/p/021.03 2007-10

Determination of refractive index

CL/k/010.02 2006-04

Measurement of refraction with the RA - 510 M refractometer (refractive index)

1.12 Determination of the physical parameter density of solids

according to the displacement method ** CL/k/014.01 2008-07

Density of solids by the immersion method (displacement method)

DIN EN ISO 845 2006-12

Cellular plastics and rubbers - Determination of apparent density

PC/p/010.01 2012-09

Determination of bulk density

1.13 Determination of the physical parameter density of liquids by the oscillation principle **

EN ISO 15212-1 2009-07

Liquid density according to the oscillation principle



CL/k/011.02 2006-04

Testing of mineral oils and related materials - Determination of density

Pa/p/016.03 2000-02

Determination of density with the flexural resonator

1.14 Determination of the physical parameter density of liquids by the areometer method ** CL/t/039.01 2008-01

Determination of density - H2SO4, MgSO4, ZnSO4 and Na2SO4 in viscose spinning baths

CL/k/011.02 2006-04


DIN 51757 2011-01


1.15 Determination of the physical parameter surface tension of liquids and latices according

to the ring method ** CL/x/007.01 2004-12

Measurement of surface tension by the ring method

DIN ISO 1409 2008-11

Plastic/rubber - polymer dispersions and rubber latices (natural and synthetic) - Determination of surface tension by the ring method

1.16 Determination of the physical parameter colour index of liquids by the visual

comparison method **

CL/x/002.01 2004-12

Iodine colour index

DIN EN ISO 6271-1 2005-03

Clear liquids - Estimation of colour by the platinum-cobalt scale - Part 1: Visual method

1.17 Determination of viscosity in polymers by capillary viscosimetry in diluted solutions ** PA/p/014.02 2002-08

Determination of solution viscosity of sulfonated polyethersulfone (SPES) in sulphuric acid with the Ubbelohde viscosimeter



CL/k/008.01 2004-12

Determination of relative viscosity of polyester

CL/k/009.04 2009-07

Determination of relative viscosity of polyamide solution

1.18 Determination of chemical parameters by visual and potentiometric endpoint

determination ** CL/d/007.01 2004-12

Coulometric KF water determination in polymer granulates

CL/t/013.01 2004-12

Potentiometric determination of free alkali and secondary products

CL/d/025.01 2010-08

HR-II laboratory approach with CuI

CL/d/026.01 2010-12

Iodate test (oxidizing contaminants) in potassium iodide

1.19 Gravimetric determination of sum parameters ** PA/d/021.03 2002-08

Gravimetric residual extraction of SPES

PA/d/034.02 2003-12

Gravimetric additive determination in polypropylene after extraction in the Büchi hot extractor

CL/d/008.01 2004-12

Gravimetric determination of preparation application to yarns and fibres after extraction in the Soxhlet

CL/d/012.02 2006-04

Dry matter content - evaporation residue - weight loss

1.20 Determination of elements in aqueous solutions by atomic absorption spectroscopy

(graphite furnace, flame AAS) **

CL/a/004.01 2005-06

Determination of manganese in lye immersion by THGA-AAS



CL/a/005.01 2010-10

Determination of manganese acetate tetrahydrate in a catalyser preparation

CL/a/006.01 2008-11

Determination of manganese in lye immersion by flame AAS after wet microwave digestion

DIN EN ISO 15586 2004-02

Water quality - Determination of trace elements using atomic absorption spectrometry with graphite furnace

1.21 Determination of elements by atomic absorption spectroscopy with inductively coupled

plasma (ICP-OES) **

CL/a/007.01 2011-04

Determination of noble metals (Pd, Pt, Rh) in ground material of autocatalysts

DIN EN ISO 11885 2009-09

Water quality - Determination of selected elements by inductively coupled plasma optical emission spectrometry (ICP-OES)

CL/a/009.01 2014-03

Determination of elements in yarn after acid digestion or incineration by ICP-OES

1.22 Elemental analysis following combustion (detection principle : ISE) CL/d/010.02 2006-03

FLUORIDE determination by ISE after Schöniger digestion

1.23 Electron microscopic investigations for the characterisation of organic and inorganic

materials by SEM and TEM and for qualitative determination of elemental composition by EDX **

EM/e/002.03 2000-03

Characterisation of pore structure in membranes

EM/e/009.04 2009-10

Characterisation of Ostim samples with TEM

1.24 Light microscopic analysis for the characterisation of organic and inorganic

materials **

EM/l/003.01 1997-11

Polished section preparation for light microscopy



EM/l/004.01 1997-11

Streakiness of fabrics, knitted fabrics and warp-knitted textiles

DIN EN ISO 1463 2004-08

Metallic and oxide coatings - Measurement of coating thickness - Microscopical method

1.25 X-ray fluorescence analysis (XRF) of solids and liquids **

SP/f/002.02 2005-09

Determination of catalysts in polyester by XRF

SP/f/004.02 2005-09

Determination of K, Cu, Br and I in polyamide by XRF

SP/f/006.03 2014-08

Qualitative XRF analysis and semi-quantitative concentration calculation of solids from atomic number 9 and powdered samples and liquids from atomic number 11

SP/f/007.05 2011-07

Quantitative determination of phosphorus and calcium by XRF in Ostim suspensions

1.26 X-ray diffraction analysis for phase analysis of solids **

XR/d/003.03 2009-09

Determination of structure parameters of PA6.6 yarn by WAXS

XR/d/010.04 2009-10

Phase analysis and crystallite size determination of Ostim samples

ISO 13779-3 2008-02

Implants for surgery - Hydroxyapatite - Part 3: Chemical analysis and characterization of crystallinity and phase purity

1.27 Electron spectroscopic investigations (ESCA/XPS) for the determination of surface

compositions, functional groups and oxidation states **

EM/x/002.04 2009-04

Execution of XPS depth profiles

EM/x/003.02 2002-07

Execution of angle-dependent XPS measurements



EM/x/004.02 2002-07

Determination of oxidation states and functional groups with ESCA

1.28 N2 sorption measurements for the characterisation of surfaces of porous solids

XR/p/001.03 2009-10

Measurement of N2 sorption of organic and inorganic chemicals and polymers with the Sorptomatic 1900

XR/p/002.03 2009-10

Measurement of N2 adsorption of organic and inorganic chemicals and polymers with the Sorptomatic 1900

2 Material testing 2.1 Fogging behaviour of polymer materials by gravimetry and reflectrometry *

Test type Measured value/test parameter

Measurement and test range

Examples of methods

Fogging behaviour Mass

0.08 mg - max. 100 mg

DIN 75201 SAE J1756 PSA D45 1727 Volvo VCS 1027,2719 GM GMW 3235 VW PV 3015

Reflection change at 60°

0 - 100 %

DIN 75201 2011-11

Determination of the fogging characteristics of trim materials in the interior of automobiles

SAE J1756 1994-12

Test procedure to determine the fogging characteristics of interior automotive materials

PSA D45 1727 1997-11

Materials - interior trim - fogging

Volvo VCS 1027,2719 2004-01

Test method - fogging - organic materials

GM GMW 3235 2005-05

Fogging characteristics of trim materials

VW PV 3015 1994-05

Non-metallic materials for interior trim - Determining condensable constituents



2.2 Fire testing of polymer materials with burning box *



Examples of methods

Fire testing Burning rate 0 - 100 cm/min DIN 75200 FMVSS 302 VW TL 1010 GM GMW 3232 DBL 5307

DIN 75200 1980-09

Determination of burning behaviour of interior materials in motor vehicles

FMVSS 302 1999-01

Flammability of interior materials

VW TL 1010 2008-01

Materials for vehicle interiors Burning behavior, material requirements

GM GMW 3232 2005-08

Test method for determining the flammability of interior trim materials

DBL 5307 2008-03

Supply specification Flame retardant properties - Interior trim parts - Requirements and test specifications

2.3 Odour testing of polymer materials by olfactory evaluation *



Examples of methods

Odour testing Odour impression (evaluation scale)

not perceptible to not acceptable

VDA 270 VW PV 3900 GM GME 60276 GM GMW 3205 Ford BO 131-03

VDA 270 1992-10

Determination of the odour characteristics of trim materials in motor vehicles

VW PV 3900 2000-08

Components in passenger compartment Odor test



GM GME 60276 2000-08

Test Method for determining the resistance to odour Propagation of trim materials

GM GMW 3205 2000-12

Test method for determining the resistance to odor propagation of interior materials

Ford BO 131-03 2013-10

Determination and assessment of odor from interior trim materials/components/assemblies

2.4 Static tensile test of polymers *



Examples of methods

Tensile test E-modulus, tensile forces

1 N - 20 kN, -70 °C - 250 °C

DIN EN ISO 527-1

Tensile forces 0.1 N - 500 N, -70 °C - 250 °C

DIN EN ISO 1798

"permanent" deformations

all normative parameters

DIN EN ISO 1856

DIN EN ISO 527-1 2012-06

Plastics - Determination of tensile properties - Part 1: General principles

DIN EN ISO 1798 2008-04

Flexible cellular polymeric materials - Determination of tensile strength and elongation at break

DIN EN ISO 1856 2008-01

Flexible cellular polymeric materials - Determination of compression set

2.5 Static hardness testing of semi-finished products, pre-products and polymer materials *



Examples of methods

Hardness testing Hardness Rockwell - C DIN EN ISO 6508-1

Hardness 49N, 132N, 358N, 961N

DIN EN ISO 2039-1

Scale ranges Scale A and Scale D DIN ISO 7619-1

DIN EN ISO 6508-1 2013-03

Metallic materials - Rockwell hardness test - Part 1: Test method



DIN EN ISO 2039-1 2003-06

Plastics - Determination of hardness - Part 1: Ball indentation method

DIN ISO 7619-1 2012-02

Rubber, vulcanized or thermoplastic - Determination of indentation hardness - Part 1: Durometer method (Shore hardness)

2.6 Testing mechanical properties of polymers *



Examples of methods

Mechanical properties

Impact energy 0.1 - 12 J (1 - 15 J pendulum)

DIN EN ISO 179-1

Impact energy 0.1 – 4.4 J (1 - 5.5 J pendulum)

DIN EN ISO 180

Heat deflection temperature

25 - 200 °C DIN EN ISO 75-1 Method A Method C

Softening temperature 25 - 200 °C DIN EN ISO 306 A50, B50, A120, B120

DIN EN ISO 179-1 2010-11

Plastics - Determination of Charpy impact properties - Part 1: Non-instrumented impact test

DIN EN ISO 180 2013-08

Plastics - Determination of Izod impact strength

DIN EN ISO 75-1 2013-08

Plastics - Determination of temperature of deflection under load - Part 1: General test method

DIN EN ISO 306 2014-03

Plastics - Thermoplastic materials - Determination of Vicat softening temperature (VST)

2.7 Thermoanalytical investigations of polymer materials ** XR/b/002.03 2002-09

Determination of melting temperature and enthalpy of fusion

XR/b/004.03 2002-09

Determination of crystallisation temperature and enthalpy of crystallisation



XR/b/006.03 2002-09

Determination of glass transition temperature Tg

XR/b/013.03 2002-09

Change in sample mass as a function of temperature

2.8 Rheological properties of polymer solutions and polymer melts * CL/r/001.01 2004-12

Determination of viscosity with the falling sphere viscometer

CL/r/002.02 2006-03

Measurement of viscosity according to Brookfield

DIN EN ISO 1133-1 2012-03

Plastics - Determination of the melt mass-flow rate (MFR) and melt volume-flow rate (MVR) of thermoplastics - Part 1: Standard method



2.9 Environmental simulation testing of the mechanical, climatic and chemical ageing of plastics *



Examples of methods

Environmental simulation testing

Irradiance Xenochrome 300: 45 - 120 W/m² Xenochrome 320: 35 - 100 W/m²

ISO 105-B06

Sample chamber temperature

20 - 80 °C

Black standard temperature

25 - 130 °C

Range of humidity 10 - 95 %

Visual evaluation Colour fastness acc. to grey scale ISO 105-A02 grey scale steps 1-5

or acc. to light fastness types 1-8

Temperature

Room temperature - 300°C

DIN 53497

Visual evaluation -

Dimensional stability/ control

0 - 2000 mm

Temperature range Room temperature - 55°C

DIN EN ISO 9227

Spray pressure max. 1.5 bar

Salt concentration 5% NaCl

Visual evaluation after load

1 , 5 , 10 N test force Repetitions: 101, 102, 103, 104, 105, 106, 107

DIN EN 60068-2-70

ISO 105-B06 1998-11

Textiles - Tests for colour fastness - Part B06: Colour fastness and ageing to artificial light at high temperatures: Xenon arc fading lamp test

DIN 53497 1969-10

Testing of plastics; Hot storage test on mouldings made of thermoplastic moulding materials without external mechanical stressing



DIN EN ISO 9227 2012-09

Corrosion tests in artificial atmospheres - Salt spray tests

DIN EN 60068-2-70 1996-07

Environmental testing - Part 2: Tests - Test Xb: Abrasion of markings and letterings caused by rubbing of fingers and hands

2.10 Measurement of volume flows MT/p/006.01 1997-09

General instruction for volume flow measurement of gaseous media in conduits (Deviation: Matrix also laboratory fume hoods) in conjunction with:

VDI/VDE 2640 sheet 3 1983-11

Measurement of gas flow in circular; annular or rectangular sections of conduits velocity area method

2.11 Testing of parts (semi-finished products, pre-products) for the evaluation of

performance characteristics TP/f/001.02 2014-08

Dimensional checks of length

TP/f/003.02 2014-08

Run-out inspection

TP/f/004.01 2005-12

Coating thickness measuring by the magnetic induction method

DIN EN ISO 4288 1998-04

Geometrical Product Specifications (GPS) - Surface texture: Profile method - Rules and procedures for the assessment of surface texture

3 Machine Acoustics 3.1 Noise at the workplace *** DIN 45645-2 2012-09

Determination of rating levels from measurement data - Part 2: Determination of the noise rating level for occupational activities at the work place for the level range underneath the given risk of hearing damage



DIN EN ISO 9612 2009-09

Acoustics - Determination of occupational noise exposure - Engineering method

4 List of testing methods for the expert module water

Version: LAWA of 23.03.2012 The expert module water distinguishes fundamentally between three areas of investigation:

Waste water (WW),

Surface water (SW),

Groundwater and untreated water (GUW), Sub-area 1: Sampling and general parameters

Parameter Method WW SW GUW

Sampling waste water DIN 38402-A 11: 1995-12

DIN 38402-A 11: 2009-02

Sampling from running waters DIN 38402-A 15: 1986-07

DIN 38402-A 15: 2010-04

Sampling from aquifiers DIN 38402-A 13: 1985-12

Sampling from barrages and lakes DIN 38402-A 12: 1985-06

Homogenisation of samples DIN 38402-A 30: 1998-07

Temperature DIN 38404-C 4: 1976-12

pH DIN 38404-C 5: 1984-01

DIN 38404-C 5: 2009-07

Conductivity (25°C) DIN EN 27888: 1993-11 (C 8)

Odour DIN EN 1622: 2006-10 (B 3) Annex C

Colour DIN EN ISO 7887: 1994-12 (C 1) Section 2

Turbidity DIN EN ISO 7027: 2000-04 (C 2)

Oxygen DIN EN 25814: 1992-11 (G 22)

Redox potential DIN 38404-C 6: 1984-05

Sub-area 2: Photometry, ion chromatography and volumetric analysis


UV absorption at 254 nm (SAC 254) DIN 38404-C 3: 2005-07

UV absorption at 436 nm (SAC 436) DIN EN ISO 7887: 1994-12 (C 1)

Ammonia nitrogen

DIN EN ISO 11732: 1997-09 (E 23)

DIN EN ISO 11732: 2005-05 (E 23)

DIN 38406-E 5: 1983-10

DIN EN ISO 14911: 1999-12 (E 34)




Nitrite nitrogen

DIN EN 26777: 1993-04 (D 10)

DIN EN ISO 10304-1: 1995-04 (D 19)

DIN EN ISO 10304-1: 2009-07 (D 20)

DIN EN ISO 10304-2: 1996-11 (D 20)

DIN EN ISO 13395: 1996-12 (D 28)

Nitrate nitrogen

DIN EN ISO 10304-1: 1995-04 (D 19)

DIN EN ISO 10304-1: 2009-07 (D 20)

DIN EN ISO 10304-2: 1996-11 (D 20)

DIN EN ISO 13395: 1996-12 (D 28)

DIN 38405-9-2 / 9-3: 1979-05

DIN 38405-D 29: 1994-11

Total phosphorus

DIN EN 1189: 1996-12 (D 11)

DIN EN ISO 6878: 2004-09 (D 11)

DIN EN ISO 15681-1: 2005-05 (D 45)

DIN EN ISO 15681-2: 2005-05 (D 46)

Orthophosphate

DIN EN ISO 10304-1: 1995-04 (D 19)

DIN EN ISO 10304-1: 2009-07 (D 20)

DIN EN 1189: 1996-12 (D 11)

DIN EN ISO 6878: 2004-09 (D 11)

DIN EN ISO 15681-1: 2005-05 (D 45)

DIN EN ISO 15681-2: 2005-05 (D 46)

Fluoride (dissolved and total)

DIN 38405-D 4: 1985-07

DIN EN ISO 10304-1: 1995-04 (D 19)

DIN EN ISO 10304-1: 2009-07 (D 20)

Chloride

DIN 38405-D 1: 1985-12

DIN EN ISO 10304-1: 1995-04 (D 19)

DIN EN ISO 10304-1: 2009-07 (D 20)

DIN EN ISO 10304-2: 1996-11 (D 20)

DIN EN ISO 10304-4: 1999-07 (D 25)

DIN EN ISO 15682: 2002-01 (D 31)

Sulphate

DIN EN ISO 10304-1: 1995-04 (D 19)

DIN EN ISO 10304-1: 2009-07 (D 20)

DIN EN ISO 10304-2: 1996-11 (D 20)

DIN 38405-D 5: 1985-01

Cyanide (readily liberated)

DIN 38405-D 13-2: 1981-02

DIN 38405-D 14-2: 1988-12

DIN EN ISO 14403: 2002-07 (D 6)

DIN 38405-D 7: 2002-04




Cyanide (total)

DIN 38405-D 13-1: 1981-02

DIN 38405-D 14-1: 1988-12

DIN EN ISO 14403: 2002-07 (D 6)

DIN 38405-D 7: 2002-04

Chromium VI DIN 38405-D 24: 1987-05

DIN EN ISO 10304-3: 1997-11 (D 22), Section 5 (dissolved chromate)

Sulphide (readily liberated) DIN 38405-D 27: 1992-07

Sub-area 3: Elemental analysis


Aluminium

DIN EN ISO 11885: 1998-04 (E 22)

DIN EN ISO 11885: 2009-09 (E 22)

DIN EN ISO 12020: 2000-05 (E 25)

DIN EN ISO 17294-2: 2005-02 (E 29)

DIN EN ISO 15586: 2004-02 (E 4)

Arsenic

DIN EN ISO 11969: 1996-11 (D 18)

DIN EN ISO 11885: 1998-04 (E 22)

DIN EN ISO 11885: 2009-09 (E 22)

DIN EN ISO 17294-2: 2005-02 (E 29)

DIN EN ISO 15586: 2004-02 (E 4)

Lead

DIN 38406-E 6: 1998-07

DIN EN ISO 11885: 1998-04 (E 22)

DIN EN ISO 11885: 2009-09 (E 22)

DIN 38406-E 16: 1990-03

DIN EN ISO 17294-2: 2005-02 (E 29)

DIN EN ISO 15586: 2004-02 (E 4)

Cadmium

DIN EN ISO 5961: 1995-05 (E 19)

DIN EN ISO 11885: 1998-04 (E 22)

DIN EN ISO 11885: 2009-09 (E 22)

DIN 38406-E 16: 1990-03

DIN EN ISO 17294-2: 2005-02 (E 29)

DIN EN ISO 15586: 2004-02(E 4)

Calcium

DIN EN ISO 11885: 1998-04 (E 22)

DIN EN ISO 11885: 2009-09 (E 22)

DIN 38406-E 3: 2002-03

DIN EN ISO 7980: 2000-07 (E 3a)

DIN EN ISO 17294-2: 2005-02 (E 29)

DIN EN ISO 14911: 1999-12 (E 34)




Chromium

DIN EN ISO 11885: 1998-04 (E 22)

DIN EN ISO 11885: 2009-09 (E 22)

DIN EN 1233: 1996-08 (E 10)

DIN EN ISO 17294-2: 2005-02 (E 29)

DIN EN ISO 15586: 2004-02 (E 4)

Iron

DIN EN ISO 11885: 1998-04 (E 22)

DIN EN ISO 11885: 2009-09 (E 22)

DIN 38406-E 1: 1983-05

DIN 38406-E 32: 2000-05

DIN EN ISO 15586: 2004-02 (E 4)

Potassium

DIN 38406-E 13: 1992-07

DIN EN ISO 11885: 1998-04(E 22)

DIN EN ISO 11885: 2009-09 (E 22)

DIN EN ISO 17294-2: 2005-02 (E 29)

DIN EN ISO 14911: 1999-12 (E 34)

Copper

DIN EN ISO 11885: 1998-04 (E 22)

DIN EN ISO 11885: 2009-09 (E 22)

DIN 38406-E 7: 1991-09

DIN 38406-E 16: 1990-03

DIN EN ISO 17294-2: 2005-02 (E 29)

DIN EN ISO 15586: 2004-02 (E 4)

Manganese

DIN EN ISO 11885: 1998-04 (E 22)

DIN EN ISO 11885: 2009-09 (E 22)

DIN EN ISO 17294-2: 2005-02 (E 29)

DIN 38406-E 33: 2000-06

DIN EN ISO 15586: 2004-02 (E 4)

DIN EN ISO 14911: 1999-12 (E 34)

Sodium

DIN 38406-E 14: 1992-07

DIN EN ISO 11885: 1998-04 (E 22)

DIN EN ISO 11885: 2009-09 (E 22)

DIN EN ISO 17294-2: 2005-02 (E 29)

DIN EN ISO 14911: 1999-12 (E 34)

Nickel

DIN EN ISO 11885: 1998-04 (E 22)

DIN EN ISO 11885: 2009-09 (E 22)

DIN 38406-E 11: 1991-09

DIN EN ISO 17294-2: 2005-02 (E 29)

DIN 38406-E 16: 1990-03

DIN EN ISO 15586: 2004-02 (E 4)




Mercury

DIN EN 1483: 1997-08 (E 12)

DIN EN 1483: 2007-07 (E 12)

DIN EN 12338: 1998-10 (E 31)

DIN EN 13506: 2002-04 (E 35)

DIN EN 17852: 2008-04 (E 35)

Zinc

DIN EN ISO 11885: 1998-04 (E 22)

DIN EN ISO 11885: 2009-09 (E 22)

DIN 38406-E 8-1: 2004-10

DIN 38406-E 16: 1990-03

DIN EN ISO 17294-2: 2005-02 (E 29)

DIN EN ISO 15586: 2004-02 (E 4)

Boron

DIN EN ISO 11885: 1998-04 (E 22)

DIN EN ISO 11885: 2009-09 (E 22)

DIN 38405-D 17: 1981-03

DIN EN ISO 17294-2: 2005-02 (E 29)

Magnesium

DIN EN ISO 11885: 1998-04 (E 22)

DIN EN ISO 11885: 2009-09 (E 22)

DIN 38406-E 3: 2002-03

DIN EN ISO 7980: 2000-07 (E 3a)

DIN EN ISO 17294-2: 2005-02 (E 29)

DIN EN ISO 14911: 1999-12 (E 34)

Phosphorus

DIN EN ISO 17294-2: 2005-02 (E 29)

DIN EN ISO 11885: 1998-04 (E 22)

DIN EN ISO 11885: 2009-09 (E 22)

Sub-area 4/5: Group and sum parameters


Biological oxygen demand (BOD5) DIN EN 1899-1: 1998-05 (H 51)

DIN EN 1899-2: 1998-05 (H 52)

Chemical oxygen demand (COD)

DIN 38409-H 41: 1980-12

DIN 38409-H 44: 1992-05

DIN ISO 15705: 2003-01 (H 45)

Phenol index (with and without distillation)

DIN 38409-H 16: 1984-06

DIN EN ISO 14402: 1999-12 (H 37)

Filterable matter DIN 38409-H 2: 1987-03

DIN EN 872: 2005-04 (H 33)

Acid and base-neutralizing capacities DIN 38409-H 7: 2005-12

Total organic carbon (TOC) DIN EN 1484: 1997-08 (H 3)

Dissolved organic carbon (DOC) DIN EN 1484: 1997-08 (H 3)




Total bound nitrogen (TNb)

DIN ENV 12260: 1996-06 (H 34)

DIN EN 12260: 2003-12 (H 34)

DIN EN ISO 11905-1: 1998-08 (H 36)

Adsorbable organically bound halogens (AOX)

DIN EN 1485: 1996-11 (H 14)

DIN EN ISO 9562: 2005-02 (H 14)

DIN 38409-H 22: 2001-02

Sub-area 6: Gas chromatographic methods

not applicable Sub-area 7: HPLC methods

not applicable Sub-area 8: Microbiological methods

not applicable Sub-area 9.1: Biological methods, biotests (Part 1)

not applicable Sub-area 9.2: Biological methods, biotests (Part 2)

not applicable Abbreviations used: AAS Atomic Absorption Spectroscopy AOX Adsorbable organically bound halogens BOD Biological Oxygen Demand CH/g In-house methods - Gas chromatography SOP CH/h In-house methods - Liquid chromatography SOP CL/a In-house methods - Atomic spectrometry SOP CL/d In-house methods - Chemical parameters/gravimetry/elemental analysis SOP CL/g In-house methods - Gas chromatography SOP CL/i In-house methods - IR spectroscopy SOP CL/k In-house methods - Physical parameters SOP CL/p In-house methods - UV-VIS/fluorescence spectroscopy SOP CL/r In-house methods - Rheology SOP CL/t In-house methods - Volumetric analyses/Titrimetric methods SOP CL/x In-house methods - Wet chemistry and parameter determination SOP COD Chemical oxygen demand



DAD Diode array detector DBL Daimler-Benz Liefervorschrift (Daimler-Benz supply specification) DIN Deutsches Institut für Normung e. V. (German Institute for Standardization) DOC Dissolved organic carbon DMpT Dimethyl-p-toluidine EDX Energy dispersive X-ray spectroscopy EM/e In-house methods - Electron microscopy SOP EM/l In-house methods - Light microscopy SOP EM/p In-house methods - Physical parameters SOP EM/x In-house methods - XPS/ESCA SOP EN European standard FID Flame ionisation detector FMVSS Federal Motor Vehicle Safety Standard Ford BO Ford Laboratory Test Method FT FTIR

Fourier transformation Fourier transform infrared spectroscopy

GC Gas chromatography GM General Motors Company GME General Motors Europe Engineering Standards GMW General Motors Worldwide Engineering Standards HPLC High performance liquid chromatography HR Heat resistance ICP/OES Inductively coupled plasma optical emission spectrometry IEC International Electrotechnical Commission IR Infrared ISE Ion-selective electrode ISO International Standards Organization KF Karl Fischer LAWA Bund/Länder-Arbeitsgemeinschaft Wasser (German Working Group on water

issues of the Federal States and the Federal Government) MFR Melt mass-flow rate MMA Methacrylic acid methyl ester MT/p In-house methods - Material- and product-specific properties SOP MS Mass spectrometry MVR Melt volume flow rate NMR Nuclear magnetic resonance NIR Near infrared PA Polyamide PA/d In-house methods - Wet chemistry and parameter determination SOP PA/p In-house methods - Physical parameters SOP PA/s In-house methods - Size exclusion chromatography SOP PES PMMA

Polyethersulfone Polymethyl methacrylate

PSA Peugeot Société Anonyme (Peugot corporation) RI Refractive index



SAC Spectral absorption coefficient SAE Society of Automotive Engineers SEC SEM SOP

Size exclusion chromatography Scanning electron microscopy Standard operating procedure

SPES Sulfonated PES SP/f In-house methods - X-ray fluorescence analysis SOP SP/i In-house methods - IR- spectroscopy SOP SP/n In-house methods - NMR spectroscopy SOP SP/r In-house methods - Raman spectroscopy SOP SP/u In-house methods - UV-VIS/ fluorescence spectroscopy SOP TEM Transmission electron microscopy THF Tetrahydrofuran Tg Glass transition temperature THGA Transversally heated graphite atomizator TN Total nitrogen TOC Total organic carbon TP/f In-house methods - Evaluation of performance characteristics SOP UV/VIS Ultraviolet/visible VCS Volvo Cars standards VDA Verband der Automobilindustrie (German Association of the Automotive

Industry) VDE Verband der Elektrotechnik Elektronik Informationstechnik e. V.

(Association for Electrical, Electronic and Information Technologies) VDI Verein Deutscher Ingenieure (The Association of German Engineers) VST Vicat softening temperature VW PV Volkswagen Prüfvorschrift (Volkswagen test specification) VW TL Volkswagen Technische Lieferbedingung

(Volkswagen technical purchase specification) WAXS Wide-angle X-ray scattering XPS/ESCA X-ray photoelectron spectroscopy/

electron spectroscopy for chemical analysis XR/b In-house methods - Thermoanalysis SOP XR/d XRF

In-house methods - X-ray diffraction SOP X-ray fluorescence analysis

XR/p In-house methods - Sorption measurements SOP

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