db contract documents part 7 engineering data …...dimensions (drilling contractor) utilizing the...

BUFFALO STATION

PIN 5761.87, Contract D900044

DB CONTRACT DOCUMENTS

PART 7ENGINEERING DATA

Final May 11, 2018

New York State Department of Transportation

Buffalo Station i Part 7 - Engineering DataPIN 5761.87, Contract D900044 Final May 11, 2018

ENGINEERING DATA


Buffalo Station ii Part 7 - Engineering DataPIN 5761.87, Contract D900044 Final May 11, 2018

PHASE II ENVIRONMENTAL ASSESSMENT REPORTPRELIMINARY SCREENING REPORT FOR THE HAZARDOUS WASTE/

CONTAMINATED MATERIALS ASSESSMENT

95 Per r y S t reet , Su i te 300 Bu f fa lo, New York 14203

p : 716.206.5100 f : 716.206.5199

PHASE II ENVIRONMENTAL SITE ASSESSMENT REPORT

FOR THE

HAZARDOUS WASTE/CONTAMINATED MATERIALS (HW/CM) INVESTIGATION

OF THE

BUFFALO AMTRAK STATION

75 EXCHANGE STREET BUFFALO, ERIE COUNTY, NEW YORK

MAY 2018

PREPARED FOR: WSP/PARSONS BRINCKERHOFF 50 LAKEFRONT BOULEVARD SUITE 111 BUFFALO, NEW YORK FOR SUBMISSION TO: NEW YORK STATE DEPARTMENT OF TRANSPORTATION 100 SENECA STREET BUFFALO, NEW YORK 14203

O:\2017\17005 NYSDOT RDSA\1700502 BUFFALO TRAIN STATION DESIGN\10. ENV\10.E. HWCM DSI\AMTRAK DSI REPORT.DOCX May 2, 2018 1

TABLE OF CONTENTS

Section Page

EXECUTIVE SUMMARY .................................................................................................... 2

1.0 INTRODUCTION ................................................................................................. 3

1.1 Purpose and Scope ..................................................................................... 3 1.2 NYSDOT Project Description ....................................................................... 3 1.3 Project Area Description .............................................................................. 3

2.0 FIELD INVESTIGATION RESULTS ............................................................................ 4

2.1 Soil Boring Investigation - Field Investigation ................................................. 4 2.1.1 Findings .......................................................................................... 6

3.0 ANALYTICAL METHODOLOGY AND LABORATORY RESULTS .................................. 8

3.1 Soil Samples .............................................................................................. 8 3.2 Analytical Findings ...................................................................................... 8

LIST OF TABLES

Table 2-1 Sample Locations .......................................................................................... 5 Table 3-1 Analytical Detections and Comparison to

NYSDEC Regulatory Criteria ........................................................ follows page 8

LIST OF FIGURES

Figure 1 Project Location Map .................................................................. follows page 3 Figure 2 Soil Boring Locations................................................................... follows page 4

LIST OF ATTACHMENTS

Attachment A Soil Boring Logs Attachment B Photographs Attachment C Laboratory Reports


EXECUTIVE SUMMARY Watts Architecture & Engineering (Watts) was retained by WSP/Parsons Brinckerhoff (WSP) to perform a Phase II Environmental Site Assessment (Phase II) for the Hazardous Waste/Contaminated Materials (HW/CM) Investigation of the proposed NYSDOT Amtrak Station Replacement project, in the City of Buffalo, Erie County, New York. The program was developed to investigate the potential of on-site subsurface environmental concerns associated with the “subject property” aka the Amtrak Exchange Street Station and the proposed project actions. The property has been used as a passenger rail line corridor for over 100 years and therefore, impacts were anticipated to be those likely to disturb the soil and fill material by the proposed construction project. As such, a soil boring investigation (SBI) was conducted at fourteen (14) boring locations identified to correspond to future facility features and areas of soil disturbance. Soils returned from each boring were screened in the field with a photoionization detector for volatile vapors and representative samples were collected and submitted for laboratory analysis. The SBI was conducted the weeks of March 12th to 19th, and April 2nd to 5th, 2018. Weather during the field activities was primarily in the 30’s°F with mostly cloudy conditions and intermittent snowfall and rainfall. The outcome of the SBI and sampling results indicate that contaminated non-hazardous fill (e.g. slag, cinders, brick, glass, wood, concrete, and reworked native soils) of an inconsistent nature is present throughout the subject property. The average thickness of the fill unit is approximately 5 to 6 feet. Based on the field investigation, the entire site has a potential to exhibit low level contaminated soils during excavation within the project limits. Any excess soils should be stockpiled and subsequently sampled, analyzed and characterized for proper handling and disposal. At this time it is our interpretation that any soil/fill that cannot be reused and incorporated into the construction plans will need to be transported off-site for disposal in a NYSDEC-permitted solid waste landfill facility.


1.0 INTRODUCTION Watts Architecture & Engineering (Watts) was retained by WSP/Parsons Brinckerhoff (WSP) to perform a Phase II Environmental Site Assessment (Phase II) for the Hazardous Waste/Contaminated Materials (HW/CM) Investigation of the proposed NYSDOT Amtrak Station Replacement project, in the City of Buffalo, Erie County, New York. This report was prepared for the NYSDOT. The project limits are shown on a USGS map in Figure 1 – Project Location Map.

1.1 Purpose and Scope

The purpose of the investigation is to identify the presence of soil contamination, fill, and other environmental concerns located within the proposed construction zone or area of property acquisition. Concerns addressed by the HW/CM Investigation are the protection of the environment, the health and safety of construction workers and the public, and the projection of construction costs due to special handling requirements for contaminated materials.

The field work consisted of a soil boring investigation at fourteen (14) locations (BH1-18 through BH14-18), collection of soil samples and laboratory analysis of the collected samples. This report presents the results of the field work.

1.2 NYSDOT Project Description

The proposed project involves the development of preliminary track, platform, station, and site layouts for the replacement of the Buffalo Exchange Street Amtrak Station, which will be advanced into construction by NYSDOT through a Design-Build Procurement process. The design for the new station is limited to the replacement of the existing Buffalo Exchange Street Station. Intercity bus is not assumed as part of this design effort. The new station will be fully ADA compliant.

1.3 Project Area Description

The general project area has been developed as a passenger rail station and has seen active rail line use for over 100 years. The Buffalo-Exchange Street Station was originally built by the New York Central Railroad. There have been four New York Central Railroad stations on Exchange Street in Buffalo, the third of which was built in 1880. It was closed on November 13, 1935 with the current station having opened on August 2, 1952.

NOT TO SCALE APRIL 2018

FIGURE 1 - SITE LOCATION MAP

DETAILED SITE INVESTIGATION REPORT

NFTA – AMTRAK/EXCHANGE ST. STATION

BUFFALO, NY

SOURCE: This figure includes information from the BUFFALO NW,

BUFFALO NE AND BUFFALO SE (1965) 7.5-minute topographic

quadrangle maps.

SITE


2.0 FIELD INVESTIGATION RESULTS The field program included a soil boring investigation at fourteen (14) locations implementing real-time measurement of volatile organic vapors using a photoionization detector (PID) calibrated to detect petroleum and other solvents. In addition, sixteen (16) soil samples were collected and submitted for laboratory analysis for both total organic and inorganic concentrations [following the NYSDEC 6 NYCRR Part 375 Target Compound and Target Analyte Lists] and following USEPA Toxicity Characteristic Leaching Procedure (TCLP) procedures for determination of toxicity as well as for the Resource Conservation and Recovery Act (RCRA) hazardous waste criteria of Ignitability (D001) and Corrosivity (D002). Soil borings were located in the field by McMahan & Mann (geotechnical Consultant) and Earth Dimensions (drilling Contractor) utilizing the preliminary design drawing provided by WSP. Soil boring locations were identified within the field by marking with white paint, and numbered sequentially based on the order of completion. See Figure 2 – Soil Boring Locations for the locations of the individual soil borings. A description of the field investigation is presented below. Refer to Section 3.0 for the laboratory analytical results.

2.1 Soil Boring Investigation - Field Investigation

The soil boring investigation and soil sampling was executed utilizing a truck-mounted Diedrich D-50 drill rig operated by Earth Dimensions, Inc. out of Elma, New York. Underground utilities were marked prior to field work in the project area. Soil borings were logged and the collected samples were sent to a laboratory for chemical analysis according to the analytical program outlined in Section 3.0.

Fourteen (14) boring locations were advanced with the depth of the investigation at each location determined by the depth to bedrock and/or depth of auger or sampler refusal, or the proposed depth of construction.

During the investigation, Watts personnel was present at all times to:

• Assist with the supervision of the drilling operations; • Perform organic vapor monitoring of the work zone and returned soils using a PID; • Log soil descriptions where soil cores were collected for laboratory analysis; • Collect soil samples; and, • Properly label, package and ship samples to the lab.

The soil boring investigation consisted of advancing 3.25-inch inner diameter hollow stem augers into the soil at each location using the drilling rig. At each boring

FIGURE 2 – SOIL BORING LOCATION MAP

DETAILED SITE INVESTIGATION REPORT

NFTA – AMTRAK/EXCHANGE ST. STATION

BUFFALO, NY

APRIL 2018

NOT TO SCALE

BH1-18

BH4-18

BH3-18

BH2-18

BH11-18

BH5-18

BH6-18

BH7-18

BH8-18

LEGEND

NEW FACILITY FOOTPRINT AREA BORINGS

PICKUP/DROP-OFF AREA/PARKING AREA BORINGS

PLATFORM AREA BORINGS

BH10-18

BH9-18

(beneath ramp)

BH12-18 BH13-18

(beneath ramp)

BH14-18

(beneath ramp)


location, volatile organic vapor concentrations were measured with a PID in the borehole. In addition, soil cores were continually obtained utilizing a 2 foot split-spoon sampler from each soil boring investigation point and examined for signs of visual contamination as well as soil lithology, color, moisture content, and compaction. PID readings were also obtained from the soils retrieved from within each 2 foot split-spoon sampler. Soil samples were then collected from the soils returned from the boring locations and submitted for laboratory analysis. Table 2-1 Sample Locations identifies the boring from where each sample was collected. Samples were not collected for analysis from each boring except for the volatile fraction. Instead, samples collected from the proposed Pick-Up/Drop-Off Area, Station Footprint Area, and Parking Area were collected using a composite sample collected from two borehole locations in each area to better gauge soil conditions across that portion of the site and be reflective of the work proposed in that area. However, samples were collected for analysis from each of the Platform Area borings, except for BH11-18, which yielded insufficient soil volume for sample collection.

TABLE 2-1 SAMPLE LOCATIONS

Sample Identification

Sample ID and Analysis Boring Sample Was Collected From

New Facility Footprint Area L1808681-01 BH1-18 (Total VOC only) Borehole 1 L1809330-01 BH2-18 (Total VOC only) Borehole 2 L1808681-02 BH3-18 (TCLP VOC only) Borehole 3 L1809330-02 BH4-18 (TCLP VOC only) Borehole 4 L1808681-03 BH1/3-18 (Remaining Parameters) Boreholes 1&3 (composite) L1809330-03 BH2/4-18 (Remaining Parameters) Boreholes 2&4 (composite)

Drop-Off/Pick-Up Area L1809330-04 BH6-18 (Total VOC only) Borehole 6 L1809330-05 BH6-18 (TCLP VOC only) Borehole 6 L1809330-06 BH5/6-18 (Remaining Parameters) Boreholes 5&6 (composite)

Parking Area L1809330-07 BH8-18 (Total VOC/TCLP VOC only) Borehole 8 L1809330-08 BH7/8-18 (Remaining Parameters) Boreholes 7&8 (composite)

Platform Area L1811425-01 BH9-18 (Full Analytical Suite) Borehole 9

L1811425-02/03 BH10-18 (Full Analytical Suite) Borehole 10 L1811694-03 BH12-18 (Full Analytical Suite) Borehole 12

L1811425-04 BH13-18 (Full Analytical Suite) Borehole 12 L1811694-01/02 BH14-18 (Full Analytical Suite) Borehole 14


2.1.1 Findings

Soil conditions from all fourteen (14) borings identified the presence of slag, cinders, brick, glass, road base material and placed fill/soil. The soil boring logs containing the observations made during the investigation for all fourteen (14) borings with basic soil descriptions and PID readings can be found in Attachment A. Photographs from the investigation are found in Attachment B.

Visual signs of fill were identified within the all of the borings. Fill material can generally be described as native silt and sand, with varying quantities of gravel and comingled debris. Fill was observed across the majority of the site to an average depth of 5 to 6 feet below ground surface (bgs). The thickness of the fill layer exhibited a general increase toward the southeast and surrounding the existing station. Beneath the fill unit, the soils consisted of fine grained silt and clay-rich lacustrine till, brown to brown-gray in color, moist/wet. For the purpose of this investigation, soil boring depths were variable, and were completed as follows:

• BH1-18: continuous sampling (2-foot intervals) to bedrock, and core 10 feet into bedrock;

• BH2-18, and BH14-18: continuous sampling (2-foot intervals) to 20’ bgs, then one final sample from 23’-25’ bgs, and install groundwater piezometer;

• BH3-18: continuous sampling (2-foot intervals) to 20’ bgs, then sample every five feet to bedrock, and core 10 feet into bedrock;

• BH4-18, BH10-18, BH11-18 and BH12-18: continuous sampling (2-foot intervals) to 20’ bgs, then one final sample from 23’-25’ bgs;

• BH5-18, BH6-18, BH7-18 and BH8-18: continuous sampling (2-foot intervals) to a final depth of 10’ bgs; and,

• BH9-18 and BH13-18: continuous sampling (2-foot intervals) to 20’ bgs, then sample every five feet to bedrock.

No obvious signs of contamination (sheen, odors, volatile vapor readings, or discoloration) were detected in the field during the investigation. Generally, no PID readings above background were recorded during the investigation.

Soil samples that were collected for laboratory analysis were composited over several feet from the interval consisting of the fill unit and its interface with the underlying native soils. Discrete grab samples were collected for the portion used for volatile organic analysis. Typically, the soil selected for volatile organic analysis was the sample fraction located at the depth interval exhibiting the highest


PID readings or most representative of the fill present in the boring if no elevated PID readings were recorded. The soil samples were packed in pre-cleaned laboratory supplied containers, placed in a cooler and delivered by field personnel directly to the analytical laboratory.


3.0 ANALYTICAL METHODOLOGY AND LABORATORY RESULTS Fifteen (15) soil samples were collected from the subsurface soils and sent to a NYS Department of Health (NYSDOH)-approved laboratory for chemical analysis according to the schedule detailed below.

3.1 Soil Samples

The samples were sent via overland courier to Alpha Analytical in Westborough, MA for analysis according to the analytical schedules identified in the contract. The analyses consisted of the following suites of parameters:

• NYSDEC Part 375 Target Compound List (TCL) Volatiles (EPA method

8260C/5035) • NYSDEC Part 375 TCL Semi-Volatiles (EPA method 8270D) • NYSDEC Part 375 Pesticides (EPA method 8081B) • NYSDEC Part 375 Herbicides (EPA method 8151A) • NYSDEC Part 375 PCBs (EPA method 8082A) • NYSDEC Part 375 Total Metals List plus cyanide (EPA method 9010C/9012B),

mercury (EPA method 7470A), and hexavalent chromium (EPA method 7196). • Ignitability (EPA method 1030) • Total Solids (Standard Method 2540) • Corrosivity - pH – Hydrogen Ion Concentration (EPA method 9045) • Toxicity Characteristic Leaching Procedure (TCLP - EPA method 1311) Complete

Analysis for Resource Conservation and Recovery Act (RCRA) volatiles, semi-volatiles, pesticides, herbicides, and metals.

The analytical results were compared to reference standards based on NYSDEC Chapter IV, Subpart 375-6 Remedial Program Soil Cleanup Objectives and NYSDEC CP-51 Soil Cleanup Guidance Policy - Issued 10/21/2010; Effective 12/03/2010 to determine if the samples would be considered contaminated. The Resource Conservation and Recovery Act (RCRA) hazardous waste parameters were used to allow for a comparison to hazardous waste regulatory levels to determine if any of the sampled soils may be considered a hazardous waste.

3.2 Analytical Findings

Laboratory detected analytes are presented in Table 3-1 for each of the collected samples based on the total concentration of each compound. These results are compared to appropriate New York State Department of Environmental Conservation (NYSDEC) guidance values for illustrative purposes. The guidance values are not intended for use as action levels on the property since the NYSDEC generally makes decisions on a

Sample ID BH1-18 BH3-18 BH2-18 BH4-18 BH1/3-18 BH2/4-18 BH6-18 BH5/6-18 BH8-18 BH7/8-18 BH9-18 BH10-18 BH12-18 BH13-18 BH14-18Laboratory Report ID L1808681-01 L1808681-02 L1809330-01 L1809330-02 L1808681-03 L1809330-03 L1809330-04 L1809330-06 L1809330-07 L1809330-08 L1811425-01 L1811425-02 L1811694-03 L1811425-04 L1811694-02Date Collected 3/12/2018 3/14/2018 3/16/2018 3/19/2018 3/14/2018 3/19/2018 3/19/2018 3/19/2018 3/19/2018 3/19/2018 4/2/2018 4/2/2018 4/4/2018 4/2/2018 4/4/2018Analyte

Benzene ND ND ND NA NA NA ND NA 0.016 J NA ND ND ND ND ND mg/kg 0.06 2.9 4.8 44 89n-Butylbenzene ND ND ND NA NA NA 0.001 J NA 0.014 J NA ND ND ND ND ND mg/kg 12 12 12 12 12sec-Butylbenzene ND ND ND NA NA NA 0.0018 NA ND NA ND ND ND ND ND mg/kg 11 11 11 11 11Methylene Chloride ND ND ND NA NA NA ND NA 0.2 J NA ND ND ND ND ND mg/kg 0.05 0.05 0.05 0.05 0.05Toluene ND ND ND NA NA NA ND NA 0.074 J NA .0003 J ND 0.00033 J .0002 J ND mg/kg 0.7 100 100 500 1,000Ethylbenzene ND ND ND NA NA NA 0.00032 J NA 0.024 J NA ND ND ND ND ND mg/kg 1 30 41 390 780p/m-Xylene ND ND ND NA NA NA 0.0014 J NA 0.14 NA ND ND ND ND ND mg/kg NSp NSp NSp NSp NSpo-Xylene ND ND ND NA NA NA 0.0014 J NA 0.046 J NA ND ND ND ND ND mg/kg NSp NSp NSp NSp NSpAcetone 0.012 ND 0.056 NA NA NA 0.026 ** NA ND NA 0.036 0.24 0.047 .0044 J 0.009 J mg/kg 0.05 100 100 500 1,0002-Butanone ND ND 0.011 NA NA NA 0.0032 J NA ND NA ND 0.048 0.0021 J ND ND mg/kg 0.12 100 100 500 1,000n-Propylbenzene ND ND ND NA NA NA 0.00083 J NA 0.02 J NA ND ND ND ND ND mg/kg 3.9 100 100 500 1,0001,3,5-Trimethylbenzene ND ND ND NA NA NA 0.0044 J NA 0.051 J NA ND ND ND ND ND mg/kg 8.4 47 52 190 3801,2,4-Trimethylbenzene ND ND ND NA NA NA 0.011 NA 0.12 J NA ND ND 0.00058 J ND ND mg/kg 3.6 47 52 190 380

Acenaphthene NA NA NA NA ND ND NA ND NA ND .13 J 0.29 0.032 J .058 J ND mg/kg 20 100 100 500 1,000Fluoranthene NA NA NA NA 0.056 J 0.038 J NA 0.29 NA 0.22 1.3 8.4 D 0.41 0.84 0.098 J mg/kg 100 100 100 500 1,000Naphthalene NA NA NA NA ND ND NA ND NA ND .17 J .21 J ND ND ND mg/kg 12 100 100 500 1,000Benzo(a)anthracene NA NA NA NA 0.028 J 0.026 J NA 0.14 NA 0.12 0.76 4.7 0.16 0.35 0.053 J mg/kg 1 1 1 5.6 11Benzo(a)pyrene NA NA NA NA ND ND NA 0.13 J NA 0.14 J 0.74 3.7 0.13 J 0.28 0.06 J mg/kg 1 1 1 1 1.1Benzo(b)fluoranthene NA NA NA NA ND ND NA 0.18 NA 0.18 1 5.2 0.16 0.4 0.074 J mg/kg 1 1 1 5.6 11Benzo(k)fluoranthene NA NA NA NA ND ND NA 0.058 J NA 0.041 J 0.29 1.50 0.056 J 0.12 ND mg/kg 0.8 1 3.9 56 110Chrysene NA NA NA NA 0.026 J ND NA 0.13 NA 0.15 0.81 4.1 0.14 0.34 0.053 J mg/kg 1 1 3.9 56 110Acenaphthylene NA NA NA NA ND ND NA ND NA ND .12 J 1 ND ND ND mg/kg 100 100 100 500 1,000Anthracene NA NA NA NA ND ND NA 0.046 J NA 0.048 J 0.35 1.3 0.1 J 0.15 ND mg/kg 100 100 100 500 1,000Benzo(ghi)perylene NA NA NA NA ND ND NA 0.081 J NA 0.24 0.42 2.2 0.083 J 0.18 0.044 J mg/kg 100 100 100 500 1,000Fluorene NA NA NA NA ND ND NA ND NA 0.024 J .15 J 0.58 0.031 J .064 J ND mg/kg 30 100 100 500 1,000Phenanthrene NA NA NA NA 0.034 J 0.03 J NA 0.16 NA 0.18 0.98 6.1 0.33 0.74 0.045 J mg/kg 100 100 100 500 1,000Dibenzo(a,h)anthracene NA NA NA NA ND ND NA ND NA ND 0.098 J 0.49 0.024 J 0.04 J ND mg/kg 0.33 0.33 0.33 0.56 1.1Indeno(1,2,3-cd)pyrene NA NA NA NA ND 0.068 J NA 0.13 J NA 0.15 J 0.45 2.6 0.085 J 0.2 0.05 J mg/kg 0.5 0.5 0.5 5.6 11Pyrene NA NA NA NA 0.052 J 0.033 J NA 0.24 NA 0.23 1.1 7.9 0.34 0.65 0.077 J mg/kg 100 100 100 500 1,000Dibenzofuran NA NA NA NA ND ND NA ND NA ND .1 J 0.45 ND .043 J ND mg/kg 7 14 59 350 1,000Phenol NA NA NA NA ND ND NA ND NA ND ND 0.057 J ND ND ND mg/kg 0.33 0.33 0.33 0.33 0.33o-&p-Cresol NA NA NA NA ND ND NA ND NA ND .037 J 0.34 ND ND ND mg/kg 0.33 0.33 0.33 0.33 0.33

Calculated Benzo(a)pyrene (BAP) Equivalent

0.00 0.00 0.00 0.00 0.0031 0.0094 0.00 0.1821 0.00 0.1906 1.008 5.19 0.1799 0.394 0.0782

Chromium, Hexavalent NA NA NA NA ND ND NA ND NA ND ND ND ND ND ND mg/kg 30 36 180 1500 6,800Solids, Total 82.6 NA 79.1 NA 79.5 82.9 86.2 80 97.9 84.7 84.4 73 84.1 85.2 77.4 % NSp NSp NSp NSp NSpCyanide, Total NA NA NA NA ND ND NA 6.2 NA ND ND ND ND ND ND mg/kg 27 27 27 27 10,000Flash Point NA NA NA NA >150 NA NA NA NA NA NA NA NA NA NA oF NSp NSp NSp NSp NSpCyanide, Reactive NA NA NA NA ND ND NA ND NA ND ND ND ND ND ND mg/kg NSp NSp NSp NSp NSpSulfide, Reactive NA NA NA NA ND ND NA ND NA ND ND ND ND ND ND mg/kg NSp NSp NSp NSp NSppH NA NA NA NA 9.3 9.1 NA 7.9 NA 7.8 9.6 8.5 9.7 8.2 8.2 SU NSp NSp NSp NSp NSp

Aroclor 1254 NA NA NA NA ND ND NA ND NA ND .00911 J ND ND .0111 J 0.00468 J mg/kg 0.1 1 1 1 25Aroclor 1260 NA NA NA NA ND ND NA ND NA 0.0226 J .00817 J ND ND ND ND mg/kg 0.1 1 1 1 25

Ignitability NA NA NA NA NI NI NA NI NA NI NI NI NI NI NI NA NSp NSp NSp NSp NSp

Endrin NA NA NA NA ND ND NA 0.000578 J NA ND ND ND ND ND ND mg/kg 0.014 0.06 0.06 0.06 0.06Dieldrin NA NA NA NA ND ND NA ND NA ND .00101 J ND ND ND ND mg/kg 0.005 0.039 0.2 1.4 2.8Endosulfan II NA NA NA NA ND ND NA ND NA ND .00111 JPI ND ND ND ND mg/kg 2.4 4.8 24 102 1024,4'-DDT NA NA NA NA ND ND NA ND NA ND ND ND ND 0.00465 ND mg/kg 0.0033 1.7 7.9 47 94

Arsenic, Total NA NA NA NA 1.54 2.63 NA 2.42 NA 1.09 10.9 3.81 1.17 1.33 1.37 mg/kg 13 16 16 16 16Barium, Total NA NA NA NA 34.6 74.6 NA 66.4 NA 31.5 82 59.2 15.7 23.6 17.5 mg/kg 350 350 400 400 10000Beryllium, Total NA NA NA NA 0.223 J 0.213 J NA 0.863 NA 0.251 0.282 .204 J 0.134 J .147 J 0.081 J mg/kg 7.2 14 72 590 2700Cadmium, Total NA NA NA NA 0.292 J 0.172 J NA 0.226 J NA 0.118 J .328 J .21 J 0.25 J .045 J 0.362 J mg/kg 2.5 2.5 4.3 9.3 60Chromium, Total NA NA NA NA 7.18 6.62 NA 8.29 NA 8.32 11.9 6.74 10.3 6.34 6.08 mg/kg NSp NSp NSp NSp NSpCopper, Total NA NA NA NA 9.6 43 NA 11.1 NA 5.58 74.8 60.3 5.94 12.2 10.4 mg/kg 50 270 270 270 10000Lead, Total NA NA NA NA 48.9 286 NA 126 NA 7.72 401 149 14.5 15.2 29.2 mg/kg 63 400 400 1000 3900Manganese, Total NA NA NA NA 182 165 NA 369 NA 74.9 358 194 158 81 86.2 mg/kg 1600 2000 2000 10000 10000Mercury, Total NA NA NA NA 0.09 0.79 NA 0.16 NA 0.1 1.6 2.37 0.091 0.063 0.27 mg/kg 0.18 0.81 0.81 2.8 5.7Nickel, Total NA NA NA NA 6.76 5.36 NA 6.61 NA 5.76 7.84 5.41 5.3 4.04 5.04 mg/kg 30 140 310 310 10000Selenium, Total NA NA NA NA 0.218 J 0.318 J NA 0.439 J NA 0.169 J 1.3 0.667 0.501 J 0.129 0.533 J mg/kg 3.9 36 180 1,500 6,800Silver, Total NA NA NA NA ND ND NA ND NA ND .187 J 0.236 ND ND ND mg/kg 2 8.3 8.3 8 8Zinc, Total NA NA NA NA 46.4 114 NA 56.5 NA 34.3 166.0 91.3 37.8 34.7 76.1 mg/kg 109 2200 10000 10000 10,000

Reference Standard based on NYSDEC Chapter IV, Subpart 375-6 Remedial Program Soil Cleanup Objectives and NYSDEC CP-51 Soil Cleanup GuidanceBold and Colored - exceeds the applicable regulatory standard, see applicable color within Soil Cleanup Ojectives columns.Laboratory Code: P = The RPD between the results for the two columns exceeds the method-specific criteria.

J = Estimated value. The target analyte concentration is below the quantitation limit (RL), but above the Method Detection Limit (MDL). I = The lower value for the two columns has been reported due to obvious interefence.ND = Not Detected NA = Not Analyzed NSp = Not SpecifiedNI = Not Ignitable

Parking Area Borings

Table 3-1: Analytical Detections and Comparison to NYSDEC Regulatory CriteriaNFTA - Amtrak Project

Herbicides (parts per million) - None Detected

PCBs (parts per million)

Volatiles (parts per million)

Semivolatiles (parts per million)

Bold if If BAP >= 3mg/kg

New York State Department of Environmental Conservation - Soil Cleanup Objectives - Protection of Public Health

General Chemistry

New Facility Footprint Area Borings Pick-Up/Drop-Off Area Borings Platform Area Borings

Metals (parts per million)

Pesticides (parts per million)

Units

Ignitability of Solids

Unrestricted ResidentialRestricted Residential

Commercial Industrial


site-by-site basis. However, the guidance values are useful as an indication of what determinations are likely to be made by the NYSDEC or others with regards to an

interpretation of the results.

The NYSDEC Soil Cleanup Objectives include three types of individual soil reuse categories including Protection of Groundwater, Protection of Ecological Resources, and Protection of Public Health. The Unrestricted Soil Cleanup Objective is based on the selection of the most stringent and restrictive value of these three different (groundwater, ecological resources and public health) categories of soil reuse. The NYSDEC has also further broken down the Protection of Public Health Criteria into four levels of protection: Residential, Restricted-Residential, Commercial and Industrial based upon the proposed reuse of the site. Table 3-1 identifies the compounds detected by the lab and whether they exceed the New York State Department of Environmental Conservation (NYSDEC) Unrestricted, Residential, Restricted-Residential, Commercial or Industrial Use Soil Cleanup Objectives as described in 6 NYCRR Part 375 Environmental Remediation Programs and CP-51 Soil Cleanup Guidance. These values were developed for the protection of human health given the proposed re-use of the site and are often referenced as concentrations that may warrant a cleanup action or specific means of material handling and off-site disposal. Volatile/Semi-Volatile Organic Results

• Two volatile organic compounds (VOC) were identified by the field investigation. Of these, acetone was detected at a concentration above the most stringent Unrestricted Use SCO in samples from soil borings 2 and 10, and methylene chloride was detected at a concentration above the Industrial Use SCO in the sample from soil boring 8. Both acetone and methylene chloride are common laboratory contaminants.

• Several semi-volatile organic compounds (SVOCs) were identified in the soil

samples at various concentrations in numerous samples but below the unrestricted use SCO. However, eight SVOCs were detected at concentrations above the residential SCO in the soils from boring 10 including three that exceeded industrial use soil cleanup objectives. To assess the potential reuse of the fill materials encountered at all of the sites, the Benzo(a)pyrene Toxic Equivalence Quotient (TEQ) was calculated as described in the NYSDEC Part 360 solid waste regulations. This calculation seeks to provide a toxicity weighted sum of analyte concentrations for a specific list of PAHs in order to provide a single, objective concentration as a Health Investigation Level (HIL). The application of benzo(a)pyrene (BaP)-toxic equivalent factor to PAH


concentrations can provide a more accurate risk assessment from environmental exposure to PAHs and is now used as the basis for fill material beneficial use determinations. Materials that exceed a 3 mg/kg BAP equivalent are restricted from reuse as fill under any of the three categories (e.g., general fill, restricted-use fill or limited use fill). Fill to be excavated from SB-10 should be considered unsuitable for reuse anywhere and will have to be disposed in a solid waste landfill.

Soils that exceed the lower level of protection of public health-residential land use and contain non soil constituents cannot be reused as general fill but as restricted use or limited use fill. Soils from SB-8 and SB-9 exceeded the residential land use soil cleanup objective limits and can only be reused on-site or off-site with these restrictions (for use in embankments or subgrade in transportation corridors or as engineered use under foundations and pavements). The soils from the remaining locations would all be allowed to remain in place, be reused on-site, or could be re-used elsewhere under the definition of restricted use fill or limited use fill only, since non-putrescible non-soil constituents are present in the fill materials. However, they cannot be used as general fill at another site. As such, it is likely that all the fill materials excavated during construction will not be able to be reused, and the construction cost estimate should presume their disposal in a permitted solid waste or as uncontaminated construction and demolition debris in an appropriate landfill.

Inorganic/Metal Results

• The laboratory results indicate that various metals were detected at levels above the Unrestricted Use SCOs in samples from soil borings 2, 4, 5, 6, 9, 10 and 14. Of these, lead and mercury were detected at concentrations above the restricted-residential use cleanup objective in soil boring 9 and mercury was detected at concentrations above the restricted-residential use cleanup objective in the sample from soil boring 10.

Pesticide/Herbicide/PCB Results

• No herbicide compounds were identified by the field investigation.

• There were no elevated concentrations of pesticide compounds identified by the field investigation.

• None of the samples had soils with elevated levels of PCBs.


TCLP and RCRA Characteristic Results

• The samples were also analyzed and the results evaluated to determine if any of the soil samples would fail TCLP testing for toxicity or exhibit the RCRA characteristic of ignitability or corrosivity that would result in their classification as a hazardous waste. The results of the analyses show that none of the samples exceeded the RCRA hazardous waste limits or characteristic limits defined by regulation. As a result, a separate table showing the results of the TCLP analysis was not prepared since no exceedances were recorded for any constituent.

• Any soil or fill materials requiring disposal in a landfill will require that the Contractor perform additional TCLP analysis is support of the development of the waste profile. Due to the heterogeneous nature of fill in the area, it is possible that excavated materials could fail this analysis and be classified as a RCRA hazardous waste. The complete laboratory analytical report can be found in Attachment C.

ATTACHMENT A Soil Boring Logs

Drill Rig: Diedrich D50 Date Drilled: 3/12/18 AJN

Probe Dia: SPT Boring Number: BH1-18 B. Bartron

x Asphalt 12"

1 x

2 Black to dark brown SILT and fine SAND; then 3" brown f SAND. FILL

2 5

3

3 6

6

4 5

2

5 1

2

6 2

2

7 10

7

8 7

3

9 4

6

10 7

Completion Notes:

Site: NYSDOT - Amtrak Exchange St. Station

Exchange Street, Buffalo, NY

Project No: 1700502 Page 1 of 1

3. Bedrock encountered at 44' bgs. Final depth of bedrock core 54.7'

bgs

2. Fill transitions to native soils at 2.5' bgs.

4" as above; then

Gray-brown clayey SILT; some fine sand; very moist-wet.

95 PERRY STREET - BUFFALO, NY 14203

PHONE (716) 206-5100 FAX (716) 206-5199

WATTS ARCHITECTURE & ENGINEERING

Logged By:

Sa

mp

le

Description

0.0 12"1

PID

(ppm)

Blow

Counts

Depth

(feet)Recovery

4" Brown m-f SAND. FILL

4 12" Brown clayey SILT; some fine sand; very moist-wet.

0.0

0.0

2

3

Driller:

5 0.0 16"

12"0.0

12"Brown SILT and f SAND; some bedding. Native soils.

USCS

Symbol

4. Total VOC sample collected from 2-4' bgs.

End of Boring

1. Continuous sampling to 10' bgs for environmental samples, then

continuous sampling to bedrock.

Brown silty CLAY.

BORING LOG



x

1 x

2

2 3

2

3 1

3

4 10

6

5 3

1

6 1

2

7 3

7

8 7

7

9 4

6

10 10

Completion Notes:





PHONE (716) 206-5100 FAX (716) 206-5199


Dark brown silty CLAY; consistent bedding throughout.

Logged By:

Sa

mp

le

Description

0.0 3"1

PID

(ppm)

Blow

Counts

Depth

(feet)

16"

18"0.0

14"

4 18"

0.0

0.0

Concrete 12"

BORING LOG

2

3

Driller:

5 0.0

Dark brown SILT and fine SAND; trace coarse gravel and brick

fragments. FILL

Dark brown-black to gray-brown SILT and fine SAND. Native soils

As above.

As above.

USCS

SymbolRecovery

Brown-gray fine SAND with silty clay interbedding.

As above.

Brown-gray fine SAND.

1. Continuous sampling to 20' bgs, then final sample from 23'-25' bgs.

2. Fill transitions to native soils at 3' bgs.

3. Groundwater monitoring well installed to 25' bgs with screened

interval from 24'-14' bgs.


End of Boring



x Asphalt 12"

1 x

2 Dark brown SILT and fine SAND. FILL

2 2

4

3 17

9

4 1

5

6

3

7 3

3

8 6

6

9 7

8

10 8

Completion Notes:




Brown SILT and f SAND with bedding. NATIVE

As above


14"

PHONE (716) 206-5100 FAX (716) 206-5199

Logged By:

Sa

mp

le

Description

0.0 4"1

Dark gray to black c SAND and GRAVEL; some slag pieces. FILL

As above

4


4. TCLP VOC sample collected from 2-4' bgs.

3. Large boulder encountered at 24.7'bgs. Cored through boulder to

27.7' bgs and continued drilling. Bedrock encountered at 41' bgs. Final

depth of bedrock core 52.5' bgs

PID

(ppm)

Blow

Counts

Depth

(feet)Recovery

USCS

Symbol


100/2"

Driller:

5 0.0 16"

2"0.0

8"0.0

0.0

Gray-brown SILT and f SAND; FILL

End of Boring

1. Continuous sampling to 10' bgs for environmental samples; then

continous sampling to 30' bgs; then every five feet to bedrock.

Brown-gray silty CLAY; little gravel. FILL

BORING LOG

2

3



x Concrete 6"

1 2

5

2 9

11

3 21

33

4 15

5

5 7

7

6 4

6

7 4

4

8 6

6

9 6

7

10 7

Completion Notes:




1. Continuous sampling to 20' bgs, then final sample from 23'-25' bgs.

2. Fill transitions to native soils between 6-8' bgs.

3. Sample S-4 was re-advanced with a 3" spoon after yielding no

recovery.

4. Total VOC sample collected from 4'-7' bgs.

End of Boring

0.0

USCS

SymbolRecovery

Gray-brown sandy SILT; large wood pieces. FILL

Brown-gray silty fine SAND. Native soils

Gray-brown silty CLAY; large wood pieces.

0.0

0.0

BORING LOG

2

3

Driller:

5

1

PID

(ppm)

Blow

Counts

Depth

(feet)

14"

16"0.0

12"

4 NR*


PHONE (716) 206-5100 FAX (716) 206-5199


Dark brown SILT and fine SAND. FILL

Wood pieces.

Logged By:

Sa

mp

le

Description

0.0 6"



x Concrete 6"

1 16

20

2 13

5

3 3

2

4 4

2

5 1

1

6 1

3

7 4

5

8 4

9 As above.

9 10

3

10 4

Completion Notes:




1. Continuous sampling to 10' bgs.

2. Fill transitions to native soils at approximately 8.5' bgs.

End of Boring

Brick pieces. FILL

BORING LOG

2

3

Driller:

5 0.0

USCS

SymbolRecovery

Brick fragments with sandy cement mortar. FILL

10"

4 4"

0.0

0.0

Logged By:

Sa

mp

le

Description

0.0 12"1

PID

(ppm)

Blow

Counts

Depth

(feet)

3. No Total or TCLP VOC sample collected.

Brown silty CLAY.


PHONE (716) 206-5100 FAX (716) 206-5199


Gray, silty SAND and GRAVEL with slag and brick fragments. FILL

Gray-brown SILT and fine SAND; large brick pieces. FILL

6"

4"0.0



x Concrete 6"

1 6

10

2 14

10

3 11

10

4 12

5

5 4

5

6 8

5

7 6

7

8 6

3

9 2

1

10 2

Completion Notes:






End of Boring

5 0.0

USCS

SymbolRecovery

Dark brown-gray SILT and f SAND.

4 16"

0.0

0.0

BORING LOG

2

3

Driller:

PID

(ppm)

Blow

Counts

Depth

(feet)

16"

20"0.0

16"


PHONE (716) 206-5100 FAX (716) 206-5199


Gray, silty SAND and GRAVEL with slag and brick fragments. FILL

Logged By:

Sa

mp

le

Description

0.0 4"1

3. Total VOC sample collected from 2'-4' bgs.

4. TCLP VOC sample collected from 4'-6' bgs.

Black cinders. FILL

Gray silty fine SAND; large brick pieces. FILL

3" Dark brown silty CLAY with gray clay lens.

Brown silty fine SAND. Native soils.

Brown-gray silty fine SAND; very moist to wet.



1 Concrete 4"

1 10

33

2 51

20

3

4

7

5 4

7

6 6

5

7 2

2

8 9

6

9 6

3

10 7

Completion Notes:




5 0.0

USCS

SymbolRecovery


End of Boring

0.0

0.0

BORING LOG

2

3

Driller:

1

PID

(ppm)

Blow

Counts

Depth

(feet)

12"

10"0.0

4"

4 12"


PHONE (716) 206-5100 FAX (716) 206-5199


Gray SAND and GRAVEL with slag and brick fragments. Broken rock

fragment at bottom of spoon. FILL

100/5"

Logged By:

Sa

mp

le

Description

0.0 14"

3. No Total or TCLP VOC sample collected.

Brown silty fine SAND with brown silt interbedding.

As above. Broken rock fragment at bottom of spoon.

4" Brown silty f SAND.

Gray-brown silty CLAY; soft.

Gray-brown silty f SAND with organic bedding.




21 Concrete 4"

1 93

17

2 17

18

3 10

5

4 13

5

5 4

8

6 10

3

7 4

7

8 12

4

9 4

9

10 8

Completion Notes:




Sa

mp

le

Description

1.9 16"1

3. Total and TCLP VOC samples collected from 1'-3' bgs.

Gray-brown silty fine SAND.

As above. Very gravelly.

Dark gray-black silty CLAY and coarse gravel; slight organic odor. FILL

Dark gray fine SAND.

18"

10"0.0

10"


PHONE (716) 206-5100 FAX (716) 206-5199


Dark gray to brown-gray silty f SAND.


0.0

BORING LOG

2

3

Driller:

PID

(ppm)

Blow

Counts

Depth

(feet)

Gray-brown SAND and SILT. Broken rock fragments. FILL

Logged By:

5 0.0

USCS

SymbolRecovery


End of Boring

4 16"

0.0



11

1 8

23

2 14

5

3 4

4

4 10

2

5 2

3

6 2

3

7 2

2

8 3

1

9 2

2

10 4

Completion Notes:




5. Composite samples collected from 0'-8' bgs.

10"1


Brown-gray to brown silty CLAY; some bedding near bottom of interval.

Native soils.

Dark brown to dark gray silty CLAY, some gravel, glass and brick

fragments, moist. FILL

24"

18"



Dark brown, silty fine SAND and GRAVEL, moist. TOPSOIL/FILL

Dark brown to dark gray silty CLAY with slag, cinders and glass; very

moist. FILL


PHONE (716) 206-5100 FAX (716) 206-5199


As above.0.0

5 0.0

3. Bedrock encountered at 42.3' bgs.

4. Total and TCLP VOC samples collected from 2-4' bgs.

Blow

Counts

Depth

(feet)

Logged By:

USCS

Symbol

0.0

14"

Sa

mp

le

Description

0.0

Recovery

End of Boring

4 6"

0.0

BORING LOG

2

3

Driller:

PID

(ppm)



x 6" Concrete

1 1

2

2 2

5

3 4

4

4 3

2

5 2

2

6 2

4 As above

7 7

8

8 7

5

9 3

7

10 10

Completion Notes:




Recovery

End of Boring

4 16"

0.0

BORING LOG

2

3

Driller:

PID

(ppm)

Blow

Counts

Depth

(feet)

Logged By:

USCS

Symbol

6"0.0

8"


PHONE (716) 206-5100 FAX (716) 206-5199


Black to red-brown organic clay/peat. Large piece of slag. Organic odor.

FILL

0.0

5 0.0

Sa

mp

le

Description

0.0 6"1


As above.

Dark brown to dark gray, clayey SILT with gravel. FILL

Dark gray to dark brown silty CLAY. FILL

12"



continous sampling to 20' bgs; then final sample from 23'-25' bgs.


Dark brown silty CLAY withorganic material. Wet near bottom of

interval. Slight organic odor. FILL

Gray fine sandy SILT.



x 6" Concrete

1 2

7

2 7

6

3 9

19

4 5

19

5 20

23

6 18

5

7 4

7

8 10

6

9 10

9

10 11

Completion Notes:




Recovery

End of Boring

4 12"

0.0Dark brown to black silty CLAY with large gravel and rock fragments.

FILL

As above, to light brown silty fine SAND.

BORING LOG

2

3

Driller:

PID

(ppm)

Blow

Counts

Depth

(feet)

Logged By:

USCS

Symbol

12"0.0

6"


PHONE (716) 206-5100 FAX (716) 206-5199


0.0

5 0.0

Sa

mp

le

Description

0.0 5"1


Light brown to tan silty fine SAND.

Dark brown silt, sand and gravel with brick pieces. FILL. Tan medium

sand at bottom.

14"

3. Insufficient recovery for sample collection.



Brown-gray silty fine SAND with bedding. Native soils.



x 6" Concrete

1 2

2

2 4

5

3 6

7

4 10

6

5 7

7

6 4

4

7 6

7

8 9

7

9 12

12

10 12

Completion Notes:




As above. Occasional soft, brown-gray silty CLAY lenses.

Sa

mp

le

Description

0.0 10"1


Brown-gray silty fine SAND; finely bedded.

Dark brown silty CLAY to yellow-brown fine SAND; trace gravel and

slag. FILL

16"



20"


PHONE (716) 206-5100 FAX (716) 206-5199


0.0

5 0.0

3. Total and TCLP VOC samples collected from 0'-2' bgs.


BORING LOG

2

3

Driller:

PID

(ppm)

Blow

Counts

Depth

(feet)

Logged By:

USCS

SymbolRecovery

End of Boring

4 18"

0.0 Tan fine SAND; moist. Native soils.

As above.

Brown-gray silty fine SAND; moist.

20"0.0



5

1 8

10

2 8

5

3 6

8

4 11

5

5 6

5

6 6

5

7 6

13

8 18

5

9 7

7

10 7

Completion Notes:





Tan-brown silty fine SAND with bedding. Native soils.

Tan-brown silty fine SAND; very moist.




End of Boring

As above. Wet to saturated.

Gray SILT, SAND and GRAVEL with brick fragments. FILL

12"

24"0.0

3. Bedrock encountered at 42.6' bgs.

3

Driller:

PID

(ppm)

Blow

Counts

Sa

mp

le

Description

0.0 10"1

Recovery

4 14"

10"

Dark brown silty CLAY. FILL

Tan, clayey medium to fine SAND.

0.0

BORING LOG

2 0.0



PHONE (716) 206-5100 FAX (716) 206-5199

Depth

(feet)

Logged By:

4" Dark brown silty CLAY. TOPSOIL

5 0.0

USCS

Symbol



5

1 4

3

2 9 1" Tan SILT. FILL

2

3 1

1

4 1

2

5 2

2

6 2

WH

7 WH

1

8 4

4

9 3

3

10 3

Completion Notes:




Recovery

End of Boring

4 20"

0.0

BORING LOG

2

3

Driller:

PID

(ppm)

Blow

Counts

Depth

(feet)

Logged By:

USCS

Symbol

Sa

mp

le

Description

0.0 10"1

As above. Moist.18"

22"0.0

12"

PHONE (716) 206-5100 FAX (716) 206-5199

Tan-brown silty very fine SAND with some bedding. Native soils. Gray

silty fine SAND layer @5.5' bgs.

Tan-brown silty fine SAND; saturated. Water in spoon.




0.0

5 0.0


4" Dark brown silty CLAY, some gravel. TOPSOIL

Dark brown to brown silty CLAY to SILT, some gravel. FILL



ATTACHMENT B Photographs

of 8 O:\2017\17005 NYSDOT RDSA\1700502 Buffalo Train Station Design\10. Env\10.e. HWCM DSI\Amtrak Photo Log.docx

Photo 1: Drill rig set up at facility footprint area boring

location BH1-18.

Photo 3: Typical rock core obtained from boring location BH1-18.

Photo 2: Typical fill material obtained from boring location BH1-18.

Photo 4: Drilling at facility footprint area boring location BH2-18.




Photo 6: Monitoring well installed at boring location BH2-18.



Photo 9: Typical rock core obtained from boring location BH3-18.



Photo 12: Chunk of wood recovered from boring location BH4-18.


Photo 13: Drilling in the proposed pickup/dropoff area.

Photo 15: Drilling in the proposed parking area.

Photo 14: Typical fill material obtained from the pickup/dropoff area.

Photo 16: Typical fill material obtained from the parking area.


Photo 17: Drilling at platform area boring location BH9-18.



Photo 20: Typical fill material obtained from boring location BH10-

18.



Photo 23: Shallow native material obtained from boring

location BH11-18.

Photo 22: Typical fill material obtained from boring

location BH11-18.




location BH12-18.


location BH13-18.





location BH14-18.

Photo 31: EDI personnel installing groundwater monitoring well in

boring BH14-18.

Photo 30: EDI personnel checking the water level inside the augers

prior to installing the groundwater monitoring well.

Photo 32: EDI personnel completing the installation of the outer

protective casing for the monitoring well.

ATTACHMENT C Laboratory Reports

L1808681

Watts Architecture & Engineering P.C

17005.02

NFTA

Client:

Project Name:

Project Number:

03/30/18

Eight Walkup Drive, Westborough, MA 01581-1019

Lab Number:

Report Date:

508-898-9220 (Fax) 508-898-9193 800-624-9220 - www.alphalab.com

95 Perry Street

Suite 300

Andrew KlimekATTN:

ANALYTICAL REPORT

Certifications & Approvals: MA (M-MA086), NH NELAP (2064), NJ NELAP (MA935), CT (PH-0574), IL (200077), ME (MA00086), MD (348), NY (11148), NC (25700/666), PA (68-03671), RI (LAO00065), TX (T104704476), VT (VT-0935), VA (460195), USDA (Permit #P330-14-00197).

Buffalo, NY 14203

(716) 206-5100Phone:

The original project report/data package is held by Alpha Analytical. This report/data package is paginated and should be reproduced only in itsentirety. Alpha Analytical holds no responsibility for results and/or data that are not consistent with the original.

Serial_No:03301815:28

Page 1 of 65

L1808681-01

L1808681-02

L1808681-03

L1808681-04

Alpha Sample ID

BH1-18

BH3-18

BH1/3-18

TRIP BLANK

Client ID

AMTRAK

AMTRAK

AMTRAK

AMTRAK

Sample Location

NFTA

17005.02

Project Name:Project Number:

Lab Number: Report Date:

L180868103/30/18

03/12/18 13:30

03/14/18 10:50

03/14/18 12:30

03/14/18 00:00

Collection Date/TimeMatrix Receive Date

SOIL

SOIL

SOIL

WATER

03/14/18

03/14/18

03/14/18

03/14/18

Serial_No:03301815:28

Page 2 of 65

NFTA

17005.02

Project Name:

Project Number:

Lab Number:

Report Date:L1808681

03/30/18

Case Narrative

The samples were received in accordance with the Chain of Custody and no significant deviations were encountered during the preparation

or analysis unless otherwise noted. Sample Receipt, Container Information, and the Chain of Custody are located at the back of the report.

Results contained within this report relate only to the samples submitted under this Alpha Lab Number and meet NELAP requirements for all

NELAP accredited parameters unless otherwise noted in the following narrative. The data presented in this report is organized by parameter

(i.e. VOC, SVOC, etc.). Sample specific Quality Control data (i.e. Surrogate Spike Recovery) is reported at the end of the target analyte list

for each individual sample, followed by the Laboratory Batch Quality Control at the end of each parameter. Tentatively Identified Compounds

(TICs), if requested, are reported for compounds identified to be present and are not part of the method/program Target Compound List,

even if only a subset of the TCL are being reported. If a sample was re-analyzed or re-extracted due to a required quality control corrective

action and if both sets of data are reported, the Laboratory ID of the re-analysis or re-extraction is designated with an "R" or "RE",

respectively. When multiple Batch Quality Control elements are reported (e.g. more than one LCS), the associated samples for each element

are noted in the grey shaded header line of each data table. Any Laboratory Batch, Sample Specific % recovery or RPD value that is outside

the listed Acceptance Criteria is bolded in the report. All specific QC information is also incorporated in the Data Usability format of our Data

Merger tool where it can be reviewed along with any associated usability implications. Soil/sediments, solids and tissues are reported on a

dry weight basis unless otherwise noted. Definitions of all data qualifiers and acronyms used in this report are provided in the Glossary

located at the back of the report.

In reference to questions H (CAM) or 4 (RCP) when "NO" is checked, the performance criteria for CAM and RCP methods allow for some

quality control failures to occur and still be within method compliance. In these instances the specific failure is not narrated but noted in the

associated QC table. The information is also incorporated in the Data Usability format of our Data Merger tool where it can be reviewed

along with any associated usability implications.

Please see the associated ADEx data file for a comparison of laboratory reporting limits that were achieved with the regulatory Numerical

Standards requested on the Chain of Custody.

HOLD POLICY

For samples submitted on hold, Alpha's policy is to hold samples (with the exception of Air canisters) free of charge for 21 calendar days

from the date the project is completed. After 21 calendar days, we will dispose of all samples submitted including those put on hold unless

you have contacted your Client Service Representative and made arrangements for Alpha to continue to hold the samples. Air canisters will

be disposed after 3 business days from the date the project is completed.

Please contact Client Services at 800-624-9220 with any questions.

Serial_No:03301815:28

Page 3 of 65

Case Narrative (continued)

NFTA

17005.02

Project Name:

Project Number:

Lab Number:


03/30/18

Report Submission

All non-detect (ND) or estimated concentrations (J-qualified) have been quantitated to the limit noted in the

MDL column.

Sample Receipt

L1808681-04: A sample identified as "TRIP BLANK" was received but not listed on the Chain of Custody and

was not analyzed.

Volatile Organics

Any reported concentrations that are below 200 ug/kg may be biased low due to the sample not being collected

according to 5035-L/5035A-L low-level specifications.

TCLP Volatiles

The ambient temperature of the area in which the TCLP/SPLP extraction of the samples and associated

Method Blank performed was outside the required 21-25 degrees C temperature range.

TCLP Semivolatiles

The WG1100953-3 LCSD recovery, associated with L1808681-03, is below the acceptance criteria for

pyridine (5%); however, it has been identified as a "difficult" analyte. The results of the associated sample are

reported.

Cyanide, Total

The WG1099068-2/-3 LCS/LCSD recoveries (63%/55%), associated with L1808681-03, are outside our in-

house acceptance criteria, but within the vendor-certified acceptance limits. The results of the original analyses

are reported.

I, the undersigned, attest under the pains and penalties of perjury that, to the best of my knowledge and belief and based upon my personal inquiry of those responsible for providing the information contained in this analytical report, such information is accurate and complete. This certificate of analysis is not complete unless this page accompanies any and all pages of this report.

Authorized Signature:

Title: Technical Director/Representative Date: 03/30/18

Serial_No:03301815:28

Page 4 of 65

ORGANICS

Serial_No:03301815:28

Page 5 of 65

VOLATILES

Serial_No:03301815:28

Page 6 of 65

FF

Methylene chloride

1,1-Dichloroethane

Chloroform

Carbon tetrachloride

Tetrachloroethene

Chlorobenzene

1,2-Dichloroethane

1,1,1-Trichloroethane

Benzene

Toluene

Ethylbenzene

Vinyl chloride

1,1-Dichloroethene

trans-1,2-Dichloroethene

Trichloroethene

1,2-Dichlorobenzene

1,3-Dichlorobenzene

1,4-Dichlorobenzene

Methyl tert butyl ether

p/m-Xylene

o-Xylene

cis-1,2-Dichloroethene

Acetone

2-Butanone

n-Butylbenzene

sec-Butylbenzene

tert-Butylbenzene

n-Propylbenzene

Parameter Result Dilution Factor

ND

ND

ND

ND

ND

ND

ND

ND

ND

ND

ND

ND

ND

ND

ND

ND

ND

ND

ND

ND

ND

ND

12

ND

ND

ND

ND

ND

ug/kg

ug/kg

ug/kg

ug/kg

ug/kg

ug/kg

ug/kg

ug/kg

ug/kg

ug/kg

ug/kg

ug/kg

ug/kg

ug/kg

ug/kg

ug/kg

ug/kg

ug/kg

ug/kg

ug/kg

ug/kg

ug/kg

ug/kg

ug/kg

ug/kg

ug/kg

ug/kg

ug/kg

1

1

1

1

1

1

1

1

1

1

1

1

1

1

1

1

1

1

1

1

1

1

1

1

1

1

1

1

Qualifier Units RL

Volatile Organics by GC/MS - Westborough Lab

SAMPLE RESULTS

Project Name:

Project Number:

Lab Number:

Report Date:

NFTA

17005.02

L1808681

9.9

1.5

1.5

0.99

0.99

0.99

0.99

0.99

0.99

1.5

0.99

2.0

0.99

1.5

0.99

5.0

5.0

5.0

2.0

2.0

2.0

0.99

9.9

9.9

0.99

0.99

5.0

0.99

03/30/18

BH1-18Client ID:03/12/18 13:30Date Collected:03/14/18Date Received:

AMTRAKSample Location:

L1808681-01Lab ID:

Field Prep: Not Specified

Matrix: SoilAnalytical Method:Analytical Date:Analyst:

1,8260C03/23/18 08:29MV 83%Percent Solids:

MDL

1.6

0.27

0.37

0.34

0.30

0.34

0.24

0.35

0.19

0.19

0.17

0.31

0.37

0.24

0.30

0.18

0.22

0.18

0.15

0.35

0.34

0.34

2.3

0.68

0.23

0.22

0.24

0.21

Sample Depth:

Serial_No:03301815:28

Page 7 of 65

1,3,5-Trimethylbenzene


1,4-Dioxane


ND

ND

ND

ug/kg

ug/kg

ug/kg

1

1

1

Qualifier Units RL


SAMPLE RESULTS

Project Name:

Project Number:

Lab Number:

Report Date:

NFTA

17005.02

L1808681

5.0

5.0

40

1,2-Dichloroethane-d4

Toluene-d8

4-Bromofluorobenzene

Dibromofluoromethane

102

98

107

88

70-130

70-130

70-130

70-130

Acceptance CriteriaSurrogate % Recovery Qualifier

03/30/18



L1808681-01Lab ID:


MDL

0.16

0.18

14.

Sample Depth:

Serial_No:03301815:28

Page 8 of 65

Chloroform


Tetrachloroethene

Chlorobenzene

1,2-Dichloroethane

Benzene

Vinyl chloride

1,1-Dichloroethene

Trichloroethene

1,4-Dichlorobenzene

2-Butanone


ND

ND

ND

ND

ND

ND

ND

ND

ND

ND

ND

ug/l

ug/l

ug/l

ug/l

ug/l

ug/l

ug/l

ug/l

ug/l

ug/l

ug/l

10

10

10

10

10

10

10

10

10

10

10

Qualifier Units RL

TCLP Volatiles by EPA 1311 - Westborough Lab

SAMPLE RESULTS

Project Name:

Project Number:

Lab Number:

Report Date:

NFTA

17005.02

L1808681

7.5

5.0

5.0

5.0

5.0

5.0

10

5.0

5.0

25

50


Toluene-d8


dibromofluoromethane

103

100

104

98

70-130

70-130

70-130

70-130


03/30/18



L1808681-02Lab ID:



1,8260C03/26/18 09:33MM

TCLP/SPLP Ext. Date: 03/23/18 10:48

MDL

2.2

1.3

1.8

1.8

1.3

1.6

0.71

1.7

1.8

1.9

19.

Sample Depth:

Serial_No:03301815:28

Page 9 of 65

Method Blank AnalysisBatch Quality Control

Project Name:

Project Number:

Lab Number:

Report Date:

NFTA

17005.02

L1808681

03/23/18 08:011,8260CAnalytical Method:

Analytical Date:

03/30/18

Analyst: MV

Methylene chloride

1,1-Dichloroethane

Chloroform


Tetrachloroethene

Chlorobenzene

1,2-Dichloroethane


Benzene

Toluene

Ethylbenzene

Vinyl chloride

1,1-Dichloroethene


Trichloroethene

1,2-Dichlorobenzene

1,3-Dichlorobenzene

1,4-Dichlorobenzene


p/m-Xylene

o-Xylene


Acetone

2-Butanone

n-Butylbenzene

sec-Butylbenzene

tert-Butylbenzene

n-Propylbenzene


Parameter Result

4.1

ND

ND

ND

ND

ND

ND

ND

ND

ND

ND

ND

ND

ND

ND

ND

ND

ND

ND

ND

ND

ND

4.0

ND

ND

ND

ND

ND

ND

RL

10

1.5

1.5

1.0

1.0

1.0

1.0

1.0

1.0

1.5

1.0

2.0

1.0

1.5

1.0

5.0

5.0

5.0

2.0

2.0

2.0

1.0

10

10

1.0

1.0

5.0

1.0

5.0

J

J

ug/kg

ug/kg

ug/kg

ug/kg

ug/kg

ug/kg

ug/kg

ug/kg

ug/kg

ug/kg

ug/kg

ug/kg

ug/kg

ug/kg

ug/kg

ug/kg

ug/kg

ug/kg

ug/kg

ug/kg

ug/kg

ug/kg

ug/kg

ug/kg

ug/kg

ug/kg

ug/kg

ug/kg

ug/kg

UnitsQualifier

Volatile Organics by GC/MS - Westborough Lab for sample(s): 01 Batch: WG1099906-5

MDL

1.6

0.27

0.37

0.34

0.30

0.35

0.25

0.35

0.19

0.20

0.17

0.32

0.37

0.24

0.30

0.18

0.22

0.18

0.15

0.35

0.34

0.34

2.3

0.69

0.23

0.22

0.25

0.22

0.16

Serial_No:03301815:28

Page 10 of 65


Project Name:

Project Number:

Lab Number:

Report Date:

NFTA

17005.02

L1808681


Analytical Date:

03/30/18

Analyst: MV


1,4-Dioxane

Parameter Result

ND

ND

RL

5.0

40

ug/kg

ug/kg

UnitsQualifier



Toluene-d8



104

97

105

99

70-130

70-130

70-130

70-130

Surrogate %Recovery QualifierAcceptance

Criteria

MDL

0.19

14.

Serial_No:03301815:28

Page 11 of 65


Project Name:

Project Number:

Lab Number:

Report Date:

NFTA

17005.02

L1808681


Analytical Date: Extraction Date: 03/23/18 10:48

03/30/18

Analyst: MM

Chloroform


Tetrachloroethene

Chlorobenzene

1,2-Dichloroethane

Benzene

Vinyl chloride

1,1-Dichloroethene

Trichloroethene

1,4-Dichlorobenzene

2-Butanone

Parameter Result

ND

ND

ND

ND

ND

ND

ND

ND

ND

ND

ND

RL

7.5

5.0

5.0

5.0

5.0

5.0

10

5.0

5.0

25

50

ug/l

ug/l

ug/l

ug/l

ug/l

ug/l

ug/l

ug/l

ug/l

ug/l

ug/l

UnitsQualifier

TCLP Volatiles by EPA 1311 - Westborough Lab for sample(s): 02 Batch: WG1100473-5


Toluene-d8



100

99

105

93

70-130

70-130

70-130

70-130


Criteria

03/23/18 10:48TCLP/SPLP Extraction Date:

MDL

2.2

1.3

1.8

1.8

1.3

1.6

0.71

1.7

1.8

1.9

19.

Serial_No:03301815:28

Page 12 of 65

Methylene chloride

1,1-Dichloroethane

Chloroform


Tetrachloroethene

Chlorobenzene

1,2-Dichloroethane


Benzene

Toluene

Ethylbenzene

Vinyl chloride

1,1-Dichloroethene


Trichloroethene

1,2-Dichlorobenzene

1,3-Dichlorobenzene

1,4-Dichlorobenzene


p/m-Xylene

o-Xylene


Acetone

116

108

101

98

91

93

109

100

101

95

96

108

97

100

100

91

90

89

107

89

89

101

142

116

108

102

102

91

93

111

101

101

95

96

108

98

99

100

92

90

90

108

89

89

100

147

70-130

70-130

70-130

70-130

70-130

70-130

70-130

70-130

70-130

70-130

70-130

67-130

65-135

70-130

70-130

70-130

70-130

70-130

66-130

70-130

70-130

70-130

54-140

0

0

1

4

0

0

2

1

0

0

0

0

1

1

0

1

0

1

1

0

0

1

3

30

30

30

30

30

30

30

30

30

30

30

30

30

30

30

30

30

30

30

30

30

30

30

ParameterLCS

%RecoveryLCSD

%Recovery%Recovery

Limits RPDRPD

Limits

Volatile Organics by GC/MS - Westborough Lab Associated sample(s): 01 Batch: WG1099906-3 WG1099906-4

Lab Control Sample AnalysisBatch Quality Control

Project Name:

Project Number:

Lab Number:

Report Date:

NFTA

17005.02

L1808681

03/30/18

Qual Qual

Q Q

Qual

Serial_No:03301815:28

Page 13 of 65

2-Butanone

n-Butylbenzene

sec-Butylbenzene

tert-Butylbenzene

n-Propylbenzene



1,4-Dioxane

125

95

94

93

96

92

95

111

121

94

94

93

96

93

95

112

70-130

70-130

70-130

70-130

70-130

70-130

70-130

65-136

3

1

0

0

0

1

0

1

30

30

30

30

30

30

30

30

ParameterLCS

%RecoveryLCSD

%Recovery%Recovery

Limits RPDRPD

Limits



Project Name:

Project Number:

Lab Number:

Report Date:

NFTA

17005.02

L1808681

1,2-Dichloroethane-d4Toluene-d84-BromofluorobenzeneDibromofluoromethane

1059910497

70-13070-13070-13070-130

1049810497

Surrogate Qual%Recovery Qual%RecoveryLCS LCSD

03/30/18

AcceptanceCriteria

Qual Qual Qual

Serial_No:03301815:28

Page 14 of 65

Chloroform


Tetrachloroethene

Chlorobenzene

1,2-Dichloroethane

Benzene

Vinyl chloride

1,1-Dichloroethene

Trichloroethene

1,4-Dichlorobenzene

2-Butanone

98

100

100

98

95

97

81

96

100

100

100

100

100

99

99

99

99

80

100

99

100

100

70-130

63-132

70-130

75-130

70-130

70-130

55-140

61-145

70-130

70-130

63-138

2

0

1

1

4

2

1

4

1

0

0

20

20

20

25

20

25

20

25

25

20

20

ParameterLCS

%RecoveryLCSD

%Recovery%Recovery

Limits RPDRPD

Limits

TCLP Volatiles by EPA 1311 - Westborough Lab Associated sample(s): 02 Batch: WG1100473-3 WG1100473-4


Project Name:

Project Number:

Lab Number:

Report Date:

NFTA

17005.02

L1808681

1,2-Dichloroethane-d4Toluene-d84-Bromofluorobenzenedibromofluoromethane

969910093

70-13070-13070-13070-130

9710010093


03/30/18

AcceptanceCriteria

Qual Qual Qual

Serial_No:03301815:28

Page 15 of 65

SEMIVOLATILES

Serial_No:03301815:28

Page 16 of 65

FF

Hexachlorobenzene

2,4-Dinitrotoluene

Hexachlorobutadiene

Hexachloroethane

Nitrobenzene

2,4,6-Trichlorophenol

Pentachlorophenol

2-Methylphenol

3-Methylphenol/4-Methylphenol


Pyridine


ND

ND

ND

ND

ND

ND

ND

ND

ND

ND

ND

ug/l

ug/l

ug/l

ug/l

ug/l

ug/l

ug/l

ug/l

ug/l

ug/l

ug/l

1

1

1

1

1

1

1

1

1

1

1

Qualifier Units RL

TCLP Semivolatiles by EPA 1311 - Westborough Lab

SAMPLE RESULTS

Project Name:

Project Number:

Lab Number:

Report Date:

NFTA

17005.02

L1808681

10

25

10

10

10

25

50

25

25

25

18

2-Fluorophenol

Phenol-d6

Nitrobenzene-d5

2-Fluorobiphenyl

2,4,6-Tribromophenol

4-Terphenyl-d14

66

57

56

79

92

96

21-120

10-120

23-120

15-120

10-120

33-120


03/30/18

BH1/3-18Client ID:03/14/18 12:30Date Collected:03/14/18Date Received:


L1808681-03Lab ID:


Matrix: Soil Extraction Method:

Analytical Method:Analytical Date:Analyst:

1,8270D03/28/18 00:43TT

EPA 3510CExtraction Date: 03/27/18 16:56


80%Percent Solids:

MDL

2.9

4.2

3.6

3.4

3.8

3.4

17.

5.1

5.6

3.6

9.4

Sample Depth:

Serial_No:03301815:28

Page 17 of 65

Acenaphthene

Hexachlorobenzene

Fluoranthene

Naphthalene

Benzo(a)anthracene

Benzo(a)pyrene

Benzo(b)fluoranthene

Benzo(k)fluoranthene

Chrysene

Acenaphthylene

Anthracene

Benzo(ghi)perylene

Fluorene

Phenanthrene

Dibenzo(a,h)anthracene

Indeno(1,2,3-cd)pyrene

Pyrene

Dibenzofuran

Pentachlorophenol

Phenol

2-Methylphenol


Parameter Result

J

J

J

J

J

Dilution Factor

ND

ND

56

ND

28

ND

ND

ND

26

ND

ND

ND

ND

34

ND

ND

52

ND

ND

ND

ND

ND

ug/kg

ug/kg

ug/kg

ug/kg

ug/kg

ug/kg

ug/kg

ug/kg

ug/kg

ug/kg

ug/kg

ug/kg

ug/kg

ug/kg

ug/kg

ug/kg

ug/kg

ug/kg

ug/kg

ug/kg

ug/kg

ug/kg

1

1

1

1

1

1

1

1

1

1

1

1

1

1

1

1

1

1

1

1

1

1

Qualifier Units RL

Semivolatile Organics by GC/MS - Westborough Lab

SAMPLE RESULTS

Project Name:

Project Number:

Lab Number:

Report Date:

NFTA

17005.02

L1808681

160

120

120

210

120

160

120

120

120

160

120

160

210

120

120

160

120

210

160

210

210

300

03/30/18



L1808681-03Lab ID:




1,8270D03/23/18 13:36CB

EPA 3546Extraction Date: 03/22/18 09:18

80%Percent Solids:

MDL

21.

23.

24.

25.

23.

50.

35.

33.

22.

32.

40.

24.

20.

25.

24.

29.

20.

20.

46.

31.

32.

32.

Sample Depth:

Serial_No:03301815:28

Page 18 of 65

Parameter Result Dilution FactorQualifier Units RL


SAMPLE RESULTS

Project Name:

Project Number:

Lab Number:

Report Date:

NFTA

17005.02

L1808681

2-Fluorophenol

Phenol-d6

Nitrobenzene-d5

2-Fluorobiphenyl


4-Terphenyl-d14

70

76

78

82

77

78

25-120

10-120

23-120

30-120

10-136

18-120


03/30/18



L1808681-03Lab ID:


MDL

Sample Depth:

Serial_No:03301815:28

Page 19 of 65


Project Name:

Project Number:

Lab Number:

Report Date:

NFTA

17005.02

L1808681

03/22/18 23:311,8270DAnalytical Method:

Analytical Date:Extraction Method: EPA 3546Extraction Date: 03/22/18 09:18

03/30/18

Analyst: RC

Acenaphthene

Hexachlorobenzene

Fluoranthene

Naphthalene

Benzo(a)anthracene

Benzo(a)pyrene



Chrysene

Acenaphthylene

Anthracene

Benzo(ghi)perylene

Fluorene

Phenanthrene



Pyrene

Dibenzofuran

Pentachlorophenol

Phenol

2-Methylphenol


Parameter Result

ND

ND

ND

ND

ND

ND

ND

ND

ND

ND

ND

ND

ND

ND

ND

ND

ND

ND

ND

ND

ND

ND

RL

130

98

98

160

98

130

98

98

98

130

98

130

160

98

98

130

98

160

130

160

160

240

ug/kg

ug/kg

ug/kg

ug/kg

ug/kg

ug/kg

ug/kg

ug/kg

ug/kg

ug/kg

ug/kg

ug/kg

ug/kg

ug/kg

ug/kg

ug/kg

ug/kg

ug/kg

ug/kg

ug/kg

ug/kg

ug/kg

UnitsQualifier

Semivolatile Organics by GC/MS - Westborough Lab for sample(s): 03 Batch: WG1099482-1

No Tentatively Identified Compounds ND ug/kg

Tentatively Identified Compounds

MDL

17.

18.

19.

20.

18.

40.

28.

26.

17.

25.

32.

19.

16.

20.

19.

23.

16.

15.

36.

25.

25.

26.

Serial_No:03301815:28

Page 20 of 65


Project Name:

Project Number:

Lab Number:

Report Date:

NFTA

17005.02

L1808681



03/30/18

Analyst: RC

Parameter Result RLUnitsQualifier


2-Fluorophenol

Phenol-d6

Nitrobenzene-d5

2-Fluorobiphenyl


4-Terphenyl-d14

72

78

75

76

73

79

25-120

10-120

23-120

30-120

10-136

18-120


Criteria

MDL

Serial_No:03301815:28

Page 21 of 65


Project Name:

Project Number:

Lab Number:

Report Date:

NFTA

17005.02

L1808681


Analytical Date:Extraction Method: EPA 3510CExtraction Date: 03/27/18 16:56

03/30/18

Analyst: TT

Hexachlorobenzene

2,4-Dinitrotoluene

Hexachlorobutadiene

Hexachloroethane

Nitrobenzene


Pentachlorophenol

2-Methylphenol



Pyridine

Parameter Result

ND

ND

ND

ND

ND

ND

ND

ND

ND

ND

ND

RL

10

25

10

10

10

25

50

25

25

25

18

ug/l

ug/l

ug/l

ug/l

ug/l

ug/l

ug/l

ug/l

ug/l

ug/l

ug/l

UnitsQualifier

TCLP Semivolatiles by EPA 1311 - Westborough Lab for sample(s): 03 Batch: WG1100953-1

2-Fluorophenol

Phenol-d6

Nitrobenzene-d5

2-Fluorobiphenyl


4-Terphenyl-d14

63

54

54

78

91

83

21-120

10-120

23-120

15-120

10-120

33-120


Criteria


MDL

2.9

4.2

3.6

3.4

3.8

3.4

17.

5.1

5.6

3.6

9.4

Serial_No:03301815:28

Page 22 of 65

Acenaphthene

Hexachlorobenzene

Fluoranthene

Naphthalene

Benzo(a)anthracene

Benzo(a)pyrene



Chrysene

Acenaphthylene

Anthracene

Benzo(ghi)perylene

Fluorene

Phenanthrene



Pyrene

Dibenzofuran

Pentachlorophenol

Phenol

2-Methylphenol


78

85

78

77

84

85

82

81

80

87

78

84

79

75

85

86

75

79

66

81

90

90

68

73

68

66

74

73

72

70

71

76

69

74

70

66

76

74

66

69

62

68

76

77

31-137

40-140

40-140

40-140

40-140

40-140

40-140

40-140

40-140

40-140

40-140

40-140

40-140

40-140

40-140

40-140

35-142

40-140

17-109

26-90

30-130.

30-130

14

15

14

15

13

15

13

15

12

13

12

13

12

13

11

15

13

14

6

17

17

16

50

50

50

50

50

50

50

50

50

50

50

50

50

50

50

50

50

50

50

50

50

50

ParameterLCS

%RecoveryLCSD

%Recovery%Recovery

Limits RPDRPD

Limits

Semivolatile Organics by GC/MS - Westborough Lab Associated sample(s): 03 Batch: WG1099482-2 WG1099482-3


Project Name:

Project Number:

Lab Number:

Report Date:

NFTA

17005.02

L1808681

03/30/18

Qual Qual Qual

Serial_No:03301815:28

Page 23 of 65

ParameterLCS

%RecoveryLCSD

%Recovery%Recovery

Limits RPDRPD

Limits



Project Name:

Project Number:

Lab Number:

Report Date:

NFTA

17005.02

L1808681

2-FluorophenolPhenol-d6Nitrobenzene-d52-Fluorobiphenyl2,4,6-Tribromophenol4-Terphenyl-d14

838890858681

25-12010-12023-12030-12010-13618-120

697575757771


03/30/18

AcceptanceCriteria

Qual Qual Qual

Serial_No:03301815:28

Page 24 of 65

Hexachlorobenzene

2,4-Dinitrotoluene

Hexachlorobutadiene

Hexachloroethane

Nitrobenzene


Pentachlorophenol

2-Methylphenol



Pyridine

88

78

81

60

55

81

75

68

68

88

25

70

63

68

49

44

64

58

54

52

70

5

40-140

40-132

28-111

21-105

40-140

30-130

9-103

30-130

30-130

30-130

10-66

23

21

17

20

22

23

26

23

27

23

130

30

30

30

30

30

30

30

30

30

30

30

ParameterLCS

%RecoveryLCSD

%Recovery%Recovery

Limits RPDRPD

Limits

TCLP Semivolatiles by EPA 1311 - Westborough Lab Associated sample(s): 03 Batch: WG1100953-2 WG1100953-3


Project Name:

Project Number:

Lab Number:

Report Date:

NFTA

17005.02

L1808681


6862588210091

21-12010-12023-12015-12010-12033-120

555046698072


03/30/18

AcceptanceCriteria

Qual Qual

Q

Qual

Q

Serial_No:03301815:28

Page 25 of 65

PCBS

Serial_No:03301815:28

Page 26 of 65

FF

Aroclor 1016

Aroclor 1221

Aroclor 1232

Aroclor 1242

Aroclor 1248

Aroclor 1254

Aroclor 1260

Aroclor 1262

Aroclor 1268


ND

ND

ND

ND

ND

ND

ND

ND

ND

ug/kg

ug/kg

ug/kg

ug/kg

ug/kg

ug/kg

ug/kg

ug/kg

ug/kg

1

1

1

1

1

1

1

1

1

Qualifier Units RL

Polychlorinated Biphenyls by GC - Westborough Lab

SAMPLE RESULTS

Project Name:

Project Number:

Lab Number:

Report Date:

NFTA

17005.02

L1808681

40.4

40.4

40.4

40.4

40.4

40.4

40.4

40.4

40.4

2,4,5,6-Tetrachloro-m-xylene

Decachlorobiphenyl


Decachlorobiphenyl

70

45

75

45

30-150

30-150

30-150

30-150

Acceptance Criteria

A

A

B

B

Surrogate % Recovery Qualifier Column

03/30/18



L1808681-03Lab ID:



Cleanup Method:Analytical Method:Analytical Date:Analyst:

1,8082A03/23/18 05:12JW

EPA 3546

EPA 3665AExtraction Date: 03/22/18 01:15

Cleanup Date: 03/22/18Cleanup Method: EPA 3660BCleanup Date: 03/23/18

80%Percent Solids:

MDL

4.58

6.15

3.97

4.94

4.53

3.30

4.22

3.32

2.86

A

A

A

A

A

A

A

A

A

Column

Sample Depth:

Serial_No:03301815:28

Page 27 of 65


Project Name:

Project Number:

Lab Number:

Report Date:

NFTA

17005.02

L1808681

03/22/18 17:041,8082AAnalytical Method:

Analytical Date:Extraction Method:

Cleanup Method:

EPA 3546


03/30/18

Cleanup Method: EPA 3660B

Analyst: WR

Aroclor 1016

Aroclor 1221

Aroclor 1232

Aroclor 1242

Aroclor 1248

Aroclor 1254

Aroclor 1260

Aroclor 1262

Aroclor 1268

Parameter Result

ND

ND

ND

ND

ND

ND

ND

ND

ND

RL

33.1

33.1

33.1

33.1

33.1

33.1

33.1

33.1

33.1

ug/kg

ug/kg

ug/kg

ug/kg

ug/kg

ug/kg

ug/kg

ug/kg

ug/kg

UnitsQualifier

Polychlorinated Biphenyls by GC - Westborough Lab for sample(s): 03 Batch: WG1099107-1


Decachlorobiphenyl


Decachlorobiphenyl

101

75

111

95

30-150

30-150

30-150

30-150

Surrogate %Recovery Qualifier ColumnAcceptance

Criteria

Cleanup Date: 03/21/18


MDL

3.75

5.04

3.26

4.05

3.72

2.70

3.46

2.72

2.34

Column

A

A

A

A

A

A

A

A

A

A

A

B

B

Serial_No:03301815:28

Page 28 of 65

Aroclor 1016

Aroclor 1260

87

80

88

83

40-140

40-140

1

4

50

50

ParameterLCS

%RecoveryLCSD

%Recovery%Recovery

Limits RPDRPD

Limits

Polychlorinated Biphenyls by GC - Westborough Lab Associated sample(s): 03 Batch: WG1099107-2 WG1099107-3


Project Name:

Project Number:

Lab Number:

Report Date:

NFTA

17005.02

L1808681

2,4,5,6-Tetrachloro-m-xyleneDecachlorobiphenyl2,4,5,6-Tetrachloro-m-xyleneDecachlorobiphenyl

1118410990

30-15030-15030-15030-150

AABB

1098810791

Surrogate Qual Column%Recovery Qual%RecoveryLCS LCSD

03/30/18

AcceptanceCriteria

Qual Qual Qual Column

A

A

Serial_No:03301815:28

Page 29 of 65

PESTICIDES

Serial_No:03301815:28

Page 30 of 65

FF

Lindane

Heptachlor

Heptachlor epoxide

Endrin

Methoxychlor

Toxaphene

Chlordane


ND

ND

ND

ND

ND

ND

ND

ug/l

ug/l

ug/l

ug/l

ug/l

ug/l

ug/l

1

1

1

1

1

1

1

Qualifier Units RL

TCLP Pesticides by EPA 1311 - Westborough Lab

SAMPLE RESULTS

Project Name:

Project Number:

Lab Number:

Report Date:

NFTA

17005.02

L1808681

0.100

0.100

0.100

0.200

1.00

1.00

1.00


Decachlorobiphenyl


Decachlorobiphenyl

88

68

93

73

30-150

30-150

30-150

30-150

Acceptance Criteria

A

A

B

B


03/30/18



L1808681-03Lab ID:




1,8081B03/23/18 16:21JW



80%Percent Solids:

MDL

0.022

0.016

0.021

0.021

0.034

0.314

0.232

A

A

A

A

A

A

A

Column

Sample Depth:

Serial_No:03301815:28

Page 31 of 65

Delta-BHC

Lindane

Alpha-BHC

Beta-BHC

Heptachlor

Aldrin

Endrin

Dieldrin

4,4'-DDE

4,4'-DDD

4,4'-DDT

Endosulfan I

Endosulfan II

Endosulfan sulfate

cis-Chlordane


ND

ND

ND

ND

ND

ND

ND

ND

ND

ND

ND

ND

ND

ND

ND

ug/kg

ug/kg

ug/kg

ug/kg

ug/kg

ug/kg

ug/kg

ug/kg

ug/kg

ug/kg

ug/kg

ug/kg

ug/kg

ug/kg

ug/kg

1

1

1

1

1

1

1

1

1

1

1

1

1

1

1

Qualifier Units RL

Organochlorine Pesticides by GC - Westborough Lab

SAMPLE RESULTS

Project Name:

Project Number:

Lab Number:

Report Date:

NFTA

17005.02

L1808681

1.89

0.788

0.788

1.89

0.945

1.89

0.788

1.18

1.89

1.89

3.54

1.89

1.89

0.788

2.36


Decachlorobiphenyl


Decachlorobiphenyl

69

74

74

78

30-150

30-150

30-150

30-150

Acceptance Criteria

B

B

A

A


03/30/18



L1808681-03Lab ID:




1,8081B03/24/18 03:46JW

EPA 3546

EPA 3620BExtraction Date: 03/22/18 04:20

Cleanup Date: 03/23/18 80%Percent Solids:

MDL

0.370

0.352

0.224

0.717

0.424

0.666

0.323

0.591

0.437

0.674

1.52

0.446

0.632

0.375

0.658

A

A

A

A

A

A

A

A

A

A

A

A

A

A

A

Column

Sample Depth:

Serial_No:03301815:28

Page 32 of 65

2,4-D

2,4,5-TP (Silvex)


ND

ND

mg/l

mg/l

1

1

Qualifier Units RL

TCLP Herbicides by EPA 1311 - Westborough Lab

SAMPLE RESULTS

Project Name:

Project Number:

Lab Number:

Report Date:

NFTA

17005.02

L1808681

0.025

0.005

DCAA

DCAA

61

51

30-150

30-150

Acceptance Criteria

A

B


03/30/18



L1808681-03Lab ID:




1,8151A03/25/18 09:53KEG



80%Percent Solids:

MDL

0.001

0.001

Methylation Date: 03/23/18 09:12

A

A

Column

Sample Depth:

Serial_No:03301815:28

Page 33 of 65

2,4,5-TP (Silvex)


ND ug/kg 1

Qualifier Units RL

Chlorinated Herbicides by GC - Westborough Lab

SAMPLE RESULTS

Project Name:

Project Number:

Lab Number:

Report Date:

NFTA

17005.02

L1808681

208

DCAA

DCAA

145

130

30-150

30-150

Acceptance Criteria

A

B


03/30/18



L1808681-03Lab ID:




1,8151A03/25/18 14:53SL


80%Percent Solids:

MDL

5.54


A

Column

Sample Depth:

Serial_No:03301815:28

Page 34 of 65


Project Name:

Project Number:

Lab Number:

Report Date:

NFTA

17005.02

L1808681

03/23/18 14:461,8081BAnalytical Method:


Cleanup Method:

EPA 3546


03/30/18

Analyst: JW

Delta-BHC

Lindane

Alpha-BHC

Beta-BHC

Heptachlor

Aldrin

Endrin

Dieldrin

4,4'-DDE

4,4'-DDD

4,4'-DDT

Endosulfan I

Endosulfan II

Endosulfan sulfate

cis-Chlordane

Parameter Result

ND

ND

ND

ND

ND

ND

ND

ND

ND

ND

ND

ND

ND

ND

ND

RL

1.52

0.635

0.635

1.52

0.762

1.52

0.635

0.952

1.52

1.52

2.86

1.52

1.52

0.635

1.90

ug/kg

ug/kg

ug/kg

ug/kg

ug/kg

ug/kg

ug/kg

ug/kg

ug/kg

ug/kg

ug/kg

ug/kg

ug/kg

ug/kg

ug/kg

UnitsQualifier

Organochlorine Pesticides by GC - Westborough Lab for sample(s): 03 Batch: WG1099404-1


Decachlorobiphenyl


Decachlorobiphenyl

102

117

102

57

30-150

30-150

30-150

30-150


Criteria


MDL

0.298

0.284

0.180

0.578

0.342

0.536

0.260

0.476

0.352

0.543

1.22

0.360

0.509

0.302

0.531

Column

A

A

A

A

A

A

A

A

A

A

A

A

A

A

A

B

B

A

A

Serial_No:03301815:28

Page 35 of 65


Project Name:

Project Number:

Lab Number:

Report Date:

NFTA

17005.02

L1808681



03/30/18

Analyst: JW

Lindane

Heptachlor

Heptachlor epoxide

Endrin

Methoxychlor

Toxaphene

Chlordane

Parameter Result

ND

ND

ND

ND

ND

ND

ND

RL

0.100

0.100

0.100

0.200

1.00

1.00

1.00

ug/l

ug/l

ug/l

ug/l

ug/l

ug/l

ug/l

UnitsQualifier

TCLP Pesticides by EPA 1311 - Westborough Lab for sample(s): 03 Batch: WG1099724-1


Decachlorobiphenyl


Decachlorobiphenyl

100

90

106

97

30-150

30-150

30-150

30-150


Criteria


MDL

0.022

0.016

0.021

0.021

0.034

0.314

0.232

Column

A

A

A

A

A

A

A

A

A

B

B

Serial_No:03301815:28

Page 36 of 65


Project Name:

Project Number:

Lab Number:

Report Date:

NFTA

17005.02

L1808681


Analytical Date:Extraction Method: EPA 8151AExtraction Date: 03/22/18 16:36

03/30/18

Analyst: SL

2,4,5-TP (Silvex)

Parameter Result

ND

RL

162ug/kg

UnitsQualifier

Chlorinated Herbicides by GC - Westborough Lab for sample(s): 03 Batch: WG1099726-1

DCAA

DCAA

102

97

30-150

30-150


Criteria

MDL

4.31


Column

A

A

B

Serial_No:03301815:28

Page 37 of 65


Project Name:

Project Number:

Lab Number:

Report Date:

NFTA

17005.02

L1808681



03/30/18

Analyst: KEG

2,4-D

2,4,5-TP (Silvex)

Parameter Result

ND

ND

RL

0.025

0.005

mg/l

mg/l

UnitsQualifier

TCLP Herbicides by EPA 1311 - Westborough Lab for sample(s): 03 Batch: WG1099782-1

DCAA

DCAA

46

47

30-150

30-150


Criteria


MDL

0.001

0.001


Column

A

A

A

B

Serial_No:03301815:28

Page 38 of 65

Delta-BHC

Lindane

Alpha-BHC

Beta-BHC

Heptachlor

Aldrin

Endrin

Dieldrin

4,4'-DDE

4,4'-DDD

4,4'-DDT

Endosulfan I

Endosulfan II

Endosulfan sulfate

cis-Chlordane

89

94

91

97

103

99

100

106

95

81

85

100

95

68

93

84

91

87

94

99

93

96

101

90

77

80

95

92

74

80

30-150

30-150

30-150

30-150

30-150

30-150

30-150

30-150

30-150

30-150

30-150

30-150

30-150

30-150

30-150

6

3

4

3

4

6

4

5

5

5

6

5

3

8

15

30

30

30

30

30

30

30

30

30

30

30

30

30

30

30

ParameterLCS

%RecoveryLCSD

%Recovery%Recovery

Limits RPDRPD

Limits

Organochlorine Pesticides by GC - Westborough Lab Associated sample(s): 03 Batch: WG1099404-2 WG1099404-3


Project Name:

Project Number:

Lab Number:

Report Date:

NFTA

17005.02

L1808681


921119774

30-15030-15030-15030-150

BBAA

881088663


03/30/18

AcceptanceCriteria


A

A

A

A

A

A

A

A

A

A

A

A

A

A

A

Serial_No:03301815:28

Page 39 of 65

Lindane

Heptachlor

Heptachlor epoxide

Endrin

Methoxychlor

114

112

111

116

116

114

110

109

113

115

30-150

30-150

30-150

30-150

30-150

0

2

2

3

1

20

20

20

20

20

ParameterLCS

%RecoveryLCSD

%Recovery%Recovery

Limits RPDRPD

Limits

TCLP Pesticides by EPA 1311 - Westborough Lab Associated sample(s): 03 Batch: WG1099724-2 WG1099724-3


Project Name:

Project Number:

Lab Number:

Report Date:

NFTA

17005.02

L1808681


10599110104

30-15030-15030-15030-150

AABB

10196104100


03/30/18

AcceptanceCriteria


A

A

A

A

A

Serial_No:03301815:28

Page 40 of 65

2,4,5-TP (Silvex) 83 80 30-150 4 30

ParameterLCS

%RecoveryLCSD

%Recovery%Recovery

Limits RPDRPD

Limits

Chlorinated Herbicides by GC - Westborough Lab Associated sample(s): 03 Batch: WG1099726-2 WG1099726-3


Project Name:

Project Number:

Lab Number:

Report Date:

NFTA

17005.02

L1808681

DCAADCAA

110109

30-15030-150

AB

111112


03/30/18

AcceptanceCriteria


A

Serial_No:03301815:28

Page 41 of 65

2,4-D

2,4,5-TP (Silvex)

103

46

85

38

30-150

30-150

19

19

25

25

ParameterLCS

%RecoveryLCSD

%Recovery%Recovery

Limits RPDRPD

Limits

TCLP Herbicides by EPA 1311 - Westborough Lab Associated sample(s): 03 Batch: WG1099782-2 WG1099782-3


Project Name:

Project Number:

Lab Number:

Report Date:

NFTA

17005.02

L1808681

DCAADCAA

6037

30-15030-150

AB

5022 Q


03/30/18

AcceptanceCriteria


A

A

Serial_No:03301815:28

Page 42 of 65

METALS

Serial_No:03301815:28

Page 43 of 65

FF

Project Name:

Project Number:

Lab Number:

Report Date:

NFTA

17005.02

L1808681

03/30/18

SAMPLE RESULTS


Matrix: Soil


L1808681-03Lab ID:


Parameter ResultDilution FactorQualifier Units RL

DateAnalyzed

AnalyticalMethod Analyst

Date Prepared

TCLP Metals by EPA 1311 - Mansfield Lab

Arsenic, TCLP

Barium, TCLP

Cadmium, TCLP

Chromium, TCLP

Lead, TCLP

Mercury, TCLP

Selenium, TCLP

Silver, TCLP

J

J

ND

0.397

ND

ND

0.035

ND

ND

ND

mg/l

mg/l

mg/l

mg/l

mg/l

mg/l

mg/l

mg/l

1

1

1

1

1

1

1

1

1.00

0.500

0.100

0.200

0.500

0.0010

0.500

0.100

03/22/18 23:59

03/22/18 23:59

03/22/18 23:59

03/22/18 23:59

03/22/18 23:59

03/22/18 15:52

03/22/18 23:59

03/22/18 23:59

1,6010C

1,6010C

1,6010C

1,6010C

1,6010C

1,7470A

1,6010C

1,6010C

AB

AB

AB

AB

AB

MG

AB

AB

03/22/18 17:24

03/22/18 17:24

03/22/18 17:24

03/22/18 17:24

03/22/18 17:24

03/21/18 15:20

03/22/18 17:24

03/22/18 17:24

EPA 3015

EPA 3015

EPA 3015

EPA 3015

EPA 3015

EPA 7470A

EPA 3015

EPA 3015

PrepMethod

03/20/18 16:22TCLP/SPLP Ext. Date:

Percent Solids: 80%

MDL

0.019

0.021

0.010

0.021

0.027

0.0003

0.035

0.028

Sample Depth:

Serial_No:03301815:28

Page 44 of 65

Project Name:

Project Number:

Lab Number:

Report Date:

NFTA

17005.02

L1808681

03/30/18

SAMPLE RESULTS


Matrix: Soil


L1808681-03Lab ID:



DateAnalyzed


Date Prepared

Total Metals - Mansfield Lab

General Chemistry - Mansfield Lab

Arsenic, Total

Barium, Total

Beryllium, Total

Cadmium, Total

Chromium, Total

Copper, Total

Lead, Total

Manganese, Total

Mercury, Total

Nickel, Total

Selenium, Total

Silver, Total

Zinc, Total

Chromium, Trivalent

J

J

J

1.54

34.6

0.223

0.292

7.18

9.60

48.9

182

0.09

6.76

0.218

ND

46.4

7.2

mg/kg

mg/kg

mg/kg

mg/kg

mg/kg

mg/kg

mg/kg

mg/kg

mg/kg

mg/kg

mg/kg

mg/kg

mg/kg

mg/kg

1

1

1

1

1

1

1

1

1

1

1

1

1

1

0.495

0.495

0.248

0.495

0.495

0.495

2.48

0.495

0.08

1.24

0.990

0.495

2.48

1.0

03/16/18 15:18

03/16/18 15:18

03/16/18 15:18

03/16/18 15:18

03/16/18 15:18

03/16/18 15:18

03/16/18 15:18

03/16/18 15:18

03/16/18 21:52

03/16/18 15:18

03/16/18 15:18

03/16/18 15:18

03/16/18 15:18

03/22/18 11:45

1,6010C

1,6010C

1,6010C

1,6010C

1,6010C

1,6010C

1,6010C

1,6010C

1,7471B

1,6010C

1,6010C

1,6010C

1,6010C

107,-

PS

PS

PS

PS

PS

PS

PS

PS

EA

PS

PS

PS

PS

03/15/18 20:50

03/15/18 20:50

03/15/18 20:50

03/15/18 20:50

03/15/18 20:50

03/15/18 20:50

03/15/18 20:50

03/15/18 20:50

03/16/18 08:20

03/15/18 20:50

03/15/18 20:50

03/15/18 20:50

03/15/18 20:50

EPA 3050B

EPA 3050B

EPA 3050B

EPA 3050B

EPA 3050B

EPA 3050B

EPA 3050B

EPA 3050B

EPA 7471B

EPA 3050B

EPA 3050B

EPA 3050B

EPA 3050B

NA

PrepMethod

Percent Solids: 80%

MDL

0.103

0.086

0.016

0.049

0.048

0.128

0.133

0.079

0.02

0.120

0.128

0.140

0.145

1.0

Sample Depth:

Serial_No:03301815:28

Page 45 of 65

FF

Parameter

Parameter

Parameter

Result

Result

Result

Dilution Factor

Dilution Factor

Dilution Factor

Qualifier

Qualifier

Qualifier

Units

Units

Units

RL

RL

RL


Project Name:

Project Number:

Lab Number:

Report Date:

NFTA

17005.02

L1808681

DateAnalyzed

DateAnalyzed

DateAnalyzed

AnalyticalMethod

AnalyticalMethod

AnalyticalMethod

Analyst

Analyst

Analyst

Date Prepared

Date Prepared

Date Prepared

03/30/18

Arsenic, Total

Barium, Total

Beryllium, Total

Cadmium, Total

Chromium, Total

Copper, Total

Lead, Total

Manganese, Total

Nickel, Total

Selenium, Total

Silver, Total

Zinc, Total

Mercury, Total

Mercury, TCLP

ND

ND

ND

ND

ND

ND

ND

ND

ND

ND

ND

ND

ND

ND

mg/kg

mg/kg

mg/kg

mg/kg

mg/kg

mg/kg

mg/kg

mg/kg

mg/kg

mg/kg

mg/kg

mg/kg

mg/kg

mg/l

1

1

1

1

1

1

1

1

1

1

1

1

1

1

0.400

0.400

0.200

0.400

0.400

0.400

2.00

0.400

1.00

0.800

0.400

2.00

0.08

0.0010

03/16/18 14:47

03/16/18 14:47

03/16/18 14:47

03/16/18 14:47

03/16/18 14:47

03/16/18 14:47

03/16/18 14:47

03/16/18 14:47

03/16/18 14:47

03/16/18 14:47

03/16/18 14:47

03/16/18 14:47

03/16/18 21:37

03/22/18 15:43

1,6010C

1,6010C

1,6010C

1,6010C

1,6010C

1,6010C

1,6010C

1,6010C

1,6010C

1,6010C

1,6010C

1,6010C

1,7471B

1,7470A

PS

PS

PS

PS

PS

PS

PS

PS

PS

PS

PS

PS

EA

MG

03/15/18 20:50

03/15/18 20:50

03/15/18 20:50

03/15/18 20:50

03/15/18 20:50

03/15/18 20:50

03/15/18 20:50

03/15/18 20:50

03/15/18 20:50

03/15/18 20:50

03/15/18 20:50

03/15/18 20:50

03/16/18 08:20

03/21/18 15:20

Total Metals - Mansfield Lab for sample(s): 03 Batch: WG1097505-1

Total Metals - Mansfield Lab for sample(s): 03 Batch: WG1097635-1

TCLP Metals by EPA 1311 - Mansfield Lab for sample(s): 03 Batch: WG1099268-1

EPA 3050B

EPA 7471B

Digestion Method:

Digestion Method:

Prep Information

Prep Information

MDL

MDL

MDL

0.083

0.070

0.013

0.039

0.038

0.103

0.107

0.064

0.097

0.103

0.113

0.117

0.02

0.0003

Serial_No:03301815:28

Page 46 of 65



Project Name:

Project Number:

Lab Number:

Report Date:

NFTA

17005.02

L1808681

DateAnalyzed


Date Prepared

03/30/18

Arsenic, TCLP

Barium, TCLP

Cadmium, TCLP

Chromium, TCLP

Lead, TCLP

Selenium, TCLP

Silver, TCLP

J

ND

ND

ND

ND

0.053

ND

ND

mg/l

mg/l

mg/l

mg/l

mg/l

mg/l

mg/l

1

1

1

1

1

1

1

1.00

0.500

0.100

0.200

0.500

0.500

0.100

03/22/18 23:23

03/22/18 23:23

03/22/18 23:23

03/22/18 23:23

03/22/18 23:23

03/22/18 23:23

03/22/18 23:23

1,6010C

1,6010C

1,6010C

1,6010C

1,6010C

1,6010C

1,6010C

AB

AB

AB

AB

AB

AB

AB

03/22/18 17:24

03/22/18 17:24

03/22/18 17:24

03/22/18 17:24

03/22/18 17:24

03/22/18 17:24

03/22/18 17:24


EPA 7470A

EPA 3015

Digestion Method:

Digestion Method:

Prep Information

Prep Information

03/20/18 16:22

03/20/18 16:22

TCLP/SPLP Extraction Date:


MDL

0.019

0.021

0.010

0.021

0.027

0.035

0.028

Serial_No:03301815:28

Page 47 of 65

Arsenic, Total

Barium, Total

Beryllium, Total

Cadmium, Total

Chromium, Total

Copper, Total

Lead, Total

Manganese, Total

Nickel, Total

Selenium, Total

Silver, Total

Zinc, Total

Mercury, Total

Mercury, TCLP

87

83

83

86

93

85

91

94

86

87

85

82

102

106

-

-

-

-

-

-

-

-

-

-

-

-

-

-

83-117

82-118

83-117

82-117

83-119

84-116

82-117

82-118

82-117

78-121

80-120

81-119

50-149

80-120

-

-

-

-

-

-

-

-

-

-

-

-

-

-

ParameterLCS

%RecoveryLCSD

%Recovery%Recovery

Limits RPD RPD Limits

Total Metals - Mansfield Lab Associated sample(s): 03 Batch: WG1097505-2 SRM Lot Number: D098-540

Total Metals - Mansfield Lab Associated sample(s): 03 Batch: WG1097635-2 SRM Lot Number: D098-540

TCLP Metals by EPA 1311 - Mansfield Lab Associated sample(s): 03 Batch: WG1099268-2


Project Name:

Project Number:

Lab Number:

Report Date:

NFTA

17005.02

L1808681

03/30/18

Qual Qual Qual

Serial_No:03301815:28

Page 48 of 65

Arsenic, TCLP

Barium, TCLP

Cadmium, TCLP

Chromium, TCLP

Lead, TCLP

Selenium, TCLP

Silver, TCLP

107

96

102

94

100

104

94

-

-

-

-

-

-

-

75-125

75-125

75-125

75-125

75-125

75-125

75-125

-

-

-

-

-

-

-

20

20

20

20

20

20

20

ParameterLCS

%RecoveryLCSD

%Recovery%Recovery




Project Name:

Project Number:

Lab Number:

Report Date:

NFTA

17005.02

L1808681

03/30/18

Serial_No:03301815:28

Page 49 of 65

Arsenic, Total

Barium, Total

Beryllium, Total

Cadmium, Total

Chromium, Total

Copper, Total

Lead, Total

Manganese, Total

Nickel, Total

Selenium, Total

Silver, Total

Zinc, Total

Mercury, Total

Mercury, TCLP

10.7

62.6

0.521

0.408J

38.4

105.

37.9

160.

27.0

0.918J

0.187J

33.8

0.29

ND

23.3

237

5.00

5.23

79.3

163

79.6

320

80.6

11.8

31.0

78.8

0.53

0.0262

92

77

79

90

180

204

72

282

94

87

91

79

157

105

-

-

-

-

-

-

-

-

-

-

-

-

-

-

-

-

-

-

-

-

-

-

-

-

-

-

-

-

75-125

75-125

75-125

75-125

75-125

75-125

75-125

75-125

75-125

75-125

75-125

75-125

80-120

80-120

-

-

-

-

-

-

-

-

-

-

-

-

-

-

20

20

20

20

20

20

20

20

20

20

20

20

20

20

ParameterNative Sample

MS Found

MS%Recovery

MSD Found

MSD %Recovery

RecoveryLimits RPD

RPD Limits

Total Metals - Mansfield Lab Associated sample(s): 03 QC Batch ID: WG1097505-3 QC Sample: L1808743-01 Client ID: MS Sample

Total Metals - Mansfield Lab Associated sample(s): 03 QC Batch ID: WG1097635-3 QC Sample: L1808901-01 Client ID: MS Sample

TCLP Metals by EPA 1311 - Mansfield Lab Associated sample(s): 03 QC Batch ID: WG1099268-3 QC Sample: L1809192-01 Client ID: MS Sample

13.6

227

5.68

5.79

22.7

28.4

57.9

56.8

56.8

13.6

34.1

56.8

0.153

0.025

MS Added

Matrix Spike AnalysisBatch Quality Control

Project Name:

Project Number:

Lab Number:

Report Date:

NFTA

17005.02

L1808681

03/30/18

Qual

Q

Q

Q

Q

Q

Qual Qual

Serial_No:03301815:28

Page 50 of 65

Arsenic, TCLP

Barium, TCLP

Cadmium, TCLP

Chromium, TCLP

Lead, TCLP

Selenium, TCLP

Silver, TCLP

ND

0.527

ND

ND

0.063J

ND

ND

1.27

19.8

0.521

1.90

5.04

1.28

0.476

106

96

102

95

99

107

95

-

-

-

-

-

-

-

-

-

-

-

-

-

-

75-125

75-125

75-125

75-125

75-125

75-125

75-125

-

-

-

-

-

-

-

20

20

20

20

20

20

20


MS Found

MS%Recovery

MSD Found

MSD %Recovery

RecoveryLimits RPD

RPD Limits


1.2

20

0.51

2

5.1

1.2

0.5

MS Added


Project Name:

Project Number:

Lab Number:

Report Date:

NFTA

17005.02

L1808681

03/30/18

Serial_No:03301815:28

Page 51 of 65

Arsenic, Total

Beryllium, Total

Cadmium, Total

Lead, Total

Nickel, Total

Selenium, Total

Silver, Total

Mercury, Total

Mercury, TCLP

Arsenic, TCLP

Barium, TCLP

Cadmium, TCLP

Chromium, TCLP

Lead, TCLP

Selenium, TCLP

Silver, TCLP

10.7

0.521

0.408J

37.9

27.0

0.918J

0.187J

0.29

ND

ND

0.527

ND

ND

0.063J

ND

ND

12.6

0.544

0.623

43.6

39.4

1.18

0.219J

0.30

ND

ND

0.409J

ND

ND

0.042J

ND

ND

mg/kg

mg/kg

mg/kg

mg/kg

mg/kg

mg/kg

mg/kg

mg/kg

mg/l

mg/l

mg/l

mg/l

mg/l

mg/l

mg/l

mg/l

16

4

NC

14

37

NC

NC

3

NC

NC

NC

NC

NC

NC

NC

NC

20

20

20

20

20

20

20

20

20

20

20

20

20

20

20

20

Units RPDParameter Native Sample Duplicate Sample RPD Limits

Total Metals - Mansfield Lab Associated sample(s): 03 QC Batch ID: WG1097505-4 QC Sample: L1808743-01 Client ID: DUP Sample

Total Metals - Mansfield Lab Associated sample(s): 03 QC Batch ID: WG1097635-4 QC Sample: L1808901-01 Client ID: DUP Sample

TCLP Metals by EPA 1311 - Mansfield Lab Associated sample(s): 03 QC Batch ID: WG1099268-4 QC Sample: L1809192-01 Client ID: DUP Sample


NFTA

17005.02

Project Name:

Project Number:

L1808681Lab Number:

Report Date:

Lab Duplicate AnalysisBatch Quality Control

03/30/18

Qual

Q

Serial_No:03301815:28

Page 52 of 65

INORGANICS&

MISCELLANEOUS

Serial_No:03301815:28

Page 53 of 65

FF


Parameter ResultDilution Factor

Matrix: Soil


L1808681-01Lab ID:

Qualifier Units RL

SAMPLE RESULTS

Project Name:

Project Number:

Lab Number:

Report Date:

NFTA

17005.02

L1808681

Field Prep:

DateAnalyzed


Not Specified

General Chemistry - Westborough LabSolids, Total 82.6 % 10.100 03/15/18 11:22 121,2540G RI

Date Prepared

-

03/30/18

MDL

NA

Sample Depth:

Serial_No:03301815:28

Page 54 of 65

FF



Matrix: Soil


L1808681-03Lab ID:

Qualifier Units RL

SAMPLE RESULTS

Project Name:

Project Number:

Lab Number:

Report Date:

NFTA

17005.02

L1808681

Field Prep:

DateAnalyzed


Not Specified

General Chemistry - Westborough LabSolids, Total

Cyanide, Total

pH (H)

Flash Point

Chromium, Hexavalent

Cyanide, Reactive

Sulfide, Reactive

79.5

ND

9.3

>150

ND

ND

ND

%

mg/kg

SU

deg F

mg/kg

mg/kg

mg/kg

1

1

1

1

1

1

1

0.100

1.2

-

70

1.0

10

10

03/15/18 11:22

03/21/18 12:03

03/15/18 16:44

03/30/18 05:30

03/22/18 11:45

03/20/18 19:35

03/20/18 19:09

121,2540G

1,9010C/9012B

1,9045D

1,1010A

1,7196A

125,7.3

125,7.3

RI

LH

MA

JD

NH

RM

RM

Date Prepared

-

03/21/18 08:00

-

-

03/21/18 18:40

03/20/18 17:48

03/20/18 17:48

03/30/18

MDL

NA

0.25

NA

NA

0.20

10.

10.

Sample Depth:

Serial_No:03301815:28

Page 55 of 65

FF



Project Name:

Project Number:

Lab Number:

Report Date:

NFTA

17005.02

L1808681

DateAnalyzed


Date Prepared

03/30/18

Sulfide, Reactive

Cyanide, Reactive

Cyanide, Total


ND

ND

ND

ND

mg/kg

mg/kg

mg/kg

mg/kg

1

1

1

1

10

10

0.97

0.80

03/20/18 19:07

03/20/18 19:34

03/21/18 11:58

03/22/18 11:45

125,7.3

125,7.3

1,9010C/9012B

1,7196A

RM

RM

LH

NH

03/20/18 17:48

03/20/18 17:48

03/21/18 08:00

03/21/18 18:40

General Chemistry - Westborough Lab for sample(s): 03 Batch: WG1098905-1




MDL

10.

10.

0.20

0.16

Serial_No:03301815:28

Page 56 of 65

pH

Sulfide, Reactive

Cyanide, Reactive

Cyanide, Total


Flash Point

100

78

38

63

98

101

-

-

-

55

-

-

99-101

60-125

30-125

80-120

80-120

96-104

-

-

-

14

-

-

40

40

35

20

ParameterLCS

%RecoveryLCSD

%Recovery%Recovery


General Chemistry - Westborough Lab Associated sample(s): 03 Batch: WG1097472-1



General Chemistry - Westborough Lab Associated sample(s): 03 Batch: WG1099068-2 WG1099068-3




Project Name:

Project Number:

Lab Number:

Report Date:

NFTA

17005.02

L1808681

03/30/18

Qual Qual

Q Q

Qual

Serial_No:03301815:28

Page 57 of 65

Cyanide, Total


ND

ND

12

910

98

95

12

-

99

-

75-125

75-125

0

-

35

20


MS Found

MS%Recovery

MSD Found

MSD %Recovery

RecoveryLimits RPD

RPD Limits

General Chemistry - Westborough Lab Associated sample(s): 03 QC Batch ID: WG1099068-4 WG1099068-5 QC Sample: L1809454-03 Client ID: MS Sample

General Chemistry - Westborough Lab Associated sample(s): 03 QC Batch ID: WG1099354-4 QC Sample: L1809330-08 Client ID: MS Sample

12

953

MS Added


Project Name:

Project Number:

Lab Number:

Report Date:

NFTA

17005.02

L1808681

03/30/18

Qual Qual Qual

Serial_No:03301815:28

Page 58 of 65

Solids, Total

pH

Sulfide, Reactive

Cyanide, Reactive


63.7

4.9

ND

ND

ND

62.2

5.0

ND

ND

ND

%

SU

mg/kg

mg/kg

mg/kg

2

2

NC

NC

NC

20

5

40

40

20


General Chemistry - Westborough Lab Associated sample(s): 01,03 QC Batch ID: WG1097318-1 QC Sample: L1808463-01 Client ID: DUP Sample

General Chemistry - Westborough Lab Associated sample(s): 03 QC Batch ID: WG1097472-2 QC Sample: L1808743-01 Client ID: DUP Sample




NFTA

17005.02

Project Name:

Project Number:

L1808681Lab Number:

Report Date:


03/30/18

Qual

Serial_No:03301815:28

Page 59 of 65

*Values in parentheses indicate holding time in days

L1808681-01A

L1808681-01X

L1808681-01Y

L1808681-01Z

L1808681-02A

L1808681-02S

L1808681-02T

L1808681-03A

L1808681-03A1

L1808681-03B

L1808681-03C

L1808681-03D

L1808681-03E

L1808681-03W

L1808681-03X

L1808681-03X9

L1808681-04A

Vial Large Septa unpreserved (4oz)

Vial MeOH preserved split

Vial Water preserved split



Vial unpreserved Extracts


Plastic 2oz unpreserved for TS


Metals Only-Glass 60mL/2oz unpreserved


Glass 500ml/16oz unpreserved


Amber 1000ml unpreserved Extracts

Plastic 120ml HNO3 preserved Extracts

Tumble Vessel

Vial HCl preserved

A

A

A

A

A

A

A

A

A

A

A

A

A

A

A

A

A

NA

NA

NA

NA

NA

NA

NA

NA

NA

NA

NA

NA

NA

NA

NA

NA

NA

3.1

3.1

3.1

3.1

3.1

3.1

3.1

3.1

3.1

3.1

3.1

3.1

3.1

3.1

3.1

3.1

3.1

Y

Y

Y

Y

Y

Y

Y

Y

Y

Y

Y

Y

Y

Y

Y

Y

Y

Absent

Absent

Absent

Absent

Absent

Absent

Absent

Absent

Absent

Absent

Absent

Absent

Absent

Absent

Absent

Absent

Absent

A AbsentCooler Custody SealCooler Information

NFTA

17005.02

NYTCL-8260-R2(14),TS(7)

NYTCL-8260-R2(14)

NYTCL-8260-R2(14)

NYTCL-8260-R2(14)

TCLP-EXT-ZHE(14)

TCLP-VOA(14)

TCLP-VOA(14)

TS(7)

TS(7)

BE-TI(180),AS-TI(180),BA-TI(180),AG-TI(180),CR-TI(180),NI-TI(180),CU-TI(180),PB-TI(180),SE-TI(180),ZN-TI(180),HG-T(28),MN-TI(180),CD-TI(180)

HEXCR-7196(30)

NYTCL-8270(14),REACTS(14),TCN-9010(14),FLASH(),PH-9045(1),NYTCL-8081(14),HERB-8151(14),NYTCL-8082(14),REACTCN(14)

NYTCL-8270(14),REACTS(14),TCN-9010(14),FLASH(),PH-9045(1),NYTCL-8081(14),HERB-8151(14),NYTCL-8082(14),REACTCN(14)

TCLP-8270(14),HERB-TCLP*(14),PEST-TCLP*(14)

CD-CI(180),AS-CI(180),BA-CI(180),HG-C(28),PB-CI(180),CR-CI(180),SE-CI(180),AG-CI(180)

-

ARCHIVE()

Project Name:

Project Number:

L1808681Lab Number:

Report Date:

Sample Receipt and Container Information

Container ID Container Type CoolerTempdeg C Pres Seal

Container Information

Analysis(*)

03/30/18

Were project specific reporting limits specified? YES

22-MAR-18 08:43

22-MAR-18 08:43

FrozenDate/Time

FinalpH

Initial pH

Serial_No:03301815:28

Page 60 of 65

Report Format: DU Report with 'J' Qualifiers

GLOSSARY

Project Name:

Project Number:

Lab Number:

Report Date:

L1808681NFTA

17005.02 03/30/18

Acronyms

EDL

EPA

LCS

LCSD

LFB

MDL

MS

MSD

NA

NC

NDPA/DPA

NI

NP

RL

RPD

SRM

STLP

TIC

Estimated Detection Limit: This value represents the level to which target analyte concentrations are reported as estimated values, when those target analyte concentrations are quantified below the reporting limit (RL). The EDL includes any adjustments from dilutions, concentrations or moisture content, where applicable. The use of EDLs is specific to the analysis of PAHs using Solid-Phase Microextraction (SPME).Environmental Protection Agency.

Laboratory Control Sample: A sample matrix, free from the analytes of interest, spiked with verified known amounts of analytes or a material containing known and verified amounts of analytes.Laboratory Control Sample Duplicate: Refer to LCS.

Laboratory Fortified Blank: A sample matrix, free from the analytes of interest, spiked with verified known amounts of analytes or a material containing known and verified amounts of analytes.Method Detection Limit: This value represents the level to which target analyte concentrations are reported as estimated values, when those target analyte concentrations are quantified below the reporting limit (RL). The MDL includes any adjustments from dilutions, concentrations or moisture content, where applicable.Matrix Spike Sample: A sample prepared by adding a known mass of target analyte to a specified amount of matrix sample forwhich an independent estimate of target analyte concentration is available. Matrix Spike Sample Duplicate: Refer to MS.

Not Applicable.

Not Calculated: Term is utilized when one or more of the results utilized in the calculation are non-detect at the parameter's reporting unit.N-Nitrosodiphenylamine/Diphenylamine.

Not Ignitable.

Non-Plastic: Term is utilized for the analysis of Atterberg Limits in soil.

Reporting Limit: The value at which an instrument can accurately measure an analyte at a specific concentration. The RL includes any adjustments from dilutions, concentrations or moisture content, where applicable.Relative Percent Difference: The results from matrix and/or matrix spike duplicates are primarily designed to assess the precision of analytical results in a given matrix and are expressed as relative percent difference (RPD). Values which are less than five times the reporting limit for any individual parameter are evaluated by utilizing the absolute difference between the values; although the RPD value will be provided in the report.Standard Reference Material: A reference sample of a known or certified value that is of the same or similar matrix as the associated field samples.Semi-dynamic Tank Leaching Procedure per EPA Method 1315.

Tentatively Identified Compound: A compound that has been identified to be present and is not part of the target compound list (TCL) for the method and/or program. All TICs are qualitatively identified and reported as estimated concentrations.

-

-

-

-

-

-

-

-

-

-

-

-

-

-

-

-

-

-

Terms

Analytical Method: Both the document from which the method originates and the analytical reference method. (Example: EPA 8260B is shown as 1,8260B.) The codes for the reference method documents are provided in the References section of the Addendum.Final pH: As it pertains to Sample Receipt & Container Information section of the report, Final pH reflects pH of container determined after adjustment at the laboratory, if applicable. If no adjustment required, value reflects Initial pH.Frozen Date/Time: With respect to Volatile Organics in soil, Frozen Date/Time reflects the date/time at which associated Reagent Water-preserved vials were initially frozen. Note: If frozen date/time is beyond 48 hours from sample collection, value will be reflected in 'bold'.Initial pH: As it pertains to Sample Receipt & Container Information section of the report, Initial pH reflects pH of container determined uponreceipt, if applicable.Total: With respect to Organic analyses, a 'Total' result is defined as the summation of results for individual isomers or Aroclors. If a 'Total' result is requested, the results of its individual components will also be reported. This is applicable to 'Total' results for methods 8260, 8081 and 8082.

Data Qualifiers

A

B

-

-

Spectra identified as "Aldol Condensation Product".

The analyte was detected above the reporting limit in the associated method blank. Flag only applies to associated field samples that have detectable concentrations of the analyte at less than ten times (10x) the concentration found in the blank. For MCP-related

1 The reference for this analyte should be considered modified since this analyte is absent from the target analyte list of the original method.

-

Footnotes

Serial_No:03301815:28

Page 61 of 65


Project Name:

Project Number:

Lab Number:

Report Date:

L1808681NFTA

17005.02 03/30/18

Data Qualifiers

C

D

E

G

H

I

M

NJ

P

Q

R

RE

S

-

-

-

-

-

-

-

-

-

-

-

-

-

projects, flag only applies to associated field samples that have detectable concentrations of the analyte at less than ten times (10x) the concentration found in the blank. For DOD-related projects, flag only applies to associated field samples that have detectable concentrations of the analyte at less than ten times (10x) the concentration found in the blank AND the analyte was detected above one-half the reporting limit (or above the reporting limit for common lab contaminants) in the associated method blank. For NJ-Air-related projects, flag only applies to associated field samples that have detectable concentrations of the analyte above the reporting limit. For NJ-related projects (excluding Air), flag only applies to associated field samples that have detectable concentrations of the analyte, which was detected above the reporting limit in the associated method blank or above five times the reporting limit for common lab contaminants (Phthalates, Acetone, Methylene Chloride, 2-Butanone). Co-elution: The target analyte co-elutes with a known lab standard (i.e. surrogate, internal standards, etc.) for co-extracted analyses.Concentration of analyte was quantified from diluted analysis. Flag only applies to field samples that have detectable concentrations of the analyte.Concentration of analyte exceeds the range of the calibration curve and/or linear range of the instrument.

The concentration may be biased high due to matrix interferences (i.e, co-elution) with non-target compound(s). The result should be considered estimated.The analysis of pH was performed beyond the regulatory-required holding time of 15 minutes from the time of sample collection.

The lower value for the two columns has been reported due to obvious interference.

Reporting Limit (RL) exceeds the MCP CAM Reporting Limit for this analyte.

Presumptive evidence of compound. This represents an estimated concentration for Tentatively Identified Compounds (TICs), where the identification is based on a mass spectral library search.The RPD between the results for the two columns exceeds the method-specified criteria.

The quality control sample exceeds the associated acceptance criteria. For DOD-related projects, LCS and/or Continuing CalibrationStandard exceedences are also qualified on all associated sample results. Note: This flag is not applicable for matrix spike recoverieswhen the sample concentration is greater than 4x the spike added or for batch duplicate RPD when the sample concentrations are lessthan 5x the RL. (Metals only.)Analytical results are from sample re-analysis.

Analytical results are from sample re-extraction.

Analytical results are from modified screening analysis.

J

ND

-

-

Estimated value. The Target analyte concentration is below the quantitation limit (RL), but above the Method Detection Limit (MDL) or Estimated Detection Limit (EDL) for SPME-related analyses. This represents an estimated concentration for Tentatively Identified Compounds (TICs).Not detected at the method detection limit (MDL) for the sample, or estimated detection limit (EDL) for SPME-related analyses.

Serial_No:03301815:28

Page 62 of 65

Alpha Analytical performs services with reasonable care and diligence normal to the analytical testinglaboratory industry. In the event of an error, the sole and exclusive responsibility of Alpha Analyticalshall be to re-perform the work at it's own expense. In no event shall Alpha Analytical be held liablefor any incidental, consequential or special damages, including but not limited to, damages in any wayconnected with the use of, interpretation of, information or analysis provided by Alpha Analytical.

We strongly urge our clients to comply with EPA protocol regarding sample volume, preservation, cooling,containers, sampling procedures, holding time and splitting of samples in the field.

LIMITATION OF LIABILITIES

1

107

121

125

Test Methods for Evaluating Solid Waste: Physical/Chemical Methods. EPA SW-846. Third Edition. Updates I - IV, 2007.

Alpha Analytical - In-house calculation method.

Standard Methods for the Examination of Water and Wastewater. APHA-AWWA-WEF. Standard Methods Online.

Test Methods for Evaluating Solid Waste: Physical/Chemical Methods. EPA SW-846. Third Edition. Updates IIIA, April 1998.

Project Name:

Project Number:

Lab Number:

Report Date:

L1808681NFTA

17005.02

REFERENCES

03/30/18

Serial_No:03301815:28

Page 63 of 65

Alpha Analytical, Inc. ID No.:17873 Facility: Company-wide Revision 11 Department: Quality Assurance Published Date: 1/8/2018 4:15:49 PM Title: Certificate/Approval Program Summary Page 1 of 1

Document Type: Form Pre-Qualtrax Document ID: 08-113

Certification Information

The following analytes are not included in our Primary NELAP Scope of Accreditation:

Westborough Facility EPA 624: m/p-xylene, o-xylene EPA 8260C: NPW: 1,2,4,5-Tetramethylbenzene; 4-Ethyltoluene, Azobenzene; SCM: Iodomethane (methyl iodide), Methyl methacrylate, 1,2,4,5-Tetramethylbenzene; 4-Ethyltoluene. EPA 8270D: NPW: Dimethylnaphthalene,1,4-Diphenylhydrazine; SCM: Dimethylnaphthalene,1,4-Diphenylhydrazine. EPA 300: DW: Bromide EPA 6860: SCM: Perchlorate EPA 9010: NPW and SCM: Amenable Cyanide Distillation SM4500: NPW: Amenable Cyanide, Dissolved Oxygen; SCM: Total Phosphorus, TKN, NO2, NO3. Mansfield Facility SM 2540D: TSS EPA 8082A: NPW: PCB: 1, 5, 31, 87,101, 110, 141, 151, 153, 180, 183, 187. EPA TO-15: Halothane, 2,4,4-Trimethyl-2-pentene, 2,4,4-Trimethyl-1-pentene, Thiophene, 2-Methylthiophene, 3-Methylthiophene, 2-Ethylthiophene, 1,2,3-Trimethylbenzene, Indan, Indene, 1,2,4,5-Tetramethylbenzene, Benzothiophene, 1-Methylnaphthalene. Biological Tissue Matrix: EPA 3050B

The following analytes are included in our Massachusetts DEP Scope of Accreditation

Westborough Facility:

Drinking Water EPA 300.0: Chloride, Nitrate-N, Fluoride, Sulfate; EPA 353.2: Nitrate-N, Nitrite-N; SM4500NO3-F: Nitrate-N, Nitrite-N; SM4500F-C, SM4500CN-CE, EPA 180.1, SM2130B, SM4500Cl-D, SM2320B, SM2540C, SM4500H-B EPA 332: Perchlorate; EPA 524.2: THMs and VOCs; EPA 504.1: EDB, DBCP. Microbiology: SM9215B; SM9223-P/A, SM9223B-Colilert-QT,SM9222D. Non-Potable Water SM4500H,B, EPA 120.1, SM2510B, SM2540C, SM2320B, SM4500CL-E, SM4500F-BC, SM4500NH3-BH: Ammonia-N and Kjeldahl-N, EPA 350.1: Ammonia-N, LACHAT 10-107-06-1-B: Ammonia-N, EPA 351.1, SM4500NO3-F, EPA 353.2: Nitrate-N, EPA 351.1, SM4500P-E, SM4500P-B, E, SM4500SO4-E, SM5220D, EPA 410.4, SM5210B, SM5310C, SM4500CL-D, EPA 1664, EPA 420.1, SM4500-CN-CE, SM2540D. EPA 624: Volatile Halocarbons & Aromatics, EPA 608: Chlordane, Toxaphene, Aldrin, alpha-BHC, beta-BHC, gamma-BHC, delta-BHC, Dieldrin, DDD, DDE, DDT, Endosulfan I, Endosulfan II, Endosulfan sulfate, Endrin, Endrin Aldehyde, Heptachlor, Heptachlor Epoxide, PCBs EPA 625: SVOC (Acid/Base/Neutral Extractables), EPA 600/4-81-045: PCB-Oil. Microbiology: SM9223B-Colilert-QT; Enterolert-QT, SM9221E, SM9222D. Mansfield Facility: Drinking Water EPA 200.7: Al, Ba, Be, Cd, Cr, Cu, Mn, Ni, Na, Ag, Ca, Zn. EPA 200.8: Al, Sb, As, Ba, Be, Cd, Cr, Cu, Pb, Mn, Ni, Se, Ag, TL, Zn. EPA 245.1 Hg. EPA 522. Non-Potable Water EPA 200.7: Al, Sb, As, Be, Cd, Ca, Cr, Co, Cu, Fe, Pb, Mg, Mn, Mo, Ni, K, Se, Ag, Na, Sr, TL, Ti, V, Zn. EPA 200.8: Al, Sb, As, Be, Cd, Cr, Cu, Pb, Mn, Ni, Se, Ag, TL, Zn. EPA 245.1 Hg. SM2340B

For a complete listing of analytes and methods, please contact your Alpha Project Manager.

Serial_No:03301815:28

Page 64 of 65

Serial_No:03301815:28

Page 65 of 65

L1809330


17005.02

NFTA

Client:

Project Name:

Project Number:

04/02/18


Lab Number:

Report Date:


95 Perry Street

Suite 300

Andrew KlimekATTN:

ANALYTICAL REPORT


Buffalo, NY 14203

(716) 206-5100Phone:


Serial_No:04021817:02

Page 1 of 115

L1809330-01

L1809330-02

L1809330-03

L1809330-04

L1809330-05

L1809330-06

L1809330-07

L1809330-08

L1809330-09

Alpha Sample ID

BH2-18

BH4-18

BH2/4-18

BH6-18

BH6-18

BH5/6-18

BH8-18

BH7/8-18

TRIP BLANK

Client ID

AMTRAK

AMTRAK

AMTRAK

AMTRAK

AMTRAK

AMTRAK

AMTRAK

AMTRAK

AMTRAK

Sample Location

NFTA

17005.02



L180933004/02/18

03/16/18 11:08

03/19/18 08:45

03/19/18 12:00

03/19/18 12:20

03/19/18 12:30

03/19/18 15:10

03/19/18 14:20

03/19/18 15:20

03/19/18 00:00


SOIL

SOIL

SOIL

SOIL

SOIL

SOIL

SOIL

SOIL

WATER

03/19/18

03/19/18

03/19/18

03/19/18

03/19/18

03/19/18

03/19/18

03/19/18

03/19/18

Serial_No:04021817:02

Page 2 of 115

NFTA

17005.02

Project Name:

Project Number:

Lab Number:


04/02/18

Case Narrative






















HOLD POLICY






Serial_No:04021817:02

Page 3 of 115


NFTA

17005.02

Project Name:

Project Number:

Lab Number:


04/02/18

Report Submission


MDL column.

Volatile Organics

L1809330-01, -04 and -07: Any reported concentrations that are below 200 ug/kg may be low due to the

sample not being collected according to 5035-L/5035A-L low-level specifications.

L1809330-07: The analysis of Volatile Organics was performed from a methanol extract due to the elevated

concentrations of non-target compounds in the sample.

TCLP Volatiles

The ambient temperature of the area in which the TCLP extraction of the samples and associated Method

Blank performed was outside the required 21-25 degrees C temperature range.

Pesticides

L1809330-08: The sample has elevated detection limits due to the dilution required by the sample matrix.

Cyanide, Total

The WG1099068-2/-3 LCS/LCSD recoveries (63%/55%), associated with L1809330-03 and -06, are outside

our in-house acceptance criteria, but within the vendor-certified acceptance limits. The results of the original

analyses are reported.

The WG1099600-2/-3 LCS/LCSD recoveies (70%/77%), associated with L1809330-08, are outside our in-

house acceptance criteria, but within the vendor-certified acceptance limits. The results of the original analyses

are reported.




Serial_No:04021817:02

Page 4 of 115

ORGANICS

Serial_No:04021817:02

Page 5 of 115

VOLATILES

Serial_No:04021817:02

Page 6 of 115

FF

Methylene chloride

1,1-Dichloroethane

Chloroform


Tetrachloroethene

Chlorobenzene

1,2-Dichloroethane


Benzene

Toluene

Ethylbenzene

Vinyl chloride

1,1-Dichloroethene


Trichloroethene

1,2-Dichlorobenzene

1,3-Dichlorobenzene

1,4-Dichlorobenzene


p/m-Xylene

o-Xylene


Acetone

2-Butanone

n-Butylbenzene

sec-Butylbenzene

tert-Butylbenzene

n-Propylbenzene


ND

ND

ND

ND

ND

ND

ND

ND

ND

ND

ND

ND

ND

ND

ND

ND

ND

ND

ND

ND

ND

ND

56

11

ND

ND

ND

ND

ug/kg

ug/kg

ug/kg

ug/kg

ug/kg

ug/kg

ug/kg

ug/kg

ug/kg

ug/kg

ug/kg

ug/kg

ug/kg

ug/kg

ug/kg

ug/kg

ug/kg

ug/kg

ug/kg

ug/kg

ug/kg

ug/kg

ug/kg

ug/kg

ug/kg

ug/kg

ug/kg

ug/kg

1

1

1

1

1

1

1

1

1

1

1

1

1

1

1

1

1

1

1

1

1

1

1

1

1

1

1

1

Qualifier Units RL


SAMPLE RESULTS

Project Name:

Project Number:

Lab Number:

Report Date:

NFTA

17005.02

L1809330

9.2

1.4

1.4

0.92

0.92

0.92

0.92

0.92

0.92

1.4

0.92

1.8

0.92

1.4

0.92

4.6

4.6

4.6

1.8

1.8

1.8

0.92

9.2

9.2

0.92

0.92

4.6

0.92

04/02/18



L1809330-01Lab ID:



1,8260C03/28/18 15:04KD 79%Percent Solids:

MDL

1.5

0.25

0.34

0.32

0.28

0.32

0.22

0.32

0.18

0.18

0.16

0.29

0.34

0.22

0.28

0.17

0.20

0.17

0.14

0.32

0.31

0.31

2.1

0.63

0.21

0.20

0.23

0.20

Sample Depth:

Serial_No:04021817:02

Page 7 of 115



1,4-Dioxane


ND

ND

ND

ug/kg

ug/kg

ug/kg

1

1

1

Qualifier Units RL


SAMPLE RESULTS

Project Name:

Project Number:

Lab Number:

Report Date:

NFTA

17005.02

L1809330

4.6

4.6

37


Toluene-d8



106

108

109

97

70-130

70-130

70-130

70-130


04/02/18



L1809330-01Lab ID:


MDL

0.15

0.17

13.

Sample Depth:

Serial_No:04021817:02

Page 8 of 115

Chloroform


Tetrachloroethene

Chlorobenzene

1,2-Dichloroethane

Benzene

Vinyl chloride

1,1-Dichloroethene

Trichloroethene

1,4-Dichlorobenzene

2-Butanone


ND

ND

ND

ND

ND

ND

ND

ND

ND

ND

ND

ug/l

ug/l

ug/l

ug/l

ug/l

ug/l

ug/l

ug/l

ug/l

ug/l

ug/l

10

10

10

10

10

10

10

10

10

10

10

Qualifier Units RL


SAMPLE RESULTS

Project Name:

Project Number:

Lab Number:

Report Date:

NFTA

17005.02

L1809330

7.5

5.0

5.0

5.0

5.0

5.0

10

5.0

5.0

25

50


Toluene-d8



108

99

104

100

70-130

70-130

70-130

70-130


04/02/18



L1809330-02Lab ID:



1,8260C03/26/18 10:23MM


MDL

2.2

1.3

1.8

1.8

1.3

1.6

0.71

1.7

1.8

1.9

19.

Sample Depth:

Serial_No:04021817:02

Page 9 of 115

Chloroform


Tetrachloroethene

Chlorobenzene

1,2-Dichloroethane

Benzene

Vinyl chloride

1,1-Dichloroethene

Trichloroethene

1,4-Dichlorobenzene

2-Butanone


ND

ND

ND

ND

ND

ND

ND

ND

ND

ND

ND

ug/l

ug/l

ug/l

ug/l

ug/l

ug/l

ug/l

ug/l

ug/l

ug/l

ug/l

10

10

10

10

10

10

10

10

10

10

10

Qualifier Units RL


SAMPLE RESULTS

Project Name:

Project Number:

Lab Number:

Report Date:

NFTA

17005.02

L1809330

7.5

5.0

5.0

5.0

5.0

5.0

10

5.0

5.0

25

50


Toluene-d8



107

99

105

100

70-130

70-130

70-130

70-130


04/02/18



L1809330-03Lab ID:



1,8260C03/26/18 10:48MM


83%Percent Solids:

MDL

2.2

1.3

1.8

1.8

1.3

1.6

0.71

1.7

1.8

1.9

19.

Sample Depth:

Serial_No:04021817:02

Page 10 of 115

Methylene chloride

1,1-Dichloroethane

Chloroform


Tetrachloroethene

Chlorobenzene

1,2-Dichloroethane


Benzene

Toluene

Ethylbenzene

Vinyl chloride

1,1-Dichloroethene


Trichloroethene

1,2-Dichlorobenzene

1,3-Dichlorobenzene

1,4-Dichlorobenzene


p/m-Xylene

o-Xylene


Acetone

2-Butanone

n-Butylbenzene

sec-Butylbenzene

tert-Butylbenzene

n-Propylbenzene

Parameter Result

J

J

J

J

J

J

Dilution Factor

ND

ND

ND

ND

ND

ND

ND

ND

ND

ND

0.32

ND

ND

ND

ND

ND

ND

ND

ND

1.4

1.4

ND

26

3.2

1.0

1.8

ND

0.83

ug/kg

ug/kg

ug/kg

ug/kg

ug/kg

ug/kg

ug/kg

ug/kg

ug/kg

ug/kg

ug/kg

ug/kg

ug/kg

ug/kg

ug/kg

ug/kg

ug/kg

ug/kg

ug/kg

ug/kg

ug/kg

ug/kg

ug/kg

ug/kg

ug/kg

ug/kg

ug/kg

ug/kg

1

1

1

1

1

1

1

1

1

1

1

1

1

1

1

1

1

1

1

1

1

1

1

1

1

1

1

1

Qualifier Units RL


SAMPLE RESULTS

Project Name:

Project Number:

Lab Number:

Report Date:

NFTA

17005.02

L1809330

11

1.6

1.6

1.1

1.1

1.1

1.1

1.1

1.1

1.6

1.1

2.1

1.1

1.6

1.1

5.4

5.4

5.4

2.1

2.1

2.1

1.1

11

11

1.1

1.1

5.4

1.1

04/02/18



L1809330-04Lab ID:




MDL

1.8

0.29

0.40

0.37

0.32

0.37

0.26

0.38

0.21

0.21

0.18

0.34

0.40

0.26

0.32

0.20

0.23

0.20

0.16

0.38

0.36

0.37

2.4

0.74

0.24

0.23

0.26

0.23

Sample Depth:

Serial_No:04021817:02

Page 11 of 115



1,4-Dioxane

Parameter Result

J

Dilution Factor

4.4

11

ND

ug/kg

ug/kg

ug/kg

1

1

1

Qualifier Units RL


SAMPLE RESULTS

Project Name:

Project Number:

Lab Number:

Report Date:

NFTA

17005.02

L1809330

5.4

5.4

43


Toluene-d8



106

106

109

96

70-130

70-130

70-130

70-130


04/02/18



L1809330-04Lab ID:


MDL

0.17

0.20

15.

Sample Depth:

Serial_No:04021817:02

Page 12 of 115

Chloroform


Tetrachloroethene

Chlorobenzene

1,2-Dichloroethane

Benzene

Vinyl chloride

1,1-Dichloroethene

Trichloroethene

1,4-Dichlorobenzene

2-Butanone


ND

ND

ND

ND

ND

ND

ND

ND

ND

ND

ND

ug/l

ug/l

ug/l

ug/l

ug/l

ug/l

ug/l

ug/l

ug/l

ug/l

ug/l

10

10

10

10

10

10

10

10

10

10

10

Qualifier Units RL


SAMPLE RESULTS

Project Name:

Project Number:

Lab Number:

Report Date:

NFTA

17005.02

L1809330

7.5

5.0

5.0

5.0

5.0

5.0

10

5.0

5.0

25

50


Toluene-d8



109

102

103

101

70-130

70-130

70-130

70-130


04/02/18



L1809330-05Lab ID:



1,8260C03/26/18 11:13AD


MDL

2.2

1.3

1.8

1.8

1.3

1.6

0.71

1.7

1.8

1.9

19.

Sample Depth:

Serial_No:04021817:02

Page 13 of 115

Chloroform


Tetrachloroethene

Chlorobenzene

1,2-Dichloroethane

Benzene

Vinyl chloride

1,1-Dichloroethene

Trichloroethene

1,4-Dichlorobenzene

2-Butanone


ND

ND

ND

ND

ND

ND

ND

ND

ND

ND

ND

ug/l

ug/l

ug/l

ug/l

ug/l

ug/l

ug/l

ug/l

ug/l

ug/l

ug/l

10

10

10

10

10

10

10

10

10

10

10

Qualifier Units RL


SAMPLE RESULTS

Project Name:

Project Number:

Lab Number:

Report Date:

NFTA

17005.02

L1809330

7.5

5.0

5.0

5.0

5.0

5.0

10

5.0

5.0

25

50


Toluene-d8



107

100

103

101

70-130

70-130

70-130

70-130


04/02/18



L1809330-06Lab ID:



1,8260C03/26/18 11:38AD


80%Percent Solids:

MDL

2.2

1.3

1.8

1.8

1.3

1.6

0.71

1.7

1.8

1.9

19.

Sample Depth:

Serial_No:04021817:02

Page 14 of 115

Chloroform


Tetrachloroethene

Chlorobenzene

1,2-Dichloroethane

Benzene

Vinyl chloride

1,1-Dichloroethene

Trichloroethene

1,4-Dichlorobenzene

2-Butanone


ND

ND

ND

ND

ND

ND

ND

ND

ND

ND

ND

ug/l

ug/l

ug/l

ug/l

ug/l

ug/l

ug/l

ug/l

ug/l

ug/l

ug/l

10

10

10

10

10

10

10

10

10

10

10

Qualifier Units RL


SAMPLE RESULTS

Project Name:

Project Number:

Lab Number:

Report Date:

NFTA

17005.02

L1809330

7.5

5.0

5.0

5.0

5.0

5.0

10

5.0

5.0

25

50


Toluene-d8



111

100

102

102

70-130

70-130

70-130

70-130


04/02/18



L1809330-07Lab ID:



1,8260C03/26/18 12:03AD


98%Percent Solids:

MDL

2.2

1.3

1.8

1.8

1.3

1.6

0.71

1.7

1.8

1.9

19.

Sample Depth:

Serial_No:04021817:02

Page 15 of 115

Methylene chloride

1,1-Dichloroethane

Chloroform


Tetrachloroethene

Chlorobenzene

1,2-Dichloroethane


Benzene

Toluene

Ethylbenzene

Vinyl chloride

1,1-Dichloroethene


Trichloroethene

1,2-Dichlorobenzene

1,3-Dichlorobenzene

1,4-Dichlorobenzene


p/m-Xylene

o-Xylene


Acetone

2-Butanone

n-Butylbenzene

sec-Butylbenzene

tert-Butylbenzene

n-Propylbenzene

Parameter Result

J

J

J

J

J

J

J

Dilution Factor

200

ND

ND

ND

ND

ND

ND

ND

16

74

24

ND

ND

ND

ND

ND

ND

ND

ND

140

46

ND

ND

ND

14

ND

ND

20

ug/kg

ug/kg

ug/kg

ug/kg

ug/kg

ug/kg

ug/kg

ug/kg

ug/kg

ug/kg

ug/kg

ug/kg

ug/kg

ug/kg

ug/kg

ug/kg

ug/kg

ug/kg

ug/kg

ug/kg

ug/kg

ug/kg

ug/kg

ug/kg

ug/kg

ug/kg

ug/kg

ug/kg

1

1

1

1

1

1

1

1

1

1

1

1

1

1

1

1

1

1

1

1

1

1

1

1

1

1

1

1

Qualifier Units RL


SAMPLE RESULTS

Project Name:

Project Number:

Lab Number:

Report Date:

NFTA

17005.02

L1809330

520

78

78

52

52

52

52

52

52

78

52

100

52

78

52

260

260

260

100

100

100

52

520

520

52

52

260

52

04/02/18



L1809330-07Lab ID:




MDL

86.

14.

19.

18.

16.

18.

13.

18.

10.

10.

8.9

16.

19.

12.

16.

9.5

11.

9.5

8.0

18.

18.

18.

120

36.

12.

11.

13.

11.

Sample Depth:

Serial_No:04021817:02

Page 16 of 115



1,4-Dioxane

Parameter Result

J

J

Dilution Factor

51

120

ND

ug/kg

ug/kg

ug/kg

1

1

1

Qualifier Units RL


SAMPLE RESULTS

Project Name:

Project Number:

Lab Number:

Report Date:

NFTA

17005.02

L1809330

260

260

2100


Toluene-d8



105

107

104

94

70-130

70-130

70-130

70-130


04/02/18



L1809330-07Lab ID:


MDL

8.4

9.7

750

Sample Depth:

Serial_No:04021817:02

Page 17 of 115

Chloroform


Tetrachloroethene

Chlorobenzene

1,2-Dichloroethane

Benzene

Vinyl chloride

1,1-Dichloroethene

Trichloroethene

1,4-Dichlorobenzene

2-Butanone


ND

ND

ND

ND

ND

ND

ND

ND

ND

ND

ND

ug/l

ug/l

ug/l

ug/l

ug/l

ug/l

ug/l

ug/l

ug/l

ug/l

ug/l

10

10

10

10

10

10

10

10

10

10

10

Qualifier Units RL


SAMPLE RESULTS

Project Name:

Project Number:

Lab Number:

Report Date:

NFTA

17005.02

L1809330

7.5

5.0

5.0

5.0

5.0

5.0

10

5.0

5.0

25

50


Toluene-d8



110

100

104

100

70-130

70-130

70-130

70-130


04/02/18



L1809330-08Lab ID:



1,8260C03/26/18 12:28AD


85%Percent Solids:

MDL

2.2

1.3

1.8

1.8

1.3

1.6

0.71

1.7

1.8

1.9

19.

Sample Depth:

Serial_No:04021817:02

Page 18 of 115

Methylene chloride

1,1-Dichloroethane

Chloroform


Tetrachloroethene

Chlorobenzene

1,2-Dichloroethane


Benzene

Toluene

Ethylbenzene

Vinyl chloride

1,1-Dichloroethene


Trichloroethene

1,2-Dichlorobenzene

1,3-Dichlorobenzene

1,4-Dichlorobenzene


p/m-Xylene

o-Xylene


Acetone

2-Butanone

n-Butylbenzene

sec-Butylbenzene

tert-Butylbenzene

n-Propylbenzene

Parameter Result

J

Dilution Factor

ND

ND

ND

ND

ND

ND

ND

ND

ND

ND

ND

ND

ND

ND

ND

ND

ND

ND

ND

ND

ND

ND

1.7

ND

ND

ND

ND

ND

ug/l

ug/l

ug/l

ug/l

ug/l

ug/l

ug/l

ug/l

ug/l

ug/l

ug/l

ug/l

ug/l

ug/l

ug/l

ug/l

ug/l

ug/l

ug/l

ug/l

ug/l

ug/l

ug/l

ug/l

ug/l

ug/l

ug/l

ug/l

1

1

1

1

1

1

1

1

1

1

1

1

1

1

1

1

1

1

1

1

1

1

1

1

1

1

1

1

Qualifier Units RL


SAMPLE RESULTS

Project Name:

Project Number:

Lab Number:

Report Date:

NFTA

17005.02

L1809330

2.5

2.5

2.5

0.50

0.50

2.5

0.50

2.5

0.50

2.5

2.5

1.0

0.50

2.5

0.50

2.5

2.5

2.5

2.5

2.5

2.5

2.5

5.0

5.0

2.5

2.5

2.5

2.5

04/02/18

TRIP BLANKClient ID:03/19/18 00:00Date Collected:03/19/18Date Received:


L1809330-09Lab ID:


Matrix: WaterAnalytical Method:Analytical Date:Analyst:

1,8260C03/28/18 14:27NLK

MDL

0.70

0.70

0.70

0.13

0.18

0.70

0.13

0.70

0.16

0.70

0.70

0.07

0.17

0.70

0.18

0.70

0.70

0.70

0.70

0.70

0.70

0.70

1.5

1.9

0.70

0.70

0.70

0.70

Sample Depth:

Serial_No:04021817:02

Page 19 of 115



1,4-Dioxane


ND

ND

ND

ug/l

ug/l

ug/l

1

1

1

Qualifier Units RL


SAMPLE RESULTS

Project Name:

Project Number:

Lab Number:

Report Date:

NFTA

17005.02

L1809330

2.5

2.5

250


Toluene-d8



94

106

116

90

70-130

70-130

70-130

70-130


04/02/18



L1809330-09Lab ID:


MDL

0.70

0.70

61.

Sample Depth:

Serial_No:04021817:02

Page 20 of 115


Project Name:

Project Number:

Lab Number:

Report Date:

NFTA

17005.02

L1809330



04/02/18

Analyst: MM

Chloroform


Tetrachloroethene

Chlorobenzene

1,2-Dichloroethane

Benzene

Vinyl chloride

1,1-Dichloroethene

Trichloroethene

1,4-Dichlorobenzene

2-Butanone

Parameter Result

ND

ND

ND

ND

ND

ND

ND

ND

ND

ND

ND

RL

7.5

5.0

5.0

5.0

5.0

5.0

10

5.0

5.0

25

50

ug/l

ug/l

ug/l

ug/l

ug/l

ug/l

ug/l

ug/l

ug/l

ug/l

ug/l

UnitsQualifier

TCLP Volatiles by EPA 1311 - Westborough Lab for sample(s): 02-03,05-08 Batch: WG1100473-5


Toluene-d8



100

99

105

93

70-130

70-130

70-130

70-130


Criteria


MDL

2.2

1.3

1.8

1.8

1.3

1.6

0.71

1.7

1.8

1.9

19.

Serial_No:04021817:02

Page 21 of 115


Project Name:

Project Number:

Lab Number:

Report Date:

NFTA

17005.02

L1809330


Analytical Date:

04/02/18

Analyst: NLK

Methylene chloride

1,1-Dichloroethane

Chloroform


Tetrachloroethene

Chlorobenzene

1,2-Dichloroethane


Benzene

Toluene

Ethylbenzene

Vinyl chloride

1,1-Dichloroethene


Trichloroethene

1,2-Dichlorobenzene

1,3-Dichlorobenzene

1,4-Dichlorobenzene


p/m-Xylene

o-Xylene


Acetone

2-Butanone

n-Butylbenzene

sec-Butylbenzene

tert-Butylbenzene

n-Propylbenzene


Parameter Result

ND

ND

ND

ND

ND

ND

ND

ND

ND

ND

ND

ND

ND

ND

ND

ND

ND

ND

ND

ND

ND

ND

ND

ND

ND

ND

ND

ND

ND

RL

10

1.5

1.5

1.0

1.0

1.0

1.0

1.0

1.0

1.5

1.0

2.0

1.0

1.5

1.0

5.0

5.0

5.0

2.0

2.0

2.0

1.0

10

10

1.0

1.0

5.0

1.0

5.0

ug/kg

ug/kg

ug/kg

ug/kg

ug/kg

ug/kg

ug/kg

ug/kg

ug/kg

ug/kg

ug/kg

ug/kg

ug/kg

ug/kg

ug/kg

ug/kg

ug/kg

ug/kg

ug/kg

ug/kg

ug/kg

ug/kg

ug/kg

ug/kg

ug/kg

ug/kg

ug/kg

ug/kg

ug/kg

UnitsQualifier

Volatile Organics by GC/MS - Westborough Lab for sample(s): 01,04 Batch: WG1101339-5

MDL

1.6

0.27

0.37

0.34

0.30

0.35

0.25

0.35

0.19

0.20

0.17

0.32

0.37

0.24

0.30

0.18

0.22

0.18

0.15

0.35

0.34

0.34

2.3

0.69

0.23

0.22

0.25

0.22

0.16

Serial_No:04021817:02

Page 22 of 115


Project Name:

Project Number:

Lab Number:

Report Date:

NFTA

17005.02

L1809330


Analytical Date:

04/02/18

Analyst: NLK


1,4-Dioxane

Parameter Result

ND

ND

RL

5.0

40

ug/kg

ug/kg

UnitsQualifier



Toluene-d8



106

106

104

94

70-130

70-130

70-130

70-130


Criteria

MDL

0.19

14.

Serial_No:04021817:02

Page 23 of 115


Project Name:

Project Number:

Lab Number:

Report Date:

NFTA

17005.02

L1809330


Analytical Date:

04/02/18

Analyst: PD

Methylene chloride

1,1-Dichloroethane

Chloroform


Tetrachloroethene

Chlorobenzene

1,2-Dichloroethane


Benzene

Toluene

Ethylbenzene

Vinyl chloride

1,1-Dichloroethene


Trichloroethene

1,2-Dichlorobenzene

1,3-Dichlorobenzene

1,4-Dichlorobenzene


p/m-Xylene

o-Xylene


Acetone

2-Butanone

n-Butylbenzene

sec-Butylbenzene

tert-Butylbenzene

n-Propylbenzene


Parameter Result

ND

ND

ND

ND

ND

ND

ND

ND

ND

ND

ND

ND

ND

ND

ND

ND

ND

ND

ND

ND

ND

ND

ND

ND

ND

ND

ND

ND

ND

RL

2.5

2.5

2.5

0.50

0.50

2.5

0.50

2.5

0.50

2.5

2.5

1.0

0.50

2.5

0.50

2.5

2.5

2.5

2.5

2.5

2.5

2.5

5.0

5.0

2.5

2.5

2.5

2.5

2.5

ug/l

ug/l

ug/l

ug/l

ug/l

ug/l

ug/l

ug/l

ug/l

ug/l

ug/l

ug/l

ug/l

ug/l

ug/l

ug/l

ug/l

ug/l

ug/l

ug/l

ug/l

ug/l

ug/l

ug/l

ug/l

ug/l

ug/l

ug/l

ug/l

UnitsQualifier


MDL

0.70

0.70

0.70

0.13

0.18

0.70

0.13

0.70

0.16

0.70

0.70

0.07

0.17

0.70

0.18

0.70

0.70

0.70

0.70

0.70

0.70

0.70

1.5

1.9

0.70

0.70

0.70

0.70

0.70

Serial_No:04021817:02

Page 24 of 115


Project Name:

Project Number:

Lab Number:

Report Date:

NFTA

17005.02

L1809330


Analytical Date:

04/02/18

Analyst: PD


1,4-Dioxane

Parameter Result

ND

ND

RL

2.5

250

ug/l

ug/l

UnitsQualifier



Toluene-d8



96

106

116

89

70-130

70-130

70-130

70-130


Criteria

No Tentatively Identified Compounds ND ug/l


MDL

0.70

61.

Serial_No:04021817:02

Page 25 of 115


Project Name:

Project Number:

Lab Number:

Report Date:

NFTA

17005.02

L1809330


Analytical Date:

04/02/18

Analyst: NLK

Methylene chloride

1,1-Dichloroethane

Chloroform


Tetrachloroethene

Chlorobenzene

1,2-Dichloroethane


Benzene

Toluene

Ethylbenzene

Vinyl chloride

1,1-Dichloroethene


Trichloroethene

1,2-Dichlorobenzene

1,3-Dichlorobenzene

1,4-Dichlorobenzene


p/m-Xylene

o-Xylene


Acetone

2-Butanone

n-Butylbenzene

sec-Butylbenzene

tert-Butylbenzene

n-Propylbenzene


Parameter Result

ND

ND

ND

ND

ND

ND

ND

ND

ND

ND

ND

ND

ND

ND

ND

ND

ND

ND

ND

ND

ND

ND

ND

ND

ND

ND

ND

ND

ND

RL

500

75

75

50

50

50

50

50

50

75

50

100

50

75

50

250

250

250

100

100

100

50

500

500

50

50

250

50

250

ug/kg

ug/kg

ug/kg

ug/kg

ug/kg

ug/kg

ug/kg

ug/kg

ug/kg

ug/kg

ug/kg

ug/kg

ug/kg

ug/kg

ug/kg

ug/kg

ug/kg

ug/kg

ug/kg

ug/kg

ug/kg

ug/kg

ug/kg

ug/kg

ug/kg

ug/kg

ug/kg

ug/kg

ug/kg

UnitsQualifier


MDL

82.

14.

18.

17.

15.

17.

12.

18.

9.6

9.8

8.5

16.

19.

12.

15.

9.1

11.

9.1

7.6

18.

17.

17.

110

34.

11.

11.

12.

11.

8.0

Serial_No:04021817:02

Page 26 of 115


Project Name:

Project Number:

Lab Number:

Report Date:

NFTA

17005.02

L1809330


Analytical Date:

04/02/18

Analyst: NLK


1,4-Dioxane

Parameter Result

ND

ND

RL

250

2000

ug/kg

ug/kg

UnitsQualifier



Toluene-d8



106

106

104

94

70-130

70-130

70-130

70-130


Criteria

MDL

9.3

720

Serial_No:04021817:02

Page 27 of 115

Chloroform


Tetrachloroethene

Chlorobenzene

1,2-Dichloroethane

Benzene

Vinyl chloride

1,1-Dichloroethene

Trichloroethene

1,4-Dichlorobenzene

2-Butanone

98

100

100

98

95

97

81

96

100

100

100

100

100

99

99

99

99

80

100

99

100

100

70-130

63-132

70-130

75-130

70-130

70-130

55-140

61-145

70-130

70-130

63-138

2

0

1

1

4

2

1

4

1

0

0

20

20

20

25

20

25

20

25

25

20

20

ParameterLCS

%RecoveryLCSD

%Recovery%Recovery

Limits RPDRPD

Limits

TCLP Volatiles by EPA 1311 - Westborough Lab Associated sample(s): 02-03,05-08 Batch: WG1100473-3 WG1100473-4


Project Name:

Project Number:

Lab Number:

Report Date:

NFTA

17005.02

L1809330


969910093

70-13070-13070-13070-130

9710010093


04/02/18

AcceptanceCriteria

Qual Qual Qual

Serial_No:04021817:02

Page 28 of 115

Methylene chloride

1,1-Dichloroethane

Chloroform


Tetrachloroethene

Chlorobenzene

1,2-Dichloroethane


Benzene

Toluene

Ethylbenzene

Vinyl chloride

1,1-Dichloroethene


Trichloroethene

1,2-Dichlorobenzene

1,3-Dichlorobenzene

1,4-Dichlorobenzene


p/m-Xylene

o-Xylene


Acetone

108

95

94

93

91

97

97

92

92

92

96

91

86

90

91

100

99

98

91

96

97

92

120

104

92

91

92

88

95

96

88

88

89

93

88

83

86

87

98

96

95

90

93

93

90

106

70-130

70-130

70-130

70-130

70-130

70-130

70-130

70-130

70-130

70-130

70-130

67-130

65-135

70-130

70-130

70-130

70-130

70-130

66-130

70-130

70-130

70-130

54-140

4

3

3

1

3

2

1

4

4

3

3

3

4

5

4

2

3

3

1

3

4

2

12

30

30

30

30

30

30

30

30

30

30

30

30

30

30

30

30

30

30

30

30

30

30

30

ParameterLCS

%RecoveryLCSD

%Recovery%Recovery

Limits RPDRPD

Limits

Volatile Organics by GC/MS - Westborough Lab Associated sample(s): 01,04 Batch: WG1101339-3 WG1101339-4


Project Name:

Project Number:

Lab Number:

Report Date:

NFTA

17005.02

L1809330

04/02/18

Qual Qual Qual

Serial_No:04021817:02

Page 29 of 115

2-Butanone

n-Butylbenzene

sec-Butylbenzene

tert-Butylbenzene

n-Propylbenzene



1,4-Dioxane

100

102

99

97

101

100

99

94

103

98

94

93

96

96

95

102

70-130

70-130

70-130

70-130

70-130

70-130

70-130

65-136

3

4

5

4

5

4

4

8

30

30

30

30

30

30

30

30

ParameterLCS

%RecoveryLCSD

%Recovery%Recovery

Limits RPDRPD

Limits



Project Name:

Project Number:

Lab Number:

Report Date:

NFTA

17005.02

L1809330


10710710296

70-13070-13070-13070-130

10910710398


04/02/18

AcceptanceCriteria

Qual Qual Qual

Serial_No:04021817:02

Page 30 of 115

Methylene chloride

1,1-Dichloroethane

Chloroform


Tetrachloroethene

Chlorobenzene

1,2-Dichloroethane


Benzene

Toluene

Ethylbenzene

Vinyl chloride

1,1-Dichloroethene


Trichloroethene

1,2-Dichlorobenzene

1,3-Dichlorobenzene

1,4-Dichlorobenzene


p/m-Xylene

o-Xylene


Acetone

81

89

84

99

90

87

82

96

87

90

95

98

91

89

83

83

87

85

85

90

90

83

100

82

90

84

99

88

85

82

94

87

90

94

97

93

88

84

82

87

86

87

90

90

82

110

70-130

70-130

70-130

63-132

70-130

75-130

70-130

67-130

70-130

70-130

70-130

55-140

61-145

70-130

70-130

70-130

70-130

70-130

63-130

70-130

70-130

70-130

58-148

1

1

0

0

2

2

0

2

0

0

1

1

2

1

1

1

0

1

2

0

0

1

10

20

20

20

20

20

20

20

20

20

20

20

20

20

20

20

20

20

20

20

20

20

20

20

ParameterLCS

%RecoveryLCSD

%Recovery%Recovery

Limits RPDRPD

Limits



Project Name:

Project Number:

Lab Number:

Report Date:

NFTA

17005.02

L1809330

04/02/18

Qual Qual Qual

Serial_No:04021817:02

Page 31 of 115

2-Butanone

n-Butylbenzene

sec-Butylbenzene

tert-Butylbenzene

n-Propylbenzene



1,4-Dioxane

91

120

110

88

100

98

100

110

86

120

110

89

100

98

99

140

63-138

53-136

70-130

70-130

69-130

64-130

70-130

56-162

6

0

0

1

0

0

1

24

20

20

20

20

20

20

20

20

ParameterLCS

%RecoveryLCSD

%Recovery%Recovery

Limits RPDRPD

Limits



Project Name:

Project Number:

Lab Number:

Report Date:

NFTA

17005.02

L1809330


9810611091

70-13070-13070-13070-130

9810611191


04/02/18

AcceptanceCriteria

Qual Qual Qual

Q

Serial_No:04021817:02

Page 32 of 115

Methylene chloride

1,1-Dichloroethane

Chloroform


Tetrachloroethene

Chlorobenzene

1,2-Dichloroethane


Benzene

Toluene

Ethylbenzene

Vinyl chloride

1,1-Dichloroethene


Trichloroethene

1,2-Dichlorobenzene

1,3-Dichlorobenzene

1,4-Dichlorobenzene


p/m-Xylene

o-Xylene


Acetone

108

95

94

93

91

97

97

92

92

92

96

91

86

90

91

100

99

98

91

96

97

92

120

104

92

91

92

88

95

96

88

88

89

93

88

83

86

87

98

96

95

90

93

93

90

106

70-130

70-130

70-130

70-130

70-130

70-130

70-130

70-130

70-130

70-130

70-130

67-130

65-135

70-130

70-130

70-130

70-130

70-130

66-130

70-130

70-130

70-130

54-140

4

3

3

1

3

2

1

4

4

3

3

3

4

5

4

2

3

3

1

3

4

2

12

30

30

30

30

30

30

30

30

30

30

30

30

30

30

30

30

30

30

30

30

30

30

30

ParameterLCS

%RecoveryLCSD

%Recovery%Recovery

Limits RPDRPD

Limits



Project Name:

Project Number:

Lab Number:

Report Date:

NFTA

17005.02

L1809330

04/02/18

Qual Qual Qual

Serial_No:04021817:02

Page 33 of 115

2-Butanone

n-Butylbenzene

sec-Butylbenzene

tert-Butylbenzene

n-Propylbenzene



1,4-Dioxane

100

102

99

97

101

100

99

94

103

98

94

93

96

96

95

102

70-130

70-130

70-130

70-130

70-130

70-130

70-130

65-136

3

4

5

4

5

4

4

8

30

30

30

30

30

30

30

30

ParameterLCS

%RecoveryLCSD

%Recovery%Recovery

Limits RPDRPD

Limits



Project Name:

Project Number:

Lab Number:

Report Date:

NFTA

17005.02

L1809330


10710710296

70-13070-13070-13070-130

10910710398


04/02/18

AcceptanceCriteria

Qual Qual Qual

Serial_No:04021817:02

Page 34 of 115

SEMIVOLATILES

Serial_No:04021817:02

Page 35 of 115

FF

Hexachlorobenzene

2,4-Dinitrotoluene

Hexachlorobutadiene

Hexachloroethane

Nitrobenzene


Pentachlorophenol

2-Methylphenol



Pyridine


ND

ND

ND

ND

ND

ND

ND

ND

ND

ND

ND

ug/l

ug/l

ug/l

ug/l

ug/l

ug/l

ug/l

ug/l

ug/l

ug/l

ug/l

1

1

1

1

1

1

1

1

1

1

1

Qualifier Units RL


SAMPLE RESULTS

Project Name:

Project Number:

Lab Number:

Report Date:

NFTA

17005.02

L1809330

10

25

10

10

10

25

50

25

25

25

18

2-Fluorophenol

Phenol-d6

Nitrobenzene-d5

2-Fluorobiphenyl


4-Terphenyl-d14

69

72

81

82

72

91

21-120

10-120

23-120

15-120

10-120

33-120


04/02/18



L1809330-03Lab ID:




1,8270D03/26/18 18:44HL



83%Percent Solids:

MDL

2.9

4.2

3.6

3.4

3.8

3.4

17.

5.1

5.6

3.6

9.4

Sample Depth:

Serial_No:04021817:02

Page 36 of 115

Acenaphthene

Hexachlorobenzene

Fluoranthene

Naphthalene

Benzo(a)anthracene

Benzo(a)pyrene



Chrysene

Acenaphthylene

Anthracene

Benzo(ghi)perylene

Fluorene

Phenanthrene



Pyrene

Dibenzofuran

Pentachlorophenol

Phenol

2-Methylphenol


Parameter Result

J

J

J

J

J

Dilution Factor

ND

ND

38

ND

26

ND

ND

ND

ND

ND

ND

ND

ND

30

ND

68

33

ND

ND

ND

ND

ND

ug/kg

ug/kg

ug/kg

ug/kg

ug/kg

ug/kg

ug/kg

ug/kg

ug/kg

ug/kg

ug/kg

ug/kg

ug/kg

ug/kg

ug/kg

ug/kg

ug/kg

ug/kg

ug/kg

ug/kg

ug/kg

ug/kg

1

1

1

1

1

1

1

1

1

1

1

1

1

1

1

1

1

1

1

1

1

1

Qualifier Units RL


SAMPLE RESULTS

Project Name:

Project Number:

Lab Number:

Report Date:

NFTA

17005.02

L1809330

160

120

120

200

120

160

120

120

120

160

120

160

200

120

120

160

120

200

160

200

200

290

04/02/18



L1809330-03Lab ID:




1,8270D03/29/18 00:41CB


83%Percent Solids:

MDL

21.

22.

23.

24.

22.

49.

34.

32.

21.

31.

39.

24.

19.

24.

23.

28.

20.

19.

44.

30.

31.

31.

Sample Depth:

Serial_No:04021817:02

Page 37 of 115



SAMPLE RESULTS

Project Name:

Project Number:

Lab Number:

Report Date:

NFTA

17005.02

L1809330

2-Fluorophenol

Phenol-d6

Nitrobenzene-d5

2-Fluorobiphenyl


4-Terphenyl-d14

58

71

64

68

64

72

25-120

10-120

23-120

30-120

10-136

18-120


04/02/18



L1809330-03Lab ID:


MDL

Sample Depth:

Serial_No:04021817:02

Page 38 of 115

Hexachlorobenzene

2,4-Dinitrotoluene

Hexachlorobutadiene

Hexachloroethane

Nitrobenzene


Pentachlorophenol

2-Methylphenol



Pyridine


ND

ND

ND

ND

ND

ND

ND

ND

ND

ND

ND

ug/l

ug/l

ug/l

ug/l

ug/l

ug/l

ug/l

ug/l

ug/l

ug/l

ug/l

1

1

1

1

1

1

1

1

1

1

1

Qualifier Units RL


SAMPLE RESULTS

Project Name:

Project Number:

Lab Number:

Report Date:

NFTA

17005.02

L1809330

10

25

10

10

10

25

50

25

25

25

18

2-Fluorophenol

Phenol-d6

Nitrobenzene-d5

2-Fluorobiphenyl


4-Terphenyl-d14

73

76

86

86

76

92

21-120

10-120

23-120

15-120

10-120

33-120


04/02/18



L1809330-06Lab ID:




1,8270D03/26/18 19:10HL



80%Percent Solids:

MDL

2.9

4.2

3.6

3.4

3.8

3.4

17.

5.1

5.6

3.6

9.4

Sample Depth:

Serial_No:04021817:02

Page 39 of 115

Acenaphthene

Hexachlorobenzene

Fluoranthene

Naphthalene

Benzo(a)anthracene

Benzo(a)pyrene



Chrysene

Acenaphthylene

Anthracene

Benzo(ghi)perylene

Fluorene

Phenanthrene



Pyrene

Dibenzofuran

Pentachlorophenol

Phenol

2-Methylphenol


Parameter Result

J

J

J

J

J

Dilution Factor

ND

ND

290

ND

140

130

180

58

130

ND

46

81

ND

160

ND

130

240

ND

ND

ND

ND

ND

ug/kg

ug/kg

ug/kg

ug/kg

ug/kg

ug/kg

ug/kg

ug/kg

ug/kg

ug/kg

ug/kg

ug/kg

ug/kg

ug/kg

ug/kg

ug/kg

ug/kg

ug/kg

ug/kg

ug/kg

ug/kg

ug/kg

1

1

1

1

1

1

1

1

1

1

1

1

1

1

1

1

1

1

1

1

1

1

Qualifier Units RL


SAMPLE RESULTS

Project Name:

Project Number:

Lab Number:

Report Date:

NFTA

17005.02

L1809330

160

120

120

210

120

160

120

120

120

160

120

160

210

120

120

160

120

210

160

210

210

300

04/02/18



L1809330-06Lab ID:




1,8270D03/29/18 03:13CB


80%Percent Solids:

MDL

21.

23.

24.

25.

23.

50.

35.

33.

21.

32.

40.

24.

20.

25.

24.

29.

20.

20.

45.

31.

32.

32.

Sample Depth:

Serial_No:04021817:02

Page 40 of 115



SAMPLE RESULTS

Project Name:

Project Number:

Lab Number:

Report Date:

NFTA

17005.02

L1809330

2-Fluorophenol

Phenol-d6

Nitrobenzene-d5

2-Fluorobiphenyl


4-Terphenyl-d14

40

72

69

68

29

82

25-120

10-120

23-120

30-120

10-136

18-120


04/02/18



L1809330-06Lab ID:


MDL

Sample Depth:

Serial_No:04021817:02

Page 41 of 115

Hexachlorobenzene

2,4-Dinitrotoluene

Hexachlorobutadiene

Hexachloroethane

Nitrobenzene


Pentachlorophenol

2-Methylphenol



Pyridine


ND

ND

ND

ND

ND

ND

ND

ND

ND

ND

ND

ug/l

ug/l

ug/l

ug/l

ug/l

ug/l

ug/l

ug/l

ug/l

ug/l

ug/l

1

1

1

1

1

1

1

1

1

1

1

Qualifier Units RL


SAMPLE RESULTS

Project Name:

Project Number:

Lab Number:

Report Date:

NFTA

17005.02

L1809330

10

25

10

10

10

25

50

25

25

25

18

2-Fluorophenol

Phenol-d6

Nitrobenzene-d5

2-Fluorobiphenyl


4-Terphenyl-d14

72

75

82

86

72

90

21-120

10-120

23-120

15-120

10-120

33-120


04/02/18



L1809330-08Lab ID:




1,8270D03/26/18 19:35HL



85%Percent Solids:

MDL

2.9

4.2

3.6

3.4

3.8

3.4

17.

5.1

5.6

3.6

9.4

Sample Depth:

Serial_No:04021817:02

Page 42 of 115

Acenaphthene

Hexachlorobenzene

Fluoranthene

Naphthalene

Benzo(a)anthracene

Benzo(a)pyrene



Chrysene

Acenaphthylene

Anthracene

Benzo(ghi)perylene

Fluorene

Phenanthrene



Pyrene

Dibenzofuran

Pentachlorophenol

Phenol

2-Methylphenol


Parameter Result

J

J

J

J

J

Dilution Factor

ND

ND

220

ND

120

140

180

41

150

ND

48

240

24

180

ND

150

230

ND

ND

ND

ND

ND

ug/kg

ug/kg

ug/kg

ug/kg

ug/kg

ug/kg

ug/kg

ug/kg

ug/kg

ug/kg

ug/kg

ug/kg

ug/kg

ug/kg

ug/kg

ug/kg

ug/kg

ug/kg

ug/kg

ug/kg

ug/kg

ug/kg

1

1

1

1

1

1

1

1

1

1

1

1

1

1

1

1

1

1

1

1

1

1

Qualifier Units RL


SAMPLE RESULTS

Project Name:

Project Number:

Lab Number:

Report Date:

NFTA

17005.02

L1809330

160

120

120

190

120

160

120

120

120

160

120

160

190

120

120

160

120

190

160

190

190

280

04/02/18



L1809330-08Lab ID:




1,8270D03/29/18 04:04CB


85%Percent Solids:

MDL

20.

22.

22.

24.

22.

47.

33.

31.

20.

30.

38.

23.

19.

24.

22.

27.

19.

18.

43.

29.

30.

30.

Sample Depth:

Serial_No:04021817:02

Page 43 of 115



SAMPLE RESULTS

Project Name:

Project Number:

Lab Number:

Report Date:

NFTA

17005.02

L1809330

2-Fluorophenol

Phenol-d6

Nitrobenzene-d5

2-Fluorobiphenyl


4-Terphenyl-d14

57

73

78

65

30

60

25-120

10-120

23-120

30-120

10-136

18-120


04/02/18



L1809330-08Lab ID:


MDL

Sample Depth:

Serial_No:04021817:02

Page 44 of 115


Project Name:

Project Number:

Lab Number:

Report Date:

NFTA

17005.02

L1809330



04/02/18

Analyst: EK

Hexachlorobenzene

2,4-Dinitrotoluene

Hexachlorobutadiene

Hexachloroethane

Nitrobenzene


Pentachlorophenol

2-Methylphenol



Pyridine

Parameter Result

ND

ND

ND

ND

ND

ND

ND

ND

ND

ND

ND

RL

10

25

10

10

10

25

50

25

25

25

18

ug/l

ug/l

ug/l

ug/l

ug/l

ug/l

ug/l

ug/l

ug/l

ug/l

ug/l

UnitsQualifier

TCLP Semivolatiles by EPA 1311 - Westborough Lab for sample(s): 03,06,08 Batch: WG1099718-1

2-Fluorophenol

Phenol-d6

Nitrobenzene-d5

2-Fluorobiphenyl


4-Terphenyl-d14

71

65

70

91

99

99

21-120

10-120

23-120

15-120

10-120

33-120


Criteria


MDL

2.9

4.2

3.6

3.4

3.8

3.4

17.

5.1

5.6

3.6

9.4

Serial_No:04021817:02

Page 45 of 115


Project Name:

Project Number:

Lab Number:

Report Date:

NFTA

17005.02

L1809330



04/02/18

Analyst: TT

Acenaphthene

Hexachlorobenzene

Fluoranthene

Naphthalene

Benzo(a)anthracene

Benzo(a)pyrene



Chrysene

Acenaphthylene

Anthracene

Benzo(ghi)perylene

Fluorene

Phenanthrene



Pyrene

Dibenzofuran

Pentachlorophenol

Phenol

2-Methylphenol


Parameter Result

ND

ND

ND

ND

ND

ND

ND

ND

ND

ND

ND

ND

ND

ND

ND

ND

ND

ND

ND

ND

ND

ND

RL

130

97

97

160

97

130

97

97

97

130

97

130

160

97

97

130

97

160

130

160

160

230

ug/kg

ug/kg

ug/kg

ug/kg

ug/kg

ug/kg

ug/kg

ug/kg

ug/kg

ug/kg

ug/kg

ug/kg

ug/kg

ug/kg

ug/kg

ug/kg

ug/kg

ug/kg

ug/kg

ug/kg

ug/kg

ug/kg

UnitsQualifier

Semivolatile Organics by GC/MS - Westborough Lab for sample(s): 03,06,08 Batch: WG1100907-1

MDL

17.

18.

18.

20.

18.

40.

27.

26.

17.

25.

32.

19.

16.

20.

19.

22.

16.

15.

36.

24.

25.

25.

Serial_No:04021817:02

Page 46 of 115


Project Name:

Project Number:

Lab Number:

Report Date:

NFTA

17005.02

L1809330



04/02/18

Analyst: TT


Semivolatile Organics by GC/MS - Westborough Lab for sample(s): 03,06,08 Batch: WG1100907-1

2-Fluorophenol

Phenol-d6

Nitrobenzene-d5

2-Fluorobiphenyl


4-Terphenyl-d14

67

78

73

85

82

92

25-120

10-120

23-120

30-120

10-136

18-120


Criteria

MDL

Serial_No:04021817:02

Page 47 of 115

Hexachlorobenzene

2,4-Dinitrotoluene

Hexachlorobutadiene

Hexachloroethane

Nitrobenzene


Pentachlorophenol

2-Methylphenol



Pyridine

88

74

84

66

70

83

68

76

75

90

54

97

81

87

67

72

85

80

78

79

91

59

40-140

40-132

28-111

21-105

40-140

30-130

9-103

30-130

30-130

30-130

10-66

10

9

4

2

3

2

16

3

5

1

9

30

30

30

30

30

30

30

30

30

30

30

ParameterLCS

%RecoveryLCSD

%Recovery%Recovery

Limits RPDRPD

Limits

TCLP Semivolatiles by EPA 1311 - Westborough Lab Associated sample(s): 03,06,08 Batch: WG1099718-2 WG1099718-3


Project Name:

Project Number:

Lab Number:

Report Date:

NFTA

17005.02

L1809330


7571708910194

21-12010-12023-12015-12010-12033-120

76707291106101


04/02/18

AcceptanceCriteria

Qual Qual Qual

Serial_No:04021817:02

Page 48 of 115

Acenaphthene

Hexachlorobenzene

Fluoranthene

Naphthalene

Benzo(a)anthracene

Benzo(a)pyrene



Chrysene

Acenaphthylene

Anthracene

Benzo(ghi)perylene

Fluorene

Phenanthrene



Pyrene

Dibenzofuran

Pentachlorophenol

Phenol

2-Methylphenol


82

84

85

81

82

81

79

82

80

84

85

84

84

83

87

86

82

83

71

81

84

88

80

85

84

78

81

78

80

76

79

84

84

83

83

82

87

86

81

82

74

81

84

90

31-137

40-140

40-140

40-140

40-140

40-140

40-140

40-140

40-140

40-140

40-140

40-140

40-140

40-140

40-140

40-140

35-142

40-140

17-109

26-90

30-130.

30-130

2

1

1

4

1

4

1

8

1

0

1

1

1

1

0

0

1

1

4

0

0

2

50

50

50

50

50

50

50

50

50

50

50

50

50

50

50

50

50

50

50

50

50

50

ParameterLCS

%RecoveryLCSD

%Recovery%Recovery

Limits RPDRPD

Limits

Semivolatile Organics by GC/MS - Westborough Lab Associated sample(s): 03,06,08 Batch: WG1100907-2 WG1100907-3


Project Name:

Project Number:

Lab Number:

Report Date:

NFTA

17005.02

L1809330

04/02/18

Qual Qual Qual

Serial_No:04021817:02

Page 49 of 115

ParameterLCS

%RecoveryLCSD

%Recovery%Recovery

Limits RPDRPD

Limits

Semivolatile Organics by GC/MS - Westborough Lab Associated sample(s): 03,06,08 Batch: WG1100907-2 WG1100907-3


Project Name:

Project Number:

Lab Number:

Report Date:

NFTA

17005.02

L1809330


798081908693

25-12010-12023-12030-12010-13618-120

768179898791


04/02/18

AcceptanceCriteria

Qual Qual Qual

Serial_No:04021817:02

Page 50 of 115

PCBS

Serial_No:04021817:02

Page 51 of 115

FF

Aroclor 1016

Aroclor 1221

Aroclor 1232

Aroclor 1242

Aroclor 1248

Aroclor 1254

Aroclor 1260

Aroclor 1262

Aroclor 1268


ND

ND

ND

ND

ND

ND

ND

ND

ND

ug/kg

ug/kg

ug/kg

ug/kg

ug/kg

ug/kg

ug/kg

ug/kg

ug/kg

1

1

1

1

1

1

1

1

1

Qualifier Units RL


SAMPLE RESULTS

Project Name:

Project Number:

Lab Number:

Report Date:

NFTA

17005.02

L1809330

39.5

39.5

39.5

39.5

39.5

39.5

39.5

39.5

39.5


Decachlorobiphenyl


Decachlorobiphenyl

73

65

78

57

30-150

30-150

30-150

30-150

Acceptance Criteria

A

A

B

B


04/02/18



L1809330-03Lab ID:




1,8082A03/28/18 09:01HT

EPA 3546



83%Percent Solids:

MDL

4.48

6.01

3.89

4.83

4.43

3.22

4.12

3.25

2.80

A

A

A

A

A

A

A

A

A

Column

Sample Depth:

Serial_No:04021817:02

Page 52 of 115

Aroclor 1016

Aroclor 1221

Aroclor 1232

Aroclor 1242

Aroclor 1248

Aroclor 1254

Aroclor 1260

Aroclor 1262

Aroclor 1268


ND

ND

ND

ND

ND

ND

ND

ND

ND

ug/kg

ug/kg

ug/kg

ug/kg

ug/kg

ug/kg

ug/kg

ug/kg

ug/kg

1

1

1

1

1

1

1

1

1

Qualifier Units RL


SAMPLE RESULTS

Project Name:

Project Number:

Lab Number:

Report Date:

NFTA

17005.02

L1809330

40.3

40.3

40.3

40.3

40.3

40.3

40.3

40.3

40.3


Decachlorobiphenyl


Decachlorobiphenyl

80

67

82

57

30-150

30-150

30-150

30-150

Acceptance Criteria

A

A

B

B


04/02/18



L1809330-06Lab ID:




1,8082A03/28/18 09:14HT

EPA 3546



80%Percent Solids:

MDL

4.57

6.13

3.96

4.93

4.52

3.29

4.21

3.31

2.85

A

A

A

A

A

A

A

A

A

Column

Sample Depth:

Serial_No:04021817:02

Page 53 of 115

Aroclor 1016

Aroclor 1221

Aroclor 1232

Aroclor 1242

Aroclor 1248

Aroclor 1254

Aroclor 1260

Aroclor 1262

Aroclor 1268

Parameter Result

J

Dilution Factor

ND

ND

ND

ND

ND

ND

22.6

ND

ND

ug/kg

ug/kg

ug/kg

ug/kg

ug/kg

ug/kg

ug/kg

ug/kg

ug/kg

1

1

1

1

1

1

1

1

1

Qualifier Units RL


SAMPLE RESULTS

Project Name:

Project Number:

Lab Number:

Report Date:

NFTA

17005.02

L1809330

38.2

38.2

38.2

38.2

38.2

38.2

38.2

38.2

38.2


Decachlorobiphenyl


Decachlorobiphenyl

81

50

88

51

30-150

30-150

30-150

30-150

Acceptance Criteria

A

A

B

B


04/02/18



L1809330-08Lab ID:




1,8082A03/28/18 17:48HT

EPA 3546



85%Percent Solids:

MDL

4.34

5.82

3.76

4.68

4.29

3.12

3.99

3.14

2.71

A

A

A

A

A

A

B

A

A

Column

Sample Depth:

Serial_No:04021817:02

Page 54 of 115


Project Name:

Project Number:

Lab Number:

Report Date:

NFTA

17005.02

L1809330



Cleanup Method:

EPA 3546


04/02/18


Analyst: HT

Aroclor 1016

Aroclor 1221

Aroclor 1232

Aroclor 1242

Aroclor 1248

Aroclor 1254

Aroclor 1260

Aroclor 1262

Aroclor 1268

Parameter Result

ND

ND

ND

ND

ND

ND

ND

ND

ND

RL

31.4

31.4

31.4

31.4

31.4

31.4

31.4

31.4

31.4

ug/kg

ug/kg

ug/kg

ug/kg

ug/kg

ug/kg

ug/kg

ug/kg

ug/kg

UnitsQualifier

Polychlorinated Biphenyls by GC - Westborough Lab for sample(s): 03,06,08 Batch: WG1100041-1


Decachlorobiphenyl


Decachlorobiphenyl

91

79

98

73

30-150

30-150

30-150

30-150


Criteria



MDL

3.56

4.78

3.09

3.84

3.52

2.56

3.28

2.58

2.22

Column

A

A

A

A

A

A

A

A

A

A

A

B

B

Serial_No:04021817:02

Page 55 of 115

Aroclor 1016

Aroclor 1260

105

110

101

108

40-140

40-140

4

2

50

50

ParameterLCS

%RecoveryLCSD

%Recovery%Recovery

Limits RPDRPD

Limits

Polychlorinated Biphenyls by GC - Westborough Lab Associated sample(s): 03,06,08 Batch: WG1100041-2 WG1100041-3


Project Name:

Project Number:

Lab Number:

Report Date:

NFTA

17005.02

L1809330


988610581

30-15030-15030-15030-150

AABB

93879977


04/02/18

AcceptanceCriteria


A

A

Serial_No:04021817:02

Page 56 of 115

PESTICIDES

Serial_No:04021817:02

Page 57 of 115

FF

Lindane

Heptachlor

Heptachlor epoxide

Endrin

Methoxychlor

Toxaphene

Chlordane


ND

ND

ND

ND

ND

ND

ND

ug/l

ug/l

ug/l

ug/l

ug/l

ug/l

ug/l

1

1

1

1

1

1

1

Qualifier Units RL


SAMPLE RESULTS

Project Name:

Project Number:

Lab Number:

Report Date:

NFTA

17005.02

L1809330

0.100

0.100

0.100

0.200

1.00

1.00

1.00


Decachlorobiphenyl


Decachlorobiphenyl

119

77

109

91

30-150

30-150

30-150

30-150

Acceptance Criteria

A

A

B

B


04/02/18



L1809330-03Lab ID:




1,8081B03/28/18 16:32KEG



83%Percent Solids:

MDL

0.022

0.016

0.021

0.021

0.034

0.314

0.232

A

A

A

A

A

A

A

Column

Sample Depth:

Serial_No:04021817:02

Page 58 of 115

Delta-BHC

Lindane

Alpha-BHC

Beta-BHC

Heptachlor

Aldrin

Endrin

Dieldrin

4,4'-DDE

4,4'-DDD

4,4'-DDT

Endosulfan I

Endosulfan II

Endosulfan sulfate

cis-Chlordane


ND

ND

ND

ND

ND

ND

ND

ND

ND

ND

ND

ND

ND

ND

ND

ug/kg

ug/kg

ug/kg

ug/kg

ug/kg

ug/kg

ug/kg

ug/kg

ug/kg

ug/kg

ug/kg

ug/kg

ug/kg

ug/kg

ug/kg

1

1

1

1

1

1

1

1

1

1

1

1

1

1

1

Qualifier Units RL


SAMPLE RESULTS

Project Name:

Project Number:

Lab Number:

Report Date:

NFTA

17005.02

L1809330

1.82

0.760

0.760

1.82

0.912

1.82

0.760

1.14

1.82

1.82

3.42

1.82

1.82

0.760

2.28


Decachlorobiphenyl


Decachlorobiphenyl

87

85

80

79

30-150

30-150

30-150

30-150

Acceptance Criteria

B

B

A

A


04/02/18



L1809330-03Lab ID:




1,8081B03/31/18 01:04SL

EPA 3546



MDL

0.357

0.340

0.216

0.692

0.409

0.642

0.312

0.570

0.422

0.651

1.47

0.431

0.610

0.362

0.635

A

A

A

A

A

A

A

A

A

A

A

A

A

A

A

Column

Sample Depth:

Serial_No:04021817:02

Page 59 of 115

2,4-D

2,4,5-TP (Silvex)


ND

ND

mg/l

mg/l

1

1

Qualifier Units RL


SAMPLE RESULTS

Project Name:

Project Number:

Lab Number:

Report Date:

NFTA

17005.02

L1809330

0.025

0.005

DCAA

DCAA

37

36

30-150

30-150

Acceptance Criteria

A

B


04/02/18



L1809330-03Lab ID:




1,8151A03/26/18 21:08BM



83%Percent Solids:

MDL

0.001

0.001


A

A

Column

Sample Depth:

Serial_No:04021817:02

Page 60 of 115

2,4,5-TP (Silvex)


ND ug/kg 1

Qualifier Units RL


SAMPLE RESULTS

Project Name:

Project Number:

Lab Number:

Report Date:

NFTA

17005.02

L1809330

199

DCAA

DCAA

122

118

30-150

30-150

Acceptance Criteria

A

B


04/02/18



L1809330-03Lab ID:




1,8151A03/25/18 15:12SL


83%Percent Solids:

MDL

5.30


A

Column

Sample Depth:

Serial_No:04021817:02

Page 61 of 115

Lindane

Heptachlor

Heptachlor epoxide

Endrin

Methoxychlor

Toxaphene

Chlordane


ND

ND

ND

ND

ND

ND

ND

ug/l

ug/l

ug/l

ug/l

ug/l

ug/l

ug/l

1

1

1

1

1

1

1

Qualifier Units RL


SAMPLE RESULTS

Project Name:

Project Number:

Lab Number:

Report Date:

NFTA

17005.02

L1809330

0.100

0.100

0.100

0.200

1.00

1.00

1.00


Decachlorobiphenyl


Decachlorobiphenyl

124

74

114

94

30-150

30-150

30-150

30-150

Acceptance Criteria

A

A

B

B


04/02/18



L1809330-06Lab ID:




1,8081B03/28/18 16:45KEG



80%Percent Solids:

MDL

0.022

0.016

0.021

0.021

0.034

0.314

0.232

A

A

A

A

A

A

A

Column

Sample Depth:

Serial_No:04021817:02

Page 62 of 115

Delta-BHC

Lindane

Alpha-BHC

Beta-BHC

Heptachlor

Aldrin

Endrin

Dieldrin

4,4'-DDE

4,4'-DDD

4,4'-DDT

Endosulfan I

Endosulfan II

Endosulfan sulfate

cis-Chlordane

Parameter Result

J

Dilution Factor

ND

ND

ND

ND

ND

ND

0.578

ND

ND

ND

ND

ND

ND

ND

ND

ug/kg

ug/kg

ug/kg

ug/kg

ug/kg

ug/kg

ug/kg

ug/kg

ug/kg

ug/kg

ug/kg

ug/kg

ug/kg

ug/kg

ug/kg

1

1

1

1

1

1

1

1

1

1

1

1

1

1

1

Qualifier Units RL


SAMPLE RESULTS

Project Name:

Project Number:

Lab Number:

Report Date:

NFTA

17005.02

L1809330

1.96

0.815

0.815

1.96

0.978

1.96

0.815

1.22

1.96

1.96

3.67

1.96

1.96

0.815

2.44


Decachlorobiphenyl


Decachlorobiphenyl

91

86

83

89

30-150

30-150

30-150

30-150

Acceptance Criteria

B

B

A

A


04/02/18



L1809330-06Lab ID:




1,8081B03/31/18 00:51SL

EPA 3546



MDL

0.383

0.364

0.231

0.742

0.438

0.688

0.334

0.611

0.452

0.698

1.57

0.462

0.654

0.388

0.681

A

A

A

A

A

A

B

A

A

A

A

A

A

A

A

Column

Sample Depth:

Serial_No:04021817:02

Page 63 of 115

2,4-D

2,4,5-TP (Silvex)


ND

ND

mg/l

mg/l

1

1

Qualifier Units RL


SAMPLE RESULTS

Project Name:

Project Number:

Lab Number:

Report Date:

NFTA

17005.02

L1809330

0.025

0.005

DCAA

DCAA

30

33

30-150

30-150

Acceptance Criteria

A

B


04/02/18



L1809330-06Lab ID:




1,8151A03/26/18 21:27BM



80%Percent Solids:

MDL

0.001

0.001


A

A

Column

Sample Depth:

Serial_No:04021817:02

Page 64 of 115

2,4,5-TP (Silvex)


ND ug/kg 1

Qualifier Units RL


SAMPLE RESULTS

Project Name:

Project Number:

Lab Number:

Report Date:

NFTA

17005.02

L1809330

204

DCAA

DCAA

140

133

30-150

30-150

Acceptance Criteria

A

B


04/02/18



L1809330-06Lab ID:




1,8151A03/25/18 15:31SL


80%Percent Solids:

MDL

5.44


A

Column

Sample Depth:

Serial_No:04021817:02

Page 65 of 115

Lindane

Heptachlor

Heptachlor epoxide

Endrin

Methoxychlor

Toxaphene

Chlordane


ND

ND

ND

ND

ND

ND

ND

ug/l

ug/l

ug/l

ug/l

ug/l

ug/l

ug/l

1

1

1

1

1

1

1

Qualifier Units RL


SAMPLE RESULTS

Project Name:

Project Number:

Lab Number:

Report Date:

NFTA

17005.02

L1809330

0.100

0.100

0.100

0.200

1.00

1.00

1.00


Decachlorobiphenyl


Decachlorobiphenyl

130

107

123

138

30-150

30-150

30-150

30-150

Acceptance Criteria

A

A

B

B


04/02/18



L1809330-08Lab ID:




1,8081B03/28/18 16:58KEG



85%Percent Solids:

MDL

0.022

0.016

0.021

0.021

0.034

0.314

0.232

A

A

A

A

A

A

A

Column

Sample Depth:

Serial_No:04021817:02

Page 66 of 115

2,4-D

2,4,5-TP (Silvex)


ND

ND

mg/l

mg/l

1

1

Qualifier Units RL


SAMPLE RESULTS

Project Name:

Project Number:

Lab Number:

Report Date:

NFTA

17005.02

L1809330

0.025

0.005

DCAA

DCAA

45

47

30-150

30-150

Acceptance Criteria

A

B


04/02/18



L1809330-08Lab ID:




1,8151A03/31/18 23:29SL



85%Percent Solids:

MDL

0.001

0.001


A

A

Column

Sample Depth:

Serial_No:04021817:02

Page 67 of 115

2,4,5-TP (Silvex)


ND ug/kg 1

Qualifier Units RL


SAMPLE RESULTS

Project Name:

Project Number:

Lab Number:

Report Date:

NFTA

17005.02

L1809330

192

DCAA

DCAA

139

129

30-150

30-150

Acceptance Criteria

A

B


04/02/18



L1809330-08Lab ID:




1,8151A03/25/18 15:50SL


85%Percent Solids:

MDL

5.10


A

Column

Sample Depth:

Serial_No:04021817:02

Page 68 of 115

Delta-BHC

Lindane

Alpha-BHC

Beta-BHC

Heptachlor

Aldrin

Endrin

Dieldrin

4,4'-DDE

4,4'-DDD

4,4'-DDT

Endosulfan I

Endosulfan II

Endosulfan sulfate

cis-Chlordane


ND

ND

ND

ND

ND

ND

ND

ND

ND

ND

ND

ND

ND

ND

ND

ug/kg

ug/kg

ug/kg

ug/kg

ug/kg

ug/kg

ug/kg

ug/kg

ug/kg

ug/kg

ug/kg

ug/kg

ug/kg

ug/kg

ug/kg

5

5

5

5

5

5

5

5

5

5

5

5

5

5

5

Qualifier Units RL


SAMPLE RESULTS

Project Name:

Project Number:

Lab Number:

Report Date:

NFTA

17005.02

L1809330

9.39

3.91

3.91

9.39

4.70

9.39

3.91

5.87

9.39

9.39

17.6

9.39

9.39

3.91

11.7


Decachlorobiphenyl


Decachlorobiphenyl

84

75

82

57

30-150

30-150

30-150

30-150

Acceptance Criteria

B

B

A

A


04/02/18



L1809330-08Lab ID:


D



1,8081B03/31/18 01:17SL

EPA 3546



MDL

1.84

1.75

1.11

3.56

2.11

3.31

1.60

2.94

2.17

3.35

7.56

2.22

3.14

1.86

3.27

A

A

A

A

A

A

B

A

A

A

A

A

A

A

A

Column

Sample Depth:

Serial_No:04021817:02

Page 69 of 115


Project Name:

Project Number:

Lab Number:

Report Date:

NFTA

17005.02

L1809330



04/02/18

Analyst: JW

Lindane

Heptachlor

Heptachlor epoxide

Endrin

Methoxychlor

Toxaphene

Chlordane

Parameter Result

ND

ND

ND

ND

ND

ND

ND

RL

0.100

0.100

0.100

0.200

1.00

1.00

1.00

ug/l

ug/l

ug/l

ug/l

ug/l

ug/l

ug/l

UnitsQualifier

TCLP Pesticides by EPA 1311 - Westborough Lab for sample(s): 03,06,08 Batch: WG1099724-1


Decachlorobiphenyl


Decachlorobiphenyl

100

90

106

97

30-150

30-150

30-150

30-150


Criteria


MDL

0.022

0.016

0.021

0.021

0.034

0.314

0.232

Column

A

A

A

A

A

A

A

A

A

B

B

Serial_No:04021817:02

Page 70 of 115


Project Name:

Project Number:

Lab Number:

Report Date:

NFTA

17005.02

L1809330



04/02/18

Analyst: SL

2,4,5-TP (Silvex)

Parameter Result

ND

RL

162ug/kg

UnitsQualifier

Chlorinated Herbicides by GC - Westborough Lab for sample(s): 03,06,08 Batch: WG1099726-1

DCAA

DCAA

102

97

30-150

30-150


Criteria

MDL

4.31


Column

A

A

B

Serial_No:04021817:02

Page 71 of 115


Project Name:

Project Number:

Lab Number:

Report Date:

NFTA

17005.02

L1809330



04/02/18

Analyst: BM

2,4-D

2,4,5-TP (Silvex)

Parameter Result

ND

ND

RL

0.025

0.005

mg/l

mg/l

UnitsQualifier

TCLP Herbicides by EPA 1311 - Westborough Lab for sample(s): 03,06 Batch: WG1100028-1

DCAA

DCAA

36

34

30-150

30-150


Criteria


MDL

0.001

0.001


Column

A

A

A

B

Serial_No:04021817:02

Page 72 of 115


Project Name:

Project Number:

Lab Number:

Report Date:

NFTA

17005.02

L1809330



Cleanup Method:

EPA 3546


04/02/18

Analyst: JW

Delta-BHC

Lindane

Alpha-BHC

Beta-BHC

Heptachlor

Aldrin

Endrin

Dieldrin

4,4'-DDE

4,4'-DDD

4,4'-DDT

Endosulfan I

Endosulfan II

Endosulfan sulfate

cis-Chlordane

Parameter Result

ND

ND

ND

ND

ND

ND

ND

ND

ND

ND

ND

ND

ND

ND

ND

RL

1.51

0.631

0.631

1.51

0.757

1.51

0.631

0.946

1.51

1.51

2.84

1.51

1.51

0.631

1.89

ug/kg

ug/kg

ug/kg

ug/kg

ug/kg

ug/kg

ug/kg

ug/kg

ug/kg

ug/kg

ug/kg

ug/kg

ug/kg

ug/kg

ug/kg

UnitsQualifier

Organochlorine Pesticides by GC - Westborough Lab for sample(s): 03,06,08 Batch: WG1100038-1


Decachlorobiphenyl


Decachlorobiphenyl

92

135

95

88

30-150

30-150

30-150

30-150


Criteria


MDL

0.296

0.282

0.179

0.574

0.339

0.533

0.259

0.473

0.350

0.540

1.22

0.358

0.506

0.300

0.527

Column

A

A

A

A

A

A

A

A

A

A

A

A

A

A

A

B

B

A

A

Serial_No:04021817:02

Page 73 of 115


Project Name:

Project Number:

Lab Number:

Report Date:

NFTA

17005.02

L1809330



04/02/18

Analyst: SL

2,4-D

2,4,5-TP (Silvex)

Parameter Result

ND

ND

RL

0.025

0.005

mg/l

mg/l

UnitsQualifier


DCAA

DCAA

48

47

30-150

30-150


Criteria


MDL

0.001

0.001


Column

A

A

A

B

Serial_No:04021817:02

Page 74 of 115

Lindane

Heptachlor

Heptachlor epoxide

Endrin

Methoxychlor

114

112

111

116

116

114

110

109

113

115

30-150

30-150

30-150

30-150

30-150

0

2

2

3

1

20

20

20

20

20

ParameterLCS

%RecoveryLCSD

%Recovery%Recovery

Limits RPDRPD

Limits

TCLP Pesticides by EPA 1311 - Westborough Lab Associated sample(s): 03,06,08 Batch: WG1099724-2 WG1099724-3


Project Name:

Project Number:

Lab Number:

Report Date:

NFTA

17005.02

L1809330


10599110104

30-15030-15030-15030-150

AABB

10196104100


04/02/18

AcceptanceCriteria


A

A

A

A

A

Serial_No:04021817:02

Page 75 of 115

2,4,5-TP (Silvex) 83 80 30-150 4 30

ParameterLCS

%RecoveryLCSD

%Recovery%Recovery

Limits RPDRPD

Limits

Chlorinated Herbicides by GC - Westborough Lab Associated sample(s): 03,06,08 Batch: WG1099726-2 WG1099726-3


Project Name:

Project Number:

Lab Number:

Report Date:

NFTA

17005.02

L1809330

DCAADCAA

110109

30-15030-150

AB

111112


04/02/18

AcceptanceCriteria


A

Serial_No:04021817:02

Page 76 of 115

2,4-D

2,4,5-TP (Silvex)

60

31

71

35

30-150

30-150

17

12

25

25

ParameterLCS

%RecoveryLCSD

%Recovery%Recovery

Limits RPDRPD

Limits

TCLP Herbicides by EPA 1311 - Westborough Lab Associated sample(s): 03,06 Batch: WG1100028-2 WG1100028-3


Project Name:

Project Number:

Lab Number:

Report Date:

NFTA

17005.02

L1809330

DCAADCAA

3932

30-15030-150

AB

4538


04/02/18

AcceptanceCriteria


A

A

Serial_No:04021817:02

Page 77 of 115

Delta-BHC

Lindane

Alpha-BHC

Beta-BHC

Heptachlor

Aldrin

Endrin

Dieldrin

4,4'-DDE

4,4'-DDD

4,4'-DDT

Endosulfan I

Endosulfan II

Endosulfan sulfate

cis-Chlordane

87

91

84

97

96

91

96

101

89

78

81

102

96

82

87

97

105

98

109

111

106

111

116

101

86

92

109

111

92

100

30-150

30-150

30-150

30-150

30-150

30-150

30-150

30-150

30-150

30-150

30-150

30-150

30-150

30-150

30-150

11

14

15

12

14

15

14

14

13

10

13

7

14

11

14

30

30

30

30

30

30

30

30

30

30

30

30

30

30

30

ParameterLCS

%RecoveryLCSD

%Recovery%Recovery

Limits RPDRPD

Limits

Organochlorine Pesticides by GC - Westborough Lab Associated sample(s): 03,06,08 Batch: WG1100038-2 WG1100038-3


Project Name:

Project Number:

Lab Number:

Report Date:

NFTA

17005.02

L1809330


82988567

30-15030-15030-15030-150

BBAA

991159782


04/02/18

AcceptanceCriteria


A

A

A

A

A

A

A

A

A

A

A

A

A

A

A

Serial_No:04021817:02

Page 78 of 115

2,4-D

2,4,5-TP (Silvex)

89

48

87

47

30-150

30-150

2

2

25

25

ParameterLCS

%RecoveryLCSD

%Recovery%Recovery

Limits RPDRPD

Limits



Project Name:

Project Number:

Lab Number:

Report Date:

NFTA

17005.02

L1809330

DCAADCAA

5640

30-15030-150

AB

5741


04/02/18

AcceptanceCriteria


A

A

Serial_No:04021817:02

Page 79 of 115

METALS

Serial_No:04021817:02

Page 80 of 115

FF

Project Name:

Project Number:

Lab Number:

Report Date:

NFTA

17005.02

L1809330

04/02/18

SAMPLE RESULTS


Matrix: Soil


L1809330-03Lab ID:



DateAnalyzed


Date Prepared


Arsenic, TCLP

Barium, TCLP

Cadmium, TCLP

Chromium, TCLP

Lead, TCLP

Mercury, TCLP

Selenium, TCLP

Silver, TCLP

J

J

ND

0.510

ND

ND

0.050

ND

0.056

ND

mg/l

mg/l

mg/l

mg/l

mg/l

mg/l

mg/l

mg/l

1

1

1

1

1

1

1

1

1.00

0.500

0.100

0.200

0.500

0.0010

0.500

0.100

03/29/18 12:12

03/28/18 22:21

03/28/18 22:21

03/29/18 12:12

03/28/18 22:21

03/23/18 16:37

03/28/18 22:21

03/28/18 22:21

1,6010C

1,6010C

1,6010C

1,6010C

1,6010C

1,7470A

1,6010C

1,6010C

PE

AB

AB

PE

AB

MG

AB

AB

03/23/18 14:06

03/23/18 14:06

03/23/18 14:06

03/23/18 14:06

03/23/18 14:06

03/23/18 11:35

03/23/18 14:06

03/23/18 14:06

EPA 3015

EPA 3015

EPA 3015

EPA 3015

EPA 3015

EPA 7470A

EPA 3015

EPA 3015

PrepMethod


Percent Solids: 83%

MDL

0.019

0.021

0.010

0.021

0.027

0.0003

0.035

0.028

Sample Depth:

Serial_No:04021817:02

Page 81 of 115

Project Name:

Project Number:

Lab Number:

Report Date:

NFTA

17005.02

L1809330

04/02/18

SAMPLE RESULTS


Matrix: Soil


L1809330-03Lab ID:



DateAnalyzed


Date Prepared



Arsenic, Total

Barium, Total

Beryllium, Total

Cadmium, Total

Chromium, Total

Copper, Total

Lead, Total

Manganese, Total

Mercury, Total

Nickel, Total

Selenium, Total

Silver, Total

Zinc, Total

Chromium, Trivalent

J

J

J

2.63

74.6

0.213

0.172

6.62

43.0

286

165

0.79

5.36

0.318

ND

114

6.6

mg/kg

mg/kg

mg/kg

mg/kg

mg/kg

mg/kg

mg/kg

mg/kg

mg/kg

mg/kg

mg/kg

mg/kg

mg/kg

mg/kg

1

1

1

1

1

1

1

1

1

1

1

1

1

1

0.454

0.454

0.227

0.454

0.454

0.454

2.27

0.454

0.08

1.13

0.908

0.454

2.27

0.96

03/23/18 20:18

03/23/18 20:18

03/23/18 20:18

03/23/18 20:18

03/23/18 20:18

03/23/18 20:18

03/23/18 20:18

03/23/18 20:18

03/21/18 16:48

03/23/18 20:18

03/23/18 20:18

03/23/18 20:18

03/23/18 20:18

03/23/18 20:18

1,6010C

1,6010C

1,6010C

1,6010C

1,6010C

1,6010C

1,6010C

1,6010C

1,7471B

1,6010C

1,6010C

1,6010C

1,6010C

107,-

AB

AB

AB

AB

AB

AB

AB

AB

MG

AB

AB

AB

AB

03/20/18 20:03

03/20/18 20:03

03/20/18 20:03

03/20/18 20:03

03/20/18 20:03

03/20/18 20:03

03/20/18 20:03

03/20/18 20:03

03/21/18 08:00

03/20/18 20:03

03/20/18 20:03

03/20/18 20:03

03/20/18 20:03

EPA 3050B

EPA 3050B

EPA 3050B

EPA 3050B

EPA 3050B

EPA 3050B

EPA 3050B

EPA 3050B

EPA 7471B

EPA 3050B

EPA 3050B

EPA 3050B

EPA 3050B

NA

PrepMethod

Percent Solids: 83%

MDL

0.094

0.079

0.015

0.045

0.044

0.117

0.122

0.072

0.02

0.110

0.117

0.128

0.133

0.96

Sample Depth:

Serial_No:04021817:02

Page 82 of 115

Project Name:

Project Number:

Lab Number:

Report Date:

NFTA

17005.02

L1809330

04/02/18

SAMPLE RESULTS


Matrix: Soil


L1809330-06Lab ID:



DateAnalyzed


Date Prepared


Arsenic, TCLP

Barium, TCLP

Cadmium, TCLP

Chromium, TCLP

Lead, TCLP

Mercury, TCLP

Selenium, TCLP

Silver, TCLP

J

J

ND

0.798

ND

ND

0.066

ND

0.039

ND

mg/l

mg/l

mg/l

mg/l

mg/l

mg/l

mg/l

mg/l

1

1

1

1

1

1

1

1

1.00

0.500

0.100

0.200

0.500

0.0010

0.500

0.100

03/29/18 12:46

03/28/18 22:53

03/28/18 22:53

03/29/18 12:46

03/28/18 22:53

03/23/18 16:38

03/28/18 22:53

03/28/18 22:53

1,6010C

1,6010C

1,6010C

1,6010C

1,6010C

1,7470A

1,6010C

1,6010C

PE

AB

AB

PE

AB

MG

AB

AB

03/23/18 14:06

03/23/18 14:06

03/23/18 14:06

03/23/18 14:06

03/23/18 14:06

03/23/18 11:35

03/23/18 14:06

03/23/18 14:06

EPA 3015

EPA 3015

EPA 3015

EPA 3015

EPA 3015

EPA 7470A

EPA 3015

EPA 3015

PrepMethod


Percent Solids: 80%

MDL

0.019

0.021

0.010

0.021

0.027

0.0003

0.035

0.028

Sample Depth:

Serial_No:04021817:02

Page 83 of 115

Project Name:

Project Number:

Lab Number:

Report Date:

NFTA

17005.02

L1809330

04/02/18

SAMPLE RESULTS


Matrix: Soil


L1809330-06Lab ID:



DateAnalyzed


Date Prepared



Arsenic, Total

Barium, Total

Beryllium, Total

Cadmium, Total

Chromium, Total

Copper, Total

Lead, Total

Manganese, Total

Mercury, Total

Nickel, Total

Selenium, Total

Silver, Total

Zinc, Total

Chromium, Trivalent

J

J

2.42

66.4

0.863

0.226

8.29

11.1

126

369

0.16

6.61

0.439

ND

56.5

8.3

mg/kg

mg/kg

mg/kg

mg/kg

mg/kg

mg/kg

mg/kg

mg/kg

mg/kg

mg/kg

mg/kg

mg/kg

mg/kg

mg/kg

1

1

1

1

1

1

1

1

1

1

1

1

1

1

0.472

0.472

0.236

0.472

0.472

0.472

2.36

0.472

0.08

1.18

0.943

0.472

2.36

1.0

03/23/18 20:22

03/23/18 20:22

03/23/18 20:22

03/23/18 20:22

03/23/18 20:22

03/23/18 20:22

03/23/18 20:22

03/23/18 20:22

03/21/18 16:50

03/23/18 20:22

03/23/18 20:22

03/23/18 20:22

03/23/18 20:22

03/23/18 20:22

1,6010C

1,6010C

1,6010C

1,6010C

1,6010C

1,6010C

1,6010C

1,6010C

1,7471B

1,6010C

1,6010C

1,6010C

1,6010C

107,-

AB

AB

AB

AB

AB

AB

AB

AB

MG

AB

AB

AB

AB

03/20/18 20:03

03/20/18 20:03

03/20/18 20:03

03/20/18 20:03

03/20/18 20:03

03/20/18 20:03

03/20/18 20:03

03/20/18 20:03

03/21/18 08:00

03/20/18 20:03

03/20/18 20:03

03/20/18 20:03

03/20/18 20:03

EPA 3050B

EPA 3050B

EPA 3050B

EPA 3050B

EPA 3050B

EPA 3050B

EPA 3050B

EPA 3050B

EPA 7471B

EPA 3050B

EPA 3050B

EPA 3050B

EPA 3050B

NA

PrepMethod

Percent Solids: 80%

MDL

0.098

0.082

0.016

0.046

0.045

0.122

0.126

0.075

0.02

0.114

0.122

0.133

0.138

1.0

Sample Depth:

Serial_No:04021817:02

Page 84 of 115

Project Name:

Project Number:

Lab Number:

Report Date:

NFTA

17005.02

L1809330

04/02/18

SAMPLE RESULTS


Matrix: Soil


L1809330-08Lab ID:



DateAnalyzed


Date Prepared


Arsenic, TCLP

Barium, TCLP

Cadmium, TCLP

Chromium, TCLP

Lead, TCLP

Mercury, TCLP

Selenium, TCLP

Silver, TCLP

J

ND

0.315

ND

ND

ND

ND

ND

ND

mg/l

mg/l

mg/l

mg/l

mg/l

mg/l

mg/l

mg/l

1

1

1

1

1

1

1

1

1.00

0.500

0.100

0.200

0.500

0.0010

0.500

0.100

03/29/18 12:51

03/28/18 22:57

03/28/18 22:57

03/29/18 12:51

03/28/18 22:57

03/23/18 16:40

03/28/18 22:57

03/28/18 22:57

1,6010C

1,6010C

1,6010C

1,6010C

1,6010C

1,7470A

1,6010C

1,6010C

PE

AB

AB

PE

AB

MG

AB

AB

03/23/18 14:06

03/23/18 14:06

03/23/18 14:06

03/23/18 14:06

03/23/18 14:06

03/23/18 11:35

03/23/18 14:06

03/23/18 14:06

EPA 3015

EPA 3015

EPA 3015

EPA 3015

EPA 3015

EPA 7470A

EPA 3015

EPA 3015

PrepMethod


Percent Solids: 85%

MDL

0.019

0.021

0.010

0.021

0.027

0.0003

0.035

0.028

Sample Depth:

Serial_No:04021817:02

Page 85 of 115

Project Name:

Project Number:

Lab Number:

Report Date:

NFTA

17005.02

L1809330

04/02/18

SAMPLE RESULTS


Matrix: Soil


L1809330-08Lab ID:



DateAnalyzed


Date Prepared



Arsenic, Total

Barium, Total

Beryllium, Total

Cadmium, Total

Chromium, Total

Copper, Total

Lead, Total

Manganese, Total

Mercury, Total

Nickel, Total

Selenium, Total

Silver, Total

Zinc, Total

Chromium, Trivalent

J

J

1.09

31.5

0.251

0.118

8.32

5.58

7.72

74.9

0.10

5.76

0.169

ND

34.3

8.3

mg/kg

mg/kg

mg/kg

mg/kg

mg/kg

mg/kg

mg/kg

mg/kg

mg/kg

mg/kg

mg/kg

mg/kg

mg/kg

mg/kg

1

1

1

1

1

1

1

1

1

1

1

1

1

1

0.456

0.456

0.228

0.456

0.456

0.456

2.28

0.456

0.08

1.14

0.912

0.456

2.28

0.94

03/23/18 21:04

03/23/18 21:04

03/23/18 21:04

03/23/18 21:04

03/23/18 21:04

03/23/18 21:04

03/23/18 21:04

03/23/18 21:04

03/21/18 16:52

03/23/18 21:04

03/23/18 21:04

03/23/18 21:04

03/23/18 21:04

03/23/18 21:04

1,6010C

1,6010C

1,6010C

1,6010C

1,6010C

1,6010C

1,6010C

1,6010C

1,7471B

1,6010C

1,6010C

1,6010C

1,6010C

107,-

AB

AB

AB

AB

AB

AB

AB

AB

MG

AB

AB

AB

AB

03/20/18 20:03

03/20/18 20:03

03/20/18 20:03

03/20/18 20:03

03/20/18 20:03

03/20/18 20:03

03/20/18 20:03

03/20/18 20:03

03/21/18 08:00

03/20/18 20:03

03/20/18 20:03

03/20/18 20:03

03/20/18 20:03

EPA 3050B

EPA 3050B

EPA 3050B

EPA 3050B

EPA 3050B

EPA 3050B

EPA 3050B

EPA 3050B

EPA 7471B

EPA 3050B

EPA 3050B

EPA 3050B

EPA 3050B

NA

PrepMethod

Percent Solids: 85%

MDL

0.095

0.079

0.015

0.045

0.044

0.118

0.122

0.073

0.02

0.110

0.118

0.129

0.134

0.94

Sample Depth:

Serial_No:04021817:02

Page 86 of 115

FF

Parameter

Parameter

Parameter

Result

Result

Result

Dilution Factor

Dilution Factor

Dilution Factor

Qualifier

Qualifier

Qualifier

Units

Units

Units

RL

RL

RL


Project Name:

Project Number:

Lab Number:

Report Date:

NFTA

17005.02

L1809330

DateAnalyzed

DateAnalyzed

DateAnalyzed

AnalyticalMethod

AnalyticalMethod

AnalyticalMethod

Analyst

Analyst

Analyst

Date Prepared

Date Prepared

Date Prepared

04/02/18

Arsenic, Total

Barium, Total

Beryllium, Total

Cadmium, Total

Chromium, Total

Copper, Total

Lead, Total

Manganese, Total

Nickel, Total

Selenium, Total

Silver, Total

Zinc, Total

Mercury, Total

Mercury, TCLP

ND

ND

ND

ND

ND

ND

ND

ND

ND

ND

ND

ND

ND

ND

mg/kg

mg/kg

mg/kg

mg/kg

mg/kg

mg/kg

mg/kg

mg/kg

mg/kg

mg/kg

mg/kg

mg/kg

mg/kg

mg/l

1

1

1

1

1

1

1

1

1

1

1

1

1

1

0.400

0.400

0.200

0.400

0.400

0.400

2.00

0.400

1.00

0.800

0.400

2.00

0.08

0.0010

03/23/18 16:03

03/23/18 16:03

03/23/18 16:03

03/23/18 16:03

03/23/18 16:03

03/23/18 16:03

03/23/18 16:03

03/23/18 16:03

03/23/18 16:03

03/23/18 16:03

03/23/18 16:03

03/23/18 16:03

03/21/18 16:23

03/23/18 16:24

1,6010C

1,6010C

1,6010C

1,6010C

1,6010C

1,6010C

1,6010C

1,6010C

1,6010C

1,6010C

1,6010C

1,6010C

1,7471B

1,7470A

AB

AB

AB

AB

AB

AB

AB

AB

AB

AB

AB

AB

MG

MG

03/20/18 20:03

03/20/18 20:03

03/20/18 20:03

03/20/18 20:03

03/20/18 20:03

03/20/18 20:03

03/20/18 20:03

03/20/18 20:03

03/20/18 20:03

03/20/18 20:03

03/20/18 20:03

03/20/18 20:03

03/21/18 08:00

03/23/18 11:35

Total Metals - Mansfield Lab for sample(s): 03,06,08 Batch: WG1098928-1

Total Metals - Mansfield Lab for sample(s): 03,06,08 Batch: WG1099016-1

TCLP Metals by EPA 1311 - Mansfield Lab for sample(s): 03,06,08 Batch: WG1099926-1

EPA 3050B

EPA 7471B

Digestion Method:

Digestion Method:

Prep Information

Prep Information

MDL

MDL

MDL

0.083

0.070

0.013

0.039

0.038

0.103

0.107

0.064

0.097

0.103

0.113

0.117

0.02

0.0003

Serial_No:04021817:02

Page 87 of 115



Project Name:

Project Number:

Lab Number:

Report Date:

NFTA

17005.02

L1809330

DateAnalyzed


Date Prepared

04/02/18

Arsenic, TCLP

Barium, TCLP

Cadmium, TCLP

Chromium, TCLP

Lead, TCLP

Selenium, TCLP

Silver, TCLP

J

J

ND

0.030

ND

ND

ND

0.040

ND

mg/l

mg/l

mg/l

mg/l

mg/l

mg/l

mg/l

1

1

1

1

1

1

1

1.00

0.500

0.100

0.200

0.500

0.500

0.100

03/29/18 12:03

03/28/18 21:45

03/28/18 21:45

03/29/18 12:03

03/28/18 21:45

03/28/18 21:45

03/28/18 21:45

1,6010C

1,6010C

1,6010C

1,6010C

1,6010C

1,6010C

1,6010C

PE

AB

AB

PE

AB

AB

AB

03/23/18 14:06

03/23/18 14:06

03/23/18 14:06

03/23/18 14:06

03/23/18 14:06

03/23/18 14:06

03/23/18 14:06

TCLP Metals by EPA 1311 - Mansfield Lab for sample(s): 03,06,08 Batch: WG1099987-1

EPA 7470A

EPA 3015

Digestion Method:

Digestion Method:

Prep Information

Prep Information

03/21/18 04:38

03/21/18 04:38



MDL

0.019

0.021

0.010

0.021

0.027

0.035

0.028

Serial_No:04021817:02

Page 88 of 115

Arsenic, Total

Barium, Total

Beryllium, Total

Cadmium, Total

Chromium, Total

Copper, Total

Lead, Total

Manganese, Total

Nickel, Total

Selenium, Total

Silver, Total

Zinc, Total

Mercury, Total

Mercury, TCLP

116

108

107

116

115

115

110

106

115

114

115

113

117

88

-

-

-

-

-

-

-

-

-

-

-

-

-

-

83-117

82-118

83-117

82-117

83-119

84-116

82-117

82-118

82-117

78-121

80-120

81-119

50-149

80-120

-

-

-

-

-

-

-

-

-

-

-

-

-

-

ParameterLCS

%RecoveryLCSD

%Recovery%Recovery


Total Metals - Mansfield Lab Associated sample(s): 03,06,08 Batch: WG1098928-2 SRM Lot Number: D098-540

Total Metals - Mansfield Lab Associated sample(s): 03,06,08 Batch: WG1099016-2 SRM Lot Number: D098-540

TCLP Metals by EPA 1311 - Mansfield Lab Associated sample(s): 03,06,08 Batch: WG1099926-2


Project Name:

Project Number:

Lab Number:

Report Date:

NFTA

17005.02

L1809330

04/02/18

Qual Qual Qual

Serial_No:04021817:02

Page 89 of 115

Arsenic, TCLP

Barium, TCLP

Cadmium, TCLP

Chromium, TCLP

Lead, TCLP

Selenium, TCLP

Silver, TCLP

96

88

94

86

89

103

86

-

-

-

-

-

-

-

75-125

75-125

75-125

75-125

75-125

75-125

75-125

-

-

-

-

-

-

-

20

20

20

20

20

20

20

ParameterLCS

%RecoveryLCSD

%Recovery%Recovery


TCLP Metals by EPA 1311 - Mansfield Lab Associated sample(s): 03,06,08 Batch: WG1099987-2


Project Name:

Project Number:

Lab Number:

Report Date:

NFTA

17005.02

L1809330

04/02/18

Serial_No:04021817:02

Page 90 of 115

Arsenic, Total

Barium, Total

Beryllium, Total

Cadmium, Total

Chromium, Total

Copper, Total

Lead, Total

Manganese, Total

Nickel, Total

Selenium, Total

Silver, Total

Zinc, Total

Mercury, Total

Mercury, TCLP

137.

27.3

0.325

1.06

10.8

30.8

20.4

298.

10.9

ND

ND

160.

0.04J

ND

65.7

142

3.34

3.19

22.5

35.3

48.7

1080

33.7

7.56

19.6

191

0.25

0.0253

0

63

66

46

64

20

61

1710

50

69

72

68

158

101

-

-

-

-

-

-

-

-

-

-

-

-

-

-

-

-

-

-

-

-

-

-

-

-

-

-

-

-

75-125

75-125

75-125

75-125

75-125

75-125

75-125

75-125

75-125

75-125

75-125

75-125

80-120

80-120

-

-

-

-

-

-

-

-

-

-

-

-

-

-

20

20

20

20

20

20

20

20

20

20

20

20

20

20


MS Found

MS%Recovery

MSD Found

MSD %Recovery

RecoveryLimits RPD

RPD Limits

Total Metals - Mansfield Lab Associated sample(s): 03,06,08 QC Batch ID: WG1098928-3 QC Sample: L1809297-01 Client ID: MS Sample

Total Metals - Mansfield Lab Associated sample(s): 03,06,08 QC Batch ID: WG1099016-3 QC Sample: L1809145-01 Client ID: MS Sample

TCLP Metals by EPA 1311 - Mansfield Lab Associated sample(s): 03,06,08 QC Batch ID: WG1099926-3 QC Sample: L1808249-01 Client ID: MS Sample

11

182

4.56

4.65

18.2

22.8

46.5

45.6

45.6

11

27.4

45.6

0.158

0.025

MS Added


Project Name:

Project Number:

Lab Number:

Report Date:

NFTA

17005.02

L1809330

04/02/18

Qual

Q

Q

Q

Q

Q

Q

Q

Q

Q

Q

Q

Q

Q

Qual Qual

Serial_No:04021817:02

Page 91 of 115

Arsenic, TCLP

Barium, TCLP

Cadmium, TCLP

Chromium, TCLP

Lead, TCLP

Selenium, TCLP

Silver, TCLP

ND

0.510

ND

ND

0.050J

0.056J

ND

1.29

20.8

0.550

2.00

5.32

1.40

0.500

108

101

108

100

104

117

100

-

-

-

-

-

-

-

-

-

-

-

-

-

-

75-125

75-125

75-125

75-125

75-125

75-125

75-125

-

-

-

-

-

-

-

20

20

20

20

20

20

20


MS Found

MS%Recovery

MSD Found

MSD %Recovery

RecoveryLimits RPD

RPD Limits

TCLP Metals by EPA 1311 - Mansfield Lab Associated sample(s): 03,06,08 QC Batch ID: WG1099987-3 QC Sample: L1809330-03 Client ID: BH2/4-18

1.2

20

0.51

2

5.1

1.2

0.5

MS Added


Project Name:

Project Number:

Lab Number:

Report Date:

NFTA

17005.02

L1809330

04/02/18

Serial_No:04021817:02

Page 92 of 115

Arsenic, Total

Mercury, Total

Mercury, TCLP

Barium, TCLP

Cadmium, TCLP

Lead, TCLP

Selenium, TCLP

Silver, TCLP

Arsenic, TCLP

Chromium, TCLP

137.

0.04J

ND

0.510

ND

0.050J

0.056J

ND

ND

ND

96.9

0.04J

ND

0.496J

ND

0.062J

ND

ND

ND

ND

mg/kg

mg/kg

mg/l

mg/l

mg/l

mg/l

mg/l

mg/l

mg/l

mg/l

34

NC

NC

NC

NC

NC

NC

NC

NC

NC

20

20

20

20

20

20

20

20

20

20


Total Metals - Mansfield Lab Associated sample(s): 03,06,08 QC Batch ID: WG1098928-4 QC Sample: L1809297-01 Client ID: DUP Sample

Total Metals - Mansfield Lab Associated sample(s): 03,06,08 QC Batch ID: WG1099016-4 QC Sample: L1809145-01 Client ID: DUP Sample

TCLP Metals by EPA 1311 - Mansfield Lab Associated sample(s): 03,06,08 QC Batch ID: WG1099926-4 QC Sample: L1808249-01 Client ID: DUP Sample



NFTA

17005.02

Project Name:

Project Number:

L1809330Lab Number:

Report Date:


04/02/18

Qual

Q

Serial_No:04021817:02

Page 93 of 115

INORGANICS&

MISCELLANEOUS

Serial_No:04021817:02

Page 94 of 115

FF


Matrix: Soil


L1809330-03Lab ID:

SAMPLE RESULTS

Project Name:

Project Number:

Lab Number:

Report Date:

NFTA

17005.02

L1809330


Ignitability of Solids - Westborough Lab

Ignitability NI 03/22/18 09:30 1,1030 JG

Test Material Information

Source of Material:

Description of Material:

Particle Size:

Preliminary Burning Time (sec):

Unknown

Non-Metallic - Damp Clay

Medium

120

Parameter ResultDate

AnalyzedAnalytical

Method Analyst

04/02/18

Sample Depth:

Serial_No:04021817:02

Page 95 of 115

FF


Matrix: Soil


L1809330-06Lab ID:

SAMPLE RESULTS

Project Name:

Project Number:

Lab Number:

Report Date:

NFTA

17005.02

L1809330





Source of Material:


Particle Size:


Unknown

Non-Metallic - Damp Soil

Medium

120


AnalyzedAnalytical

Method Analyst

04/02/18

Sample Depth:

Serial_No:04021817:02

Page 96 of 115

FF


Matrix: Soil


L1809330-08Lab ID:

SAMPLE RESULTS

Project Name:

Project Number:

Lab Number:

Report Date:

NFTA

17005.02

L1809330





Source of Material:


Particle Size:


Unknown


Medium

120


AnalyzedAnalytical

Method Analyst

04/02/18

Sample Depth:

Serial_No:04021817:02

Page 97 of 115

FF



Matrix: Soil


L1809330-01Lab ID:

Qualifier Units RL

SAMPLE RESULTS

Project Name:

Project Number:

Lab Number:

Report Date:

NFTA

17005.02

L1809330

Field Prep:

DateAnalyzed


Not Specified


Date Prepared

-

04/02/18

MDL

NA

Sample Depth:

Serial_No:04021817:02

Page 98 of 115

FF



Matrix: Soil


L1809330-03Lab ID:

Qualifier Units RL

SAMPLE RESULTS

Project Name:

Project Number:

Lab Number:

Report Date:

NFTA

17005.02

L1809330

Field Prep:

DateAnalyzed


Not Specified


Cyanide, Total

pH (H)


Cyanide, Reactive

Sulfide, Reactive

82.9

ND

9.1

ND

ND

ND

%

mg/kg

SU

mg/kg

mg/kg

mg/kg

1

1

1

1

1

1

0.100

1.2

-

0.96

10

10

03/20/18 12:00

03/21/18 12:25

03/20/18 05:38

03/22/18 11:45

03/21/18 17:45

03/21/18 17:18

121,2540G

1,9010C/9012B

1,9045D

1,7196A

125,7.3

125,7.3

RI

LH

UN

NH

RM

RM

Date Prepared

-

03/21/18 08:00

-

03/21/18 18:40

03/21/18 15:35

03/21/18 15:35

04/02/18

MDL

NA

0.24

NA

0.19

10.

10.

Sample Depth:

Serial_No:04021817:02

Page 99 of 115

FF



Matrix: Soil


L1809330-04Lab ID:

Qualifier Units RL

SAMPLE RESULTS

Project Name:

Project Number:

Lab Number:

Report Date:

NFTA

17005.02

L1809330

Field Prep:

DateAnalyzed


Not Specified


Date Prepared

-

04/02/18

MDL

NA

Sample Depth:

Serial_No:04021817:02

Page 100 of 115

FF



Matrix: Soil


L1809330-06Lab ID:

Qualifier Units RL

SAMPLE RESULTS

Project Name:

Project Number:

Lab Number:

Report Date:

NFTA

17005.02

L1809330

Field Prep:

DateAnalyzed


Not Specified


Cyanide, Total

pH (H)


Cyanide, Reactive

Sulfide, Reactive

80.0

6.2

7.9

ND

ND

ND

%

mg/kg

SU

mg/kg

mg/kg

mg/kg

1

1

1

1

1

1

0.100

1.2

-

1.0

10

10

03/20/18 12:00

03/21/18 12:10

03/20/18 05:38

03/22/18 11:45

03/21/18 17:45

03/21/18 17:18

121,2540G

1,9010C/9012B

1,9045D

1,7196A

125,7.3

125,7.3

RI

LH

UN

NH

RM

RM

Date Prepared

-

03/21/18 08:00

-

03/21/18 18:40

03/21/18 15:35

03/21/18 15:35

04/02/18

MDL

NA

0.25

NA

0.20

10.

10.

Sample Depth:

Serial_No:04021817:02

Page 101 of 115

FF



Matrix: Soil


L1809330-07Lab ID:

Qualifier Units RL

SAMPLE RESULTS

Project Name:

Project Number:

Lab Number:

Report Date:

NFTA

17005.02

L1809330

Field Prep:

DateAnalyzed


Not Specified


Date Prepared

-

04/02/18

MDL

NA

Sample Depth:

Serial_No:04021817:02

Page 102 of 115

FF



Matrix: Soil


L1809330-08Lab ID:

Qualifier Units RL

SAMPLE RESULTS

Project Name:

Project Number:

Lab Number:

Report Date:

NFTA

17005.02

L1809330

Field Prep:

DateAnalyzed


Not Specified


Cyanide, Total

pH (H)


Cyanide, Reactive

Sulfide, Reactive

84.7

ND

7.8

ND

ND

ND

%

mg/kg

SU

mg/kg

mg/kg

mg/kg

1

1

1

1

1

1

0.100

1.1

-

0.94

10

10

03/20/18 12:00

03/23/18 10:05

03/20/18 05:38

03/22/18 11:45

03/21/18 17:46

03/21/18 17:18

121,2540G

1,9010C/9012B

1,9045D

1,7196A

125,7.3

125,7.3

RI

LH

UN

NH

RM

RM

Date Prepared

-

03/22/18 15:25

-

03/21/18 18:40

03/21/18 15:35

03/21/18 15:35

04/02/18

MDL

NA

0.24

NA

0.19

10.

10.

Sample Depth:

Serial_No:04021817:02

Page 103 of 115

FF



Project Name:

Project Number:

Lab Number:

Report Date:

NFTA

17005.02

L1809330

DateAnalyzed


Date Prepared

04/02/18

Cyanide, Total

Sulfide, Reactive

Cyanide, Reactive


Cyanide, Total

ND

ND

ND

ND

ND

mg/kg

mg/kg

mg/kg

mg/kg

mg/kg

1

1

1

1

1

0.97

10

10

0.80

0.96

03/21/18 11:58

03/21/18 17:17

03/21/18 17:45

03/22/18 11:45

03/23/18 09:59

1,9010C/9012B

125,7.3

125,7.3

1,7196A

1,9010C/9012B

LH

RM

RM

NH

LH

03/21/18 08:00

03/21/18 15:35

03/21/18 15:35

03/21/18 18:40

03/22/18 15:25

General Chemistry - Westborough Lab for sample(s): 03,06 Batch: WG1099068-1

General Chemistry - Westborough Lab for sample(s): 03,06,08 Batch: WG1099291-1




MDL

0.20

10.

10.

0.16

0.20

Serial_No:04021817:02

Page 104 of 115

pH

Cyanide, Total

Sulfide, Reactive

Cyanide, Reactive


Cyanide, Total

100

63

90

43

98

70

-

55

-

-

-

77

99-101

80-120

60-125

30-125

80-120

80-120

-

14

-

-

-

1

35

40

40

20

35

ParameterLCS

%RecoveryLCSD

%Recovery%Recovery


General Chemistry - Westborough Lab Associated sample(s): 03,06,08 Batch: WG1098664-1

General Chemistry - Westborough Lab Associated sample(s): 03,06 Batch: WG1099068-2 WG1099068-3




General Chemistry - Westborough Lab Associated sample(s): 08 Batch: WG1099600-2 WG1099600-3


Project Name:

Project Number:

Lab Number:

Report Date:

NFTA

17005.02

L1809330

04/02/18

Qual Qual

Q

Q

Q

Q

Qual

Serial_No:04021817:02

Page 105 of 115

Cyanide, Total


Cyanide, Total

ND

ND

ND

12

910

11

98

95

94

12

-

11

99

-

98

75-125

75-125

75-125

0

-

0

35

20

35


MS Found

MS%Recovery

MSD Found

MSD %Recovery

RecoveryLimits RPD

RPD Limits

General Chemistry - Westborough Lab Associated sample(s): 03,06 QC Batch ID: WG1099068-4 WG1099068-5 QC Sample: L1809454-03 Client ID: MS Sample

General Chemistry - Westborough Lab Associated sample(s): 03,06,08 QC Batch ID: WG1099354-4 QC Sample: L1809330-08 Client ID: BH7/8-18

General Chemistry - Westborough Lab Associated sample(s): 08 QC Batch ID: WG1099600-4 WG1099600-5 QC Sample: L1809729-10 Client ID: MS Sample

12

953

12

MS Added


Project Name:

Project Number:

Lab Number:

Report Date:

NFTA

17005.02

L1809330

04/02/18

Qual Qual Qual

Serial_No:04021817:02

Page 106 of 115

pH

Solids, Total

Sulfide, Reactive

Cyanide, Reactive


6.6

87.2

ND

ND

ND

6.6

87.4

ND

ND

ND

SU

%

mg/kg

mg/kg

mg/kg

0

0

NC

NC

NC

5

20

40

40

20


General Chemistry - Westborough Lab Associated sample(s): 03,06,08 QC Batch ID: WG1098664-2 QC Sample: L1809256-01 Client ID: DUP Sample

General Chemistry - Westborough Lab Associated sample(s): 01,03-04,06-08 QC Batch ID: WG1098802-1 QC Sample: L1809345-01 Client ID: DUP Sample



General Chemistry - Westborough Lab Associated sample(s): 03,06,08 QC Batch ID: WG1099354-6 QC Sample: L1809330-08 Client ID: BH7/8-18

NFTA

17005.02

Project Name:

Project Number:

L1809330Lab Number:

Report Date:


04/02/18

Qual

Serial_No:04021817:02

Page 107 of 115


L1809330-01A

L1809330-01X

L1809330-01Y

L1809330-01Z

L1809330-02A

L1809330-02S

L1809330-02T

L1809330-03A

L1809330-03A1

L1809330-03B

L1809330-03C

L1809330-03D

L1809330-03E

L1809330-03S

L1809330-03T

L1809330-03W

L1809330-03X


















A

A

A

A

A

A

A

A

A

A

A

A

A

A

A

A

A

NA

NA

NA

NA

NA

NA

NA

NA

NA

NA

NA

NA

NA

NA

NA

NA

NA

3.1

3.1

3.1

3.1

3.1

3.1

3.1

3.1

3.1

3.1

3.1

3.1

3.1

3.1

3.1

3.1

3.1

Y

Y

Y

Y

Y

Y

Y

Y

Y

Y

Y

Y

Y

Y

Y

Y

Y

Absent

Absent

Absent

Absent

Absent

Absent

Absent

Absent

Absent

Absent

Absent

Absent

Absent

Absent

Absent

Absent

Absent


NFTA

17005.02

NYTCL-8260-R2(14),TS(7)

NYTCL-8260-R2(14)

NYTCL-8260-R2(14)

NYTCL-8260-R2(14)

TCLP-EXT-ZHE(14)

TCLP-VOA(14)

TCLP-VOA(14)

TS(7)

TS(7)


TCLP-EXT-ZHE(14)

IGNIT-1030(14),NYTCL-8270(14),REACTS(14),TCN-9010(14),PH-9045(1),NYTCL-8081(14),HERB-8151(14),NYTCL-8082(14),REACTCN(14),HEXCR-7196(30)


TCLP-VOA(14)

TCLP-VOA(14)



Project Name:

Project Number:

L1809330Lab Number:

Report Date:




Analysis(*)

04/02/18


23-MAR-18 08:56

23-MAR-18 08:56

FrozenDate/Time

FinalpH

Initial pH

Serial_No:04021817:02

Page 108 of 115


L1809330-03X9

L1809330-04A

L1809330-04X

L1809330-04Y

L1809330-04Z

L1809330-05A

L1809330-05S

L1809330-05T

L1809330-06A

L1809330-06A1

L1809330-06B

L1809330-06C

L1809330-06D

L1809330-06E

L1809330-06S

L1809330-06T

L1809330-06W

L1809330-06X

L1809330-06X9

L1809330-07A

L1809330-07B

L1809330-07S

Tumble Vessel


















Tumble Vessel




A

A

A

A

A

A

A

A

A

A

A

A

A

A

A

A

A

A

A

A

A

A

NA

NA

NA

NA

NA

NA

NA

NA

NA

NA

NA

NA

NA

NA

NA

NA

NA

NA

NA

NA

NA

NA

3.1

3.1

3.1

3.1

3.1

3.1

3.1

3.1

3.1

3.1

3.1

3.1

3.1

3.1

3.1

3.1

3.1

3.1

3.1

3.1

3.1

3.1

Y

Y

Y

Y

Y

Y

Y

Y

Y

Y

Y

Y

Y

Y

Y

Y

Y

Y

Y

Y

Y

Y

Absent

Absent

Absent

Absent

Absent

Absent

Absent

Absent

Absent

Absent

Absent

Absent

Absent

Absent

Absent

Absent

Absent

Absent

Absent

Absent

Absent

Absent

NFTA

17005.02

-

NYTCL-8260-R2(14),TS(7)

NYTCL-8260-R2(14)

NYTCL-8260-R2(14)

NYTCL-8260-R2(14)

TCLP-EXT-ZHE(14)

TCLP-VOA(14)

TCLP-VOA(14)

TS(7)

TS(7)


TCLP-EXT-ZHE(14)



TCLP-VOA(14)

TCLP-VOA(14)



-

NYTCL-8260-R2(14),TS(7)

TCLP-EXT-ZHE(14)

TCLP-VOA(14)

Project Name:

Project Number:

L1809330Lab Number:

Report Date:



Analysis(*)

04/02/18

23-MAR-18 08:56

23-MAR-18 08:56

FrozenDate/Time

FinalpH

Initial pH

Serial_No:04021817:02

Page 109 of 115


L1809330-07T

L1809330-07X

L1809330-07Y

L1809330-07Z

L1809330-08A

L1809330-08A1

L1809330-08B

L1809330-08C

L1809330-08D

L1809330-08E

L1809330-08S

L1809330-08T

L1809330-08W

L1809330-08W1

L1809330-08X

L1809330-08X9

L1809330-09A
















Tumble Vessel

Vial HCl preserved

A

A

A

A

A

A

A

A

A

A

A

A

A

A

A

A

A

NA

NA

NA

NA

NA

NA

NA

NA

NA

NA

NA

NA

NA

NA

NA

NA

NA

3.1

3.1

3.1

3.1

3.1

3.1

3.1

3.1

3.1

3.1

3.1

3.1

3.1

3.1

3.1

3.1

3.1

Y

Y

Y

Y

Y

Y

Y

Y

Y

Y

Y

Y

Y

Y

Y

Y

Y

Absent

Absent

Absent

Absent

Absent

Absent

Absent

Absent

Absent

Absent

Absent

Absent

Absent

Absent

Absent

Absent

Absent

NFTA

17005.02

TCLP-VOA(14)

NYTCL-8260-R2(14)

NYTCL-8260-R2(14)

NYTCL-8260-R2(14)

TS(7)

TS(7)


TCLP-EXT-ZHE(14)



TCLP-VOA(14)

TCLP-VOA(14)




-

NYTCL-8260(14)

Project Name:

Project Number:

L1809330Lab Number:

Report Date:



Analysis(*)

04/02/18

23-MAR-18 08:56

23-MAR-18 08:56

FrozenDate/Time

FinalpH

Initial pH

Serial_No:04021817:02

Page 110 of 115


GLOSSARY

Project Name:

Project Number:

Lab Number:

Report Date:

L1809330NFTA

17005.02 04/02/18

Acronyms

EDL

EPA

LCS

LCSD

LFB

MDL

MS

MSD

NA

NC

NDPA/DPA

NI

NP

RL

RPD

SRM

STLP

TIC




Not Applicable.


Not Ignitable.




-

-

-

-

-

-

-

-

-

-

-

-

-

-

-

-

-

-

Terms


Data Qualifiers

A

B

-

-




-

Footnotes

Serial_No:04021817:02

Page 111 of 115


Project Name:

Project Number:

Lab Number:

Report Date:

L1809330NFTA

17005.02 04/02/18

Data Qualifiers

C

D

E

G

H

I

M

NJ

P

Q

R

RE

S

-

-

-

-

-

-

-

-

-

-

-

-

-









J

ND

-

-


Serial_No:04021817:02

Page 112 of 115




1

107

121

125





Project Name:

Project Number:

Lab Number:

Report Date:

L1809330NFTA

17005.02

REFERENCES

04/02/18

Serial_No:04021817:02

Page 113 of 115










Serial_No:04021817:02

Page 114 of 115

Serial_No:04021817:02

Page 115 of 115

L1811425


17005-02

NFTA

Client:

Project Name:

Project Number:

04/16/18


Lab Number:

Report Date:


95 Perry Street

Suite 300

Andrew KlimekATTN:

ANALYTICAL REPORT


Buffalo, NY 14203

(716) 206-5100Phone:


Serial_No:04161816:43

Page 1 of 118

L1811425-01

L1811425-02

L1811425-03

L1811425-04

L1811425-05

Alpha Sample ID

BH9-18

BH10-18

BH10-18

BH13-18

TRIP BLANK

Client ID

AMTRAK-EXCHANGE ST.

AMTRAK-EXCHANGE ST.

AMTRAK-EXCHANGE ST.

AMTRAK-EXCHANGE ST.

AMTRAK-EXCHANGE ST.

Sample Location

NFTA

17005-02



L181142504/16/18

04/02/18 08:40

04/02/18 13:10

04/02/18 13:50

04/03/18 11:45

04/02/18 00:00


SOIL

SOIL

SOIL

SOIL

WATER

04/03/18

04/03/18

04/03/18

04/03/18

04/03/18

Serial_No:04161816:43

Page 2 of 118

NFTA

17005-02

Project Name:

Project Number:

Lab Number:


04/16/18

Case Narrative






















HOLD POLICY






Serial_No:04161816:43

Page 3 of 118


NFTA

17005-02

Project Name:

Project Number:

Lab Number:


04/16/18

Report Submission


MDL column.

Volatile Organics

L1811425-01, -02 and -04: Any reported concentrations that are below 200 ug/kg may be biased low due to

the sample not being collected according to 5035-L/5035A-L low-level specifications.

Cyanide, Total

The WG1103345-2/-3 LCS/LCSD recoveries (62%/53%), associated with L1811425-01, -03 and -04, are

outside our in-house acceptance criteria, but within the vendor-certified acceptance limits. The results of the

original analyses are reported.




Serial_No:04161816:43

Page 4 of 118

ORGANICS

Serial_No:04161816:43

Page 5 of 118

VOLATILES

Serial_No:04161816:43

Page 6 of 118

FF

Chloroform


Tetrachloroethene

Chlorobenzene

1,2-Dichloroethane

Benzene

Vinyl chloride

1,1-Dichloroethene

Trichloroethene

1,4-Dichlorobenzene

2-Butanone


ND

ND

ND

ND

ND

ND

ND

ND

ND

ND

ND

ug/l

ug/l

ug/l

ug/l

ug/l

ug/l

ug/l

ug/l

ug/l

ug/l

ug/l

10

10

10

10

10

10

10

10

10

10

10

Qualifier Units RL


SAMPLE RESULTS

Project Name:

Project Number:

Lab Number:

Report Date:

NFTA

17005-02

L1811425

7.5

5.0

5.0

5.0

5.0

5.0

10

5.0

5.0

25

50


Toluene-d8



94

108

106

94

70-130

70-130

70-130

70-130


04/16/18


AMTRAK-EXCHANGE ST.Sample Location:

L1811425-01Lab ID:



1,8260C04/13/18 09:25MM


84%Percent Solids:

MDL

2.2

1.3

1.8

1.8

1.3

1.6

0.71

1.7

1.8

1.9

19.

Sample Depth:

Serial_No:04161816:43

Page 7 of 118

Methylene chloride

1,1-Dichloroethane

Chloroform


Tetrachloroethene

Chlorobenzene

1,2-Dichloroethane


Benzene

Toluene

Ethylbenzene

Vinyl chloride

1,1-Dichloroethene


Trichloroethene

1,2-Dichlorobenzene

1,3-Dichlorobenzene

1,4-Dichlorobenzene


p/m-Xylene

o-Xylene


Acetone

2-Butanone

n-Butylbenzene

sec-Butylbenzene

tert-Butylbenzene

n-Propylbenzene

Parameter Result

J

Dilution Factor

ND

ND

ND

ND

ND

ND

ND

ND

ND

0.30

ND

ND

ND

ND

ND

ND

ND

ND

ND

ND

ND

ND

36

ND

ND

ND

ND

ND

ug/kg

ug/kg

ug/kg

ug/kg

ug/kg

ug/kg

ug/kg

ug/kg

ug/kg

ug/kg

ug/kg

ug/kg

ug/kg

ug/kg

ug/kg

ug/kg

ug/kg

ug/kg

ug/kg

ug/kg

ug/kg

ug/kg

ug/kg

ug/kg

ug/kg

ug/kg

ug/kg

ug/kg

1

1

1

1

1

1

1

1

1

1

1

1

1

1

1

1

1

1

1

1

1

1

1

1

1

1

1

1

Qualifier Units RL


SAMPLE RESULTS

Project Name:

Project Number:

Lab Number:

Report Date:

NFTA

17005-02

L1811425

12

1.8

1.8

1.2

1.2

1.2

1.2

1.2

1.2

1.8

1.2

2.4

1.2

1.8

1.2

5.9

5.9

5.9

2.4

2.4

2.4

1.2

12

12

1.2

1.2

5.9

1.2

04/16/18



L1811425-01Lab ID:



1,8260C04/10/18 13:25JC 84%Percent Solids:

MDL

2.0

0.32

0.44

0.41

0.36

0.41

0.29

0.41

0.23

0.23

0.20

0.37

0.44

0.28

0.36

0.22

0.26

0.22

0.18

0.42

0.40

0.40

2.7

0.82

0.27

0.26

0.29

0.25

Sample Depth:

Serial_No:04161816:43

Page 8 of 118



1,4-Dioxane


ND

ND

ND

ug/kg

ug/kg

ug/kg

1

1

1

Qualifier Units RL


SAMPLE RESULTS

Project Name:

Project Number:

Lab Number:

Report Date:

NFTA

17005-02

L1811425

5.9

5.9

47


Toluene-d8



88

91

80

106

70-130

70-130

70-130

70-130


04/16/18



L1811425-01Lab ID:


MDL

0.19

0.22

17.

Sample Depth:

Serial_No:04161816:43

Page 9 of 118

Chloroform


Tetrachloroethene

Chlorobenzene

1,2-Dichloroethane

Benzene

Vinyl chloride

1,1-Dichloroethene

Trichloroethene

1,4-Dichlorobenzene

2-Butanone


ND

ND

ND

ND

ND

ND

ND

ND

ND

ND

ND

ug/l

ug/l

ug/l

ug/l

ug/l

ug/l

ug/l

ug/l

ug/l

ug/l

ug/l

10

10

10

10

10

10

10

10

10

10

10

Qualifier Units RL


SAMPLE RESULTS

Project Name:

Project Number:

Lab Number:

Report Date:

NFTA

17005-02

L1811425

7.5

5.0

5.0

5.0

5.0

5.0

10

5.0

5.0

25

50


Toluene-d8



93

111

93

89

70-130

70-130

70-130

70-130


04/16/18



L1811425-02Lab ID:



1,8260C04/13/18 09:59MM


55%Percent Solids:

MDL

2.2

1.3

1.8

1.8

1.3

1.6

0.71

1.7

1.8

1.9

19.

Sample Depth:

Serial_No:04161816:43

Page 10 of 118

Methylene chloride

1,1-Dichloroethane

Chloroform


Tetrachloroethene

Chlorobenzene

1,2-Dichloroethane


Benzene

Toluene

Ethylbenzene

Vinyl chloride

1,1-Dichloroethene


Trichloroethene

1,2-Dichlorobenzene

1,3-Dichlorobenzene

1,4-Dichlorobenzene


p/m-Xylene

o-Xylene


Acetone

2-Butanone

n-Butylbenzene

sec-Butylbenzene

tert-Butylbenzene

n-Propylbenzene


ND

ND

ND

ND

ND

ND

ND

ND

ND

ND

ND

ND

ND

ND

ND

ND

ND

ND

ND

ND

ND

ND

240

48

ND

ND

ND

ND

ug/kg

ug/kg

ug/kg

ug/kg

ug/kg

ug/kg

ug/kg

ug/kg

ug/kg

ug/kg

ug/kg

ug/kg

ug/kg

ug/kg

ug/kg

ug/kg

ug/kg

ug/kg

ug/kg

ug/kg

ug/kg

ug/kg

ug/kg

ug/kg

ug/kg

ug/kg

ug/kg

ug/kg

1

1

1

1

1

1

1

1

1

1

1

1

1

1

1

1

1

1

1

1

1

1

1

1

1

1

1

1

Qualifier Units RL


SAMPLE RESULTS

Project Name:

Project Number:

Lab Number:

Report Date:

NFTA

17005-02

L1811425

17

2.6

2.6

1.7

1.7

1.7

1.7

1.7

1.7

2.6

1.7

3.4

1.7

2.6

1.7

8.6

8.6

8.6

3.4

3.4

3.4

1.7

17

17

1.7

1.7

8.6

1.7

04/16/18



L1811425-02Lab ID:




MDL

2.8

0.46

0.64

0.59

0.52

0.60

0.42

0.60

0.33

0.34

0.29

0.54

0.64

0.41

0.52

0.31

0.38

0.31

0.26

0.60

0.58

0.59

3.9

1.2

0.39

0.37

0.42

0.37

Sample Depth:

Serial_No:04161816:43

Page 11 of 118



1,4-Dioxane


ND

ND

ND

ug/kg

ug/kg

ug/kg

1

1

1

Qualifier Units RL


SAMPLE RESULTS

Project Name:

Project Number:

Lab Number:

Report Date:

NFTA

17005-02

L1811425

8.6

8.6

69


Toluene-d8



91

96

93

108

70-130

70-130

70-130

70-130


04/16/18



L1811425-02Lab ID:


MDL

0.28

0.32

25.

Sample Depth:

Serial_No:04161816:43

Page 12 of 118

Chloroform


Tetrachloroethene

Chlorobenzene

1,2-Dichloroethane

Benzene

Vinyl chloride

1,1-Dichloroethene

Trichloroethene

1,4-Dichlorobenzene

2-Butanone


ND

ND

ND

ND

ND

ND

ND

ND

ND

ND

ND

ug/l

ug/l

ug/l

ug/l

ug/l

ug/l

ug/l

ug/l

ug/l

ug/l

ug/l

10

10

10

10

10

10

10

10

10

10

10

Qualifier Units RL


SAMPLE RESULTS

Project Name:

Project Number:

Lab Number:

Report Date:

NFTA

17005-02

L1811425

7.5

5.0

5.0

5.0

5.0

5.0

10

5.0

5.0

25

50


Toluene-d8



96

108

106

95

70-130

70-130

70-130

70-130


04/16/18



L1811425-04Lab ID:



1,8260C04/13/18 10:32MM


85%Percent Solids:

MDL

2.2

1.3

1.8

1.8

1.3

1.6

0.71

1.7

1.8

1.9

19.

Sample Depth:

Serial_No:04161816:43

Page 13 of 118

Methylene chloride

1,1-Dichloroethane

Chloroform


Tetrachloroethene

Chlorobenzene

1,2-Dichloroethane


Benzene

Toluene

Ethylbenzene

Vinyl chloride

1,1-Dichloroethene


Trichloroethene

1,2-Dichlorobenzene

1,3-Dichlorobenzene

1,4-Dichlorobenzene


p/m-Xylene

o-Xylene


Acetone

2-Butanone

n-Butylbenzene

sec-Butylbenzene

tert-Butylbenzene

n-Propylbenzene

Parameter Result

J

J

Dilution Factor

ND

ND

ND

ND

ND

ND

ND

ND

ND

0.20

ND

ND

ND

ND

ND

ND

ND

ND

ND

ND

ND

ND

4.4

ND

ND

ND

ND

ND

ug/kg

ug/kg

ug/kg

ug/kg

ug/kg

ug/kg

ug/kg

ug/kg

ug/kg

ug/kg

ug/kg

ug/kg

ug/kg

ug/kg

ug/kg

ug/kg

ug/kg

ug/kg

ug/kg

ug/kg

ug/kg

ug/kg

ug/kg

ug/kg

ug/kg

ug/kg

ug/kg

ug/kg

1

1

1

1

1

1

1

1

1

1

1

1

1

1

1

1

1

1

1

1

1

1

1

1

1

1

1

1

Qualifier Units RL


SAMPLE RESULTS

Project Name:

Project Number:

Lab Number:

Report Date:

NFTA

17005-02

L1811425

7.6

1.1

1.1

0.76

0.76

0.76

0.76

0.76

0.76

1.1

0.76

1.5

0.76

1.1

0.76

3.8

3.8

3.8

1.5

1.5

1.5

0.76

7.6

7.6

0.76

0.76

3.8

0.76

04/16/18



L1811425-04Lab ID:




MDL

1.2

0.20

0.28

0.26

0.23

0.26

0.19

0.27

0.15

0.15

0.13

0.24

0.28

0.18

0.23

0.14

0.17

0.14

0.12

0.27

0.26

0.26

1.7

0.52

0.17

0.16

0.19

0.16

Sample Depth:

Serial_No:04161816:43

Page 14 of 118



1,4-Dioxane


ND

ND

ND

ug/kg

ug/kg

ug/kg

1

1

1

Qualifier Units RL


SAMPLE RESULTS

Project Name:

Project Number:

Lab Number:

Report Date:

NFTA

17005-02

L1811425

3.8

3.8

30


Toluene-d8



86

94

90

102

70-130

70-130

70-130

70-130


04/16/18



L1811425-04Lab ID:


MDL

0.12

0.14

11.

Sample Depth:

Serial_No:04161816:43

Page 15 of 118

Methylene chloride

1,1-Dichloroethane

Chloroform


Tetrachloroethene

Chlorobenzene

1,2-Dichloroethane


Benzene

Toluene

Ethylbenzene

Vinyl chloride

1,1-Dichloroethene


Trichloroethene

1,2-Dichlorobenzene

1,3-Dichlorobenzene

1,4-Dichlorobenzene


p/m-Xylene

o-Xylene


Acetone

2-Butanone

n-Butylbenzene

sec-Butylbenzene

tert-Butylbenzene

n-Propylbenzene


ND

ND

ND

ND

ND

ND

ND

ND

ND

ND

ND

ND

ND

ND

ND

ND

ND

ND

ND

ND

ND

ND

ND

ND

ND

ND

ND

ND

ug/l

ug/l

ug/l

ug/l

ug/l

ug/l

ug/l

ug/l

ug/l

ug/l

ug/l

ug/l

ug/l

ug/l

ug/l

ug/l

ug/l

ug/l

ug/l

ug/l

ug/l

ug/l

ug/l

ug/l

ug/l

ug/l

ug/l

ug/l

1

1

1

1

1

1

1

1

1

1

1

1

1

1

1

1

1

1

1

1

1

1

1

1

1

1

1

1

Qualifier Units RL


SAMPLE RESULTS

Project Name:

Project Number:

Lab Number:

Report Date:

NFTA

17005-02

L1811425

2.5

2.5

2.5

0.50

0.50

2.5

0.50

2.5

0.50

2.5

2.5

1.0

0.50

2.5

0.50

2.5

2.5

2.5

2.5

2.5

2.5

2.5

5.0

5.0

2.5

2.5

2.5

2.5

04/16/18



L1811425-05Lab ID:



1,8260C04/12/18 18:08AD

MDL

0.70

0.70

0.70

0.13

0.18

0.70

0.13

0.70

0.16

0.70

0.70

0.07

0.17

0.70

0.18

0.70

0.70

0.70

0.70

0.70

0.70

0.70

1.5

1.9

0.70

0.70

0.70

0.70

Sample Depth:

Serial_No:04161816:43

Page 16 of 118



1,4-Dioxane


ND

ND

ND

ug/l

ug/l

ug/l

1

1

1

Qualifier Units RL


SAMPLE RESULTS

Project Name:

Project Number:

Lab Number:

Report Date:

NFTA

17005-02

L1811425

2.5

2.5

250


Toluene-d8



105

103

103

93

70-130

70-130

70-130

70-130


04/16/18



L1811425-05Lab ID:


MDL

0.70

0.70

61.

Sample Depth:

Serial_No:04161816:43

Page 17 of 118


Project Name:

Project Number:

Lab Number:

Report Date:

NFTA

17005-02

L1811425


Analytical Date:

04/16/18

Analyst: MV

Methylene chloride

1,1-Dichloroethane

Chloroform


Tetrachloroethene

Chlorobenzene

1,2-Dichloroethane


Benzene

Toluene

Ethylbenzene

Vinyl chloride

1,1-Dichloroethene


Trichloroethene

1,2-Dichlorobenzene

1,3-Dichlorobenzene

1,4-Dichlorobenzene


p/m-Xylene

o-Xylene


Acetone

2-Butanone

n-Butylbenzene

sec-Butylbenzene

tert-Butylbenzene

n-Propylbenzene


Parameter Result

ND

ND

ND

ND

ND

ND

ND

ND

ND

0.28

ND

ND

ND

ND

ND

ND

ND

ND

ND

ND

ND

ND

ND

ND

ND

ND

ND

ND

ND

RL

10

1.5

1.5

1.0

1.0

1.0

1.0

1.0

1.0

1.5

1.0

2.0

1.0

1.5

1.0

5.0

5.0

5.0

2.0

2.0

2.0

1.0

10

10

1.0

1.0

5.0

1.0

5.0

J

ug/kg

ug/kg

ug/kg

ug/kg

ug/kg

ug/kg

ug/kg

ug/kg

ug/kg

ug/kg

ug/kg

ug/kg

ug/kg

ug/kg

ug/kg

ug/kg

ug/kg

ug/kg

ug/kg

ug/kg

ug/kg

ug/kg

ug/kg

ug/kg

ug/kg

ug/kg

ug/kg

ug/kg

ug/kg

UnitsQualifier

Volatile Organics by 8260/5035 - Westborough Lab for sample(s): 01-02,04 Batch: WG1105131-5

MDL

1.6

0.27

0.37

0.34

0.30

0.35

0.25

0.35

0.19

0.20

0.17

0.32

0.37

0.24

0.30

0.18

0.22

0.18

0.15

0.35

0.34

0.34

2.3

0.69

0.23

0.22

0.25

0.22

0.16

Serial_No:04161816:43

Page 18 of 118


Project Name:

Project Number:

Lab Number:

Report Date:

NFTA

17005-02

L1811425


Analytical Date:

04/16/18

Analyst: MV


1,4-Dioxane

Parameter Result

ND

ND

RL

5.0

40

ug/kg

ug/kg

UnitsQualifier

Volatile Organics by 8260/5035 - Westborough Lab for sample(s): 01-02,04 Batch: WG1105131-5


Toluene-d8



92

92

81

104

70-130

70-130

70-130

70-130


Criteria

MDL

0.19

14.

Serial_No:04161816:43

Page 19 of 118


Project Name:

Project Number:

Lab Number:

Report Date:

NFTA

17005-02

L1811425


Analytical Date:

04/16/18

Analyst: NLK

Methylene chloride

1,1-Dichloroethane

Chloroform


Tetrachloroethene

Chlorobenzene

1,2-Dichloroethane


Benzene

Toluene

Ethylbenzene

Vinyl chloride

1,1-Dichloroethene


Trichloroethene

1,2-Dichlorobenzene

1,3-Dichlorobenzene

1,4-Dichlorobenzene


p/m-Xylene

o-Xylene


Acetone

2-Butanone

n-Butylbenzene

sec-Butylbenzene

tert-Butylbenzene

n-Propylbenzene


Parameter Result

ND

ND

ND

ND

ND

ND

ND

ND

ND

ND

ND

ND

ND

ND

ND

ND

ND

ND

ND

ND

ND

ND

ND

ND

ND

ND

ND

ND

ND

RL

2.5

2.5

2.5

0.50

0.50

2.5

0.50

2.5

0.50

2.5

2.5

1.0

0.50

2.5

0.50

2.5

2.5

2.5

2.5

2.5

2.5

2.5

5.0

5.0

2.5

2.5

2.5

2.5

2.5

ug/l

ug/l

ug/l

ug/l

ug/l

ug/l

ug/l

ug/l

ug/l

ug/l

ug/l

ug/l

ug/l

ug/l

ug/l

ug/l

ug/l

ug/l

ug/l

ug/l

ug/l

ug/l

ug/l

ug/l

ug/l

ug/l

ug/l

ug/l

ug/l

UnitsQualifier


MDL

0.70

0.70

0.70

0.13

0.18

0.70

0.13

0.70

0.16

0.70

0.70

0.07

0.17

0.70

0.18

0.70

0.70

0.70

0.70

0.70

0.70

0.70

1.5

1.9

0.70

0.70

0.70

0.70

0.70

Serial_No:04161816:43

Page 20 of 118


Project Name:

Project Number:

Lab Number:

Report Date:

NFTA

17005-02

L1811425


Analytical Date:

04/16/18

Analyst: NLK


1,4-Dioxane

Parameter Result

ND

ND

RL

2.5

250

ug/l

ug/l

UnitsQualifier



Toluene-d8



102

104

104

92

70-130

70-130

70-130

70-130


Criteria

MDL

0.70

61.

Serial_No:04161816:43

Page 21 of 118


Project Name:

Project Number:

Lab Number:

Report Date:

NFTA

17005-02

L1811425



04/16/18

Analyst: MM

Chloroform


Tetrachloroethene

Chlorobenzene

1,2-Dichloroethane

Benzene

Vinyl chloride

1,1-Dichloroethene

Trichloroethene

1,4-Dichlorobenzene

2-Butanone

Parameter Result

ND

ND

ND

ND

ND

ND

ND

ND

ND

ND

ND

RL

7.5

5.0

5.0

5.0

5.0

5.0

10

5.0

5.0

25

50

ug/l

ug/l

ug/l

ug/l

ug/l

ug/l

ug/l

ug/l

ug/l

ug/l

ug/l

UnitsQualifier

TCLP Volatiles by EPA 1311 - Westborough Lab for sample(s): 01-02,04 Batch: WG1106264-5


Toluene-d8



95

109

104

93

70-130

70-130

70-130

70-130


Criteria


MDL

2.2

1.3

1.8

1.8

1.3

1.6

0.71

1.7

1.8

1.9

19.

Serial_No:04161816:43

Page 22 of 118

Methylene chloride

1,1-Dichloroethane

Chloroform


Tetrachloroethene

Chlorobenzene

1,2-Dichloroethane


Benzene

Toluene

Ethylbenzene

Vinyl chloride

1,1-Dichloroethene


Trichloroethene

1,2-Dichlorobenzene

1,3-Dichlorobenzene

1,4-Dichlorobenzene


p/m-Xylene

o-Xylene


Acetone

92

96

84

89

98

93

86

81

88

84

80

97

90

90

86

99

97

95

84

94

94

93

185

88

88

78

76

84

86

83

70

79

73

71

80

75

78

75

95

92

91

81

84

86

84

123

70-130

70-130

70-130

70-130

70-130

70-130

70-130

70-130

70-130

70-130

70-130

67-130

65-135

70-130

70-130

70-130

70-130

70-130

66-130

70-130

70-130

70-130

54-140

4

9

7

16

15

8

4

15

11

14

12

19

18

14

14

4

5

4

4

11

9

10

40

30

30

30

30

30

30

30

30

30

30

30

30

30

30

30

30

30

30

30

30

30

30

30

ParameterLCS

%RecoveryLCSD

%Recovery%Recovery

Limits RPDRPD

Limits

Volatile Organics by 8260/5035 - Westborough Lab Associated sample(s): 01-02,04 Batch: WG1105131-3 WG1105131-4


Project Name:

Project Number:

Lab Number:

Report Date:

NFTA

17005-02

L1811425

04/16/18

Qual Qual

Q

Qual

Q

Serial_No:04161816:43

Page 23 of 118

2-Butanone

n-Butylbenzene

sec-Butylbenzene

tert-Butylbenzene

n-Propylbenzene



1,4-Dioxane

140

78

87

86

76

84

86

125

98

69

75

75

67

75

79

117

70-130

70-130

70-130

70-130

70-130

70-130

70-130

65-136

35

12

15

14

13

11

8

7

30

30

30

30

30

30

30

30

ParameterLCS

%RecoveryLCSD

%Recovery%Recovery

Limits RPDRPD

Limits

Volatile Organics by 8260/5035 - Westborough Lab Associated sample(s): 01-02,04 Batch: WG1105131-3 WG1105131-4


Project Name:

Project Number:

Lab Number:

Report Date:

NFTA

17005-02

L1811425


889182108

70-13070-13070-13070-130

889282108


04/16/18

AcceptanceCriteria

Qual Qual

Q

Q

Q

Qual

Q

Serial_No:04161816:43

Page 24 of 118

Methylene chloride

1,1-Dichloroethane

Chloroform


Tetrachloroethene

Chlorobenzene

1,2-Dichloroethane


Benzene

Toluene

Ethylbenzene

Vinyl chloride

1,1-Dichloroethene


Trichloroethene

1,2-Dichlorobenzene

1,3-Dichlorobenzene

1,4-Dichlorobenzene


p/m-Xylene

o-Xylene


Acetone

110

120

100

93

91

100

110

100

100

100

100

130

100

100

96

100

100

100

100

105

105

100

110

110

120

100

93

92

100

110

99

100

110

100

130

100

100

95

100

99

100

110

105

105

99

120

70-130

70-130

70-130

63-132

70-130

75-130

70-130

67-130

70-130

70-130

70-130

55-140

61-145

70-130

70-130

70-130

70-130

70-130

63-130

70-130

70-130

70-130

58-148

0

0

0

0

1

0

0

1

0

10

0

0

0

0

1

0

1

0

10

0

0

1

9

20

20

20

20

20

20

20

20

20

20

20

20

20

20

20

20

20

20

20

20

20

20

20

ParameterLCS

%RecoveryLCSD

%Recovery%Recovery

Limits RPDRPD

Limits



Project Name:

Project Number:

Lab Number:

Report Date:

NFTA

17005-02

L1811425

04/16/18

Qual Qual Qual

Serial_No:04161816:43

Page 25 of 118

2-Butanone

n-Butylbenzene

sec-Butylbenzene

tert-Butylbenzene

n-Propylbenzene



1,4-Dioxane

130

110

110

100

110

110

98

68

130

110

110

110

110

110

99

68

63-138

53-136

70-130

70-130

69-130

64-130

70-130

56-162

0

0

0

10

0

0

1

0

20

20

20

20

20

20

20

20

ParameterLCS

%RecoveryLCSD

%Recovery%Recovery

Limits RPDRPD

Limits



Project Name:

Project Number:

Lab Number:

Report Date:

NFTA

17005-02

L1811425


10110210393

70-13070-13070-13070-130

10310310293


04/16/18

AcceptanceCriteria

Qual Qual Qual

Serial_No:04161816:43

Page 26 of 118

Chloroform


Tetrachloroethene

Chlorobenzene

1,2-Dichloroethane

Benzene

Vinyl chloride

1,1-Dichloroethene

Trichloroethene

1,4-Dichlorobenzene

2-Butanone

100

90

120

110

94

100

93

83

100

100

120

94

88

110

100

87

100

96

87

98

100

93

70-130

63-132

70-130

75-130

70-130

70-130

55-140

61-145

70-130

70-130

63-138

6

2

9

10

8

0

3

5

2

0

25

20

20

20

25

20

25

20

25

25

20

20

ParameterLCS

%RecoveryLCSD

%Recovery%Recovery

Limits RPDRPD

Limits

TCLP Volatiles by EPA 1311 - Westborough Lab Associated sample(s): 01-02,04 Batch: WG1106264-3 WG1106264-4


Project Name:

Project Number:

Lab Number:

Report Date:

NFTA

17005-02

L1811425


9511010894

70-13070-13070-13070-130

9510910994


04/16/18

AcceptanceCriteria

Qual Qual Qual

Q

Serial_No:04161816:43

Page 27 of 118

SEMIVOLATILES

Serial_No:04161816:43

Page 28 of 118

FF

Hexachlorobenzene

2,4-Dinitrotoluene

Hexachlorobutadiene

Hexachloroethane

Nitrobenzene


Pentachlorophenol

2-Methylphenol



Pyridine


ND

ND

ND

ND

ND

ND

ND

ND

ND

ND

ND

ug/l

ug/l

ug/l

ug/l

ug/l

ug/l

ug/l

ug/l

ug/l

ug/l

ug/l

1

1

1

1

1

1

1

1

1

1

1

Qualifier Units RL


SAMPLE RESULTS

Project Name:

Project Number:

Lab Number:

Report Date:

NFTA

17005-02

L1811425

10

25

10

10

10

25

50

25

25

25

18

2-Fluorophenol

Phenol-d6

Nitrobenzene-d5

2-Fluorobiphenyl


4-Terphenyl-d14

76

78

69

69

92

78

21-120

10-120

23-120

15-120

10-120

33-120


04/16/18



L1811425-01Lab ID:




1,8270D04/12/18 09:47TT



84%Percent Solids:

MDL

2.9

4.2

3.6

3.4

3.8

3.4

17.

5.1

5.6

3.6

9.4

Sample Depth:

Serial_No:04161816:43

Page 29 of 118

Acenaphthene

Hexachlorobenzene

Fluoranthene

Naphthalene

Benzo(a)anthracene

Benzo(a)pyrene



Chrysene

Acenaphthylene

Anthracene

Benzo(ghi)perylene

Fluorene

Phenanthrene



Pyrene

Dibenzofuran

Pentachlorophenol

Phenol

2-Methylphenol


Parameter Result

J

J

J

J

J

J

J

Dilution Factor

130

ND

1300

170

760

740

1000

290

810

120

350

420

150

980

98

450

1100

100

ND

ND

ND

37

ug/kg

ug/kg

ug/kg

ug/kg

ug/kg

ug/kg

ug/kg

ug/kg

ug/kg

ug/kg

ug/kg

ug/kg

ug/kg

ug/kg

ug/kg

ug/kg

ug/kg

ug/kg

ug/kg

ug/kg

ug/kg

ug/kg

1

1

1

1

1

1

1

1

1

1

1

1

1

1

1

1

1

1

1

1

1

1

Qualifier Units RL


SAMPLE RESULTS

Project Name:

Project Number:

Lab Number:

Report Date:

NFTA

17005-02

L1811425

160

120

120

200

120

160

120

120

120

160

120

160

200

120

120

160

120

200

160

200

200

280

04/16/18



L1811425-01Lab ID:




1,8270D04/11/18 00:07CB


84%Percent Solids:

MDL

20.

22.

23.

24.

22.

48.

33.

32.

20.

30.

38.

23.

19.

24.

23.

27.

20.

19.

43.

30.

30.

31.

Sample Depth:

Serial_No:04161816:43

Page 30 of 118



SAMPLE RESULTS

Project Name:

Project Number:

Lab Number:

Report Date:

NFTA

17005-02

L1811425

2-Fluorophenol

Phenol-d6

Nitrobenzene-d5

2-Fluorobiphenyl


4-Terphenyl-d14

58

90

85

77

42

65

25-120

10-120

23-120

30-120

10-136

18-120


04/16/18



L1811425-01Lab ID:


MDL

Sample Depth:

Serial_No:04161816:43

Page 31 of 118

Hexachlorobenzene

2,4-Dinitrotoluene

Hexachlorobutadiene

Hexachloroethane

Nitrobenzene


Pentachlorophenol

2-Methylphenol



Pyridine


ND

ND

ND

ND

ND

ND

ND

ND

ND

ND

ND

ug/l

ug/l

ug/l

ug/l

ug/l

ug/l

ug/l

ug/l

ug/l

ug/l

ug/l

1

1

1

1

1

1

1

1

1

1

1

Qualifier Units RL


SAMPLE RESULTS

Project Name:

Project Number:

Lab Number:

Report Date:

NFTA

17005-02

L1811425

10

25

10

10

10

25

50

25

25

25

18

2-Fluorophenol

Phenol-d6

Nitrobenzene-d5

2-Fluorobiphenyl


4-Terphenyl-d14

81

81

78

76

89

74

21-120

10-120

23-120

15-120

10-120

33-120


04/16/18



L1811425-03Lab ID:




1,8270D04/11/18 23:05CB



73%Percent Solids:

MDL

2.9

4.2

3.6

3.4

3.8

3.4

17.

5.1

5.6

3.6

9.4

Sample Depth:

Serial_No:04161816:43

Page 32 of 118

Acenaphthene

Hexachlorobenzene

Fluoranthene

Naphthalene

Benzo(a)anthracene

Benzo(a)pyrene



Chrysene

Acenaphthylene

Anthracene

Benzo(ghi)perylene

Fluorene

Phenanthrene



Pyrene

Dibenzofuran

Pentachlorophenol

Phenol

2-Methylphenol


Parameter Result

E

J

J

Dilution Factor

290

ND

9600

210

4700

3700

5200

1500

4100

1000

1300

2200

580

6100

490

2600

7900

450

ND

57

ND

340

ug/kg

ug/kg

ug/kg

ug/kg

ug/kg

ug/kg

ug/kg

ug/kg

ug/kg

ug/kg

ug/kg

ug/kg

ug/kg

ug/kg

ug/kg

ug/kg

ug/kg

ug/kg

ug/kg

ug/kg

ug/kg

ug/kg

1

1

1

1

1

1

1

1

1

1

1

1

1

1

1

1

1

1

1

1

1

1

Qualifier Units RL


SAMPLE RESULTS

Project Name:

Project Number:

Lab Number:

Report Date:

NFTA

17005-02

L1811425

180

130

130

220

130

180

130

130

130

180

130

180

220

130

130

180

130

220

180

220

220

320

04/16/18



L1811425-03Lab ID:




1,8270D04/10/18 23:40CB


73%Percent Solids:

MDL

23.

25.

26.

27.

25.

54.

38.

36.

23.

34.

44.

26.

22.

27.

26.

31.

22.

21.

49.

34.

34.

35.

Sample Depth:

Serial_No:04161816:43

Page 33 of 118



SAMPLE RESULTS

Project Name:

Project Number:

Lab Number:

Report Date:

NFTA

17005-02

L1811425

2-Fluorophenol

Phenol-d6

Nitrobenzene-d5

2-Fluorobiphenyl


4-Terphenyl-d14

115

133

122

113

108

100

25-120

10-120

23-120

30-120

10-136

18-120

Acceptance Criteria

Q

Q

Surrogate % Recovery Qualifier

04/16/18



L1811425-03Lab ID:


MDL

Sample Depth:

Serial_No:04161816:43

Page 34 of 118

Fluoranthene


8400 ug/kg 2

Qualifier Units RL


SAMPLE RESULTS

Project Name:

Project Number:

Lab Number:

Report Date:

NFTA

17005-02

L1811425

270

04/16/18



L1811425-03Lab ID:


D



1,8270D04/12/18 01:44CB


73%Percent Solids:

MDL

51.

Sample Depth:

Serial_No:04161816:43

Page 35 of 118

Hexachlorobenzene

2,4-Dinitrotoluene

Hexachlorobutadiene

Hexachloroethane

Nitrobenzene


Pentachlorophenol

2-Methylphenol



Pyridine


ND

ND

ND

ND

ND

ND

ND

ND

ND

ND

ND

ug/l

ug/l

ug/l

ug/l

ug/l

ug/l

ug/l

ug/l

ug/l

ug/l

ug/l

1

1

1

1

1

1

1

1

1

1

1

Qualifier Units RL


SAMPLE RESULTS

Project Name:

Project Number:

Lab Number:

Report Date:

NFTA

17005-02

L1811425

10

25

10

10

10

25

50

25

25

25

18

2-Fluorophenol

Phenol-d6

Nitrobenzene-d5

2-Fluorobiphenyl


4-Terphenyl-d14

72

70

68

66

78

68

21-120

10-120

23-120

15-120

10-120

33-120


04/16/18



L1811425-04Lab ID:




1,8270D04/11/18 23:31CB



85%Percent Solids:

MDL

2.9

4.2

3.6

3.4

3.8

3.4

17.

5.1

5.6

3.6

9.4

Sample Depth:

Serial_No:04161816:43

Page 36 of 118

Acenaphthene

Hexachlorobenzene

Fluoranthene

Naphthalene

Benzo(a)anthracene

Benzo(a)pyrene



Chrysene

Acenaphthylene

Anthracene

Benzo(ghi)perylene

Fluorene

Phenanthrene



Pyrene

Dibenzofuran

Pentachlorophenol

Phenol

2-Methylphenol


Parameter Result

J

J

J

J

Dilution Factor

58

ND

840

ND

350

280

400

120

340

ND

150

180

64

740

40

200

650

43

ND

ND

ND

ND

ug/kg

ug/kg

ug/kg

ug/kg

ug/kg

ug/kg

ug/kg

ug/kg

ug/kg

ug/kg

ug/kg

ug/kg

ug/kg

ug/kg

ug/kg

ug/kg

ug/kg

ug/kg

ug/kg

ug/kg

ug/kg

ug/kg

1

1

1

1

1

1

1

1

1

1

1

1

1

1

1

1

1

1

1

1

1

1

Qualifier Units RL


SAMPLE RESULTS

Project Name:

Project Number:

Lab Number:

Report Date:

NFTA

17005-02

L1811425

150

110

110

190

110

150

110

110

110

150

110

150

190

110

110

150

110

190

150

190

190

270

04/16/18



L1811425-04Lab ID:




1,8270D04/10/18 22:47CB


85%Percent Solids:

MDL

20.

21.

22.

23.

21.

46.

32.

30.

20.

29.

37.

22.

18.

23.

22.

27.

19.

18.

42.

29.

30.

30.

Sample Depth:

Serial_No:04161816:43

Page 37 of 118



SAMPLE RESULTS

Project Name:

Project Number:

Lab Number:

Report Date:

NFTA

17005-02

L1811425

2-Fluorophenol

Phenol-d6

Nitrobenzene-d5

2-Fluorobiphenyl


4-Terphenyl-d14

98

111

90

91

99

85

25-120

10-120

23-120

30-120

10-136

18-120


04/16/18



L1811425-04Lab ID:


MDL

Sample Depth:

Serial_No:04161816:43

Page 38 of 118


Project Name:

Project Number:

Lab Number:

Report Date:

NFTA

17005-02

L1811425



04/16/18

Analyst: CB

Acenaphthene

Hexachlorobenzene

Fluoranthene

Naphthalene

Benzo(a)anthracene

Benzo(a)pyrene



Chrysene

Acenaphthylene

Anthracene

Benzo(ghi)perylene

Fluorene

Phenanthrene



Pyrene

Dibenzofuran

Pentachlorophenol

Phenol

2-Methylphenol


Parameter Result

ND

ND

ND

ND

ND

ND

ND

ND

ND

ND

ND

ND

ND

ND

ND

ND

ND

ND

ND

ND

ND

ND

RL

130

98

98

160

98

130

98

98

98

130

98

130

160

98

98

130

98

160

130

160

160

240

ug/kg

ug/kg

ug/kg

ug/kg

ug/kg

ug/kg

ug/kg

ug/kg

ug/kg

ug/kg

ug/kg

ug/kg

ug/kg

ug/kg

ug/kg

ug/kg

ug/kg

ug/kg

ug/kg

ug/kg

ug/kg

ug/kg

UnitsQualifier

Semivolatile Organics by GC/MS - Westborough Lab for sample(s): 01,03-04 Batch: WG1104559-1

MDL

17.

18.

19.

20.

18.

40.

28.

26.

17.

25.

32.

19.

16.

20.

19.

23.

16.

15.

36.

25.

25.

26.

Serial_No:04161816:43

Page 39 of 118


Project Name:

Project Number:

Lab Number:

Report Date:

NFTA

17005-02

L1811425



04/16/18

Analyst: CB


Semivolatile Organics by GC/MS - Westborough Lab for sample(s): 01,03-04 Batch: WG1104559-1

2-Fluorophenol

Phenol-d6

Nitrobenzene-d5

2-Fluorobiphenyl


4-Terphenyl-d14

96

105

87

86

100

93

25-120

10-120

23-120

30-120

10-136

18-120


Criteria

MDL

Serial_No:04161816:43

Page 40 of 118


Project Name:

Project Number:

Lab Number:

Report Date:

NFTA

17005-02

L1811425



04/16/18

Analyst: TT

Hexachlorobenzene

2,4-Dinitrotoluene

Hexachlorobutadiene

Hexachloroethane

Nitrobenzene


Pentachlorophenol

2-Methylphenol



Pyridine

Parameter Result

ND

ND

ND

ND

ND

ND

ND

ND

ND

ND

ND

RL

10

25

10

10

10

25

50

25

25

25

18

ug/l

ug/l

ug/l

ug/l

ug/l

ug/l

ug/l

ug/l

ug/l

ug/l

ug/l

UnitsQualifier

TCLP Semivolatiles by EPA 1311 - Westborough Lab for sample(s): 01 Batch: WG1105470-1

2-Fluorophenol

Phenol-d6

Nitrobenzene-d5

2-Fluorobiphenyl


4-Terphenyl-d14

84

85

76

72

99

81

21-120

10-120

23-120

15-120

10-120

33-120


Criteria


MDL

2.9

4.2

3.6

3.4

3.8

3.4

17.

5.1

5.6

3.6

9.4

Serial_No:04161816:43

Page 41 of 118


Project Name:

Project Number:

Lab Number:

Report Date:

NFTA

17005-02

L1811425



04/16/18

Analyst: CB

Hexachlorobenzene

2,4-Dinitrotoluene

Hexachlorobutadiene

Hexachloroethane

Nitrobenzene


Pentachlorophenol

2-Methylphenol



Pyridine

Parameter Result

ND

ND

ND

ND

ND

ND

ND

ND

ND

ND

ND

RL

10

25

10

10

10

25

50

25

25

25

18

ug/l

ug/l

ug/l

ug/l

ug/l

ug/l

ug/l

ug/l

ug/l

ug/l

ug/l

UnitsQualifier

TCLP Semivolatiles by EPA 1311 - Westborough Lab for sample(s): 03-04 Batch: WG1105473-1

2-Fluorophenol

Phenol-d6

Nitrobenzene-d5

2-Fluorobiphenyl


4-Terphenyl-d14

81

80

73

74

88

72

21-120

10-120

23-120

15-120

10-120

33-120


Criteria


MDL

2.9

4.2

3.6

3.4

3.8

3.4

17.

5.1

5.6

3.6

9.4

Serial_No:04161816:43

Page 42 of 118

Acenaphthene

Hexachlorobenzene

Fluoranthene

Naphthalene

Benzo(a)anthracene

Benzo(a)pyrene



Chrysene

Acenaphthylene

Anthracene

Benzo(ghi)perylene

Fluorene

Phenanthrene



Pyrene

Dibenzofuran

Pentachlorophenol

Phenol

2-Methylphenol


96

96

100

96

100

103

103

99

100

102

100

103

100

100

101

106

98

97

89

98

106

112

99

102

104

94

107

111

110

109

105

102

103

110

103

103

107

113

101

101

94

98

109

112

31-137

40-140

40-140

40-140

40-140

40-140

40-140

40-140

40-140

40-140

40-140

40-140

40-140

40-140

40-140

40-140

35-142

40-140

17-109

26-90

30-130.

30-130

3

6

4

2

7

7

7

10

5

0

3

7

3

3

6

6

3

4

5

0

3

0

50

50

50

50

50

50

50

50

50

50

50

50

50

50

50

50

50

50

50

50

50

50

ParameterLCS

%RecoveryLCSD

%Recovery%Recovery

Limits RPDRPD

Limits

Semivolatile Organics by GC/MS - Westborough Lab Associated sample(s): 01,03-04 Batch: WG1104559-2 WG1104559-3


Project Name:

Project Number:

Lab Number:

Report Date:

NFTA

17005-02

L1811425

04/16/18

Qual Qual

Q Q

Qual

Serial_No:04161816:43

Page 43 of 118

ParameterLCS

%RecoveryLCSD

%Recovery%Recovery

Limits RPDRPD

Limits

Semivolatile Organics by GC/MS - Westborough Lab Associated sample(s): 01,03-04 Batch: WG1104559-2 WG1104559-3


Project Name:

Project Number:

Lab Number:

Report Date:

NFTA

17005-02

L1811425


96105878810087

25-12010-12023-12030-12010-13618-120

100107898911090


04/16/18

AcceptanceCriteria

Qual Qual Qual

Serial_No:04161816:43

Page 44 of 118

Hexachlorobenzene

2,4-Dinitrotoluene

Hexachlorobutadiene

Hexachloroethane

Nitrobenzene


Pentachlorophenol

2-Methylphenol



Pyridine

70

82

54

59

68

82

66

80

84

78

56

78

90

61

66

74

87

67

82

88

85

52

40-140

40-132

28-111

21-105

40-140

30-130

9-103

30-130

30-130

30-130

10-66

11

9

12

11

8

6

2

2

5

9

7

30

30

30

30

30

30

30

30

30

30

30

ParameterLCS

%RecoveryLCSD

%Recovery%Recovery

Limits RPDRPD

Limits

TCLP Semivolatiles by EPA 1311 - Westborough Lab Associated sample(s): 01 Batch: WG1105470-2 WG1105470-3


Project Name:

Project Number:

Lab Number:

Report Date:

NFTA

17005-02

L1811425


737766638771

21-12010-12023-12015-12010-12033-120

767969679172


04/16/18

AcceptanceCriteria

Qual Qual Qual

Serial_No:04161816:43

Page 45 of 118

Hexachlorobenzene

2,4-Dinitrotoluene

Hexachlorobutadiene

Hexachloroethane

Nitrobenzene


Pentachlorophenol

2-Methylphenol



Pyridine

81

89

82

76

86

92

77

90

97

95

48

84

90

87

84

88

90

80

89

96

99

36

40-140

40-132

28-111

21-105

40-140

30-130

9-103

30-130

30-130

30-130

10-66

4

1

6

10

2

2

4

1

1

4

29

30

30

30

30

30

30

30

30

30

30

30

ParameterLCS

%RecoveryLCSD

%Recovery%Recovery

Limits RPDRPD

Limits

TCLP Semivolatiles by EPA 1311 - Westborough Lab Associated sample(s): 03-04 Batch: WG1105473-2 WG1105473-3


Project Name:

Project Number:

Lab Number:

Report Date:

NFTA

17005-02

L1811425


858880789279

21-12010-12023-12015-12010-12033-120

859079779182


04/16/18

AcceptanceCriteria

Qual Qual Qual

Serial_No:04161816:43

Page 46 of 118

PCBS

Serial_No:04161816:43

Page 47 of 118

FF

Aroclor 1016

Aroclor 1221

Aroclor 1232

Aroclor 1242

Aroclor 1248

Aroclor 1254

Aroclor 1260

Aroclor 1262

Aroclor 1268

Parameter Result

J

J

Dilution Factor

ND

ND

ND

ND

ND

9.11

8.17

ND

ND

ug/kg

ug/kg

ug/kg

ug/kg

ug/kg

ug/kg

ug/kg

ug/kg

ug/kg

1

1

1

1

1

1

1

1

1

Qualifier Units RL


SAMPLE RESULTS

Project Name:

Project Number:

Lab Number:

Report Date:

NFTA

17005-02

L1811425

39.0

39.0

39.0

39.0

39.0

39.0

39.0

39.0

39.0


Decachlorobiphenyl


Decachlorobiphenyl

68

62

90

56

30-150

30-150

30-150

30-150

Acceptance Criteria

A

A

B

B


04/16/18



L1811425-01Lab ID:




1,8082A04/13/18 09:59WR

EPA 3546



84%Percent Solids:

MDL

4.42

5.93

3.84

4.77

4.37

3.18

4.07

3.20

2.76

A

A

A

A

A

B

A

A

A

Column

Sample Depth:

Serial_No:04161816:43

Page 48 of 118

Aroclor 1016

Aroclor 1221

Aroclor 1232

Aroclor 1242

Aroclor 1248

Aroclor 1254

Aroclor 1260

Aroclor 1262

Aroclor 1268


ND

ND

ND

ND

ND

ND

ND

ND

ND

ug/kg

ug/kg

ug/kg

ug/kg

ug/kg

ug/kg

ug/kg

ug/kg

ug/kg

1

1

1

1

1

1

1

1

1

Qualifier Units RL


SAMPLE RESULTS

Project Name:

Project Number:

Lab Number:

Report Date:

NFTA

17005-02

L1811425

44.8

44.8

44.8

44.8

44.8

44.8

44.8

44.8

44.8


Decachlorobiphenyl


Decachlorobiphenyl

64

45

65

41

30-150

30-150

30-150

30-150

Acceptance Criteria

A

A

B

B


04/16/18



L1811425-03Lab ID:




1,8082A04/10/18 18:03WR

EPA 3546



73%Percent Solids:

MDL

5.08

6.81

4.40

5.48

5.02

3.65

4.67

3.68

3.17

A

A

A

A

A

A

A

A

A

Column

Sample Depth:

Serial_No:04161816:43

Page 49 of 118

Aroclor 1016

Aroclor 1221

Aroclor 1232

Aroclor 1242

Aroclor 1248

Aroclor 1254

Aroclor 1260

Aroclor 1262

Aroclor 1268

Parameter Result

J

Dilution Factor

ND

ND

ND

ND

ND

11.1

ND

ND

ND

ug/kg

ug/kg

ug/kg

ug/kg

ug/kg

ug/kg

ug/kg

ug/kg

ug/kg

1

1

1

1

1

1

1

1

1

Qualifier Units RL


SAMPLE RESULTS

Project Name:

Project Number:

Lab Number:

Report Date:

NFTA

17005-02

L1811425

37.5

37.5

37.5

37.5

37.5

37.5

37.5

37.5

37.5


Decachlorobiphenyl


Decachlorobiphenyl

75

54

80

49

30-150

30-150

30-150

30-150

Acceptance Criteria

A

A

B

B


04/16/18



L1811425-04Lab ID:




1,8082A04/10/18 18:16WR

EPA 3546



85%Percent Solids:

MDL

4.26

5.71

3.69

4.60

4.21

3.06

3.92

3.09

2.66

A

A

A

A

A

A

A

A

A

Column

Sample Depth:

Serial_No:04161816:43

Page 50 of 118


Project Name:

Project Number:

Lab Number:

Report Date:

NFTA

17005-02

L1811425



Cleanup Method:

EPA 3546


04/16/18


Analyst: WR

Aroclor 1016

Aroclor 1221

Aroclor 1232

Aroclor 1242

Aroclor 1248

Aroclor 1254

Aroclor 1260

Aroclor 1262

Aroclor 1268

Parameter Result

ND

ND

ND

ND

ND

ND

ND

ND

ND

RL

32.0

32.0

32.0

32.0

32.0

32.0

32.0

32.0

32.0

ug/kg

ug/kg

ug/kg

ug/kg

ug/kg

ug/kg

ug/kg

ug/kg

ug/kg

UnitsQualifier

Polychlorinated Biphenyls by GC - Westborough Lab for sample(s): 01,03-04 Batch: WG1104565-1


Decachlorobiphenyl


Decachlorobiphenyl

74

74

77

62

30-150

30-150

30-150

30-150


Criteria



MDL

3.63

4.88

3.15

3.92

3.59

2.61

3.34

2.63

2.27

Column

A

A

A

A

A

A

A

A

A

A

A

B

B

Serial_No:04161816:43

Page 51 of 118

Aroclor 1016

Aroclor 1260

80

90

84

93

40-140

40-140

5

3

50

50

ParameterLCS

%RecoveryLCSD

%Recovery%Recovery

Limits RPDRPD

Limits

Polychlorinated Biphenyls by GC - Westborough Lab Associated sample(s): 01,03-04 Batch: WG1104565-2 WG1104565-3


Project Name:

Project Number:

Lab Number:

Report Date:

NFTA

17005-02

L1811425


86908771

30-15030-15030-15030-150

AABB

85918573


04/16/18

AcceptanceCriteria


A

A

Serial_No:04161816:43

Page 52 of 118

PESTICIDES

Serial_No:04161816:43

Page 53 of 118

FF

Lindane

Heptachlor

Heptachlor epoxide

Endrin

Methoxychlor

Toxaphene

Chlordane


ND

ND

ND

ND

ND

ND

ND

ug/l

ug/l

ug/l

ug/l

ug/l

ug/l

ug/l

1

1

1

1

1

1

1

Qualifier Units RL


SAMPLE RESULTS

Project Name:

Project Number:

Lab Number:

Report Date:

NFTA

17005-02

L1811425

0.100

0.100

0.100

0.200

1.00

1.00

1.00


Decachlorobiphenyl


Decachlorobiphenyl

76

99

78

76

30-150

30-150

30-150

30-150

Acceptance Criteria

A

A

B

B


04/16/18



L1811425-01Lab ID:




1,8081B04/11/18 15:23KEG



84%Percent Solids:

MDL

0.022

0.016

0.021

0.021

0.034

0.314

0.232

A

A

A

A

A

A

A

Column

Sample Depth:

Serial_No:04161816:43

Page 54 of 118

Delta-BHC

Lindane

Alpha-BHC

Beta-BHC

Heptachlor

Aldrin

Endrin

Dieldrin

4,4'-DDE

4,4'-DDD

4,4'-DDT

Endosulfan I

Endosulfan II

Endosulfan sulfate

cis-Chlordane

Parameter Result

J

JPI

Dilution Factor

ND

ND

ND

ND

ND

ND

ND

1.01

ND

ND

ND

ND

1.11

ND

ND

ug/kg

ug/kg

ug/kg

ug/kg

ug/kg

ug/kg

ug/kg

ug/kg

ug/kg

ug/kg

ug/kg

ug/kg

ug/kg

ug/kg

ug/kg

1

1

1

1

1

1

1

1

1

1

1

1

1

1

1

Qualifier Units RL


SAMPLE RESULTS

Project Name:

Project Number:

Lab Number:

Report Date:

NFTA

17005-02

L1811425

1.87

0.780

0.780

1.87

0.936

1.87

0.780

1.17

1.87

1.87

3.51

1.87

1.87

0.780

2.34


Decachlorobiphenyl


Decachlorobiphenyl

74

110

96

116

30-150

30-150

30-150

30-150

Acceptance Criteria

B

B

A

A


04/16/18



L1811425-01Lab ID:




1,8081B04/13/18 07:50KEG

EPA 3546



MDL

0.367

0.349

0.222

0.710

0.420

0.659

0.320

0.585

0.433

0.668

1.50

0.442

0.626

0.371

0.652

A

A

A

A

A

A

A

A

A

A

A

A

A

A

A

Column

Sample Depth:

Serial_No:04161816:43

Page 55 of 118

2,4-D

2,4,5-TP (Silvex)


ND

ND

mg/l

mg/l

1

1

Qualifier Units RL


SAMPLE RESULTS

Project Name:

Project Number:

Lab Number:

Report Date:

NFTA

17005-02

L1811425

0.025

0.005

DCAA

DCAA

75

67

30-150

30-150

Acceptance Criteria

A

B


04/16/18



L1811425-01Lab ID:




1,8151A04/10/18 09:51SL



84%Percent Solids:

MDL

0.001

0.001


A

A

Column

Sample Depth:

Serial_No:04161816:43

Page 56 of 118

2,4,5-TP (Silvex)


ND ug/kg 1

Qualifier Units RL


SAMPLE RESULTS

Project Name:

Project Number:

Lab Number:

Report Date:

NFTA

17005-02

L1811425

195

DCAA

DCAA

150

118

30-150

30-150

Acceptance Criteria

A

B


04/16/18



L1811425-01Lab ID:




1,8151A04/12/18 05:48SL


84%Percent Solids:

MDL

5.19


A

Column

Sample Depth:

Serial_No:04161816:43

Page 57 of 118

Lindane

Heptachlor

Heptachlor epoxide

Endrin

Methoxychlor

Toxaphene

Chlordane


ND

ND

ND

ND

ND

ND

ND

ug/l

ug/l

ug/l

ug/l

ug/l

ug/l

ug/l

1

1

1

1

1

1

1

Qualifier Units RL


SAMPLE RESULTS

Project Name:

Project Number:

Lab Number:

Report Date:

NFTA

17005-02

L1811425

0.100

0.100

0.100

0.200

1.00

1.00

1.00


Decachlorobiphenyl


Decachlorobiphenyl

126

135

114

132

30-150

30-150

30-150

30-150

Acceptance Criteria

A

A

B

B


04/16/18



L1811425-03Lab ID:




1,8081B04/15/18 18:35JW



73%Percent Solids:

MDL

0.022

0.016

0.021

0.021

0.034

0.314

0.232

A

A

A

A

A

A

A

Column

Sample Depth:

Serial_No:04161816:43

Page 58 of 118

Delta-BHC

Lindane

Alpha-BHC

Beta-BHC

Heptachlor

Aldrin

Endrin

Dieldrin

4,4'-DDE

4,4'-DDD

4,4'-DDT

Endosulfan I

Endosulfan II

Endosulfan sulfate

cis-Chlordane


ND

ND

ND

ND

ND

ND

ND

ND

ND

ND

ND

ND

ND

ND

ND

ug/kg

ug/kg

ug/kg

ug/kg

ug/kg

ug/kg

ug/kg

ug/kg

ug/kg

ug/kg

ug/kg

ug/kg

ug/kg

ug/kg

ug/kg

1

1

1

1

1

1

1

1

1

1

1

1

1

1

1

Qualifier Units RL


SAMPLE RESULTS

Project Name:

Project Number:

Lab Number:

Report Date:

NFTA

17005-02

L1811425

2.10

0.873

0.873

2.10

1.05

2.10

0.873

1.31

2.10

2.10

3.93

2.10

2.10

0.873

2.62


Decachlorobiphenyl


Decachlorobiphenyl

70

111

82

132

30-150

30-150

30-150

30-150

Acceptance Criteria

B

B

A

A


04/16/18



L1811425-03Lab ID:




1,8081B04/15/18 20:14JW

EPA 3546



MDL

0.410

0.390

0.248

0.794

0.470

0.738

0.358

0.655

0.484

0.747

1.68

0.495

0.700

0.416

0.730

A

A

A

A

A

A

A

A

A

A

A

A

A

A

A

Column

Sample Depth:

Serial_No:04161816:43

Page 59 of 118

2,4-D

2,4,5-TP (Silvex)


ND

ND

mg/l

mg/l

1

1

Qualifier Units RL


SAMPLE RESULTS

Project Name:

Project Number:

Lab Number:

Report Date:

NFTA

17005-02

L1811425

0.025

0.005

DCAA

DCAA

99

82

30-150

30-150

Acceptance Criteria

A

B


04/16/18



L1811425-03Lab ID:




1,8151A04/10/18 11:25SL



73%Percent Solids:

MDL

0.001

0.001


A

A

Column

Sample Depth:

Serial_No:04161816:43

Page 60 of 118

2,4,5-TP (Silvex)


ND ug/kg 1

Qualifier Units RL


SAMPLE RESULTS

Project Name:

Project Number:

Lab Number:

Report Date:

NFTA

17005-02

L1811425

227

DCAA

DCAA

139

112

30-150

30-150

Acceptance Criteria

A

B


04/16/18



L1811425-03Lab ID:




1,8151A04/12/18 06:07SL


73%Percent Solids:

MDL

6.04


A

Column

Sample Depth:

Serial_No:04161816:43

Page 61 of 118

Lindane

Heptachlor

Heptachlor epoxide

Endrin

Methoxychlor

Toxaphene

Chlordane


ND

ND

ND

ND

ND

ND

ND

ug/l

ug/l

ug/l

ug/l

ug/l

ug/l

ug/l

1

1

1

1

1

1

1

Qualifier Units RL


SAMPLE RESULTS

Project Name:

Project Number:

Lab Number:

Report Date:

NFTA

17005-02

L1811425

0.100

0.100

0.100

0.200

1.00

1.00

1.00


Decachlorobiphenyl


Decachlorobiphenyl

99

83

108

99

30-150

30-150

30-150

30-150

Acceptance Criteria

A

A

B

B


04/16/18



L1811425-04Lab ID:




1,8081B04/15/18 18:47JW



85%Percent Solids:

MDL

0.022

0.016

0.021

0.021

0.034

0.314

0.232

A

A

A

A

A

A

A

Column

Sample Depth:

Serial_No:04161816:43

Page 62 of 118

Delta-BHC

Lindane

Alpha-BHC

Beta-BHC

Heptachlor

Aldrin

Endrin

Dieldrin

4,4'-DDE

4,4'-DDD

4,4'-DDT

Endosulfan I

Endosulfan II

Endosulfan sulfate

cis-Chlordane


ND

ND

ND

ND

ND

ND

ND

ND

ND

ND

4.65

ND

ND

ND

ND

ug/kg

ug/kg

ug/kg

ug/kg

ug/kg

ug/kg

ug/kg

ug/kg

ug/kg

ug/kg

ug/kg

ug/kg

ug/kg

ug/kg

ug/kg

1

1

1

1

1

1

1

1

1

1

1

1

1

1

1

Qualifier Units RL


SAMPLE RESULTS

Project Name:

Project Number:

Lab Number:

Report Date:

NFTA

17005-02

L1811425

1.83

0.762

0.762

1.83

0.914

1.83

0.762

1.14

1.83

1.83

3.43

1.83

1.83

0.762

2.29


Decachlorobiphenyl


Decachlorobiphenyl

102

107

119

132

30-150

30-150

30-150

30-150

Acceptance Criteria

B

B

A

A


04/16/18



L1811425-04Lab ID:




1,8081B04/10/18 17:30KEG

EPA 3546



MDL

0.358

0.341

0.216

0.694

0.410

0.644

0.312

0.572

0.423

0.652

1.47

0.432

0.611

0.363

0.637

A

A

A

A

A

A

A

A

A

A

A

A

A

A

A

Column

Sample Depth:

Serial_No:04161816:43

Page 63 of 118

2,4-D

2,4,5-TP (Silvex)


ND

ND

mg/l

mg/l

1

1

Qualifier Units RL


SAMPLE RESULTS

Project Name:

Project Number:

Lab Number:

Report Date:

NFTA

17005-02

L1811425

0.025

0.005

DCAA

DCAA

80

68

30-150

30-150

Acceptance Criteria

A

B


04/16/18



L1811425-04Lab ID:




1,8151A04/10/18 11:43SL



85%Percent Solids:

MDL

0.001

0.001


A

A

Column

Sample Depth:

Serial_No:04161816:43

Page 64 of 118

2,4,5-TP (Silvex)


ND ug/kg 1

Qualifier Units RL


SAMPLE RESULTS

Project Name:

Project Number:

Lab Number:

Report Date:

NFTA

17005-02

L1811425

191

DCAA

DCAA

127

108

30-150

30-150

Acceptance Criteria

A

B


04/16/18



L1811425-04Lab ID:




1,8151A04/13/18 11:50KEG


85%Percent Solids:

MDL

5.08


A

Column

Sample Depth:

Serial_No:04161816:43

Page 65 of 118


Project Name:

Project Number:

Lab Number:

Report Date:

NFTA

17005-02

L1811425



04/16/18

Analyst: SL

2,4-D

2,4,5-TP (Silvex)

Parameter Result

ND

ND

RL

0.025

0.005

mg/l

mg/l

UnitsQualifier


DCAA

DCAA

64

59

30-150

30-150


Criteria


MDL

0.001

0.001


Column

A

A

A

B

Serial_No:04161816:43

Page 66 of 118


Project Name:

Project Number:

Lab Number:

Report Date:

NFTA

17005-02

L1811425



04/16/18

Analyst: SL

2,4-D

2,4,5-TP (Silvex)

Parameter Result

ND

ND

RL

0.025

0.005

mg/l

mg/l

UnitsQualifier

TCLP Herbicides by EPA 1311 - Westborough Lab for sample(s): 03-04 Batch: WG1104128-1

DCAA

DCAA

83

72

30-150

30-150


Criteria


MDL

0.001

0.001


Column

A

A

A

B

Serial_No:04161816:43

Page 67 of 118


Project Name:

Project Number:

Lab Number:

Report Date:

NFTA

17005-02

L1811425



Cleanup Method:

EPA 3546


04/16/18

Analyst: KEG

Delta-BHC

Lindane

Alpha-BHC

Beta-BHC

Heptachlor

Aldrin

Endrin

Dieldrin

4,4'-DDE

4,4'-DDD

4,4'-DDT

Endosulfan I

Endosulfan II

Endosulfan sulfate

cis-Chlordane

Parameter Result

ND

ND

ND

ND

ND

ND

ND

ND

ND

ND

ND

ND

ND

ND

ND

RL

1.54

0.640

0.640

1.54

0.768

1.54

0.640

0.960

1.54

1.54

2.88

1.54

1.54

0.640

1.92

ug/kg

ug/kg

ug/kg

ug/kg

ug/kg

ug/kg

ug/kg

ug/kg

ug/kg

ug/kg

ug/kg

ug/kg

ug/kg

ug/kg

ug/kg

UnitsQualifier

Organochlorine Pesticides by GC - Westborough Lab for sample(s): 01,04 Batch: WG1104562-1


Decachlorobiphenyl


Decachlorobiphenyl

100

95

92

134

30-150

30-150

30-150

30-150


Criteria


MDL

0.301

0.286

0.182

0.582

0.344

0.541

0.262

0.480

0.355

0.548

1.24

0.363

0.513

0.305

0.535

Column

A

A

A

A

A

A

A

A

A

A

A

A

A

A

A

B

B

A

A

Serial_No:04161816:43

Page 68 of 118


Project Name:

Project Number:

Lab Number:

Report Date:

NFTA

17005-02

L1811425



04/16/18

Analyst: KEG

2,4,5-TP (Silvex)

Parameter Result

ND

RL

162ug/kg

UnitsQualifier

Chlorinated Herbicides by GC - Westborough Lab for sample(s): 01,03 Batch: WG1105231-1

DCAA

DCAA

103

100

30-150

30-150


Criteria

MDL

4.32


Column

A

A

B

Serial_No:04161816:43

Page 69 of 118


Project Name:

Project Number:

Lab Number:

Report Date:

NFTA

17005-02

L1811425



04/16/18

Analyst: KEG

Lindane

Heptachlor

Heptachlor epoxide

Endrin

Methoxychlor

Toxaphene

Chlordane

Parameter Result

ND

ND

ND

ND

ND

ND

ND

RL

0.100

0.100

0.100

0.200

1.00

1.00

1.00

ug/l

ug/l

ug/l

ug/l

ug/l

ug/l

ug/l

UnitsQualifier

TCLP Pesticides by EPA 1311 - Westborough Lab for sample(s): 01 Batch: WG1105464-1


Decachlorobiphenyl


Decachlorobiphenyl

72

92

73

53

30-150

30-150

30-150

30-150


Criteria


MDL

0.022

0.016

0.021

0.021

0.034

0.314

0.232

Column

A

A

A

A

A

A

A

A

A

B

B

Serial_No:04161816:43

Page 70 of 118


Project Name:

Project Number:

Lab Number:

Report Date:

NFTA

17005-02

L1811425



04/16/18

Analyst: KEG

2,4,5-TP (Silvex)

Parameter Result

ND

RL

164ug/kg

UnitsQualifier

Chlorinated Herbicides by GC - Westborough Lab for sample(s): 04 Batch: WG1106052-1

DCAA

DCAA

110

91

30-150

30-150


Criteria

MDL

4.35


Column

A

A

B

Serial_No:04161816:43

Page 71 of 118


Project Name:

Project Number:

Lab Number:

Report Date:

NFTA

17005-02

L1811425



Cleanup Method:

EPA 3546


04/16/18

Analyst: JW

Delta-BHC

Lindane

Alpha-BHC

Beta-BHC

Heptachlor

Aldrin

Endrin

Dieldrin

4,4'-DDE

4,4'-DDD

4,4'-DDT

Endosulfan I

Endosulfan II

Endosulfan sulfate

cis-Chlordane

Parameter Result

ND

ND

ND

ND

ND

ND

ND

ND

ND

ND

ND

ND

ND

ND

ND

RL

1.59

0.663

0.663

1.59

0.795

1.59

0.663

0.994

1.59

1.59

2.98

1.59

1.59

0.663

1.99

ug/kg

ug/kg

ug/kg

ug/kg

ug/kg

ug/kg

ug/kg

ug/kg

ug/kg

ug/kg

ug/kg

ug/kg

ug/kg

ug/kg

ug/kg

UnitsQualifier

Organochlorine Pesticides by GC - Westborough Lab for sample(s): 03 Batch: WG1106186-1


Decachlorobiphenyl


Decachlorobiphenyl

83

76

82

101

30-150

30-150

30-150

30-150


Criteria


MDL

0.311

0.296

0.188

0.603

0.356

0.560

0.272

0.497

0.368

0.567

1.28

0.376

0.531

0.315

0.554

Column

A

A

A

A

A

A

A

A

A

A

A

A

A

A

A

B

B

A

A

Serial_No:04161816:43

Page 72 of 118


Project Name:

Project Number:

Lab Number:

Report Date:

NFTA

17005-02

L1811425



04/16/18

Analyst: JW

Lindane

Heptachlor

Heptachlor epoxide

Endrin

Methoxychlor

Toxaphene

Chlordane

Parameter Result

ND

ND

ND

ND

ND

ND

ND

RL

0.100

0.100

0.100

0.200

1.00

1.00

1.00

ug/l

ug/l

ug/l

ug/l

ug/l

ug/l

ug/l

UnitsQualifier

TCLP Pesticides by EPA 1311 - Westborough Lab for sample(s): 03-04 Batch: WG1106593-1


Decachlorobiphenyl


Decachlorobiphenyl

123

160

110

150

Q

30-150

30-150

30-150

30-150


Criteria


MDL

0.022

0.016

0.021

0.021

0.034

0.314

0.232

Column

A

A

A

A

A

A

A

A

A

B

B

Serial_No:04161816:43

Page 73 of 118

2,4-D

2,4,5-TP (Silvex)

104

58

137

88

30-150

30-150

27

41

25

25

ParameterLCS

%RecoveryLCSD

%Recovery%Recovery

Limits RPDRPD

Limits



Project Name:

Project Number:

Lab Number:

Report Date:

NFTA

17005-02

L1811425

DCAADCAA

8057

30-15030-150

AB

132100


04/16/18

AcceptanceCriteria

Qual Qual Qual

Q

Q

Column

A

A

Serial_No:04161816:43

Page 74 of 118

2,4-D

2,4,5-TP (Silvex)

99

65

106

64

30-150

30-150

7

2

25

25

ParameterLCS

%RecoveryLCSD

%Recovery%Recovery

Limits RPDRPD

Limits

TCLP Herbicides by EPA 1311 - Westborough Lab Associated sample(s): 03-04 Batch: WG1104128-2 WG1104128-3


Project Name:

Project Number:

Lab Number:

Report Date:

NFTA

17005-02

L1811425

DCAADCAA

9374

30-15030-150

AB

9784


04/16/18

AcceptanceCriteria


A

A

Serial_No:04161816:43

Page 75 of 118

Delta-BHC

Lindane

Alpha-BHC

Beta-BHC

Heptachlor

Aldrin

Endrin

Dieldrin

4,4'-DDE

4,4'-DDD

4,4'-DDT

Endosulfan I

Endosulfan II

Endosulfan sulfate

cis-Chlordane

119

111

114

134

125

115

125

122

107

110

115

118

115

104

108

102

92

96

120

106

98

107

105

93

93

101

103

100

89

92

30-150

30-150

30-150

30-150

30-150

30-150

30-150

30-150

30-150

30-150

30-150

30-150

30-150

30-150

30-150

15

19

17

11

16

16

16

15

14

17

13

14

14

16

16

30

30

30

30

30

30

30

30

30

30

30

30

30

30

30

ParameterLCS

%RecoveryLCSD

%Recovery%Recovery

Limits RPDRPD

Limits

Organochlorine Pesticides by GC - Westborough Lab Associated sample(s): 01,04 Batch: WG1104562-2 WG1104562-3


Project Name:

Project Number:

Lab Number:

Report Date:

NFTA

17005-02

L1811425


129112113150

30-15030-15030-15030-150

BBAA

1067693134


04/16/18

AcceptanceCriteria


A

A

A

A

A

A

A

A

A

A

A

A

A

A

A

Serial_No:04161816:43

Page 76 of 118

2,4,5-TP (Silvex) 86 84 30-150 2 30

ParameterLCS

%RecoveryLCSD

%Recovery%Recovery

Limits RPDRPD

Limits

Chlorinated Herbicides by GC - Westborough Lab Associated sample(s): 01,03 Batch: WG1105231-2 WG1105231-3


Project Name:

Project Number:

Lab Number:

Report Date:

NFTA

17005-02

L1811425

DCAADCAA

114113

30-15030-150

AB

115112


04/16/18

AcceptanceCriteria


A

Serial_No:04161816:43

Page 77 of 118

Lindane

Heptachlor

Heptachlor epoxide

Endrin

Methoxychlor

115

120

130

126

126

84

88

94

91

96

30-150

30-150

30-150

30-150

30-150

31

31

32

32

27

20

20

20

20

20

ParameterLCS

%RecoveryLCSD

%Recovery%Recovery

Limits RPDRPD

Limits

TCLP Pesticides by EPA 1311 - Westborough Lab Associated sample(s): 01 Batch: WG1105464-2 WG1105464-3


Project Name:

Project Number:

Lab Number:

Report Date:

NFTA

17005-02

L1811425


9512395100

30-15030-15030-15030-150

AABB

72957377


04/16/18

AcceptanceCriteria

Qual Qual Qual

Q

Q

Q

Q

Q

Column

A

A

A

A

A

Serial_No:04161816:43

Page 78 of 118

2,4,5-TP (Silvex) 84 80 30-150 5 30

ParameterLCS

%RecoveryLCSD

%Recovery%Recovery

Limits RPDRPD

Limits

Chlorinated Herbicides by GC - Westborough Lab Associated sample(s): 04 Batch: WG1106052-2 WG1106052-3


Project Name:

Project Number:

Lab Number:

Report Date:

NFTA

17005-02

L1811425

DCAADCAA

10297

30-15030-150

AB

10295


04/16/18

AcceptanceCriteria


A

Serial_No:04161816:43

Page 79 of 118

Delta-BHC

Lindane

Alpha-BHC

Beta-BHC

Heptachlor

Aldrin

Endrin

Dieldrin

4,4'-DDE

4,4'-DDD

4,4'-DDT

Endosulfan I

Endosulfan II

Endosulfan sulfate

cis-Chlordane

94

93

98

103

100

102

108

107

96

90

100

105

89

59

98

88

86

92

95

97

98

103

100

91

87

96

98

76

41

92

30-150

30-150

30-150

30-150

30-150

30-150

30-150

30-150

30-150

30-150

30-150

30-150

30-150

30-150

30-150

7

8

6

8

3

4

5

7

5

3

4

7

16

36

6

30

30

30

30

30

30

30

30

30

30

30

30

30

30

30

ParameterLCS

%RecoveryLCSD

%Recovery%Recovery

Limits RPDRPD

Limits

Organochlorine Pesticides by GC - Westborough Lab Associated sample(s): 03 Batch: WG1106186-2 WG1106186-3


Project Name:

Project Number:

Lab Number:

Report Date:

NFTA

17005-02

L1811425


889187103

30-15030-15030-15030-150

BBAA

869083112


04/16/18

AcceptanceCriteria

Qual Qual Qual

Q

Column

A

A

A

A

A

A

A

A

A

A

A

A

A

A

A

Serial_No:04161816:43

Page 80 of 118

Lindane

Heptachlor

Heptachlor epoxide

Endrin

Methoxychlor

119

110

115

118

132

143

129

136

141

154

30-150

30-150

30-150

30-150

30-150

18

16

17

18

15

20

20

20

20

20

ParameterLCS

%RecoveryLCSD

%Recovery%Recovery

Limits RPDRPD

Limits

TCLP Pesticides by EPA 1311 - Westborough Lab Associated sample(s): 03-04 Batch: WG1106593-2 WG1106593-3


Project Name:

Project Number:

Lab Number:

Report Date:

NFTA

17005-02

L1811425


111143100136

30-15030-15030-15030-150

AABB

127157116152

Q

Q


04/16/18

AcceptanceCriteria

Qual Qual

Q

Qual Column

A

A

A

A

A

Serial_No:04161816:43

Page 81 of 118

METALS

Serial_No:04161816:43

Page 82 of 118

FF

Project Name:

Project Number:

Lab Number:

Report Date:

NFTA

17005-02

L1811425

04/16/18

SAMPLE RESULTS


Matrix: Soil


L1811425-01Lab ID:



DateAnalyzed


Date Prepared


Arsenic, TCLP

Barium, TCLP

Cadmium, TCLP

Chromium, TCLP

Lead, TCLP

Mercury, TCLP

Selenium, TCLP

Silver, TCLP

ND

0.746

ND

ND

0.733

ND

ND

ND

mg/l

mg/l

mg/l

mg/l

mg/l

mg/l

mg/l

mg/l

1

1

1

1

1

1

1

1

1.00

0.500

0.100

0.200

0.500

0.0010

0.500

0.100

04/06/18 00:32

04/06/18 00:32

04/06/18 00:32

04/06/18 00:32

04/06/18 00:32

04/09/18 12:52

04/06/18 00:32

04/06/18 00:32

1,6010C

1,6010C

1,6010C

1,6010C

1,6010C

1,7470A

1,6010C

1,6010C

AB

AB

AB

AB

AB

MG

AB

AB

04/05/18 16:16

04/05/18 16:16

04/05/18 16:16

04/05/18 16:16

04/05/18 16:16

04/06/18 15:49

04/05/18 16:16

04/05/18 16:16

EPA 3015

EPA 3015

EPA 3015

EPA 3015

EPA 3015

EPA 7470A

EPA 3015

EPA 3015

PrepMethod


Percent Solids: 84%

MDL

0.019

0.021

0.010

0.021

0.027

0.0003

0.035

0.028

Sample Depth:

Serial_No:04161816:43

Page 83 of 118

Project Name:

Project Number:

Lab Number:

Report Date:

NFTA

17005-02

L1811425

04/16/18

SAMPLE RESULTS


Matrix: Soil


L1811425-01Lab ID:



DateAnalyzed


Date Prepared



Arsenic, Total

Barium, Total

Beryllium, Total

Cadmium, Total

Chromium, Total

Copper, Total

Lead, Total

Manganese, Total

Mercury, Total

Nickel, Total

Selenium, Total

Silver, Total

Zinc, Total

Chromium, Trivalent

J

J

10.9

82.0

0.282

0.328

11.9

74.8

401

358

1.60

7.84

1.30

0.187

166

12

mg/kg

mg/kg

mg/kg

mg/kg

mg/kg

mg/kg

mg/kg

mg/kg

mg/kg

mg/kg

mg/kg

mg/kg

mg/kg

mg/kg

1

1

1

1

1

1

1

1

1

1

1

1

1

1

0.455

0.455

0.228

0.455

0.455

0.455

2.28

0.455

0.075

1.14

0.911

0.455

2.28

0.95

04/05/18 16:18

04/05/18 16:18

04/05/18 16:18

04/05/18 16:18

04/05/18 16:18

04/05/18 16:18

04/05/18 16:18

04/05/18 16:18

04/05/18 18:31

04/05/18 16:18

04/05/18 16:18

04/05/18 16:18

04/05/18 16:18

04/05/18 16:18

1,6010C

1,6010C

1,6010C

1,6010C

1,6010C

1,6010C

1,6010C

1,6010C

1,7471B

1,6010C

1,6010C

1,6010C

1,6010C

107,-

PE

PE

PE

PE

PE

PE

PE

PE

EA

PE

PE

PE

PE

04/04/18 21:22

04/04/18 21:22

04/04/18 21:22

04/04/18 21:22

04/04/18 21:22

04/04/18 21:22

04/04/18 21:22

04/04/18 21:22

04/05/18 07:30

04/04/18 21:22

04/04/18 21:22

04/04/18 21:22

04/04/18 21:22

EPA 3050B

EPA 3050B

EPA 3050B

EPA 3050B

EPA 3050B

EPA 3050B

EPA 3050B

EPA 3050B

EPA 7471B

EPA 3050B

EPA 3050B

EPA 3050B

EPA 3050B

NA

PrepMethod

Percent Solids: 84%

MDL

0.095

0.079

0.015

0.045

0.044

0.117

0.122

0.072

0.016

0.110

0.117

0.129

0.133

0.95

Sample Depth:

Serial_No:04161816:43

Page 84 of 118

Project Name:

Project Number:

Lab Number:

Report Date:

NFTA

17005-02

L1811425

04/16/18

SAMPLE RESULTS


Matrix: Soil


L1811425-03Lab ID:



DateAnalyzed


Date Prepared


Arsenic, TCLP

Barium, TCLP

Cadmium, TCLP

Chromium, TCLP

Lead, TCLP

Mercury, TCLP

Selenium, TCLP

Silver, TCLP

J

J

J

ND

0.457

ND

ND

0.072

ND

0.040

ND

mg/l

mg/l

mg/l

mg/l

mg/l

mg/l

mg/l

mg/l

1

1

1

1

1

1

1

1

1.00

0.500

0.100

0.200

0.500

0.0010

0.500

0.100

04/05/18 23:33

04/05/18 23:33

04/05/18 23:33

04/05/18 23:33

04/05/18 23:33

04/07/18 15:33

04/05/18 23:33

04/05/18 23:33

1,6010C

1,6010C

1,6010C

1,6010C

1,6010C

1,7470A

1,6010C

1,6010C

AB

AB

AB

AB

AB

BV

AB

AB

04/05/18 16:16

04/05/18 16:16

04/05/18 16:16

04/05/18 16:16

04/05/18 16:16

04/06/18 15:49

04/05/18 16:16

04/05/18 16:16

EPA 3015

EPA 3015

EPA 3015

EPA 3015

EPA 3015

EPA 7470A

EPA 3015

EPA 3015

PrepMethod


Percent Solids: 73%

MDL

0.019

0.021

0.010

0.021

0.027

0.0003

0.035

0.028

Sample Depth:

Serial_No:04161816:43

Page 85 of 118

Project Name:

Project Number:

Lab Number:

Report Date:

NFTA

17005-02

L1811425

04/16/18

SAMPLE RESULTS


Matrix: Soil


L1811425-03Lab ID:



DateAnalyzed


Date Prepared



Arsenic, Total

Barium, Total

Beryllium, Total

Cadmium, Total

Chromium, Total

Copper, Total

Lead, Total

Manganese, Total

Mercury, Total

Nickel, Total

Selenium, Total

Silver, Total

Zinc, Total

Chromium, Trivalent

J

J

J

J

3.81

59.2

0.204

0.210

6.74

60.3

149

194

2.37

5.41

0.667

0.236

91.3

6.7

mg/kg

mg/kg

mg/kg

mg/kg

mg/kg

mg/kg

mg/kg

mg/kg

mg/kg

mg/kg

mg/kg

mg/kg

mg/kg

mg/kg

1

1

1

1

1

1

1

1

1

1

1

1

1

1

0.538

0.538

0.269

0.538

0.538

0.538

2.69

0.538

0.086

1.34

1.08

0.538

2.69

1.1

04/05/18 16:22

04/05/18 16:22

04/05/18 16:22

04/05/18 16:22

04/05/18 16:22

04/05/18 16:22

04/05/18 16:22

04/05/18 16:22

04/05/18 18:33

04/05/18 16:22

04/05/18 16:22

04/05/18 16:22

04/05/18 16:22

04/05/18 16:22

1,6010C

1,6010C

1,6010C

1,6010C

1,6010C

1,6010C

1,6010C

1,6010C

1,7471B

1,6010C

1,6010C

1,6010C

1,6010C

107,-

PE

PE

PE

PE

PE

PE

PE

PE

EA

PE

PE

PE

PE

04/04/18 21:22

04/04/18 21:22

04/04/18 21:22

04/04/18 21:22

04/04/18 21:22

04/04/18 21:22

04/04/18 21:22

04/04/18 21:22

04/05/18 07:30

04/04/18 21:22

04/04/18 21:22

04/04/18 21:22

04/04/18 21:22

EPA 3050B

EPA 3050B

EPA 3050B

EPA 3050B

EPA 3050B

EPA 3050B

EPA 3050B

EPA 3050B

EPA 7471B

EPA 3050B

EPA 3050B

EPA 3050B

EPA 3050B

NA

PrepMethod

Percent Solids: 73%

MDL

0.112

0.094

0.018

0.053

0.052

0.139

0.144

0.086

0.018

0.130

0.139

0.152

0.158

1.1

Sample Depth:

Serial_No:04161816:43

Page 86 of 118

Project Name:

Project Number:

Lab Number:

Report Date:

NFTA

17005-02

L1811425

04/16/18

SAMPLE RESULTS


Matrix: Soil


L1811425-04Lab ID:



DateAnalyzed


Date Prepared


Arsenic, TCLP

Barium, TCLP

Cadmium, TCLP

Chromium, TCLP

Lead, TCLP

Mercury, TCLP

Selenium, TCLP

Silver, TCLP

J

ND

0.366

ND

ND

ND

ND

ND

ND

mg/l

mg/l

mg/l

mg/l

mg/l

mg/l

mg/l

mg/l

1

1

1

1

1

1

1

1

1.00

0.500

0.100

0.200

0.500

0.0010

0.500

0.100

04/05/18 23:38

04/05/18 23:38

04/05/18 23:38

04/05/18 23:38

04/05/18 23:38

04/07/18 15:35

04/05/18 23:38

04/05/18 23:38

1,6010C

1,6010C

1,6010C

1,6010C

1,6010C

1,7470A

1,6010C

1,6010C

AB

AB

AB

AB

AB

BV

AB

AB

04/05/18 16:16

04/05/18 16:16

04/05/18 16:16

04/05/18 16:16

04/05/18 16:16

04/06/18 15:49

04/05/18 16:16

04/05/18 16:16

EPA 3015

EPA 3015

EPA 3015

EPA 3015

EPA 3015

EPA 7470A

EPA 3015

EPA 3015

PrepMethod


Percent Solids: 85%

MDL

0.019

0.021

0.010

0.021

0.027

0.0003

0.035

0.028

Sample Depth:

Serial_No:04161816:43

Page 87 of 118

Project Name:

Project Number:

Lab Number:

Report Date:

NFTA

17005-02

L1811425

04/16/18

SAMPLE RESULTS


Matrix: Soil


L1811425-04Lab ID:



DateAnalyzed


Date Prepared



Arsenic, Total

Barium, Total

Beryllium, Total

Cadmium, Total

Chromium, Total

Copper, Total

Lead, Total

Manganese, Total

Mercury, Total

Nickel, Total

Selenium, Total

Silver, Total

Zinc, Total

Chromium, Trivalent

J

J

J

J

1.33

23.6

0.147

0.045

6.34

12.2

15.2

81.0

0.063

4.04

0.129

ND

34.7

6.3

mg/kg

mg/kg

mg/kg

mg/kg

mg/kg

mg/kg

mg/kg

mg/kg

mg/kg

mg/kg

mg/kg

mg/kg

mg/kg

mg/kg

1

1

1

1

1

1

1

1

1

1

1

1

1

1

0.446

0.446

0.223

0.446

0.446

0.446

2.23

0.446

0.074

1.11

0.892

0.446

2.23

0.94

04/05/18 16:26

04/05/18 16:26

04/05/18 16:26

04/05/18 16:26

04/05/18 16:26

04/05/18 16:26

04/05/18 16:26

04/05/18 16:26

04/05/18 18:35

04/05/18 16:26

04/05/18 16:26

04/05/18 16:26

04/05/18 16:26

04/05/18 16:26

1,6010C

1,6010C

1,6010C

1,6010C

1,6010C

1,6010C

1,6010C

1,6010C

1,7471B

1,6010C

1,6010C

1,6010C

1,6010C

107,-

PE

PE

PE

PE

PE

PE

PE

PE

EA

PE

PE

PE

PE

04/04/18 21:22

04/04/18 21:22

04/04/18 21:22

04/04/18 21:22

04/04/18 21:22

04/04/18 21:22

04/04/18 21:22

04/04/18 21:22

04/05/18 07:30

04/04/18 21:22

04/04/18 21:22

04/04/18 21:22

04/04/18 21:22

EPA 3050B

EPA 3050B

EPA 3050B

EPA 3050B

EPA 3050B

EPA 3050B

EPA 3050B

EPA 3050B

EPA 7471B

EPA 3050B

EPA 3050B

EPA 3050B

EPA 3050B

NA

PrepMethod

Percent Solids: 85%

MDL

0.093

0.078

0.015

0.044

0.043

0.115

0.120

0.071

0.016

0.108

0.115

0.126

0.131

0.94

Sample Depth:

Serial_No:04161816:43

Page 88 of 118

FF

Parameter

Parameter

Parameter

Result

Result

Result

Dilution Factor

Dilution Factor

Dilution Factor

Qualifier

Qualifier

Qualifier

Units

Units

Units

RL

RL

RL


Project Name:

Project Number:

Lab Number:

Report Date:

NFTA

17005-02

L1811425

DateAnalyzed

DateAnalyzed

DateAnalyzed

AnalyticalMethod

AnalyticalMethod

AnalyticalMethod

Analyst

Analyst

Analyst

Date Prepared

Date Prepared

Date Prepared

04/16/18

Arsenic, Total

Barium, Total

Beryllium, Total

Cadmium, Total

Chromium, Total

Copper, Total

Lead, Total

Manganese, Total

Nickel, Total

Selenium, Total

Silver, Total

Zinc, Total

Mercury, Total

Arsenic, TCLP

Barium, TCLP

Cadmium, TCLP

Chromium, TCLP

Lead, TCLP

ND

ND

ND

ND

ND

ND

ND

ND

ND

ND

ND

ND

ND

ND

ND

ND

ND

ND

mg/kg

mg/kg

mg/kg

mg/kg

mg/kg

mg/kg

mg/kg

mg/kg

mg/kg

mg/kg

mg/kg

mg/kg

mg/kg

mg/l

mg/l

mg/l

mg/l

mg/l

1

1

1

1

1

1

1

1

1

1

1

1

1

1

1

1

1

1

0.400

0.400

0.200

0.400

0.400

0.400

2.00

0.400

1.00

0.800

0.400

2.00

0.083

1.00

0.500

0.100

0.200

0.500

04/05/18 15:11

04/05/18 15:11

04/05/18 15:11

04/05/18 15:11

04/05/18 15:11

04/05/18 15:11

04/05/18 15:11

04/05/18 15:11

04/05/18 15:11

04/05/18 15:11

04/05/18 15:11

04/05/18 15:11

04/05/18 18:17

04/05/18 21:22

04/05/18 21:22

04/05/18 21:22

04/05/18 21:22

04/05/18 21:22

1,6010C

1,6010C

1,6010C

1,6010C

1,6010C

1,6010C

1,6010C

1,6010C

1,6010C

1,6010C

1,6010C

1,6010C

1,7471B

1,6010C

1,6010C

1,6010C

1,6010C

1,6010C

PE

PE

PE

PE

PE

PE

PE

PE

PE

PE

PE

PE

EA

AB

AB

AB

AB

AB

04/04/18 21:22

04/04/18 21:22

04/04/18 21:22

04/04/18 21:22

04/04/18 21:22

04/04/18 21:22

04/04/18 21:22

04/04/18 21:22

04/04/18 21:22

04/04/18 21:22

04/04/18 21:22

04/04/18 21:22

04/05/18 07:30

04/05/18 16:16

04/05/18 16:16

04/05/18 16:16

04/05/18 16:16

04/05/18 16:16

Total Metals - Mansfield Lab for sample(s): 01,03-04 Batch: WG1103561-1

Total Metals - Mansfield Lab for sample(s): 01,03-04 Batch: WG1103661-1

TCLP Metals by EPA 1311 - Mansfield Lab for sample(s): 03-04 Batch: WG1103919-1

EPA 3050B

EPA 7471B

Digestion Method:

Digestion Method:

Prep Information

Prep Information

MDL

MDL

MDL

0.083

0.070

0.013

0.039

0.038

0.103

0.107

0.064

0.097

0.103

0.113

0.117

0.018

0.019

0.021

0.010

0.021

0.027

Serial_No:04161816:43

Page 89 of 118

Parameter

Parameter

Parameter

Result

Result

Result

Dilution Factor

Dilution Factor

Dilution Factor

Qualifier

Qualifier

Qualifier

Units

Units

Units

RL

RL

RL


Project Name:

Project Number:

Lab Number:

Report Date:

NFTA

17005-02

L1811425

DateAnalyzed

DateAnalyzed

DateAnalyzed

AnalyticalMethod

AnalyticalMethod

AnalyticalMethod

Analyst

Analyst

Analyst

Date Prepared

Date Prepared

Date Prepared

04/16/18

Selenium, TCLP

Silver, TCLP

Arsenic, TCLP

Barium, TCLP

Cadmium, TCLP

Chromium, TCLP

Lead, TCLP

Selenium, TCLP

Silver, TCLP

Mercury, TCLP

Mercury, TCLP

ND

ND

ND

ND

ND

ND

ND

ND

ND

ND

ND

mg/l

mg/l

mg/l

mg/l

mg/l

mg/l

mg/l

mg/l

mg/l

mg/l

mg/l

1

1

1

1

1

1

1

1

1

1

1

0.500

0.100

1.00

0.500

0.100

0.200

0.500

0.500

0.100

0.0010

0.0010

04/05/18 21:22

04/05/18 21:22

04/06/18 00:05

04/06/18 00:05

04/06/18 00:05

04/06/18 00:05

04/06/18 00:05

04/06/18 00:05

04/06/18 00:05

04/07/18 15:21

04/09/18 12:49

1,6010C

1,6010C

1,6010C

1,6010C

1,6010C

1,6010C

1,6010C

1,6010C

1,6010C

1,7470A

1,7470A

AB

AB

AB

AB

AB

AB

AB

AB

AB

BV

MG

04/05/18 16:16

04/05/18 16:16

04/05/18 16:16

04/05/18 16:16

04/05/18 16:16

04/05/18 16:16

04/05/18 16:16

04/05/18 16:16

04/05/18 16:16

04/06/18 15:49

04/06/18 15:49




EPA 3015

EPA 3015

EPA 7470A

Digestion Method:

Digestion Method:

Digestion Method:

Prep Information

Prep Information

Prep Information

04/04/18 16:03

04/04/18 16:03

04/04/18 16:03




MDL

MDL

MDL

0.035

0.028

0.019

0.021

0.010

0.021

0.027

0.035

0.028

0.0003

0.0003

Serial_No:04161816:43

Page 90 of 118


Project Name:

Project Number:

Lab Number:

Report Date:

NFTA

17005-02

L1811425

04/16/18

EPA 7470ADigestion Method:

Prep Information


Serial_No:04161816:43

Page 91 of 118

Arsenic, Total

Barium, Total

Beryllium, Total

Cadmium, Total

Chromium, Total

Copper, Total

Lead, Total

Manganese, Total

Selenium, Total

Silver, Total

Zinc, Total

Mercury, Total

87

82

85

85

86

89

92

85

87

86

82

106

-

-

-

-

-

-

-

-

-

-

-

-

83-117

82-118

83-117

82-117

83-119

84-116

82-117

82-118

78-121

80-120

81-119

50-149

-

-

-

-

-

-

-

-

-

-

-

-

ParameterLCS

%RecoveryLCSD

%Recovery%Recovery


Total Metals - Mansfield Lab Associated sample(s): 01,03-04 Batch: WG1103561-2 SRM Lot Number: D098-540

Total Metals - Mansfield Lab Associated sample(s): 01,03-04 Batch: WG1103661-2 SRM Lot Number: D098-540


Project Name:

Project Number:

Lab Number:

Report Date:

NFTA

17005-02

L1811425

04/16/18

Qual Qual Qual

Serial_No:04161816:43

Page 92 of 118

Arsenic, TCLP

Barium, TCLP

Cadmium, TCLP

Chromium, TCLP

Lead, TCLP

Selenium, TCLP

Silver, TCLP

Arsenic, TCLP

Barium, TCLP

Cadmium, TCLP

Chromium, TCLP

Lead, TCLP

Selenium, TCLP

Silver, TCLP

Mercury, TCLP

102

95

97

94

94

102

89

98

91

94

92

92

97

85

108

-

-

-

-

-

-

-

-

-

-

-

-

-

-

-

75-125

75-125

75-125

75-125

75-125

75-125

75-125

75-125

75-125

75-125

75-125

75-125

75-125

75-125

80-120

-

-

-

-

-

-

-

-

-

-

-

-

-

-

-

20

20

20

20

20

20

20

20

20

20

20

20

20

20

ParameterLCS

%RecoveryLCSD

%Recovery%Recovery


TCLP Metals by EPA 1311 - Mansfield Lab Associated sample(s): 03-04 Batch: WG1103919-2




Project Name:

Project Number:

Lab Number:

Report Date:

NFTA

17005-02

L1811425

04/16/18

Serial_No:04161816:43

Page 93 of 118

Mercury, TCLP 100 - 80-120 -

ParameterLCS

%RecoveryLCSD

%Recovery%Recovery




Project Name:

Project Number:

Lab Number:

Report Date:

NFTA

17005-02

L1811425

04/16/18

Serial_No:04161816:43

Page 94 of 118

Arsenic, Total

Barium, Total

Beryllium, Total

Cadmium, Total

Chromium, Total

Copper, Total

Lead, Total

Manganese, Total

Nickel, Total

Selenium, Total

Silver, Total

Zinc, Total

Mercury, Total

2.52

115.

0.598

0.086J

15.0

9.32

10.6

645.

19.6

0.189J

ND

44.0

0.204

8.49

199

2.94

2.41

22.6

21.0

31.1

621

39.0

4.99

15.3

62.8

0.340

58

48

54

55

44

54

46

0

45

48

59

43

96

-

-

-

-

-

-

-

-

-

-

-

-

0.372

-

-

-

-

-

-

-

-

-

-

-

-

119

75-125

75-125

75-125

75-125

75-125

75-125

75-125

75-125

75-125

75-125

75-125

75-125

80-120

-

-

-

-

-

-

-

-

-

-

-

-

9

20

20

20

20

20

20

20

20

20

20

20

20

20


MS Found

MS%Recovery

MSD Found

MSD %Recovery

RecoveryLimits RPD

RPD Limits

Total Metals - Mansfield Lab Associated sample(s): 01,03-04 QC Batch ID: WG1103561-3 QC Sample: L1811417-01 Client ID: MS Sample

Total Metals - Mansfield Lab Associated sample(s): 01,03-04 QC Batch ID: WG1103661-3 WG1103661-4 QC Sample: L1811488-08 Client ID: MS Sample

10.4

173

4.32

4.41

17.3

21.6

44.1

43.2

43.2

10.4

26

43.2

0.141

MS Added


Project Name:

Project Number:

Lab Number:

Report Date:

NFTA

17005-02

L1811425

04/16/18

Qual

Q

Q

Q

Q

Q

Q

Q

Q

Q

Q

Q

Q

Qual Qual

Serial_No:04161816:43

Page 95 of 118

Arsenic, TCLP

Barium, TCLP

Cadmium, TCLP

Chromium, TCLP

Lead, TCLP

Selenium, TCLP

Silver, TCLP

Arsenic, TCLP

Barium, TCLP

Cadmium, TCLP

Chromium, TCLP

Lead, TCLP

Selenium, TCLP

Silver, TCLP

Mercury, TCLP

Mercury, TCLP

ND

0.550

ND

ND

ND

0.061J

ND

ND

7.39

ND

ND

0.781

ND

ND

ND

ND

1.29

20.5

0.525

2.02

5.02

1.33

0.477

1.18

26.4

0.484

1.85

5.50

1.18

0.444

0.0255

0.0249

108

100

103

101

98

111

95

98

95

95

92

92

98

89

102

99

-

-

-

-

-

-

-

-

-

-

-

-

-

-

-

-

-

-

-

-

-

-

-

-

-

-

-

-

-

-

-

-

75-125

75-125

75-125

75-125

75-125

75-125

75-125

75-125

75-125

75-125

75-125

75-125

75-125

75-125

80-120

80-120

-

-

-

-

-

-

-

-

-

-

-

-

-

-

-

-

20

20

20

20

20

20

20

20

20

20

20

20

20

20

20

20


MS Found

MS%Recovery

MSD Found

MSD %Recovery

RecoveryLimits RPD

RPD Limits

TCLP Metals by EPA 1311 - Mansfield Lab Associated sample(s): 03-04 QC Batch ID: WG1103919-3 QC Sample: L1811390-03 Client ID: MS Sample



TCLP Metals by EPA 1311 - Mansfield Lab Associated sample(s): 01 QC Batch ID: WG1104297-3 QC Sample: L1811425-01 Client ID: BH9-18

1.2

20

0.51

2

5.1

1.2

0.5

1.2

20

0.51

2

5.1

1.2

0.5

0.025

0.025

MS Added


Project Name:

Project Number:

Lab Number:

Report Date:

NFTA

17005-02

L1811425

04/16/18

Serial_No:04161816:43

Page 96 of 118

Arsenic, Total

Beryllium, Total

Cadmium, Total

Chromium, Total

Copper, Total

Lead, Total

Nickel, Total

Selenium, Total

Silver, Total

Zinc, Total

Arsenic, TCLP

Barium, TCLP

Cadmium, TCLP

Chromium, TCLP

Lead, TCLP

Selenium, TCLP

Silver, TCLP

2.52

0.598

0.086J

15.0

9.32

10.6

19.6

0.189J

ND

44.0

ND

0.550

ND

ND

ND

0.061J

ND

2.51

0.601

0.083J

14.1

7.39

10.1

18.9

0.224J

ND

40.4

ND

0.517

ND

ND

ND

0.040J

ND

mg/kg

mg/kg

mg/kg

mg/kg

mg/kg

mg/kg

mg/kg

mg/kg

mg/kg

mg/kg

mg/l

mg/l

mg/l

mg/l

mg/l

mg/l

mg/l

0

1

NC

6

23

5

4

NC

NC

9

NC

6

NC

NC

NC

NC

NC

20

20

20

20

20

20

20

20

20

20

20

20

20

20

20

20

20


Total Metals - Mansfield Lab Associated sample(s): 01,03-04 QC Batch ID: WG1103561-4 QC Sample: L1811417-01 Client ID: DUP Sample

TCLP Metals by EPA 1311 - Mansfield Lab Associated sample(s): 03-04 QC Batch ID: WG1103919-4 QC Sample: L1811390-03 Client ID: DUP Sample

NFTA

17005-02

Project Name:

Project Number:

L1811425Lab Number:

Report Date:


04/16/18

Qual

Q

Serial_No:04161816:43

Page 97 of 118

Arsenic, TCLP

Barium, TCLP

Cadmium, TCLP

Chromium, TCLP

Lead, TCLP

Selenium, TCLP

Silver, TCLP

Mercury, TCLP

Mercury, TCLP

ND

7.39

ND

ND

0.781

ND

ND

ND

ND

ND

7.94

ND

0.022J

0.845

ND

ND

ND

ND

mg/l

mg/l

mg/l

mg/l

mg/l

mg/l

mg/l

mg/l

mg/l

NC

7

NC

NC

8

NC

NC

NC

NC

20

20

20

20

20

20

20

20

20




TCLP Metals by EPA 1311 - Mansfield Lab Associated sample(s): 01 QC Batch ID: WG1104297-4 QC Sample: L1811425-01 Client ID: BH9-18

NFTA

17005-02

Project Name:

Project Number:

L1811425Lab Number:

Report Date:


04/16/18

Serial_No:04161816:43

Page 98 of 118

INORGANICS&

MISCELLANEOUS

Serial_No:04161816:43

Page 99 of 118

FF


Matrix: Soil


L1811425-01Lab ID:

SAMPLE RESULTS

Project Name:

Project Number:

Lab Number:

Report Date:

NFTA

17005-02

L1811425



Ignitability NI 04/05/18 02:05 1,1030 JD


Source of Material:


Particle Size:


Unknown


Coarse

120


AnalyzedAnalytical

Method Analyst

04/16/18

Sample Depth:

Serial_No:04161816:43

Page 100 of 118

FF


Matrix: Soil


L1811425-03Lab ID:

SAMPLE RESULTS

Project Name:

Project Number:

Lab Number:

Report Date:

NFTA

17005-02

L1811425





Source of Material:


Particle Size:


Unknown


Coarse

120


AnalyzedAnalytical

Method Analyst

04/16/18

Sample Depth:

Serial_No:04161816:43

Page 101 of 118

FF


Matrix: Soil


L1811425-04Lab ID:

SAMPLE RESULTS

Project Name:

Project Number:

Lab Number:

Report Date:

NFTA

17005-02

L1811425





Source of Material:


Particle Size:


Unknown


Medium

120


AnalyzedAnalytical

Method Analyst

04/16/18

Sample Depth:

Serial_No:04161816:43

Page 102 of 118

FF



Matrix: Soil


L1811425-01Lab ID:

Qualifier Units RL

SAMPLE RESULTS

Project Name:

Project Number:

Lab Number:

Report Date:

NFTA

17005-02

L1811425

Field Prep:

DateAnalyzed


Not Specified


Cyanide, Total

pH (H)


Cyanide, Reactive

Sulfide, Reactive

84.4

ND

9.6

ND

ND

ND

%

mg/kg

SU

mg/kg

mg/kg

mg/kg

1

1

1

1

1

1

0.100

1.1

-

0.95

10

10

04/04/18 13:08

04/04/18 13:56

04/04/18 09:52

04/05/18 14:12

04/04/18 18:04

04/04/18 17:34

121,2540G

1,9010C/9012B

1,9045D

1,7196A

125,7.3

125,7.3

RI

LH

GD

NH

RM

RM

Date Prepared

-

04/04/18 09:25

-

04/04/18 23:30

04/04/18 15:40

04/04/18 15:40

04/16/18

MDL

NA

0.24

NA

0.19

10.

10.

Sample Depth:

Serial_No:04161816:43

Page 103 of 118

FF



Matrix: Soil


L1811425-02Lab ID:

Qualifier Units RL

SAMPLE RESULTS

Project Name:

Project Number:

Lab Number:

Report Date:

NFTA

17005-02

L1811425

Field Prep:

DateAnalyzed


Not Specified


Date Prepared

-

04/16/18

MDL

NA

Sample Depth:

Serial_No:04161816:43

Page 104 of 118

FF



Matrix: Soil


L1811425-03Lab ID:

Qualifier Units RL

SAMPLE RESULTS

Project Name:

Project Number:

Lab Number:

Report Date:

NFTA

17005-02

L1811425

Field Prep:

DateAnalyzed


Not Specified


Cyanide, Total

pH (H)


Cyanide, Reactive

Sulfide, Reactive

73.0

ND

8.5

ND

ND

ND

%

mg/kg

SU

mg/kg

mg/kg

mg/kg

1

1

1

1

1

1

0.100

1.3

-

1.1

10

10

04/04/18 13:08

04/04/18 13:57

04/04/18 09:52

04/05/18 14:12

04/04/18 18:04

04/04/18 17:34

121,2540G

1,9010C/9012B

1,9045D

1,7196A

125,7.3

125,7.3

RI

LH

GD

NH

RM

RM

Date Prepared

-

04/04/18 09:25

-

04/04/18 23:30

04/04/18 15:40

04/04/18 15:40

04/16/18

MDL

NA

0.28

NA

0.22

10.

10.

Sample Depth:

Serial_No:04161816:43

Page 105 of 118

FF



Matrix: Soil


L1811425-04Lab ID:

Qualifier Units RL

SAMPLE RESULTS

Project Name:

Project Number:

Lab Number:

Report Date:

NFTA

17005-02

L1811425

Field Prep:

DateAnalyzed


Not Specified


Cyanide, Total

pH (H)


Cyanide, Reactive

Sulfide, Reactive

85.2

ND

8.2

ND

ND

ND

%

mg/kg

SU

mg/kg

mg/kg

mg/kg

1

1

1

1

1

1

0.100

1.1

-

0.94

10

10

04/04/18 13:08

04/04/18 13:58

04/04/18 09:52

04/05/18 14:13

04/04/18 18:05

04/04/18 17:35

121,2540G

1,9010C/9012B

1,9045D

1,7196A

125,7.3

125,7.3

RI

LH

GD

NH

RM

RM

Date Prepared

-

04/04/18 09:25

-

04/04/18 23:30

04/04/18 15:40

04/04/18 15:40

04/16/18

MDL

NA

0.24

NA

0.19

10.

10.

Sample Depth:

Serial_No:04161816:43

Page 106 of 118

FF



Project Name:

Project Number:

Lab Number:

Report Date:

NFTA

17005-02

L1811425

DateAnalyzed


Date Prepared

04/16/18

Cyanide, Total

Sulfide, Reactive

Cyanide, Reactive


ND

ND

ND

ND

mg/kg

mg/kg

mg/kg

mg/kg

1

1

1

1

1.0

10

10

0.80

04/04/18 13:47

04/04/18 17:31

04/04/18 18:01

04/05/18 13:58

1,9010C/9012B

125,7.3

125,7.3

1,7196A

LH

RM

RM

NH

04/04/18 09:25

04/04/18 15:40

04/04/18 15:40

04/04/18 23:30

General Chemistry - Westborough Lab for sample(s): 01,03-04 Batch: WG1103345-1




MDL

0.21

10.

10.

0.16

Serial_No:04161816:43

Page 107 of 118

Cyanide, Total

pH

Sulfide, Reactive

Cyanide, Reactive


62

100

103

81

89

53

-

-

-

-

80-120

99-101

60-125

30-125

80-120

21

-

-

-

-

35

40

40

20

ParameterLCS

%RecoveryLCSD

%Recovery%Recovery


General Chemistry - Westborough Lab Associated sample(s): 01,03-04 Batch: WG1103345-2 WG1103345-3

General Chemistry - Westborough Lab Associated sample(s): 01,03-04 Batch: WG1103377-1





Project Name:

Project Number:

Lab Number:

Report Date:

NFTA

17005-02

L1811425

04/16/18

Qual Qual

Q Q

Qual

Serial_No:04161816:43

Page 108 of 118

Cyanide, Total


ND

ND

10

1100

88

110

9.8

-

85

-

75-125

75-125

2

-

35

20


MS Found

MS%Recovery

MSD Found

MSD %Recovery

RecoveryLimits RPD

RPD Limits

General Chemistry - Westborough Lab Associated sample(s): 01,03-04 QC Batch ID: WG1103345-4 WG1103345-5 QC Sample: L1811390-03 Client ID: MS Sample

General Chemistry - Westborough Lab Associated sample(s): 01,03-04 QC Batch ID: WG1103634-4 QC Sample: L1811425-04 Client ID: BH13-18

11

971

MS Added


Project Name:

Project Number:

Lab Number:

Report Date:

NFTA

17005-02

L1811425

04/16/18

Qual Qual Qual

Serial_No:04161816:43

Page 109 of 118

pH (H)

Solids, Total

Sulfide, Reactive

Cyanide, Reactive


9.6

74.5

ND

ND

ND

9.6

76.1

ND

ND

ND

SU

%

mg/kg

mg/kg

mg/kg

0

2

NC

NC

NC

5

20

40

40

20



General Chemistry - Westborough Lab Associated sample(s): 01-04 QC Batch ID: WG1103465-1 QC Sample: L1811487-01 Client ID: DUP Sample

General Chemistry - Westborough Lab Associated sample(s): 01,03-04 QC Batch ID: WG1103535-3 QC Sample: L1811484-01 Client ID: DUP Sample

General Chemistry - Westborough Lab Associated sample(s): 01,03-04 QC Batch ID: WG1103543-3 QC Sample: L1811484-01 Client ID: DUP Sample


NFTA

17005-02

Project Name:

Project Number:

L1811425Lab Number:

Report Date:


04/16/18

Qual

Serial_No:04161816:43

Page 110 of 118


L1811425-01A

L1811425-01A1

L1811425-01B

L1811425-01C

L1811425-01D

L1811425-01E

L1811425-01F

L1811425-01G

L1811425-01S

L1811425-01T

L1811425-01V

L1811425-01W

L1811425-01W9

L1811425-01X

L1811425-01Y

L1811425-01Z

L1811425-02A

L1811425-02B













Tumble Vessel






A

A

A

A

A

A

A

A

A

A

A

A

A

A

A

A

A

A

NA

NA

NA

NA

NA

NA

NA

NA

NA

NA

NA

NA

NA

NA

NA

NA

NA

NA

3.2

3.2

3.2

3.2

3.2

3.2

3.2

3.2

3.2

3.2

3.2

3.2

3.2

3.2

3.2

3.2

3.2

3.2

Y

Y

Y

Y

Y

Y

Y

Y

Y

Y

Y

Y

Y

Y

Y

Y

Y

Y

Absent

Absent

Absent

Absent

Absent

Absent

Absent

Absent

Absent

Absent

Absent

Absent

Absent

Absent

Absent

Absent

Absent

Absent


NFTA

17005-02

TS(7)

TS(7)

BE-TI(180),AS-TI(180),AG-TI(180),CR-TI(180),NI-TI(180),CU-TI(180),PB-TI(180),SE-TI(180),ZN-TI(180),HG-T(28),MN-TI(180),CD-TI(180)

NYTCL-8260-R2(14),TCLP-EXT-ZHE(14)


HEXCR-7196(30)

IGNIT-1030(14),NYTCL-8270(14),REACTS(14),TCN-9010(14),PH-9045(1),NYTCL-8081(14),HERB-8151(14),NYTCL-8082(14),REACTCN(14)

IGNIT-1030(14),NYTCL-8270(14),REACTS(14),TCN-9010(14),BA-TI(180),PH-9045(1),NYTCL-8081(14),HERB-8151(14),NYTCL-8082(14),REACTCN(14)

TCLP-VOA(14)

TCLP-VOA(14)



-

NYTCL-8260-R2(14)

NYTCL-8260-R2(14)

NYTCL-8260-R2(14)

NYTCL-8260-R2(14),TCLP-EXT-ZHE(14),TS(7)

NYTCL-8260-R2(14),TCLP-EXT-ZHE(14),TS(7)

Project Name:

Project Number:

L1811425Lab Number:

Report Date:




Analysis(*)

04/16/18


04-APR-18 12:06

04-APR-18 12:06

FrozenDate/Time

FinalpH

Initial pH

Serial_No:04161816:43

Page 111 of 118


L1811425-02S

L1811425-02T

L1811425-02X

L1811425-02Y

L1811425-02Z

L1811425-03A

L1811425-03A1

L1811425-03B

L1811425-03C

L1811425-03D

L1811425-03E

L1811425-03W

L1811425-03W1

L1811425-03X

L1811425-03X9

L1811425-04A

L1811425-04A1

L1811425-04B

L1811425-04C

L1811425-04D

L1811425-04E















Tumble Vessel







A

A

A

A

A

A

A

A

A

A

A

A

NA

A

A

A

A

A

A

A

A

NA

NA

NA

NA

NA

NA

NA

NA

NA

NA

NA

NA

NA

NA

NA

NA

NA

NA

NA

NA

NA

3.2

3.2

3.2

3.2

3.2

3.2

3.2

3.2

3.2

3.2

3.2

3.2

3.2

3.2

3.2

3.2

3.2

3.2

3.2

3.2

Y

Y

Y

Y

Y

Y

Y

Y

Y

Y

Y

Y

Y

Y

Y

Y

Y

Y

Y

Y

Y

Absent

Absent

Absent

Absent

Absent

Absent

Absent

Absent

Absent

Absent

Absent

Absent

Absent

Absent

Absent

Absent

Absent

Absent

Absent

Absent

Absent

NFTA

17005-02

TCLP-VOA(14)

TCLP-VOA(14)

NYTCL-8260-R2(14)

NYTCL-8260-R2(14)

NYTCL-8260-R2(14)

TS(7)

TS(7)


HEXCR-7196(30)

IGNIT-1030(14),NYTCL-8270(14),REACTS(14),TCN-9010(14),TRICR-CALC(30),PH-9045(1),NYTCL-8081(14),HERB-8151(14),NYTCL-8082(14),REACTCN(14)

IGNIT-1030(14),NYTCL-8270(14),REACTS(14),TCN-9010(14),TRICR-CALC(30),PH-9045(1),NYTCL-8081(14),HERB-8151(14),NYTCL-8082(14),REACTCN(14)




-

TS(7)

TS(7)

BE-TI(180),AS-TI(180),AG-TI(180),CR-TI(180),NI-TI(180),CU-TI(180),PB-TI(180),SE-TI(180),ZN-TI(180),HG-T(28),MN-TI(180),CD-TI(180)



HEXCR-7196(30)

Project Name:

Project Number:

L1811425Lab Number:

Report Date:



Analysis(*)

04/16/18

04-APR-18 12:06

04-APR-18 12:06

FrozenDate/Time

FinalpH

Initial pH

Serial_No:04161816:43

Page 112 of 118


L1811425-04F

L1811425-04G

L1811425-04S

L1811425-04T

L1811425-04V

L1811425-04V1

L1811425-04W

L1811425-04W9

L1811425-04X

L1811425-04Y

L1811425-04Z

L1811425-05A








Tumble Vessel




Vial HCl preserved

A

A

A

A

A

NA

A

A

A

A

A

A

NA

NA

NA

NA

NA

NA

NA

NA

NA

NA

NA

NA

3.2

3.2

3.2

3.2

3.2

3.2

3.2

3.2

3.2

3.2

3.2

Y

Y

Y

Y

Y

Y

Y

Y

Y

Y

Y

Y

Absent

Absent

Absent

Absent

Absent

Absent

Absent

Absent

Absent

Absent

Absent

Absent

NFTA

17005-02

IGNIT-1030(14),NYTCL-8270(14),REACTS(14),TCN-9010(14),PH-9045(1),NYTCL-8081(14),HERB-8151(14),NYTCL-8082(14),REACTCN(14)

IGNIT-1030(14),NYTCL-8270(14),REACTS(14),TCN-9010(14),BA-TI(180),PH-9045(1),NYTCL-8081(14),HERB-8151(14),NYTCL-8082(14),REACTCN(14)

TCLP-VOA(14)

TCLP-VOA(14)




-

NYTCL-8260-R2(14)

NYTCL-8260-R2(14)

NYTCL-8260-R2(14)

NYTCL-8260-R2(14)

Project Name:

Project Number:

L1811425Lab Number:

Report Date:



Analysis(*)

04/16/18

04-APR-18 12:06

04-APR-18 12:06

FrozenDate/Time

FinalpH

Initial pH

Serial_No:04161816:43

Page 113 of 118


GLOSSARY

Project Name:

Project Number:

Lab Number:

Report Date:

L1811425NFTA

17005-02 04/16/18

Acronyms

EDL

EPA

LCS

LCSD

LFB

MDL

MS

MSD

NA

NC

NDPA/DPA

NI

NP

RL

RPD

SRM

STLP

TIC




Not Applicable.


Not Ignitable.




-

-

-

-

-

-

-

-

-

-

-

-

-

-

-

-

-

-

Terms


Data Qualifiers

A

B

-

-




-

Footnotes

Serial_No:04161816:43

Page 114 of 118


Project Name:

Project Number:

Lab Number:

Report Date:

L1811425NFTA

17005-02 04/16/18

Data Qualifiers

C

D

E

G

H

I

M

NJ

P

Q

R

RE

S

-

-

-

-

-

-

-

-

-

-

-

-

-









J

ND

-

-


Serial_No:04161816:43

Page 115 of 118




1

107

121

125





Project Name:

Project Number:

Lab Number:

Report Date:

L1811425NFTA

17005-02

REFERENCES

04/16/18

Serial_No:04161816:43

Page 116 of 118










Serial_No:04161816:43

Page 117 of 118

Serial_No:04161816:43

Page 118 of 118

L1811694


17005-02

NFTA

Client:

Project Name:

Project Number:

04/11/18


Lab Number:

Report Date:


95 Perry Street

Suite 300

Andrew KlimekATTN:

ANALYTICAL REPORT


Buffalo, NY 14203

(716) 206-5100Phone:


Serial_No:04111816:15

Page 1 of 92

L1811694-01

L1811694-02

L1811694-03

L1811694-04

Alpha Sample ID

BH14-18

BH14-18

BH12-18

TRIP BLANK

Client ID

AMTRAK-EXCHANGE ST.

AMTRAK-EXCHANGE ST.

AMTRAK-EXCHANGE ST.

AMTRAK-EXCHANGE ST.

Sample Location

NFTA

17005-02



L181169404/11/18

04/04/18 08:00

04/04/18 10:05

04/04/18 14:45

04/04/18 00:00


SOIL

SOIL

SOIL

WATER

04/04/18

04/04/18

04/04/18

04/04/18

Serial_No:04111816:15

Page 2 of 92

NFTA

17005-02

Project Name:

Project Number:

Lab Number:


04/11/18

Case Narrative






















HOLD POLICY






Serial_No:04111816:15

Page 3 of 92


NFTA

17005-02

Project Name:

Project Number:

Lab Number:


04/11/18

Report Submission


MDL column.

Sample Receipt

L1811694-01 and -03: The analysis of TCLP Volatiles was not received in the recommended container. The

analysis was performed at the client's request.

Volatile Organics

Any reported concentrations that are below 200 ug/kg may be biased low due to the sample not being collected

according to 5035-L/5035A-L low-level specifications.

Total Metals

L1811694-02 and -03: The sample has elevated detection limits for all elements, with the exception of

mercury, due to the dilution required by matrix interferences encountered during analysis.

Cyanide, Total

The WG1105168-2/-3 LCS/LCSD recoveries (74%/63%), associated with L1811694-02 and -03, are outside

our in-house acceptance criteria, but within the vendor-certified acceptance limits. The results of the original

analyses are reported.

Hexavalent Chromium

The WG1103718-2 LCS recovery (73%), associated with L1811694-02 and -03, is outside our in-house

acceptance criteria, but within the vendor-certified acceptance limits. The results of the original analyses are

reported.

The WG1103718-5 The Soluble MS recovery (72%) was below criteria. This has been attributed to matrix

interference. A post-spike was performed with an acceptable recovery (107%).




Serial_No:04111816:15

Page 4 of 92

ORGANICS

Serial_No:04111816:15

Page 5 of 92

VOLATILES

Serial_No:04111816:15

Page 6 of 92

FF

Chloroform


Tetrachloroethene

Chlorobenzene

1,2-Dichloroethane

Benzene

Vinyl chloride

1,1-Dichloroethene

Trichloroethene

1,4-Dichlorobenzene

2-Butanone

Parameter Result

J

Dilution Factor

ND

ND

ND

ND

ND

ND

ND

ND

2.2

ND

ND

ug/l

ug/l

ug/l

ug/l

ug/l

ug/l

ug/l

ug/l

ug/l

ug/l

ug/l

10

10

10

10

10

10

10

10

10

10

10

Qualifier Units RL


SAMPLE RESULTS

Project Name:

Project Number:

Lab Number:

Report Date:

NFTA

17005-02

L1811694

7.5

5.0

5.0

5.0

5.0

5.0

10

5.0

5.0

25

50


Toluene-d8



93

106

102

95

70-130

70-130

70-130

70-130


04/11/18



L1811694-01Lab ID:



1,8260C04/10/18 09:40MM


80%Percent Solids:

MDL

2.2

1.3

1.8

1.8

1.3

1.6

0.71

1.7

1.8

1.9

19.

Sample Depth:

Serial_No:04111816:15

Page 7 of 92

Methylene chloride

1,1-Dichloroethane

Chloroform


Tetrachloroethene

Chlorobenzene

1,2-Dichloroethane


Benzene

Toluene

Ethylbenzene

Vinyl chloride

1,1-Dichloroethene


Trichloroethene

1,2-Dichlorobenzene

1,3-Dichlorobenzene

1,4-Dichlorobenzene


p/m-Xylene

o-Xylene


Acetone

2-Butanone

n-Butylbenzene

sec-Butylbenzene

tert-Butylbenzene

n-Propylbenzene

Parameter Result

J

Dilution Factor

ND

ND

ND

ND

ND

ND

ND

ND

ND

ND

ND

ND

ND

ND

ND

ND

ND

ND

ND

ND

ND

ND

9.0

ND

ND

ND

ND

ND

ug/kg

ug/kg

ug/kg

ug/kg

ug/kg

ug/kg

ug/kg

ug/kg

ug/kg

ug/kg

ug/kg

ug/kg

ug/kg

ug/kg

ug/kg

ug/kg

ug/kg

ug/kg

ug/kg

ug/kg

ug/kg

ug/kg

ug/kg

ug/kg

ug/kg

ug/kg

ug/kg

ug/kg

1

1

1

1

1

1

1

1

1

1

1

1

1

1

1

1

1

1

1

1

1

1

1

1

1

1

1

1

Qualifier Units RL


SAMPLE RESULTS

Project Name:

Project Number:

Lab Number:

Report Date:

NFTA

17005-02

L1811694

9.8

1.5

1.5

0.98

0.98

0.98

0.98

0.98

0.98

1.5

0.98

2.0

0.98

1.5

0.98

4.9

4.9

4.9

2.0

2.0

2.0

0.98

9.8

9.8

0.98

0.98

4.9

0.98

04/11/18



L1811694-01Lab ID:




MDL

1.6

0.26

0.36

0.34

0.30

0.34

0.24

0.34

0.19

0.19

0.17

0.31

0.36

0.24

0.30

0.18

0.21

0.18

0.15

0.34

0.33

0.34

2.2

0.68

0.22

0.21

0.24

0.21

Sample Depth:

Serial_No:04111816:15

Page 8 of 92



1,4-Dioxane


ND

ND

ND

ug/kg

ug/kg

ug/kg

1

1

1

Qualifier Units RL


SAMPLE RESULTS

Project Name:

Project Number:

Lab Number:

Report Date:

NFTA

17005-02

L1811694

4.9

4.9

39


Toluene-d8



112

107

107

95

70-130

70-130

70-130

70-130


04/11/18



L1811694-01Lab ID:


MDL

0.16

0.18

14.

Sample Depth:

Serial_No:04111816:15

Page 9 of 92

Chloroform


Tetrachloroethene

Chlorobenzene

1,2-Dichloroethane

Benzene

Vinyl chloride

1,1-Dichloroethene

Trichloroethene

1,4-Dichlorobenzene

2-Butanone


ND

ND

ND

ND

ND

ND

ND

ND

ND

ND

ND

ug/l

ug/l

ug/l

ug/l

ug/l

ug/l

ug/l

ug/l

ug/l

ug/l

ug/l

10

10

10

10

10

10

10

10

10

10

10

Qualifier Units RL


SAMPLE RESULTS

Project Name:

Project Number:

Lab Number:

Report Date:

NFTA

17005-02

L1811694

7.5

5.0

5.0

5.0

5.0

5.0

10

5.0

5.0

25

50


Toluene-d8



94

106

103

95

70-130

70-130

70-130

70-130


04/11/18



L1811694-03Lab ID:



1,8260C04/10/18 10:14MM


84%Percent Solids:

MDL

2.2

1.3

1.8

1.8

1.3

1.6

0.71

1.7

1.8

1.9

19.

Sample Depth:

Serial_No:04111816:15

Page 10 of 92

Methylene chloride

1,1-Dichloroethane

Chloroform


Tetrachloroethene

Chlorobenzene

1,2-Dichloroethane


Benzene

Toluene

Ethylbenzene

Vinyl chloride

1,1-Dichloroethene


Trichloroethene

1,2-Dichlorobenzene

1,3-Dichlorobenzene

1,4-Dichlorobenzene


p/m-Xylene

o-Xylene


Acetone

2-Butanone

n-Butylbenzene

sec-Butylbenzene

tert-Butylbenzene

n-Propylbenzene

Parameter Result

J

J

Dilution Factor

ND

ND

ND

ND

ND

ND

ND

ND

ND

0.33

ND

ND

ND

ND

ND

ND

ND

ND

ND

ND

ND

ND

47

2.1

ND

ND

ND

ND

ug/kg

ug/kg

ug/kg

ug/kg

ug/kg

ug/kg

ug/kg

ug/kg

ug/kg

ug/kg

ug/kg

ug/kg

ug/kg

ug/kg

ug/kg

ug/kg

ug/kg

ug/kg

ug/kg

ug/kg

ug/kg

ug/kg

ug/kg

ug/kg

ug/kg

ug/kg

ug/kg

ug/kg

1

1

1

1

1

1

1

1

1

1

1

1

1

1

1

1

1

1

1

1

1

1

1

1

1

1

1

1

Qualifier Units RL


SAMPLE RESULTS

Project Name:

Project Number:

Lab Number:

Report Date:

NFTA

17005-02

L1811694

8.1

1.2

1.2

0.81

0.81

0.81

0.81

0.81

0.81

1.2

0.81

1.6

0.81

1.2

0.81

4.1

4.1

4.1

1.6

1.6

1.6

0.81

8.1

8.1

0.81

0.81

4.1

0.81

04/11/18



L1811694-03Lab ID:




MDL

1.3

0.22

0.30

0.28

0.24

0.28

0.20

0.28

0.16

0.16

0.14

0.26

0.30

0.20

0.24

0.15

0.18

0.15

0.12

0.28

0.28

0.28

1.9

0.56

0.18

0.18

0.20

0.18

Sample Depth:

Serial_No:04111816:15

Page 11 of 92



1,4-Dioxane

Parameter Result

J

Dilution Factor

ND

0.58

ND

ug/kg

ug/kg

ug/kg

1

1

1

Qualifier Units RL


SAMPLE RESULTS

Project Name:

Project Number:

Lab Number:

Report Date:

NFTA

17005-02

L1811694

4.1

4.1

32


Toluene-d8



109

117

124

82

70-130

70-130

70-130

70-130


04/11/18



L1811694-03Lab ID:


MDL

0.13

0.15

12.

Sample Depth:

Serial_No:04111816:15

Page 12 of 92

Methylene chloride

1,1-Dichloroethane

Chloroform


Tetrachloroethene

Chlorobenzene

1,2-Dichloroethane


Benzene

Toluene

Ethylbenzene

Vinyl chloride

1,1-Dichloroethene


Trichloroethene

1,2-Dichlorobenzene

1,3-Dichlorobenzene

1,4-Dichlorobenzene


p/m-Xylene

o-Xylene


Acetone

2-Butanone

n-Butylbenzene

sec-Butylbenzene

tert-Butylbenzene

n-Propylbenzene


ND

ND

ND

ND

ND

ND

ND

ND

ND

ND

ND

ND

ND

ND

ND

ND

ND

ND

ND

ND

ND

ND

ND

ND

ND

ND

ND

ND

ug/l

ug/l

ug/l

ug/l

ug/l

ug/l

ug/l

ug/l

ug/l

ug/l

ug/l

ug/l

ug/l

ug/l

ug/l

ug/l

ug/l

ug/l

ug/l

ug/l

ug/l

ug/l

ug/l

ug/l

ug/l

ug/l

ug/l

ug/l

1

1

1

1

1

1

1

1

1

1

1

1

1

1

1

1

1

1

1

1

1

1

1

1

1

1

1

1

Qualifier Units RL


SAMPLE RESULTS

Project Name:

Project Number:

Lab Number:

Report Date:

NFTA

17005-02

L1811694

2.5

2.5

2.5

0.50

0.50

2.5

0.50

2.5

0.50

2.5

2.5

1.0

0.50

2.5

0.50

2.5

2.5

2.5

2.5

2.5

2.5

2.5

5.0

5.0

2.5

2.5

2.5

2.5

04/11/18



L1811694-04Lab ID:



1,8260C04/09/18 10:15PK

MDL

0.70

0.70

0.70

0.13

0.18

0.70

0.13

0.70

0.16

0.70

0.70

0.07

0.17

0.70

0.18

0.70

0.70

0.70

0.70

0.70

0.70

0.70

1.5

1.9

0.70

0.70

0.70

0.70

Sample Depth:

Serial_No:04111816:15

Page 13 of 92



1,4-Dioxane


ND

ND

ND

ug/l

ug/l

ug/l

1

1

1

Qualifier Units RL


SAMPLE RESULTS

Project Name:

Project Number:

Lab Number:

Report Date:

NFTA

17005-02

L1811694

2.5

2.5

250


Toluene-d8



97

105

117

90

70-130

70-130

70-130

70-130


04/11/18



L1811694-04Lab ID:


MDL

0.70

0.70

61.

Sample Depth:

Serial_No:04111816:15

Page 14 of 92


Project Name:

Project Number:

Lab Number:

Report Date:

NFTA

17005-02

L1811694


Analytical Date:

04/11/18

Analyst: MV

Methylene chloride

1,1-Dichloroethane

Chloroform


Tetrachloroethene

Chlorobenzene

1,2-Dichloroethane


Benzene

Toluene

Ethylbenzene

Vinyl chloride

1,1-Dichloroethene


Trichloroethene

1,2-Dichlorobenzene

1,3-Dichlorobenzene

1,4-Dichlorobenzene


p/m-Xylene

o-Xylene


Acetone

2-Butanone

n-Butylbenzene

sec-Butylbenzene

tert-Butylbenzene

n-Propylbenzene


Parameter Result

ND

ND

ND

ND

ND

ND

ND

ND

ND

0.67

ND

ND

ND

ND

ND

ND

ND

ND

ND

ND

ND

ND

ND

ND

ND

ND

ND

ND

ND

RL

10

1.5

1.5

1.0

1.0

1.0

1.0

1.0

1.0

1.5

1.0

2.0

1.0

1.5

1.0

5.0

5.0

5.0

2.0

2.0

2.0

1.0

10

10

1.0

1.0

5.0

1.0

5.0

J

ug/kg

ug/kg

ug/kg

ug/kg

ug/kg

ug/kg

ug/kg

ug/kg

ug/kg

ug/kg

ug/kg

ug/kg

ug/kg

ug/kg

ug/kg

ug/kg

ug/kg

ug/kg

ug/kg

ug/kg

ug/kg

ug/kg

ug/kg

ug/kg

ug/kg

ug/kg

ug/kg

ug/kg

ug/kg

UnitsQualifier


MDL

1.6

0.27

0.37

0.34

0.30

0.35

0.25

0.35

0.19

0.20

0.17

0.32

0.37

0.24

0.30

0.18

0.22

0.18

0.15

0.35

0.34

0.34

2.3

0.69

0.23

0.22

0.25

0.22

0.16

Serial_No:04111816:15

Page 15 of 92


Project Name:

Project Number:

Lab Number:

Report Date:

NFTA

17005-02

L1811694


Analytical Date:

04/11/18

Analyst: MV


1,4-Dioxane

Parameter Result

ND

ND

RL

5.0

40

ug/kg

ug/kg

UnitsQualifier



Toluene-d8



108

106

105

92

70-130

70-130

70-130

70-130


Criteria

MDL

0.19

14.

Serial_No:04111816:15

Page 16 of 92


Project Name:

Project Number:

Lab Number:

Report Date:

NFTA

17005-02

L1811694


Analytical Date:

04/11/18

Analyst: PD

Methylene chloride

1,1-Dichloroethane

Chloroform


Tetrachloroethene

Chlorobenzene

1,2-Dichloroethane


Benzene

Toluene

Ethylbenzene

Vinyl chloride

1,1-Dichloroethene


Trichloroethene

1,2-Dichlorobenzene

1,3-Dichlorobenzene

1,4-Dichlorobenzene


p/m-Xylene

o-Xylene


Acetone

2-Butanone

n-Butylbenzene

sec-Butylbenzene

tert-Butylbenzene

n-Propylbenzene


Parameter Result

ND

ND

ND

ND

ND

ND

ND

ND

ND

ND

ND

ND

ND

ND

ND

ND

ND

ND

ND

ND

ND

ND

ND

ND

ND

ND

ND

ND

ND

RL

2.5

2.5

2.5

0.50

0.50

2.5

0.50

2.5

0.50

2.5

2.5

1.0

0.50

2.5

0.50

2.5

2.5

2.5

2.5

2.5

2.5

2.5

5.0

5.0

2.5

2.5

2.5

2.5

2.5

ug/l

ug/l

ug/l

ug/l

ug/l

ug/l

ug/l

ug/l

ug/l

ug/l

ug/l

ug/l

ug/l

ug/l

ug/l

ug/l

ug/l

ug/l

ug/l

ug/l

ug/l

ug/l

ug/l

ug/l

ug/l

ug/l

ug/l

ug/l

ug/l

UnitsQualifier


MDL

0.70

0.70

0.70

0.13

0.18

0.70

0.13

0.70

0.16

0.70

0.70

0.07

0.17

0.70

0.18

0.70

0.70

0.70

0.70

0.70

0.70

0.70

1.5

1.9

0.70

0.70

0.70

0.70

0.70

Serial_No:04111816:15

Page 17 of 92


Project Name:

Project Number:

Lab Number:

Report Date:

NFTA

17005-02

L1811694


Analytical Date:

04/11/18

Analyst: PD


1,4-Dioxane

Parameter Result

ND

ND

RL

2.5

250

ug/l

ug/l

UnitsQualifier



Toluene-d8



96

104

115

92

70-130

70-130

70-130

70-130


Criteria

MDL

0.70

61.

Serial_No:04111816:15

Page 18 of 92


Project Name:

Project Number:

Lab Number:

Report Date:

NFTA

17005-02

L1811694



04/11/18

Analyst: MM

Chloroform


Tetrachloroethene

Chlorobenzene

1,2-Dichloroethane

Benzene

Vinyl chloride

1,1-Dichloroethene

Trichloroethene

1,4-Dichlorobenzene

2-Butanone

Parameter Result

ND

ND

ND

ND

ND

ND

ND

ND

ND

ND

ND

RL

7.5

5.0

5.0

5.0

5.0

5.0

10

5.0

5.0

25

50

ug/l

ug/l

ug/l

ug/l

ug/l

ug/l

ug/l

ug/l

ug/l

ug/l

ug/l

UnitsQualifier

TCLP Volatiles by EPA 1311 - Westborough Lab for sample(s): 01,03 Batch: WG1105103-5


Toluene-d8



97

106

103

95

70-130

70-130

70-130

70-130


Criteria


MDL

2.2

1.3

1.8

1.8

1.3

1.6

0.71

1.7

1.8

1.9

19.

Serial_No:04111816:15

Page 19 of 92

Methylene chloride

1,1-Dichloroethane

Chloroform


Tetrachloroethene

Chlorobenzene

1,2-Dichloroethane


Benzene

Toluene

Ethylbenzene

Vinyl chloride

1,1-Dichloroethene


Trichloroethene

1,2-Dichlorobenzene

1,3-Dichlorobenzene

1,4-Dichlorobenzene


p/m-Xylene

o-Xylene


Acetone

85

91

83

85

85

90

96

83

84

94

92

92

73

80

82

94

93

91

94

85

85

82

189

85

93

85

87

87

92

96

86

85

97

93

95

74

82

83

95

95

93

91

88

87

84

196

70-130

70-130

70-130

70-130

70-130

70-130

70-130

70-130

70-130

70-130

70-130

67-130

65-135

70-130

70-130

70-130

70-130

70-130

66-130

70-130

70-130

70-130

54-140

0

2

2

2

2

2

0

4

1

3

1

3

1

2

1

1

2

2

3

3

2

2

4

30

30

30

30

30

30

30

30

30

30

30

30

30

30

30

30

30

30

30

30

30

30

30

ParameterLCS

%RecoveryLCSD

%Recovery%Recovery

Limits RPDRPD

Limits



Project Name:

Project Number:

Lab Number:

Report Date:

NFTA

17005-02

L1811694

04/11/18

Qual Qual

Q Q

Qual

Serial_No:04111816:15

Page 20 of 92

2-Butanone

n-Butylbenzene

sec-Butylbenzene

tert-Butylbenzene

n-Propylbenzene



1,4-Dioxane

137

98

96

94

97

94

98

89

137

101

99

97

101

97

100

85

70-130

70-130

70-130

70-130

70-130

70-130

70-130

65-136

0

3

3

3

4

3

2

5

30

30

30

30

30

30

30

30

ParameterLCS

%RecoveryLCSD

%Recovery%Recovery

Limits RPDRPD

Limits



Project Name:

Project Number:

Lab Number:

Report Date:

NFTA

17005-02

L1811694


10510610491

70-13070-13070-13070-130

10410710591


04/11/18

AcceptanceCriteria

Qual Qual

Q Q

Qual

Serial_No:04111816:15

Page 21 of 92

Methylene chloride

1,1-Dichloroethane

Chloroform


Tetrachloroethene

Chlorobenzene

1,2-Dichloroethane


Benzene

Toluene

Ethylbenzene

Vinyl chloride

1,1-Dichloroethene


Trichloroethene

1,2-Dichlorobenzene

1,3-Dichlorobenzene

1,4-Dichlorobenzene


p/m-Xylene

o-Xylene


Acetone

84

96

98

110

90

90

92

110

95

94

100

57

79

88

95

89

94

92

92

100

95

90

110

86

96

97

110

91

91

95

100

94

93

100

56

76

88

95

90

92

92

94

95

95

88

110

70-130

70-130

70-130

63-132

70-130

75-130

70-130

67-130

70-130

70-130

70-130

55-140

61-145

70-130

70-130

70-130

70-130

70-130

63-130

70-130

70-130

70-130

58-148

2

0

1

0

1

1

3

10

1

1

0

2

4

0

0

1

2

0

2

5

0

2

0

20

20

20

20

20

20

20

20

20

20

20

20

20

20

20

20

20

20

20

20

20

20

20

ParameterLCS

%RecoveryLCSD

%Recovery%Recovery

Limits RPDRPD

Limits



Project Name:

Project Number:

Lab Number:

Report Date:

NFTA

17005-02

L1811694

04/11/18

Qual Qual Qual

Serial_No:04111816:15

Page 22 of 92

2-Butanone

n-Butylbenzene

sec-Butylbenzene

tert-Butylbenzene

n-Propylbenzene



1,4-Dioxane

95

130

120

97

110

110

110

78

100

120

120

94

110

100

110

118

63-138

53-136

70-130

70-130

69-130

64-130

70-130

56-162

5

8

0

3

0

10

0

41

20

20

20

20

20

20

20

20

ParameterLCS

%RecoveryLCSD

%Recovery%Recovery

Limits RPDRPD

Limits



Project Name:

Project Number:

Lab Number:

Report Date:

NFTA

17005-02

L1811694


9510011494

70-13070-13070-13070-130

10010211295


04/11/18

AcceptanceCriteria

Qual Qual Qual

Q

Serial_No:04111816:15

Page 23 of 92

Chloroform


Tetrachloroethene

Chlorobenzene

1,2-Dichloroethane

Benzene

Vinyl chloride

1,1-Dichloroethene

Trichloroethene

1,4-Dichlorobenzene

2-Butanone

92

82

100

96

86

93

86

84

92

94

86

90

80

100

96

88

93

85

82

92

93

82

70-130

63-132

70-130

75-130

70-130

70-130

55-140

61-145

70-130

70-130

63-138

2

2

0

0

2

0

1

2

0

1

5

20

20

20

25

20

25

20

25

25

20

20

ParameterLCS

%RecoveryLCSD

%Recovery%Recovery

Limits RPDRPD

Limits

TCLP Volatiles by EPA 1311 - Westborough Lab Associated sample(s): 01,03 Batch: WG1105103-3 WG1105103-4


Project Name:

Project Number:

Lab Number:

Report Date:

NFTA

17005-02

L1811694


9210610695

70-13070-13070-13070-130

9210810796


04/11/18

AcceptanceCriteria

Qual Qual Qual

Serial_No:04111816:15

Page 24 of 92

SEMIVOLATILES

Serial_No:04111816:15

Page 25 of 92

FF

Hexachlorobenzene

2,4-Dinitrotoluene

Hexachlorobutadiene

Hexachloroethane

Nitrobenzene


Pentachlorophenol

2-Methylphenol



Pyridine


ND

ND

ND

ND

ND

ND

ND

ND

ND

ND

ND

ug/l

ug/l

ug/l

ug/l

ug/l

ug/l

ug/l

ug/l

ug/l

ug/l

ug/l

1

1

1

1

1

1

1

1

1

1

1

Qualifier Units RL


SAMPLE RESULTS

Project Name:

Project Number:

Lab Number:

Report Date:

NFTA

17005-02

L1811694

10

25

10

10

10

25

50

25

25

25

18

2-Fluorophenol

Phenol-d6

Nitrobenzene-d5

2-Fluorobiphenyl


4-Terphenyl-d14

59

90

59

78

93

85

21-120

10-120

23-120

15-120

10-120

33-120


04/11/18



L1811694-02Lab ID:




1,8270D04/09/18 12:36RC



77%Percent Solids:

MDL

2.9

4.2

3.6

3.4

3.8

3.4

17.

5.1

5.6

3.6

9.4

Sample Depth:

Serial_No:04111816:15

Page 26 of 92

Acenaphthene

Hexachlorobenzene

Fluoranthene

Naphthalene

Benzo(a)anthracene

Benzo(a)pyrene



Chrysene

Acenaphthylene

Anthracene

Benzo(ghi)perylene

Fluorene

Phenanthrene



Pyrene

Dibenzofuran

Pentachlorophenol

Phenol

2-Methylphenol


Parameter Result

J

J

J

J

J

J

J

J

J

Dilution Factor

ND

ND

98

ND

53

60

74

ND

53

ND

ND

44

ND

45

ND

50

77

ND

ND

ND

ND

ND

ug/kg

ug/kg

ug/kg

ug/kg

ug/kg

ug/kg

ug/kg

ug/kg

ug/kg

ug/kg

ug/kg

ug/kg

ug/kg

ug/kg

ug/kg

ug/kg

ug/kg

ug/kg

ug/kg

ug/kg

ug/kg

ug/kg

1

1

1

1

1

1

1

1

1

1

1

1

1

1

1

1

1

1

1

1

1

1

Qualifier Units RL


SAMPLE RESULTS

Project Name:

Project Number:

Lab Number:

Report Date:

NFTA

17005-02

L1811694

170

130

130

210

130

170

130

130

130

170

130

170

210

130

130

170

130

210

170

210

210

310

04/11/18



L1811694-02Lab ID:




1,8270D04/10/18 07:10TT


77%Percent Solids:

MDL

22.

24.

24.

26.

24.

52.

36.

34.

22.

33.

42.

25.

21.

26.

25.

30.

21.

20.

47.

32.

33.

34.

Sample Depth:

Serial_No:04111816:15

Page 27 of 92



SAMPLE RESULTS

Project Name:

Project Number:

Lab Number:

Report Date:

NFTA

17005-02

L1811694

2-Fluorophenol

Phenol-d6

Nitrobenzene-d5

2-Fluorobiphenyl


4-Terphenyl-d14

69

75

66

52

73

34

25-120

10-120

23-120

30-120

10-136

18-120


04/11/18



L1811694-02Lab ID:


MDL

Sample Depth:

Serial_No:04111816:15

Page 28 of 92

Hexachlorobenzene

2,4-Dinitrotoluene

Hexachlorobutadiene

Hexachloroethane

Nitrobenzene


Pentachlorophenol

2-Methylphenol



Pyridine


ND

ND

ND

ND

ND

ND

ND

ND

ND

ND

ND

ug/l

ug/l

ug/l

ug/l

ug/l

ug/l

ug/l

ug/l

ug/l

ug/l

ug/l

1

1

1

1

1

1

1

1

1

1

1

Qualifier Units RL


SAMPLE RESULTS

Project Name:

Project Number:

Lab Number:

Report Date:

NFTA

17005-02

L1811694

10

25

10

10

10

25

50

25

25

25

18

2-Fluorophenol

Phenol-d6

Nitrobenzene-d5

2-Fluorobiphenyl


4-Terphenyl-d14

43

59

41

72

91

77

21-120

10-120

23-120

15-120

10-120

33-120


04/11/18



L1811694-03Lab ID:




1,8270D04/09/18 13:03RC



84%Percent Solids:

MDL

2.9

4.2

3.6

3.4

3.8

3.4

17.

5.1

5.6

3.6

9.4

Sample Depth:

Serial_No:04111816:15

Page 29 of 92

Acenaphthene

Hexachlorobenzene

Fluoranthene

Naphthalene

Benzo(a)anthracene

Benzo(a)pyrene



Chrysene

Acenaphthylene

Anthracene

Benzo(ghi)perylene

Fluorene

Phenanthrene



Pyrene

Dibenzofuran

Pentachlorophenol

Phenol

2-Methylphenol


Parameter Result

J

J

J

J

J

J

J

J

Dilution Factor

32

ND

410

ND

160

130

160

56

140

ND

100

83

31

330

24

85

340

ND

ND

ND

ND

ND

ug/kg

ug/kg

ug/kg

ug/kg

ug/kg

ug/kg

ug/kg

ug/kg

ug/kg

ug/kg

ug/kg

ug/kg

ug/kg

ug/kg

ug/kg

ug/kg

ug/kg

ug/kg

ug/kg

ug/kg

ug/kg

ug/kg

1

1

1

1

1

1

1

1

1

1

1

1

1

1

1

1

1

1

1

1

1

1

Qualifier Units RL


SAMPLE RESULTS

Project Name:

Project Number:

Lab Number:

Report Date:

NFTA

17005-02

L1811694

160

120

120

190

120

160

120

120

120

160

120

160

190

120

120

160

120

190

160

190

190

280

04/11/18



L1811694-03Lab ID:




1,8270D04/11/18 13:19EK


84%Percent Solids:

MDL

20.

22.

22.

24.

22.

48.

33.

31.

20.

30.

38.

23.

19.

24.

22.

27.

19.

18.

43.

29.

30.

30.

Sample Depth:

Serial_No:04111816:15

Page 30 of 92



SAMPLE RESULTS

Project Name:

Project Number:

Lab Number:

Report Date:

NFTA

17005-02

L1811694

2-Fluorophenol

Phenol-d6

Nitrobenzene-d5

2-Fluorobiphenyl


4-Terphenyl-d14

74

74

66

72

86

79

25-120

10-120

23-120

30-120

10-136

18-120


04/11/18



L1811694-03Lab ID:


MDL

Sample Depth:

Serial_No:04111816:15

Page 31 of 92


Project Name:

Project Number:

Lab Number:

Report Date:

NFTA

17005-02

L1811694



04/11/18

Analyst: ALS

Acenaphthene

Hexachlorobenzene

Fluoranthene

Naphthalene

Benzo(a)anthracene

Benzo(a)pyrene



Chrysene

Acenaphthylene

Anthracene

Benzo(ghi)perylene

Fluorene

Phenanthrene



Pyrene

Dibenzofuran

Pentachlorophenol

Phenol

2-Methylphenol


Parameter Result

ND

ND

ND

ND

ND

ND

ND

ND

ND

ND

ND

ND

ND

ND

ND

ND

ND

ND

ND

ND

ND

ND

RL

130

100

100

170

100

130

100

100

100

130

100

130

170

100

100

130

100

170

130

170

170

240

ug/kg

ug/kg

ug/kg

ug/kg

ug/kg

ug/kg

ug/kg

ug/kg

ug/kg

ug/kg

ug/kg

ug/kg

ug/kg

ug/kg

ug/kg

ug/kg

ug/kg

ug/kg

ug/kg

ug/kg

ug/kg

ug/kg

UnitsQualifier




MDL

17.

19.

19.

20.

19.

41.

28.

27.

17.

26.

32.

20.

16.

20.

19.

23.

16.

16.

37.

25.

26.

26.

Serial_No:04111816:15

Page 32 of 92


Project Name:

Project Number:

Lab Number:

Report Date:

NFTA

17005-02

L1811694



04/11/18

Analyst: ALS



2-Fluorophenol

Phenol-d6

Nitrobenzene-d5

2-Fluorobiphenyl


4-Terphenyl-d14

76

79

70

67

80

72

25-120

10-120

23-120

30-120

10-136

18-120


Criteria

MDL

Serial_No:04111816:15

Page 33 of 92


Project Name:

Project Number:

Lab Number:

Report Date:

NFTA

17005-02

L1811694



04/11/18

Analyst: RC

Hexachlorobenzene

2,4-Dinitrotoluene

Hexachlorobutadiene

Hexachloroethane

Nitrobenzene


Pentachlorophenol

2-Methylphenol



Pyridine

Parameter Result

ND

ND

ND

ND

ND

ND

ND

ND

ND

ND

ND

RL

10

25

10

10

10

25

50

25

25

25

18

ug/l

ug/l

ug/l

ug/l

ug/l

ug/l

ug/l

ug/l

ug/l

ug/l

ug/l

UnitsQualifier

TCLP Semivolatiles by EPA 1311 - Westborough Lab for sample(s): 02-03 Batch: WG1104502-1

2-Fluorophenol

Phenol-d6

Nitrobenzene-d5

2-Fluorobiphenyl


4-Terphenyl-d14

70

83

78

75

95

82

21-120

10-120

23-120

15-120

10-120

33-120


Criteria


MDL

2.9

4.2

3.6

3.4

3.8

3.4

17.

5.1

5.6

3.6

9.4

Serial_No:04111816:15

Page 34 of 92


Project Name:

Project Number:

Lab Number:

Report Date:

NFTA

17005-02

L1811694



04/11/18

Analyst: EK

Acenaphthene

Hexachlorobenzene

Fluoranthene

Naphthalene

Benzo(a)anthracene

Benzo(a)pyrene



Chrysene

Acenaphthylene

Anthracene

Benzo(ghi)perylene

Fluorene

Phenanthrene



Pyrene

Dibenzofuran

Pentachlorophenol

Phenol

2-Methylphenol


Parameter Result

ND

ND

ND

ND

ND

ND

ND

ND

ND

ND

ND

ND

ND

ND

ND

ND

ND

ND

ND

ND

ND

ND

RL

130

97

97

160

97

130

97

97

97

130

97

130

160

97

97

130

97

160

130

160

160

230

ug/kg

ug/kg

ug/kg

ug/kg

ug/kg

ug/kg

ug/kg

ug/kg

ug/kg

ug/kg

ug/kg

ug/kg

ug/kg

ug/kg

ug/kg

ug/kg

ug/kg

ug/kg

ug/kg

ug/kg

ug/kg

ug/kg

UnitsQualifier




MDL

17.

18.

19.

20.

18.

40.

27.

26.

17.

25.

32.

19.

16.

20.

19.

22.

16.

15.

36.

24.

25.

25.

Serial_No:04111816:15

Page 35 of 92


Project Name:

Project Number:

Lab Number:

Report Date:

NFTA

17005-02

L1811694



04/11/18

Analyst: EK



2-Fluorophenol

Phenol-d6

Nitrobenzene-d5

2-Fluorobiphenyl


4-Terphenyl-d14

78

75

66

71

76

74

25-120

10-120

23-120

30-120

10-136

18-120


Criteria

MDL

Serial_No:04111816:15

Page 36 of 92

Acenaphthene

Hexachlorobenzene

Fluoranthene

Naphthalene

Benzo(a)anthracene

Benzo(a)pyrene



Chrysene

Acenaphthylene

Anthracene

Benzo(ghi)perylene

Fluorene

Phenanthrene



Pyrene

Dibenzofuran

Pentachlorophenol

Phenol

2-Methylphenol


74

76

80

72

78

83

84

76

77

77

81

79

80

77

81

86

77

78

76

83

81

85

75

74

79

74

78

83

83

76

77

77

79

79

78

76

80

84

76

76

74

84

84

88

31-137

40-140

40-140

40-140

40-140

40-140

40-140

40-140

40-140

40-140

40-140

40-140

40-140

40-140

40-140

40-140

35-142

40-140

17-109

26-90

30-130.

30-130

1

3

1

3

0

0

1

0

0

0

3

0

3

1

1

2

1

3

3

1

4

3

50

50

50

50

50

50

50

50

50

50

50

50

50

50

50

50

50

50

50

50

50

50

ParameterLCS

%RecoveryLCSD

%Recovery%Recovery

Limits RPDRPD

Limits



Project Name:

Project Number:

Lab Number:

Report Date:

NFTA

17005-02

L1811694

04/11/18

Qual Qual Qual

Serial_No:04111816:15

Page 37 of 92

ParameterLCS

%RecoveryLCSD

%Recovery%Recovery

Limits RPDRPD

Limits



Project Name:

Project Number:

Lab Number:

Report Date:

NFTA

17005-02

L1811694


838475688975

25-12010-12023-12030-12010-13618-120

868676698875


04/11/18

AcceptanceCriteria

Qual Qual Qual

Serial_No:04111816:15

Page 38 of 92

Hexachlorobenzene

2,4-Dinitrotoluene

Hexachlorobutadiene

Hexachloroethane

Nitrobenzene


Pentachlorophenol

2-Methylphenol



Pyridine

84

92

81

82

76

88

84

77

81

102

29

88

93

79

63

70

93

83

68

72

105

37

40-140

40-132

28-111

21-105

40-140

30-130

9-103

30-130

30-130

30-130

10-66

5

1

3

26

8

6

1

12

12

3

24

30

30

30

30

30

30

30

30

30

30

30

ParameterLCS

%RecoveryLCSD

%Recovery%Recovery

Limits RPDRPD

Limits

TCLP Semivolatiles by EPA 1311 - Westborough Lab Associated sample(s): 02-03 Batch: WG1104502-2 WG1104502-3


Project Name:

Project Number:

Lab Number:

Report Date:

NFTA

17005-02

L1811694


454668779577

21-12010-12023-12015-12010-12033-120

10091627710085


04/11/18

AcceptanceCriteria

Qual Qual Qual

Serial_No:04111816:15

Page 39 of 92

Acenaphthene

Hexachlorobenzene

Fluoranthene

Naphthalene

Benzo(a)anthracene

Benzo(a)pyrene



Chrysene

Acenaphthylene

Anthracene

Benzo(ghi)perylene

Fluorene

Phenanthrene



Pyrene

Dibenzofuran

Pentachlorophenol

Phenol

2-Methylphenol


71

73

75

71

74

75

72

77

76

78

76

72

76

72

72

73

77

74

52

72

71

80

72

74

75

70

74

75

73

76

75

78

75

71

75

71

72

73

74

75

53

72

72

82

31-137

40-140

40-140

40-140

40-140

40-140

40-140

40-140

40-140

40-140

40-140

40-140

40-140

40-140

40-140

40-140

35-142

40-140

17-109

26-90

30-130.

30-130

1

1

0

1

0

0

1

1

1

0

1

1

1

1

0

0

4

1

2

0

1

2

50

50

50

50

50

50

50

50

50

50

50

50

50

50

50

50

50

50

50

50

50

50

ParameterLCS

%RecoveryLCSD

%Recovery%Recovery

Limits RPDRPD

Limits



Project Name:

Project Number:

Lab Number:

Report Date:

NFTA

17005-02

L1811694

04/11/18

Qual Qual Qual

Serial_No:04111816:15

Page 40 of 92

ParameterLCS

%RecoveryLCSD

%Recovery%Recovery

Limits RPDRPD

Limits



Project Name:

Project Number:

Lab Number:

Report Date:

NFTA

17005-02

L1811694


727264687270

25-12010-12023-12030-12010-13618-120

707163677269


04/11/18

AcceptanceCriteria

Qual Qual Qual

Serial_No:04111816:15

Page 41 of 92

PCBS

Serial_No:04111816:15

Page 42 of 92

FF

Aroclor 1016

Aroclor 1221

Aroclor 1232

Aroclor 1242

Aroclor 1248

Aroclor 1254

Aroclor 1260

Aroclor 1262

Aroclor 1268

Parameter Result

J

Dilution Factor

ND

ND

ND

ND

ND

4.68

ND

ND

ND

ug/kg

ug/kg

ug/kg

ug/kg

ug/kg

ug/kg

ug/kg

ug/kg

ug/kg

1

1

1

1

1

1

1

1

1

Qualifier Units RL


SAMPLE RESULTS

Project Name:

Project Number:

Lab Number:

Report Date:

NFTA

17005-02

L1811694

40.8

40.8

40.8

40.8

40.8

40.8

40.8

40.8

40.8


Decachlorobiphenyl


Decachlorobiphenyl

89

55

79

78

30-150

30-150

30-150

30-150

Acceptance Criteria

A

A

B

B


04/11/18



L1811694-02Lab ID:




1,8082A04/06/18 07:28HT

EPA 3546



77%Percent Solids:

MDL

4.62

6.20

4.01

4.99

4.57

3.32

4.26

3.35

2.88

A

A

A

A

A

B

B

A

A

Column

Sample Depth:

Serial_No:04111816:15

Page 43 of 92

Aroclor 1016

Aroclor 1221

Aroclor 1232

Aroclor 1242

Aroclor 1248

Aroclor 1254

Aroclor 1260

Aroclor 1262

Aroclor 1268


ND

ND

ND

ND

ND

ND

ND

ND

ND

ug/kg

ug/kg

ug/kg

ug/kg

ug/kg

ug/kg

ug/kg

ug/kg

ug/kg

1

1

1

1

1

1

1

1

1

Qualifier Units RL


SAMPLE RESULTS

Project Name:

Project Number:

Lab Number:

Report Date:

NFTA

17005-02

L1811694

38.7

38.7

38.7

38.7

38.7

38.7

38.7

38.7

38.7


Decachlorobiphenyl


Decachlorobiphenyl

79

56

69

87

30-150

30-150

30-150

30-150

Acceptance Criteria

A

A

B

B


04/11/18



L1811694-03Lab ID:




1,8082A04/06/18 07:40HT

EPA 3546



84%Percent Solids:

MDL

4.39

5.89

3.81

4.74

4.34

3.16

4.04

3.18

2.74

A

A

A

A

A

A

A

A

A

Column

Sample Depth:

Serial_No:04111816:15

Page 44 of 92


Project Name:

Project Number:

Lab Number:

Report Date:

NFTA

17005-02

L1811694



Cleanup Method:

EPA 3546


04/11/18


Analyst: HT

Aroclor 1016

Aroclor 1221

Aroclor 1232

Aroclor 1242

Aroclor 1248

Aroclor 1254

Aroclor 1260

Aroclor 1262

Aroclor 1268

Parameter Result

ND

ND

ND

ND

ND

ND

ND

ND

ND

RL

32.5

32.5

32.5

32.5

32.5

32.5

32.5

32.5

32.5

ug/kg

ug/kg

ug/kg

ug/kg

ug/kg

ug/kg

ug/kg

ug/kg

ug/kg

UnitsQualifier

Polychlorinated Biphenyls by GC - Westborough Lab for sample(s): 02-03 Batch: WG1103833-1


Decachlorobiphenyl


Decachlorobiphenyl

78

70

83

57

30-150

30-150

30-150

30-150


Criteria



MDL

3.69

4.95

3.20

3.98

3.65

2.65

3.39

2.67

2.30

Column

A

A

A

A

A

A

A

A

A

A

A

B

B

Serial_No:04111816:15

Page 45 of 92

Aroclor 1016

Aroclor 1260

84

95

72

85

40-140

40-140

15

11

50

50

ParameterLCS

%RecoveryLCSD

%Recovery%Recovery

Limits RPDRPD

Limits

Polychlorinated Biphenyls by GC - Westborough Lab Associated sample(s): 02-03 Batch: WG1103833-2 WG1103833-3


Project Name:

Project Number:

Lab Number:

Report Date:

NFTA

17005-02

L1811694


86788263

30-15030-15030-15030-150

AABB

75707357


04/11/18

AcceptanceCriteria


A

A

Serial_No:04111816:15

Page 46 of 92

PESTICIDES

Serial_No:04111816:15

Page 47 of 92

FF

Lindane

Heptachlor

Heptachlor epoxide

Endrin

Methoxychlor

Toxaphene

Chlordane


ND

ND

ND

ND

ND

ND

ND

ug/l

ug/l

ug/l

ug/l

ug/l

ug/l

ug/l

1

1

1

1

1

1

1

Qualifier Units RL


SAMPLE RESULTS

Project Name:

Project Number:

Lab Number:

Report Date:

NFTA

17005-02

L1811694

0.100

0.100

0.100

0.200

1.00

1.00

1.00


Decachlorobiphenyl


Decachlorobiphenyl

97

107

89

109

30-150

30-150

30-150

30-150

Acceptance Criteria

A

A

B

B


04/11/18



L1811694-02Lab ID:




1,8081B04/10/18 20:05JW



77%Percent Solids:

MDL

0.022

0.016

0.021

0.021

0.034

0.314

0.232

A

A

A

A

A

A

A

Column

Sample Depth:

Serial_No:04111816:15

Page 48 of 92

Delta-BHC

Lindane

Alpha-BHC

Beta-BHC

Heptachlor

Aldrin

Endrin

Dieldrin

4,4'-DDE

4,4'-DDD

4,4'-DDT

Endosulfan I

Endosulfan II

Endosulfan sulfate

cis-Chlordane


ND

ND

ND

ND

ND

ND

ND

ND

ND

ND

ND

ND

ND

ND

ND

ug/kg

ug/kg

ug/kg

ug/kg

ug/kg

ug/kg

ug/kg

ug/kg

ug/kg

ug/kg

ug/kg

ug/kg

ug/kg

ug/kg

ug/kg

1

1

1

1

1

1

1

1

1

1

1

1

1

1

1

Qualifier Units RL


SAMPLE RESULTS

Project Name:

Project Number:

Lab Number:

Report Date:

NFTA

17005-02

L1811694

1.94

0.810

0.810

1.94

0.971

1.94

0.810

1.21

1.94

1.94

3.64

1.94

1.94

0.810

2.43


Decachlorobiphenyl


Decachlorobiphenyl

70

81

74

95

30-150

30-150

30-150

30-150

Acceptance Criteria

B

B

A

A


04/11/18



L1811694-02Lab ID:




1,8081B04/10/18 21:07JW

EPA 3546



MDL

0.380

0.362

0.230

0.737

0.436

0.684

0.332

0.607

0.449

0.693

1.56

0.459

0.649

0.385

0.677

A

A

A

A

A

A

A

A

A

A

A

A

A

A

A

Column

Sample Depth:

Serial_No:04111816:15

Page 49 of 92

2,4-D

2,4,5-TP (Silvex)


ND

ND

mg/l

mg/l

1

1

Qualifier Units RL


SAMPLE RESULTS

Project Name:

Project Number:

Lab Number:

Report Date:

NFTA

17005-02

L1811694

0.025

0.005

DCAA

DCAA

72

71

30-150

30-150

Acceptance Criteria

A

B


04/11/18



L1811694-02Lab ID:




1,8151A04/09/18 18:11SL



77%Percent Solids:

MDL

0.001

0.001


A

A

Column

Sample Depth:

Serial_No:04111816:15

Page 50 of 92

2,4,5-TP (Silvex)


ND ug/kg 1

Qualifier Units RL


SAMPLE RESULTS

Project Name:

Project Number:

Lab Number:

Report Date:

NFTA

17005-02

L1811694

214

DCAA

DCAA

124

116

30-150

30-150

Acceptance Criteria

A

B


04/11/18



L1811694-02Lab ID:




1,8151A04/10/18 04:32SL


77%Percent Solids:

MDL

5.70


A

Column

Sample Depth:

Serial_No:04111816:15

Page 51 of 92

Lindane

Heptachlor

Heptachlor epoxide

Endrin

Methoxychlor

Toxaphene

Chlordane


ND

ND

ND

ND

ND

ND

ND

ug/l

ug/l

ug/l

ug/l

ug/l

ug/l

ug/l

1

1

1

1

1

1

1

Qualifier Units RL


SAMPLE RESULTS

Project Name:

Project Number:

Lab Number:

Report Date:

NFTA

17005-02

L1811694

0.100

0.100

0.100

0.200

1.00

1.00

1.00


Decachlorobiphenyl


Decachlorobiphenyl

95

101

86

97

30-150

30-150

30-150

30-150

Acceptance Criteria

A

A

B

B


04/11/18



L1811694-03Lab ID:




1,8081B04/10/18 20:18JW



84%Percent Solids:

MDL

0.022

0.016

0.021

0.021

0.034

0.314

0.232

A

A

A

A

A

A

A

Column

Sample Depth:

Serial_No:04111816:15

Page 52 of 92

Delta-BHC

Lindane

Alpha-BHC

Beta-BHC

Heptachlor

Aldrin

Endrin

Dieldrin

4,4'-DDE

4,4'-DDD

4,4'-DDT

Endosulfan I

Endosulfan II

Endosulfan sulfate

cis-Chlordane


ND

ND

ND

ND

ND

ND

ND

ND

ND

ND

ND

ND

ND

ND

ND

ug/kg

ug/kg

ug/kg

ug/kg

ug/kg

ug/kg

ug/kg

ug/kg

ug/kg

ug/kg

ug/kg

ug/kg

ug/kg

ug/kg

ug/kg

1

1

1

1

1

1

1

1

1

1

1

1

1

1

1

Qualifier Units RL


SAMPLE RESULTS

Project Name:

Project Number:

Lab Number:

Report Date:

NFTA

17005-02

L1811694

1.82

0.760

0.760

1.82

0.912

1.82

0.760

1.14

1.82

1.82

3.42

1.82

1.82

0.760

2.28


Decachlorobiphenyl


Decachlorobiphenyl

74

106

76

109

30-150

30-150

30-150

30-150

Acceptance Criteria

B

B

A

A


04/11/18



L1811694-03Lab ID:




1,8081B04/10/18 21:19JW

EPA 3546



MDL

0.357

0.340

0.216

0.692

0.409

0.642

0.312

0.570

0.422

0.651

1.47

0.431

0.610

0.362

0.636

A

A

A

A

A

A

A

A

A

A

A

A

A

A

A

Column

Sample Depth:

Serial_No:04111816:15

Page 53 of 92

2,4-D

2,4,5-TP (Silvex)


ND

ND

mg/l

mg/l

1

1

Qualifier Units RL


SAMPLE RESULTS

Project Name:

Project Number:

Lab Number:

Report Date:

NFTA

17005-02

L1811694

0.025

0.005

DCAA

DCAA

78

70

30-150

30-150

Acceptance Criteria

A

B


04/11/18



L1811694-03Lab ID:




1,8151A04/09/18 18:30SL



84%Percent Solids:

MDL

0.001

0.001


A

A

Column

Sample Depth:

Serial_No:04111816:15

Page 54 of 92

2,4,5-TP (Silvex)


ND ug/kg 1

Qualifier Units RL


SAMPLE RESULTS

Project Name:

Project Number:

Lab Number:

Report Date:

NFTA

17005-02

L1811694

198

DCAA

DCAA

105

98

30-150

30-150

Acceptance Criteria

A

B


04/11/18



L1811694-03Lab ID:




1,8151A04/10/18 04:50SL


84%Percent Solids:

MDL

5.25


A

Column

Sample Depth:

Serial_No:04111816:15

Page 55 of 92


Project Name:

Project Number:

Lab Number:

Report Date:

NFTA

17005-02

L1811694



04/11/18

Analyst: KEG

2,4,5-TP (Silvex)

Parameter Result

ND

RL

165ug/kg

UnitsQualifier

Chlorinated Herbicides by GC - Westborough Lab for sample(s): 02-03 Batch: WG1103793-1

DCAA

DCAA

108

132

30-150

30-150


Criteria

MDL

4.40


Column

A

A

B

Serial_No:04111816:15

Page 56 of 92


Project Name:

Project Number:

Lab Number:

Report Date:

NFTA

17005-02

L1811694



Cleanup Method:

EPA 3546


04/11/18

Analyst: KEG

Delta-BHC

Lindane

Alpha-BHC

Beta-BHC

Heptachlor

Aldrin

Endrin

Dieldrin

4,4'-DDE

4,4'-DDD

4,4'-DDT

Endosulfan I

Endosulfan II

Endosulfan sulfate

cis-Chlordane

Parameter Result

ND

ND

ND

ND

ND

ND

ND

ND

ND

ND

ND

ND

ND

ND

ND

RL

1.56

0.651

0.651

1.56

0.782

1.56

0.651

0.977

1.56

1.56

2.93

1.56

1.56

0.651

1.95

ug/kg

ug/kg

ug/kg

ug/kg

ug/kg

ug/kg

ug/kg

ug/kg

ug/kg

ug/kg

ug/kg

ug/kg

ug/kg

ug/kg

ug/kg

UnitsQualifier

Organochlorine Pesticides by GC - Westborough Lab for sample(s): 02-03 Batch: WG1103818-1


Decachlorobiphenyl


Decachlorobiphenyl

86

82

83

72

30-150

30-150

30-150

30-150


Criteria


MDL

0.306

0.291

0.185

0.593

0.350

0.550

0.267

0.488

0.362

0.558

1.26

0.369

0.522

0.310

0.545

Column

A

A

A

A

A

A

A

A

A

A

A

A

A

A

A

B

B

A

A

Serial_No:04111816:15

Page 57 of 92


Project Name:

Project Number:

Lab Number:

Report Date:

NFTA

17005-02

L1811694



04/11/18

Analyst: SL

2,4-D

2,4,5-TP (Silvex)

Parameter Result

ND

ND

RL

0.025

0.005

mg/l

mg/l

UnitsQualifier

TCLP Herbicides by EPA 1311 - Westborough Lab for sample(s): 02-03 Batch: WG1104435-1

DCAA

DCAA

98

90

30-150

30-150


Criteria


MDL

0.001

0.001


Column

A

A

A

B

Serial_No:04111816:15

Page 58 of 92


Project Name:

Project Number:

Lab Number:

Report Date:

NFTA

17005-02

L1811694



04/11/18

Analyst: KEG

Lindane

Heptachlor

Heptachlor epoxide

Endrin

Methoxychlor

Toxaphene

Chlordane

Parameter Result

ND

ND

ND

ND

ND

ND

ND

RL

0.100

0.100

0.100

0.200

1.00

1.00

1.00

ug/l

ug/l

ug/l

ug/l

ug/l

ug/l

ug/l

UnitsQualifier

TCLP Pesticides by EPA 1311 - Westborough Lab for sample(s): 02-03 Batch: WG1104501-1


Decachlorobiphenyl


Decachlorobiphenyl

97

112

100

97

30-150

30-150

30-150

30-150


Criteria


MDL

0.022

0.016

0.021

0.021

0.034

0.314

0.232

Column

A

A

A

A

A

A

A

A

A

B

B

Serial_No:04111816:15

Page 59 of 92

2,4,5-TP (Silvex) 72 83 30-150 14 30

ParameterLCS

%RecoveryLCSD

%Recovery%Recovery

Limits RPDRPD

Limits

Chlorinated Herbicides by GC - Westborough Lab Associated sample(s): 02-03 Batch: WG1103793-2 WG1103793-3


Project Name:

Project Number:

Lab Number:

Report Date:

NFTA

17005-02

L1811694

DCAADCAA

95117

30-15030-150

AB

97107


04/11/18

AcceptanceCriteria


A

Serial_No:04111816:15

Page 60 of 92

Delta-BHC

Lindane

Alpha-BHC

Beta-BHC

Heptachlor

Aldrin

Endrin

Dieldrin

4,4'-DDE

4,4'-DDD

4,4'-DDT

Endosulfan I

Endosulfan II

Endosulfan sulfate

cis-Chlordane

82

78

88

76

84

82

78

86

86

80

83

80

71

55

68

73

71

81

71

77

75

71

77

78

73

77

73

64

47

61

30-150

30-150

30-150

30-150

30-150

30-150

30-150

30-150

30-150

30-150

30-150

30-150

30-150

30-150

30-150

12

9

8

7

9

9

9

11

10

9

8

9

10

16

11

30

30

30

30

30

30

30

30

30

30

30

30

30

30

30

ParameterLCS

%RecoveryLCSD

%Recovery%Recovery

Limits RPDRPD

Limits

Organochlorine Pesticides by GC - Westborough Lab Associated sample(s): 02-03 Batch: WG1103818-2 WG1103818-3


Project Name:

Project Number:

Lab Number:

Report Date:

NFTA

17005-02

L1811694


89878766

30-15030-15030-15030-150

BBAA

80788070


04/11/18

AcceptanceCriteria


A

A

A

A

A

A

A

A

A

A

A

A

A

A

A

Serial_No:04111816:15

Page 61 of 92

2,4-D

2,4,5-TP (Silvex)

97

56

92

67

30-150

30-150

5

18

25

25

ParameterLCS

%RecoveryLCSD

%Recovery%Recovery

Limits RPDRPD

Limits

TCLP Herbicides by EPA 1311 - Westborough Lab Associated sample(s): 02-03 Batch: WG1104435-2 WG1104435-3


Project Name:

Project Number:

Lab Number:

Report Date:

NFTA

17005-02

L1811694

DCAADCAA

9182

30-15030-150

AB

7774


04/11/18

AcceptanceCriteria


A

A

Serial_No:04111816:15

Page 62 of 92

Lindane

Heptachlor

Heptachlor epoxide

Endrin

Methoxychlor

104

105

114

111

111

89

88

92

89

89

30-150

30-150

30-150

30-150

30-150

16

18

21

22

22

20

20

20

20

20

ParameterLCS

%RecoveryLCSD

%Recovery%Recovery

Limits RPDRPD

Limits

TCLP Pesticides by EPA 1311 - Westborough Lab Associated sample(s): 02-03 Batch: WG1104501-2 WG1104501-3


Project Name:

Project Number:

Lab Number:

Report Date:

NFTA

17005-02

L1811694


104129107106

30-15030-15030-15030-150

AABB

89949381


04/11/18

AcceptanceCriteria

Qual Qual Qual

Q

Q

Q

Column

A

A

A

A

A

Serial_No:04111816:15

Page 63 of 92

METALS

Serial_No:04111816:15

Page 64 of 92

FF

Project Name:

Project Number:

Lab Number:

Report Date:

NFTA

17005-02

L1811694

04/11/18

SAMPLE RESULTS


Matrix: Soil


L1811694-02Lab ID:



DateAnalyzed


Date Prepared


Arsenic, TCLP

Barium, TCLP

Cadmium, TCLP

Chromium, TCLP

Lead, TCLP

Mercury, TCLP

Selenium, TCLP

Silver, TCLP

J

J

J

0.024

0.235

ND

ND

0.360

ND

ND

ND

mg/l

mg/l

mg/l

mg/l

mg/l

mg/l

mg/l

mg/l

1

1

1

1

1

1

1

1

1.00

0.500

0.100

0.200

0.500

0.0010

0.500

0.100

04/09/18 14:58

04/09/18 14:58

04/09/18 14:58

04/09/18 14:58

04/09/18 14:58

04/09/18 13:23

04/09/18 14:58

04/09/18 14:58

1,6010C

1,6010C

1,6010C

1,6010C

1,6010C

1,7470A

1,6010C

1,6010C

AB

AB

AB

AB

AB

MG

AB

AB

04/07/18 18:02

04/07/18 18:02

04/07/18 18:02

04/07/18 18:02

04/07/18 18:02

04/06/18 15:49

04/07/18 18:02

04/07/18 18:02

EPA 3015

EPA 3015

EPA 3015

EPA 3015

EPA 3015

EPA 7470A

EPA 3015

EPA 3015

PrepMethod


Percent Solids: 77%

MDL

0.019

0.021

0.010

0.021

0.027

0.0003

0.035

0.028

Sample Depth:

Serial_No:04111816:15

Page 65 of 92

Project Name:

Project Number:

Lab Number:

Report Date:

NFTA

17005-02

L1811694

04/11/18

SAMPLE RESULTS


Matrix: Soil


L1811694-02Lab ID:



DateAnalyzed


Date Prepared



Arsenic, Total

Barium, Total

Beryllium, Total

Cadmium, Total

Chromium, Total

Copper, Total

Lead, Total

Manganese, Total

Mercury, Total

Nickel, Total

Selenium, Total

Silver, Total

Zinc, Total

Chromium, Trivalent

J

J

J

1.37

17.5

0.081

0.362

6.08

10.4

29.2

86.2

0.270

5.04

0.533

ND

76.1

6.1

mg/kg

mg/kg

mg/kg

mg/kg

mg/kg

mg/kg

mg/kg

mg/kg

mg/kg

mg/kg

mg/kg

mg/kg

mg/kg

mg/kg

2

2

2

2

2

2

2

2

1

2

2

2

2

1

1.01

1.01

0.503

1.01

1.01

1.01

5.03

1.01

0.081

2.52

2.01

1.01

5.03

1.0

04/06/18 15:26

04/06/18 15:26

04/06/18 15:26

04/06/18 15:26

04/06/18 15:26

04/06/18 15:26

04/06/18 15:26

04/06/18 15:26

04/06/18 18:38

04/06/18 15:26

04/06/18 15:26

04/06/18 15:26

04/06/18 15:26

04/06/18 15:26

1,6010C

1,6010C

1,6010C

1,6010C

1,6010C

1,6010C

1,6010C

1,6010C

1,7471B

1,6010C

1,6010C

1,6010C

1,6010C

107,-

AB

AB

AB

AB

AB

AB

AB

AB

EA

AB

AB

AB

AB

04/05/18 20:25

04/05/18 20:25

04/05/18 20:25

04/05/18 20:25

04/05/18 20:25

04/05/18 20:25

04/05/18 20:25

04/05/18 20:25

04/06/18 06:30

04/05/18 20:25

04/05/18 20:25

04/05/18 20:25

04/05/18 20:25

EPA 3050B

EPA 3050B

EPA 3050B

EPA 3050B

EPA 3050B

EPA 3050B

EPA 3050B

EPA 3050B

EPA 7471B

EPA 3050B

EPA 3050B

EPA 3050B

EPA 3050B

NA

PrepMethod

Percent Solids: 77%

MDL

0.209

0.175

0.033

0.099

0.097

0.260

0.270

0.160

0.017

0.244

0.260

0.285

0.295

1.0

Sample Depth:

Serial_No:04111816:15

Page 66 of 92

Project Name:

Project Number:

Lab Number:

Report Date:

NFTA

17005-02

L1811694

04/11/18

SAMPLE RESULTS


Matrix: Soil


L1811694-03Lab ID:



DateAnalyzed


Date Prepared


Arsenic, TCLP

Barium, TCLP

Cadmium, TCLP

Chromium, TCLP

Lead, TCLP

Mercury, TCLP

Selenium, TCLP

Silver, TCLP

J

ND

0.242

ND

ND

ND

ND

ND

ND

mg/l

mg/l

mg/l

mg/l

mg/l

mg/l

mg/l

mg/l

1

1

1

1

1

1

1

1

1.00

0.500

0.100

0.200

0.500

0.0010

0.500

0.100

04/09/18 15:03

04/09/18 15:03

04/09/18 15:03

04/09/18 15:03

04/09/18 15:03

04/09/18 13:25

04/09/18 15:03

04/09/18 15:03

1,6010C

1,6010C

1,6010C

1,6010C

1,6010C

1,7470A

1,6010C

1,6010C

AB

AB

AB

AB

AB

MG

AB

AB

04/07/18 18:02

04/07/18 18:02

04/07/18 18:02

04/07/18 18:02

04/07/18 18:02

04/06/18 15:49

04/07/18 18:02

04/07/18 18:02

EPA 3015

EPA 3015

EPA 3015

EPA 3015

EPA 3015

EPA 7470A

EPA 3015

EPA 3015

PrepMethod


Percent Solids: 84%

MDL

0.019

0.021

0.010

0.021

0.027

0.0003

0.035

0.028

Sample Depth:

Serial_No:04111816:15

Page 67 of 92

Project Name:

Project Number:

Lab Number:

Report Date:

NFTA

17005-02

L1811694

04/11/18

SAMPLE RESULTS


Matrix: Soil


L1811694-03Lab ID:



DateAnalyzed


Date Prepared



Arsenic, Total

Barium, Total

Beryllium, Total

Cadmium, Total

Chromium, Total

Copper, Total

Lead, Total

Manganese, Total

Mercury, Total

Nickel, Total

Selenium, Total

Silver, Total

Zinc, Total

Chromium, Trivalent

J

J

J

1.17

15.7

0.134

0.250

10.3

5.94

14.5

158

0.091

5.30

0.501

ND

37.8

10

mg/kg

mg/kg

mg/kg

mg/kg

mg/kg

mg/kg

mg/kg

mg/kg

mg/kg

mg/kg

mg/kg

mg/kg

mg/kg

mg/kg

2

2

2

2

2

2

2

2

1

2

2

2

2

1

0.895

0.895

0.447

0.895

0.895

0.895

4.47

0.895

0.075

2.24

1.79

0.895

4.47

0.95

04/06/18 15:30

04/06/18 15:30

04/06/18 15:30

04/06/18 15:30

04/06/18 15:30

04/06/18 15:30

04/06/18 15:30

04/06/18 15:30

04/06/18 18:40

04/06/18 15:30

04/06/18 15:30

04/06/18 15:30

04/06/18 15:30

04/06/18 15:30

1,6010C

1,6010C

1,6010C

1,6010C

1,6010C

1,6010C

1,6010C

1,6010C

1,7471B

1,6010C

1,6010C

1,6010C

1,6010C

107,-

AB

AB

AB

AB

AB

AB

AB

AB

EA

AB

AB

AB

AB

04/05/18 20:25

04/05/18 20:25

04/05/18 20:25

04/05/18 20:25

04/05/18 20:25

04/05/18 20:25

04/05/18 20:25

04/05/18 20:25

04/06/18 06:30

04/05/18 20:25

04/05/18 20:25

04/05/18 20:25

04/05/18 20:25

EPA 3050B

EPA 3050B

EPA 3050B

EPA 3050B

EPA 3050B

EPA 3050B

EPA 3050B

EPA 3050B

EPA 7471B

EPA 3050B

EPA 3050B

EPA 3050B

EPA 3050B

NA

PrepMethod

Percent Solids: 84%

MDL

0.186

0.156

0.030

0.088

0.086

0.231

0.240

0.142

0.016

0.216

0.231

0.253

0.262

0.95

Sample Depth:

Serial_No:04111816:15

Page 68 of 92

FF

Parameter

Parameter

Parameter

Result

Result

Result

Dilution Factor

Dilution Factor

Dilution Factor

Qualifier

Qualifier

Qualifier

Units

Units

Units

RL

RL

RL


Project Name:

Project Number:

Lab Number:

Report Date:

NFTA

17005-02

L1811694

DateAnalyzed

DateAnalyzed

DateAnalyzed

AnalyticalMethod

AnalyticalMethod

AnalyticalMethod

Analyst

Analyst

Analyst

Date Prepared

Date Prepared

Date Prepared

04/11/18

Arsenic, Total

Barium, Total

Beryllium, Total

Cadmium, Total

Chromium, Total

Copper, Total

Lead, Total

Manganese, Total

Nickel, Total

Selenium, Total

Silver, Total

Zinc, Total

Mercury, Total

Mercury, TCLP

ND

ND

ND

ND

ND

ND

ND

ND

ND

ND

ND

ND

ND

ND

mg/kg

mg/kg

mg/kg

mg/kg

mg/kg

mg/kg

mg/kg

mg/kg

mg/kg

mg/kg

mg/kg

mg/kg

mg/kg

mg/l

1

1

1

1

1

1

1

1

1

1

1

1

1

1

0.400

0.400

0.200

0.400

0.400

0.400

2.00

0.400

1.00

0.800

0.400

2.00

0.083

0.0010

04/06/18 14:16

04/06/18 14:16

04/06/18 14:16

04/06/18 14:16

04/06/18 14:16

04/06/18 14:16

04/06/18 14:16

04/06/18 14:16

04/06/18 14:16

04/06/18 14:16

04/06/18 14:16

04/06/18 14:16

04/06/18 17:38

04/09/18 13:15

1,6010C

1,6010C

1,6010C

1,6010C

1,6010C

1,6010C

1,6010C

1,6010C

1,6010C

1,6010C

1,6010C

1,6010C

1,7471B

1,7470A

AB

AB

AB

AB

AB

AB

AB

AB

AB

AB

AB

AB

EA

MG

04/05/18 20:25

04/05/18 20:25

04/05/18 20:25

04/05/18 20:25

04/05/18 20:25

04/05/18 20:25

04/05/18 20:25

04/05/18 20:25

04/05/18 20:25

04/05/18 20:25

04/05/18 20:25

04/05/18 20:25

04/06/18 06:30

04/06/18 15:49

Total Metals - Mansfield Lab for sample(s): 02-03 Batch: WG1103956-1

Total Metals - Mansfield Lab for sample(s): 02-03 Batch: WG1104051-1


EPA 3050B

EPA 7471B

Digestion Method:

Digestion Method:

Prep Information

Prep Information

MDL

MDL

MDL

0.083

0.070

0.013

0.039

0.038

0.103

0.107

0.064

0.097

0.103

0.113

0.117

0.018

0.0003

Serial_No:04111816:15

Page 69 of 92



Project Name:

Project Number:

Lab Number:

Report Date:

NFTA

17005-02

L1811694

DateAnalyzed


Date Prepared

04/11/18

Arsenic, TCLP

Barium, TCLP

Cadmium, TCLP

Chromium, TCLP

Lead, TCLP

Selenium, TCLP

Silver, TCLP

ND

ND

ND

ND

ND

ND

ND

mg/l

mg/l

mg/l

mg/l

mg/l

mg/l

mg/l

1

1

1

1

1

1

1

1.00

0.500

0.100

0.200

0.500

0.500

0.100

04/09/18 13:41

04/09/18 13:41

04/09/18 13:41

04/09/18 13:41

04/09/18 13:41

04/09/18 13:41

04/09/18 13:41

1,6010C

1,6010C

1,6010C

1,6010C

1,6010C

1,6010C

1,6010C

LC

LC

LC

LC

LC

LC

LC

04/07/18 18:02

04/07/18 18:02

04/07/18 18:02

04/07/18 18:02

04/07/18 18:02

04/07/18 18:02

04/07/18 18:02


EPA 7470A

EPA 3015

Digestion Method:

Digestion Method:

Prep Information

Prep Information

04/05/18 14:47

04/05/18 14:47



MDL

0.019

0.021

0.010

0.021

0.027

0.035

0.028

Serial_No:04111816:15

Page 70 of 92

Arsenic, Total

Barium, Total

Beryllium, Total

Cadmium, Total

Chromium, Total

Copper, Total

Lead, Total

Manganese, Total

Nickel, Total

Selenium, Total

Silver, Total

Zinc, Total

Mercury, Total

Mercury, TCLP

112

101

108

102

107

107

103

98

102

108

111

106

108

105

-

-

-

-

-

-

-

-

-

-

-

-

-

-

83-117

82-118

83-117

82-117

83-119

84-116

82-117

82-118

82-117

78-121

80-120

81-119

50-149

80-120

-

-

-

-

-

-

-

-

-

-

-

-

-

-

ParameterLCS

%RecoveryLCSD

%Recovery%Recovery


Total Metals - Mansfield Lab Associated sample(s): 02-03 Batch: WG1103956-2 SRM Lot Number: D098-540

Total Metals - Mansfield Lab Associated sample(s): 02-03 Batch: WG1104051-2 SRM Lot Number: D098-540



Project Name:

Project Number:

Lab Number:

Report Date:

NFTA

17005-02

L1811694

04/11/18

Qual Qual Qual

Serial_No:04111816:15

Page 71 of 92

Arsenic, TCLP

Barium, TCLP

Cadmium, TCLP

Chromium, TCLP

Lead, TCLP

Selenium, TCLP

Silver, TCLP

104

94

102

98

100

108

92

-

-

-

-

-

-

-

75-125

75-125

75-125

75-125

75-125

75-125

75-125

-

-

-

-

-

-

-

20

20

20

20

20

20

20

ParameterLCS

%RecoveryLCSD

%Recovery%Recovery




Project Name:

Project Number:

Lab Number:

Report Date:

NFTA

17005-02

L1811694

04/11/18

Serial_No:04111816:15

Page 72 of 92

Arsenic, Total

Barium, Total

Beryllium, Total

Cadmium, Total

Chromium, Total

Copper, Total

Lead, Total

Manganese, Total

Nickel, Total

Selenium, Total

Silver, Total

Zinc, Total

Mercury, Total

Mercury, TCLP

48.6

475.

0.204J

6.54

5570

78.3

1040

200.

18.5

2.39J

ND

1500

0.534

ND

43.7

1040

4.90

7.79

2030

88.2

1170

235

68.2

13.7

30.6

944

0.533

0.0266

0

286

99

25

0

40

258

71

100

115

103

0

0

106

48.7

953

5.10

9.73

2020

89.7

841

202

67.3

13.8

31.4

819

0.528

-

1

238

101

62

0

45

0

4

97

114

104

0

0

-

75-125

75-125

75-125

75-125

75-125

75-125

75-125

75-125

75-125

75-125

75-125

75-125

80-120

80-120

11

9

4

22

0

2

33

15

1

1

3

14

1

-

20

20

20

20

20

20

20

20

20

20

20

20

20

20


MS Found

MS%Recovery

MSD Found

MSD %Recovery

RecoveryLimits RPD

RPD Limits

Total Metals - Mansfield Lab Associated sample(s): 02-03 QC Batch ID: WG1103956-3 WG1103956-4 QC Sample: L1810714-01 Client ID: MS Sample

Total Metals - Mansfield Lab Associated sample(s): 02-03 QC Batch ID: WG1104051-3 WG1104051-4 QC Sample: L1800004-49 Client ID: MS Sample


11.9

198

4.94

5.04

19.8

24.7

50.4

49.4

49.4

11.9

29.7

49.4

0.126

0.025

MS Added


Project Name:

Project Number:

Lab Number:

Report Date:

NFTA

17005-02

L1811694

04/11/18

Qual

Q

Q

Q

Q

Q

Q

Q

Q

Q

Qual

Q

Q

Q

Q

Q

Q

Q

Q

Q

Qual

Q

Q

Serial_No:04111816:15

Page 73 of 92

Arsenic, TCLP

Barium, TCLP

Cadmium, TCLP

Chromium, TCLP

Lead, TCLP

Selenium, TCLP

Silver, TCLP

ND

0.411J

ND

ND

0.101J

ND

ND

1.27

19.4

0.528

1.99

5.16

1.28

0.458

106

97

104

100

101

107

92

-

-

-

-

-

-

-

-

-

-

-

-

-

-

75-125

75-125

75-125

75-125

75-125

75-125

75-125

-

-

-

-

-

-

-

20

20

20

20

20

20

20


MS Found

MS%Recovery

MSD Found

MSD %Recovery

RecoveryLimits RPD

RPD Limits


1.2

20

0.51

2

5.1

1.2

0.5

MS Added


Project Name:

Project Number:

Lab Number:

Report Date:

NFTA

17005-02

L1811694

04/11/18

Serial_No:04111816:15

Page 74 of 92

Mercury, TCLP

Lead, TCLP

ND

0.101J

ND

0.097J

mg/l

mg/l

NC

NC

20

20




NFTA

17005-02

Project Name:

Project Number:

L1811694Lab Number:

Report Date:


04/11/18

Qual

Serial_No:04111816:15

Page 75 of 92

INORGANICS&

MISCELLANEOUS

Serial_No:04111816:15

Page 76 of 92

FF


Matrix: Soil


L1811694-02Lab ID:

SAMPLE RESULTS

Project Name:

Project Number:

Lab Number:

Report Date:

NFTA

17005-02

L1811694





Source of Material:


Particle Size:


Unknown

Non-Metallic - Wet Soil

Medium

120


AnalyzedAnalytical

Method Analyst

04/11/18

Sample Depth:

Serial_No:04111816:15

Page 77 of 92

FF


Matrix: Soil


L1811694-03Lab ID:

SAMPLE RESULTS

Project Name:

Project Number:

Lab Number:

Report Date:

NFTA

17005-02

L1811694





Source of Material:


Particle Size:


Unknown


Medium

120


AnalyzedAnalytical

Method Analyst

04/11/18

Sample Depth:

Serial_No:04111816:15

Page 78 of 92

FF



Matrix: Soil


L1811694-01Lab ID:

Qualifier Units RL

SAMPLE RESULTS

Project Name:

Project Number:

Lab Number:

Report Date:

NFTA

17005-02

L1811694

Field Prep:

DateAnalyzed


Not Specified


Date Prepared

-

04/11/18

MDL

NA

Sample Depth:

Serial_No:04111816:15

Page 79 of 92

FF



Matrix: Soil


L1811694-02Lab ID:

Qualifier Units RL

SAMPLE RESULTS

Project Name:

Project Number:

Lab Number:

Report Date:

NFTA

17005-02

L1811694

Field Prep:

DateAnalyzed


Not Specified


Cyanide, Total

pH (H)


Cyanide, Reactive

Sulfide, Reactive

77.4

ND

8.2

ND

ND

ND

%

mg/kg

SU

mg/kg

mg/kg

mg/kg

1

1

1

1

1

1

0.100

1.2

-

1.0

10

10

04/05/18 07:48

04/11/18 10:45

04/05/18 08:00

04/05/18 14:37

04/05/18 19:12

04/05/18 18:42

121,2540G

1,9010C/9012B

1,9045D

1,7196A

125,7.3

125,7.3

RI

LH

GD

NH

RM

RM

Date Prepared

-

04/10/18 15:30

-

04/05/18 07:18

04/05/18 16:55

04/05/18 16:55

04/11/18

MDL

NA

0.26

NA

0.21

10.

10.

Sample Depth:

Serial_No:04111816:15

Page 80 of 92

FF



Matrix: Soil


L1811694-03Lab ID:

Qualifier Units RL

SAMPLE RESULTS

Project Name:

Project Number:

Lab Number:

Report Date:

NFTA

17005-02

L1811694

Field Prep:

DateAnalyzed


Not Specified


Cyanide, Total

pH (H)


Cyanide, Reactive

Sulfide, Reactive

84.1

ND

9.7

ND

ND

ND

%

mg/kg

SU

mg/kg

mg/kg

mg/kg

1

1

1

1

1

1

0.100

1.1

-

0.95

10

10

04/05/18 07:48

04/11/18 10:48

04/05/18 08:00

04/05/18 14:38

04/05/18 19:12

04/05/18 18:43

121,2540G

1,9010C/9012B

1,9045D

1,7196A

125,7.3

125,7.3

RI

LH

GD

NH

RM

RM

Date Prepared

-

04/10/18 15:30

-

04/05/18 07:18

04/05/18 16:55

04/05/18 16:55

04/11/18

MDL

NA

0.23

NA

0.19

10.

10.

Sample Depth:

Serial_No:04111816:15

Page 81 of 92

FF



Project Name:

Project Number:

Lab Number:

Report Date:

NFTA

17005-02

L1811694

DateAnalyzed


Date Prepared

04/11/18


Sulfide, Reactive

Cyanide, Reactive

Cyanide, Total

ND

ND

ND

ND

mg/kg

mg/kg

mg/kg

mg/kg

1

1

1

1

0.80

10

10

0.93

04/05/18 14:29

04/05/18 18:38

04/05/18 19:09

04/11/18 10:39

1,7196A

125,7.3

125,7.3

1,9010C/9012B

NH

RM

RM

LH

04/05/18 07:18

04/05/18 16:55

04/05/18 16:55

04/10/18 15:30

General Chemistry - Westborough Lab for sample(s): 02-03 Batch: WG1103718-1




MDL

0.16

10.

10.

0.20

Serial_No:04111816:15

Page 82 of 92

pH


Sulfide, Reactive

Cyanide, Reactive

Cyanide, Total

100

73

114

96

74

-

-

-

-

63

99-101

80-120

60-125

30-125

80-120

-

-

-

-

1

20

40

40

35

ParameterLCS

%RecoveryLCSD

%Recovery%Recovery


General Chemistry - Westborough Lab Associated sample(s): 02-03 Batch: WG1103700-1




General Chemistry - Westborough Lab Associated sample(s): 02-03 Batch: WG1105168-2 WG1105168-3


Project Name:

Project Number:

Lab Number:

Report Date:

NFTA

17005-02

L1811694

04/11/18

Qual Qual

Q

Q Q

Qual

Serial_No:04111816:15

Page 83 of 92


Cyanide, Total

ND

ND

810

8.8

88

84

-

9.1

-

87

75-125

75-125

-

3

20

35


MS Found

MS%Recovery

MSD Found

MSD %Recovery

RecoveryLimits RPD

RPD Limits

General Chemistry - Westborough Lab Associated sample(s): 02-03 QC Batch ID: WG1103718-4 QC Sample: L1811694-02 Client ID: BH14-18

General Chemistry - Westborough Lab Associated sample(s): 02-03 QC Batch ID: WG1105168-4 WG1105168-5 QC Sample: L1812210-12 Client ID: MS Sample

918

10

MS Added


Project Name:

Project Number:

Lab Number:

Report Date:

NFTA

17005-02

L1811694

04/11/18

Qual Qual Qual

Serial_No:04111816:15

Page 84 of 92

pH


Solids, Total

Sulfide, Reactive

Cyanide, Reactive

7.9

ND

83.5

ND

ND

7.9

ND

83.0

ND

ND

SU

mg/kg

%

mg/kg

mg/kg

0

NC

1

NC

NC

5

20

20

40

40



General Chemistry - Westborough Lab Associated sample(s): 02-03 QC Batch ID: WG1103718-6 QC Sample: L1811694-02 Client ID: BH14-18

- Associated sample(s): 01-03 QC Batch ID: WG1103736-1 QC Sample: L1811683-01 Client ID: DUP Sample



NFTA

17005-02

Project Name:

Project Number:

L1811694Lab Number:

Report Date:


04/11/18

Qual

Serial_No:04111816:15

Page 85 of 92


L1811694-01A

L1811694-01B

L1811694-01S

L1811694-01T

L1811694-01X

L1811694-01Y

L1811694-01Z

L1811694-02A

L1811694-02A1

L1811694-02B

L1811694-02C

L1811694-02D

L1811694-02E

L1811694-02W

L1811694-02X

L1811694-02X9

L1811694-03A

L1811694-03A1
















Tumble Vessel



A

A

A

A

A

A

A

A

A

A

A

A

A

A

A

A

A

A

NA

NA

NA

NA

NA

NA

NA

NA

NA

NA

NA

NA

NA

NA

NA

NA

NA

NA

4.7

4.7

4.7

4.7

4.7

4.7

4.7

4.7

4.7

4.7

4.7

4.7

4.7

4.7

4.7

4.7

4.7

4.7

Y

Y

Y

Y

Y

Y

Y

Y

Y

Y

Y

Y

Y

Y

Y

Y

Y

Y

Absent

Absent

Absent

Absent

Absent

Absent

Absent

Absent

Absent

Absent

Absent

Absent

Absent

Absent

Absent

Absent

Absent

Absent


NFTA

17005-02

TCLP-EXT-ZHE(14),TS(7),NYTCL-8260(14)

TCLP-EXT-ZHE(14),NYTCL-8260(14)

TCLP-VOA(14)

TCLP-VOA(14)

NYTCL-8260(14)

NYTCL-8260(14)

NYTCL-8260(14)

TS(7)

TS(7)


HEXCR-7196(30)

IGNIT-1030(14),NYTCL-8270(14),REACTS(14),HERB-APA(14),PH-9045(1),NYTCL-8081(14),NYTCL-8082(14),REACTCN(14)




-

TS(7)

TS(7)

Project Name:

Project Number:

L1811694Lab Number:

Report Date:




Analysis(*)

04/11/18


05-APR-18 11:34

05-APR-18 11:34

FrozenDate/Time

FinalpH

Initial pH

Serial_No:04111816:15

Page 86 of 92


L1811694-03B

L1811694-03C

L1811694-03D

L1811694-03E

L1811694-03F

L1811694-03G

L1811694-03S

L1811694-03T

L1811694-03V

L1811694-03V9

L1811694-03W

L1811694-03X

L1811694-03Y

L1811694-03Z

L1811694-04A










Tumble Vessel





Vial HCl preserved

A

A

A

A

A

A

A

A

A

A

A

A

A

A

A

NA

NA

NA

NA

NA

NA

NA

NA

NA

NA

NA

NA

NA

NA

NA

4.7

4.7

4.7

4.7

4.7

4.7

4.7

4.7

4.7

4.7

4.7

4.7

4.7

4.7

4.7

Y

Y

Y

Y

Y

Y

Y

Y

Y

Y

Y

Y

Y

Y

Y

Absent

Absent

Absent

Absent

Absent

Absent

Absent

Absent

Absent

Absent

Absent

Absent

Absent

Absent

Absent

NFTA

17005-02




HEXCR-7196(30)



TCLP-VOA(14)

TCLP-VOA(14)


-


NYTCL-8260(14)

NYTCL-8260(14)

NYTCL-8260(14)

NYTCL-8260(14)

Project Name:

Project Number:

L1811694Lab Number:

Report Date:



Analysis(*)

04/11/18

05-APR-18 11:34

05-APR-18 11:34

FrozenDate/Time

FinalpH

Initial pH

Serial_No:04111816:15

Page 87 of 92


GLOSSARY

Project Name:

Project Number:

Lab Number:

Report Date:

L1811694NFTA

17005-02 04/11/18

Acronyms

EDL

EPA

LCS

LCSD

LFB

MDL

MS

MSD

NA

NC

NDPA/DPA

NI

NP

RL

RPD

SRM

STLP

TIC




Not Applicable.


Not Ignitable.




-

-

-

-

-

-

-

-

-

-

-

-

-

-

-

-

-

-

Terms


Data Qualifiers

A

B

-

-




-

Footnotes

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Project Name:

Project Number:

Lab Number:

Report Date:

L1811694NFTA

17005-02 04/11/18

Data Qualifiers

C

D

E

G

H

I

M

NJ

P

Q

R

RE

S

-

-

-

-

-

-

-

-

-

-

-

-

-









J

ND

-

-


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1

107

121

125





Project Name:

Project Number:

Lab Number:

Report Date:

L1811694NFTA

17005-02

REFERENCES

04/11/18

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Buffalo Station iii Part 7 - Engineering DataPIN 5761.87, Contract D900044 Final May 11, 2018

PRE-DEMOLITION SURVEY

PRE-DEMOLITION SURVEY

FOR

ASBESTOS-CONTAINING MATERIALS, LEAD-BASED PAINT,

AND POLYCHLORINATED BIPHENYLS IN CAULK

FOR THE

BUFFALO AMTRAK STATION 75 EXCHANGE STREET

BUFFALO, ERIE COUNTY, NEW YORK

APRIL 2018

PREPARED FOR: WSP/Parson Brinckerhoff 50 Lakefront Boulevard, Suite 111 Buffalo, New York PREPARED BY

95 Per ry S t reet , Su i te 300 Bu f fa lo, New York 14203

p : 716.206.5100 f : 716.206.5199

TABLE OF CONTENTS

1.0 – EXECUTIVE SUMMARY 2.0 – ASBESTOS-CONTAINING MATERIALS

2.1 – ASBESTOS SAMPLE LOCATION DRAWING 2.2 – PHOTOGRAPHS 2.3 – LABORATORY REPORT AND CHAIN-OF-CUSTODY FORMS

3.0 – LEAD BASED PAINT

3.1 – X-RAY FLUORESCENCE ANALYZER (XRF) LEAD DATA TABLE 3.2 – LEAD REFERENCE DRAWING

4.0 – POLYCHLORINATED BIPHENYLS IN CAULK

4.1 – PCB SAMPLE LOCATION DRAWING 4.2 – LABORATORY REPORT AND CHAIN-OF-CUSTODY FORM

5.0 – LABORATORY ACCREDITATIONS 6.0 – CONSULTANT’S LICENSES AND CERTIFICATIONS

1.0 – EXECUTIVE SUMMARY

1.0 EXECUTIVE SUMMARY Watts Architecture & Engineering (Watts) was retained by WSP | Parsons Brinckerhoff to perform a pre-demolition survey for asbestos-containing materials (ACM), lead-based paint (LBP), and polychlorinated biphenyls (PCBs) in caulks and sealants for the Buffalo Amtrak Station located at 75 Exchange Street in Buffalo, New York. The purpose of the survey was to determine the presence, location, and quantity of ACM, LBP, and PCBs in caulk and sealants throughout the interior and exterior of the building that may be disturbed during the planned demolition of the Buffalo Amtrak Station. The field survey was conducted during March and April 2018 and included the following:

• A visual site inspection to identify suspect ACM, LBP, and PCBs throughout the interior and exterior of the building.

• Collection and laboratory analysis of samples for asbestos and PCBs in caulk from each identified suspect material.

• Performing X-Ray Fluorescence (XRF) readings to detect the presence of lead-based paint on suspect surfaces.

• Documentation of asbestos and PCB sample locations on drawings and chain-of-custody forms.

ASBESTOS-CONTAINING MATERIALS The inspection included the collection of eighty-two (82) asbestos bulk samples representing thirty-nine (39) suspect materials identified that may be disturbed during the project. ACM is defined as any material containing more than one percent (1%) of asbestos. Based on the testing performed for this project, the following ACM have been identified:

• 12” x 12” floor tile and mastic in the Ticket Office and associated closet (approximately 280 square feet of tile and mastic). These materials are non-friable and in good condition. Note, the tile is located beneath carpeting;

• Window caulk associated with the 8 windows of the building (approximately 170 linear feet/3.6 square feet of caulk). This material is non-friable and in fair condition;

• Aluminizer paint on the perimeter of the roof above the bathrooms, Ticket Office, Lobby, Boiler Room and Baggage Room (approximately 200 square feet of aluminizer paint). This material is non-friable and in fair condition; and

• Roof flashing associated with the canopy roof approximately 350 square feet of roof flashing). This material is non-friable and in poor condition.

The following suspect materials within the project limits have been tested by Watts as part of this investigation and have been determined to be non-ACM:

• Ceramic wall tile grout and associated mastic;

• 12” x 12” tan vinyl floor tile and associated mastic; • Ceiling plaster top and base coats; • Wall plaster top and base coats; • Drywall and associated drywall joint compound; • 1” x 1” ceramic floor tile grout and mudset; • Carpet mastic; • 2’ x 4’ ceiling tile; • Mastic on HVAC ductwork; • Vinyl cove base mastic; • Quarry tile grout and mudset; • Quarry tile cove base mastic; • Interior door caulk; • Window glazing compound*; • Vent caulk; • Foundation mortar; • Brick mortar; • Roof shingles and associated tar paper; • Flashing membrane associated with flat roof; • Flashing tar associated with flat roof; • Parapet seam caulk; • Rolled roof - top and middle layers; • Rolled roof – lower layer*; • Perlite insulation; and • Built-up roofing on canopy.

*Material does not exceed the threshold of greater than 1% asbestos which would classify the material as ACM, however a trace amount of asbestos does exist in this material. LEAD-BASED PAINT Representative XRF readings were taken on select building components throughout the project limits. In general, the following building components were tested:

• Drywall walls; • Plaster Walls and ceilings; • Metal window frames; • Wooden window sashes, casing, mullions and stools; • Metal doors and door frames; • Ceiling tile and metal grid work; • Metal light fixtures; • Metal electrical panels and conduit; • Ceramic wall and floor tile; • Metal window lintels; • Exterior structural steel for canopy;

• Exterior wooden roof trim; • Plumbing vent boot; and • Metal vent grate.

The paint on the following tested components contained lead at 1.0 milligram per square centimeter or greater and are therefore considered lead-paint paint:

• Window lintels; • Structural steel for canopy; and • Plumbing vent boot.

POLYCHLORINATED BIPHENYLS Watts investigated caulks and sealants within the project limits to determine if polychlorinated biphenyls (PCBs) were present. Four samples were collected from representative locations identified by Watts based on visual observations made at the time of the site visit. EPA banned the production of PCBs in 1979 and their distribution after 1984. The purpose of the laboratory testing was to determine if the materials contained PCBs and subsequent proper handling and disposal procedures that will be required if they are removed. The samples were analyzed by Schneider Laboratories Global of Richmond, Virginia. Schneider Laboratories Global is a New York State Department of Health (NYSDOH) approved laboratory. The samples were analyzed using USEPA SW-846 Method 8082, PCBs. The Environmental Protection Agency (EPA) regulates PCBs and considers any debris generated from construction materials manufactured with PCBs derived from building renovation projects with a concentration of greater than 50 ppm PCB bulk waste product. The Toxic Substances Control Act (TSCA) regulations (40 CFR Part 761) prescribes requirements for the proper management of PCB materials, including their handling and disposal. PCB bulk product waste at concentrations >50 ppm must follow specific storage, transport and disposal requirements. The following suspect caulk materials were sampled:

• Exterior window caulk; • Interior door caulk; • Parapet seam caulk; and • Vent grate caulk.

No PCBs were identified in the caulk materials sampled. Therefore, special handling and disposal are not required for these materials in regards to PCBs.

2.0 – ASBESTOS-CONTAINING MATERIALS

2.0 ASBESTOS-CONTAINING MATERIALS Sampling and Laboratory Methodology A NYSDOL-certified asbestos inspector from Watts collected bulk samples of all suspect ACMs that were identified within the project limits. Bulk samples were collected using simple hand tools from each matrix identified as a potential ACM. Samples were delivered with the proper chain-of-custody forms to AmeriSci, a New York State accredited laboratory that is a participant in the Environmental Laboratory Approval Program (ELAP) and National Voluntary Laboratory Approval Program (NVLAP). All materials, except non-friable organically bound (NOB) materials, were analyzed using Polarized Light Microscopy (PLM) using ELAP Method 198.1. NOBs, which include but are not limited to, mastics, window caulks, and floor tiles underwent gravimetric reduction prior to being analyzed by PLM method 198.6 and Transmission Electron Microscopy (TEM) under ELAP Method 198.4. The New York State Department of Health (NYSDOH) protocol requires analysis by TEM to confirm a material is non-ACM if the PLM analysis does not confirm the presence of > 1% asbestos. The following Homogeneous Materials List identifies all suspect materials identified, their approximate sample locations, corresponding sample numbers, and asbestos analytical results:

HOMOGENEOUS MATERIALS LIST BUFFALO AMTRAK STATION

75 EXCHANGE STREET BUFFALO, NEW YORK

Material Description

Sample Location Type Sample Number

Results (% Asbestos) ACM Y/N PLM TEM

Ceramic Wall Tile Grout

Men’s Bathroom M 1700502-01 1700502-02

NAD NAD

NAD NAD

N

Ceramic Wall Tile Mastic

Men’s Bathroom M 1700502-03 1700502-04

NAD NAD

NAD NAD

N

12” x 12” Tan Vinyl Floor Tile

Waiting Area West Side Waiting Area East Side

M 1700502-05 1700502-06

NAD NAD

NAD NAD

N

Mastic for 12” x 12” Tan

Vinyl Floor Tile

Waiting Area West Side Waiting Area East Side

M 1700502-07 1700502-08

NAD NAD

NAD NAD

N

Ceiling Plaster Top Coat

Boiler Room Boiler Room

Baggage Room S

1700502-09 1700502-10 1700502-11

NAD NAD NAD

NA NA NA

N

Ceiling Plaster Base Coat

Boiler Room Boiler Room

Baggage Room S

1700502-12 1700502-13 1700502-14

NAD NAD NAD

NA NA NA

N






Wall Plaster Top Coat

Ticket Office S 1700502-15 1700502-16 1700502-17

NAD NAD NAD

NA NA NA

N

Wall Plaster Base Coat

Ticket Office S 1700502-18 1700502-19 1700502-20

NAD NAD NAD

NA NA NA

N

Drywall Men’s Bathroom

Entrance Vestibule M

1700502-21 1700502-22

NAD NAD

NA NA

N

Drywall Joint Compound

Men’s Bathroom Entrance Vestibule

M 1700502-23 1700502-24

NAD NAD

NA NA

N

12” x 12” Yellow

Streaked Vinyl Floor Tile

Ticket Office M 1700502-25 1700502-26

1.8% Chrysotile 1.2% Chrysotile

NA NA

Y

Mastic for 12” x 12”

Yellow Streaked Vinyl

Floor Tile

Ticket Office M 1700502-27 1700502-28


NA NA

Y

1” x 1” Ceramic Floor

Tile Grout Men’s Bathroom M

1700502-29 1700502-30

NAD NAD

NA NA

N

1” x 1” Ceramic Tile

Mudset Men’s Bathroom M

1700502-31 1700502-32

NAD NAD

NA NA

N

Carpet Mastic Ticket Office M 1700502-33 1700502-34

NAD NAD

NAD NAD

N

2” x 4’ Ceiling Tile

Waiting Area Men’s Bathroom

M 1700502-35 1700502-36

NAD NAD

NAD NAD

N

Mastic on HVAC

Ductwork Boiler Room M

1700502-37 1700502-38

NAD NAD

NAD NAD

N

Vinyl Cove Base Mastic

Waiting Area M 1700502-39 1700502-40

NAD NAD

NAD NAD

N

Quarry Tile Grout

Rear Lobby M 1700502-41 1700502-42

NAD NAD

NA NA

N






Quarry Tile Mudset

Rear Lobby M 1700502-43 1700502-44

NAD NAD

NA NA

N

Quarry Cove Base Mastic

Vestibule M 1700502-45 1700502-46

NAD NAD

NAD NAD

N

Interior Door Caulk

Men’s Bathroom Baggage Door

M 1700502-47 1700502-48

NAD NAD

NAD NAD

N

Window Glazing

Compound

East Side of the Building West Side of the Building

M 1700502-49

1700502-50

NAD

NAD

Trace Anthophyllite

Trace Anthophyllite

N

Window Caulk

East Side of the Building South Side of the Building

M 1700502-51 1700502-52

2.5% Chrysotile NAD

NA NAD

Y

Vent Caulk South Side of Building M 1700502-53 1700502-54

NAD NAD

NAD NAD

N

Foundation Mortar

East Side of Building South Side of Building

M 1700502-55 1700502-56

NAD NAD

NA NA

N

Brick Mortar West Side of Building North Side of Building

M 1700502-57 1700502-58

NAD NAD

NA NA

N

Roof Shingle East Side of Shingled Roof

West Side of Shingled Roof

M 1700502-59 1700502-60

NAD NAD

NAD NAD

N

Tar Paper under Roof

Shingles

East Side of Shingled Roof West Side of Shingled

Roof M

1700502-61 1700502-62

NAD NAD

NAD NAD

N

Aluminizer Paint

West End of Flat Roof East End of Flat Roof

M 1700502-63 1700502-64

1.1% Chrysotile NAD

NA NAD

Y

Flashing Membrane

West Side of Flat Roof South Side of Flat Roof

M 1700502-65 1700502-66

NAD NAD

NAD NAD

N

Flashing Tar West Side of Flat Roof South Side of Flat Roof

M 1700502-67 1700502-68

NAD NAD

NAD NAD

N

Parapet Seam Caulk

West Side of Flat Roof South Side of Flat Roof

M 1700502-69 1700502-70

NAD NAD

NAD NAD

N






Rolled Roof – Top Layer


M 1700502-71 1700502-72

NAD NAD

NAD NAD

N

Rolled Roof – Middle Layer


M 1700502-73 1700502-74

NAD NAD

NAD NAD

N

Rolled Roof – Bottom Layer


M 1700502-75 1700502-76

NAD <0.25% Chrysotile

NAD Trace Chrysotile

N

Perlite Insulation


M 1700502-77 1700502-78

NAD NAD

NA NA

N

Built-up Roofing

East Canopy West Canopy

M 1700502-79 1700502-80

NAD NAD

NAD NAD

N

Flashing East Canopy West Canopy

M 1700502-81 1700502-82


NA NA

Y

Abbreviations: Type ACM NA – Not analyzed. M = Miscellaneous Y = Yes NAD – No Asbestos detected. S= Surfacing N = No

A drawing depicting the approximate asbestos bulk sample locations is included in Section 2.1. It is the belief of Watts that this investigation has identified all suspect asbestos-containing materials that will be disturbed by this project. However, if additional suspect materials are identified during the construction period that have not been previously sampled or sampled as part of this assessment, samples of each material should be collected and analyzed for asbestos content.

2.1 – ASBESTOS SAMPLE LOCATION DRAWING

WATTSARCHITECTURE& ENGINEERING95 Perry Street, Suite 300Buffalo, New York 14203

(716) 206-5100 | (716) 206-5199 Fax

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ASBESTOS BULK SAMPLE LOCATIONS FIRST FLOOR

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APRIL 2018

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NOT TO SCALE

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BUFFALO AMTRAK STATION 75 EXCHANGE STREET BUFFALO, NEW YORK

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ALL SAMPLES ARE PREFIXED BY 1700502- 1700502-

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INDICATES APPROXIMATE SAMPLE LOCATION

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FIRST FLOOR PLAN

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45

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22,24

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05,07

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SAMPLE WAS COLLECTED ON MARCH 20, 2018.


(716) 206-5100 | (716) 206-5199 Fax

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ASBESTOS BULK SAMPLE LOCATIONS ROOF

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ROOF PLAN

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2.2 – PHOTOGRAPHS


Ph: (716) 206-5100 Fax: (716) 206-5199

Prepared By: JGPage No.

PHOTO #1- Photograph of asbestos-containing 12" x 12" floor tile and associated asbestos-containing floor tile mastic in the ticket Office. Note: the floor tile is located beneath non-ACM carpeting and mastic.

PROJECT PHOTOGRAPHS

Buffalo, NY 14203

PRE-DEMOLITION SURVEY FOR ASBESTOS CONTAINING MATERIALS, LEAD-BASED PAINT

AND PCBS IN CAULK/SEALANTS

PHOTO #2- Photograph of asbestos-containing window caulk.

Watts Project No. 1700502

95 Perry Street, Suite 300

1BUFFALO AMTRAK STATION 75 EXCHANGE STREETBUFFALO, NEW YORK


Ph: (716) 206-5100 Fax: (716) 206-5199


PHOTO #3 - Photograph of asbestos-containing aluminizer paint located along the perimeter of the flat roof.

PHOTO #4 - Photograph of the station's Waiting Room. The floor tile and mastic within the Waiting Room were determined to be non-ACM.




PROJECT PHOTOGRAPHS


2Buffalo, NY 14203

BUFFALO AMTRAK STATION 75 EXCHANGE STREETBUFFALO, NEW YORK


Ph: (716) 206-5100 Fax: (716) 206-5199


PHOTO #5 - Photograph of trpical ceiling tile within the station. The ceiling tile was determined to be non-ACM.

PHOTO #6 - Photograph of the ceramic floor and wall tile. All materials associated with the floor and wall tiles were determined to be non-ACM.




PROJECT PHOTOGRAPHS


3Buffalo, NY 14203

BUFFALO AMTRAK STATION 75 EXCHANGE STREETBUFFALO, NEW YORK

2.3 – LABORATORY REPORT AND CHAIN-OF-CUSTODY FORMS

3.0 – LEAD-BASED PAINT

3.0 LEAD-BASED PAINT Methodology

Painted building components were grouped by testing combinations. A testing combination is characterized by location, component type, substrate, and visible color. Refer to section 3.1 for a complete listing of all XRF readings that were taken for this project. The LBP survey was performed using the Department of Housing and Urban Development (HUD) protocol. Certain aspects of the HUD guidelines are typically applied to public and commercial buildings, most commonly the levels used to establish LBP. HUD defines LBP, when analyzed by a portable XRF, as paint that contains lead at 1.0 milligram per square centimeter or greater. When paint chips are analyzed by Atomic Absorption Spectroscopy (AAS), HUD defines LBP as paint containing 0.5 percent or greater (>0.5%) lead by weight. For the purposes of this project, the Occupational Safety & Health Administration’s (OSHA) Lead in Construction Standard (29 CFR 1926.62) applies. This standard applies to all construction work where an employee may be occupationally exposed to lead. Construction work is defined as work for construction, alteration and/or repair, including painting and decorating. It includes but is not limited to the following:

• Demolition or salvage of structures where lead or materials containing lead are present;

• Removal or encapsulation of materials containing lead;

• New construction, alteration, repair, or renovation of structures, substrates, or portions thereof, that contain lead, or materials containing lead;

• Installation of products containing lead;

• Lead contamination/emergency cleanup;

• Transportation, disposal, storage, or containment of lead or materials containing lead on the site or location at which construction activities are performed; and

• Maintenance operations associated with the construction activities.

XRF Calibration In order to field verify the calibration and accuracy of the XRF equipment, “calibration checks” are made both by the equipment itself and by the operator. Before the XRF will allow any testing for lead-based paint, it requires a “standardization” reading. This is accomplished by placing the standardization clip over the end of the XRF when prompted by the XRF. Upon the completion of the standardization reading, the XRF will display a Pass or Fail result. If the standardization is successful, the operator checks the calibration of the XRF against National Institute of Standards and Technology (NIST) lead samples that were provided by the manufacturer. The operator’s

calibration checks are taken at the beginning and the end of the testing period, and approximately every four hours, if necessary. The calibration checks are acceptable if the average of the three readings is between 1.0 and 1.1 mg/cm2 (utilizing the error correction factor). Standardization and calibration readings were within the acceptable limits for the readings collected for this project. A table presenting XRF readings and results is included in the following subsection. Disclaimer

This report is based primarily on the results of visual site observations and a general survey of the conditions at Buffalo Amtrak Station at 75 Exchange Street in Buffalo, New York. Watts did not perform a comprehensive inspection (room by room) of all interior and exterior building components. Representative XRF readings were taken from each distinct type of building component associated with building in order to be able to determine if those components were covered with lead-based paint. The lead-based paint survey was performed by Watts on March 20, 2018. Mark Beyer

Lead Risk Assessor

________________________________________

Signature

NY-R-120605-1 Certification Number

Address and Phone Number: Buffalo Amtrak Station

75 Exchange Street Buffalo, NY 14203

(800) 872-7245 Dates of Construction: 1952

3.1 – X-RAY FLUORESCENCE ANALYZER (XRF)

LEAD DATA TABLE

XRF READINGS

AMTRACK STATION

EXCHANGE STREET

BUFFALO, NEW YORK

Testing Date: MARCH 20, 2018 Innov-X Serial No. 571370, Model DCC-4000

ReadingRoom or

AreaSide Component Substrate Color Condition Floor

Results

(mg/cm2)

1 Standardization Pass

2 Calibration 1.03

3 Calibration 0.99

4 Calibration 1.02

5 Lobby East Wall Drywall White Intact First 0

6 Lobby East Window Frame Metal Black Intact First 0.09

7 Lobby East Sash Wood Black Intact First 0.85

8 Lobby South Door Metal Brown Intact First 0.04

9 Lobby South Door Jamb/casing Metal Brown Intact First 0.08

10 Lobby West Drinking Fountain Metal Beige Intact First 0.01

11 Lobby West Floor Vinyl Beige Intact First 0

12 Garage West Ceiling Concrete White Intact First 0.07

13 Garage North Crown Moulding Wood White Intact First 0.04

14 Garage North Electrical Panel Metal Grey Intact First 0.01

15Furnace

RoomNorth Conduit Metal White Intact First 0

16Furnace

RoomNorth Shelf Wood White Intact First 0

17Furnace

RoomNorth Light Fixture Metal White Intact First 0

18Mens

RestroomEast Wall Ceramic Cream Intact First 0.05

19Mens

RestroomEast Window Stool Wood Black Intact First 0

20Mens

RestroomEast Sash Wood Black Intact First 0.77

21Mens

RestroomEast Ceiling Tile Celulose White Intact First 0

22Mens

RestroomNorth Stall Divider Metal Blue Intact First 0

23 Vestibule North Floor Ceramic Brown Intact First 0

24 Vestibule North Heater cover Metal Beige Intact First 0

25 Vestibule North Lintel Metal Beige Intact First 0.79

26 Office East Wall Plaster White Intact First 0

27 Office North Electrical Panel Metal Tan Intact First 0.01

29 Office North Covebase Vinyl Black Intact First 0

30 Exterior East Window casing Wood Brown Fair First 0.39

31 Exterior East Sign Post Metal Brown Fair First 0.19

32 Exterior East Window Mullion Wood Brown Fair First 0.1

33 Exterior West Canopy Post Metal Grey Fair First 5

34 Exterior West Door Metal Brown Intact First 0

35 Exterior West Lintel Metal Green Fair First 1.81

XRF READINGS

AMTRACK STATION

EXCHANGE STREET

BUFFALO, NEW YORK

Testing Date: MARCH 20, 2018 Innov-X Serial No. 571370, Model DCC-4000

ReadingRoom or

AreaSide Component Substrate Color Condition Floor

Results

(mg/cm2)

36 Roof West AC Compressor Metal Beige Intact Roof 0

37 Roof North Trim Wood Brown Poor Roof 0.11

38 Roof WestPlumbing Vent

BootMetal Grey Intact Roof 5

39 Roof West Vent Grate Metal Grey Intact Roof 0

40 Calibration 1.03

41 Calibration 1.05

42 Calibration 1.03

Bold Indicates results equal to or greater than 1.0 mg/cm2

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NORTH

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EAST

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WEST

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SOUTH


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4.0 – POLYCHLORINATED BIPHENYLS IN CAULK

4.0 POLYCHLORINATED BIPHENYLS (PCBs) IN CAULKS Sampling and Laboratory Methodology The Environmental Protection Agency (EPA) regulates PCBs and considers any debris generated from construction materials manufactured with PCBs derived from building renovation projects with a concentration of greater than 50 parts per million (ppm) as PCB bulk product waste. The Toxic Substances Control Act (TSCA) regulations (40 CFR Part 761) prescribes requirements for the proper management of PCB materials, including their handling and disposal. PCB bulk product waste at concentrations >50 ppm must follow specific storage, transport and disposal requirements. Watts collected four (4) bulk samples of suspect PCB-containing caulks and sealants identified within the Buffalo Amtrak Station project limits. Bulk samples were collected using simple hand tools from each matrix identified as a potential PCB-containing material. The samples were analyzed by Schneider Laboratories Global, Inc. (SLGI) in Richmond, Virginia. SLGI is a New York State Department of Health (NYSDOH) approved laboratory and participant in the National Voluntary Laboratory Approval Program (NVLAP). The samples were analyzed using USEPA SW-846 Method 8082, PCBs. The following table identifies the suspect materials identified, their corresponding sample numbers, and individual PCB aroclor analytical results:

POLYCHLORINATED BIPHENYLS (PCBs) BUFFALO AMTRAK STATION


PCB Concentration reported in milligrams per kilogram (mg/kg) (equivalent to ppm)

Sample Number

Aroclor 1016

Aroclor 1221

Aroclor 1232

Aroclor 1242

Aroclor 1248

Aroclor 1254

Aroclor 1260

Aroclor 1262

Aroclor 1268

Sample Description

1700502-PCB-01

<0.313 <0.313 <0.313 <0.313 <0.313 <0.313 <0.313 <0.313 <0.313 Window Caulk

1700502-PCB-02

<0.344 <0.344 <0.344 <0.344 <0.344 <0.344 <0.344 <0.344 <0.344 Interior Door Caulk

1700502-PCB-03 <0.422 <0.422 <0.422 <0.422 <0.422 <0.422 <0.422 <0.422 <0.422 Parapet Wall

Seam Caulk

1700502-PCB-04 <0.471 <0.471 <0.471 <0.471 <0.471 <0.471 <0.471 <0.471 <0.471 Vent Caulk

Drawings depicting the approximate PCB sample locations are included in Section 4.1. It is the belief of Watts that this investigation has identified all suspect PCB-containing materials that will be disturbed by this project. However, if additional suspect materials are identified during the construction period that have not been previously sampled or sampled as part of this assessment, samples of each material should be collected and analyzed for PCB content.

4.1 – PCB SAMPLE LOCATION DRAWING


(716) 206-5100 | (716) 206-5199 Fax

AutoCAD SHX Text

PCB BULK SAMPLE LOCATIONS FIRST FLOOR

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APRIL 2018

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NOT TO SCALE

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ALL SAMPLES ARE PREFIXED BY 1700502-PCB- 1700502-PCB-

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FIRST FLOOR PLAN

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02

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04

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01

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(716) 206-5100 | (716) 206-5199 Fax

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PCB BULK SAMPLE LOCATIONS ROOF

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APRIL 2018

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NOT TO SCALE

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SAMPLE IS PREFIXED BY 1700502-PCB- 1700502-PCB-

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03

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ROOF PLAN

4.2 – LABORATORY REPORT AND CHAIN-OF-CUSTODY FORM

Attn:

Address: 95 Perry Street Suite 300Order #: 252681

Buffalo, NY 14203

Project: Buffalo Train Station

7628

Watts Architecture & Engineering (4637)Customer:

1700502Number: PO Number:

Received 03/23/18

Matrix Bulk

Schneider Laboratories Global, Inc2512 W. Cary Street • Richmond, Virginia • 23220-5117804-353-6778 • 800-785-LABS (5227) • Fax 804-359-1475

Location: Buffalo, NY

03/26/18Reported

Analysis Report

Cust. Sample ID

Parameter

Sample ID Location

UnitsRL* AnalystAnalysis DateResultMethod

252681-001 1700502-PCB-01 Window

Semi-volatile Organic Compounds

Aroclor - 1016 µg/Kg AE03/26/18313<313SW846 8082A









PCB - Surrogate Recoveries

MIDCB

MITCMX

252681-002 1700502-PCB-02 Int Door












MIDCB

MITCMX

All internal QC parameters were met. Unusual sample conditions, if any, are described. Surrogate Spike results designated with "D" indicate that the analyte was diluted out. "MI" indicates matrix interference. Concentration and *Reporting Limit (RL) based on areas provided by client. Values are reported to three significant figures. Solid PPM = mg/kg | PPB = µg/kg and Water PPM = mg/L | PPB = µg/L. The test results reported relate only to the samples submitted.

Page 1 of 3

Attn:


Buffalo, NY 14203


7628



Received 03/23/18

Matrix Bulk



03/26/18Reported

Analysis Report

Cust. Sample ID

Parameter

Sample ID Location


252681-003 1700502-PCB-03 Parapet












MIDCB

MITCMX

252681-004 1700502-PCB-04 Vent












MIDCB

MITCMX


Page 2 of 3

Attn:


Buffalo, NY 14203


7628



Received 03/23/18

Matrix Bulk



03/26/18Reported

Analysis Report

Cust. Sample ID

Parameter

Sample ID Location


252681-03/26/18 05:37 PM

Analyst

Reviewed By: Ben Wood

Method Parameter New York Virginia

State Certifications

Aroclor - 1016 ELAP Certified VELAP CertifiedSW846 8082A









State Certificate Number

New York ELAP 56000

Virginia VELAP 9567


Page 3 of 3

5.0 – LABORATORY ACCREDITATIONS

6.0 – CONSULTANT’S LICENSES AND CERTIFICATIONS

120 E. Washington St., Suite 414 Syracuse, NY 13202

95 Perry Street, Suite 300 Buffalo, NY 14203

44 W 28th Street, 5th Floor New York, NY 10001

WATTS A r c h i t e c t u r e & E n g i n e e r i n g

E x c e l l e n c e i n a l l w e d o .






Jerry Grady C – Air Sampling Technician D – Inspector H – Project Monitor I – Project Designer






Mark Beyer

C – Air Sampling Technician D - Inspector H – Project Monitor I – Project Designer

db contract documents part 7 engineering data …...dimensions (drilling contractor) utilizing the...

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