date: may 2 7 2016united states environmental protection agency region 7 300 minnesota avenue kansas...
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United States Environmental Protection Agency Region 7
300 Minnesota Avenue Kansas City, KS 66101
Date: MAY 2 7 2016 Subject: Transmittal of Sample Analysis Results for ASR #: 7137
Project ID: TH07PZ01
Project Description: Oak Grove Village well - RA sampling
From: Margaret E.W. St. Germain, Chief - Laboratory Technology & Analysis Branch, Environmental Sciences & Technology Division
To: Tonya Howell SUPR/MOKS ,
Enclosed are the analytical data for the above-referenced Analytical Services Request (ASR) and Project. The Regional Laboratory has reviewed and verified the results in accordance with procedures described in our Quality Manual (QM). In addition to all of the analytical results, this transmittal contains pertinent information that may have influenced the reported results and documents any deviations from the established requirements of the QM.
Please contact us within 14 days of receipt of this package if you determine there is a need for any changes. Please complete the enclosed Customer Satisfaction Survey and Data Disposition/Sample Release memo for this ASR as soon as possible. The process of disposing of the samples for this ASR will be initiated 30 days from the date of this transmittal unless an alternate release date is specified on the Data Disposition/Sample Release memo.
If you have any questions or concerns relating to this data package, contact our customer service line at 913-551-5295.
Enclosures
cc: Analytical Data File.
30286020 Superfund
Page 1 of 7
ASR Number: 7137 Summary of Project Information 05/27/2016
Project Manager: Tonya Howell Org: SUPR/MOKS Phone: 913-551-7589
Project ID: TH07PZ01
Project Desc: Oak Grove Village well - RA sampling
Location: Oak Grove State: Missouri Program: Superfund
Site Name: OAK GROVE VILLAGE WELL - OAK GROVE VILLAGE Site ID: 07PZ Site OU: 01 WELL GPRA PRC: 303DD2
Purpose: Site Characterization
To determine the nature and extent of VOC contamination in air from an undefined TCE plume & determine if VOC concentrations in cave air are increasing or decreasing.
Explanation of Codes, Units and Qualifiers used on this report
Sample QC Codes: QC Codes identify the type of Units: Specific units in which results are sample for quality control purpose. reported.
= Field Sample ug/m3 = Micrograms per Cubic Meter
Data Qualifiers: Specific codes used in conjunction with data values to provide additional information on the quality of reported results, or used to explain the absence of a specific value.
(Blank)= Values have been reviewed and found acceptable for use. U = The analyte was not detected at or above the reporting limit.
Page 2 of 7
ASR Number: 7137 Sample Information Summary 05/27/2016
Project ID:TH07PZ01 Project Desc: Oak Grove Village well - RA sampling
Sample QC External Start Start End End Receipt No Code Matrix Location Description Sample No Date Time Date Time Date
1 - _ Air PI 1
05/23/2016 10:01 05/23/2016 15:53 05/24/2016 2 - Air P1A-3 05/23/2016 10:03 05/23/2016 15:54 05/24/2016
3 - _ Air P2 05/23/2016 10:04 05/23/2016 15:55 05/24/2016 4 - _ Air P2-A3 05/23/2016 10:02 05/23/2016 15:54 05/24/2016 5 - _ Air P3 05/23/2016 09:55 05/23/2016 15:56 05/24/2016 6 - _ Air Gift shop 05/23/2016 09:58 05/23/2016 15:32 05/24/2016 7 - Air Ballroom 05/23/2016 10:01 05/23/2016 17:03 05/24/2016 8 - _ Air Honeymoon ' 05/23/2016 10:04 05/23/2016 16:04 05/24/2016 9 - Air Air lock 05/23/2016 10:07 05/23/2016 15:40 05/24/2016
10 - Air Jungle Room 05/23/2016 10:11 05/23/2016 16:28 •05/24/2016
Page 3 of 7
ASR Number: 7137
Project ID: TH07PZ01
RLAB Approved Analysis Comments
Project Desc Oak Grove Village well - RA sampling
05/27/2016
Analysis Comments About Results For This Analysis
1 VOCs in Air at Ambient Levels by GC/MS
Lab: RASP Contract Lab (Out-Source)
Method: Similar to EPA Region 7 RLAB Method 3230.4G (see comments)
Samples: 1- 2- 3- 4- 5- 6- 7-8-_ 9- 10-_
Comments: Sample 7137-10 required a dilutions due to target analyte concentration.
Page 4 of 7
ASR Number: 7137 RLAB Approved Sample Analysis Results 05/27/2016
Project ID: TH07PZ01 Project Desc: Oak Grove Village well - RA sampling
Analysis/ Analyte Units 1- 2- 3- 4-
1 VOCs in Air at Ambient Levels by GC/MS Trichloroethene ug/m3 5.16 3.98 4.4 4.78
Page 5 of 7
ASR Number: 7137 RLAB Approved Sample Analysis Results 05/27/2016
Project ID: TH07PZ01 Project Desc: Oak Grove Village well - RA sampling
Analysis/ Analyte Units 5- 6- 7- 8-—
1 VOCs in Air at Ambient Levels by GC/MS Trichloroethene ug/m3 0.43 U 4.35 11.5 13.8
Page 6 of 7
ASR Number: 7137 RLAB Approved Sample Analysis Results 05/27/2016
Project ID: TH07PZ01 Project Desc: Oak Grove Village well - RA sampling
Analysis/ Analyte Units 9- 10-
1 VOCs in Air at Ambient Levels by GC/MS Trichloroethene ug/m3 48.5 316
Page 7 of 7
CHAIN OF CUSTODY RECORD ENVIRONMENTAL PROTECTION AftENCY REGION VII
ACTIVITY LEADERfPri
mrnjimMMM&k CONTENTS OF^SHIPMENT
NAME OF SURVEY OR ACTIVITY
DESCRIPTION OF SHIPMENT MODE OF SHIPMENT
i s . PIECE(S) CONSISTING nF Z ICE CHEST(S): OTHER
.COMMERCIAL CARRIER -COURIER -SAMPLER CONVEYED (SHIPPING DOCUMENT NUMBER)
PERSONNEL CUSTODY RECORD RELINQUISHED BY (SAMPLER)
t mw Lm&l ~1?EALEO| / | I UNSEALED F
DATE TIME
iir^n
RECEIVED BY
—J SEALED UNSEALED r
REASON FOR CHANGE OF CUSTODY
RELINQUISHED BY
~1 SEALED UNSEALED P
DATE TIME
fOSS
RECEIVED BY
SEALED UNSEALED r
REASON FOR CHANGE OF CUSTODY
RELINQUISHED BY DATE TIME RECEIVED BY
"~] SEALED UNSEALEOT
REASON FOR CHANGE OF CUSTOOY
7-EPA-9262(Revised 5/85) *11,S, 3P0:2002-756-917/40053
Sample Collection Field Sheet US EPA Region 7 Kansas City, KS
ASR Number: 7137 Sample Number: 1 QC Code: Matrix: Air Tag ID: 7137-l-_
Project ID: TH07PZ01 Project Manager: Tonya Howell Project Desc: Oak Grove Village well - RA sampling
City: Oak Grove State: Missouri Program: Superfund
Site Name: OAK GROVE VILLAGE WELL - OAK GROVE VILLAGE WELL Site ID: 07PZ Site OU: 01
Location Desc:
Expected Cone:
Latitude:
Longitude:
EL
External Sample Number:
(or Circle One: ^Low^ledium High) Date Time(24 hr)
Sample Collection: Start: 5 1 / O. Of End: 5_i23j±b /S_.S3
Laboratory Analyses: Container Preservative
1 - 6 Liter Canister None
Holding Time Analysis
60 Days 1 VOCs in Air at Ambient Levels by GC/NIS
Sample Comments:
(N/A)
L-j-J-oo r
fVldH
Sample Collected By: USGS
1 of 1
Sample Collection Field Sheet US EPA Region 7 Kansas City, KS
ASR Number: 7137 Sample Number: 2 QC Code: Matrix: Air Tag ID: 7137-2
Project ID: TH07PZ01 Project Manager: Tonya Howell Project Desc: Oak Grove Village well - RA sampling
City: Oak Grove State: Missouri Program: Superfund
Site Name: OAK GROVE VILLAGE WELL - OAK GROVE VILLAGE WELL Site ID: 07PZ Site OU: 01
Location Desc:
Expected Cone:
Latitude:
Longitude:
PI A-3 External Sample Number:
(or Circle One: ^Low^ledium High)
Sample Collection: Start: S / cfy j b Date
End: 5 [P>! llp>
Time(24 hr)
/0:G3 / e - y y
Laboratory Analyses: Container Preservative
1 - 6 Liter Canister None
Holding Time Analysis
60 Days 1 VOCs in Air at Ambient Levels by GC/MS
Sample Comments:
(N/A)
p^clc* U fa* I ̂ i
M>laf
*
3oal
A o i l f S - S 4 - 2 _
0,0
-23
Sample Collected By: USGS
1 of 1
Sample Collection Field Sheet US EPA Region 7 Kansas City, KS
ASR Number: 7137 Sample Number: 3 QC Code: Matrix: Air Tag ID: 7137-3-_
Project ID: TH07PZ01 Project Manager: Tonya Howell Project Desc: Oak Grove Village well - RA sampling
City: Oak Grove State: Missouri Program: Superfund
Site Name: OAK GROVE VILLAGE WELL - OAK GROVE VILLAGE WELL Site ID: 07PZ Site OU: 01
Location Desc:
Expected Cone:
Latitude:
Longitude:
m External Sample Number:
Date (or Circle One: ^Sw)Medium High)
Sample Collection: Start: j t) -O
End: 5I
Time(24 hr)
Laboratory Analyses: Container Preservative
1 - 6 Liter Canister None
Holding Time Analysis
60 Days . 1 VOCs in Air at Ambient Levels by GC/MS
Sample Comments:
(N/A)
Patl<>5
(h race Phi)pL^
L 6 I %
it /)mtpbtfty-Q ̂ ~ l ' °
-fmJ sJiQ—
Sample Collected By: USGS
1 of 1
Sample Collection Field Sheet US EPA Region 7 Kansas City, KS
ASR Number: 7137 Sample Number: 4 QC Code: Matrix: Air Tag ID: 7137-4-
Project ID: TH07PZ01 Project Manager: Tonya Howell Project Desc: Oak Grove Village well - RA sampling
City: Oak Grove State: Missouri Program: Superfund
Site Name: OAK GROVE VILLAGE WELL - OAK GROVE VILLAGE WELL Site ID: 07PZ Site OU: 01
Location Desc:
Expected Cone:
Latitude:
Longitude:
External Sample Number:
(or Circle One: Low Medium High) Date
Sample Collection: Start: 5j&±b
End:
Time(24 hr)
s&oa. /£: 5V
Laboratory Analyses: Container Preservative
1 - 6 Liter Canister None Holding Time Analysis
60 Days 1 VOCs in Air at Ambient Levels by GC/MS
Sample Comments:
(N/A)
pexcic fr firOj0 bbb3
P>0
Sample Collected By: USGS
1 of 1
Sample Collection Field Sheet US EPA Region 7 Kansas City, KS
ASR Number: 7137 Sample Number: 5 QC Code: Matrix: Air Tag ID: 7137-5-.
Project ID: TH07PZ01 Project Manager: Tonya Howell Project Desc: Oak Grove Village well - RA sampling
City: Oak Grove State: Missouri Program: Superfund
Site Name: OAK GROVE VILLAGE WELL - OAK GROVE VILLAGE WELL Site ID: 07PZ Site OU: 01
Location Desc:
Expected Cone:
Latitude:
Longitude:
P3
External Sample Number:
(or Circle One: Low Medium High) Date
Sample Collection: Start:
End: 5 /2-1
Time(24 hr)
Q1-.5S
Laboratory Analyses: Container Preservative
1 - 6 Liter Canister None
Holding Time Analysis 60 Days 1 VOCs in Air at Ambient Levels by GC/MS
Sample Comments:
(N/A)
pGecic -1
\oUip
Cm>I ̂
f{ep)
city
0^6 7
- I .O
Ld
- Cow:^ o C_ Suu, u,/ Salo
pAilc 10£i*xVs b^
bo\v\A " f roS tZ J lowij*-*
Sample Collected By: USGS
1 of 1
Sample Collection Field Sheet US EPA Region 7 Kansas City, KS
ASR Number: 7137 Sample Number: 6 QC Code: Matrix: Air Tag ID: 7137-6-
Project ID: TH07PZ01 Project Manager: Tonya Howell Project Desc: Oak Grove Village well - RA sampling
City: Oak Grove State: Missouri Program: Superfund
Site Name: OAK GROVE VILLAGE WELL - OAK GROVE VILLAGE WELL Site ID: 07PZ Site OU: 01
Location Desc:
Expected Cone:
Latitude:
Longitude:
G i - A s K o p
External Sample Number:
(or Circle One: Low Medium High) Date
Sample Collection: Start: S_jX,U> End: 5_/^} Jfc
Time(24 hr)
C±:5g> 1^:3,^
Laboratory Analyses: Container Preservative
1 - 6 Liter Canister None Holding Time Analysis
60 Days 1 VOCs in Air at Ambient Levels by GC/MS
Sample Comments:
(N/A)
S>\\(1V*} e^-ooa *h» CCffc
(0 I 4 .
Cm A "tt M-573
ftes # ixiOHz
|vM")id' O' ̂
d ItM -Zo.o
- 1 0
Sample Collected By: USGS
1 of 1
Sample Collection Field Sheet US EPA Region 7 Kansas City, KS
ASR Number: 7137 Sample Number: 7 QC Code: Matrix: Air Tag ID: 7137-7-
Project ID: TH07PZ01 Project Manager: Tonya Howell Project Desc: Oak Grove Village well - RA sampling
City: Oak Grove State: Missouri Program: Superfund
Site Name: OAK GROVE VILLAGE WELL - OAK GROVE VILLAGE WELL Site ID: 07PZ Site OU: 01
Locaition Desc:
Expected Cone:
Latitude:
Longitude:
M YDO VV\
External Sample Number:
(or Circle One: Low Medium High) Date Time(24 hr)
Sample Collection: Start: 5_j2j±b /O.-.0] End: jZhLb
Laboratory Analyses: Container Preservative
1 - 6 Liter Canister None
Holding Time Analysis 60 Days 1 VOCs in Air at Ambient Levels by GC/MS
Sample Comments:
(N/A)
O- WAc J (?_ aw scvu^W IO'k**-
CiKAjt
Gtvx it
HM-W c;
jo1b\
-7^730^5
O.O -3 , 0 ,0
-AO
J J\*(j c M p z A
Sample Collected By: USGS
1 of 1
Sample Collection Field Sheet US EPA Region 7 Kansas City, KS
ASR Number: 7137 Sample Number: 8 QC Code: Matrix: Air Tag ID: 7137-8-
Project ID: TH07PZ01 Project Manager: Tonya Howell Project Desc: Oak Grove Village well - RA sampling
City: Oak Grove State: Missouri Program: Superfund
Site Name: OAK GROVE VILLAGE WELL - OAK GROVE VILLAGE WELL Site ID: 07PZ Site OU: 01
Location Desc:
Expected Cone:
Latitude:
Longitude:
few? yr\t>oy\ 4ov*pu frYYoon^
External Sample Number:
(or Circle One: Lojw' ^ecjjjjjyi High) Date Time(24 hr)
Sample Collection: Start: 5_j3±I? /o-.oy-End: S1=
Laboratory Analyses: Container
1 - 6 Liter Canister Preservative None
Holding Time Analysis 60 Days 1 VOCs in Air at Ambient Levels by GC/MS
Sample Comments:
(N/A)
CPY\ j&dJL jvuV- \v\s.i<^£ rwJl.
CiW
Cm. 3 o\3-f{e^ & AOIOW2S-Z'
~* 9 tC?
c\^pio^ -yiD
-£-\ y\ 3>JL)
Q-ob ̂
Sample Collected By: USGS
1 of 1
Sample Collection Field Sheet US EPA Region 7 Kansas City, KS
ASR Number: 7137 Sample Number: 9 QC Code: Matrix: Air Tag ID: 7137-9-.
Project ID: TH07PZ01 Project Manager: Tonya Howell Project Desc: Oak Grove Village well - RA sampling
City: Oak Grove State: Missouri Program: Superfund
Site Name: OAK GROVE VILLAGE WELL - OAK GROVE VILLAGE WELL Site ID: 07PZ Site OU: 01
Location Desc:
Expected Cone:
Latitude:
Longitude:
f\\r |OC C
External Sample Number:
(or Circle One: L^w^i^^^OHigh) Date Time(24 hr)
Sample Collection: Start: "LVfCj'li?, ^ ^ End: /S:9£>
Laboratory Analyses: Container Preservative
1 - 6 Liter Canister None
Holding Time Analysis 60 Days 1 VOCs in Air at Ambient Levels by GC/MS
Sample Comments:
(N/A)
Oh h.Vi boy
a \oo J[~ ^ 0 -^vOwv
cXoDr-
9 o '
Loaf Rocl< tfiotfv
# 1 dnMW
0,0
rZ %.Q
j-\v\0l "IS
<l0 -fit: /o- 2oO
Sample Collected By: USGS
1 of 1
Sample Collection Field Sheet US EPA Region 7 Kansas City, KS
ASR Number: 7137 Sample Number: 10 QC Code: Matrix: Air Tag ID: 7137-10-_
Project ID: TH07PZ01 Project Manager: Tonya Howell Project Desc: Oak Grove Village well - RA sampling
City: Oak Grove State: Missouri Program: Superfund
Site Name: OAK GROVE VILLAGE WELL - OAK GROVE VILLAGE WELL Site ID: 07PZ Site OU: 01
Location Desc:
Expected Cone:
Latitude:
Longitude:
l e f t OD VY\ External Sample Number:
(or Circle One: Low Medium HiqhL> Date Time(24 hr)
Sample Collection: Start: 5JO, Jt /OJI End: . ^ P-% !b , U>.JP'
Laboratory Analyses: Container Preservative
1 - 6 Liter Canister None
Holding Time Analysis 60 Days 1 VOCs in Air at Ambient Levels by GC/MS
Sample Comments:
(N/A)
0 \
Iooy
C -evJL 'I ~}"oirr
O " *
it
jh|4w
CA
4-3. OR
frOlSObOlJ
o.o
- Z°i, 5.
- 5 , 5
Sample Collected By: USGS
1 of 1