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Pg1}{\bkmkend Pg1}\par\pard\sect\sectd\sbknone\cols2\colno1\colw10308\colsr160\colno2\colw1292\colsr160\ql \li2198\sb0\sl-161\slmult0 \par\pard\ql \li2198\sb0\sl-161\slmult0 \par\pard\ql \li2198\sb0\sl-161\slmult0 \par\pard\ql \li2198\sb0\sl-161\slmult0 \par\pard\ql \li2198\sb0\sl-161\slmult0 \par\pard\ql \li2198\sb0\sl-161\slmult0 \par\pard\ql \li2198\sb0\sl-161\slmult0 \par\pard\ql \li2198\sb61\sl-161\slmult0 \up0 \expndtw-1\charscalex100 \ul0\nosupersub\cf2\f3\fs14 Journal of Advanced Concrete Technology Vol. 6, No. 2, 287-301, June 2008 / Copyright 2008 Japan Concrete Institute\par\pard\column \ql \li10468\sb0\sl-207\slmult0 \par\pard\ql \li10468\sb0\sl-207\slmult0 \par\pard\ql \li10468\sb0\sl-207\slmult0 \par\pard\ql \li10468\sb0\sl-207\slmult0 \par\pard\ql \li10468\sb0\sl-207\slmult0 \par\pard\ql \li20\sb115\sl-207\slmult0 \up0 \expndtw-2\charscalex100 \ul0\nosupersub\cf3\f4\fs18 287 \par\pard\sect\sectd\sbknone \ql \li1132\sb0\sl-207\slmult0 \par\pard\ql\li1132\sb44\sl-207\slmult0 \up0 \expndtw-2\charscalex100 \ul0\nosupersub\cf4\f5\fs18 Scientific paper \par\pard\qj \li1132\ri1823\sb137\sl-300\slmult0 \up0 \expndtw-4\charscalex100 \ul0\nosupersub\cf5\f6\fs28 Chloride Binding Capacity of Mortars Made with Various Portland \up0 \expndtw-4\charscalex100 Cements and Mineral Admixtures \par\pard\ql \li1132\sb170\sl-264\slmult0 \up0 \expndtw-4\charscalex100 \ul0\nosupersub\cf6\f7\fs24 Tetsuya Ishida\ul0\super\cf7\f8\fs24 1\ul0\nosupersub\cf6\f7\fs24 , Shigeyoshi Miyahara\ul0\super\cf7\f8\fs24 2\ul0\nosupersub\cf6\f7\fs24 and Tsuyoshi Maruya\ul0\super\cf7\f8\fs24 2 \par\pard\ql \li1132\sb0\sl-161\slmult0 \par\pard\ql\li1132\sb0\sl-161\slmult0 \par\pard\ql\li1132\sb40\sl-161\slmult0 \up0 \expndtw-1\charscalex100 \ul0\nosupersub\cf2\f3\fs14 Received 9 May 2007, accepted 18 February 2008 \par\pard\ql \li1132\sb103\sl-253\slmult0 \up0 \expndtw-3\charscalex100 \ul0\nosupersub\cf8\f9\fs22 Abstract \par\pard\qj \li1132\ri815\sb45\sl-232\slmult0 \up0 \expndtw-2\charscalex100 \ul0\nosupersub\cf9\f10\fs20 The authors experimentally studied the chloride binding capacity of mortar specimens made with various combinations of \line \up0 \expndtw-3\charscalex100 Portland cement, blast furnace slag, and pozzolans. In the experiment, a pore liquid extraction method, chloride titration \line \up0 \expndtw-1\charscalex100 test, a quantitative analysis of Friedel's salt based on the XRD method, and a mercury intrusion porosimetry test were \line \up0 \expndtw-3\charscalex100 conducted in order to measure chloride ions, adsorbed chlorides on the pore wall, and solid-phase chlorides (Friedel's salt), \line \up0 \expndtw-1\charscalex100 separately. It was clearly shown that the amount of Friedel's salt strongly depends on the type of binder used, whereas \line \up0 \expndtw-1\charscalex100 adsorbed chlorides is controlled by the micropore structure and the characteristics of the hydrated products.\par\pard\sect\sectd\sbknone\cols2\colno1\colw6075\colsr160\colno2\colw5525\colsr160\ql \li1132\sb0\sl-253\slmult0 \par\pard\ql \li1132\sb0\sl-253\slmult0 \par\pard\ql \li1132\sb42\sl-253\slmult0 \up0 \expndtw-3\charscalex100 \ul0\nosupersub\cf8\f9\fs22 1. Introduction\par\pard\qj \li1132\ri356\sb201\sl-229\slmult0 \up0 \expndtw0\charscalex102 \ul0\nosupersub\cf9\f10\fs20 The framework for the prediction of service life, dura-\line \up0 \expndtw-1\charscalex100 bility design and maintenance of concrete structures has \line \up0 \expndtw0\charscalex107 recently been under improvement. For example, the \line \up0 \expndtw0\charscalex105 Standard Specifications for Concrete Structures pub-\line \up0 \expndtw0\charscalex103 lished by the Japan Society of Civil Engineers (2002) \line \up0 \expndtw0\charscalex101 specifies the verification for reinforcing bars corrosion \line \up0 \expndtw0\charscalex103 caused by the ingress of chloride ions in the design of \line \up0 \expndtw0\charscalex100 concrete structures. The method of testing the diffusion \line \up0 \expndtw0\charscalex102 coefficient of chloride ions is also standardized (JSCE \line \up0 \expndtw0\charscalex107 2003). Challenges for the future are to improve per-\line \up0 \expndtw-2\charscalex100 formance evaluation techniques and durability design by \line \up0 \expndtw-1\charscalex100 quantifying and generalizing the movement and equilib-\line \up0 \expndtw-2\charscalex100 rium of chlorides based on the latest framework.\par\pard\qj \li1132\ri357\sb2\sl-229\slmult0\fi199 \up0 \expndtw-1\charscalex100 Chlorides present in hardened cement pastes are gen-\line \up0 \expndtw0\charscalex101 erally classified into chloride ions and bound chlorides \line \up0 \expndtw0\charscalex102 (Maruya \ul0\nosupersub\cf11\f12\fs20 et al\ul0\nosupersub\cf9\f10\fs20 . 1998) (\ul0\nosupersub\cf12\f13\fs20 Fig. 1\ul0\nosupersub\cf9\f10\fs20 ). Chloride ions present in \line \up0 \expndtw0\charscalex106 concrete are dissolved in the pore liquid and are in a \line \up0 \expndtw-1\charscalex100 freely-mobile form. Bound chlorides, on the other hand, \line \up0 \expndtw0\charscalex102 apparently do not move at ordinary concentration gra-\line \up0 \expndtw0\charscalex105 dients or in ordinary advective environments. Bound \line \up0 \expndtw0\charscalex103 chlorides can be further classified into constituents of \line \up0 \expndtw0\charscalex103 hydrates, as Friedel's salt \up0 \expndtw-1\charscalex100 (C\ul0\sub\cf13\f14\fs19 3\ul0\nosupersub\cf9\f10\fs20 A\u8226?CaCl\ul0\sub\cf13\f14\fs19 2\ul0\nosupersub\cf9\f10\fs20 \u8226?10H\ul0\sub\cf13\f14\fs19 2\ul0\nosupersub\cf9\f10\fs20 O), and \line \up0 \expndtw-3\charscalex100 chlorides adsorbed into the pore walls. The total quantity \line \up0 \expndtw-2\charscalex100 of chlorides in a hardened cement paste is the sum of the \line \up0 \expndtw-1\charscalex100 amount of chloride ions and bound chlorides. Hardened \line \up0 \expndtw-3\charscalex100 cement pastes with good binding capacity are expected to \line \up0 \expndtw0\charscalex101 be relatively low in chloride ion content and highly re-\line \up0 \expndtw-1\charscalex100 sistant to steel corrosion. Accordingly, it is important to \line \up0 \expndtw0\charscalex103 have a grasp of the relationship between chloride ions \line \up0 \expndtw-3\charscalex100 and bound chlorides in concrete under various conditions\par\pard\column \qj \li1132\sb0\sl-230\slmult0 \par\pard\qj \li1132\sb0\sl-230\slmult0 \par\pard\qj \li20\ri930\sb88\sl-230\slmult0 \up0 \expndtw0\charscalex105 the chloride-induced corrosion of reinforcing bars in \up0 \expndtw-2\charscalex100 concrete.\par\pard\qj \li20\ri930\sb1\sl-230\slmult0\fi199 \up0 \expndtw0\charscalex103 Chlorides bound as Friedel's salt (solid-phase chlo-\line \up0 \expndtw0\charscalex100 rides) are thought to be dependent on the Al\ul0\sub\cf13\f14\fs19 2\ul0\nosupersub\cf9\f10\fs20 O\ul0\sub\cf13\f14\fs19 3\ul0\nosupersub\cf9\f10\fs20 content \line \up0 \expndtw0\charscalex105 in the binder and the quantity of monosulfate formed \line \up0 \expndtw-1\charscalex100 (Glass \ul0\nosupersub\cf11\f12\fs20 et al\ul0\nosupersub\cf9\f10\fs20 . 1997). Further, it is expected that the quan-\line \up0 \expndtw0\charscalex100 tity of chlorides adsorbed into hydrates (adsorbed chlo-\line \up0 \expndtw-1\charscalex100 rides) will vary depending on the geometric characteris-\line \up0 \expndtw-2\charscalex100 tics of pore structure, electric charge of pore surface, etc. \line \up0 \expndtw0\charscalex100 The objective of this research is to quantify the equilib-\line \up0 \expndtw0\charscalex109 rium between chloride ions and bound chlorides in \line \up0 \expndtw0\charscalex103 hardened cement pastes. The specimens consist of ce-\line \up0 \expndtw0\charscalex105 ment and varying mineral compositions and gypsum \line \up0 \expndtw0\charscalex100 contents as well as some made with cement and ground \line \up0 \expndtw0\charscalex100 granulated blast furnace slag and pozzolans to examine \line \up0 \expndtw-2\charscalex100 the effects of mineral admixtures.\par\pard\ql \li20\sb229\sl-253\slmult0 \up0 \expndtw-4\charscalex100 \ul0\nosupersub\cf8\f9\fs22 2. Test methods\par\pard\ql \li20\sb200\sl-230\slmult0 \up0 \expndtw-2\charscalex100 \ul0\nosupersub\cf15\f16\fs20 (1) Materials and mix proportions\par\pard\qj \li20\ri882\sb0\sl-230\slmult0\fi0 \up0 \expndtw-2\charscalex100 \ul0\nosupersub\cf9\f10\fs20 The physical properties and chemical composition of the \line \up0 \expndtw0\charscalex103 ordinary Portland cement \up0 \expndtw0\charscalex103 (OPC), high early-strength \line \up0 \expndtw-3\charscalex100 Portland cement (HPC), low-heat Portland cement (LPC), \line \up0 \expndtw-1\charscalex100 ground granulated blast furnace slag (BFS), fly ash (FS) \line \up0 \expndtw-3\charscalex100 and silica fume (SF) used in the test are listed in \ul0\nosupersub\cf12\f13\fs20 Table 1\ul0\nosupersub\cf9\f10\fs20 . \line \up0 \expndtw0\charscalex103 In this test, the used blast furnace slag did not contain \line \up0 \expndtw0\charscalex101 gypsum. The specific surface area of each material ex-\line \up0 \expndtw0\charscalex101 cept for the silica fume corresponds to the Blaine fine-\par\pard\ql \li1132\sb0\sl-195\slmult0 \par\pard\ql \li1132\sb0\sl-195\slmult0 \par\pard\ql \li1004\sb57\sl-195\slmult0 \up0 \expndtw-2\charscalex100 \ul0\nosupersub\cf16\f17\fs17 Cement hydrate\par\pard\ql \li879\sb73\sl-172\slmult0\tx1918\tx2434 \up0 \expndtw-1\charscalex100 \ul0\nosupersub\cf17\f18\fs14 Cl\tab \up0 \expndtw-2\charscalex100 Cl\tab \up0 \expndtw-2\charscalex100 \ul0\nosupersub\cf16\f17\fs17 Cl\ul0\super\cf19\f20\fs16 -\ul0\nosupersub\cf16\f17\fs17 Chloride ion\par\pard\sect\sectd\sbknone\cols3\colno1\colw7054\colsr40\colno2\colw1400\colsr160\colno3\colw3116\colsr160\ql \li6592\sb0\sl-123\slmult0 \up0 \expndtw-1\charscalex100 \ul0\nosupersub\cf17\f18\fs14 Cl\ul0\super\cf18\f19\fs14 -\par\pard\ql \li1132\sb0\sl-160\slmult0 \up0 \expndtw-1\charscalex100 \ul0\nosupersub\cf9\f10\fs20 so as to improve the accuracy of method used to predict\par\pard\ql \li6837\sb41\sl-172\slmult0 \up0 \expndtw-1\charscalex100 \ul0\nosupersub\cf17\f18\fs14 Cl\ul0\super\cf18\f19\fs14 -\par\pard\ql \li1132\sb0\sl-172\slmult0 \par\pard\ql \li6592\sb52\sl-172\slmult0 \up0 \expndtw-1\charscalex100 \ul0\nosupersub\cf17\f18\fs14 Cl\ul0\super\cf18\f19\fs14 -\par\pard\qj \li1132\ri1217\sb0\sl-201\slmult0 \up0 \expndtw0\charscalex100 \ul0\super\cf13\f14\fs19 1\ul0\nosupersub\cf9\f10\fs20 Associate Professor, Department of Civil Engineering, \up0 \expndtw-3\charscalex100 University of Tokyo, Japan.\par\pard\ql \li1132\sb1\sl-230\slmult0 \up0 \expndtw-2\charscalex100 \ul0\nosupersub\cf11\f12\fs20 E-mail\ul0\nosupersub\cf9\f10\fs20 :\ul0\nosupersub\cf14\f15\fs20 tetsuya.ishida@civil.t.u-tokyo.ac.jp\par\pard\column \ql \li610\sb0\sl-135\slmult0 \up0 \expndtw-1\charscalex100 \ul0\nosupersub\cf17\f18\fs14 Cl\ul0\super\cf18\f19\fs14 -\par\pard\ql \li147\sb49\sl-195\slmult0 \up0 \expndtw-2\charscalex100 \ul0\nosupersub\cf16\f17\fs17 Pore\par\pard\ql \li670\sb0\sl-120\slmult0 \up0 \expndtw-1\charscalex100 \ul0\nosupersub\cf17\f18\fs14 Cl\ul0\super\cf18\f19\fs14 -\par\pard\ql \li147\sb0\sl-136\slmult0 \up0 \expndtw-2\charscalex100 \ul0\nosupersub\cf16\f17\fs17 liquid\par\pard\ql \li20\ri168\sb87\sl-175\slmult0\fi590\tx1057 \up0 \expndtw-1\charscalex100 \ul0\nosupersub\cf17\f18\fs14 Cl\ul0\super\cf18\f19\fs14 -\line \up0 \expndtw-1\charscalex100 \ul0\nosupersub\cf17\f18\fs14 Cl \tab \up0 \expndtw-2\charscalex100 Cl\par\pard\column \ql \li1132\sb0\sl-195\slmult0 \par\pard\ql \li20\sb80\sl-195\slmult0 \up0 \expndtw0\charscalex100 \ul0\nosupersub\cf16\f17\fs17 Cl\ul0\super\cf19\f20\fs16 -\ul0\nosupersub\cf16\f17\fs17 Adsorbed\par\pard\ql \li342\sb0\sl-136\slmult0\tx1530 \up0 \expndtw-2\charscalex100 Chloride\tab \up0 \expndtw-3\charscalex100 Bound\par\pard\ql \li1525\sb1\sl-168\slmult0 \up0 \expndtw-2\charscalex100 Chloride\par\pard\qj \li37\ri1832\sb109\sl-136\slmult0\tx352 \up0 \expndtw0\charscalex101 Cl Solid-phase \line\tab \up0 \expndtw-2\charscalex100 Chloride\par\pard\sect\sectd\sbknone\cols2\colno1\colw6044\colsr160\colno2\colw5556\colsr160\qj \li1132\ri320\sb15\sl-230\slmult0 \up0 \expndtw-3\charscalex100 \ul0\super\cf13\f14\fs19 2\ul0\nosupersub\cf9\f10\fs20 Civil Engineering Laboratory, Taisei Technology Center \up0 \expndtw-3\charscalex100 Taisei Corporation, Japan.\par\pard\column \qj \li20\ri879\sb0\sl-199\slmult0 \up0 \expndtw-3\charscalex100 \ul0\nosupersub\cf20\f21\fs18 Fig. 1 Classification and definition of chlorides in hardened \up0 \expndtw-2\charscalex100 cement pastes\ul0\super\cf21\f22\fs18 3)\ul0\nosupersub\cf20\f21\fs18 . \par\pard\sect\sectd\fs24\paperw11900\paperh16840{\shp{\*\shpinst\shpleft1180\shptop9360\shpright10660\shpbottom15480\shpwr3\shpfblwtxt0\shpbxpage\shpbypage\shpz852\shplid1{\sp{\sn shapeType}{\sv 75}}{\sp{\sn fBehindDocument}{\sv 1}}{\sp{\sn pib}{\sv 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