THE EIGHTY-EIGHTH PRESENTATION OF THE

WILLARD GIBBS MEDAL (Founded by William A. Converse)

to DR. LAWRENCE F. DAHL

sponsored by the

MAY •1999

CHICAGO SECTION AMERICAN CHEMICAL SOCIETY FRIDAY, MAY 21, 1999

MONASTERO'S RESTORANTE 3945 Devon Avenue Chicago, IL

DIRECTIONS TO THE MEETING

Take 1-94 either north or south and exit at Touhy Avenue East. Go a very short distance and turn south (right) . Go one mile to Devon Avenue and turn east (left). Go one mile to Pulaski Avenue. The restaurant is about 100 yards east of the intersection. FREE VALET PARKING

SOCIAL HOUR 6:00-7:00 P.M. Cash Bar and Hors d'oeuvres

DINNER 7:00P.M.

Dinner reservations at $35.00 each may be made by using the special reservation form in your Bulletin (see page 4) and enclose your check made out to the Chicago Section ACS. Mail to the Section Office at 7173 N. Austin Avenue, Niles, Illinois 60714. Tickets will be mailed if a pre-paid reservation is received by Friday, May 14th. Seat­ing will be assigned, tables may be reserved in advance. Reservations should be received by noon, Monday, May 17, 1999. Refunds cannot be made after noon on Tuesday, May 18.

The menu consists of Fettunta (spe­cial Sicilian bread), Mixed Salad with Italian or Ranch Dressing, Vegetable Soup with Barley, Rigatoni with Mari­nara Sauce, choice of Steak Palermi­tana, Salmon Genovese, or Eggplant Parmigiana, G.reen Beans with Toma­toes and Pearl Onions, Cannoli, Coffee or Tea, Red and White Wine.

AWARD CEREMONY 8:00P.M.

The Willard Gibbs Medal

Margaret Stowell Levenberg, Chair Chicago Section, ACS

Introduction of the Medalist Tobin Marks Northwestern University

Presentation of the Medal Ellis K. Fields, Past President (1985) American Chemical Society

Citation: For outstanding contributions in organometallic and high-nuclearity metal cluster chemistry synthesis and structural characterization of nanome­ter-sized molecules, in work that has been described as "unique" and "superb science"; and for youthful enthusiasm in research and teaching, demonstrated by leadership of an inter­nationally recognized research group which has aided in the understanding of inorganic materials.

Acceptance of the Award Lawrence F. Dahl R. E. Rundle Professor of Chemistry and Hilldale Chair in Chemistry University cif Wisconsin - Madison

Visit the Chicago Section

at http://membership.acs.org/C/Chicago

Lawrence F. Dahl (continued ·on pag~ 2)

JOB CLUB The next meeting of the Chicago

Section Job Club will be held on Friday, May 21 at Monastero's Restorarite at 5 p.m. The Job Club provides a continuing opportunity for unemployed members of the Section to meet with one another, share their experiences and develop a network that may help in identifying employ­ment opportunities. Bring plenty of resumes and business cards to dis­tribute to your colleagues.

Should you wish to attend the Section meeting following the Job Club, the fee for unemployed mem­bers is only $35, and you can con­tinue your networking activities. There will be no discount since this is the Willard Gibbs Award Night. Please call the Section office for reservations.

2

(continued from page 1)

ACCEPTANCE ADDRESS "Giant-Size Homometallic and Het­

erometallic Carbonyl Clusters: The Joys of Synthetic/Stereochemical Explo­rations"

Our recent research has focused on the preparation, isolation , crystalliza­tion, structure/bonding analysis , and physical/chemical characterization of high-nuclearity metal carbonyl clusters; specifically, those with at least 10 core atoms of platinum, palladium or nickel that form direct metal-metal bonds. Because most of these metal clusters possess well-defined stoichiometries and precise geometries, detailed inves­tigations of their physical behaviors should provide insight into the onset of metallic-l ike character with increasing metal-core size (especially for clusters with interior atoms within their metal cores). It will be important to correlate their physical properties (e.g., variable temperature magnetic moments and specific heats) with those of naked and ligand-stabilized nanoparticles with non-uniform size distributions. These clusters are possible precursors of new materials with useful catalytic, electron­ic, magnetic, optical and/or photochemi­cal/electrochemical properties. This presentation will highlight some remark­able new clusters in cluding : 1 )two isostructural 38-atom trimetallic Au-Pd­Ni and bimetallic Au-Ni carbonyl clus­ters of pseudo-D3d symmetry with sub­stitutional Pd/Ni crystal disorder occurr­ing at only six equivalent metal sites (coloring problem) ; 2) two crystallo­graph ically superimposed Au-Ni car­bonyl clusters of pseudo-D4d symmetry contain ing a 26-atom gold cage (with either one or two interior Au prisoners) surrounded by 40 Ni atoms that are lig­ated by 56 COs; and 3) a three-shell palladium carbonyl phosphine cluster of pseudo-icosahedral symmetry contain­ing 55 interior Pd atoms in the first two shells encapsulated by a 60-vertex 3rd shell polyhedron (a geometrical metallo

brouhnan

isomer of C60 buckyball) with 30 addi­tional capping Pd atoms.

THE MEDALIST

Lawrence F. Dahl was born in 1929 and received his B.Sc. degree in 1951 from the University of Louisville (Ken ­tucky). He subsequently moved to Iowa State University where he obtained his Ph.D. with the late Robert E. Rundle. In 1957 he joined the faculty of the Univer­sity of Wisconsin in Madison where over the last 42 years, he has emerged as one of the world's great pioneers in the synthesis, structure and bonding of transition metal cluster compounds. He has been the R.E. Rundle Professor of Chemistry at Wisconsin since 1978, the Hilldale Professor since 1991 and in 1994 he received the Hilldale award in the Physical Sciences at University of Wisconsin-Madison.

His honors and recognition include: Alfred P. Sloan Foundation Fellow (1963-65); Walter Hieber (70th Geburt­stag) Lectureship , Techn ischen Hochschule Munchen (1965); First Dis­tinguished Alumni Lecture in Chemistry, University of Lou isville (1 969) ; Guggen­heim Fellow (1969-70) ; Edgar Fahs Smith Memorial Lecturer, University of Pennsylvan ia (1971 ); First Howard L. Ritter Memorial Lecturer, Miami Univer­sity (1971 ); American Chemical Society Award in Inorganic Chemistry (1974); Elected Fellow of the New York Acade­my of Sciences (1975); Chairman of ACS Division of Inorganic Chemistry (1979); Elected Fellow of the American Association for the Advancement of Science (1980); Appointed a "Kentucky Colonel " by Governor of Kentucky (1982); Named Distinguished Alumnus of the College of Letter and Science, University of Louisville (1983); Recipi­ent of the Brotherton Research Profes­sorship , University of Leeds (1983); Recipient of a Senior U.S. Scientist Humboldt Foundation Award by the Alexander von -Humboldt-Stiftung

(1985) ; Sir Ronald Nyholm Lectureship and Medal, Royal Society of Chemistry (1985-86); P .C. Reilly Lectureship, Uni­versity of Notre Dame (1987); Elected to the National Academy of Sciences (1988) ; Recipient of the H. Willard Davis Lectureship, University of S. Car­olina (1989); Paolo Chini Lectureship endowed by the Italian Society of Chemistry (1989); J. C. Bailar, Jr. Lec­tureship and Medal , Un iversity of Illinois at Urbana-Champaign (1990); Recipi­ent of the First Alumnus Award from the College of Arts and Science, University of Louisville (1990); Recipient of Hon­orary Doctorate Degree, University of Louisville (1991 ); Elected to the Ameri­can Academy of Arts and Sciences (1992); Kazuo Nakamoto Distinguished Lectureship, Marquette University (1994), Major Lecturer at the Robert A. Welch Foundation Conference on Nanochemistry (1995); Fred Basolo Lecturesh ip and Medal, Northwestern University (1996), Frontie r Lectureship Series , Texas A&M University (1996); Gordon Stone Lectureship, Bristol Uni­versity (1 997) ; and Hans B. Jonassen Lectureship , Tulane University (1998) .

He is a member of the editorial board of the Journal of Cluster Science and fo rmer member of the editorial boards of the Journal of Physical Chemistry, Journal of Organometallic Chemistry, Journal of Coordination Chemistry, and Chemical Reviews.

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'CHEM SHORTS'' . This column Is presented by the Ele­

mentary Education Committee. They hope that it wil l reach young children and help increase science literacy. Please cut it out and pass it on to your children,grandchildren , or elementary teachers. It is hoped that teachers will try to incorporate some of these pro­jects in th is column into their lesson plans.

"Epsom Salt Towers"

Kids , can you say "super-satura­tion"? This is a big word but by using the principle behind i , you can make some cool formations. Follow me ...

You' ll need o measure 3 cup of Epsom salts into 1 cup of ho tap wa er (have an adult do this) and stir. Divide the solution into two small clear glasses or jars. Put a large paper clip onto each end of a 12-inch piece of cotton string. Soak the string for 5 minutes in one of the solutions. Spread aluminum foil on a work surface, and hang the wet string between the two containers. The paper clips will weight the ends down in each glass or jar. The glasses will be about 4-6 inches apart. Let the string hang with a litt le slack between the two glasses. After about 30 minutes, you should see a tower growing down from the string (a "stalactite"), and a tower growing up from the table under the string (a "stalagmite"). Let it go overnight to see how large your towers can grow.

What's happening here? The solution you made was supersaturated - which means that there is more magnesium sulfate (which is what epsom salts is) dissolved in the solution than in possi­ble at regular temperatures. How can that be? Remember that you used hot water, which lets more MgSO. (which is another way of "saying" magnesium sulfate ... ) dissolve. As the solution drips from the string, the water evaporates. This leaves the MgSO. behind to solidi­fy into your towers. In other words, we see the results of an evaporation pro­cess as the MgSO. crystallizes.

Think about a place where you might have seen such formations but on a much grander scale. Were you ever in a cave that had stalactites and stalag­mites? These towers are usually made of calcium carbonate (limestone) rather than magnesium sulfate, but they form in much the same way - by evaporation of water from solutions containing a lot of ca lcium and carbonate ions. We hope you learned a lot of chemistry today, from the physical processes of

supersaturation, evaporation, and crys­tallization, to some of the geochemical processes that occur in caves. Try out this experiment and then go visit a cave this summer - happy spelunking! (another big funny word ... we dare you to look it up).

References: "Planet Chemistry" from the American Chemical Society's National Chemistry Week Office, 1997 (www.acs.org/ncw).

"ChemShorts" are on the internet at: http://membership.acs.org/C/Chicago/C hmShort/kidindex.html.

KATHLEEN CARRADO Elementary Education Committee.

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' 3

May & June, 1999 Vol. 86, No.5 & 6 Published by the Chicago Sec­tion of The American Chemical Society, Fran Karen Kravitz, Edi­tor; Ronald Sykstus, Business Manager. Address: 7173 North Austin, Niles, Illinois 60714. 847/647-8405. Subscription rates: $15 per year, $15 outside North America. Frequency: monthly­September thru June

GLOBAL CLIMATE CHANGE Now available from ACS--an updated

pamphlet that details the science behind global climate change. The 12-page pamphlet is written for the educat­ed nonscientist.

Single copies of this publication are free and may be obtained by writing to American Chemical Society, Office of Legislative and Government Affairs, 1155 Sixteenth Street, NW, Room 330, Washington, DC 20036, phoning 202/872-4386, or e-mailing govtrela­tions@acs .org.

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4

GOVERNMENT AFFAIRS WORKSHOPS

Frustrated by the lack of scientific input in public policy matters? Interest­ed in issues like federal research fund­ing, state science education standards, or state environmental issues? Then come to a government affairs training workshop at an ACS regional meeting! The ACS Office of Legislative & Gov­ernment Affairs (OLGA) will be holding government affairs workshops at the spring regional meetings . The work­shops will provide individual and local section project ideas, tips on working with elected officials, and suggestions for building state-wide coalitions of ACS local sections to work on government relations issues relevant to them all . The half-day workshops will include panel discussions with state legislators or congressional staff.

The workshops will be held at the Mid-Atlantic Regional Meeting (Madi­son, N J, Wednesday, May 19 from 8:30 a.m. to 12:00 p.m.) , Northwest Regional Meeting (Portland, OR, Mon­day, June 21 , 1 :30 p.m. 5:00 p.m.) , Central Regional Meeting (Columbus, OH, Wednesday, June 23, 8:30 a.m. -12:00 p.m.), and Northeast Regional Meeting (Potsdam, NY, Friday, June 25, 9:00 a.m. - 12:00 p.m.). To prereg­ister, send your telephone number and home (voting) address to govtrela­tions@ acs .orq, or telephone Debbie Fillinich at (800) 227-5558 ext. 4476. Preregistering will enable OLGA staff to prepare individualized materials for workshop participants.

INDUSTRIAL SEMINAR Chemir/Polytech Laboratories is

offering a two-day seminar and labora­tory workshop on September 14-15, 1999. At their facilities in St. Louis, Mis­souri. This course covers spectroscopy, chromatography, microscopy and ther­mal analytical techniques for solving manufacturing problems. Additional fea­tures include case study discussion , laboratory demonstrations and individu­al consultation with Chemir/Polytech scientists. All registered attendees receive a ticket to the Cardinals base­ball game with the Milwaukee Brewers on September 14th. Contact Christina Pehlman, Chemir/Polytech Laboratories for information. Call (314) 291-6620 or e-mail cmpehlman@chemir.com.

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WILLARD GIBBS MEDAL AWARD PRESENTATION Friday, May 21,1999

PHARMACEUTICAL WEB SITE

There's no quicker way to explore what STN (R) has to offer the pharma­ceutical industry than by visiting : http://www.cas.org/PHARM/pharm.html You 'll discover that STN provides you with the information you need to:

• discover and develop new drugs and medical devices

• assess market potential and commer­cial opportunities

• maximize your patent portfolio and protect your patent rights

Topics you 'll want to investigate at the Web site include:

• discovering new chemical entities

• finding drug names

• locating toxicology data

• researching pharmacology and phar­macognosy

• searching for pharmaceutics

• patent watch

• monitoring worldwide drug develop­ments

For more information about CAS con­tact Customer Service at 800-753-4227 or send email to help@cas.org.

Please reserve the following number of tickets at $35, _ _ at $37, __

for the Gibbs Award Banquet on Friday, May 21

at Monastero's Ristorante in Chicago.

I enclose my check for $ __ for _ Steak

_ Salmon, or_ Eggplant dinner(s).

You and your guest(s) are cordially invited to attend the 88th presentation of the Josiah Willard Gibbs Medal to Dr. Lawrence F. Dahl of the University of Wisconsin on Friday, May 21, 1999 at Monastero's Ristorante, 3945 West Devon Avenue, Chicago, Illinois. Cocktail hour with hot hors d'oeuvres and cash bar from 6:00 to 7:00 pm; dinner at 7:00pm. NAME __________________________ _

For this special occasion, a gourmet dinner including Fettunta (special Sicilian bread), vegetable soup with barley, mixed green salad with ranch dressing, rigatoni with marinara sauce, choice of either Steak Palermitana, Salmon Genovese, or Eggplant Parmigiana, green beans with tomatoes and pearl onions, cannoli, coffe, tea red and white wine. The complete price will be $35 for ACS members with one guest, and $37 for nonmembers. Tables of ten can be reserved. If you wish to request seating for groups of three to seven at one table, please attach a notice with names to your ticket request form.

The Gibbs Award Dinner is always a memorable occasion. Only the Nobel Prize is considered more prestigious. Please come to salute and greet the recipient, Dr. Lawrence F. Dahl of the University of Wisconsin, and rejoice in his achievements in and contributions to the science of chemistry.

Walter Kramer, Chair Gibbs Arrangements Committee

AFFILIATION-----------------------

TELEPHONE ______________________ _ ADDRESS ________________________ __

CITY ______ STATE ____ ZIP

Orders received by Friday, May 14, 1999 will be filled by mail. There will be no refunds on charges or cancellations

made after Tuesday noon. May 18 or for no-shows. Please include a list of all the names in your party on an attached sheet of paper for name tags.

Please return this form to:

CHICAGO SECTION, AMERICAN CHEMICAL SOCIETY 7173 N. Austin Avenue, Niles, IL 60714

ACS FELLOWSHIPS The ACS Congressional Fellowship

program will place two ACS members in congressional offices for one year beginning in September 2000 to:

• ga in first-hand knowledge of the operation of the legislative branch;

• make scienti fic and technical exper­tise availab le to th e government; and

• forge links between the scientific and government communities. Applicat ions are du e January 3,

2000. The ACS is seeking applicants from among ACS members who range from the "seasoned" chemical profes­sional to the recent graduate with or without work experie ce. ACS provides a stipend and an allowa ce or reloca­tion expenses.

ACS also selects a Science Policy Fellow who works in the Headquarters Office of Legislative and Government Affairs, usually for two years. The Sci­ence Policy Fellowship offers a unique opportunity for a scientist to contribute to the Society's discussions and recom­mendations in areas of importance to the chemical community.

Contact the program office for appli­cation information: Congressional Fellowship program/ Science Policy Fellowship Program Office of Legislative and Government Affairs American Chemical Society 1155 16th Street, NW Washington, DC 20036 202/452-8917 E-mail: congfellow@acs.org Information on the Web: http://www.acs.org/govt

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DEADLINES FOR CHEMICAL BULLETIN

Please submit all Chemical Bulletin copy to the editor before the deadlines listed for each issue. Articles can be mailed or faxed to the editor: Fran Karen Kravitz, 28W230 Belleau Drive, Winfield, Illinois 60190. FAX: 630/293-4211.

Do not send your articles or any other correspondence for the Chemical Bulletin to the section office, as they will arrive to the editor late.

Articles must be typed, Font Size 14 or 16, DOUBLE SPACED, on 8.5" X 11 " paper, leaving an one inch margin on either side. Please put the author's name on the articles, together with a phone number in case we need to con­tact the author. Arti cles should be no longer than three DOUBLE SPACED pages. THE PREFERRED FORMAT IS TO SUBMIT ARTICLES ON 3.5" IBM FORMATTED DISK IN EITHER WORDPERFECT OR ASCII FILES. Articles submitted without author's name and phone number or withou t using the above publication requi re­ments will be rejected!

The Chemical Bulletin must be mailed about 20 days before the dinner meeting each month. We would like the Bulletin to be as timely as possible, but we need the lead time indicated. You can help by early planning and submis­sion of your data or articles.

ISSUE September 1999 · October 1999 November 1999 December 1999 January 2000 February 2000 Marach 2000 April2000 May - June 2000

DEADLINE 7/22/99 8/19/99 9/16/99 10/7/99 11/18/99 12/23/99 1/14/00 2/11/00 3/18/00

5

ACS NATIONAL MEETING

The ACS Council Meeting opened with Memorial Resolutions for deceased Councilors, including Hertsell Conway from Chicago. Later, a eulogy for Glenn Seaberg was read.

Of the four nominees for ACS Presi­dent F. Peter Boer, James Bristol, Attila Pavlath, and Alan Shriesheim the Council chose the latter two to be can­didates for the fall election . The Council also voted to:

1) extend the responsibilities of the Divisional Activities Committee on formation and dissolution of Divisions

2) exercise the dues escalator annual dues for 2000 will increase from $105 to $108

3) remove the dues reinstatement penalty for those rejoining the ACS

The Council received an explanation why the ACS Board raised the National Meeting Registration even though the Council voted against it. More detailed financial information was available and more will be made available for Council consideration in the future.

Other news about the meeting includes registered attendance of 10,517 and NECH news that more positions were advertised than candidates seeking positions. On Monday, the Symposium Commemorating the 1 OOth Anniversary of the Birth of Percy Julian was attended by a few hundred people. Even more attended the luncheon, which featured as speaker David Satcher, Surgeon General of the United States.

ROBERT E. BUNTROCK Councilor, Chicago Section

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